Faculty: Technology and Engineering Department: Chemical ......UNIT – X Hydrogen Power & aspects...
Transcript of Faculty: Technology and Engineering Department: Chemical ......UNIT – X Hydrogen Power & aspects...
The Maharaja Sayajirao University of Baroda
Faculty: Technology and Engineering
Department: Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
Email ID: [email protected]
Name of the Programme: B.E.-I Chemical
Type of the Programme :S.S. of B.E.- I Chemical
Year I CORE / ELECTIVE / FOUNDATION 1: CORE
PAPER CODE:CHL1201
PAPER NAME: PROCESS CALCULATIONS
CREDIT
Semester II HOURS 45
UNIT – I
Introduction:
Chemical Engineering and Chemical Industry.
Steady state and unsteady state processes.
Unit Operations, Unit Processes and Process Flow Diagrams.
04
UNIT – II
Basic Calculations:
State properties: Molecular weight, compositions, density, vapor pressure etc. for
gas, liquid and solid systems.
Thermal properties: Heat capacity, sensible heat, latent heat, heat of reaction, heat
of solution, enthalpy calculations etc. for gas, liquid and solid systems.
Techniques of problem Solution: Analytical, Graphical and Numerical.
12
UNIT – III
Material Balances:
Material balance equations based on conservation principle.
Material balances for non-reactive processes(Unit Operations).
Material balances for reactive processes.
10
UNIT – IV
Energy Balances:
Energy balances for closed and open systems based on energy conservation
principle.
Energy balances for non-reactive processes (Unit Operations),
Energy balances for reactive processes.
Coupled material and energy balances for single unit process.
11
UNIT – V
Multiple Unit Processes:
Introduction to processes with multiple Units.
Material balances on processes with recycle, purge, and bypass.
Introduction to DOF analysis and solution strategy for multi-unit process.
08
REFERENCES
1 Bhatt and Vora: Stoichiometry, 4th Ed, Tata McGraw-Hill
2 D.M. Himmelblau and J. B. Riggs: Basic Principles and Calculations in Chemical Engineering, 8th
Ed, Prentice Hall.
3 R.M. Felder and R.W. Rousseau ‘Elementary Principles of Chemical Processes’ 3rd Ed, John Wiley
and Sons, 2000.
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID :[email protected]
Name of the Program: B.E.CHEMICAL
Type of the Program: S.S. of B.E. -II CHEMICAL
Year II CORE / ELECTIVE / FOUNDATION 1 : CORE
PAPER CODE :
PAPER NAME : MECHANICAL OPERATIONS
CREDIT
Semester I HOURS 45
UNIT – I
Properties of particulate solid
Introduction to particle technology, Characterization of solid particles (size,
shape, size distribution), particle size measurement techniques, Mixed
particles, specific surface of mixture, Particle population.
05
UNIT – II
Screen analysis:
Screening equipment, Method of reporting screen analysis, Capacity and
effectiveness of screens
05
UNIT – III
Size reduction and enlargement:
Principles of comminution, Energy and power required for comminution,
Laws of crushing, size reduction equipments, Industrial processes for particle
size enlargement, size enlargement equipments
05
UNIT – IV
Properties of masses of solids:
Storage of solids: Angle of repose, bulk storage, storage in bins and silos,
Conveying of solids: Codes for characterization of solids, screw conveyers,
belt conveyers, bucket elevators, pneumatic conveying of solids.
04
UNIT – V Mixing of powders and pastes:
Mixers for cohesive and non-cohesive solids, Mixing Index 03
UNIT – VI
Agitation and mixing of liquids:
Basic stirred tank design, Types of impellers, flow patterns, power
consumption and scale up
04
UNIT – VII
Filtration:
Principles of filtration, constant pressure, constant rate filtration,
compressible and incompressible cakes, cake resistance, filter media
resistance, filter media, filter aids, filtration equipments (batch, continuous),
Selection criteria, Washing of filter cakes.
05
UNIT – VIII Gravity setting and sedimentation: Gravity clarifiers, sorting clarifiers, Batch
sedimentation, rate of sedimentation, Design of thickeners and clarifiers 05
UNIT – IX Centrifugal sedimentation: Principles of centrifugal sedimentation, Solid gas
separation, liquid solid separation. 04
UNIT – X
Fluidization: Types of fluidization, Geldart classification of particles.
Minimum fluidization velocity, Pressure drop. Particulate and bubbling
fluidization. Applications of fluidization.
05
REFERENCES
1 W.L. Mc Cabe, J.C. Smith, P.Harriot ‘Unit Operations of Chemical Engineering’ 7th Ed. McGraw
Hill, 2006.
2 J.M. Coulson & J.F. Richardson ‘Chemical Engineering’ Vol.- II, 6th Ed. Elsevier, 2003
3 G.G. Brown Ed. ‘Unit Operations’ John Wiley & Sons, 1950
4 C.G. Geankopolis ‘Transport Processes and Separation Process Principles’ 4th Ed, Prentice Hall
India, 2003.
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara
Contact Details :
E.mail ID :
Name of the Programme: B.E.CHEMICAL
Type of the Programme:S.S. of B.E.-II CHEMICAL
Year II CORE / ELECTIVE / FOUNDATION 1 : CORE
PAPER CODE : CHL1401
PAPER NAME : FLUID FLOW OPERATIONS
CREDIT
Semester II HOURS 45
UNIT – I Nature of Fluids, Fluid statics and its applications, Manometers, Pressure
measurements. 06
UNIT – II
Introduction to fluid dynamics, classification of fluids, concept of viscosity,
viscometers, concept of potential flow, steam lines, average velocity, mass
velocity etc. Laminar and Turbulent flow, dimensional analysis, Reynolds
number and its significance, Concept of boundary layer.
06
UNIT – III Basic equations of fluid flow, Equation of continuity, Bernoulli’s Theorem. 06
UNIT – IV
Incompressible flow in pipes and channels, Frictional losses in closed
channels and pipe fittings, contraction and expansion losses, power
requirement for flow.
08
UNIT – V
Transportation of fluids, Pipes, pipe standards, fittings, pipe joints, valves and
their constructional features, Fluid moving machinery: Positive displacement
and centrifugal pumps, centrifugal pump theory, concept of NPSH, pump
performance and characteristics.
06
UNIT – VI
Flow measurement, Classification and selection of flow meters, Variable head
and variable area meters including notched weirs, positive displacement
meters, coirolismeters, ultrasonic meters and various other quantity meters.
05
UNIT – VII Introduction to compressible flow, flow through pipes and nozzles, Fans,
Blowers ejectors and compressors. 06
UNIT – VIII Special cases: Single and two phase flow through packed beds, two-phase gas
liquid flow in pipes, Essentials of gas solid flows. 02
REFERENCES
1 W.L. Mc Cabe, J.C. Smith, P.Harriot, ‘Unit Operations of Chemical Engineering’ 7th Ed, McGraw
Hill, 2006.
2 P.K. Kundu& I.M. Cohen ‘Fluid Mechanics’ 5th Ed, Academic Press, 2002
3 G.S. Sawhney ‘Fundamentals of fluid mechanics’, 2nded,I.K. International
4 J.M. Coulson & J.F. Richardson ‘Chemical Engineering’ Vol. I, 6th Ed, Elsevier, 2004.
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID :[email protected]
Name of the Program: B.E.CHEMICAL
Type of the Program:S. S of B.E.-II Chemical
Year II CORE / ELECTIVE / FOUNDATION 1 : CORE
PAPER CODE : CHL1403
PAPER NAME : THERMODYNAMICS AND ENERGY
SYSTEM
CREDIT
Semester II HOURS 45
UNIT – I Laws of thermodynamics, thermodynamic functions & their inter relations. 06
UNIT – II PVT relationship and thermodynamic and Property estimation/calculations
(U, H, S, G etc.) property charts. 07
UNIT – III Thermodynamics of flow processes 05
UNIT – IV Refrigeration and Liquefaction 02
UNIT – V Energy / lost work analysis. 03
UNIT – VI Energy forms, Sources and Resources, flow of energy in ecosystem. 02
.
UNIT – VII Key alternative energy Sources such as Solar Energy, Wind Energy and
Tidal power etc.
09
UNIT – VIII Nuclear energy: Fission reaction, nuclear reactors including safety aspects,
Fusion reactions and their prospects. 04.
UNIT – IX Fuel cells 03
UNIT – X Hydrogen Power & aspects of energy storage and other developments. 04
REFERENCES
1 A.W. Culp ‘Principles of Energy conversion’ 2nd Ed, McGraw Hill, 1991,
2 M.M. El-Wakil ‘Power Plant Technology’2nd Ed, McGraw Hill, 1985
3 J.M. Smith, H.C. Van Ness & M.M. Abbot ‘Introduction to Chemical Engineering
Thermodynamics’, 7th Ed, McGraw Hill, 2004.
4 S.R. Turns ‘Thermodynamics concepts and applications’, Cambridge University Press, 2006.
The Maharaja Sayajirao University of Baroda
Faculty: Technology and Engineering
Department: Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
Email ID: [email protected]
Name of the Programme: B.E.II Chemical Engineering
Type of the Programme : S.S. BE II Chemical Engineering
Year II CORE / ELECTIVE / FOUNDATION 1 : CORE
PAPER CODE:
PAPER NAME: UNIT PROCESSES
CREDIT
Semester II HOURS 45
UNIT – I Concept of Unit operation and unit processes and their role in systematizing the
cognitive structure of Chemical industry.
02
UNIT – II
Classification of Unit processes. Their Characteristic features, thermochemistry
etc.
03
UNIT – III Nitration: Classification of nitro-compounds, nitrating agents, types of nitration,
equipments, typical nitration processes such as Nitrobenzene, tri nitrotoluene etc.
10
UNIT-IV Hydrogenation: Hydrogen production technologies, Hydrogenation of Fats and
oils, petroleum fractions etc.
12
UNIT-V Oxidation, Sulphonation and sulfation: General aspects, reagents, catalysts,
equipments, use of SO3, SO2, H2SO4
12
UNIT-VI Esterification and Hydrolysis, Alkylation, Halogenation: General aspects, reagents,
equipments and typical processes.
06
REFERENCES
1 Groggins, P.H., Unit Processes of Organic Synthesis, McGraw-Hill Book Company, NewYork,
1966
2 Desikan, P and Sivakumar, T.C., Unit Processes in Organic Chemical Industries, Chemical
Engineering Education Development Centre, IIT Madras, 1982.
The Maharaja Sayajirao University of Baroda
Faculty: Technology and Engineering
Department: Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
Email ID: [email protected]
Name of the Programme: BE II Chemical Engineering
Type of the Programme : S.S. BE II Chemical Engineering
Year II CORE / ELECTIVE / FOUNDATION 1: CORE
PAPER CODE:
PAPER NAME: ENGLISH COMMUNICATION
SKILLS
CREDIT
Semester II HOURS 28
1.
UNIT – I
GRAMMAR AND VOCABULARY
1. Contextualized grammar
2. Error analysis
3. Word formation
07
UNIT – II
READING SKILLS
1. Skimming
2. Scanning
3. Word meanings and linking devices
Inferring and predicting
07
UNIT – III
WRITING SKILLS
1. Situational Dialogues
2. Paragraph Writing
3. Transfer of information (visual/verbal)
4. Letter writing ( Job Application)
07
UNIT-IV
ORAL and Aural SKILLS
1. Situational Dialogues (oral)
2. Oral presentation
3. Group Discussion
4. Listening comprehension
07
REFERENCES
1 Achar, Deeptha, et.al. Basics of Academic English, Book 1 and 2. Hyderabad: Orient Blackswan.
2012.
2 Grains, Ruth and Redman Stuart. Oxford Word Skills. Oxford: Oxford University Press. 2008.
3 Lynch, Tony. Study Listening. Cambridge: Cambridge University Press. 2004
4 McCarthy & Felicity O’Dell: Cambridge University Press, New Delhi, 1996
5. Michael McCarthy & Felicity O’Dell. English Vocabulary in Use: Upper-Intermediate: (II
Edition): Cambridge University Press, New Delhi, 2001
6. Raman, M. and Sharma S. Technical Communication Principles and Practice. New Delhi: OUP,
2004.
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID : [email protected]
Name of the Program: B.E. CHEMICAL
Type of the Program:F.S. of B.E.-III CHEMICAL
Year III CORE / ELECTIVE / FOUNDATION 1 : CORE
PAPER CODE : CHL1501
PAPER NAME :MASS TRANSFER OPERATIONS – I
CREDIT
Semester I HOURS 45
UNIT – I Molecular diffusion in fluids:
Stefan- Maxwell's diffusion equations Prediction of diffusion coefficients for gases and
liquids.
08
UNIT – II Fundamentals of mass transfer, mass transfer coefficients, interphase mass
transfer,mass transfer theories
04
UNIT – III
Gas absorption: Gas- liquid equilibria, solvent selection criteria, analysis of absorption
columns, graphical design of plate columns, Kremsers Soudres& Brown’s method.
Mass transfer analysis for design of packed absorption columns for gas absorption
(HETP, HTU, NTU concept) Gas-liquid contacting equipments their classification and
selection.
08
UNIT – IV Humidification and dehumidification: Basic concepts, cooling towers and their
classification and selection, cooling tower design by enthalpy potential method.
06
.
UNIT – V
Distillation: Introduction to distillation. Vapor liquid equilibria. Distillation techniques
viz. differential, flash, steam, fractionation, azeotropic and extractive distillation etc.
vapor liquid contacting equipment their constructional and operational features and
design aspects.
08
UNIT – VI
Analysis of binary distillation: Material and energy balance around a distillation
column, concept of reflux, Lewis Sorel method of calculation, McCabe & Thiele
method for determining number of ideal plates, feed stage location, optimum reflux
ratio, condenser and reboiler heat duty, Ponchon & Savarit method for design of plate
column. Concept of plate efficiencies. Distillation in packed columns.
11
REFERENCES
1. R.E. Treybal ‘Mass – Transfer Operation’ 3rd Ed, Mc Graw Hill, 1981
2. J.D. Seader and E.J. Henley “Separation Process Principles”, 3rd Ed, J.Wiley & Sons, 1998
3. C.G. Geankopolis ‘Transport Processes and Separation Process Principles 4th Ed, Prentice Hall
India, 2003.
4. A.S. Foust et.al. ‘Principles of Unit Operations, 2nd Ed, John Wiley, 1972
5. W.L. Mc Cabe, J.C. Smith, P. Harriot, ‘Unit Operations of Chemical Engineering’ 7th Ed, McGraw
Hill, 2006.
6. J.M. Coulson & J.F. Richardson ‘Chemical Engineering’ Vol I, 6th Ed, Elsevier, 2004
7. J.M. Coulson & J.F. Richardson’Chemical Engineering’ Vol II, 5th Ed, Elsevier,2003
8. B.K. Dutta ‘Mass Transfer’ TMH, 2006.
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID : [email protected]
Name of the Programme : B.E. CHEMICAL
Type of the Programme: F.S. of B.E.-III CHEMICAL
Year III CORE / ELECTIVE / FOUNDATION 1 : CORE
PAPER CODE : CHL1502
PAPER NAME : HEAT TRANSFER OPERATIONS
CREDIT
Semester I HOURS 45
UNIT – I
Modes of heat Transfer: Transfer by conduction. General differential
equation for heat conduction, steady state analytical and numerical
methods for flat, cylindrical and spherical geometry. Extended surface
heat transfer, Insulation.
07
UNIT – II
Heat transfer by convection: Free & forced convection, film & overall
heat transfer coefficients, concept of convective resistances in series.
Dimensional analysis of convection, physical significance of the
dimensionless numbers. Laminar & turbulent flow heat transfer inside
tubes & outside of tubes.
07
UNIT – III
Heat exchangers: Classification and selection, double pipe heat
exchanger analysis, parallel and counter flow heat transfer, LMTD,
design considerations, NTU method of heat exchanger analysis and
design, Shell & tube heat exchanger calculations.
09
UNIT – IV
Heat transfer with phase change: Regimes of boiling heat transfer,
various correlations. Heat transfer during condensation, drop and film
condensation, Nusselt’s equation and its applications, condensation
over tube banks.
07
UNIT – V
Heat transfer by radiation: Laws of radiant heat transfer, concept of
black body and grey body. Radiation between surfaces, view factors,
radiation between reflecting surfaces, absorption and emission by
gases, luminous & non luminous gases, combined modes of heat
transfer.
09
UNIT – VI
Evaporation:Types of evaporators their classification and selection.
Single effect and multiple effect evaporators, capacity and economy,
feed arrangement to multiple effect evaporators. Evaporator
calculations for single effect and multiple effects.
06
REFERENCES
1. D.Q. Kern, Process Heat Transfer, 5th Ed, McGraw-Hill, 1965
2. Y.V.C. Rao, Heat transfer, 2nd, Ed.
3. J.M. Coulson & J.F. Richardson ‘Chemical Engineering’ Vol.I, 6th Ed, Elsevier, 2004
4. F.P. Incropera& D.P. Dewitt ‘Fundamental of Heat and Mass transfer’, John Wiley & Sons,
1996
5. J.D. Seader and E.J. Hanley “Separation Process Principles”, J.Wiley & Sons, 1998.
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID : [email protected]
Name of the Program: B.E. CHEMICAL
Type of the Program: F.S of B.E.-III CHEMICAL
Year III CORE / ELECTIVE / FOUNDATION 1 : CORE
PAPER CODE : CHL1503
PAPER NAME :CHEMICAL ENGINEERING
THERMODYNAMICS
CREDIT
Semester I HOURS 45
UNIT – I
Thermodynamic functions and relations for mixtures:
Partial molar property, chemical potential, residual properties, fugacity
& fugacity coefficients, excess functions and activity coefficients,
correlations for excess Gibbs free energy.
09
UNIT – II PVT behaviour including EOS for mixtures; Fugacity estimation/
calculations based on PVT behaviour
06
.
UNIT – III Phase equilibrium criteria and VLE calculations for different pressure
ranges including flash calculations.
03
UNIT – IV Activity coefficient calculation from experimental VLE data and data
reduction, applications of Gibbs-Duhem relation for calculations of
and consistency check for VLE data
06
UNIT – V Phase diagrams for miscible, partially miscible and immiscible liquid
mixtures, introduction to LLE and VLLE calculations.
04
UNIT – VI
Criteria of chemical equilibrium, effect of P and T on equilibrium
conversion (Xe) and equilibrium constant (K), methods of evaluation
of K &Xe, Xe charts for Exothermic, Endothermic, Reversible and
irreversible reactions etc.
06
UNIT – VII
Equilibrium of complex reactions, introduction to equilibrium
conversion calculation under adiabatic and non-isothermal conditions,
introduction to liquid phase, heterogeneous and electrochemical
reaction equilibria, thermodynamic analysis of some chemical
reactions of industrial importance.
08
UNIT – VIII Prediction of thermodynamic properties by group contribution and
other methods.
03
REFERENCES
1. B.G. Kyle ‘Chemical Process Thermodynamics 3rd Ed, Prentice Hall India, 1994
2. J.M. Smith, H.C. Van Ness & M.M. Abbot ,“Introduction to Chemical Engineering
Thermodynamics”, 7th Ed, McGraw Hill, 2004.
3. Y.V.C. Rao, Chemical Engineering Thermodynamics, Universities Press (1997)
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID : [email protected]
Name of the Programme : B.E. CHEMICAL
Type of the Programme: F.S. of B.E.-III CHEMICAL
Year III CORE / ELECTIVE / FOUNDATION 1 : CORE
PAPER CODE : CHL1504
PAPER NAME : CHEMICAL REACTION
ENGINEERING I
CREDIT
Semester I HOURS 45
UNIT – I Introduction to chemical kinetics, types of reactions, kinetics of
homogeneous reactions, temperature dependency of reactions.
04
UNIT – II Formulation and analysis of simple and complex rate equations.
Interpretation of rate data in constant and variable volume systems.
06
UNIT – III
Introduction to reactor design, concept of ideal reactors, development of
design expression for batch, tubular and stirred tank and semi-batch
reactors, multiple reactor systems, reactors in series and parallel, recycle
reactor, advantages and limitations in applications.
11
UNIT – IV Multiple reactions, concept of selectivity, maximizing the desired
product in series and parallel reaction system. Introduction to process
design for some industrial reactors.
09
UNIT – V
RTD and non-ideal reactor analysis, one parameter models for non-ideal
reactor RTD and their equivalence, conversion calculations using RTD
measurements. The use of RTD models for evaluation of reactor
performance.
10
UNIT – VI
Equilibrium conversions, heats of reaction and temperature, Optimum
temperatures for isothermal and non-isothermal operations, product
distribution and effect of temperature in multiple (complex) reactions.
Evaluation of adiabatic and non-adiabatic reactor performance, thermal
stability or reactors.
05
REFERENCES
1. O.Levenspiel “Chemical Reaction Engineering”, 3rd Ed, John Wiley & Sons, 1999
2. H. Scott Fogler ‘Elements of Chemical Reaction Engineering’, 4th Ed, Prentice Hall India,
2005.
3. L Schmidt, ‘The Engineering of Chemical Reactions’, 2nd Ed, Oxford, 2008.
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID :
Name of the Programme:B.E. Chemical
Type of the Programme:F.S. of B.E.-III CHEMICAL
Year III CORE / ELECTIVE / FOUNDATION 1 : CORE
PAPER CODE : CHL1505
PAPER NAME : PROCESS EQUIPMENT DESIGN I
CREDIT
Semester I HOURS 45
UNIT – I
Selection of Materials of Construction for Process equipments and
ancillary equipments. Fabrication techniques used for process
equipments with emphasis on bending of plates, welding and various
finishing techniques. Non destructive testing of vessels.
07
UNIT – II
Design of unfired process vessels subjects to internal pressure, design of
end closures and head, nozzles, flanges, manholes etc. Design of unfired
pressure vessels subjected to external pressure. Design codes for
pressure vessels. Testing of pressure vessels.
14.
UNIT – III Design of non-pressure storage vessels with fixed and floating roofs.
Design of Horton spheres. Design codes for storage tanks and bullets.
06
UNIT – IV Design of tall vertical vessels with considerations of wind loads, seismic
activity and various eccentric loads.
04
UNIT – V Design and construction of autoclaves and high - pressure vessels. 05
UNIT – VI Design of foundation and supports, with special emphasis on skirt
supports and saddle supports.
04
UNIT – VII Design of ancillary equipments: Agitator design, tube sheet design,
ejector design etc. 04.
UNIT – VIII Layout of process equipment in the chemical process industries.
01
REFERENCES
1. L.E. Brownell and E.H. Young, ‘Process Equipment Design’, Wiley, 1959
2. B.C. Bhattacharya, ‘Introduction to chemical equipment design – Mechanical aspects’. CBS
publishing Co., 2008
3. B.C. Bhattacharya and C.M. Narayanan, ’Computer aided design of chemical process
equipment’, New Central Book Agency, 1992.
4. M.V. Joshi and V.V. Mahajani, ‘Process equipment design’, 3rd Ed.
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID : [email protected]
Name of the Program: B.E. Chemical
Type of the Program:S.S of B.E.-III CHEMICAL
Year III CORE / ELECTIVE / FOUNDATION 1 : CORE
PAPER CODE : CHL1601
PAPER NAME : PROCESS EQUIPMENT DESIGN II
USE OF PERRY’S CHEMICAL ENGINEERS HANDBOOK
IS PERMITTED DURING EXAMINATION.
CREDIT
Semester II HOURS 45
UNIT – I
Design of piping systems for single phase and two-phase flows, piping colours
and codes. Selection and specifications of pipes, fittings, valves, pumps and
compressors.
12
UNIT – II Design of gas – liquid, gas – solid, liquid – liquid and solid – liquid separators. 07
UNIT – III Design of the heat exchanges (Kern’s method and Bell’s method), condensers
and reboilers. 08
UNIT – IV Design of vapour – liquid contacting equipments: Plate columns and packed
columns. 08
UNIT – V Specification of design variables. Design of multi-component distillation
systems: FUG method and elements of rigorous methods. 07
UNIT – VI Design of absorbers, driers and crystallizers. 03
REFERENCES
1. Don Green and Robert H.Perry, ‘Perry’s Chemical Engineers Handbook’, 8th Ed, Mc-Graw Hill, 2008
2. S.M. Walas ‘Chemical Process Equipment’ Butterworth- Heinemann, 1999.
3. E.E. Ludwig ‘Applied Process Design of Chemical and Petrochemical Plants’ 4th Ed, Vol. I,II,III, Gulf
professional Publications, 1999.
4. N.P. Chopey ‘Handbook of Chemical Engineering Calculations’ 4nd Ed, McGraw Hill, 1994.
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID : [email protected]
Name of the Program : B.E. Chemical
Type of the Program: S.S. of B.E.-III Chemical
Year III CORE / ELECTIVE / FOUNDATION 1 : CORE
PAPER CODE : CHL1603
PAPER NAME : CHEMICAL REACTION
ENGINEERING II
CREDIT
Semester II HOURS 45
UNIT – I
Fundamentals of heterogeneous reacting systems, the influence of mass
transfer on reaction rates, introduction and analysis of fluid-fluid
systems, kinetic regimes and rate analysis.
08
UNIT – II Classification and selection of fluid-fluid reactors based on reaction
regimes. Design of fluid-fluid reactors.
05
UNIT – III
Kinetics of fluid-solid non catalytic reactions, determination of rate
determining steps, various models of gas solid reactions. Classification
and design of non catalytic fluid particle reactors.
11
UNIT – IV
Heterogeneous catalysis, nature of catalysis, components of commercial
catalysts, catalyst preparation characterization of catalysts, catalyst
poisoning and regeneration.
03
UNIT – V
Fluid solid catalytic reaction kinetics (surface catalysis intrinsic
kinetics), kinetics in porous catalyst particles, effective diffusivity,
particle effectiveness factors, temperature dependency, Laboratory
reactors and analysis of rate data.
09
UNIT – VI Design outline of fixed-bed, fluid-bed, trickle-bed and slurry reactors,
isothermal and adiabatic operations. Selected case studies in design.
09
REFERENCES
1. O.Levenspiel “Chemical Reaction Engineering”, 3rd Ed, John Wiley & Sons, 1999
2. H. Scott Fogler ‘Elements of Chemical Reaction Engineering’, 4th Ed, Prentice Hall India,
2005.
3. L Schmidt, ‘The Engineering of Chemical Reactions’, 2nd Ed, Oxford, 2008.
4. J.M. Smith, ‘Chemical Engineering Kinetics’, 3rd Ed, McGraw-Hill, 1981
5. C.N. Satterfield ‘Heterogeneous Catalysis in Industrial Practice 2nd Ed, McGraw-Hill 1993.
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID : [email protected]
Name of the Program : B.E. CHEMICAL
Type of the Program: S.S. of B.E.-III CHEMICAL
Year III CORE / ELECTIVE / FOUNDATION 1 : CORE
PAPER CODE : CHL1604
PAPER NAME : CHEMICAL PROCESS
INDUSTRIES
CREDIT
Semester II HOURS 45
UNIT – I Chemical Industries in India: An overview, Unit Process concept,
Flow sheet symbols. 02
UNIT – II Industrial acids and gases:
Sulfuric acid, Phosphoric acid, hydrogen etc. 06
UNIT – III
Nitrogenous and Phosphatic Fertilizers:
Ammonia, Urea, Diammonium phosphate, triple super phosphate
etc.
06
UNIT – IV Chlor-alkali Industries: Soda ash, Caustic soda 06
UNIT – V Pulp and paper: Pulping techniques, paper making, paper
machines, black liquor, recovery etc. 02
UNIT – VI Cement and Lime:
Types of cement, manufacture by wet process and dry process, etc. 02
UNIT – VII Petroleum and petrochemicals:
General outlook, various products and derivatives 09
UNIT – VIII Polymerization processes:
Polyolefins, polystyrene, nylons etc. 04
UNIT – IX Pharmaceuticals and pesticides:
Bulk drugs and antibiotics, DDT,BHC, malathion etc. 02
UNIT – X Detergents, oils and fats:
LAB derivatives, fat splitting, transesterification, biodiesel etc. 02
UNIT – XI Dyes, intermediates and pigments: Classification, chromophores,
synthesis techniques, H acid, titanium dioxide etc. 02
UNIT – XII Coal and coal chemicals:
Classification, coking, liquefaction, destructive distillation. 02
REFERENCES
1. R.N. Shreve, ‘Chemical Process Industries’, 5th Ed, McGraw-Hill, 1997
2. C. Dryden, ‘Outline of Chemical Technology’,3rd Ed, TMH, 1974
3. J.A. Kent ‘Riegel’s Handbook of Industrial Chemistry’10th Ed., Springer Science &
Business Media, 2003
4. Kirk and Othmer, ‘Encyclopedia of Chemical Technology’, 5th Ed, 24 volumes, 2006.
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID : [email protected]
Name of the Program : B.E. CHEMICAL
Type of the Program: S.S. of B.E.- III CHEMICAL
Year III CORE / ELECTIVE / FOUNDATION 1 : CORE
PAPER CODE : CHL1605
PAPER NAME : MASS TRANSFER OPERATIONS II
CREDIT
Semester II HOURS 45
UNIT – I
Liquid–Liquid extraction: Extraction equilibria and its graphical
representation, tie line correlations, prediction of 1-1 equilibria. Stage wise &
continuous contacting equipments their classification and selection, design of
multistage counter current extraction with and without reflux.
12
UNIT – II Leaching: Principles and leaching equilibria, unsteady state & steady state
operations, design of leaching systems, leaching equipment and systems.
05
UNIT – III
Membrane Separation Processes: Reverse osmosis, ultra filtration, micro
filtration, dialysis, per vaporation etc. concepts and analysis, flux equations,
fouling and concentration polarization. Membrane modules their fabrication
and design.
08
UNIT – IV Drying: Concepts, calculations of rate of drying, classification and selection of
drying equipment. Design of batch and continuous driers.
07
UNIT – V
Crystallization: Crystal geometry, solubility curves, supersaturation, theories
of nucleation & crystal growth, calculation of yield, classification and
selection of equipment for solution crystallization, MSMPR crystallization
model, melt crystallization.
05
UNIT – VI
Adsorption & Ion exchange: Equilibrium considerations, stage wise
adsorption and continuous contact adsorption. Fixed bed adsorption, scale up
for constant pattern front, Thermal swing and pressure swing adsorption.
Counter current adsorption, simulated moving bed. Chromatographic
separations.
08
REFERENCES
1. R.E. Treybal ‘Mass-Transfer Operation’ 3rd Ed. Mc Graw Hill, 1981
2. J.D. Seader and E.J. Henley “Separation Process Principles”, 3rd Ed, J.Wiley & Sons,
3. C.G. Geankopolis’Transport Process and Separation Process Principles’ 4th Ed, Prentice Hall India
2003.
4. A.S. Foust et.al. ‘Principles of Unit Operations, 2nd Ed, John Wiley, 1972
5. W.L. Mc Cabe, J.C. Smith, P. Harriot, ‘Unit Operations of Chemical Engineering’ 7th Ed, McGraw
Hill, 2006.
6. J.K. Coulson & J.F. Richardson ‘Chemical Engineering’ Vol. 1, 6th Ed, Elsevier 2004.
7. J.K. Coulson & J.F. Richardson ‘Chemical Engineering’ Vol. 2, 5th Ed, Elsevier 2003.
8. B.K.Dutta ‘Mass transfer’ TMH, 2006
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID : [email protected]
Name of the Program: B.E. CHEMICAL
Type of the Program: F.S of B.E.-IV CHEMICAL
Year IV CORE / ELECTIVE / FOUNDATION 1 :
PAPER CODE : 1702
PAPER NAME : INDUSTRIAL TRAINING
CREDIT
Semester I HOURS
UNIT – I
Each student will undergo industrial training for minimum period
of two weeks during summer vacations after appearing in S.S. BE
III examinations. After the training students will prepare a report
on the training incurred by them in the industry, this report has to
be duly certified by the trainers from the industry where training
was undertaken.
UNIT - II
During the time of training the students will either identify a
suitable product to prepare a detailed project report or the product
will be assigned to them by the department to work out a project
report that has to be submitted by the end of SS BE IV for
evaluation.
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID : [email protected]
Name of the Programme: B.E. CHEMICAL
Type of the Programme: F.S. of B.E.- CHEMICAL
Year IV CORE / ELECTIVE / FOUNDATION 1 : CORE
PAPER CODE : CHL 1703
PAPER NAME : INSTRUMENTATION AND PROCESS
CONTROL
CREDIT
Semester I HOURS 45
UNIT – I
Introduction to measurement: instruments for measurement of process
variables such as, temperature, flow, liquid level, Pressure.
Instrumentation symbols and labels, Essentials of error analysis.
12
UNIT – II
Introduction to process control, block diagram representation of control loop,
control strategies, mathematical modelling of physical systems, linear system
analysis, dynamics of first order, second order and higher order systems
using transfer functions, transient response, linearization of non linear
models.
08
UNIT – III
Open loop and closed loop transfer functions. Design of single loop feedback
control system. Stability of closed loop, effect of loop parameters on ultimate
gain, effect of dead time, Routh’s test.
06
UNIT – IV
Basic components of control system, sensors and transmitters, control valves,
feedback controllers, actions, types, reset-windup. Tuning of feedback
controllers, tuning controllers for integrating processes, synthesis of
feedback controllers, tuning rules.
07
UNIT – V Stability of control systems, Frequency response analysis, Bode and Nyquist
stability criteria. 06
UNIT – VI
Advanced control strategies, feed forward, cascade, advanced supervisory,
model predictive control, multivariable control, introduction to digital
control principles, microprocessor based control.
06
REFERENCES
1. Luyben, ‘Process Modeling, Simulation and Control for Chemical Engineers’, 2nd Ed, McGraw-
Hill – 1990.
2. Bequette, ‘Process Dynamics’, Prentice Hall, 1998.
3. Coughanor ‘Process systems analysis and control’ 2nd Ed, McGraw-Hill, 1991.
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID : [email protected]
Name of the Program: B.E. CHEMICAL
Type of the Program: F.S. of B.E. - IV CHEMICAL
Year IV CORE / ELECTIVE / FOUNDATION 1 : CORE
PAPER CODE : CHL1704
PAPER NAME : POLYMER SCIENCE AND
TECHNOLOGY
CREDIT
Semester I HOURS 45
UNIT – I Introduction & Basic Concepts, Polymer based industries and feed stocks.
Classification of Polymers. 02
UNIT – II
State of polymer, structure property relations and transition temperatures.
Polymer solutions and characterization of polymers (MW & its experimental
determination), polymer fractionation.
11
UNIT – III
Chain polymerization: Mechanism and kinetics; copolymerization.
Condensation polymerization, coordination polymerization, Techniques of
polymerization.
08
UNIT – IV Plastics–Materials & some typical manufacturing process, (poly olefins,
PVC, PS, PMMA, Epoxy resins etc.) Testing of Polymers. 09
UNIT – V
Rubbers and fibres, materials & some typical manufacturing process, Testing
of rubbers and elastomers. Mechanical properties: Elasticity, visco elasticity,
factors affecting mechanical behaviour etc.
08
UNIT – VI Processing of plastics and rubbers. 07
REFERENCES
1. F.W. Billmeyer, Text book of Polymer Science, 3rd Ed, Wiley, 1984
2. C.E. Carraher, Introduction to polymer chemistry, Traylor and Francis, 2007
3. F. Rodriguez, ‘Principles of polymer systems’ 4th Ed, Traylor and Francis, 1996.
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID : [email protected]
Name of the Program: B.E. Chemical
Type of the Program:F.S. of B.E.-IV Chemical
Year IV CORE / ELECTIVE / FOUNDATION 1 : CORE
PAPER CODE: CHL1705
PAPER NAME: SAFETY HEALTH AND
ENVIRONMENT
CREDIT
Semester I HOURS 45
UNIT – I Types of hazards in the chemical industry, accident and loss statistics,
nature of the accident process.
Toxicology and industrial hygiene, models for toxic release.
04
UNIT – II General aspects of fires and explosions, design to prevent fires and
explosions, Fire and explosion indices, Phenomena of vapour cloud
explosion, flash fires and BLEVE
06
UNIT – III Safety considerations in design, installation, operation and maintenance of
selected process equipment, relief system and flares etc.
05
UNIT – IV Hazard and operability studies Hazard analysis ‘What if’ analysis.
Failure modes and effect analysis, fault tree analysis, event tree analysis.
04
UNIT – V
Acceptable risk and safety properties, protective equipment for personal
and plant for various hazards, safety procedure, emergency response.
Disaster management, insurance, workers safety and public liability, other
liabilities.
04
UNIT – VI
Ecology, classification of ecological factors, fundamental ecological
variables, Ecological principles governing use of natural resources,
Atmosphere, hydrosphere and climates, cycles of principal biogenetic
elements and water cycle, perturbation of cycles due to human
interference, its consequences and mitigation.
Green house effect, global warming, air pollution acts & legislations.
08
UNIT – VII
Assessment of air quality, sampling and measurement. Control of dusts,
mists and aerosols in industrial processes using different equipments.
Control of toxic releases, SOX &NOX ,using absorption, and adsorption
other chemical treatment techniques.
06
UNIT VIII
Water quality assessment and water quality management, Physical,
chemical and biochemical techniques of water pollution control. Water
pollution prevention and control acts.
Solid waste management. Landfills, nuclear waste management schemes.
08
REFERENCES
1. Crowl and Louver ‘Chemical Process safety: Fundamentals with Applications:’ 3nd Ed., Prentice
Hall, 2011
2. Valsaraj, ‘Elements of environmental engineering’ CRC press, 1998
3. Sanders, ‘Chemical process safety’ 3rd Ed, Elsevier, 2005.
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID :[email protected]
Name of the Program : B.E. CHEMICAL
Type of the Program :F.S. of B.E.-IV CHEMICAL
Year IV CORE/ELECTIVE/FOUNDATION 1 : CORE
PAPER CODE : CHL 1706
PAPER NAME : TRANSPORT PHENOMENA
CREDIT
Semester I HOURS 45
UNIT – I
The role of transport phenomena in the understanding of chemical
engineering.
Fluids classification. Transport properties. Introduction to non-
Newtonian fluids. Two parameter models.
03
UNIT – II Lagrangian and Eulerian concept of motion, control volume
approach, overall and differential mass balances in Cartesian,
cylindrical co-ordinate systems.
04
UNIT – III Shell momentum balance approach; Application to selected problem.
06
UNIT – IV Equation of motion and its application. 04
UNIT – V Boundary Layer theory von Karman’s analysis, exact solutions using
stream functions. Turbulence concepts mixing length hypothesis,
universal velocity profile and its application.
06
UNIT – VI Shell energy balance approach: Applications to selected problems. 05
UNIT – VII Convective Heat transport : Asymptotic solutions of typical flow
problems etc.
04
UNIT – VIII Fick’s law of diffusion application of differential balances to mass
transfer, critical analysis correlations for mass transfer. 04
UNIT – IX Mass transfer theories Convection – Diffusion problems in
homogenous and heterogeneous media.
04
UNIT – X Analogy between Momentum heat and mass transfer.
05
REFERENCES
1. Bird Stewart and Lightfoot, ‘Transport Phenomena’ 2nd Ed, Wiley, 2002
2. Welty, Wicks, Wilson &Rorer ‘Fundamentals of Momentum heat & mass transfer,
Wiley, 2001.
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID : [email protected]
Name of the Program: B.E. CHEMICAL
Type of the Program: F.S of B.E.-IV CHEMICAL
Year IV CORE / ELECTIVE / FOUNDATION 1 :
PAPER CODE : 1711L
PAPER NAME : COMPUTER AIDED DESIGN
LABORATORY
CREDIT
Semester I HOURS
UNIT – I
Students will be assigned computational / simulation exercises
to be worked out using flow sheet simulators with special
emphasis on property estimation and process optimization.
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID :[email protected]
Name of the Program: B.E. CHEMICAL
Type of the Program:F.S. of B.E.IV CHEMICAL
Year IV CORE / ELECTIVE / FOUNDATION 1 : ELECTIVE
PAPER CODE :CHL1701
PAPER NAME ELECTIVE : C ADVANCES IN
SEPARATION SCIENCE
CREDIT
Semester I HOURS 45
UNIT – I
The structure of separation processes, definitions of separation and separative
work, characterization of concentration distribution. The morphology of
separations processes.
04
UNIT – II Adsorptive bubble separation techniques, principles, application and design. 04
UNIT – III Membrane processes, classification, principles, applications and design. 06
UNIT – IV Melt crystallization, zone refining, short path distillation and super critical
extraction. 08
UNIT – V Electrical separations: Electrophoresis, electrodialysis, protein purification
using isoelectric focusing in gels, field flow fractionation. 07
UNIT – VI Chromatographic separation principles. Applications and scale up, separations
based on simulated moving beds, affinity chromatography. 07
UNIT – VII Extractive separations using liquid membranes, reverse micelles and micro
emulsions. 05
UNIT – VIII Features of separation of isotopes, isomers and other complex molecules using
novel separation techniques.
04
REFERENCES
1. Wankat, ‘Rate based separation’, Elsevier, 2005.
2. King, ‘Separation processes’, 2nd Ed, Mc-Graw Hill, 1980.
3. Li, ‘Recent developments in separation science’, Vol I –V, CRC press, 1980
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID : [email protected]
Name of the Programme: B.E. CHEMICAL
Type of the Programme: F.S. of B.E.-IV CHEMICAL
Year IV CORE / ELECTIVE / FOUNDATION 1 : ELECTIVE
PAPER CODE :CHL1707
PAPER NAMEELECTIVE:D PETROLEUM
ENGINEERING
CREDIT
Semester I HOURS 45
UNIT – I Prospecting for petroleum, exploration methods, reserve appraisals,
Exploration & production, petroleum management. 05
UNIT – II Well logging and Basin modelling, Natural gas coal bed methane, gas
hydrate and deep water exploration 09.
UNIT – III Reservoir characterization, Physico-Chemical environment of petroleum
reservoirs in relation to oil and gas recovery systems. 10
UNIT – IV Flow through porous media, mechanism of entrapment and mobilization of
oil in porous media. 05
UNIT – V Enhanced oil recovery techniques using surfactant & polymer flooding,
reservoir management techniques. 06
UNIT – VI Drilling, Production, platform engineering and transportation.
Safety aspects in Petroleum production. 06
UNIT – VII Hydrocarbon resources and petroleum supply scenario. 04
REFERENCES
1 James Speight, The Chemistry and Technology of Petroleum, CRS Press, Fifthe Edition.
2 Boyun Guo, William C. Lynos, Ali Ghalambor, Petroleum Production Engineering: A Computer
Assisted approach. Gulf Publiacation.
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID :[email protected]
Name of the Program : B.E. CHEMICAL
Type of the Program: F.S. of B.E.-IV CHEMICAL
Year IV CORE / ELECTIVE / FOUNDATION 1 : ELECTIVE
PAPER CODE: CHL 1708
PAPER NAME ELECTIVE-I : A: COLLOID AND
SURFACE SCIENCE
CREDIT
Semester I HOURS 45
UNIT – I Nature of colloidal dispersions: Scope and variables. 04
UNIT – II Particle size and shape, transport properties of suspensions, sedimentation
and diffusion. 05
UNIT – III Liquid surfaces and interfaces, thermodynamics of surfaces, surface tension,
contact angle, interfacial tensions, surface energies. 05
UNIT – IV
Colloidal structures in surfactant solutions, micellar phase diagrams,
adsorption from solution and monolayer formation, soft interfaces,
Langmuir, Blodge films.
05
UNIT – V
Dispersions, rheology of dispersions, electrical charges in dispersions, forces
of attraction and repulsion between particles Electro kinetics and zeta
potential.
06
UNIT – VI Colloidal and dispersion stability, DLVO theory, electrostatic and polymer
induces colloidal stability. 07
UNIT – VII Emulsions, foams and micro emulsion. 07
UNIT VIII Industrial applications to surface coating industry, pharmaceutical industry,
oil recovery etc.
06
REFERENCES
1. R.J. Hunter, Foundations of colloid science, 2nd Ed Oxford, 2006
2. Lyklema, ‘Fundamentals of interfacial and colloid science’, Vol. I – V Academic press, 1982
3. Cosgrove, ‘Colloid Science’ Blackwell Publishing, 2005.
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID :[email protected]
Name of the ProgramB.E. Chemical
Type of the Program F.S. of B.E.-IV CHEMICAL
Year IV CORE / ELECTIVE / FOUNDATION 1 : ELECTIVE
PAPER CODE : CHL1709
PAPER NAME ELECTIVE : B CATALYSIS: SCIENCE &
TECHNOLOGY
CREDIT
Semester I HOURS 45
UNIT – I
Basics of Catalysis: Emergence of catalysis science & technology, a brief
history importance of catalysis and catalyst technology, Foundation catalytic
phenomena & principles.
03.
UNIT – II
Homogeneous and Enzyme catalysis: Elementary steps in homogeneous
catalysis, metal complex catalysis in liquid phase, liquid exchange dissociation
&coordination, oxidative addition, reductive elimination, insertion and
migration. Structure/Activity relationships, steric effects. A symmetric
homogeneous catalysis, industrial examples, homogeneous catalysis without
metals, cleric acid/base catalysis, organocolysis,
Essentials of enzyme catalysis –Michaelis – Mentenreaction, Scaling up
homogeneous catalysis, catalyst recovery & recycle, Hybrid catalysts.
10.
UNIT – III
Heterogeneous Catalysis: Concept of active site model catalyst systems, real
catalysts, promoters, modifiers, poisons, preparation of solid catalysts, selection
of support catalyst characterization. Surface characterization, temperature
programmed techniques, spectroscopy & microscopy, selected care studies.
10.
UNIT – IV
Catalytic Reactor Design: The LHHW model, general behavior of catalyst
particles & pellets, heat and mass transfer aspects, Thiele modulus and
effectiveness factor. Choice of reactors in lab and plants collection & analysis
of data from lab. Reactors. Fundamentals of catalytic reactor design, selected
care studies.
08.
UNIT – V
Catalyst Deactivation: Causes and mechanism of deactivation, prevention and
regenerative treatment of catalyst decay, selected care studies.
Optimal distribution of catalyst in a single pellet. Optimal distribution of
catalyst in a reactor.
07
UNIT – VI
Environmental Catalysis :
1. Mobile sources: Automotive gasoline catalytic converters, catalytic
abatement of emissions from diesel engines, Trends in emission control for
mobile sources.
2. Stationary sources: Catalytic reduction of NOy catalytic oxidation of VOC
emissions, catalytic oxidation of CO emission, Kinetics & reactor design for
CO & VOC oxidation.
07.
REFERENCES
1. Morbidelli, Cavnilidis& Varma Catalyst design Cambridge Univ. press 2001.
2. Twigg, ‘Catalyst Handbook’ Manson publications, 1996.
3. Bartholonew and Farrauto ‘Fundamentals of Industrial catalytic processes’ Wiley Interscience, 2006.
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID : [email protected]
Name of the Program B.E. Chemical
Type of the Program: S.S. of B.E.-IV Chemical
Year IV CORE / ELECTIVE / FOUNDATION 1 : CORE
PAPER CODE : CHL 1801
PAPER NAME : MODELING SIMULATION AND
OPTIMIATION
CREDIT
Semester II HOURS 45
UNIT – I Role of Modeling, Simulation and Optimization (MSO) in process design –
Synthesis Analysis, 02
UNIT – II Modeling: Introduction, Classification of process models, Model Building,
Characteristics of mathematical models. 08
UNIT – III
Simulation: Analytical and Numerical methods for solving model equations,
Accuracy and error analysis, Approaches to Process Simulation, Commercial
simulators.
06
UNIT – IV
Optimization Introduction: Optimization problem and its formulation,
General approach for solution, Objective functions, Classification of
Optimization problems and methods. 07
UNIT – V
Optimization techniques:
-Continuity, convexity and conditions for maxima / minima
-Analytical methods: Direct search (without constraints) Lagrangian
Multiplier (with constraints),Calculus of Variation.
-Newton and quasi Newton methods for single and multivariable search
-Linear (LP) and non linear (NLP) programming with constraints
-Mixed Integer Programming: MILP and MINLP
-Global Optimization Techniques
16
UNIT – VI
Applications of modelling simulation and optimization to chemical processes
and equipments. Fluid flow, heat Transfer, separations, reaction systems and
reactors etc. Use of spreadsheets and MATLAB for Simulation and
Optimization.
06
REFERENCES
1. Edgar, Himmelblau, and Lasdon ‘Optimization of Chemical Process’ McGraw-Hill, 1990
2. Babu, ‘Process Plant Simulation’. Oxford, 2005
3. Ramiez, ‘Computational methods for process simulation’, Butterworth, 1992.
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID :
Name of the Program: B.E. Chemical
Type of the Program:S.S. of B.E.-IVChemical
Year IV CORE / ELECTIVE / FOUNDATION 1 : CORE
PAPER CODE : CHL1803
PAPER NAME : PETROLEUM REFINERY
ENGINEERING
CREDIT
Semester II HOURS 45
UNIT – I Development of Petroleum Refining industry in India. Crude evaluation
and Testing of refinery products. 04
UNIT – II Primary processing of crude, preparation, atmospheric and vacuum
distillation, flow sheets process, conditions and Equipment. 05
UNIT – III Catalytic cracking and hydrocracking. Principles, feed-stocks, catalysts and
hardware 08
UNIT – IV Catalytic reforming: Principles, feed-stocks, catalysts and hardware.
Extraction of aromatics 06
UNIT – V Vis-breaking, coking, isomerization, alkylation and polymerization 06
UNIT – VI Treatment of petroleum products. Hydrodesulphurization. 04
UNIT – VII Refining of Lube distillates: Deasphalting, solvent extraction, dewaxing
etc. Production of bitumen, waxes and greases 08
UNIT – VIII Processing natural and associated gases. 04
REFERENCES
1. James Speight, "The Chemistry and technology of petroleum", 2nd ed., Marcel Dekker, 1991
2. R.A. Meyers, ’Handbook of Petroleum refining processes’, 3rd Ed., McGraw-Hill, 2004.
3. Nelson, ‘Petroleum Refining Engineering’, McGraw-Hill, 1949
4. B. K. Bhaskarrao, "Modern Petroleum Refining Processes", Oxford and IBH, 1984
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID : [email protected]
Name of the Program: B.E. Chemical
Type of the Program: SS BEIV CHEMICAL
Year IV CORE / ELECTIVE / FOUNDATION 1 : CORE
PAPER CODE : CHL 1804
PAPER NAME : PROCESS SYNTHESIS AND
ECONOMICS
CREDIT
Semester II HOURS 45
UNIT – I
Introduction, role of process synthesis in process design, hierarchy of
synthesis steps. Synthesis Tree, approaches for synthesis, heuristics for
process synthesis. Project engineering, plant location, plant layout and
utilities.
08
UNIT – II Attainable Regions and reactor networks: Concepts and implementation
techniques, reactor – separator – recycle network. 06
UNIT – III
Heat & Power integration: Heat Exchanger Networks –Stream matching,
heat loops and minimum heat exchangers. Heat integration in
Distillation trains. Minimum energy requirement targets and pinch
analysis
08
UNIT – IV
Project scheduling. Scheduling of batch processes. Optimization of
cycle time and number of units. CPM/PERT, identification of critical
path & critical activities
08
UNIT – V
Project cost estimation and cost of production estimation. Interest,
investment costs, depreciation, profitability, criteria cash flow diagram,
cost indices.
08
UNIT – VI
Economics of selecting alternatives and replacement cost, economy of
scale, marginal cost, break even analysis and optimization. Inventory
Control, taxes and insurance, legal aspects, liabilities, patent indemnity
etc.
07
REFERENCES
1. Robin Smith, ‘Chemical Process Design and Integration’, Wiley, 2005.
2. Biegler, Grossmann and Westerberg, ‘Systematic Methods of Chemical Process Design’, Prentice
Hall, 1997.
3. Seider, Seader, Lewin, ‘Product and Process Design Principles’, 2nd Ed., Wiley 2004.
4. Peters and Timmerhaus, ‘Plant design and economics for chemical engineers’ 4th Ed,
McGraw-Hill, 1991.
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID : [email protected]
Name of the Program: B.E. Chemical
Type of the Program: SS BEIV CHEMICAL
Year IV CORE / ELECTIVE / FOUNDATION 1 :
PAPER CODE : 1805
PAPER NAME : PROJECT
CREDIT
Semester II HOURS
UNIT – I
Identify a suitable product and prepare a detailed project report or the product will
be assigned to them by the department to work out a project report. The report has
to be submitted at the end of SS BE IV for evaluation.
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID : [email protected]
Name of the Program: B.E. Chemical
Type of the Program: SS BEIV CHEMICAL
Year IV CORE / ELECTIVE / FOUNDATION 1 :
PAPER CODE : 1806
PAPER NAME : SEMINAR
CREDIT
Semester II HOURS
UNIT – I
Students will be assigned a topic for which a detailed literature survey has to be
carried out. Students will refer to various books and journals for the same and
prepare a report. The report has to be submitted at the end of SS BE IV for
evaluation.
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID : [email protected]
Name of the Program: B.E. Chemical
Type of the Program: SS. of B.EIVChemical
Year IV CORE / ELECTIVE / FOUNDATION 1 : ELECTIVE
PAPER CODE:CHL1807
PAPER NAME ELECTIVE II: D PETROCHEMICAL
TECHNOLOGY
CREDIT
Semester II HOURS 45
UNIT – I Scope of Petrochemical industry in India, Feedstock for petrochemicals 03
UNIT – II Naphtha cracking/Gas Cracking – separation and purification of cracker
products (olefins and diolefins) 06
UNIT – III Production and purification of synthesis gas. C1 based petrochemicals
(methanol, formaldehyde, acetic acid etc.) 06
UNIT – IV
Petrochemicals from various unit processes like oxidation, dehydrogenation, chlorination, oxychlorination, ammoxidation, hydration, dehydration, nitration, polymerization etc.
12
UNIT – V
Aromatics production, isolation of aromatics, separation of C8 aromatics.
Benzene derivatives, ethylbenzene, styrene etc, xylene derivatives, phthalic
anhydride, terpthalic acid, dimethyl terpthalate etc.
12
UNIT – VI
Miscellaneous aspects of petrochemical production: Safety and Health aspects,
environmental aspects, Clean Technologies, Future beyond Petroleum. 06
REFERENCES
1. P. Desikan and T.C. Sivakumar, ‘Unit processes in Organic Chemical Industries’, IIT Madras,
1982.
2. E.C. Leonard, ‘Vinyl and Diene Monomers’, Wiley 1969.
3. H.G. Franck & J.W. Stadelhofer, ‘Industrial Aromatic Chemistry’, Springer Verlag, 1988.
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID :[email protected]
Name of the Program : B.E. CHEMICAL
Type of the Program: SS BE IV CHEMICAL
Year IV CORE / ELECTIVE / FOUNDATION 1 : ELECTIVE
PAPER CODE : CHL 1808
PAPER NAME : ELECTIVE II : A :
NANOTECHNOLOGY
CREDIT
Semester II HOURS 45
UNIT – I Nanotechnology foundations: Definition, historical perspective, effects of
nanoscience and nanotechnology in various fields 03
UNIT – II
Properties of nanostructured materials: Shape and size dependent
properties, colour, melting point, density of states, band gap, magnetism
etc.
07
UNIT – III
Synthesis of nanoparticles: Top down and bottom up approaches, Nano
particles via colloids, micelles, vesicles, polymers, crystalline and zeolite
hosts. Mechanical attrition, high energy ball milling.
10
UNIT – IV
Characterization techniques of nanostructured materials: Scanning electron
microscopy, Transmission electron microscopy, scanning tunneling
microscopy, atomic force microscopy, X-ray diffractometer, spectroscopy,
UV-Vis, Raman, EDX, AES etc.
10
UNIT – V Fabrication : Crystal growth, epitaxy, lithography, etching, masking,
MEMs 07
UNIT – VI
Applications relevant to the chemical industry: Catalysis, fuel cells,
coatings, nanocomposite polymers, fluid inks, dyes, block copolymers and
dendrimers.
08
REFERENCES
1. K.J.Klabunde , ‘Nanoscale materials in Chemistry’, Wiley Interscience, 2001.
2. J.Poole and S. Owens, ‘ Introduction to Nanotechnology’ Wiley, 1998
3. C.N.R Rao, Chemistry of Nanomaterials’ Wiley, 2007
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID : [email protected]
Name of the Program : B.E. CHEMICAL
Type of the Program: S.S. of B.E.-IV CHEMICAL
Year IV CORE / ELECTIVE / FOUNDATION 1 : ELECTIVE
PAPER CODE : CHL 1809
PAPER NAME ELECTIVE II : B BIOTECHNOLOGY
CREDIT
Semester II HOURS 45
UNIT – I Introduction to Biotechnology. Basic microbiology and recombinant DNA
technology 04
UNIT – II Kinetics of enzyme catalysis including immobilized enzyme technology 06
UNIT – III Kinetics of substrate utilization product formation and biomass production in
cell culture. 07
UNIT – IV Transport phenomena in Bioprocess systems. 07
UNIT – V Aeration/Agitation/Mediasterilization/Air fertilization. 05
UNIT – VI Design and analysis of bioreactors. 06
UNIT – VII Downstream processing techniques. 03
UNIT – VIII
Industrial Biotech products – Ethyl alcohol based on various substrates
including lignocelluloses. Penicillin citric Acid, SCP, Bio-fertilizers, Baker’s
yeast – other modern biotech products.
07
REFERENCES
1 Bailey &Ollis, ‘Biochemical Engineering’,2nd Ed, McGraw – Hill, 1986.
2 Moo-Young, ‘Comprehensive biotechnology’ Vol I to V, Elsevier, 1984.
3 Belter, Cussler and Hu, ‘Bioseparations’ Wiley, 1988.
The Maharaja Sayajirao University of Baroda
Faculty : Technology and Engineering
Department : Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
E.mail ID : [email protected]
Name of the Program: B.E. Chemical
Type of the Program:S.S. of B.E.-IV Chemical
Year IV CORE / ELECTIVE / FOUNDATION 1 :ELECTIVE
PAPER CODE: CHL1810
PAPER NAME: POLYMER PROCESSING
CREDIT
Semester II HOURS 45
UNIT – I Basic aspects of Polymers: Functionality, types, structure-property
relationship, processing fundamentals, processing aids and additives.
04
UNIT – II Morphology, rheology and flow of polymers. 06
UNIT – III Heat and mass transfer in polymer systems, mixing of polymers, mixing
equipments.
07
UNIT – IV Extrusion of polymers, extrusion equipment, calendering. 10
UNIT – V Moulding of polymers: Blow, compression, transfer, rotational and
injection moulding techniques, analysis and equipments.
10
UNIT – VI Other processing techniques: Sheet forming, fiber spinning, pultrusion,
techniques and equipments.
08
REFERENCES
1. B.R.Gupta, ‘Polymer Processing Technology’, Asian Books Pvt. Ltd, 2008
2. Z. Tadmor and C.G.Gogos, ’Principles of Polymer Processing’ John Wiley and Sons, 1979