Experiment #4: Sodium borohydride reduction of...

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EXPERIMENT #4: SODIUM BOROHYDRIDE REDUCTION OF VANILLIN

Transcript of Experiment #4: Sodium borohydride reduction of...

Page 1: Experiment #4: Sodium borohydride reduction of vanillinpeople.morrisville.edu/~habera/PDFFiles/SPRING_2020... · EXPERIMENT #4: SODIUM BOROHYDRIDE REDUCTION OF VANILLIN 7. When butanoic

EXPERIMENT #4: SODIUM BOROHYDRIDE REDUCTION OF VANILLIN

Page 2: Experiment #4: Sodium borohydride reduction of vanillinpeople.morrisville.edu/~habera/PDFFiles/SPRING_2020... · EXPERIMENT #4: SODIUM BOROHYDRIDE REDUCTION OF VANILLIN 7. When butanoic

EXPERIMENT #4: SODIUM BOROHYDRIDE REDUCTION OF VANILLIN

Page 3: Experiment #4: Sodium borohydride reduction of vanillinpeople.morrisville.edu/~habera/PDFFiles/SPRING_2020... · EXPERIMENT #4: SODIUM BOROHYDRIDE REDUCTION OF VANILLIN 7. When butanoic

EXPERIMENT #4: SODIUM BOROHYDRIDE REDUCTION OF VANILLIN

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EXPERIMENT #4: SODIUM BOROHYDRIDE REDUCTION OF VANILLIN

7. When butanoic acid is treated with sodium borohydride, 1-butanol is not obtained.

There are, however, definite signs of reaction (bubbling, heat). What might the reaction be?

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EXPERIMENT #4: SODIUM BOROHYDRIDE REDUCTION OF VANILLIN


Synthesis of Alcohols Reduction of Aldehydes and Ketones Common reducing agents and conditions: NaBH 4 ( sodium borohydride ) alcohol, ether, or H 2 O.

Synthesis of Alcohols Reduction of Aldehydes and Ketones Common reducing agents and conditions: NaBH 4 ( sodium borohydride ) alcohol, ether, or H 2 O.

CHEMICAL METHODS USED IN PURIFICATIONtraxanh.free.fr/Download/Purification_of_laboratory_chemicals/37617_02.pdf · 50 Chemical Methods used in Purification Sodium borohydride. This

CHEMICAL METHODS USED IN PURIFICATIONtraxanh.free.fr/Download/Purification_of_laboratory_chemicals/37617_02.pdf · 50 Chemical Methods used in Purification Sodium borohydride. This

Low Cost, Off-board Regeneration of Sodium Borohydride€¦ · Millenium Cell sodium borohydride for H2 storage project presentation for the 2004 Hydrogen, Fuel Cells & Infrastructure

Low Cost, Off-board Regeneration of Sodium Borohydride€¦ · Millenium Cell sodium borohydride for H2 storage project presentation for the 2004 Hydrogen, Fuel Cells & Infrastructure

Sodium Borohydride Production and Utilisation for Improved ...306237/s... · Sodium borohydride (NaBH4) has been the subject of extensive investigation as a potential hydrogen storage

Sodium Borohydride Production and Utilisation for Improved ...306237/s... · Sodium borohydride (NaBH4) has been the subject of extensive investigation as a potential hydrogen storage

Process for the Regeneration of Sodium Borate to …Process for the Regeneration of Sodium Borate to Sodium Borohydride for Use as a Hydrogen Storage Source Ying Wu Millennium Cell

Process for the Regeneration of Sodium Borate to …Process for the Regeneration of Sodium Borate to Sodium Borohydride for Use as a Hydrogen Storage Source Ying Wu Millennium Cell

SYNTHESIS OF MAGNESIUM HYDRIDE AND SODIUM BOROHYDRIDE …library.iyte.edu.tr/tezler/master/kimya/T000567.pdf · synthesis of magnesium hydride and sodium borohydride at low ... synthesis

SYNTHESIS OF MAGNESIUM HYDRIDE AND SODIUM BOROHYDRIDE …library.iyte.edu.tr/tezler/master/kimya/T000567.pdf · synthesis of magnesium hydride and sodium borohydride at low ... synthesis

Dyeing Wool with Metal-free Dyes The Use of Sodium Borohydride … › pdfs › 25004 › InTech-Dyeing_wool_with… · Vat dyes are amongst the oldest colouring materials used for

Dyeing Wool with Metal-free Dyes The Use of Sodium Borohydride … › pdfs › 25004 › InTech-Dyeing_wool_with… · Vat dyes are amongst the oldest colouring materials used for

Water Reactive Materials (WRs) · 2016. 2. 11. · 16940-66-2 Sodium borohydride pellets 2 Exhibit 1 7440-23-5 Sodium pieces in mineral oil 1 Exhibit 1 7440-23-5 sodium metal 1 Exhibit

Water Reactive Materials (WRs) · 2016. 2. 11. · 16940-66-2 Sodium borohydride pellets 2 Exhibit 1 7440-23-5 Sodium pieces in mineral oil 1 Exhibit 1 7440-23-5 sodium metal 1 Exhibit

Successive Loadings of Reactant in the Hydrogen Generation by … · 2019-07-15 · Successive Loadings of Reactant in the Hydrogen Generation by Hydrolysis of Sodium Borohydride

Successive Loadings of Reactant in the Hydrogen Generation by … · 2019-07-15 · Successive Loadings of Reactant in the Hydrogen Generation by Hydrolysis of Sodium Borohydride

SODIUM BOROHYDRIDE AS HYDROGEN CARRIER

SODIUM BOROHYDRIDE AS HYDROGEN CARRIER

Supporting Information Selective Reduction of Aldehydes ... · Supporting Information Selective Reduction of Aldehydes and Ketones to Alcohols with Ammonia ... (AB) using Sodium Borohydride

Supporting Information Selective Reduction of Aldehydes ... · Supporting Information Selective Reduction of Aldehydes and Ketones to Alcohols with Ammonia ... (AB) using Sodium Borohydride

ALDEHYDES AND KETONES - chemweb.calpoly.educhemweb.calpoly.edu/cbailey/BaileyText/SGpdf/Chapter11.pdf · E. Reduction to Alcohols with Sodium Borohydride ... cyclohexanone; (d) 4-bromo-2-pentanone

ALDEHYDES AND KETONES - chemweb.calpoly.educhemweb.calpoly.edu/cbailey/BaileyText/SGpdf/Chapter11.pdf · E. Reduction to Alcohols with Sodium Borohydride ... cyclohexanone; (d) 4-bromo-2-pentanone

Basic Organic Chemistry Laboratory Course The Synthesesreagenssi.kemia.helsinki.fi/nettilabra/tiedostot/introductory_course... · magnetically and add the sodium borohydride in small

Basic Organic Chemistry Laboratory Course The Synthesesreagenssi.kemia.helsinki.fi/nettilabra/tiedostot/introductory_course... · magnetically and add the sodium borohydride in small

Glionitrin B, a Cancer Invasion Inhibitory Diketopiperazine … · 2020. 1. 20. · Sodium borohydride (10 mg) in methanol (200 μL) and iodomethane (200 μL) were added successively,

Glionitrin B, a Cancer Invasion Inhibitory Diketopiperazine … · 2020. 1. 20. · Sodium borohydride (10 mg) in methanol (200 μL) and iodomethane (200 μL) were added successively,

Manufacturing of Sodium Borohydride (Sodium ... · Reducing agent for aldehydes, ketones and Schiff bases in no binary compound solvents. Also reduces acids, esters, acid chlorides,

Manufacturing of Sodium Borohydride (Sodium ... · Reducing agent for aldehydes, ketones and Schiff bases in no binary compound solvents. Also reduces acids, esters, acid chlorides,

Kinetics, Stereochemistry, and Mechanism of the Sodium Borohydride

Kinetics, Stereochemistry, and Mechanism of the Sodium Borohydride

Journal of Molecular Liquids - Pathpath.web.ua.pt/publications/j.molliq.2019.03.084.pdf · 264.6 mmol) was added to a stirred suspension of sodium borohydride (25.0 g, 661.5 mmol)

Journal of Molecular Liquids - Pathpath.web.ua.pt/publications/j.molliq.2019.03.084.pdf · 264.6 mmol) was added to a stirred suspension of sodium borohydride (25.0 g, 661.5 mmol)

Dynamics of Dihydrogen Bonding in Aqueous Solutions of Sodium Borohydride · 2015. 10. 13. · Sodium borohydride and sodium hydroxide were purchased from Fisher Scientific and used

Dynamics of Dihydrogen Bonding in Aqueous Solutions of Sodium Borohydride · 2015. 10. 13. · Sodium borohydride and sodium hydroxide were purchased from Fisher Scientific and used

Microscale Reduction of Cyclohexanone of... · Microscale Reduction of Cyclohexanone Read: Chapter 5 Chapter 7 (pipet filtering ... of the sodium borohydride solution dropwise while

Microscale Reduction of Cyclohexanone of... · Microscale Reduction of Cyclohexanone Read: Chapter 5 Chapter 7 (pipet filtering ... of the sodium borohydride solution dropwise while

Hydrogen Storage via Sodium Borohydride

Hydrogen Storage via Sodium Borohydride