FAPAS PROGRAMME & PROFICIENCY TEST ORDER FORM … (2013-2014) v2 EN.… · fapas programme &...

FAPAS PROGRAMME & PROFICIENCY TEST ORDER FORM APRIL 2013 – MARCH 2014

FAPAS® 2013-14 (Contact Details, Declaration & Notes) – Rev: 20121207 of 2

Please read carefully all of the Notes given in this document. FAPAS cannot be held responsible for incorrectly completed order forms.

1. Please give contact details of the person placing this order: Contact Name: Company tel. no.:

Company Name: Company fax. no.:

Address: Company email:

VAT reg. no.:

City:

Postcode: Direct tel no.:

Country: Direct email:

Notes a) This address will be used for ALL correspondence.

b) Courier dispatches cannot be delivered to PO Box addresses.

c) If the address for invoicing is different, please give that separately.

d) See below for how to give contact name and email address for each test you order.

2. On the programme pages, please use a �� to indicate clearly the tests you have ordered.

Notes a) An index is provided to help you locate tests of interest to you.

b) Registrations for proficiency tests in the FAPAS® Programme will close 14 days before the start date of the test.

c) The dispatch date shown is our planned dispatch date. You will be notified by email if any of the tests you order are delayed for any reason. The majority of test close dates are 6-8 weeks after dispatch.

d) Indicate a contact name and email address for each test you order, otherwise the name given above will be used.

e) The approximate quantity of test material we will supply is given for each test. If your method needs more material please indicate the number of extra test materials you require. There is a charge for additional test materials.

f) The purchase of extra test materials does not entitle you to receive an extra performance assessment. You must place multiple orders for the test if you require this service.

g) Test materials are dispatched by normal post unless courier service is purchased EXCEPT for tests with code numbers marked ‘F’. These are dispatched by courier and incur courier charges.

3. Give a Purchase Order number and sign the declaration below: I apply to join the FAPAS® Programme on the basis of the Fera Standard Terms and Conditions for Proficiency Testing Schemes available at www.fapas.com.

Your Purchase Order Number:

Total no. of Proficiency Tests Ordered:

Signed: Date:

Notes a) We cannot accept unsigned order forms.

b) If you have not received confirmation of this order within 30 days of placing it please contact FAPAS.

c) Remittance should only be made on receipt of an invoice. Your invoice will contain our banking details and full information on how to pay.

d) The invoice will be issued shortly after your order is received. This means that you will be paying for some tests in advance.


FAPAS® 2013-14 (Contact Details, Declaration & Notes) – Rev: 20121207 of 2

4. Return the signed declaration and completed order form: Post: FAPAS®, The Food & Environment Research Agency, Sand Hutton, York, YO41 1LZ, UK

Fax: +44 1904 500440

email: [email protected]

Notes a) Keep a copy of your order form for your own records.

b) Please do not send duplicate copies of your form, e.g. if you send your order by fax, please do not also send it by post or email.

c) Alternatively, use this form as a guide and submit your order as a ‘wishlist’ via our website at www.fapas.com.

5. Additional notes: i. Dispatch

a) As indicated above, tests with code numbers marked ‘F’ are automatically dispatched by courier. This is to reduce the time taken in transit. Some packages include ice blocks to minimise large temperature fluctuations in transit but they are not transported in refrigerated vehicles. Even if your sample does not arrive refrigerated it is still acceptable for use, as it will have been chilled for the majority of its journey.

b) Please contact us if your postal dispatch has not arrived within 10 days or your courier dispatch has not arrived within 4 days.

c) FAPAS will send the Airway Bill Number of your courier consignment to the email address given for the sample contact and the delivery contact for that test. The message will include a link to the courier’s tracking system on their website.

d) Airway Bill Numbers are also available from the participant’s secure pages on the FAPAS® website.

e) It is the responsibility of a participant to monitor the progress of their courier dispatch.

ii. Import / Customs a) FAPAS is not responsible for damage or loss of test materials due to problems in customs or for import fees.

b) If you require special import permits for importing certain types of test material into your country please inform us at least 3 weeks prior to dispatch date. There is a charge for this service.

c) Phytosanitary certificates can be provided where appropriate. There is a charge for this service.

iii. Results a) Participants generally have 6 weeks to return results after a test material is dispatched. For some analyses a

shorter timescale is necessary due to the nature of the material/analyte. Such tests are indicated on the programme.

b) Result submission will only be allowed via the FAPAS® website.

iv. Reports a) The cost of the test includes access to an electronic copy of the report for the person placing the order and

designated sample contact.

b) Reports are normally available on our website within 30 days of the closing date of the test.

c) The reports are in PDF format and are secured by a digital signature. Adobe Reader version 7 or greater is required to open these files and verify the validity of the signature.


FAPAS® 2013-14 (Index) – Rev: 20121207 Page 1 of 2

Index 3-MCPD & 1,3 DCP .......................... 3

acesulfame-k .................................. 15

acidity ............................................. 16

acrylamide ........................................ 3

aflatoxin M1 .................................... 10

aflatoxins ........................................ 10

ALA ................................................ 16

alcoholic strength ........................... 15

allergens .......................................... 8

almond ............................................. 8

almond protein ................................. 8

aluminium ....................................... 14

animal (pork) fat ............................. 17

animal feed.............. 3, 6, 7, 10, 11, 12

anisidine value ............................... 16

anthelmintics ................................ 5, 6

antimony ........................................ 14

antioxidants .................................... 13

apple juice ................................ 11, 15

apple purée .............................. 11, 19

apricot (dried) ................................. 13

apricot purée .................................. 19

ARA ............................................... 16

arsenic ........................................... 14

arsenic, inorganic ........................... 14

ash ........................................... 1, 2, 7

aspartame ...................................... 15

avermectins .................................. 5, 6

baby food (powdered)..................... 13

barley flour ..................................... 11

beef .................................................. 4

benzoic acid ............................. 13, 15

beta-agonists ................................ 5, 6

beta-lactams ................................. 5, 6

biscuit (cookie) ................................. 1

biscuits ............................................. 3

bisphenol A ...................................... 9

BLG .................................................. 8

bovine milk ....................................... 6

bovine urine .................................. 5, 6

brandy ............................................ 15

Brazil nut ........................................ 10

breadcrumbs .................................... 1

breakfast cereal .................... 2, 12, 13

brilliant green .................................... 6

brix ........................................... 13, 15

broccoli purée ................................. 19

butter .......................................... 2, 17

butyric acid ................................. 2, 16

cabbage purée ................................. 4

cadmium ........................................ 14

caffeine .................................... 13, 15

cake mix ..................................... 8, 13

calcium ................................... 2, 7, 15

canned fish ............................. 2, 8, 14

canned meat ................................ 1, 2

canned meat meal ............................ 1

carbadox........................................... 6

casein ............................................... 8

celery ................................................ 8

cephalosporins ................................. 6

cereal ................................... 1, 10, 12

cheese .............................................. 2

chicken ............................................. 4

chicken egg ...................................... 5

chilli powder .............................. 10, 14

chilli powder (spice) ........................ 19

chilli sugar paste ............................. 14

chloramphenicol ........................... 5, 6

chloride ................................... 1, 2, 13

chlormequat .................................... 18

chocolate ...................................... 2, 8

chocolate cake mix ......................... 13

cholesterol ...................................... 16

chromium........................................ 14

citric acid .................................. 13, 15

coccidiostats ................................. 5, 6

cocoa ........................................ 11, 14

coffee (green) ................................. 11

coffee (ground) ............................... 15

coffee (instant) ................................ 11

coffee (roasted) .............................. 11

cola drink ........................................ 15

colours ............................................ 15

colours (non-permitted) ................... 13

colours (permitted) .......................... 13

condensed milk ................................. 2

copper .................................... 2, 7, 14

coriander (herb) purée .................... 19

corn/maize ........................................ 2

corned beef ...................................... 5

courgette (zucchini) purée .............. 19

crab meat ....................................... 14

cranberry juice ................................ 15

crispbread ......................................... 3

crude fibre ........................................ 7

crystal violet ...................................... 6

cucumber purée .............................. 19

cyanuric acid .................................... 3

cyclamate ....................................... 15

dairy ration ........................................ 7

deoxynivalenol (DON) ............... 10, 12

dextrose ........................................... 2

diastase ............................................ 3

dietary fibre ....................................... 1

dihydrostreptomycin.......................... 6

edible oil ......................................... 14

egg ................................................... 8

egg white protein .............................. 8

ELISA ............................................... 8

equine kidney ................................... 6

ergot alkaloids ................................ 12

esters of 3-MCPD ............................. 3

ethanal (acetaldehyde) ................... 15

ethephon ......................................... 19

ethyl acetate ................................... 15

ethyl carbamate .............................. 15

fatty acids ....................................... 16

figs (dried) ....................................... 10

fish .................. 2, 4, 5, 6, 8, 14, 16, 17

fish (oily) ..................................... 5, 17

fish identification ............................... 4

fish muscle .................................... 5, 6

fish oil ............................................. 16

fish paste .......................................... 2

food simulant .................................... 9

formaldehyde .................................... 9

fructose ................................... 2, 3, 15

fruit juice ............................. 11, 14, 15

fruit purée ........................... 11, 13, 19

fumonisins ................................ 10, 12

galactose .......................................... 2

glucose ................................... 2, 3, 15

gluten ................................................ 8

glyphosate ................................ 18, 19

grapefruit ........................................ 14

grapefruit juice ................................ 15

green bean (inc pods) purée ........... 19

higher alcohols (sum) ...................... 15

histamine .......................................... 8

honey ........................................ 3, 5, 6

hot pepper sauce ............................ 13

hydrogenated vegetable oil ............. 17

hydrolysed vegetable protein ............ 3

hydroxymethylfurfural (HMF) ............. 3

hydroxyproline .................................. 1

illegal dyes ...................................... 13

infant cereal .................................... 14

infant food ........................... 10, 12, 18

infant formula ........................ 2, 14, 16

infant soya formula ............................ 8

iodine .................................... 2, 14, 16

iodine value .................................... 16

iron ......................................... 2, 7, 14

jam .............................................. 8, 13

k232 & k270 .................................... 16

lactose .............................................. 2

lamb .................................................. 4

LC-PUFAs ...................................... 16

lead ............................................. 7, 14

lemon purée .................................... 19

lettuce purée ............................... 4, 19

leucocrystal violet.............................. 6

leucomalachite green .................... 5, 6

linoleic acid ..................................... 16

macrolides .................................... 5, 6

magnesium ............................. 2, 7, 15

maize .............................................. 10

maize flour .......................... 11, 12, 18

maltose ............................................. 2

manganese ................................... 2, 7


FAPAS® 2013-14 (Index) – Rev: 20121207 Page 2 of 2

meat ........................................... 4, 13

melamine ..................................... 3, 9

mepiquat ........................................ 18

mercury .......................................... 14

mercury, methyl .............................. 14

metallic contaminants ..................... 14

methanol ........................................ 15

methylbutanol ................................. 15

migration (overall) ............................. 9

migration (specific) ........................... 9

milk .................................................. 8

milk (BLG) ........................................ 8

milk (casein) ..................................... 8

milk powder ....... 2, 3, 4, 10, 13, 14, 17

milkshake powder ............................. 2

mixed fat spread ............................. 16

moisture ............................... 1, 2, 3, 7

molybdenum ................................... 14

mushroom powder ............................ 3

mustard ............................................ 8

nitrate ............................................... 4

nitrite ................................................ 4

nitrofuran metabolites ................... 5, 6

nitrogen ........................................ 1, 2

nitroimidazoles ................................. 5

non-fat solids .................................... 2

NSAIDs ........................................ 5, 6

NSP fibre .......................................... 1

nut contamination ............................. 8

nutmeg ........................................... 10

nutritional supplement ...................... 2

nutritionally fortified oil .................... 16

nylon film .......................................... 9

oat flour .......................................... 12

oats ............................................ 8, 18

ochratoxin A (OTA) ................... 10, 11

offal (liver) ...................................... 14

oil ............................................... 9, 13

oils & fats ....................................... 16

olive oil ..............................7, 9, 16, 17

omega-3 & omega-6 ....................... 16

orange juice .................................... 15

orange purée .................................. 19

PAHs ................................................ 7

PAHs (EU priority) ............................ 7

palm oil ............................................. 7

palm oil (refined)............................... 3

paprika ..................................... 10, 11

patulin ............................................ 11

peanut ........................................ 8, 10

peanut protein................................... 8

pear purée ...................................... 19

penicillins .......................................... 6

peroxide value ................................ 16

pesticide residues ....17, 18, 19, 20, 21

pH .................................. 2, 13, 14, 15

phosphoric acid (as P2O5) ............... 15

phosphorus ............................. 2, 7, 15

photo initiators .................................. 9

phthlates ........................................... 9

pig kidney ......................................... 6

pig liver ......................................... 5, 6

pig muscle ........................................ 6

pig ration........................................... 7

pistachio (water/nut slurry) .............. 10

plastic film ......................................... 9

pork .................................................. 4

porridge oats .................................... 1

potassium ................................... 2, 15

potato purée ................................... 19

poultry ration ..................................... 7

prawns .............................................. 6

premix .............................................. 7

processed food ................................. 4

protein .......................................... 1, 7

quinine ............................................ 15

quinolones & fluoroquinolones ...... 5, 6

red grape purée .............................. 19

rice ................................................. 10

rice (brown) .................................... 18

rice (powdered) ............................... 14

rye flour .......................................... 12

saccharin ........................................ 15

salt ................................................... 1

saturated FAs ............................. 1, 16

selenium ................................. 2, 7, 14

sesame oil ...................................... 17

sheep feed ........................................ 7

smoked meat .................................... 7

snack food ........................................ 2

sodium .......................... 1, 2, 7, 13, 15

soft drink ................................... 14, 15

sorbic acid ................................ 13, 15

soup powder (instant) ....................... 8

soy sauce ......................................... 3

soya.................................................. 8

soya bean purée ............................. 19

soya flour ........................................ 14

soya protein ...................................... 8

spinach purée ................................... 4

starch ............................................ 1, 7

strawberry purée ............................. 19

sucrose ............................. 2, 3, 13, 15

sugar confectionary ......................... 13

sulfonamides................................. 5, 6

sulphites ........................................... 8

sulphur dioxide ................................ 13

synthetic hormones ....................... 5, 6

T-2 & HT-2 toxins ...................... 10, 12

tea (green) ...................................... 19

tetracyclines .................................. 5, 6

theobromine .................................... 13

thiamphenicol .................................... 5

thyrostats ...................................... 5, 6

tin.................................................... 14

titratable acidity ................................. 2

tomato paste ................................... 14

tomato purée................................... 19

tomato sauce .................................. 13

tonic water ...................................... 15

total acidity ................................ 13, 15

total dietary fibre ............................... 1

total fat .................................... 1, 2, 16

total folate ....................................... 13

total malachite green ..................... 5, 6

total niacin ...................................... 13

total oil .............................................. 7

total primary aromatic amines ........... 9

total SO2 ......................................... 15

total sugars ................... 1, 2, 7, 13, 15

total volatile basic nitrogen (TVB-N) .. 2

tranquilizers ...................................... 6

trans fatty acids ............................... 16

tricothecenes .................................. 12

unsaturated FAs, mono ................... 16

unsaturated FAs, poly ..................... 16

vegetable oil.................................... 16

vegetable purée .............................. 14

veterinary drug residues ................ 5, 6

vine fruit (dried) ......................... 11, 19

vitamin supplement (liquid) ............. 13

vitamins ...................................... 7, 13

volatile acidity ................................. 15

wheat flour .................. 1, 8, 11, 12, 18

whisky ............................................. 15

wine .................................... 11, 14, 15

zearalenone (ZON) ................... 10, 12

zinc ......................................... 2, 7, 14


FAPAS® 2013-14 (Programme) – Rev: 20121207 Page 1 of 21

Please read carefully all of the NOTES given in this document. FAPAS cannot be held responsible for any incorrectly completed order forms.

Notes a) Please indicate, with a ��, against the tests you wish to order.

b) Only give a sample contact name and email if different to that given on the front sheet.

c) Purchase extra test materials only if the approx. quantity given is insufficient for your method, not to participate more than once. Place multiple orders for the test for that service.

Nutritional Components dispatch

date test details place order

dd/mm/yyyy code matrix analyte approx. quantity

�� sample contact name & email

extra TMs

18/04/2013 0185 canned meat moisture, ash, total fat, nitrogen, sodium & chloride

150 g

19/06/2013 0186 canned meat meal

moisture, ash, total fat, nitrogen, sodium & chloride

150 g

17/07/2013 0187 canned meat moisture, ash, total fat, nitrogen & hydroxyproline 150 g


total fat, saturated fatty acids, protein, total sugars, dietary fibre� & salt

150 g

20/11/2013 0189 canned meat moisture, ash, total fat, nitrogen & hydroxyproline 150 g


moisture, ash, total fat, nitrogen, sodium, chloride & total sugars

150 g

12/02/2014 0191 canned meat moisture, ash, total fat, nitrogen, sodium & chloride

150 g

27/03/2014 0192 canned cured meat


150 g

30/04/2013 2451 wheat flour moisture at 130°C, ash, nitrogen & total dietary fibre by AOAC

150 g

27/06/2013 2452 porridge oats moisture at 130°C, ash, total fat, nitrogen, total dietary fibre by AOAC &

NSP fibre by Englyst

150 g

26/09/2013 2453 cereal moisture at 130oC, ash, nitrogen & total dietary fibre by AOAC

150 g

16/01/2014 2454 breadcrumbs moisture, ash, nitrogen, starch, sodium & total dietary fibre by AOAC

150 g

05/03/2014 2455 biscuit (cookie) moisture at 130 oC, ash, total fat, nitrogen & total dietary fibre by AOAC

150 g

Footnotes � as defined by Codex total sugars = that measured by a defined titration method (e.g. Layne-Eynon, Luff-Schoorl, Munson Walker) or, if measured by HPLC, the sum of fructose, glucose, sucrose, lactose, galactose and maltose (NB not all sugars may be present)

/continued



Nutritional Components (continued) dispatch




extra TMs

03/04/2013 25108 corn/maize snack food


50 g

29/05/2013 25109 fish paste moisture, ash, total fat, nitrogen, sodium & chloride

150 g

21/06/2013 25110 canned fish total volatile basic nitrogen (TVB-N) 150 g

01/08/2013 25111 condensed milk moisture, ash, total fat, nitrogen & total sugars 150 mL

20/09/2013 25112 milkshake powder

fructose, glucose, sucrose, lactose, galactose, maltose & dextrose

50 g

22/10/2013 25113F chocolate moisture, total fat, nitrogen, butyric acid, lactose & sucrose

150 g

13/12/2013 25114 milk powder moisture, ash, total fat, nitrogen, titratable acidity & lactose

50 g

22/01/2014 25115 infant formula moisture, ash, total fat, nitrogen & lactose 50 g

13/02/2014 25116 cheese & pasta meal


100 g

25/02/2014 25117 F butter moisture, total fat, non-fat solids, pH & chloride 200 g

21/03/2014 25118 canned fish total volatile basic nitrogen (TVB-N) 150 g

Nutritional Elements

dispatch date

test details place order



extra TMs

19/04/2013 1871 canned meat calcium, phosphorus & zinc (all natural levels) 150 g

15/08/2013 1872 breakfast cereal calcium, iron, magnesium, phosphorus, potassium, sodium, & zinc (fortified)

50 g

21/11/2013 1873 milk powder calcium, magnesium, phosphorus, potassium, iodine selenium & sodium (all natural levels)

50 g

18/02/2014 1874 F nutritional supplement

copper, manganese, magnesium, potassium & zinc (fortified)

30 mL

Footnotes F test incurs courier charges



Acrylamide / Melamine / 3-MCPD dispatch




extra TMs

10/04/2013 3039 milk powder melamine & cyanuric acid (> 5mg/kg) 50 g

23/05/2013 3040 crispbread acrylamide 50 g

26/06/2013 3041 mushroom powder

melamine & cyanuric acid (low levels, <5 mg/kg)

50 g

08/08/2013 3042 potato crisps acrylamide 50 g

16/10/2013 3043 animal feed melamine & cyanuric acid

50 g

27/11/2013 3044 biscuits acrylamide 50 g

07/03/2014 3045 milk powder melamine & cyanuric acid (low levels, <5 mg/kg) 50 g

29/05/2013 2637 soy sauce 3-MCPD & 1,3 DCP 40 g

27/09/2013 2638 refined palm oil esters of 3-MCPD 50 mL

10/01/2014 2639 hydrolysed vegetable protein

3-MCPD & 1,3 DCP 40 g

14/03/2014 2640 soy sauce 3-MCPD & 1,3 DCP 40 g

Honey dispatch




extra TMs

29/07/2013 2826F honey moisture, fructose, glucose, sucrose, hydroxymethylfurfural (HMF) & diastase

100 g

28/01/2014 2827F honeya fructose, glucose, sucrose, hydroxymethylfurfural (HMF) & diastase

100 g

Footnotes F test incurs courier charges a this test material may be adulterated honey



Authenticity dispatch




extra TMs

10/04/2013 2950D chicken adulteration/contamination (presence/absence) of matrix with one or more from: beef, lamb or pork

30 g

07/05/2013 2951F processed food adulteration/contamination (presence/absence) of matrix (2 samples) with pork

2 x 30 g

18/07/2013 2952D lamb adulteration/contamination (presence/absence) of matrix with one or more from: beef, chicken or pork

30 g

17/09/2013 2953F fish identification of unknown fish (3 samples) selected from the following list:

Gadus morhua, (Linnaeus 1758) Limanda limanda, (Linnaeus 1758)

Melanogrammus aeglefinus, (Linnaeus 1758) Merluccius merluccius, (Linnaeus 1758)

Hippoglossus hippoglossus, (Linnaeus 1758) Pleuronectes platessa, (Linnaeus 1758)

Pollachius virens, (Linnaeus 1758) Merlangius merlangus, (Linnaeus 1758)

3 x 10 g

09/12/2013 2954F processed food adulteration/contamination (presence/absence) of matrix (2 samples) with pork

2 x 30 g

12/02/2014 2955D beef adulteration/contamination (presence/absence) of matrix with one or more from: chicken, lamb or pork

30 g

Nitrate & Nitrite dispatch




extra TMs

04/04/2013 1588 DDφ meat nitrate as NaNO3 & nitrite NaNO2 25 g

30/05/2013 1589φ milk powder nitrate as NaNO3 & nitrite NaNO2 (low level) 40 g

30/07/2013 1590F cabbage purée nitrate 70 g

03/09/2013 1591F lettuce purée nitrate 70 g


04/02/2014 1593F spinach purée nitrate 70 g


Footnotes D freeze dried matrix, to be reconstituted (by participants) prior to testing F test incurs courier charges DD freeze dried matrix, not to be reconstituted (by participants) prior to testing φ test has a shortened timescale



Veterinary Drug Residues We intend to use material containing incurred residues wherever possible.

Refer to the list below this table for details of potential residues in tests where only general categories are stated.

dispatch date




extra TMs

02/04/2013 02206Fφ# chicken eggs nitrofuran metabolites 20 g

23/04/2013 02207Fφ fish muscle (oily fish)

leucomalachite green & total malachite green 20 g

20/05/2013 02208F# honey tetracyclines 20 g

20/05/2013 02209Fφ# fish muscle quinolones & fluoroquinolones 20 g

04/06/2013 02210Fφ# bovine urine thyrostats 25 mL

25/06/2013 02211F honey chloramphenicol 20 g

22/07/2013 02212Fφ# corned beef avermectins 20 g

22/07/2013 02213Fφ# pig liver β-agonists

20 g

19/08/2013 02214F# honey sulfonamides 20 g

19/08/2013 02215Fφ# chicken eggs coccidiostats 20 g

11/09/2013 02216 bovine milk powder

chloramphenicol & thiamphenicol 20 g

24/09/2013 02217Fφ# chicken eggs nitroimidazoles 20 g

Footnotes F test incurs courier charges # test includes identification and quantification of analytes, see List A, below φ test has a shortened timescale

Potential veterinary drug residues in tests where only general categories are stated – List A. tetracyclines chlortetracycline (total), doxycycline, oxytetracycline (total), tetracycline (total)

nitrofuran metabolites AHD (bound), AHD (total), AOZ (bound), AOZ (total), AMOZ (bound), AMOZ (total), SEM (bound), SEM (total)

sulfonamides sulfachloropyridazine, sulfadiazine, sulfadimethoxine, sulfadimidine (sulfamethazine), sulfadoxine, sulfaguanadine, sulfamerazine, sulfamethizole, sulfamethoxazole, sulfamethoxypyridazine, sulfamonomethoxine, sulfamoxole, sulfanilamide, sulfapyridine, sulfaquinoxaline, sulfathiazole, sulfisoxazole

quinolones & fluoroquinolones flumequine, nalidixic acid, oxolinic acid, ciprofloxacin, danofloxacin, difloxacin, enrofloxacin, marbofloxacin, norfloxacin, sarafloxacin

avermectins abamectin, doramectin, emamectin, eprinomectin, ivermectin, moxidectin

β-agonists bromobuterol, cimaterol, cimbuterol, clenbuterol, clenpenterol , clenproperol, hydroxyclenbuterol, mabuterol, mapenterol, ractopamine, salbutamol, salmeterol, terbutaline, tulobuterol, zilpaterol

synthetic hormones α-boldenone, methylboldenone, diethylstilbestrol (DES), dienestrol, hexoestrol, methyltestosterone, α-nortestosterone, stanozolol, 16β-hydroxystanozolol, trenbolone, zeranol

nonsteroidal anti- inflammatory drugs (NSAIDs)

diclofenac, 5-hydroxyflunixin, ibuprofen, meloxicam, naproxen, phenylbutazone

coccidiostats clopidol, decoquinate,diclazuril, halofuginone, lasalocid, maduramycin, monensin, narasin, DNC, robenidine, salinomycin, semduramycin, toltrazuril sulfone

anthelmintics albendazole sulfone, albendazole-2-amino-sulfone, albendazole sulfoxide, total albendazole sulfone, closantel, fenbantel, fenbendazole, oxfendazole, oxfendazole sulfone, total oxfendazole sulfone, flubendazole, levamisole, mebendazole, hydroxymebendazole, mebendazole amine, total mebendazole, nitroxynil, thiabendazole, triclabendazole, triclabendazole sulfone, triclalbendazole sulfoxide, ketotriclabendazole, total triclabendazole sulfone

thyrostats 6-methyl-2-thiouracil (methylthiouracil), dimethylthiouracil, ethylthiouracil, methimazole (Tapazole), mercaptobenzimidazole, thiouracil, phenylthiouracil, propylthiouracil

beta-lactams amoxicillin , ampicillin , benzylpenicillin (Penicillin G), Penicillin V, cloxacillin, dicloxacillin, nafpicillin , oxacillin, cefalexin, cefalonium, cefapirin, desacetylcefapirin, cefazolin, cefoperazone, cefquinome

macrolides erythromycin, josamycin, lincomycin, oleandamycin, rifampicin, spiramycin, tilmicosin, tylosin A, tylosin B, virginiamycin

nitroimidazoles dimetridazole, 2-hydroxydimetridazole, ipronidazole, 2-hydroxyipronidazole, metronidazole, 2-hydroxymetronidazole, ronidazole

/continued



Veterinary Drug Residues (continued) We intend to use material containing incurred residues wherever possible.

Refer to the list below this table for details of potential residues in tests where only general categories are stated.

dispatch date




extra TMs

15/10/2013 02218 Fφ# fish muscle leucomalachite green & total malachite green, crystal violet, leucocrystal violet & brilliant green

20 g

29/10/2013 02219 Fφ# equine kidney NSAIDs (nonsteroidal anti-inflammatory drugs)

20 g

11/11/2013 02220 Fφ# bovine urine synthetic hormones 25 mL

19/11/2013 02221F# honey quinolones & fluoroquinolones & macrolides 20 g

19/11/2013 02222Fφ# bovine milk anthelmintics & dihydrostreptomycin 50 mL

10/12/2013 02223Fφ# pig muscle tranquilizers 20 g

10/12/2013 02224Fφ pig liver carbadox 20 g

13/01/2014 02225Fφ# bovine milk beta-lactams (penicillins & cephalosporins) 25 mL

06/02/2014 02226# animal feed coccidiostats (medicinal concentrations) 50 g

17/02/2014 02227Fφ# pig kidney sulfonamides 20 g

17/02/2014 02228Fφ# pig kidney tetracyclines 20 g

17/03/2014 02229Fφ# prawns nitrofuran metabolites 20 g

17/03/2014 02230 Fφ prawns chloramphenicol 20 g

Footnotes F test incurs courier charges # test includes identification and quantification of analytes, see List A, below φ test has a shortened timescale

Potential veterinary drug residues in tests where only general categories are stated – List A. tetracyclines chlortetracycline (total), doxycycline, oxytetracycline (total), tetracycline (total)

nitrofuran metabolites AHD (bound), AHD (total), AOZ (bound), AOZ (total), AMOZ (bound), AMOZ (total), SEM (bound), SEM (total)

sulfonamides sulfachloropyridazine, sulfadiazine, sulfadimethoxine, sulfadimidine (sulfamethazine), sulfadoxine, sulfaguanadine, sulfamerazine, sulfamethizole, sulfamethoxazole, sulfamethoxypyridazine, sulfamonomethoxine, sulfamoxole, sulfanilamide, sulfapyridine, sulfaquinoxaline, sulfathiazole, sulfisoxazole

quinolones & fluoroquinolones flumequine, nalidixic acid, oxolinic acid, ciprofloxacin, danofloxacin, difloxacin, enrofloxacin, marbofloxacin, norfloxacin, sarafloxacin

avermectins abamectin, doramectin, emamectin, eprinomectin, ivermectin, moxidectin

β-agonists bromobuterol, cimaterol, cimbuterol, clenbuterol, clenpenterol , clenproperol, hydroxyclenbuterol, mabuterol, mapenterol, ractopamine, salbutamol, salmeterol, terbutaline, tulobuterol, zilpaterol

synthetic hormones α-boldenone, methylboldenone, diethylstilbestrol (DES), dienestrol, hexoestrol, methyltestosterone, α-nortestosterone, stanozolol, 16β-hydroxystanozolol, trenbolone, zeranol

nonsteroidal anti- inflammatory drugs (NSAIDs)

diclofenac, 5-hydroxyflunixin, ibuprofen, meloxicam, naproxen, phenylbutazone

coccidiostats clopidol, decoquinate,diclazuril, halofuginone, lasalocid, maduramycin, monensin, narasin, DNC, robenidine, salinomycin, semduramycin, toltrazuril sulfone

anthelmintics albendazole sulfone, albendazole-2-amino-sulfone, albendazole sulfoxide, total albendazole sulfone, closantel, fenbantel, fenbendazole, oxfendazole, oxfendazole sulfone, total oxfendazole sulfone, flubendazole, levamisole, mebendazole, hydroxymebendazole, mebendazole amine, total mebendazole, nitroxynil, thiabendazole, triclabendazole, triclabendazole sulfone, triclalbendazole sulfoxide, ketotriclabendazole, total triclabendazole sulfone

thyrostats 6-methyl-2-thiouracil (methylthiouracil), dimethylthiouracil, ethylthiouracil, methimazole (Tapazole), mercaptobenzimidazole, thiouracil, phenylthiouracil, propylthiouracil

beta-lactams amoxicillin, ampicillin, benzylpenicillin (Penicillin G), Penicillin V, cloxacillin, dicloxacillin, nafpicillin, oxacillin, cefalexin, cefalonium, cefapirin, desacetylcefapirin, cefazolin cefoperazone, cefquinome

macrolides erythromycin, josamycin, lincomycin, oleandamycin, rifampicin, spiramycin, tilmicosin, tylosin A, tylosin B, virginiamycin

tranquilizers acepromazine, azaperol, azaperone, carazolol, chlorpromazine hydrochloride, haloperidol, propionylpromazine hydrochloride, xylazine



Feeding Stuffs Please note that there are further proficiency tests in the Programme with animal feed as the matrix: 02226, 04219, 04226, 04229, 17131, 2299, 22100, 22102 & 3043.

dispatch date




extra TMs

24/05/2013 10109 dairy ration moisture, ash, total oil, protein & crude fibre 150 g

24/05/2013 10110 dairy ration iron, lead, magnesium, manganese & selenium 150 g

27/06/2013 10111 sheep feed moisture, ash, total oil, protein & copper 150 g

19/09/2013 10112 pig ration moisture, ash, total oil, protein, crude fibre, vitamin E & zinc

150 g

06/12/2013 10113 poultry ration moisture, ash, total oil, protein & crude fibre 150 g

06/12/2013 10114 poultry ration starch, total sugars, calcium & phosphorus 150 g

26/02/2014 10115 premix calcium, manganese, magnesium, phosphorus, sodium & zinc

150 g

26/02/2014 10116 premix vitamin A, D3 & E 150 g

Environmental Contaminants dispatch




extra TMs

19/04/2013 0654 palm oil PAHs 30 mL

01/10/2013 0655F smoked meat product

PAHs 50 g

29/01/2014 0656 olive oil all 16 EU priority PAHs 30 mL




Allergens EXCEPT for histamine & sulphites tests (which are designed primarily for HPLC based methods), results will be grouped and assessed according to the brand of ELISA kit used. Thus limited data may preclude assessment of small categories.

dispatch date




extra TMs

03/04/2013 27118§ infant soya formula

milk (casein) 2 x 20 g

25/04/2013 27119§ cake mix egg, egg white protein 2 x 20 g

15/05/2013 27120 canned fish histamine (high level) 145 g


gluten 2 x 20 g

28/06/2013 27122‡ instant soup powder

celery, mustard 1 x 20 g

26/07/2013 27123§ chocolate peanut, peanut protein 2 x 20 g


milk (BLG) 2 x 20 g

28/08/2013 27125§ cake mix gluten 2 x 20 g

12/09/2013 27126 canned fish histamine (low level) 145 g

02/10/2013 27127§ chocolate hazelnut, hazelnut protein 2 x 20 g

28/10/2013 27128F jam sulphites 20 g

15/11/2013 27129‡ cake mix gluten, milk and egg 30 g

05/12/2013 27130§ wheat flour soya, soya protein 2 x 20 g

08/01/2014 27131♦ chocolate contamination (presence/absence) of matrix with one or more from the following list:

Almond, (Amygdalus communis L.) Hazelnut, (Corylus avellana)

Walnut, (Juglans regia) Cashew, (Anacardium occidentale)

Pecan nut, (Carya illinoiesis (Wangenh.) K. Koch)) Brazil nut, (Bertholletia excelsa)

Pistachio nut, (Pistacia vera) Macadamia / Queensland nut (Macadamia ternifolia)

50 g

30/01/2014 27132 canned fish histamine (high level) 145 g

19/02/2014 27133§ oat based foodstuff

gluten 2 x 20 g

19/03/2014 27134§ chocolate almond, almond protein 2 x 20 g

Footnotes § two test materials supplied and both qualitative & quantitative results can be submitted ‡ both qualitative & quantitative results can be submitted ♦ qualitative assessment only F test incurs courier charges



Migration – Overall & Specific dispatch




extra TMs

02/05/2013 1146 nylon film overall migration into ethanol by total immersion 40 cm x 22 cm

30/10/2013 1147 plastic film overall migration into olive oil by total immersion 40 cm x 22 cm

17/04/2013 1256B food simulant (oil)

phthalates 2 x 50 mL

17/07/2013 1257 food simulant (3% w/v acetic acid

in water)

melamine 50 mL

20/08/2013 1258 food simulant (50% w/v ethanol)

bisphenol A 50 mL


in water)

formaldehyde 50 mL


in water)

total primary aromatic amines >300 mL

07/03/2014 1261B food simulant (oil)

photo initiators 2 x 50 mL

Footnotes B includes blank matrix



Mycotoxins – Aflatoxins dispatch




extra TMs

11/04/2013 04214 maize aflatoxin B1, DON, ZON & OTA 150 g

23/04/2013 04215F pistachio (water/nut slurry)

aflatoxins B & G &/or total 100 g

09/05/2013 04216 maize aflatoxins B & G &/or total 55 g

15/05/2013 04217 milk powder aflatoxin M1 55 g

06/06/2013 04218 chilli powder aflatoxins B & G &/or total 55 g

20/06/2013 04219 animal feed (cereal based)


04/07/2013 04220 peanut aflatoxins B & G &/or total 55 g

25/07/2013 04221 infant food contamination of matrix with one or more from the following list: aflatoxins B & G &/or total, OTA, ZON,

DON, FB1 & FB2 & total fumonisins (as a sum of FB1 & FB2)

150 g

05/08/2013 04222F Brazil nut (water/nut slurry)


23/08/2013 04223 maize aflatoxin B1, DON, ZON, OTA, FB1 & FB2 & total fumonisins (as a sum of FB1 & FB2), T-2 & HT-2

toxins & as sum of T-2 & HT-2 toxins

150 g


23/09/2013 04225F hazelnut (water/nut slurry)



contamination of matrix with one or more from the following list: aflatoxin B1, OTA, ZON, DON, FB1 & FB2 & total fumonisins (as a sum of FB1 & FB2)

150 g

24/10/2013 04227 maize aflatoxins B & G &/or total 55 g

06/11/2013 04228 nutmeg aflatoxins B & G &/or total 55 g



11/12/2013 04230 maize aflatoxin B1, DON, ZON & OTA 150 g

06/01/2014 04231F pistachio (water/nut slurry)


22/01/2014 04232 rice aflatoxins B & G &/or total 55 g

29/01/2014 04233 peanut aflatoxins B & G &/or total 55 g

06/02/2014 04234 paprika aflatoxins B & G &/or total & OTA 150 g

04/03/2014 04235F dried figs (water/fruit slurry)




/continued



Mycotoxins (continued) – Patulin dispatch




extra TMs

01/07/2013 1650F apple juice (clear)

patulin 50 mL

16/09/2013 1651F apple purée patulin 60 g

18/02/2014 1652F apple juice (cloudy)

patulin 50 mL

Mycotoxins – Ochratoxin A Please note that there are further proficiency tests in the Programme that may contain OTA in Series 04.

dispatch date




extra TMs

02/05/2013 17122 wheat flour ochratoxin A 55 g

03/06/2013 17123F dried vine fruit (water/fruit slurry)

ochratoxin A 100 g

10/07/2013 17124 barley flour ochratoxin A 55 g

14/08/2013 17125 green coffee ochratoxin A 55 g

18/09/2013 17126 paprika ochratoxin A 55 g

30/10/2013 17127 instant coffee ochratoxin A 55 g

11/12/2013 17128 wine ochratoxin A 55 mL

10/01/2014 17129 maize flour ochratoxin A 55 g

07/02/2014 17130 roasted coffee ochratoxin A 55 g

27/02/2014 17131 animal feed ochratoxin A 55 g

26/03/2014 17132 cocoa ochratoxin A 55 g


/continued



Mycotoxins (continued) – Fusarium toxins Please note that there are further proficiency tests in the Programme that may contain fusarium toxins: 04214, 04221, 04223, 04226 & 04230.

dispatch date




extra TMs

12/04/2013 2292 maize flour deoxynivalenol (DON) 55 g

12/04/2013 2293 infant food deoxynivalenol (DON) 55 g

05/06/2013 2294 breakfast cereal zearalenone (ZON) 55 g

05/06/2013 2295 breakfast cereal deoxynivalenol (DON) 55 g

18/07/2013 2296 oat flour T-2 & HT-2 toxins & as a sum of T-2 & HT-2 toxins 55 g

29/08/2013 2297 maize flour FB1 & FB2 and total fumonisins (as a sum of FB1 & FB2)

55 g

09/10/2013 2298 maize flour tricothecenes: nivalenol, DON, 3 Ac DON, 15 Ac DON, T-2 & HT-2

toxins & as a sum of T-2 & HT-2 toxins

150 g

13/11/2013 2299 animal feed zearalenone (ZON) 55 g

13/11/2013 22100 animal feed deoxynivalenol (DON) 55 g

15/01/2014 22101 wheat flour deoxynivalenol (DON) 55 g

14/02/2014 22102 animal feed T-2 & HT-2 toxins & as a sum of T-2 & HT-2 toxins 55 g

12/03/2014 22103 rye flour ergot alkaloids: contamination of matrix with one or more from

ergometrine, ergotamine, ergosine, ergocristine, ergocryptine & ergocornine & their related -inines

55 g



Vitamins dispatch




extra TMs

22/05/2013 2181 breakfast cereal vitamins B1, B2 (total) & B6, total niacin & total folate

50 g

19/07/2013 2182φ fruit purée vitamin C 100 mL

05/11/2013 2183F liquid vitamin supplement

vitamins B1, B2 (total) & B6 40 mL

17/01/2014 2184 milk powder vitamins A & D3 50 g

14/03/2014 2185 powdered baby food

vitamins A, B12, C & E 50 g

Food Ingredients dispatch




extra TMs

17/04/2013 2099 tomato sauce brix, pH, total acidity, sodium & chloride 150 g

07/05/2013 20100F meat sulphur dioxide 100 g

12/06/2013 20101 jam brix, pH, benzoic acid, citric acid & sorbic acid 70 g

02/08/2013 20102 chocolate cake mix

caffeine, sorbic acid, theobromine & total sugars (expressed as sucrose)

50 g

27/08/2013 20103F dried apricot (water/fruit slurry)

sulphur dioxide 100 g

23/10/2013 20104§ sugar confectionary (boiled sweets)

permitted colours up to 4 selected from the following list:

Allura Red, Brilliant Blue FCF, Carmoisine, Erythrosine, Green S, Indigo Carmine,

Patent Blue V, Ponceau 4R, Quinoline Yellow, Sunset Yellow FCF, Tartrazine

50 g

27/11/2013 20105 oil antioxidants: total BHA (E320), BHT (E321) & propyl gallate (E310)

50 mL

06/03/2014 20106§ hot pepper sauce (or similar)

non-permitted colours (illegal dyes) up to 4 selected from the following list:

Butter Yellow (Dimethyl Yellow), Orange II, Para Red, Rhodamine B, Sudan I, Sudan II,

Sudan III, Sudan IV, Sudan Black B, Sudan Orange G, Sudan Red B, Sudan Red 7B,

Sudan Red G, Toluidine Red

50 mL

Footnotes total sugars = that measured by a defined titration method (e.g. Layne-Eynon, Luff-Schoorl, Munson Walker) or, if measured by HPLC, the sum of fructose, glucose, sucrose, lactose, galactose and maltose (NB not all sugars may be present) F test incurs courier charges φ test has a short timescale § both qualitative & quantitative results can be submitted



Metallic Contaminants dispatch




extra TMs

04/04/2013 07190 milk powder arsenic (total), cadmium, mercury (total) & lead (all natural / low levels)

50 g

24/04/2013 07191 soft drink antimony, arsenic (total) cadmium, chromium copper & zinc (all high levels)

50 mL

16/05/2013 07192 canned crab meat

arsenic (total), arsenic (inorganic), cadmium, lead & mercury (total) (all natural levels)

150 g

04/06/2013 07193F tomato paste cadmium, lead, iron & tin (all high levels)

50 g

03/07/2013 07194 canned fish arsenic (total), cadmium & mercury (total) (all natural levels)

150 g

24/07/2013 07195 infant formula aluminium, chromium, molybdenum, selenium & iodine (all natural / low levels)

50 g

07/08/2013 07196 chilli powder arsenic (total), cadmium & lead (all high levels)

50 g

21/08/2013 07197 chilli sugar paste lead 25 g

04/09/2013 07198 edible oil arsenic (total), copper, iron & lead (all high levels)

50 mL

25/09/2013 07199DD offal (liver) arsenic (total), mercury (total), lead & cadmium (all high levels)

50 g

11/10/2013 07200 wine pH, cadmium, lead & copper 50 mL

31/10/2013 07201 milk powder arsenic (total), cadmium, mercury (total) & lead (all natural / low levels)

50 g

14/11/2013 07202 infant cereal cadmium, chromium, lead, mercury (total) & selenium (all natural / low levels)

50 g

28/11/2013 07203 canned fish arsenic (total), cadmium, mercury (total) (all natural levels)

150 g

12/12/2013 07204 soya flour aluminium, arsenic (total), cadmium, lead & mercury (total) (all high levels)

50 g

07/01/2014 07205F fruit juice cadmium, iron, lead, & tin (all high levels) 50 mL

23/01/2014 07206 cocoa powder cadmium & lead (both natural levels)

50 g

11/02/2014 07207F vegetable purée cadmium, lead & tin (all high levels) 50 g

27/02/2014 07208 powdered rice arsenic (inorganic), arsenic (total) & cadmium mercury (total) & lead (all high levels)

50 g

13/03/2014 07209 canned fish arsenic (total), methyl mercury & mercury (total) (all natural levels)

150 g

25/03/2013 07210F grapefruit cadmium, lead, iron & tin (all high levels)

50 g

Footnotes F test incurs courier charges DD freeze dried matrix, not to be reconstituted (by participants) prior to testing



Fruit Juice, Soft Drinks & Alcoholic Drinks dispatch




extra TMs

17/05/2013 0848 apple juice brix, pH, total acidity, total sugars, magnesium, potassium & sodium

250 mL

18/09/2013 0849 orange juice brix, pH, citric acid, sucrose, glucose, fructose & total sugars

250 mL

02/01/2014 0850 grapefruit juice brix, pH, total acidity, total sugars, calcium, magnesium & potassium

250 mL

05/03/2014 0851 cranberry juice brix, pH, total acidity, total sugars, phosphorus & potassium

250 mL

01/05/2013 03109 cola drink benzoic acid, caffeine, acesulfame-K & saccharin

150 mL

19/07/2013 03110 ground coffee caffeine (2 test materials supplied,

one regular, one decaffeinated)

2 x 30 g

16/08/2013 03111 soft drink brix, pH, citric acid, sorbic acid, cyclamate & saccharin

150 mL

08/11/2013 03112§ soft drink up to 4 colours from the following list: Allura Red, Brilliant Blue FCF, Carmoisine, Erythrosine,

Green S, Indigo Carmine, Patent Blue V, Ponceau 4R, Quinoline Yellow,

Sunset Yellow FCF, Tartrazine

150 mL

26/11/2013 03113 cola drink caffeine, benzoic acid, total sugars & phosphoric acid (as P2O5)

150 mL

14/02/2014 03114 tonic water benzoic acid, quinine, acesulfame-K & aspartame

150 mL

08/05/2013 1368 whisky alcoholic strength, ethanal (acetaldehyde), ethyl acetate, methanol, propan-1-ol, 2-methylpropanol &

2-methylbutanol + 3-methylbutanol (sum)

200 mL

09/10/2013 1369 brandy alcoholic strength, butan-1-ol, ethanal (acetaldehyde), ethyl acetate, methanol, propan-1-ol,

2-methylpropanol & 2-methylbutanol + 3-methylbutanol (sum) & ethyl

carbamate

200 mL

15/01/2014 1370 wine alcoholic strength, total SO2, total acidity & volatile acidity

220 mL

Footnotes total sugars = that measured by a defined titration method (e.g. Layne-Eynon, Luff-Schoorl, Munson Walker) or, if measured by HPLC, the sum of fructose, glucose, sucrose, lactose, galactose and maltose (NB not all sugars may be present) § both qualitative & quantitative results can be submitted



Oils & Fats dispatch




extra TMs

15/04/2013 14122 vegetable oil saturates, mono-unsaturates & poly-unsaturates

30 mL

03/05/2013 14123 infant formula (may contain LC-PUFAs)

total fat, saturates, mono-unsaturates, poly-unsaturates, total trans fatty acids

(& possibly individual fatty acids: linoleic acid, α-linolenic acid (ALA), ARA & DHA )

50 g

03/06/2013 14124Fφ olive oil peroxide value, acidity, anisidine value & iodine value 100 mL

02/07/2013 14125 nutritionally fortified oil

(may contain LC-PUFAs)

saturates, mono-unsaturates, poly-unsaturates & total trans fatty acids

(& possibly individual fatty acids: linoleic acid, α-linolenic acid (ALA), ARA & DHA )

30 mL

12/08/2013 14126F mixed fat spread total fat, saturates, mono-unsaturates, poly-unsaturates, & trans fatty acids

50 g

30/09/2013 14127Fφ olive oil peroxide value, acidity, anisidine value & iodine value

100 mL

17/10/2013 14128 fish oil omega-3 & omega-6 series fatty acids 30 mL

18/11/2013 14129F mixed fat spread total fat, butyric acid & cholesterol 50 g

30/01/2014 14130 vegetable oil saturates, mono-unsaturates & poly-unsaturates 30 mL

11/03/2014 14131Fφ olive oil peroxide value, acidity, K232 & K270 100 mL

Footnotes F test incurs courier charges φ test has a shortened timescale



Pesticide Residues – Animal Products/Fats and Oils Each test material will contain any number of the pesticides given in List 1.

dispatch date




extra TMs

03/04/2013 0589 hydrogenated vegetable oil

selection from List 1 25 g

0589b blank hydrogenated vegetable oil

BLANK (only available if ordered with test 0589) 25 g

22/05/2013 0590 milk powder selection from List 1 50 g

0590b blank milk powder BLANK (only available if ordered with test 0590) 50 g

31/07/2013 0591 olive oil selection from List 1 50 g

0591b blank olive oil BLANK (only available if ordered with test 0591) 50 g

19/09/2013 0592 sesame oil selection from List 1 50 g

0592b blank sesame oil BLANK (only available if ordered with test 0592) 50 g

11/11/2013 0593F oily fish selection from List 1 50 g

0593bF blank oily fish BLANK (only available if ordered with test 0593) 50 g

21/01/2014 0594F animal (pork) fat selection from List 1 50 g

0594bF blank animal (pork) fat BLANK (only available if ordered with test 0594) 50 g

11/03/2014 0595F butter selection from List 1 50 g

0595bF blank butter BLANK (only available if ordered with test 0595) 50 g

Potential pesticide residues (parent compound only unless otherwise stated) – List 1

aldrin cyproconazole fenthion trans-heptachlor epoxide quintozene

azinphos-ethyl pp′-DDE fenthion sulfone indocacarb spinosad

bifenthrin pp′-DDD (TDE) fenthion sulfoxide metazachlor tebuconazole

boscalid op′-DDT fenvalerate methacrifos tecnazene

cis-chlordane pp’-DDT fluazifop methidathion thiacloprid

trans-chlordane deltamethrin fluquinconazole 4,4’-methoxychlor triazophos

oxychlordane diazinon flusilazole nitrofen vinclozolin

chlorfenvinphos dieldrin formothion parathion-ethyl PCB 28

chlorobenzilate alpha-endosulfan (endosulfan I) haloxyfop parathion-methyl PCB 52

chlorpropham beta-endosulfan (endosulfan II) hexachlorobenzene (HCB) pendimethalin PCB 101

chlorpyrifos (-ethyl) endosulfan sulfate alpha-hexachlorocyclohexane (α-HCH) permethrin (sum isomers) PCB 118

chlorpyrifos-methyl endrin beta-hexachlorocyclohexane (β-HCH) pirimiphos-methyl PCB 138

cyfluthrin (sum isomers) epoxiconazole gamma- hexachlorocyclohexane (lindane) prochloraz PCB 153

lambda-cyhalothrin famoxadone heptachlor profenofos PCB 180

cypermethrin fenpropimorph cis-heptachlor epoxide pyrazophos




Pesticide Residues (continued) – Cereal Products Each test material (except test 0984) will contain any number of the pesticides given in List 2.

dispatch date




extra TMs

08/05/2013 0982 maize flour selection from list 2 50 g

0982b blank maize flour BLANK (only available if ordered with test 0982) 50 g

26/06/2013 0983 wheat flour selection from list 2 50 g

0983b blank wheat flour BLANK (only available if ordered with test 0983) 50 g

09/08/2013 0984 oats chlormequat, mepiquat & glyphosate 100 g

0984b blank oats BLANK (only available if ordered with test 0984) 100 g

02/10/2013 0985 brown rice selection from List 2 50 g

0985b blank brown rice BLANK (only available if ordered with test 0985) 50 g

13/12/2013 0986 infant food (rusk) selection from list 2 50 g

0986b blank infant food (rusk) BLANK (only available if ordered with test 0986) 50 g

13/02/2014 0987 wheat flour selection from list 2 50 g

0987b blank wheat flour BLANK (only available if ordered with test 0987) 50 g

Potential pesticide residues (parent compound only unless otherwise stated) – List 2 2-phenylphenol disulfoton sulfone fenthion sulfoxide metribuzin procymidone

acephate deltamethrin fenthion sulfone malathion propiconazole

azinphos-methyl demeton-S-methyl sulfone fenpropimorph methacrifos pyrimethanil

azoxystrobin diazinon fenvalerate(sum of isomers) methamidophos quinoxyfen

bifenthrin dichlorvos fipronil methomyl quintozene

boscalid difenoconazole fludioxonil omethoate spiroxamine

bromophos-ethyl diflubenzuron fluquinconazole oxydemeton-methyl (demeton-S-methyl sulfoxide)

tebuconazole

captan dimethoate flusilazole paclobutrazole tebufenozide

carbaryl dimoxystrobin flutriafol parathion-ethyl terbufos

carbendazim disulfoton formothion penconazole terbufos sulfone

carbofuran alpha-endosulfan (endosulfan I) alpha-hexachlorocyclohexane (α-HCH)

pendimethalin terbufos sulfoxide

3-hydroxycarbofuran beta-endosulfan (endosulfan II) beta-hexachlorocyclohexane (β-HCH)

permethrin (sum) tetrachlorvinphos

carboxin endosulfan sulfate gamma-HCH (lindane) phorate thiabendazole

chlorfenvinphos epoxiconazole hexaconazole phorate sulfoxide thiacloprid

chlorothalonil ethion imazalil phorate sulfone thiamethoxam

chlorpropham ethoprophos imidacloprid phosalone thiodicarb

chlorpyrifos (-ethyl) etrimfos iprodione phosmet triadimefon

chlorpyrifos-methyl fenamiphos isofenphos-methyl phosphamidon (sum of isomers)

triadimenol

clothianidin fenamiphos sulfoxide isoprothiolane pirimicarb triazophos

cyfluthrin (sum of isomers) fenamiphos sulfone isoproturon desmethyl-pirimicarb tricyclazole

lambda-cyhalothrin fenbuconazole kresoxim-methyl pirimiphos-methyl trifloxystrobin

cypermethrin fenhexamid linuron prochloraz trifluralin

cyproconazole fenitrothion malaoxon pyraclostrobin triticonazole

cyprodinil fenpropidin metconazole pyridaphenthion vinclozolin

disulfoton sulfoxide fenthion



Pesticide Residues (continued) – Fresh Fruits, Dried Fruit, Fresh Vegetables, Tea & Herbs The fruit, vegetable and herb test matrices will be made prepared from fresh fruit, vegetables or herbs that have been made into a purée.

Each test material will contain any number of the pesticides given in List 3, except test 19157 (courgette (zucchini)) and test 19162 (green tea) which will contain any number of the pesticides given in List 4 and test 19164 which is for a single residue.

dispatch date




extra TMs

29/04/2013 19150PF apple pesticide residues from List 3 90 g 19150bPF blank apple BLANK 90 g

29/04/2013 19151PF lemon pesticide residues from List 3 90 g 19151bPF blank lemon BLANK 90 g

17/06/2013 19152PF tomato pesticide residues from List 3 90 g 19152bPF blank tomato BLANK 90 g

15/07/2013 19153PF apricot pesticide residues from List 3 90 g

19153bPF blank apricot BLANK 90 g

15/07/2013 19154PF dried vine fruit (currant)

pesticide residues from List 3 90 g

19154bPF blank dried vine fruit (currant)

BLANK 90 g

13/08/2013 19155 chilli powder (spice)


19155b blank chilli powder (spice)

BLANK 90 g

09/09/2013 19156PF strawberry pesticide residues from List 3 90 g 19156bPF blank strawberry BLANK 90 g

09/09/2013 19157PF courgette (zucchini)


19157bPF blank courgette (zucchini)

BLANK 90 g

21/10/2013 19158PF lettuce pesticide residues from List 3 90 g

19158b PF blank lettuce BLANK 90 g

21/10/2013 19159PF cucumber pesticide residues from List 3 90 g

19159bPF blank cucumber BLANK 90 g

25/11/2013 19160PF coriander (herb) pesticide residues from List 3 90 g

19160bPF blank coriander (herb) BLANK 90 g

25/11/2013 19161PF green beans (inc. pods)


19161bPF blank green beans (inc. pods)

BLANK 90 g

09/01/2014 19162 green tea pesticide residues from List 4 50 g 19162b blank green tea BLANK 50 g

27/01/2014 19163PF broccoli pesticide residues from List 3 90 g 19163bPF blank broccoli BLANK 90 g

27/01/2014 19164PFφ red grape ethephon (single residue) 90 g 19164bPF blank red grape BLANK 90 g

24/02/2014 19165PF pear pesticide residues from List 3 90 g 19165bPF blank pear BLANK 90 g

24/02/2014 19166PF potato pesticide residues from List 3 90 g

19166bPF blank potato BLANK 90 g

31/03/2014 19167PF soya beans pesticide residues from List 3 plus glyphosate 90 g

19167bPF blank soya beans BLANK 90 g

31/03/2014 19168PF orange pesticide residues from List 3 90 g

19168bPF blank orange BLANK 90 g

Footnotes BLANKS can only be ordered with their corresponding proficiency test P matrix will be a purée F test incurs courier charges φ test has a shortened timescale



Potential pesticide residues (parent compound only unless otherwise stated) – List 3

2,4-D cyproconazole fenarimol mecarbam propoxur

2-phenylphenol cyprodinil fenazaquin mepanipyrim propyzamide acephate pp’-DDD (TDE) fenbuconazole metaflumizone

(sum of isomers) prothiofos

acetamiprid pp’-DDE fenhexamid metalaxyl pymetrozine acrinathrin op’-DDT fenitrothion metolcarb pyraclostrobin

aldicarb pp’-DDT fenoxycarb metconazole pyrazophos aldicarb sulfone

(aldoxycarb) deltamethrin fenpropathrin methamidophos pyrethrins (sum)

aldicarb sulfoxide demeton-S-methyl sulfone fenpropimorph methidathion pyridaben atrazine desmethyl-pirimicarb fenpyroximate methiocarb pyrimethanil

azinphos-methyl diazinon fenthion methiocarb sulfone pyriproxyfen azoxystrobin dichlorvos fenthion sulfoxide methiocarb sulfoxide quinalphos

benalaxyl dicloran fenthion sulfone methomyl quinoxyfen benfuracarb dicrotophos fenvalerate

(sum of isomers) 4,4’-methoxychlor quintozene

bifenthrin diethofencarb fipronil methoxyfenozide spinosad (spinosyn A + spinosyn D)

biphenyl diethofencarb sulfoxide fipronil sulfone monocrotophos spiroxamine bitertanol diethofencarb sulfone fluazifop-P-butyl (sum) monolinuron tebuconazole boscalid difenoconazole fludioxonil myclobutanil tebufenozide

bromopropylate diflubenzuron flufenoxuron omethoate tebufenpyrad bromuconazole

(sum of isomers) dimethoate fluquinconazole oxadixyl tecnazene

bupirimate dimethomorph (sum of isomers)

flusilazole oxydemeton-methyl (demeton-S-methyl sulfoxide)

teflubenzuron

buprofezin diniconazole flutriafol oxyfluorfen tefluthrin butocarboxim diphenylamine formetanate HCl paclobutrazol terbufos

butocarboxim sulfoxide disulfoton fosthiazate parathion (-ethyl) terbufos sulfoxide cadusafos disulfoton sulfone furalaxyl parathion-methyl terbufos sulfone carbaryl disulfoton sulfoxide gamma-HCH (lindane) penconazole terbuthylazine

carbendazim DMST haloxyfop (free acid) pencycuron tetraconazole carbofuran dodine HCB (hexachlorobenzene) pendimethalin tetradifon

3-hydroxy carbofuran alpha-endosulfan (endosulfan I)

heptenophos permethrin (sum of isomers)

thiabendazole

carbosulfan beta-endosulfan (endosulfan II)

hexaconazole phenthoate thiacloprid

chlorfenapyr endosulfan sulfate hexythiazox phosalone thiamethoxam chlorfenvinphos (sum of isomers)

EPN imazalil phosmet thiodicarb

chlorobenzilate epoxiconazole imidacloprid phoxim tolclofos-methyl chlorpropham ethiofencarb indoxacarb

(sum isomers) pirimicarb tolylfluanid

chlorpyrifos (-ethyl) ethiofencarb sulfone iprodione pirimiphos-methyl triadimefon chlorpyrifos-methyl ethiofencarb sulfoxide iprovalicarb prochloraz triadimenol chlorthal-dimethyl ethion isofenphos-methyl procymidone triazophos

chlozolinate ethoprophos isoprocarb profenofos trifloxystrobin clofentezine etofenprox isoproturon propamocarb trifluralin clothianidin famoxadone kresoxim-methyl propaquizafop triticonazole cyfluthrin

(sum of isomers) fenamiphos lenacil propargite vinclozolin

lambda-cyhalothrin fenamiphos sulfone linuron propiconazole zoxamide cypermethrin

(sum of isomers) fenamiphos sulfoxide lufenuron



Potential pesticide residues (parent compound only unless otherwise stated) – List 4 acetamiprid dicofol ethion imidacloprid pirimiphos-methyl bifenthrin dimethoate fenazaquin isofenphos procymidone

chlorfenvinphos pp’-DDD (TDE) fenitrothion linuron propargite chlorothalonil pp’-DDE fenpropathrin methomyl pyridaben

chlorpyrifos (-ethyl) op’-DDT fenpropimorph mevinphos pyrimethanil lambda-cyhalothrin pp’-DDT fenvalerate (sum isomers) phenthoate quinalphos

cypermethrin (sum isomers) alpha-endosulfan (endosulfan I) HCB (hexachlorobenzene) phosalone terbuthylazine deltamethrin beta-endosulfan (endosulfan II) alpha-HCH pirimiphos (-ethyl) trifloxystrobin

diazinon endosulfan sulfate gamma-HCH (lindane)

FAPAS PROGRAMME & PROFICIENCY TEST ORDER FORM … (2013-2014) v2 EN.… · fapas programme &...

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