EXECUTIVE SUMMARY OF HYDROGEOLOGIC INVESTIGATION OF ...
Transcript of EXECUTIVE SUMMARY OF HYDROGEOLOGIC INVESTIGATION OF ...
MEMO
Christian iVIatta (EPA) .Cynthia Weiss (EPA) Robert Asreen (DNREC)
Copies:
John Kindschuh Karen Burke Michael Teichnnan Joe Grillo File
SDMS DocID 2121921
_J
ARCADIS U.S., Inc
10 Friend Lane6 Terry
Drive_xOOOD_Suite 300
Newtown
Pennsylvania 18940
-Tel 267.685.1800 '
Fax 267.685.1801
Christopher Sharpe Darren Scillieri
October 29, 2010 ARCADIS Project No.:
NP000686.0001
Subject:
Executive Summary of Hydrogeologic Investigation of the Downward Migration Potential of Dissolved Solutes Present in the Columbia Aquifer to Reach the Manokin Aquifer i
On behalf of Merck and Co!, Inc. (Merck) and Mallinckrodt Veterinary, Inc. (Mallinckrodt), ARCADIS has
developed this memorandum to summarize the hydrogeologic evaluation conducted at the Millsboro TCE
Groundwater Contamination Site located in Millsboro, Delaware. The results of the evaluation were
presented to the Environmental Protection Agency (EPA), Delaware Department of Natural.Resources
and Environmental Control (DNREC), and Town of Millsboro public officials during the August 3, 2010
meeting. This memorandum has been expanded to include additipnal model simulations requested by the
Town of Millsboro to evaluate projected operation of the Millsboro Well field. As a follow-up to the August
S"* meeting, a copy of the presentation and data collected during the study were provided to the EPA and
DNREC on August 24*. Additionally, a memorandum providing the technical information requested by
DNREC, Division of Water Resources to facilitate acceptance of the Town's water allocations permit
application was provided to the Town of Millsboro on August 23, 2010.
Hydrogeologic Investigation
Th% scope of worksumlTiarizedirTthis^memd^wasconipleted in accordance with the final Hydrogeologic ^ Evaluation Workplan dated May 21, 2010. The initial workplan dated May 3, 2010 was conditionally approved by the EPA in their May 5, 2010 letter "pending comments contained therein being incorporated into a final Workplan. The EPA comments were addressed in the comment response letter dated May 13, 2010 and were subsequently incorporated into the final. Workplan dated May 21, 2010.
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The hydrogeologic evaluation was conducted to evaluate the hydraulic interaction of the Manokin Aquifer,
Bethany formation and Columbia Aquifer near the Millsboro Public Well field. The investigation activities
were completed to accomplish the following objectives:
Collect data to support analytical model construction
Monitor transient water levels under controlled pumping conditions
Define hydraulic parameters from pumping test results to expand and update existing model
Utilize the updated model to perform predictive analyses and develop recommendations
During the first two quarters of 2010 ARCADIS implemented a hydrogeologic study to assess the potential for dissolved solutes present in the Columbia Aquifer to reach the Manokin Aquifer. This investigation began with a review of the available site data as compiled by DNREC Site Investigation and Restoration Branch (SIRB). Tlje existing data provided detailed informafion about the Columbia Aquifer, the Town of Millsboro Well Field, and the existence of dissolved concentrations of trichloroethylene (TCE) and nitrate (a regional situation) in.shallow groundwater. A.reviewof the existing Site model indicated that an . expansion of the model was needed in order to properly evaluate the potential for downward migration.
To collect the data needed to expand the model a field program was implemented including monitoring well installation, groundwater sampling, and aquifer pump testing. Production Well PW-05, recently installed by the Town of Millsboro,'was selected as the extraction well for the aquifer pump test due to its location in W.B. Atkins Park, approximately 0.25 miles from the TCE plume. The field activities implemented during the hydrogeologic study are discussed in the following sections:
Monitoring Well Network
Fourteen observation wells were installed to supplement the three exisfing observation wells in the park
for the purpose of monitoring water levels in the vicinity of Millsboro Production Well PW-05. Five of the
new monitoring wells were completed in the Columbia Aquifer along two axes at distances between 120
feet (ft) and 900 ft from PW-05. Four wells were installed in a relafively high permeability zone of the
Bethany Formation, which at the Site is characterized as a leaky aquitard, although it becomes a viable
source of public water supply to the east of the Site. The remaining five wells were installed in the
Manokin Aquifer, the unit from which the Town of Millsboro intends to obtain nearly all of its drinking water.
Monitoring well locations are shown on Figure 1.
Monitoring wells completed in the Manokin aquifer were installed using rotosonic drillirig methodologies to
facilitate the collection of continuous soil cores. Monitoring well construction for wells completed in the
Bethany and Columbia formations were determined through interpretation of the soil cores collected
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during rotosonic drilling activities. Monitoring wells completed in the Columbia and Bethany formations were installed using mud rotary drilling techniques.- Each well installed (whether in the Columbia Aquifer, Bethany Formation, or Manokin Aquifer) was wholly screened in their respective targeted aquifer or formation. Wells were not screened across different aquifers or formations. Grout was injected into the annular space of the borehole using a tremie pipe to ensure a proper seal is installed to hydraulically isolate each well from the overlying and/or underlying aquifer/formation. Well constnjction logs are provided as Appendix A.
Following the completion of the wells, they were developed to ensure a good connection with the aquifer and therefore demonstrate an adequate response under aquifer pumping from the various production wells. Approximately two weeks after development, each of the wells were purged and sampled to verify the absence of VOC contaminafion in this area. Monitoring wells MW-16S and MW-16D were also sampled during the aquifer pump test to monitor groundwater quality during implementation of the pump test. During each sampling event groundwater samples were collected from the monitoring wells using low-flow sampling methods. Samples were preserved in the field and submitted to Shealy Environmental Services, Inc., located in West Columbia, South Carolina for analysis of VOCs by USEPA method 8260C. All wells were shown to be free from TCE. The analytical laboratory reports are provided electronically as At tachment ! . , .
Aquifer Testing
Upon successful demonstration of the lack of contamination in the newly installed monitoring wells, data logging pressure transducers (dataloggers) were installed to collect background water levels in the period leading up to the aquifer test. Approximately two weeks of data was collected before initiating the aquifer test at PW-05. The Town.of Millsboro initiated pumping of PW-05 on June 28, 2010 and continued operation over the course of the aquifer pump test through July 6, 2010. PW-05 was pumped at a rate of 500 gallons per minute (gpm) for the first four days and at 580 gpm for the next three days with well PW-01 running to supplement the water needs of the town. Water generated during the aquifer test was routed to the town's water treatment plant.
The pumping test data were used to evaluate the degree of vertical connection between the Columbia
Aquifer, Bethany Formation and Manokin Aquifer as well as to calculate hydraulic characterisfics of the
Manokin Aquifer. During the pumping test, measurable drawdown was observed in the Manokin aquifer
and the Bethany formation wells indicating a significant degree of leakage through the Bethany formation.
Modeling
The numerical model previously developed for the Site was updated and expanded to support simulation of the aquifer test and evaluation of predictive pumping scenarios as well as the evaluations of capture profiles under those pumping scenarios.
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The model boundaries were moved outward to nearby natural hydraulic boundaries resulting in an active
model slightly more than four square miles with a thickness of approximately 300feet.. Calibration testing
of the model produced a good match of both steady state and transient data indicating that the model
provided a good representation of the system behavior.
Once the model performance was established, several predictive scenarios were run to evaluate the
potential for vertical migration from the contaminated Columbia Aquifer down to the Manokin Aquifer.
These included: the existing operation of the Town of Millsboro well field; operation of the Columbia
aquifer wells with well PW-05; operation of the Columbia aquifer wells with wells PW-03 and PW.-05;
operation of all Manokin Aquifer wells at the capacity of the Town's water treatment system; and operation
of all Columbia and Manokin wells.
r The results ofthe numerical modeling indicated the following:
• Pumping of the Manokin Aquifer produces a rapid discernable response in the Bethany formation;
Pumping of wells PW-01 and PW-02 produce an enhanced upward flow of water from the Manokin Aquifer through the Bethany Formation to the Columbia Aquifer;
Increased pumping in the Manokin Aquifer progressively negates the beneficial upward gradient;
that naturally occurs and that is enhanced by pumping in PW-01 and PW-02; and
• ' Operation of PW-01 and PW-02 is required to control lateral and vertical plume migration.
Additional Simulations
At the meeting on August 3"* the Town of Millsboro and EPA requested that ARCADIS conduct additional
simulations to evaluate specific details of the projected operation the Millsboro Well field.
Specifically, Mr. Niblett from the Town of Millsboro requested that ARCADIS run the following scenarios: 600 gpm at PW-05; 200 gpm at PW-03 or PW-04; and pumping PW-01 and-PW-02 at a minimum level to maintain plume control, Mr. Niblett informed the participants at the August 3 * meeting that if Millsboro would be able to run the wells at these specified levels, Millsboro would have a sufficient amount of water for the near future.
In summary, ARCADIS was asked to conduct additional simulations for the following scenarios:
. 1. Interference Evaluation: evaluation of the operation of well PW-04 as a periodic replacement for well PW-03 thereby spreading the equipment use between wells PW-03 and PW-04.
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2. Minimum for Capture: evaluation of the minimum pumping rate of wells PW-01 and PW-02 required to maintain control of the plume; and
3. Reinjection: reinjection of the.water recovered by wells PW-01 and PW-02.
The above scenarios were simulated using the updated numerical model and the maximum extraction
rates for the Manokjn supply wells including a maximum extraction rate of 600 gpm at PW-05 and a
m'aximum extraction rate of 200 gpm at PW-03. A summary of the additional simulations including
assumed extraction rates, aquifer interaction analysis between the Bethany and Columbia formafions, and
simulated capture analysis for each of the three scenarios is provided as Appendix B.
The results of the additional simulafions indicated the following:
• Given the close proximity of PW-03 and PW-04 (within 125 feet of each other), wells PW-03 and PW-04 can be used interchangeably (one at a time) at a maximum rate of 200 gpm without altering the Columbia Aquifer groundwater flow direction;
• The minimum combined extraction rate from wells, F'W-01 and PW-02 required td maintain adequate control of the plume is betv/een 220 and 280 gpm, based on the mapped distribution of the plume; and '
• The predicted minimurh extraction rate between 220 and 280 gpm could be reinjected as near as the northwest corner of Atkins park without adversely impacting the upward flow fi-om the Manokin formation in the plume vicinity. . -
Recommendations
A reduction in pumping of the Columbia Aquifer (i.e., PW-01 and PW-02) risks a loss of the lateral and vertical migration control established under the present pumping scenario. The results ofthe hydrogeologic study and the numerical flow simulations indicate that pumping of the Manokin aquifer can be achieved with a reasonable degree of safety if pumping is carefully managed. Therefore, pumping of the Manokin Aquifer should be carefully managed with the maximum pumping rate at PW-05 limited to 600 gpm, and short term interrriittent pumping of wells PW-03 and PW-04 at a combined rate limited to 200 gpm. Importantly, wells PW-03 and PW-04 cannot be running at the same time. Wells PW-01 and PW-02 should operate at the current combined minimum rate of 280 gpm to balance the pumping from the Manokin Aquifer described above. Under this scenario the Town of Millsboro will not only be able to maintain plume control, but also will be able to provide a sufficient amount of water to accommodate public demand. This minimum rate should be re-evaluated as new data is obtained.
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Attachments: Figure 1: Well Location Map Appendix A; Well Construction Logs Appendix B: Supplemental Predictive Scenarios Attachment 1: Laboratory Analytical Reports
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Appendix A
Well Construcfion Logs
AR000221
Well Construction Log
LAND SURFACE
s
QBackfil l
I^Grout bentonite slurry (pressure injected)
6 inch diameter drilled noie
• Well casing,
2 inch diameter, PVC
77 ft*
80 ft*
"Well Screen. 2 inch diameter
0.02-slot PVC
/Qcrave l Pack
^—[x lsandPack^ #2 Sand
l l Formation Collaspse
90 tt*
90 ft*
Project Public Well TCE Site
Town/City Millsboro
Well r^W-11S
County Sussex State DE
Permit No. 231091 ; Land-Surface Elevation and Datum:
23.32 feet |x] Surveyed
Installation Date{s) 5/14/2010
Drilling Method
I I Estimated
Mud Rotary
Drilling Contractor Advanced Environmental Concepts
Drilling Fluid Water
Development Technique{s) and Date(s)
Surge and purge - 5/21/2010
Pumping Duration hours
Well Purpose Monitoring Well
Prepared by Dave Heuer
Depth Below Land Surface
AR000222
Well Construction Log
LAND SURFACE
I
£ ] Backfill
•(^Grout bentonite slurry. (pressure injected)
6 inch diameter dnlled hole
• Well casing,
2 inch diameter, PVC
120 ft*
122 ft*
"Well Screen. 2 inch diameter
PVC , • 0.02 slot
/Qc rave l Pack
iK. — 0 S a n d Pack " #2 Sand
[[Formation Collaspse
127 ft*
127 ft*
Project Public Well TCE Site
Town/City Millsboro
Well MW-11M
County Sussex State DE
Permit No. 231097
Land-Surface Elevation and Datum
23.05 feet [x] Surveyed
Installation Date(s). 5/13/2010
Drilling Method
I I Estimated
Mud Rotary
Drilling Contractor Advanced Environmental Concepts
Drilling Fluid. Water
Development Technique(syand Date(s)
Surge and purge - 5/24/2010
Pumping Duration hours
Well Purpose Monitoring Well
Prepared by Dave Heuer
Depth Below Land Surface
AR000223
Well Construction Log
LAND SURFACE
6 inch diameter dnlled hole
^ Well casing,
2 inch diameter,
PVC I
Q Backfill
'[xjcrout bentonite slurry (pressure injected)
77 ft*
80 ft*
"Well Screen. 2 inch diameter
PVC , 0.02 slot
/ Q c r a v e l Pack
K —[xlsand Pack #2 Sand
|_| Formation Collaspse
90 ft*
90 ft*
Project Public Well TCE Site Well MW-11S
Town/City Millsboro
County Sussex State DE
Permit No 231091
Land-Surface Elevation and Datum:
23.32 _feet [x] Surveyed
Installation Date(s) 5/14/2010
Drilling Method
r~| Estimated
Mud Rotary
Drilling Contractor Advanced Environmental Concepts
Drilling Fluid Water
Development Technique(s)and Date(s)
Surge and purge - 5/21/2010
Pumping Duration hours
Well Purpose Monitoring Well
Prepared by Dave Heuer
Depth Below Land Surface
AR000224
Well Construction Log
LAND SURFACE
6 inch diameter dnlled hole
• Well casing,
2 inch diameter, PVC
QBaokfill
[x]Grout bentonite slurry (pressure injected)
83 ft*
85 ft*
"Well Screen. 2 inch diameter
, PVC , 0.02 slot
/Qc rave l Pack
'( —[xlsand Pack #2 Sand
l l Formation Collaspse
95 ft*
95 ft*
Project . Public Well TCE Site _Wel l MW-12S
Tov^n/City Millsboro
County Sussex State DE
Permit No. 231093
Land-Surface Elevation and Datum:
26.21 feet [x] Surveyed
Installation Date(s) 5/19/2010
Drilling Method
r~| Estimated
Mud Rotary
• Drilling Contractor Advanced Environmental Concepts '
Drilling Fluid Water
Development Technique(s) and Date(s)
Surge and purge - 5/21/2010
Pumping Duration hours
Well Purpose Monitoring Well
. \
Prepared by , Dave Heuer
Depth Below Land Surface
AR000225
Well Construction Log
LWD SURFACE
b
Qsackf i l l
'I^Grout bentonite slurry (pressure injected)
6 inch diameter . dnlled hole
• Well casing.
2 inch diameter, PVC
127 ft*
129 ft*
"Well Screen. 2 inch diameter
PVC , 0.02 slot
/Qcrave l Pack
•( —[xlsand Pack #2 Sand
\ ~ l l Formation Collaspse
134 ft*
134 ft*
Project Public Well TCE Site Well MW-12M
Town/City Millsboro .
County Sussex State DE
Permit No. 231098
Land-Surface Elevation and Datum:
26^3 feet |x] Surveyed
Installation Date(s) 5/18/2010
Drilling Method
r~| Estimated
Mud Rotary
Drilling Contractor Advanced Environmental Concepts
Drilling Fluid Water ^
Development Technique(s) and Date(s)
Surge and purge - 5/21/2010
Pumping Duration hours
Well Purpose Monitoring Well
Prepared by Dave Heuer
Depth Below Land Surface
AR000226
Well Construction Log
LAND SURFACE
- Well casing,
2 inch diameter, PVC
/ / / L QBackfil l
I^Grout type I portland cement
/
= \
dnlled hole 6 inch diameter
203 ft*
Bentonite 206
#00 Sand 208 ft*
210 ft*
"Well Screen. 2 inch diameter
PVC , 0 02 slot
/ [^Gravel Pack
r.—|x]sandPack #2 Sand
l l Formation Collaspse
220 ft*
220 ft*
Project Public Well TCE Site Well MW-12D
Town/City Millsboro .
County Sussex (. State DE
Permit No. 231103
Land-Surface Elevation and Datum:
26.33 feet [x] Surveyed
Installation Date(s) 5/17/2010
Drilling Method
r~| Estimated
Rotosonic
Drilling Contractor
Drilling Fluid
Boarl Longyear
Water
Development Technique(s) and Date(s)
Surge and purge - 5/20/2010
Pumping Duration hours
Well Purpose Monitonng Well
Prepared by Dave Heuer
Depth Below Land Surface
AR000227
Well Construction Log
LAND SURFACE
S
6 inch diameter-drilled noie
^ Well casing,
2 inch diameter, PVC
Q Backfill
I^Grout bentonite slurry (pressure injected)
79 ft*.
82 ft*
"Well Screen. 2 inch diameter
PVC , 0.02 slot
Tl
Gravel Pack
'( —[TJsand Pack #2 Sand
Formation Collaspse
92 , ft*
92 ft*
• • ;
Project Public Well TCE Site Well MW-13S
Town/City Millsboro
County Sussex State DE
Permit No. 231094
Land-Surface Elevation and Datum:
) 23.69 feel [x] Surveyed
Installation Date(s) 5/20/2010
Drilling Method
r~| Estimated
Mud Rotary
Drilling Contractor Advanced Environmental Concepts
Drilling Fluid Water.
Development Technique(s) and Date(s)
Surge and purge - 5/24/2010
Pumping Duration hours
Well Purpose Monitoring Well
Prepared by Dave Heuer
Depth Below Land Surface
AR000228
Well Construction Log
LAND SURFACE
•[^Backfill
IxjGrout bentonite sluny (pressure injected)
•dniied hole
- Well casing,
6 inch diameter
2 inch diameter, PVC
117 ft*
119 ,ft*
"Well Screen. 2 inch diameter
PVC . 0.02 slot
/[|]Gravel Pack
^ —jxlsand Pack #2 Sand
Vi |_|Formation Collaspse
124 ft*
124 ft*
Project Public Well TCE Site Well MW-13M
Town/City Millsboro
County Sussex State DE
Permit No. 231099
Land-Surface Elevation and Datum:
23.51 feel [x] Surveyed
Installation Date(s) 5/17/2010
Drilling Method
[~| Estimated
Mud Rotary
Drilling Contractor Advanced Environmenlal Concepts
Drilling Fluid . Water
Development Technique(s) and Date(s)
Surge and purge - 5/24/2010
Pumping Duration 2 hours
Well Purpose Monitoring Well
Prepared by Dave Heuer
Depth Below Land Surface
AR000229
Well Construction Log
Fl / / / / / / / /
/ / 1
LAND SURFACE
/ /
i / /
• j" ] Backfill
[^Grout type I portland cement
204 ft*
\
drilled noie 6 inch diameter
Well casing,
2 inch diameter, PVC
Bentonite 206
#00 Sand 208 ft*
210 ft*
"Well Screen. 2 inch diameter
0.02 slot PVC
/[^Gravel Pack
•( —[xlsand Pack #2 Sand
V. l l Formation Collaspse
220 ft*
220 ft*
Project Public Well TCE Site Well MW-13D
Town/City Millsboro
County Sussex State DE
Permit No. 231101
Land-Surface Elevation and Datum:
23.54 feet [x] Surveyed^
Installation Date(s) 5/11/2010
Drilling Method
r~| Estimated
Rotosonic
Drilling Contractor Boarl Longyear
Drilling Fluid Water
Development Technique(s) and Date(s)
Surge and purge - 5/12/2010
Pumping Duration hours
Well Purpose . Monitoring Well
Prepared by V
Dave Heuer
* Depth Below Land Surface
AR000230
Well Construction Log
LAND SURFACE
Q Backfill
[xJCrout bentonite sluny • (pressure injected)
6 inch diameter drilled hole
• Well casing,
2 inch diameter. PVC
?6 ft*
60 ft*
"Well Screen. • 2 inch diameter
PVC , 0.02 slot
/ Q c r a v e l Pack
•( — R s a n d Pack #2 Sand
LJFormation Collaspse
90. ft*
90 ft*
Project Public Well TCE Site Well MW-14S
Town/City Millsboro
County Sussex State DE
Permit No. 231207
Land-Surface Elevation and Datum:
24.37 feet [x] Surveyed
Installation Date(s) 5/12/2010
Drilling Method
r~| Estimated
Mud Rotary
Drilling Contractor Advanced Environmental Concepts
Water ' Drilling Fluid r
Development Technique(s) and Date(s)
Surge and purge - 5/21/2010
Pumping Duration hours
Well Purpose Monitoring Well
Prepared by Dave Heuer
Depth Below Land Surface
AR000231
Well Construction Log
LAND SURFACE
£ ] Backfill .
•j^Grout bentonite slurry (pressure injected)
6 inch diameter drilled hole
• Well casing,
2 inch diameter, PVC
121 ft*
123 ft*
"Well Screen.-2 inch diameter
0.02 slot PVC
/Qc rave l Pack
•^—0Sand'Pack . #2 Sand
_ /^Formation Collaspse
128 ft*
128 ft*
Project Public Well TCE Site. Well MW-14M
Town/City Millsboro ' •
County Sussex State DE
Permit No. 231205
Land-Surface Elevation and Datum:
24.33 feet |x] Surveyed
Installation Date(s), 5/12/2010
Drilling Method
|~| Estimated
Mud Rotary
Drilling Contractor Advanced Environmental Concepts
Drilling Fluid Water
Development Technique(s) and Date(s)
Surge and purge - 5/21/2010
Pumping Duration hours
Well Purpose Monitoring Well
Prepared by Dave Heuer
Depth Below Land Surface
AR000232
Well Construction Log
Fl / / / / / / / /
/ / 1 I
LAND SURFACE
dnlled noie 6 inch diameter
• Well casing,
Fl / / / <
/ / / |~|Backfill
'[^Grout type I portland cement
/ 202.5 ft*
2 inch diameter, PVC
Bentonite 205.5
#00 Sand 207 ft*
210 ft*
^ , Well Screen. 2 inch diameter
0.02 slot PVC
/[^Gravel Pack
^ —[xlsand Pack #2 Sand
V i . l l Formation Collaspse
220 ft*
220 ft*
Project Public Well TCE Site ^ W e l l MW-14D
Town/City Millsboro •
County Sussex State DE
Permit No. 231206
Land-Surface Elevation and Datum:
24.52 feet [x] Surveyed
Installation Date(s) 5/7/2010
Drilling Method
I I Estimated
Rotosonic
Drilling Contractor Boart Longyear
Drilling Fluid ^ Water
Development Technique(s) and Date(s)
Surge and purge - 5/10/2010
Pumping Duration hours
Well Purpose Monitoring Well
Prepared by Dave Heuer
Depth Below Land Surface
AR000233
Well Construction Log
LAND SURFACE
6 inch diameter drilled noie
- Well casing,
2 inch diameter, PVC
Q Backfill
'I^Grout bentonite slurry (pressure injected)
81 ft*
83 ft*
"Well Screen. 2 inch diameter
PVC , 0.02 slot
/Qc rave l Pack
'( —[xlsand Pack #2 Sand
\ ~ l l Formation Collaspse
93 ft*
93 ft*
Project Public Well TCE Site
Town/City Millsboro
Well MW-16S
County Sussex State DE
Permit No. 231095
Land-Surface Elevation and Datum:
23.02 feet [x] Surveyed
Installation Date(s) 5/24/2010
Drilling Method
r~| Estimated
Mud Rotary
-Drilling Contractor Advanced Environmental Concepts
Drilling Fluid Water
Development Technique(s) and Date(s)
Surge and purge - 5/24/2010
Pumping Duration. 2 hours
Well Purpose Monitoring Well
Prepared by Dave Heuer
Depth Below Land Surface
AR000234
Well Construction Log
LAND SURFACE
i2
\
dniieo noie 6. inch diameter
• Well casing,
2 inch diameter, PVC
Backfill
'[^Grout type I portland cement
199 ft*
Bentonite
204 ft*
/ 208 fi*^
"Well Screen. 2 inch diameter
PVC , 0.02 slot
/ [ ]Gravel Pack
^ —jxjsand Pack • #2 Sand
^ ] Formation Collaspse ,
218 ft*
218 ft*
-Project Public Well TCE Site Well MW-16D
Town/City Millsboro
County Sussex State DE
Permit No. 231102
Land-Surface Elevation and Datum:
22.99 feet [x] Surveyed
Installation Date(s) 5/19/2010
Drilling Method
I I Estimated
Rotosonic
Drilling Contractor Boart Longyear
Drilling Fluid Water
Development Technique(s) and Date(s)
Surge and purge - 5/20/2010
Pumping Duration hours
Well Purpose Monitoring Well
Prepared by Dave Heuer
Depth Below Land Surface
AR000235
ARCADIS
Appendix B
AR000236
Supplemental Predictive Scenarios Extraction Rates (GPM)
',1
^S.1
wis
SCENARIO
. ' . i . ** : • Interference i^M:l • « * » -
SWi**-- , '^ V '^ -^ ,
mvy-1
• P " ^ " -
" Evalbatiori
Minimum for Capture;
Minimum for fe' -Capture with:?^!^. * Reinjection-!--
Current Pumping with Reinjection
14(3 'v.iT'
110
110.
140
^ iVV-2 f •••pW.a^*|""^^PW.41pPMif""5 I In jec t ion , •ti^-si,- if
miy. .'A?
110 200
.•r? S.t-^
0 600
, »tr r \ *^ j ,y , K^ViS*- t
140 200 0 600
NA
,220;
280
• W . i
« # • ' "
^ - J
7, " ]
Mi#»»'*?|^fe* •»-• • ; • • • ' • • • • • • ' ^ ' g i s i * ' - . " . . . . ^ * • . • • • . . : ; , . . . • : ' . • : • • • • •
RECOWMENHED PUMPING
Recommended l i n^
140 140 200 combined
rate (not to exceed)
600 NA
W;..---;iifi%i 'ii ii,-- rSyms'SifiKsassmmiiiin:^^ " i'miSiM»gagm.^ •wiaswvjjJMMj'gi. r—STrz. tr- .i v.:..:.: T*?'^ro»«ss^jggES"':^ ?!• !..^ai«g-B»>aM^g: .:...\.t„'c\,-'-:i'n-S'!Sei
M L \
ARCADIS
AR000237
• . . . ' : ' • " • ^ • _ • • c
JVIodel Prediction: Relative Head Upper Bethany and Lower Columbia (Interference Evaluation) Aquifer Interaction Analysis
iWelllD ^ n
PW-1
PW-2
:PW|^
PW-4
PW-5
. -.Mmm^ -
^•^IliS'?-''
F ate (GPM) ••, , : s s y f •"!
• • 1 : 4 ^
140
200
200
600
Difference in Heads (feet)'
^^^ . ^ rqo q^ ^ <^^ ^^ o u> ^v^ ^ ^^ <? <? >
Areas with
Downward' Flow
^s''^^
Areas with Upward Flow
0 ARCADIS
AR000238
Model Prediction: Relative Head Upper Bethany and Lower Columbia (Minimum for Capture) Aquifer Interaction Analysis
1
IWelllD
,iiSi.PW-1:-;.::;•#.
la^iiPM)!
-v^^v iC. !^
PW-2
''w-s,^^^^^. PW-4
110
'^•- 200
0
;;;fft;.tf.
^Mfcv.-
^^PW-5^ ^ + ,* * ^ ^ v '
" pa-^' '*"" ' ' * '™^*^
600 •'>• . - . >"'j,'A"--
* ^ ] ! -
V i t . , . .
Difference in Heads (feet)
v - ^ ^ ^ ^ - ^ ^ v v ^ v ' «?^^ Q^ ^ ^ ^ ^ ^ ^ o>^^ ^ ^ ' ^
Areas i with .
Downward Flow I
Areas with Upward Flow *-•• . • Aft-
^S'SffeT;'
e ARCADIS
AR000239
Model Prediction: Relative Head Upper Bethany and Lower Columbia (Minimum for Capture with Reinjection) Aquifer Interaction Analysis
^ • . • - I K * / .
•mNeWiD
mPSf\l-^
PW-2
PW-4
INJ-1
INJ-2
i - i -
a:.-. • ' tR '
• - ^ • f g ; ' ^ - ^ , - . .
^ ^ ' • ' t^..
Rate{GPM|
110
200
0
600 .
110
.110
^ ^ j g ^ ' ^ - ' g ^ y ^ Difference in Heads (feet)
v^^^v-^^-^ v^ v^^^^ o^ ^^ ^^ ^^ ^ V ^
Areas with
Downward Flow .
Areas with Upward Flow
I
A ^ . -
. i : ^ t . m k • . » « ^ f t k . ^ i - t •"'.:•!
^ARCADIS
AR000240
Model Prediction: Relative Head Upper Bethany and Lower Columbia (Current Pumping with Reinjection) Aquifer Interaction Analysis
JAd-
P W - 5 • ' . • 1 % ^ . , •,
Rate^(GPM
140
140
^ i - » : . .
> ^ i -'T^wr 200^
0
; J , « i — t , - . —
140 - ' - I M l iO: 5%r-L- , .%«S> INI -?- -•• ' ^ t V , . •»"<v. l 40''-
V.-. ^"1jrfUSuu.i
. ' 1
Difference in Heads (feet)
V ^ J - ^ V - ^ ^ - ^ V ^ V ' , 9 ^ ^ <?^ / ^ ^ ^ ^ ^ o> J-,^ ^ V ^ ^
Areas with
Downward' Flow
Areas with Upward Flow
5 i<V
j^'^'-..y.
ARCADIS
AR000241
Model Prediction: Capture of Lower Columbia Aquifer Water (Interference Evaluation) Predictive Capture Analysis
wkwmi PW-1
PW-2
iRatipSM);:*'^
t» -K pw-a A..: - . , i ? i ^Wl^ ' (Jf-'> H^t- 'Vi^. ' ' ' •
PW-4
nJ^dsJiPk. . H 4^ A - r f ^ A *
140^::
140
.20dVi ^
200
6O|0lS.>
Capture Legend
n PW-1
.. H PW-2
• PW-3,
PW-4
PW-5
-10—
PVv'-1
e
/33
ni^
\^#l? 's'Cf
LEGEND
Simulated Water Levels (ft msl)
Extraction Well
Simulated Groundwater Particle Flow within the Plume
. . ^ - • • • ' • ' • • " : ^ - ^ m ^ S S t
i^ t i^ . -^X"^
^„,'2rai,.,;:.S&.,A.,'. >., .„.a>,^
ARCADIS
AR000242
Model Prediction: Capture of Lower Columbia Aquifer Water (Minimum for Capture) Predictive Capture Analysis
i/VilPID. m^mmiGPrn-^ f
1% l l i i';-^&-\!'. '•Ml. 'JK
' .'.l- " i^
PW-2
PW-3
PW-4
^4. PW-5.t K ^ l l l ^ , ..^^'•Z 'w>. -.Si^feh. ^'U.'Sa:^ - : # 1 ' ^ " ' •• .*-'a-«
110
20¥ 0
600^ ^'S^^^iii^^r^^ •,i;f*- V - ? ^ - 4 J \ I \ . - *• ••%r=*> y-^^-- . • t% «i>i«;«;.\^u*/
™ j - ,
'.1
i*"'i
Capture Legend
• PW-1
S PW-2
[ 3 PW-3
M PW-4
0 PW-5
5>,> ti
-10-
e
LEGEND
Simulated Water Levels (fl msl}
Extraction Well
Simulated Groundwater Particle Flow within the Plume
-^
S, t* i^^t , f%
:s.
ARCADIS
AR000243
Model Prediction: Capture of Lower Columbia Aquifer Water (Minimum for Capture with Reinjection) Predictive Capture Analysis
Well ID
Mm ;«.'S'J?V«
^ ^ ^ '
^™*.„:i:'^ .-..-'_ , ,i.s."
fiatfe m m
110
0
110
. H PW-3
• PW-4
O'PW-S
I!^p "Ty4'''i".^'"
-10-
PW-1
e
LEGEND
Simulated Water Levels {ft msl)
Extraction Well
Simulated Groundwater Pairticle Flow within the Plume
—IT*
©ARCADIS
AR000244
Model Prediction: Capture of Lower Columbia Aquifer Water (Current Pumping with Reinjection) Predictive Capture Analysis
Wei Iii D; RatefSClpiii
.•^•*^1'40 p W
1 ARCADIS
AR000245
ARCAD/S
^^tachmenti
Lafaoi
-s^s:sr
AR000246
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
ARCADIS 6 Terry Drive
Suite 300 Newtown, PA 18940
Attention: Darren Scillieri
Project Name; Millsboro TCE
Project Number:NP000686
- LotNumber:LG03004
Date Completed:07/07/2010
Nisreen Saikaly
Project Manager
This report shall not be reproduced, except In its entirety, without the written approval of Shealy Environmental Services, Inc. ^ , •
The following non-paginated documents are considered part of this report; Chain of Custody Record and Sample Receipt Checklist.
• c •
Shealy Environmental Services. Inc. Page: 1 of 19 106 Vantage Point Drive West Columbia, SO 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com Level i Report v2. i
AR000247
SHEALY ENVIRONMENTAL SERVICES, INC. SCDHEC No: 32010 NELAC No: E87653 NC DEHNR No: 329
Case Narrative^ ARCADIS
Lot Number: LG03004
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the \ Shealy Environrnental Services, Inc. ("Shealy") Quality Assurance Managennent Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Shealy Environmental Services. Inc. Page: 2 of 19. 106 Vantage Point Drive West Columbia, SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com Level i Report v2 1
AR000248
SHEALY ENVIRONMENTAL SERVICES, INC. 1
y
Sample Number
001
002
003
004
(4 samples)
Sample ID
MW-16S070210RM
MW-16D070210RM
FIELD BLANK
TRIP BLANK
s •
Sample Summary ARCADIS
Lot Number: LG03004
Matrix
Aqueous
Aqueous
. Aqueous
Aqueous
Date Sampled
07/02/2010 0815
07/02/2010 0930
. 07/02/2010 0950
07/02/2010
Date Received
07/03/2010 ^
07/03/2010
07/03/2010
07/03/2010
Shealy Environmental Services, Inc. . , 106 Vantage Point Drive West Columbia, SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 3 of 19 Level 1 Report v2 1
AR000249
SHEALY ENVIRONMENTAL SERVICES, INC.
(1 detection)
Executive Summary ARCADIS
Lot Number: LG03004
Sample Sample ID
004 TRIPBLANK^
tl/latrix
Aqueous
Parameter
Bromoform
Method
8260B
Result
1.5
Q
J
Units
ug/L
Page.,
11
L
Shealy Environmental Services, Inc. , . . 106 Vantage Point Drive West Columbia, SO 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab com
Page: 4 of 19 Level 1 Report v2.1
AR000250
Client: ARCADIS
Description: MW-16 S070210 RM
Date Sampled:07/02/2010 0815
Date Received: 07/03/2010
Volatile Organic Compounds by GC/MS / Laboratory ID: LG03004-001
Matrix: Aqueous
Run 1
Prep Method 5030B
Analytical Method Dilution Analysis Date Analyst Prep Date Batch 8260B 1 07/07/2010 0050 DLB 37143
Parameter CAS
Number
Analyt ical
Method Result ' PQL MDL Units Run
Acetone
•Benzene
Bromodichloromethane ,
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethan6 (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane .
1.2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dlchloroethene
, trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1.3-Dichloropropene
trans-1.3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,2,4-Trichloroben2ene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
67-64-1
71-43-2
75-27-4
75-25-2
74.83-9
78-93-3
. 75-15-0
56-23-5
108-90-7
75-00-3
67-66-3 •
74-87-3
110-82-7
96-12-8
124-48-1
106-93-4
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
1.0061-01-5
10061-02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
108-10-1
108-87-2
75-09-2
100-42-5
. 79-34-5
127-18-4
108-88-3
76-13-1
120-82-1
71-55-6
79-00-5
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B 8260B
8260B
8260B
8260B
8260B
8260B ,'
8260B
8260B
8260B _
82608
8260B
8260B
82608
8260B•
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
82608
' 8260B
8260B
8260B
8260B
ND
ND
ND ^
ND
ND
ND
ND
ND
. ND
ND
ND
ND
ND
ND
ND
ND.
ND
ND .
ND
ND
ND-
ND
ND
ND
-ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND '
ND
. ND
ND
ND
ND
ND
ND
ND
ND
20
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0 .
10
5.0
5.0
5.0
. 5 . 0
5.0
5.0
5.0
5.0
. 5.0
5.0
6.7
0.20
1.7
0.40
0.80
1.8
0.30 0.40
1.7
0.50^
1.7
0.30
0.98
, 0.60
1.7
0.30
1.7
1.7
1.7
0.20
0.30
0.30
0.50
0.20
0.40
0.30
0.30
0.30 '
1.7
1.0
1 .0 '
0.72
0.40
0.80
0.95
1.7
0.10
0.40
0.40
1.7
0.30
1.7
0.20
0.30
ug/L 1
ug/L 1
ug/L 1
ug/L 1
. ug/L . 1
ug/L 1
ug/L 1
ug/\l 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L • 1
ug/L 1
ug/L 1
• ug/L 1
ug/L 1
• ug/L 1
ug/L 1
• ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L • 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1 1
ug/L . 1
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on <
B = Detected in the method blank
J = Estimated result < PQL and > MDL
dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GO columns exceeds 40%
N = Recovery is out oi alteria H = Out of holding lime
Shealy Environmental Services. Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803) 791-9700 Fax (803) 791-9111 wvAv.shealyiab.com
Page: 5 of 19 Level 1 Report v2.1
AR000251
Client: ARCADIS
Description: MW-16 S070210 RM
Date Sampled:07/02/2010 0815
Date Received:07/03/2010
Volatile Organic Compounds by GC/MS Laboratory ID: LG03004-001
Matrix: Aqueous
R u n
1 P r e p M e t h o d
5 0 3 0 8
A n a l y t i c a l M e t h o d
8260B
D i l u t i o n A n a l y s i s D a t e
1 07/07/2010 0050 A n a l y s t
D L B
P r e p D a t e B a t c h
3 7 1 4 3
P a r a m e t e r C A S
N u m b e r
A n a l y t i c a l
M e t h o d R e s u l t P Q L M D L U n i t s R u n
Tr i ch lo roe thene
T r i ch lo ro f l uo romethane
Viny l ch lor ide
Xy lenes (total)
S u r r o g a t e
79-01-6
75-69-4
75-01-4
1330-20-7
8260B
8260B
8260B
8260B
ND
' ND
ND
ND
5.0
5.0
2.0'
5.0
0.30
0.30
0.10
1.7
ug/L
ug/L '
ug/L
ug/L
1
1
1
1
R u n 1 A c c e p t a n c e % R e c o v e r y L i m i t s
1 ,2-D ich loroethane-d4
B r o m o f l u o r o b e n z e n e
To luene -d8
81
76
81
7 0 - 1 3 0
7 0 - 1 3 0
70 -130
B = Detected in the method blank , )
PQL = Practical quantitation limit
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where appficabte. ail soil sample analysis are reported on a dry weight basis unless flagged with a "W
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 wwv/.shealylab.com
P a g e : 6 o f 19 Level 1 Report v2.1..
AR000252
Client: ARCADIS
Description: MW-16 D070210 RM
Date Sampled :07/02/2010 0930
Date Received:07/03/2010
Volatile Organic Compounds by GC/MS Laboratory ID: LG03004-002 ^
^ Matrix: Aqueous
•
Run 1
Prep Method 50308
Analytical Method 8260B
Dilution Analysis Date 1 07/07/2010 0111
Analyst DLB
Prep Date Batch 37143
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-8utanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene , '
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobehzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
•1,1-Dichloroethane .
1.2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1.2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloroprope'ne i
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,2-Trichlpro-1,2,2-Trifluoroethane
1,2,4-Trichlorobenzene
1.1,1-Trichloroethane
1,1,2-Trichloroethane
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5'
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8,
124-48-1 106-93-4
95-50-1
541-73-1
106-46-7
;. 75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
108-10-1
108-87-2
75-09-2
100-42-5
79-34-5 127-18-4 ,
' 108-88-3
76-13-1
120-82-1
71-55-6
79-o'o-5
8260B
8260B
^82608
82608 .
8260B
82608
82608
8260B
82608
82608
82608
82608
82608
8260B
82608
8260B
82608
8260B
82608
82608
82608
8260B ,
82608
^ 8260B
82608
82608
82608
8260B
8260B
82608
82608
82608 .
82608
8260B
8260B
82608
82608
82608
8260B
8260B
82608
8260B
82608
82608
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
. ND
ND
ND
ND
ND •
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
• ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
20
5.0
5.0
5.0
5.0 •
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0 5.0
5.0
5.0
5.0
5.0
• 5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
6.7
0.20
1.7
O.fO
0.80
1.8
0.30
0.40
1.7
0.50
1.7
0.30
o:98
0.60
1.7
0.30
1-7 1.7 •
1.7
0.20
0.30
0^30
0.50
0.20
0.40
0.30
0.30
0.30
1.7
1.0
1.0
0.72
0.40
0.80
0.95
1-7 0.10
0.40
0.40
1-7
0.30-
1.7
0.20
0.30
ug/L 1
ug/L • 1
ug/L 1
ug/L 1
ug/L 1
lig/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L i
ug/L 1
ug/L. 1
ug/L 1
• ug/L 1
ug/L 1
ug/L 1
ug/L .1
ug/L . 1
ug/L ' 1
ug/L 1
ug/L y 1
- ug/L 1
ug/L 1
ug/L 1
ug/L . 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
u'g/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L . 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L . 1
ug/L 1
ug/L 1
PQL = Practical quantitation limit ^ B = Detected in the method blank
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" ,
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 .Fax (803) 791-9111 -www.shealylab.com
Page; 7 of 19 Level 1 Report v2.1
AR000253
Volatile Organic Compounds by GC/MS Client: ARCADIS
Description: MW-16 D070210 RM
Date Sampled:07/02/2010 0930
Date Received:07/03/2010 • ,
Laboratory ID: LG03004-002
Matrix: Aqueous
Run 1
Prep Method 50308
Analyt ical Method 82608
Dilution 1
Analysis Date 07/07/2010 0111
Analyst DLB
Prep Date Batch 37143
Parameter CAS
Number
Analyt ical Result PQL MDL Units Run
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
79-01-6
75-69-4
75-01-4
1330-20-7
8260B
82608
82608
82608
ND
ND'
ND
ND
5.0
5.0
2.0
5.0
0.30
0.30
0.10 •
1.7
ug/L
ug/L
ug/L
ug/L
1
1
1
1
Run 1 Acceptance % Recovery Limits
1,2-Dichloroethane-d4
Bromofluorobenzene
.Toluene-d8
104 99 105
70-130 70-130 70-130
PQL = Practical quantitation limit B = Detected in the method blank
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria , H = Out of holding time
Shealy Environmental Seivices, Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803) 791-9700 Fax (803) 791-9111 • www.shealylab.com
Page; 8 of 19 Level 1 Report v2.1
AR000254
Volatile Organic Compounds by GC/MS Client: ARCADIS
Description: FIELD BLANK
Date Sampled:07/02/2010 0950
Date Received:07/03/2010
Laboratory ID: LG03004-003
Matrix: Aqueous
Run 1
Prep Method 50308
Analytical Method Dilution 'Analysis Date Analyst 8260B 1 07/07/2010 0133 DLB
Prep Date Batch 37143
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene-
1.3-Dichlorobenzene
1,4-DichlDrobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
l.l-Dichloroethene
cis-1,2-Dlctiloroethene -,
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1.3-Dichloropropene
Ethylbenzene
2rl-lexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2.2-Tetrachloroethane
Tetrachlproethene
Toluene
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,2,4-Trichlorobenzene
1,1,1 -Trichloroethane
1,1,2-Trichloroethane
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1 106-93-4
• 95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2 75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4
591-78-6
98-82-8
79-20-9~^
1634-04-4
108-10-1
108-87-2
75-09-2
100-42-5
79-34-5;.
127-18-4'
108-88-3
76-13-1
120-82-1
71-55-6
79-00^5
82608
8260B
82608
82608
82608
82608
82608 .
82608
82608
82608
82608
82608
8260B
. 82608
82608
82608
82608
8260B
82608
82608
'8260B
82608
82608
, 82608 •
82608
82608
8260B
'8260B"
8260B
82608
( 82608
82608
82608
82608
82608
82608 •
8260B
82608
82608
82608
82608
82608
82608
8260B
ND
ND .
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
_ND
ND
ND
ND
ND
ND
ND
ND ND
. ND
ND
ND .
ND
ND
ND
ND
ND
ND
ND'
, ND
ND
ND
ND
ND
ND
ND
ND
• ND
ND
ND
20
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
.5.0
• 5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0 •
5.0
5.6 10
5.0
5.0
5.0
5.0
. 5.0
5.0
5.0
^ 5° 5.0
5.0
6.7
0.20
1.7 .
0.40
0.80
1.8
0.30
0.40
1.7
0.50
1 1.7
0.30
0.98
0.60
• 1.7
0.30
. 1.7 •
1.7
1.7
0.20
0.30
0.30
0.50
0.20
0.40
0.30
0.30
0.30
1.7
1.0
1.0
• 0.72
0.40
0.80
0.95
1.7
0,10
0.40
0.40
1.7
0.30
1.7
0.20
0.30
ug/L 1
ug/L 1
ug/L 1
ug/L • 1
ug/L 1
ug/L • ' 1
ug/L 1
ug/L . 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L. 1
ug/L 1
ug/L 1
ug/L 1
• ug/L 1
ug/L 1
ug/L 1
ug/L • 1
ug/L 1
ug/L 1
ug/L • 1
ug/L 1
. ug/L • 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank
ND = Not detected at or above the MDL . J = Estimated result < PQL and > MDL ^
Where applicable, ail soil sample analysis are reported on a dry weight basis unless flagged with a "W
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services. Inc. -106 Vantage Point Drive West Columbia. SC 29172 (803) 791-9700 Fax (803) 791-9111 vww.shealylab.com
Page: 9 of 19 Level 1 Report v2.1
AR000255
Client: ARCADIS
Description: FIELD BLANK
Date Sampled:07/02/2010 0950
Date Received:07/03/2010 '
Volatile Organic Compounds by GC/MS Laboratory ID: LG03064-O03
Matrix: Aqueous
Run 1
Prep Method 5030B
Analyt ical Method Dilution Analysis Date Analyst 82608 1 . 07/07/2010 0133 DLB
Prep Date Batch 37143
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
.Xylenes (total)
Surrogate {
79-01-6
75-69-4
75-01-4
1330-20-7
8260B
82608
82608
82608
ND
ND
ND
ND
5.0
5.0
2.0
5.0
0.30
0.30
0.10
1.7
ug/L
ug/L'
ug/L
ug/L
1
1
1
1
Run 1 Acceptance % Recovery Limits
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
103 100 107
70-130 70-130 70-130
PQL = Practical quantitation limit B = Detected in the method blank
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 Fa"x (803) 791-9111 Vkww.shealylab.com
Page: 10 of 19 . Level 1 Report v2.1
AR000256
(
Client: ARCADIS
Description: TRIP BLANK
Date Sampled:07/02/2010
Date Received:07/03/2010
Volatile Organic Compounds by GC/MS Laboratory ID: LG03004-004
Matrix: Aqueous
^
Run 1
Prep Method 50308
Analytical Method 8260B
Dilut ion Analysis Date 1 07/07/2010 0154
Analyst DLB
Prep Date Batch 37143
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Acetone
Benzene
Bromodichloromethane '
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlproethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane '
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,2,4-Trichlorobenzene
1,1,17Trichloroethane
1,1,2-Trichloroethane
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
,96-12-8 •
124-48-1
106-93-4
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2 75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
. 100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
108-10-1
108-87-2
75-09-2
100-42-5
79-34-5 127-18-4
108-88-3
76-13-1
120-82-1
71-55-6
79-00-5
82608 '
8280B
82608 ^
B260B
82608
82608-
, 82608
82608
82608
82608
82608
82608
82608
82608
82608
8260B
8260B
82608 ,
82608
8260B
82608
82608
82608 .
8260B
82608
82608
82608
82608
8260B
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608 .
8260B
82608
82608
ND
ND
ND
1-5
ND
ND
ND ND
ND
ND
ND
ND'
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND ND
ND
ND
ND
ND
r ND
ND
ND
ND
•• N D
ND
ND
• ND
ND
ND
' N D
ND
ND
ND
ND
ND
ND
20
5.0
5.0
J 5.0
5.0
10
5.0
5.0
5.0
5.0
•5.0
5.0
5.0
. 5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0 5.0
5.0
5.0
5.0
5.0
5.0 V
5.0
10
5.0
5.0
5.Ci
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
6.7
0.20
1.7
0.40
0.80
1.8
0.30
0.40
1.7
0.50
1.7
0:30
0.98
0.60
1.7
0.30
1.7
1.7
1.7
0.20
0.30
0.30
0.50
0.20
0.40
0.30
0.30
0.30
1.7
1.0
1.0
0.72 .
0.40
0.80
0.95
1:7
0.10
0.40
0.40
1.7
0.30
1.7
0.20
0.30
ug/L . 1
ug/L ^ 1
ug/L 1
ug/L 1
ug/L • 1
ug/L 1
ug/L 1
ug/L 1
ug/L . , 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L . 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
. ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L . 1
ug/L 1
ug/L 1
ug/L 1
ug/L . 1
ug/L 1
ug/L 1
PQL = Practical quantitation limit • B = Detected in the metriod blank ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "V^
E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria . H = Out of holding time '
Shealy Envirortmental Services. Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 11 of 19 Level 1 Report v2.1
AR000257
Client: ARCADIS
Description: TRIP BLANK
Date Sampled:07/02/2010
Date Received: 07/03/2010
Volatile Organic Compounds by GC/MS Laboratory ID: LG03004-004
Matrix: Aqueous
) . • •
Run Prep Method 1 50308
Analytical Method 82608
Dilution Analysis Date Analyst 1 07/07/2010 0154 DLB
Prep Date Batch 37143
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
79-01-6
75-69-4
75-01-4
1330-20-7
82608
82608 .
82608
8260B
ND
ND
ND
ND
5.0
5.0
2.0
5.0
0.30
0.30 .
0.10
1.7
ug/L
ug/L
ug/L
ug/L
1
1
1
1
'. Run 1 Acceptance % Recovery Limits
1,2-Dichloroethane-d4
Bromofluorobenzene Toluene-d8
106
100 109
70-130 70-130 70-130
N
PQL = Practical quantitation limit B = Detected in the method blank
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services. Inc. 106 Vantage Point Drive West Columbia, SC. 29172 (803)791-9700 Fax (803) 791-9111 wvw.shealyiab.com
Page: 12 of 19 Level 1 Report v2.1
AR000258
QC Summary
Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 .'Fax (803) 791-9111 vrtvw.shealylab.com
Page: 13 of 19 Level 1 Report v2.1
AR000259
Volatile Organic Compounds by GC/MS - MB
Sample ID; LQ37143-001
Batch: 37143
Analyt ical Method: 8260B
Matrix: Aqueous
Prep Method: 50308
Parameter Result Dil PQL MDL Units Analysis Date
L
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
' 2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methylchloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,3-bichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
1 •,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pehtanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
ND' ND
20
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
6.7
0.20
1.7
0.40
0.80
1.8
0.30
0.40
, 1.7
0.50
1.7
0.30
0.98
0.60
1.7
0.30
1.7
1.7
1.7
0.20 -
0.30
0.30,
0.50
0.40
0.20
0.30
0.30
0.30
17. 1.0
1.0
0.72
0.40
0.80
0.95
1.7
0.10
0.40
0.40
1.7 . 0.30
1.7
0.20
0.30
ug/L .
ug/L
ug/L
ug/L
'ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L '
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L •
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L -
ug/L
ug/L
ug/L
ug/L
07/06/2010 2325
07/06/20102325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
' 07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/()6/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/(36/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40%
ND = Not detected at or above the MDL J = Estimated result < PQL and i MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
N - Recovery is out of criteria
+ - RPD is out of critena
Shealy Environmental Services. Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 vww.shealylab.com
Page: 14 of 19 Level 1 Report v2.1
AR000260
Volatile Organic Compounds by GC/MS - MB
Sample ID: LQ37143-001
Batch: 37143
Analyt ical Method: 82608
Matrix: Aqueous
Prep Method: 50308
Parameter Result Dil PQL MDL Units Analysis Date
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
ND
ND
ND
ND
Q % Rec
103
103
109
1
1
1
1.
Acceptance Limit
70-130
70-130
70-130
5.0
5.0
2.0 .
5.0
0.30
0.30*
. 0.10
1-7
ug/L
ug/L
ug/L
ug/L
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
07/06/2010 2325
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40%
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged v^th a "W
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
. N - Recovery is out of criteria
+ - RPD is out of criteria
Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 15 of 19 Level 1 Report v2.1
AR000261
Volatile Organic Compounds by GC/MS - LCS
Sample ID: LQ37143-002
Batch: 37143
Analyt ical Method: 82608
Matrix: Aqueous
Prep Method: . 5030B
Parameter
Spike Amount
(ug/L) Result (ug/L) Dil % Rec
% Rec Limit Analysis Date
Acetone
Benzene
Bromodichloromethane
Bromoforrn
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbpn tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1;1-Dichloroethene
trans-1,2-Dictiloroethene
cis-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloro6thane
Tetrachloroethene
Toluene
1,1,2-Trichloro-1,2,2-Trifluoroethane
1.2,4-Trichlorobenzene
1,1,1 -Trichloroethane
1,1,2-Trlchloroethane
100
50,
50
50
50
100
50 •
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
50
50
100
50
50
50
50
50
50
50
50
50
50
110
46
49
43
45
92
53
49
47
48
44
51
48
43
45
50
46
48
45
52
43
44
44
46
45
. 4 3 •
47
47
48
99
48
50
44
100
52
• 44
52
47
49
47
50
49
46
47
1 .,
113
91
97 1
87
90
92
106
97
93
96
88
103
97
85
89
100
91
96
91.
104
85
89-
: 88
91
90
87 -
95
95
96
99
96
99
88
104
104
88
104
95
98
94
100
98
9 2 ^
94
46-153
72-127
71-143
65-131
36-168
60-140
60-140
37-166
78-129
42-163
63-123
20-158
70-130
70-130
74-134
70-130
70-130
70-130
70-130
10-158
69-132
59-143
50-132
70-130-
70-130
'71-126
69-130
73-131
79-132
60-140
70-130
15-128
70-130
60-140
70-130
69-129
70-130
60-155
70-130
75-125
' 70-130
70-130
77-132
77-132
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157!
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
, 07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40%
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reporied on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
N - Recovery is out of criteria
+ - RPD IS out of criteria
Shealy Environmental Services, Inc. 106 Vantage Point Drive' West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 www;shealylab.com
Page: 16 of 19 Level 1 Report v2.1
AR000262
Volatile Organic Compounds by GC/MS - LCS
Sample ID:
Batch:
Analyt ical Method:
Parameter
Trichloroethene
LQ37143-002
37143
82608
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
Bromofluorobenzene
1.2-Dichloroethane-d4
Toluene-d8
Spike Amount (ug/L)
50
. 50
50
100
Q % Rec
106
109 ,
113
Result (ug/L) ' Q
46
48
50
98
Acceptance Limit
70-130
70-130
70-130
Prep
\
Matrix:
Method:
Dil
1
1
1
1
Aqueous'
5030B
-
% Rec
92
96
100
98
% Rec Limi t
73-124
41-173
29-159
70-130
Analysis Date
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
07/06/2010 2157
PQL = Practical quantitation limit ' . P = The RPD between two GC columns exceeds 40%
ND = Not detected at or above the MDL J = Estimated result <• PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" • • • \
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
N - Recovery Is out of critena
+ - RPD is out of cnteria
Shealy Environmental Services, Inc. ' ' 106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 viww.shealylab.com
Page: 17 of 19 Level 1 Report v2.1
AR000263
Volatile Organic Compounds by GC/MS - LCSD
Sample ID: LQ37143-003
Batch: 37143
Analyt ical Method: 8260B
) Parameter
Spike Amount
(ug/L)
V
Result (ug/L) Q
Matrix: Aqueous
Prep Method: 5030B
Dil % Rec % RPD % Rec Limit
% RPD Limit Analysis Date
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2^Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibrorrio-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichldroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene -•
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE) ,
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1;2-Trichloro-1,2,2-Trifluoroethane
1,2;4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
100
50
50
50
50.
100
50
50
50
50
50
50
50
50
50
50
50
50
50 *
50
50
50
50
50
50
50
50 '
50
50
100
50
50
50
100
50 .
50
50
50
50
50
50
50
50
50
100
46
47
43
48
90
/ 52 46
46
48
44
49
45
40
44
51
45
46
45
45
42
42
43
, 45
• 45
43
47
47
47
96
47
46
44
98
4 8 ,
44
50
47
48
45
46
47
43
46
1 \
105
91
95
86
96
90 "
105 91
91
•96
87
98
90
, .8° 87
102
89
92
90
89
85
85
. 86
89
89
87
94
. 9 4
94
96
93 •
92
88
98
95
•88
101
95
96
. 91
93
94
87
92
7.9
0.17
2.9
0.88
7.0
2.1
. 1.2
6.6
1.9
0.41
1.3
4.5
7.5
6.4
2.2
2.1
2.1
4.2
1.3
15
0.41
4.4
2.5 .
2.6
0.74
0.053
1.2
0.58
,2.3
3.1^
2.7
7.1
0.16
5.1
8.8
0.31
2.9
0.14
2.3
3.0
7.8
4.0
5.5
1.4
46-153
72-127
71-143
65-131
36-168
60-140
60-140
37-166
78-129
42-163
63-123
20-158
70-130
70-130
74-134
70-130
70-130
70-130
70-130
10-158
69-132
59-143
50-132
70-130
70-130
71-126
69-130
73-131
79-132
60-140
70-130
15-128
70-130
60-140
70-130
69-129
70-130
60-155
70-130
75-125
70-130
70-130
77-132
77-132
20
20
- 20
20
20
20
20
20
20
. 20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
.20
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
20 " 07/06/2010 2219
20
20
20
20
20
20
20
20
20
• 20
20
20
20
20
20
20
20
20
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
PQL = Pradical quantitation limit P = The RPD between two GC coluhins exceeds 40%
ND = Not detected at or aljove the MDL J ^.Estimated result < PQL and >.MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
N - Recovery is out of criteria
+ - RPD is out of cnteria
Shealy Environmental Services. Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 18 of 19 Level 1 Report v2.1
AR000264
Volatile Organic Compounds by GC/MS - LCSD
Sample ID: LQ37143-'o03
Batch: 37143
Analyt ical Method: 82608
Parameter
Trichloroethene
Trichlorofluoromethane ;
Vinyl chloride
Xylenes (total)
Surrogate
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8-
Spike Amount
(ug/L)
50
50
50
100
Q % Rec
103
104
113
Result (ug/L)
45
43
47
95
Q
'
Acceptance Limit
70-130
70-130
70-130
Prep
Dil
1
1
1
1
Matrix:
Method:
Aqueous
50308
% Rec % RPD
91
86
94
95
1.1
11
6.8
2.5
% Rec Limit
73-124
41-173
29-159
70-130
% RPD Limit
20
20
20
20
V
Analysis Date
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
07/06/2010 2219
-
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40%
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Wtiere applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
N - Recovery is out of criteria
+ - RPD is out of criteria
Shealy Environmental Services, Inc. ^ 106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page:19 of 19 Level 1 Report v2.1
AR000265
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AR000266
SHEALY ENVIRONMENTAL SERVICES, INC.
r. / : : : M t ^ ^ L
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^ l . ; : I ' . : . . ' j j ; . ,:"-!r;it.t): K i ;h;- :..;>i K;'
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Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 vrtvw.shealylab.com Level 1 Report v2 1
AR000267
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
ARCADIS I 6 Terry Drive;
Suite 300 Newtown, PA 18940
Attention: Christopher Stiarpe
Project Name: Millsboro TCE
Project Number:NP000686
Lot Number:LF04059
Date Completed:06/16/2010
Nisreen Saikaly
) Project Manager
" : . ""^^
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Shealy Environmental Services, Inc. " . 106 Vantage Point Drive' West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 vmw.shealylab.com
Page: 1 of 23 Level 1 Report v2.1
AR000268
SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010 . NELAC No: E87653 , NC DEHNR No: 329
Case Narrative ARCADIS
Lot Number: LF04059
This Report of Analysis contains the analytical resultts) for thesample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date Is documented iri the header information associated with each sample.
Sample receipt, sample analysis, and data review have'been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating,procedures (SOPs), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results.page or discussed below. ,
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page,
Volatile Organic Compounds
The LCS recovery for 1,1,1-Trichloroethane was outside method control limits in batch 35826. The LCSD results were within limits. Therefore the
associated sample results were reported and no corrective action was required.
Shealy Environmental Services, Inc. , ' Page: 2 of 23 106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 vww.shealylab.com Level i Report v2 1
AR000269
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary ARCADIS
Lot Number: LF04059
Sample Number Sample ID Matrix Date Sampled Date Received
001
002
003
004
005
006
MW-16S060310
MW-BAPD060310
MW-16D060310
MW-1APD060310
FB-060310
TRip Blank
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
06/03/2010 1000
06/03/2010 1330
06/03/2010 1030
06/03/2010 1335
0'6/d3/2010 1350
06/02/2010
06/04/2010
06/04/2010
06/04/2010
06/04/2010
06/04/2010
06/04/2010
(6 samples)
Shealy Environmental Services, Inc. • 106 Vantage Point Drive WestColumbia.SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 3 of 23 Level 1 Report v2.1
AR000270
SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary ARCADIS
Lot Number: LF04059
Sample Sample ID Matrix Parameter Method Result Q Units Page
(0 detections):
Shealy Environmental Services, Inc Page: 4 of 23 106 Vantage Point Drive West Columbia, SC 29172 (803)791-9700 Fax (803) 791-9111 vww.sheaiylab.com Level! Report v2. i
AR000271
Client: ARCADIS
Description: MW-16S080310
Date Sampled:06/03/2010 1000
Date Received: 06/04/2010
Volatile Organic Compounds by GC/IVIS
Laboratory ID: LF04059-001
Matrix: Aqueous '
, .
Run Prep Method 1 5030B
Analytical Method 8260B
Dilution Analysis Date 1 06/15/2010 1837
Analyst LBS
Prep Date Batch 35826
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
' Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride) -
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichtoropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,'2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,2-Trichioro-1,2,2-Trifluoroethane
1,2,4-Trichlorobenzene
1,1,1 -Trichloroetharie
1,1,2-Trichloroethane
67-64-1
71-43-2
, 75-27-4
75-25-2
74-83-9
78-93-3
75-15-0 56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1 106-93-4
95-50-1
541-73-1
106-46-7 .
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
108-10-1
108-87-2
75-09-2
100-42-5
79-34-5
127-18-4
108-88-3
76-13-1
120-82-1
71-55-6'
79-00-5
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B.
82608
8260B
8260B -
8260B
8260B
8260B
8260B-
8260B .
8260B ,
8260B
8260B
ND
ND
ND
ND
ND
ND
, ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND .
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
20
5.0
5.0
.5.0
5.0
10
5.0
5.0
5,0 -
5.0
5.0
5.0'
5.0
5.0
5.0 5.0
.5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
- 5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
6.7
0.20
1.7
0.40
0.80
1.8
1 0.30
0.40
1.7
0.50
• 1.7
0.30
0.98
o:6o 1.7
0.30
1.7.
1.7
1.7
0.20
0.30
0.30
0.50
0.20
0.40
0.30
0.30
0.30
1.7
1.0
1.0
0.72
0.40
0.80
0.95
1.7
0.10
0.40
0.40
1.7
0.30
1.7
0.20
0.30
ug/L. 1
ug/L 1
ug/L 1
ug/L 1
.. ug/L .1
ug/L 1
.ug/L . 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L ' 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L .. 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L . 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L, • 1
ug/L . 1
.' ug/L • 1
ug/L 1
ug/L 1
ug/L 1
iJg/L 1
ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out ot criteria H = Out of holding time
^\\eB\'^ Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 \AWW.shealylab.com
Page: 5 of 23 Level 1 Report v2.1
AR000272
Client:ARCADiS
Description: MW-16S060310
Date Sampled:06/03/2010 1000
Date Received: 06/04/2010 ,
Volatile Organic Compounds by GC/MS ' - Laboratory ID: LF04059-001
Matrix: Aqueous
-
' • J
Run 1
Prep Method 5030B
Analytical Method 8260B
Dilution Analysis Date Analyst 1 06/15/2010 1837 LBS
Prep Date Batch 35826
Parameter CAS
Number
Analyt ical
Method Result P Q L M D L Units R u n
Trichloroethene
Trichloroflupromethane
Vinyl chloride
Xylenes (total)
Surrogate
79-01-6
75-69-4
75-01-4
1330-20-7
8260B .
8260B
8260B
8260B
ND
ND
ND
ND
5.0 .
5.0
2.0
5.0
0.30
0.30
0.10
1.7
ug/L
ug/L
ug/L
ug/L
1
1
1
.1
Run 1 Acceptance % Recovery Limits
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
124 103 106
70-130 70-130
• 70-130
PQL = Practical quantitation limit ,, B = Detected in the method blank
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria ^ H = Out of holding time
Shealy Environmental Services, Inc. 106 Vantage Point Drive. West Columbia, SC 29172 (803)791-9700 • Fax (803) 791-9111 www.shealylab.com
. 1 •
P a g e : 6 o f 23 Level 1 Report v2.1
AR000273
Volatile Organic Compounds by GC/MS Client: ARCADIS
Description: MW-BAPD060310
Date Sampled:06/03/2010 1330
Date Received:06/04/2010
Laboratory ID: LF04059-002
Matrix: Aqueous
Run 1
Prep Method 5030B
Analyt ical Method 8260B
Dilution Analysis Date 1 06/15/2010 1858
Analyst LBS
Prep Date Batch 35826
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane'(Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1.3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene-
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
• 78-93-3
75-15:0
56-23-5
., 108-90-7
75-00-3 .
67-66-3
74-87-3
110-82-7'
96-12-8
124-48-1 106-93-4
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
• 78-87-5
10061-01-5
10061-02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
108-10-1
108-87-2
75-09-2
100-42-5
79-34-5 127-18-4
108-88-3
-'76-13-1 ' _
120-82-1
71-55-6
79-00-5
8260B
8260B ' ,
8260B
8260B
8260B
8260B
8260B
82eOB
8260B
8260B •
8260B
8260B
8260B '
8260B
8260B '•
8260B
8260B ,
8260B
8260B
8260B
8260 B
'8260B 8260B
- 8260B
8260B
8260B
82606
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
._8260B
8260B
8260B
e260B .
82606-
8260B
8260B
8260B
ND
ND
ND
ND
ND
- ND
ND
ND
ND
ND ,
ND
ND
ND
ND
ND ND
ND
^ ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND 1
ND
ND
ND " •
ND
ND
ND
ND
ND
ND
ND
- - ND •
ND
ND
ND
20
5.0
5.0
5.0 .
5.0
10
- 5.0
5.0
5.0
'5.0
5.0
5.0
5.0
5.0
5.0 5.0
5.0
5.0
5.0
5.0
5.0"
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
' 5.0
5.0
5.0
5.0
-5:0 '
5.0
5.0
5.0
6.7
0.20
1.7
0 4 0
0.80
1.8
0.30 .
0.40
1.7
0.50
1.7
0:30
0.98
0.60,
1.7
0.30
1.7
1.7
1.7.
0.20
0.30
. '0.30
0.50
0.20
0.40
0.30
0.30
0.30
1.7
1.0
1.0
0.72
. 0.40
0.80,
0.95
1.7
0.10
0.40 -
0.40
1.7
0.30
1.7
0.20
0.30
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
, ug/L 1
ug/L 1
ug/L 1
ug/L 1
, ug/L 1 ug/L 1
ug/L . 1
ug/L 1
ug/L 1
ug/L 1
ug/L • 1
ug/L " 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L • ' 1
ug/L 1
- ug/L 1
^ ug/L . 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L- • 1
ug/L 1
ug/L 1
ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank ND = Not detected at or above the MDL J = Estimated result < PQL and ; MDL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged witil a "W
E = Quantitation of compound exceeded the calibration range P = The RPD tjetween two GC columns exceeds 40% N = Recovery is out ot criteria H = Out of holding time
Shealy Environmental Services. Inc. 106 Vantage Point Drive WestColumbia.SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 7 of 23 Level V Report v2.1
AR000274
Volatile Organic Compounds by GC/MS ClienLARCADIS
Description: MW-BAPD060310
Date Sampled:06/03/2010 1330
Date Received:06/04/2010
Run Prep Method 1 5030B
Parameter
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
Analytics
• \
1 Method 8260B
Q
Dilution Analysis Date 1 06/15/2010 1858
'
Analyst LBS
CAS Analyt ical
Number Method
79-01-6
75-69-4
75-01-4
1330-20-7
Run 1 Acceptance % Recovery Limits
127 7 0 - 1 3 0 - ^
104 70-130
104 70-130
8260B
8260B
8260B
8260B
Prep Date
Result
ND
ND
ND
ND
Laboratory ID
Matrix:
Batch 35826
Q PQL
5.0
5.0
2.0
5.0 .
LF04059-002
Aqueous
MDL
0.30
0.30
0.10
1.7
Units
ug/L
ug/L
ug/L
ug/L
Run
1
1
1 ,
' 1 .
PQL = Practical quantitation limit B = Detected in the method blank
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services, Inc. 106 Vantage Point Drive WestColumbia.SC 29172 (803)791-9700 Fax (803) 791-9111 vww.shealylab.com
Page: 8 of 23 Level 1 Report v2.1
AR000275
Client: ARCADIS
Description: MW-16D060310
Date Sampled:06/03/2010 1030
Date Received:06/04/2010
Volatile Organic Compounds by GC/MS Laboratory ID: LF04059-003
Matrix: Aqueous
Run Prep Method 1 - 5030B
Analyt ical Method 8260B
Dilution Analysis Date 1 06/15/2010 1921
Analyst LBS
Prep Date Batch 35826
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
I Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride .
Chlorobenzene
Chloroethane
Chloroform .
Chloromethane (Methyl chloride)
Cyclohexane
1,2"-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane c
1,1,2-Trichloroethane
67-64-1
• 71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
' 75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1 106-93-4
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2 75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
108-10-1
108-87-2
75-09-2
100-42-5
79-34-5 127-18-4
108-88-3
76-13-1 •
120-82-1
71-55-6
79-00-5
8260B
8260B
8260B
8260B
8260B
8260B
8260B 8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B 8260B
8260B
8260B
8260B .
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
826PB
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B .
8260B
8260B
8260B
8260B
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND ( l,ND
ND
ND
ND
ND
ND
ND
ND
. ND
ND
ND '
ND
20
5:0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0 •
5.0
5.0
5.0
5.0
5.0
5.0
5.0 •
5.0 -5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
.. 5.0 '•
-- 5.0
5.0
5.0
6.7
0.20
1.7
0.40
0.80
1.8
0.30
0.40
1.7
0.50
1.7
0.30
0.98
0.60
1.7 0.30
1.7
1.7
1.7
0.20
0.30
0.30
0.50
0.20
0.40 .
0.30
0.30
0.30
1.7
1.0
1.0
0.72
0.40
0.80
0.95
1.7
0.10
0.40 '
0.40
1.7
0.30
.1.7
0.20
0.30
' ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L , 1
ug/L ' 1 ug/L 1
ug/L 1
ug/L 1
.ug/L 1
ug/L 1
ug/L 1
• ug/L 1
ug/L • 1
ug/L 1
ug/L 1
ug/L .1
ug/L 1
ug/L 1
ug/L . 1
ug/L 1
ug/L • 1
ug/L 1
ug/L .1
ug/L 1
. ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L . 1
ug/L J
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
•ug/L 1
ug/L 1
ug/L 1
ug/L 1
PQL = Practical quantitation limit B = Detected in the method biani<
ND = Not detected at or above the MDL J = Estimated result < PQL and > f^DL
V^here applicable, all soli sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services. Inc. 106 Vantage Point Drive West Columbia" SC 29172 (803)791-9700 Fax (803)791-9111 www.shealylab.com
Page: 9 of 23 Level 1 Report v2.1
AR000276
Client:ARCADIS
Description: MW-16D060310
Date Sampled:06/03/2010 1030
Date Received:06/04/2010
Volatile Organic Compounds by GC/MS Laboratoiy ID: LF04059-003
Matrix: Aqueous
. - . •
Run 1
Prep Method 5030B
Analytical Method 8260B
Dilution Analysis Date 1 06/15/2010 1921
Analyst LBS
Prep Date Batch 35826
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Trichloroethene
Trichlorofluoromethane
Vinyl chloride '
Xylenes (total)
Surrogate
79-01-6
75-69-4
75-01-4
1330-20-7
8260B
8260B
8260B
8260B
ND
ND
ND
ND
5.0
5.0
2.0
5.0.
0.30
0.30
0.10
1.7
ug/L
ug/L
ug/L
ug/L
1
1
1
. 1
Run 1 Acceptance % Recovery Limits
1,2-Dicliloroethane-d4
Bromofluorobenzene
Toluene-d8
127
103
102
70-130
70-130
70-130
PQL = Practical quantitation limit B = Detected in the method blank
ND = Not detected at or above the MDL J = Estimated result < PQL and MDL
Where applicable,.all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range
, P = The RPD tietween two GC columns exceeds 40%
N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services. Inc. 106 Vantage Point Drive WestColumbia.SC 29172 (803)791-9700 Fax (803) 791-9111 wviw.shealylab.com
Page:10 of 23 Level 1 Report v2.1
AR000277
, Client: ARCADIS
Description: MW-1APD060310
Date Sampled:06/03/2010 1335
Date Received: 06/04/2010
Volatile Organic Compounds by GC/MS Laboratory ID: LF04059-004
, Matrix: Aqueous
Run 1
Prep Method 5030B
Analyt ical Method 8260B
Dilution Analysis Date 1 06/15/2010 1942
Analyst LBS
Prep Date Batch 35826
Parameter CAS Analyt ical
Number Method Result PQL MDL Units Run
Acetone
Benzene .
Bromodichloromethane ^
Bromoform
Bromomethane (Methyl bromide)
2~Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-bibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-pichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichl6ropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3 .
74-87-3 .
110-82-7
96-12-8
124-48-1
106-93-4
95-50-1 •
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4
/ 591-78-6
98-82-8
79-20-9
1634-04-4
108-10-1
108-87-2
75-09-2
100-42-5
79-34-5
127-18-4^
108-88-3
76-13-1
120-82-1
71-55-6
79-00-5
8260B
8260B.
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B '
8260B
(_ 8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
ND
ND
ND
ND
ND
ND
ND
ND
ND .
ND
ND
ND
ND
ND
'ND
ND
ND
ND
ND
ND
' ND
ND
ND
ND
ND
ND .
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
20
5.0
• 5.0
5.0
5.0
10 5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0.
5.0
5.0
5.0
5.0
, 5 . 0
5.0
5.0
5.0
5.0
5:0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0,
5.0 •
5.0
5.0
5.0
5.0
5.0 .
5.0
5.0 .
5.0
6.7
0.20
1.7
0.40
0.80
1.8
0.30
0.40
1.7
0.50
1.7
0.30
0.98
0.60
1.7
0.30
1.7
1.7
1.7
0.20
0.30
0.30
0.50
0.20
0.40
0.30
0.30
0.30
1.7
1.0
1.0
0.72
0.40
0.80
• 0.95
1.7
0.10
0.40
0.40
1.7
0.30
1-7 0.20
0.30 '
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1 ug/L 1
ug/L 1
ug/L 1
ug/L 1
. ug/L 1
• ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L . 1
ug/L 1
ug/L 1
ug/L 1
• ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
, ug/L 1
ug/L 1
ug/L 1
ug/L . 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L ,1
ug/L 1
ug/L • 1
ug/L 1
ug/L 1
ug/L' 1
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a
B = Detected in the method blank
J = Estimated result < PQL and > MDL
dry weight basis unless flagged with a "W
, E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria H = Out of holding time
Shealy Environniental Services. Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803) 791-9700 Fax (803) 791-9.111 v/ww.shealylab.com
Page: 11 of 23 Level 1 Report v2 1
AR000278
Client: ARCADIS
Description: MW-1APD060310
Date Sampled:06/03/2010 1335
Date Received: 06/04/2010
Volatile Organic Compounds by GC/MS Laboratory ID: LF04059-004
Matrix: Aqueous
Run Prep Method 1 5030B
Analyt ical Method 8260B
Dilution Analysis Date Analyst 1 06/15/2010 1942 LBS
Prep Date Batch 35826
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
79-01-6
75-69-4
75-01-4
1330-20-7
8260B
8260B
8260B
8260B .
ND
ND .
ND
ND
5.0
5.0
2.0
,5.0
- 0.30
0.30
, " OJO
V 1.7
ug/L
ug/L-
ug/L
ug/L
1
1
1
1
Run 1 Acceptance % Recovery Limits
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
126 102 107
70-130 70-130 70-130
PQL = Practical quantitation limit B = Detected in the method blank
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, atl soil sample analysis are reported on a dry weight basis unless flagged with a ' W
E = Quantitation of compound exceeded the caJibration range
P = The RPD t>etween two GC columns exceeds 40%
N = Recovery is out of criteria • H = Out of holding time
Shealy Environmental Services, Inc. .106 Vantage Point Drive WestColumbia.SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 12 of 23 Level 1 Report v2.i
AR000279
Client: ARCADIS
• Description: FB-060310
Date Sampled:06/03/2010 1350
Date Received: 06/04/2010
Volatile Organic Compounds by GC/MS , Laboratory ID: LF04059-005
. Matrix: Aqueous
•
Run 1
Prep Method 5030B
Analyt ical Method 8260B
Dilution Analysis Date Analyst 1 06/15/2010 2004 LBS
Prep Date Batch 35826
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Acetone
Benzene
Bromodichloromethane
Bromoform
- Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethen6
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1.3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate . •
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene.
1,1,2-Trichloro-.1,2,2-Trifluoroethane
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
67-64-1
71-43-2
75-27-4
75-25,-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1
'106-93-4
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4 .
591-78-6
98-82-8
, 79-20-9
1634-04-4
108-10-1
108-87-2
75-09-2
100-42-5
79-34-5
127-18-4
108-88-3
76-13-1
120-82-1
71-55-6
79-00-5
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B'
8260B
8260B
'8260B
8260B
8260B
8260B
8260B
8260B
8260B
ND
ND
ND
ND
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
. N D '
ND
ND
ND
ND •
ND
ND
ND
ND
ND
ND
ND
1 ND
ND
ND
ND
ND
ND
ND
ND
ND ,
ND .
ND
ND
ND
ND
ND
ND
20
. 5 . 0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0 '
5.0
5.0'
5.0
5.0
. 5.0
5.0
5.0
5.0
• 5.0 5.0
/ • 5.0
5.0
5.0
5.0
5;o 5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0 5.0
5.0
5.0.
5.0
5.0 .
• 5.0
6-7
0.20
1.7
0.40
0.80
. 1.8 '
0.30 0.40'
1.7
0.50
1'.7
0.30
0.98
' 0.60
1.7
0.30
1.7
1.7
1.7
0.20
0.30
0.30
0.50
0.20
0.40
0.30
0.30
0.30
1.7
1.0
1.0
0.72
0.40
0.80
0.95
1.7
0.10
0.40 0.40
1.7
0.30
1.7 •
0.20
0.30
ug/L
ug/L
"ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L .
ug/L
ug/L
ug/L
ug/L
ug/L .
ug/L
ug/L :
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
• • ug /L
. ug/L
ug/L
ug/L
ug/L
ug/L
• ug /L
ug/L
ug/L
ug /L
ug /L
ug/L .
ug/L
ug/L
ug /L
ug/L
ug /L
ug /L .
\ 1
-1
PQL = Practical quantitation limit B = Detected in the mettiod blank
ND = Not detected at or alrave the MDL ' J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless nagged with a "W
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services. Inc. 1C6 Vantage Point Drive WestColumbia.SC 29172 (803)791-9700 Fax (803)791-9111 www.shealylab.com
Page: 13 of 23 Level 1 Report v2.1
AR000280
Volatile Organic Compounds by GC/MS Client:ARCADIS
Description: FB-060310
Date Sampled:06/03/2010 1350
Date Received:06/04/2010
Laboratory ID: LF04059-005
Matrix: Aqueous
Run Prep Method 1 5030B
Analyt ical Method Dilution Analysis Date Analyst .8260B 1 06/15/2010 2004 LBS
Prep Date Batch 35826
Parameter CAS
Number
Analyt ical
Method ' Result PQL MDL Units Run
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate -
79-01-6 .
75-69-4
75-01-4
1330-20-7
8260B
8260B
8260B
8260B
ND
ND
ND
ND
5.0
5.0
2.0
5.0
0.30 .
0.30
,0 .10
1.7
ug/L
ug/L
ug/L
ug/L
1
1
1
1
Run 1 Acceptance % Recovery Limits
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
127
104
108
70-130
70-130
70-130
PQL = Practicai quantitation limit B = Detected in the method blank ND = Not delected at or above the MDL ' J = Estimated result < PQL and > MDL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range P = The RPD tjetween r*o GC columns exceeds 40% N = Recovery is out of criteria H = Out of tiolding time
Shealy Environmental Services. Inc. 106 Vantage Point Drive WestColumbia.SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 14 of 23 Level 1 Report v2.1
AR000281
Volatile Organic Compounds by GC/MS Client: ARCADIS
Description: TRip Blank
Date Sampled:06/02/2010
Date Received: 06/04/2010
Laboratory ID: LF04059-006 (
Matrix: Aqueous
Run 1
Prep Method 5030B
Analytical Method 8260B
Dilution Analysis Date 1 06/15/2010 2026
Analyst LBS
Prep Date Batch 35826
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Acetone
Benzene >
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloroprbpane (DBCP)
• Dibromochloromethane
1,2-Dibromoethane (EDB) ,
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
. 1,1-bichloroethane_
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1.2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-l-lexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene ^ .
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,2-Trichloro-1^2,2-Trifluoroethane
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
^
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1
106-93-4
95-50-1
541-73-1
106-46-7
75-71-8'
,75-34-3
107-06-2
75-35-4 '
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
' 108-10-1
• 108-87-2
75-09-2
100-42-5
79-34-5
127-18-4
108-88-3
76-13-1
120-82-1
71-55-6
79-00-5
8260B
8260B
. 8260B
, 8260B
8260B-
8260B
8260B
8260B .
8260B
8260B
8260B
8260B
8260B
8 2 6 0 B '
8260 B
8260B
8260B 8260B
8260B
8260B
8260B
8260B
8260B
8260B •
8260B
8260B
8260B
8260B
8260B
^ 8260B
8260B
8260B
8260B
' 8260B
8260B
8260B
8260B
8260B
8260B
826tJB
8260B •
8260B
8260B
8260B
ND
ND '
ND
ND
ND
ND
ND
ND ,
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND'
ND
ND
ND
IMD ND
ND
ND
• ND
ND
ND
ND
20
' 5.0
5.0
• 5.0
5.0
10
5.0
5.0
,- 5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
s.p • 5.0
5.0.
. 5.0
5.0
5.0-
"5.0
5.0
5.0
10
\ 5.0
5.0
5.0
10
5.0
5.0
5.0
5.0 5.0
5.0.
• "5.0
5.0
5.0 .
5.0
6.7
0.20
1.7
0.40
0.80
i;8
0.30 0.40
I.."?
0.50
1.7
0.30
0.98.
0.60.
1.7 .
0.30
1.7
1.7
1.7
0.20
o.3o; 0.30
I 0.50
0.20
0.40
0.30
0.30
0.30
1.7
1.0
. 1.0
0.72
0.40
0.80
0.95
(• 1.7
0.10
0.40
0.40
1.7
•"0.30 '
• 1.7
0.20
0.30
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L • 1
ug/L 1
ug/L 1 ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
.ug/L. . . 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L • 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L^ • 1
ug/L. 1
ug/L 1
ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services, Inc.
106 Vantage Point Drive WestColumbia.SC 29172' (803)791-9700 Fax (803)791-9111 vrtvw.shealylab.com
Page: 15 of 23 Level 1 Report v2.1
AR000282
Client: ARCADIS
Description: TRip Blank
Date Sampled:06/02/2010
Date Received:06/04/2010
Volatile Organic Compounds by GC/MS Laboratory ID: LF04059-006
Matrix: Aqueous ' ^
• _ .
Run Prep Method Analyt ical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B 1 06/15/2010 2026. LBS 35826 • .
CAS Analyt ical Parameter Number Method Result Q PQL MDL Units Run
Trichloroethene
Trichlorofluoromethane [
Vinyl chloride .
Xylenes (total) '
Run 1 Acceptance Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8 '
79-01-6
75-69-4
75-01-4
1330-20-7
8260B
8260B
8260B
8260B
ND
ND
ND
ND
5.0
5.0
2.0
5.0
0.30'
0.30
0.10
1.7
ug/L
ug/L
ug/L
ug/L
1
1
1
1
127 103 107
70-130 70-130 70-130
POL = Practical quantitation limit B = Detected in ttie method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the MDL . J = Estimated result < PQL and ; MDL P = The RPD betv/een two GC columns exceeds 40% Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W N = Recovery is out of criteria H = Out of holding time
Shealy Environmenlal Services. Inc . ' Page: 16 of 23 106 Vantage Point Drive West Columbia, SC 29172 (803)791-9700 Fax (803) 791-9111 wviw.shealylab.com Level i Report v2 1
AR000283
QC Summary
Shealy Environmental Services. Inc. Page: 17 of 23 ^ 106 Vantage Point Drive West Columbia. SC 29172 .(803)791-9700 Fax (803) 791-9111 vmw.shealylab.com . Level i Report v2.l
AR000284
Volatile Organic Compounds by GC/MS - MB
Sample ID: LQ35826-001
Batch: 35826
Analyt ical Method: 8260B
Matrix: Aqueous
Prep Method: 5030B
Parameter Result Dil PQL MDL Units Analysis Date
Acetone ND
Benzene ND
Bromodichloromethane ND
Bromoform . ND
Bromomethane (Methyl bromide) ND
2-Butanotie (MEK) ND
Carbon disulfide ND
Carbon tetrachloride ~ ND
Chlorobenzene ND
Chloroethane ' ND
Chloroform ND
Chloromethane (Methyl chloride) ND
Cyclohexane ' ND
1,2-Dibromo-3-chloropropane (DBCP) ND
Dibromochloromethane ND
1,2-Dibromoethane (EDB) ND
1,4-Dichlorobenzene ' ND
1,3-Dichlorobenzehe ND
1,2-Dichlorobenzene ND
Dichlorodifluoromethane ND
1,2-Dichloroethane ND
1,1-Dichloroethane ND
trans-l,2-Dichloroethene ND
cis-1,2-Dichloroethene ND
1,1-Dichl6roethene ND
1,2-Dichloropropane ND
trans-1,3-Dichl6ropropene ND
cis-1,3-Dichloropropene ND
Ethylbenzene ND
2-Hexanone ND
Isopropylbenzene ND
Methyl acetate ND
Methyl tertiary butyl ether (MTBE) ND
4-Methyl-2-pentanone ND^
Methylcyclohexane ND
Methylene chloride ND
Styrene ' ND
1,1,2,2-Tetrachloroethane ND
Tetrachloroethene ND
Toluene ND
1,1,2-Trichloro-1,2,2-Trifluoroethane ND
1,2,4-Trichlorobenzene ND
1,1,2-Trichloroethano ND
1,1,1-Trichloroethane ND
20
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0-
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
6.7
0.20
1.7
0.40
0.80
1.8
0.30
0.40
1.7
0.50
1.7
0.30
0.98
0.60
1.7
0.30
1.7
1.7
1.7
0.20
0.30
0.30
0.40
0.20
0.50
0.30
0.30
0.30
1.7
1.0
1.0
0.72
0.40
0.80
0.95
1.7
0.10
0.40
0.40 1.7 0.30 1.7 0.3Ci 0.20
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L .
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L ^
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L •
ug/L
ug/L '
ug/L
ug/L
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010'1426(
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
.06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
^ 06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/20101426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
PQL = Practical quantitation limit P = TheiRPD between two GC columns exceeds 40%
ND = Not detected at or above the MDL J = Estimated result < PQL and ^MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
N - Recovery Is out of criteria
+ - RPD is out of criteria
Shealy Environmental Services. Inc. 106 Vantage Point Drive West Columbia, SC 29172. (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 18 of 23 Level 1 Report v2.1
AR000285
Volatile Organic Compounds by GC/MS - MB
Sample ID: LQ35826-001
Batch: 35826
Analyt ical Method: 8260B
Matrix: Aqueous
Prep Method: 5030B
Parameter Result Dil PQL MDL Units Analysis Date
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
ND
ND
ND
ND
<,Rec
104 "
117
108
i
1
1
1
Acceptance Limit
70-130
70-130
70-130
5.0
5.0.
2.0
5.0
v^
0.30
0.30
0.10
1.7'.
ug/L
ug/L
ug/L
ug/L
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
06/15/2010 1426
-
Bromofluorobenzene
1,2-Dichl6roethane-d4
Toluene-d8
PQL = Practical quantitation limit P = Ttie RPD between two GC columns exceeds 40%
ND = Not detected at or above the MDL J = Estimated result < PQL and >. MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W
Note: Calculations are performed before-rounding to avoid round-off errors in calculated results
N - Recovery Is out of criteria
+ - RPD is out of criteria
Shealy Environmental Services. Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 ' www.shealylab.com
Page: 19 of 23 Level 1 Report v2 1
AR000286
Volatile Organic Compounds by GC/MS - LCS
Sample ID: LQ35826-002
Batch: 35826
Analyt ical Method: 8260B
Matrix: Aqueous
Prep Method: 5030B
Parameter
Spike Amount (ug/L)
Result (ug/L) Dil % Rec
% Rec Limit Analysis Date
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloroproparie (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,4-Dichlqrobenzene
1,3-Dichlorobenzene
1,2-Dichlorobenzene
Dichlorodifluoromethane
1,2-Dichloroethane
1,1-Dichloroethane
trans-1,2-Dichloroethene
cis-1,2-Dlchloroethene
1,1-Dichloroethene
1,2-Dichloropropane
trans-1,3-Dichloropropene
cis-1,37Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,2-Trichloro-1,2.2-Trifluoroethane
1,2,4-Trichlorobenzene
1,1,2-Trichloroethane
1,1,1-Trichloroethane
40
20
20
20
20
40
20 '
20 .
20
20
20
20
20
20
20
20.
20
20 '
20
20 ,
20
20
20
20
20
20
20
20
20
40
20
20
20
40
20
20
20
20
20
20
20
20
20
20
32
18
18
17
. 15
33
20
17
17
• 17
19
17
• 19
17
18
,18
18
18
18
16
20
18
18
18
17
18
16
17
18
36
.. 18
18
18
38
18
16"
18
19
18
18
21
19
18
13
1 80
1 89
1 92
1 85
1 77
1 82
1 101
1 84
1 87
1 86
1 ' 9 4
1 84
1 94
1 85
1 88
1 / 90
1 90.
1 89
1 89
1 78
1 98 '
1 92
1 88
1 . . 8 8
1 83
1 91
1 80
1 84
1 88
1 90.
1 92
1 91
1 91
1 95
1 88
1 82
1 88
1 96
1 ' 86
1 91 ,
1 105
1 94
1 88
1 67
46-153
72-127
71-143
65-131
36-168
60-140
60-140
37-166 .
78-129
42-163
63-123
20-158
70-130
70-130
74-134
70-130
70-130
70-130
70-130
10-158
59-143
69-132
70-130
70-130 .
50-132
71-126
73-131
69-130
79-132
60T140
70-130
15-128
70-130
60-140
70-130
69-129
70-130
60-155
70-130
75-125
70-130
70-130
77-132
77-132
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1256
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
PQL = Practical quantitation limit P = Ihe RPD between two GC columns exceeds 40%
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
N - Recovery is out of criteria
+ - RPD is out of criteria i
Shealy Environmental Services. Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 20 of 23 Level 1 Report v2.1
AR000287
Volatile Organic Compounds by GC/MS - LCS
Sample ID: LQ35826-002
Batch: 35826
Analytical Method: 8260B
Parameter
Trichloroethene
.Trichlorofluoroniethane
Vinyl chloride
Xylenes (total)
Surrogate
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
Spike Amount
. (ug/L)
20
20
20
40
Q , % Rec
105
115
109
Result (ug/L) Q
17
18
16
36
Acceptance Limit
70-130
70-130
70-130
Matrix:
Prep Method:
Dil
1
1
1
1
Aq, jeous
5030B
% Rec
85
88
82
89
% Rec Limit
73-124
41-173
29-159
70-130
Analysis Date
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
06/15/2010 1258
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40%
ND = Not detected at orabove the MDL J = Estimated result < PQL and >^MDL .
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged v/ith a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
N - Recovery is out of critena
+ - RPD is out of criteria
Shealy Environmental Services. Inc. i 106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 www shealylab com
Page: 21 of 23 Level 1 Report v2.1
AR000288
Volatile Organic Compounds by GC/MS - LCSD Sample ID
Batch
Analyt ical Method:
Parameter
LQ35826-003
35826
8260B
Spike Amount (ug/L)
Result (ug/L) Q
Matrix: Aqueous
Prep Method: 5030B
Dil % Rec % R P D '
% Rec Limit
% RPD Limit
(
Analys is Date
Acetone .
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,4-Dichlorobenzene
1,3-Dichlorobenzene
1,2-pichlorobenzene
Dichlorodifluoromethane
1,2-Dichloroethane
1,1-Dichloroethane
trans-1,27Dichloroethene
cis-1,2-Dichloroethene
1,1-DiGhloroethene
1,2-Dichloropropane i
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate •
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene Toluene
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,2,4-Trichlorobenzene
1,1,2-Trichloroethane I
1,1,1-Trichloroethane
40
20
20
20
20
40
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20 . .
20
20
20
20
20
20
40
20
20
20
40 i
20 .
20
20
20
20
20
20
20
20
20
32
18
18
17
• 16
33
20
17
18
17
19
17
18
16
18
18
18
18
18
15
20
19 ,
. • , 18
18
17
19
16
17
18
36
19
18
18
37 ,
17
17
18
19
18 18
20
18
18
19
1 80
1 89
1 92 '
1 .'- 83
1 78
1 83
1 99
1 83
1 88
1 87
1 95
1 . 83
1 .92 -
1 80
1 88
1 89
1 90
1 / 91
1 90
1 76
1 98
1 93
1 89
1 • 90
1 85
1 , „ 93
1 79
1 84
1 88
1 89
1 • 93
1 88
1 . 9 2
1 v' 9 3 '
1 87
1 83
1 88
1 96
1 89
1 92
1 102
1 .92
'1 88
1 95
0.12
0.21
0.13
2.4
2.1
0.90
1.9
0.70
1 0.42
0.84
0.75
0.57
2.0
6.2
0.023
1.1
0.72
1.8 •
1.1
3.2
r 0.12
0.91
0.62
1.9
1.8
2.2-
1.8
1.0
0.22
1.8
.0 .50
3.8
0.98
1.5
1.2
1.2
0.16
0.56
1.4
1.3
2.9
, • 2.4
6.086
34
46-153
72 -127 '
71-143
65-131
36-168
60-140
60-140
37-166
78-129
' 42-163
63-123 .
20-158
70-130
70-130
74-134
70-130
70-130
70-130
70-130
10-158
59-143
69-132
70-130
70-130
50-132
71-126
73-131
69-130
79-132
60-140
70-130
15-128
70-130
60-140
70-130
69-129
70-130
60-155
70-130
75-125
7.0-130
70-130
77-132
77-132
20
20
20
' 2 0
20
20
20
20
20
.20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
. 20
20
20
20
20
20
20
20
20
20
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
,06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
PQL = Practical quantitation limit . P = The RPD between two GC columns exceeds 40%
ND = Not detected at or above the MDL J = Estimated result < PQL and >. MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
N - Recovery is out of criteria
+ - RPD is out of cnteria
Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 22 of 23 Level 1 Report v2.1
AR000289
Volatile Organic Compounds by GC/MS - LCSD
Sample ID: LQ35826-003 '
Batch: 35826
Analyt ical Method: 8260B
Parameter
Trichloroethene
Trichlorofluoromethane .
Vinyl chloride
Xylenes (total)
Surrogate
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
Spike Amount (ug/L) •
20 •
20
20
40
Q %Rec
105
113
108
Result (ug/L)
17
/17
16
36
Q
Acceptance Limit
70-130
70-130
70-130
Matrix:
Prep Method:
Dil
1
1
1
1
Aqueous
5030B 1
% Rec
86
86 ,
82
90
% RPD
0.39
2.4 ' -
0.29
1.3 {
% Rec Limit
73-124'
41-173
29-159.
70-130
'
% RPD Limit
20
20
20
20
Analysis Date
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
06/15/2010 1320
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
P = The RPD between two GC columns exceeds 40%
J = Estimated result < PQL and > MDL
N - Recovery is out of criteria
+ - RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a ."W" ) . I
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 23 of 23 Level 1 Report v2.1
AR000290
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AR000291
SHEALY ENVIRONMENTAL SERVICES. INC.
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Shealy Environmental Services, Inc. . V 106 Vantage Point Drive .v:West Columbia, SC 29172 (803)791-9700 Fax (803) 791-9111 vww.shiealylab.com Level 1 Report v2.1
AR000292
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
ARCADIS 6 Terry Drive . Suite 300
Newtown, PA 18940 Attention: Christopher Sharpe
Project Name: Mil lsboro TCE
Project Number;NP000686
Lot Number: LF03012
Date Completed:06/11/2010
Nisreen Saikaly
-Project Manager
4« l r - - r r *J^o^
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environnnehtal Services, Inc.
The following non-paginated docurrients are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Shealy Environmental Services. Inc. Page: 1 of 63 106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 www.stiealylab.com Level i Report v2.1
AR000293
SHEALY ENVIRONMENTAL SERVICES, INC. SCDHEC No: 32010 NELAC No: E87653 NC DEHNR No: 329
Case Narrative ARCADIS
Lot Number: LF03012
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
r
Volatile Organic Compounds
The LCSD recovery for Carbon disulfide was outside method control limits in batch 35603. The LCS results were within limits. Therefore the
associated sample results,were reported and no corrective action was required. -
The LCS recovery for Acetone and 2-Butanone (MEK) was outside method control limits in batch 35610. The LCSD results were within limits. Therefore the associated sample results were reported and no corrective action was required.
Shealy Environmental Services, Inc. Page: 2 of 63 106 Vantage Point Drive West Columbia: SC 29172 (803)791-9700 Fax (803) 791-9111' vww.shealylablcom Leveii Report v2.1
AR000294
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary ARCADIS
Lot Number: LF03012
Sample Number Sample ID Matrix Date Sampled Date Received
001
002
003
004
005
006
007
008
009
010
O i l
.012
013
014
015
016
017
(17 samples)
MW-11D060110.
MW-11M060l' l0 :
MW-11S060110
MW-12S060110
MW-12SA060110
MW-14S060110
MW-14M060110
MW-14D060110
FB-060110
MW-UNS-060110
MW-13S060210
MW-13M060210
MW-12M060210
MW-12D060210
MW-13D060210
FB-0602i0
Trip Blank
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
06/01/2010 1055
06/01/2010 1230
06/01/2010 1450
06/01/2010 1610
06/01/2010 1630
06/01/2010 1510
06/01/2010 1405
06/01/2010 1030
06/01/2010 1630
06/02/2010 1340
06/02/2010 1100
06/02/2010 0920
06/02/2010 0850
06/02/2010 1030
06/02/2010 1320
06/02/2010 1405
06/03/2010
06/03/2010
06/03/2010
06/03/2010
06/03/2010
06/03/2010
06/03/2010
06/03/2010
06/03/2010
06/03/2010
06/03/2010
06/03/2010
06/03/2010
06/03/2010
06/03/2010
06/03/2010
06/03/2010
06/03/2010
Shealy Environrnental Services. Inc. 106 Vantage Point Drive West Columbia. SC ,29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 3 of 63 Level 1 Report v2.1
AR000295
SHEALY ENVIRONMENTAL SERVICES, INC.
y *
Sample Sample ID
002
002
002
003
003'
003
003
004
004
004
004
004
005.
005
005
005
005
006
006
006
007
007
007
008
009 .
014
MW-11M060110
MW-11M060110
MW-11M060110
MW-11S060110
MW-11S060110 '
MW-11S060110
MW-11S060110
MW-12S060110
MW-12S060110
MW-12S060110
MW-12S060110
MW-12S060110
MW-12SA060110
MW-12SA060110
MW-12SA060110
MW-12SA060110
MW-12SA060110
MW-14S060110
MW-14S060110
MW-14S060110
MW-14M060110
MW-14M060110
MW-14M060110
MW-14D060110
FB-060110
MW/-12D060210
(26 detections)
. Matrix
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
. Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
, Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
. Aqueous
Aqueous
Aqueous
Executive Summary ARCADIS
Lot Number: LF03012
Parameter '
Carbon tetrachloride
4-Methyl-2-pentanone
1,2,4-Trichlorobenzene
Carbon tetrachloride
cis-1,3-Dichloropropene
4'-Methyl-2-pentanone
1,2,4-Trichlorobenzene
Carbon tetrachloride
Dibromochloromethane
cis-1,3-Dichloropropene
4-Methyl-2-pentanone
1,2,4-Trichlorobenzene
Carbon tetrachloride
Dibromochloromethane
cis-1,3-pichloropropene
4-Methyl-2-pentanone
1,2,4-Trichlorobenzene f
Carbon tetrachloride '
cis-1,3-Dichloropropene
4-Methyl-2-pentanone
Carbon tetrachloride
cis-1,3-Dichloropropene
4-Methyl-2-pentanone
Carbon disulfide
Carbon disulfide
Carbon disulfide \ .
Method
82608
8260B
8260B
82608
82608
82608
82608
82608
8260B
8260B
8260B
82608
82608
82608
82608
82608
82608
82608
82608
8260B
8260B
82608
8260B
82608
82608
82608
Result
0.77
0.85
2.2
0.77
3.8
0.87
2.2
0.76
4.8
3.8
0.83,
2.2
•"" • 0.77
4.8
3.8
C).88
2.2
0.73
3.8
0.85 •
0.84
3.8
0.86
0.42
0.35
0.48
Q
J
J
BJ
J
J
J
BJ
J
J
J
J
BJ
J .
J
J
J
B j '
J
J
J
J :
J
J
J
J
J
J
Units
ug/L- .
ug/L
ug/L
ug/L,
ug/L-
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L ,
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L .
ug/L
Page
7
7
7
9
9
9
9
11
11
11
11
11
13
13
13 .
13
13
15
15
15
17
17
17 .
19
• 21
31
Shealy Environmental Services, Inc. 106 Vantage, Point Drive WestColumbia.SC 29172 (803)791-9700 Fax (803) 791-9111 vww.shealylab.com
Page: 4 of 63 Level 1 Report v2.1
AR000296
Volatile Organic Compounds by GC/MS Client: ARCADIS
Description: MW-11D060110
Date Sampled:06/01/2010 1055
Date Received:06/03/2010
Laboratory ID: LF03012-001
Matrix: Aqueous
Run 1
Prep Method 50308
Analyt ical Method 82608
Dilution Analysis Date Analyst 1 06/08/2010 1935 DLB
Prep Date Batch 35427
' Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Acetone
Benzene ^
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butan'one (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform ••
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-pichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene >
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene •
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
i ; i ,2-Trichlor6-1,2,2-Triflijoroethahe "
1,2,4-Trichlorobenzene
1,1,1 -Trichloroethane
1,1,2-Trichloroethane
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3 1
74-87-3
110-82-7
96-12-8 .
124-48-1 106-93-4
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2 75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
108-10-1
108-87-2
75-09-2
100-42-5
79-34-5
127-18-4
108^88-3
76-13- r
120-82-1
71-55-6
, 79-00-5
8260B
8260B •
8260B
8260B
- 8260B
8260B
82608
82608 .
82608
82608
8260B
8260B
.82608
8260B
8260B
8260B
8260B
8260B
8260B
. 8260B
82608 ^
82608
82608
82608
8260B
8260B '
8260B
8260B
8260B
, 8260B
82608
82608
82608
82608
8260B
8260B •
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
' ND
ND
ND
ND
ND
ND ND
ND
ND
ND
ND
ND .
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
20
5.0
5.0
5.0
5.0
10
5.0
1 5.0
5.0
5.0
5.0
5.0
5.0
-5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
• 5.0
5.0
•5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0 ,.
5.0
' 5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
6.7
0.20
1.7
0.40
0.80
1.8
0.30
0.40
1.7
0.50
1.7
0.30
0.98
0.60
1.7 0.30
1.7
1.7
1.7
0.20
0.30
0.30
0.50
0.20
0.40'
0.30
0.30
0.30
1.7
1.0
1.0
0.72
0.40
0.80
0.95
.1.7
0.10
0.40
0.40
1.7
' 0.30 '
' 1.7'
0:20
0.30
ug/L 1
, ug/L 1
ug/L 1
ug/L ,1
ug/L 1
ug/L 1
ug/L 1 ' ug/L -1
ug/L 1
ug/L 1
ug/L 1
ug/L • 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
•ug/L 1
ug/L 1
"S'-k , , -1 ug/L 1
.ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L • 1
ug/L 1
ug/L 1
ug/L . 1
ug/L 1
ug/L 1
ug/L 1
ug/L -I
ug/L • 1
ug/L ' 1
ug/L 1
PQL = Practical quantitation limit . B = Detected in the method blank
ND = Not detected at or above the MDL , J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation ot compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria H = Out ot holding time
Shealy Environmental Services, Inc. 106 Vantage Point Drive WestColumbia.SC 29172 (803) 791-9700 Fax (803) 791-9111 wvw.shealylab.com
Page: 5 of 63 Level 1 Report v2.i
AR000297
Client: ARCADIS
Description: MW-11D0601.10
Date Sampled:06/01/2010 1055
Date Received:06/03/2010
Volatile Organic Compounds by GC/MS Laboratory ID: LF03012-001
•^ Matrix: Aqueous ' \ , . • . \ • .
. ^
Run 1
Prep Method 50308
Analy t ica lMethod 8260B
Dilution Analysis Date 1 06/08/2010 l"935
Analyst DLB
Prep Date Batch 35427
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
79-01-6
75-69-4
75-01-4
1330-20-7
8260B
8260B
8260B
8260B
ND
ND
ND
ND
5.0
5.0
2.0
5.0
0.30,
0.30
0.10
1.7
ug/L
ug/L
ug/L
ug/L
1
1
1
1
Run 1 Acceptance % Recovery Limits
1,2-Dichloroethane-d4
.Bromofluorobenzene
Toluene-d8
105
102
111
70-130
70-130 70-130
PQL = Practical quantitation limit B = Detected in the method blank
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services. Inc. 106 Vantage Point Drive WestColumbia.SC 29172 (803)791-9700 . Fax (803) 791-9111 www.shealylab.com
Page: 6 of 63 Level 1 Report v2.1
AR000298
Client: ARCADIS
Description: MW-11M060110
Date Sampled:06/01/2010 1230
Date Received:06/03/2010
Volatile Organic Compounds by GC/MS Laboratory ID: LF03012-002
Matrix: Aqueous
Run 1
Prep Method 5030B
Analytical Method 82608
Dilution 1
Analysis Date 06/10/2010 1126
Analyst DLB
Prep Date Batch 35603
Parameter CAS
Number
Analyt ical
- Method Result PQL MDL Units Run
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1.2-Dichloroethene
trans-1.2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate '
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,2-Trichloro-1,2,2-Trifluoroethane '
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
67-64-1
• 71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1
106-93-4
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2 75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
108-10-1
108-87-2
75-09-2
• 100-42-5
79-34-5
. 127-18-4 V
108-88-3
76-13-1
120-82-1
71-55-6
79-00-5 ,,
8260B
8260B
82608
8260B
8260B
8260B
8260B
8260B
82608
82608
82608
82608
8260B
, ^ 8260B
82608
82608
82608
8260B
8260B
8260B
8260B
•' 82608
82608
8260B
8260B
82608
82608
,82608
8260B
8260B
82608
82608
82608
8260B
8260B
8260B
8260B
82608
82608
8260B
8260B
B260B
82608
82608
ND
ND
ND
ND
ND
ND
ND
0.77
ND
ND
ND
ND
ND..
,ND '
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
' N D , ,
ND
ND
ND
• ND
ND
0.85
ND
ND
ND
ND
ND
ND
ND
2.2
ND
ND
20
5.0
5.0
5.0 .
- 5.0
10
5.0
J 5.0
5.0
5.0
5.0
5.0
5.0 5.0
5.0
5.0
5.0
J 5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
. 5.0
5.0
10
5.0
5.0
5.0
J 10
5.0-
5.0
5.0
5.0
5.0
5.0
5.0
BJ 5.0
5.0
5.0
6.7
0.20
1.7
, 0.40
0.80
.1.8
0.30
0.40
1.7
0.50
1.7 .
0.30
0.98
0.60
1.7
0.30
1.7
1.7
1.7
0.20
0.30
0.30
0.50
0.20
0.40
0.30
0.30
0.30
1.7
1.0
1.0
0.72
0.40
0.80
0.95
1.7
0.10
0.40
0.40
1.7
0.30
1.7
0.20
0.30 .
: ug/L 1
ug/L 1
ug/L . 1
ug/L • 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L. ' 1
ug/L 1
ug/L 1
ug/L 1
' ug/L 1
ug/L 1
ug/L 1 ug/L . 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
' ug/L 1
ug/L " '1
ug/L 1
ug/L 1
ug/L 1
ug/L . 1
ug/L 1
ug/L 1
, ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank ND = Nol detected at or above the MDL J = Estimated result < PQL and ; MDL VVhere applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "VT
E = Quantitation ot compound exceeded the calibration range P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services. Inc. 106 Vantage Point Drive • West Columbia, SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 7 of 63 Level 1 Report v2 1
AR000299
Volatile Organic Compounds by GC/MS Client: ARCADIS
Description: MW-11M060110
Date Sampled:06/01/2010 1230
Date Recelved;06/03/2010
Laboratory ID: LF03012-002
Matrix: Aqueous
Run 1
Prep Method - •5O30B
Analyt ical Method 82608
Dilution Analysis Date 1 06/10/2010 1126
Analyst DLB
Prep Date Batch 35603
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
79-01-6
75-69-4
75-01-4
1330-20-7
8260B •
- 8260B
1 82608"
82608
ND
ND
ND
ND
5.0
5.0
• 2 .0 '
5.0
0.30
0.30
0.10 .
1.7
ug/L
ug/L.
ug/L
ug/L
1
1
1
1
Run 1 Acceptance % Recovery Limits
1,2-Dichloroethane-d4
Bromofluorobenzene Toluene-d8
108 100 106
70-130 70-130 70-130
PQL = Practical quantitation limit B = Detected in the method blank
ND = Not detected at or above the MDL . J = Estimated result < PQL and > MDL
Where ap'pficable. all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range
P = The RPD t)etween two GC columns exceeds 40%
N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services, Inc. ,106 Vantage Point Drive WestColumbia.SC 29172 (803)791-9700 Fax (803) 791-9111 vww.shealylab.com
Page: 8 of 63 Level 1 Report v2.i
AR000300
Volatile Organic Compounds by GC/MS Client: ARCADIS
Description: MW-11S060110
Date Sampled:06/01/2010 1450
Date Received:06/03/2010
Laboratory ID: LF03012-003
> Matrix: Aqueous
Run Prep Method 1 50308
Analyt ical Method Dilution Analysis Date Analyst 82608 1 ,06/10/2010 1147 DLB
Prep Date Batch 35603
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Acetone
Benzene
BromodicWoromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1.3-Dichlorobenzehe
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene.
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dich|oropropene
trans-1,3-Dichlor6propene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,2,4-Trichlorobenzene
1,1,1 -Trichloroethane
1,1,2-Trichloroethane
67-64-1
. 71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1 106-93-4
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
' 107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4'
108-10-1
108-87-2
75-09-2
100-42-5
79-34-5
127-18-4
108-88-3
76-13-1
120-82-1
71-55-6
79-00-5
82608
82608
82608
82608
8260B
8260B
8260B
8260B
8260B
8260B
8260B
82608
82608
82608
82608
82608
82608
8260B
8260B ~
82608
82608
82608
82608
82608
82608
82608
8260B
82608
82608
82606
8260B
8260B
82608
8260B
82608
82608
82608
82608 ' 8260B
82608
82608
8260B
8260B
82608
ND
ND
ND
ND
ND
ND
ND
0.77
ND-
ND
ND
ND
ND
ND
ND
ND
ND
ND' '
ND
ND
ND
ND
ND
ND
ND
ND
3.8
ND
ND
ND
ND
ND
ND
0.87
ND
ND
ND
ND
ND
ND
ND
20
5.0
5.0
5.0
5.0
10
5.0 5.0
• 5.0
5.0
5.0
5.0
5.0
5.0
5.0
sfo 5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.(3
5.0
'5.0
5.0
5.0
5.0
10
5.0
5.0
• 5.0 .
10 5.0
5.0
5.0
5.0
5.0
5.0
5.0
2.2 BJ 5.0
ND •
ND •
5.0
5.0
6.7
,0.20
1.7
0.40
0.80
1.8
0.30
0.40
1.7
0.50
1.7
0.30
0.98
0.60
1.7
0.30
1.7
1.7
1.7
0.20
0.30
0.30
0.50
0.20
0.40
0.30
0.30
0.30
1.7
1.0
1.0
0.72
0.40
0.80
0.95
1.7
0.10
0.40
0.40
1.7
0.30
1.7
0.20
0.30
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L " 1
ug/L 1
- ug/L 1
ug/L 1
ug/L 1
ug/L • 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L • 1
ug/L 1
ug/L- 1
ug/L 1
ug/L 1
ug/L . 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
• ug/L . 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
, ug/L 1
ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL Where applicable, atl soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range . P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria , . H = Out of holding time
Shealy Environmental Services. Inc. 106 Vantage Point Drive WestColumbia.SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 9 of 63 Level 1 Report v2.1
AR000301
Volatile OrganicXompounds by GC/MS Client: ARCADIS
Description: MW-11S060110
Date Sampled:06/01/2010 1450
Date Received:d6/03/2010
Laboratory ID: LF03012-003
Matrix: Aqueous
Run 1
Prep Method 50308
Analyt ical Method 82608
Dilution Analysis Date 1 06/10/2010 1147
Analyst DLB
Prep Date Batch 35603
Parameter CAS
Number Analyt ical
Method Result PQL MDL Units -Run
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate.
79-01-6
75-69-4
75-01-4
1330-20.7
8260B
8260B
8260B
8260B
ND
ND
ND
ND
5.0
5.0
2.0
5.0
0.30
0.30
0.10
1.7
ug/L
ug/L
ug/L
ug/L
1
1
1
1
Run 1 Acceptance °/o Recovery Limits
1,2-Dichloroethane-d4
Bromofluorobenzene TQluene-d8
109
102 107
70-130
70-130
70-130
PQL = Practical quantitation limit
h;D = Not detected at or above ttie MDL
Wtiere applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
B = Detected in the method blank
J ~ Estimated resuK < PQL and > MDL
E 7 Quantitation ot compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803) 791-9700 Fax (803) 791-9111 wv^w.shealylab.com
Page: 10 of 63 Level 1 Report v2.1
AR000302
• ~
Client: ARCADIS
Description: MW-12S060110 ,
Date Sampled:06/01/2010 1610
Date Received:06/03/2010
Volatile Organic Compounds by GC/MS , Laboratory ID: LF03012-004
Matrix: Aqueous
Run 1
Prep Method 5030B
Analytical Method Dilution Analysis Date Analyst 8260B 1 06/10/2010 1209 DLB
Prep Date Batch 35603
Parameter CAS
Number
Analyt ical
Methott Result PQL MDL Units Run
Acetone
Benzene
Bromodichloromethane -
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
.Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane .
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1.3-Dich/orobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1.2-Dichloroethane
1,1-Dichloroethene
cis-1'i2-pichloroethene
trans-1,2-Dichloroethene
1,2-Dichlor'opropane,
cls-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9 ^
78-93-3
75-15-0' . 56-23-5
•108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
' 96-12-8-
124-48-1
^ 106-93-4 '
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41:4
591-78-6
98-82-a
79-20-9
1634-04-4
; 108-10-1
108-87-2
75-09-2
100-42-5
79-34-5
127-18-4
108-88-3
76-13-1
120-82-1
71-55-6
79-00-5
82608
82608
82608
82608
8260B
82608
82608
8260B
82608
82608
82608
82608
82608
82608
8260B
8260B
82608
8260B
82608
8260B
82608
82608
82608
" 82608
82608
82608
8260B
82608 '
8260B
82608
82608 .
82608
82608
8260B
82608
82608
82608
82608
82608
, 8260B
8260B
8260B
82608
8260B
ND
ND
ND
ND
ND
ND
ND 0.76
ND
ND
ND .
ND
ND
ND
4.8 V-
• ND
ND
ND
ND
ND
ND
ND.
ND
ND
ND
ND
3.8
ND
ND
ND
ND
ND
ND
0.83
ND
ND
ND
ND
ND
ND'
ND
20
5.0
5.0
5.0
5.0
10
5.0
j 5.0
5.0
5.0
5.0
5.0
5.0
5.0
J 5.0
5.0
5.0
5.0
5.0
v5.0
5.0
' 5.0
5.0
5.0
5.0
5.0 .
J 5.0
5.0
. 5.0
10
5.0
5.0
. 5.0
J 10
5.0
5.0
5.0
'5.0
5.0
5.0
5.0
2.2 BJ 5.0
ND
ND
5.0
5.0
6.7
0.20
1.7
0.40
0.80
. 1.8
0.30 0.40
1.7
0:50
1.7
0.30
' 0.98
0.60
1-7 0.30
1.7
''-7 1.7
0.20
• 0.30
0.30
0.50
0.20
0.40 .
0.30
0.30
0.30
1.7
1.0
1.0
0.72,
0.40
0.80
0.95
1.7
0.10
0.40
0.40
1.7
0.30
1.7
0.20
0.30
ug/L . 1
ug/L 1
ug/L 1
• • ug /L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L • 1
. ug/L 1
ug/L 1
ug/L 1
ug/L . 1
ug/L , 1
ug/L 1
ug/L 1
ug/L • 1
. ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L . 1
ug/L 1
ug/L 1
ug/L 1
. ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
PQL = Practical quantitation linnit B = Detected in the method blank ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL Where applicable, ail soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803)791-9700 Fax (803) 791-9111 wvw.stiealylab.com
Page: 11 of 63 Level 1 Report v2.1
AR000303
Volatile Organic Compounds by GC/MS Client: ARC Ab lSx -
Description: MW-12S060110
Date Sampled:06/01/2010 1610
Date Received:06/03/2010
Laboratory ID: LF03012-004
Matrix: Aqueous
Run 1
Prep Method 50308
Analyt ical Method 8260B
Dilution Analysis Date 1 06/10/2010 1209
Analyst DLB
Prep Date Batch 35603
Parameter CAS Analyt ical
Number Method Result PQL MDL Units Run
Trichloroethene
Trichlorofluoromethane
Vinyl chloride /-
Xylenes (total)
Surrogate
79-01-6
75-69-4
75-01-4
1330-20-7
8260B
82608
82608
82608
ND
ND
ND
ND
5.0
5.0
2.0
5.0
0.30
0.30
. 0.10
1.7
ug/L
ug/L
ug/L
ug/L
. 1
1
1
' 1
I Run 1 Acceptance % Recovery Limits
1,2-Dichloroefhane-d4
Bromofluorobenzene Toluene-d8
110
99 107
70-130
70-130
70-130
PQL = Practical quantitation limit B = Detected in the method blank ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40% N = Recovery is out of cfiteria H = Out of holding time
Shealy Environmental Services. Inc. 106 Vantage Point Drive WestColumbia.SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com.
Page: 12 of 63 Level 1 Report v2.1
AR000304
Client: ARCADIS
Description: MW-12SA060110
bate Sampled:06/01/2010 1630
Date Received: 06/03/2010
Volatile Organic Compounds by GC/MS • , ( _ Laboratory ID: LF03012-005
Matrix: Aqueous
'
Run Prep Method 1 • 50308
Analytical Method 8260B
Dilution Analysis Date Analyst 1 06/10/2010 1231 DLB
Prep Date Batch 35603
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibrombethane (EDB)
1,2-Dichlorobenze'ne
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane 1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1.2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene'
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride '^
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene ->
Toluene
1,1,2-Trichloro-1,2,2-Trlfluoroethane
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7 ,
96-12-8
124-48-1 106-93-4
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2 75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4
591-78-6
' 98-82-8
79-20-9
1634-04-4
108-10-1
108-87-2
75-09-2
100-42-5
79-34-5 127-18-4
108-88-3^
76-13-l '
120-82-1
71-55-6
79-00-5
. 8260B
8260B
82608
82608
82608
82608
82608
8260B
• 82608
82608
82608
82608
• 82608 •
82608
8260B
8260B
82608
8260B
82608
82608
82608
82608
-'82608
8260B
8260B
82608
8260B
82608
82608
82608
8260B
82608
8260B
8260B
82608
82608
82608
82608
8260B
8260B
8260B
82608
82608
82608
ND
ND
ND
ND
ND
ND
ND
0.77
ND •
ND
ND
ND •
ND
ND
4.8
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
3.8
ND
ND
- ND
ND
.. ND
ND
0.88
ND
ND
ND
ND
ND
ND
ND
20
5.0
5.0
5.0
5.0
10
5.0
J 5.0
5.0
5.0
5.0
5.0
5.0
• 5.0
J 5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0 5.0 •
5.0
5.0
5.0
J 5.0
5.0
5.0
10
5.0
5.0
5.0
J 10
5.0
5.0
5.0
5.0 5.0
5.0
5.0
2.2 BJ 5.0
ND
ND
5.0
5.0
6.7
0.20
1.7
0.40
0.80
1.8
0.30 0.40.
. 1.7
0.50
1.7
0.30
0.98
0.60
1.7
0.30
1.7
.1 '?' 1.7
0.20
'0 .30
0.30
0.50
0.20
0.40^
0.30 J
0.30
0.30
1.7
1.0
1.0
0.72
0.40
0.80
0.95
1.7
0.10
0.40
0.40
1.7
0.30
1.7
0.20 '
0.30
ug/L . 1
ug/L 1
ug/L . 1
ug/L - 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L • 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L . 1
ug/L 1 ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank' ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "VT
E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services. Inc. 106 Vantage Point Drive West Columbia, SC 29172 ' (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 13 of 63 Levell ReportV2.1
AR000305
Client:ARCADIS
Description: MW-12SA060110 _
Date Sampled:06/01/2010 1630
Date Received: 06/03/2010
Volatile Organic Compounds by GC/MS Laboratory ID: LF03012-00S
Matrix: Aqueous
' ' • '
Run 1
Prep Method 5030B
Analytical,Method 82608
Dilution Analysis Date 1 06/10/2010 1231
Analyst DLB •
Prep Date Batch 35603
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Trichloroethene
' Trichlorofluoromethane
Vinyl chloride^
Xylenes (total)
Surrogate. .
79-01-6
75-69-4
75-01-4 -
1330-20-7
8260B •
8260B
8260B
8260B
ND
ND
ND
ND
5.0
^ • 5.0
2.0
5.0
0.30
0.30
0.10
1.7.
ug/L
ug/L
ug/L
ug/L
• 1
1
1
1
Run 1 Acceptance % Recovery Limits
1,2-Dichloroethane-d4
Bromofluorobenzene Toluene-d8
107
100 107
• 70-130
• 70-130
70-130
PQL = Practical quantitation limit B = Detected in the method blank
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, atl soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation ot compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of cnteria H = Out of holding time
Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803)791-9700
/ Fax (803)791-9111 www.shealylab.com
Page: 14 of 63 Level 1 Report v2.1
AR000306
Volatile Organic Compounds by GC/MS Client:ARCADIS
Description: MW-14S060110
Date Sampled:06/01/2010 1510
Date Received: 06/03/2010
Run Prep Method Analyt ica lMethod 1 5030B 82608
Pararneter
Acetone
Benzene
Bromodichloromethane
Bromoform
• Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide Carbon tetrachloride
Chlorobenzene
Chloroethane •
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane ' -.
1,2-DibrorTio-3-chloropropane (DBCP) )
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichlbroethene
trans-1,2-Dichloroethene
1.2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone " -
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane.
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane Tetrachloroethene
Toluene
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Dilution Analysis Date Analyst 1 06/10/2010 1253 DLB
CAS Number
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
.124-48-1
106-93-4
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
'75-35-4
156-59-2
156-60-5
,78-87-5
10061-01-5
10061-02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
108-10-1
108-87-2
75-09-2
100-42-5
79-34-5
127-18-4
108-88-3
• 76-13-1 .
120-82-1
71-55-6
79-00-5
Analyt ical
Method
8260B
8260B
82608
82608
82608
8260B
8260B 8260B
8260B
82608
8260B
82608
82606
8260B
. 8260B 8260B
82608
82608
82608
,82608
8260B
8260B
82608'
82608
82608
82608
8260B
82608
82608
82608
8260B
8260B
8260B •
8260B
82608
82608 .
82608
82608 • .
8260B
8260B
82608' -^
• 82608
• 82608
82608
Prep Date i
Result
ND
ND
ND
ND
, ND
ND
ND
0.73
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND •
ND
ND
ND
3.8
ND'
ND
ND
ND
ND
ND
0.85
ND
ND
ND
ND
ND
ND .
ND
ND
ND ,
ND
Laboratory ID
Matrix:
Batch 35603
Q PQL
20
5.0 .
• 5.0
5.0
5.0
10
5.0
J 5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
J 5.0
5.0
5.0
10
5.0
5.0
5.0
J 10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0 ,
LF03012-006
Aqueous
MDL
6.7
0.20 •
1.7
0.40
0.80
1.8.
0.30
0.40
1.7-
0.50
1.7
0.30
0.98
0.60
1.7
0.30
1-7 1.7
1.7
0.20
0.30
0.30 0.50
0.20
0.40
0.30
0.30
0.30
1.7
1.0
1.0
0.72
0.40
0.80
0.95
1.7
0.10
0.40
0.40
1.7
0.30
1.7
0.20
0.30
^
Units R
ug/L
ug/L
ug/L.
ug/L.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
u g / L .
ug/L
ug/L .
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L ,
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L 1
ug/L
ug/L
j n
•i
PQL = Practical quantitation limit
ND = Not detected at or above ttie MDL
Wtiere applicable, all soil sample analysis are reported on a
B = Detected in ttie method blanl<
J = Estimated result < PQL and > MDL
dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services, Inc. 106 Vantage Point Drive WestColumbia.SC 29172 (803) 791-9700 Fax (803)791-9111 www.shealylab.com
Page: 15 of 63 Level 1 Report v2.1
AR000307
Volatile Organic Compounds by GC/MS Client: ARCADIS
Descripfion: MW-14S060110
Date Sampled:06/01/2010 1510
Date Received:06/03/2010
Laboratory ID: LF03012-006
Matrix: Aqueous
Run 1
Prep Method 5030B
Analyt ical Method 82608
Dilution Analysis Date Analyst 1 06/10/2010 1253 DLB
Prep Date Batch 35603
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
79-01-6
75-69-4
75-01-4
1330-20-7
8260B
8260B
8260B
82608
ND
ND
ND
ND
5.0
5.0"
2.0
5.0
0.30
0.30
0.10
1.7
ug/L
ug/L .
ug/L
ug/L
1
1
1
1
Run 1 Acceptance % Recovery Limits
1,2-pichloroethane-d4
Bromofluorobenzene
Toluene-d8
109
100
107
70-130
70-130
70-130
PQL = Practical quantitation limit B = Detected in the method blank
ND = Not detected at or above the MDL U = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.sheafylab.com
Page: 16 of 63 Level 1 Report v2.1
AR000308
Client: ARCADIS
Description: MW-14M060110
Date Sampled:06/01/2010 1405
Date Received:06/03/2010
Volatile Organic Compounds by GC/MS Laboratory ID: LF03012-007
Matrix: Aqueous
Run 1
Prep Method 50308
Analytical Method 8260B
Dilution Analysis Date Analyst 1 06/10/2010 1315 DLB
Prep Date Batch 35603
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Acetone
Benzene
Bromodichloromethane
Bromoforrn
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
r 1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
-1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,2,4-Trichlorobenzene
1.1,1-Trichloroethane
1,1,2-Trichloroethane
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7'
96-12-8
124-48-1
106-93-4
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2 75-35-4
156T59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4 •
591-78-6
98-82-8
79-20-9
1634-04-4
108-10-1
108-87-2
75-09-2
100-42-5
79-34-5
127-18-4
108-88-3
76-13-1
120-82-1
71-55-6
79-00-5
82608
82608
82608
• 8260B
82608
82608
82608
8260 B
82608
8260B
8260B
8260B
8260B
82608
82608
82608
82608
82608
8260B
8260B
82608
82608
82608
8260B
82608
82608
8260B
82608
8260B
8260B
82608
82608
82608
8260B
82608
82608
82608
8260B
82608
82608
, 82608
8260B
82608
82608
ND
ND-
ND
ND
ND
ND
ND
0.84
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
A_ ND
ND
ND
ND
3.8
ND
ND
ND
ND
ND
ND
0.86
ND
ND
ND
ND
ND
ND
ND •
ND
ND
ND
20
5.0
, 5.0
5;o 5.0
10 '
5.0
J 5.0
, 5.0 . •
5.0
5.0
5.0 .
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0 5.0
5.0
5.0
5.0
J 5.0
5.0
' ' 5.0
10
- 5.0
5.0
,. 5.0
J 10
5.0
5.0
5.0
5.0 5.0
5.0
5.0
5.0
5.0
5.0
6.7
0.20
1.7
0.40
0.80
1.8
0.30
0.40
1.7
0.50
1.7
0.30
0.98
0:60
1.7
0.30
1.7
1.7
1.7
0.20
0.30
0.30
0.50
0.20 .
0.40
0.30
0.30
0.30
1.7
1.0
1.0
0.72
0.40
0.80
0.95
1.7
0.10
•0.40
0.40
1.7
0.30
1.7
0.20
0.30
ug/L 1
ug/L 1
ug/L 1
ug/L •' 1
ug/L 1
ug/L 1
ug/L 1
ug/L ;1
ug/L 1
ug/L 1
ug/L 1
"' ug/J. 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L , .1
ug/L 1
. ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
u g / L 1
ug/L 1
ug/L 1
ug/L 1
ug /L 1
ug/L 1
ug/L 1
ug/L ,1
ug/L 1
ug /L 1
ug/L 1 1
PQL = Practical quantitation limit B = Detected in the method blank
ND = Nol delected at or above the MDL J = Estimated result < PQL and ; MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quanlilation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out ot criteria H = Out of holding time
Shealy Environmental Services. Inc. 106 Vantage Point Drive WestColumbia.SC 29172 (803)791-9700 Fax (803) 791-911.1 www.shealylab.com
Page: 17 of 63, Level 1 Report v2.1
AR000309
Volatile Organic Compounds by GC/MS ClientARCADIS
Description: MW>14M060110
Date Sampled:06/01/2010 1405
Date Received: 06/03/2010
Laboratory ID: LF03012-007
Matrix: Aqueous
Run 1
Prep Method 50308
Analyt ical Method 82608
Dilution Analysis Date 1 06/10/2010 1315
Analyst DLB
Prep Date Batch 35603
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
79-01-6
75-69-4
, 75-01-4
1330-20-7
82608
82608
82608
82608
ND
ND
ND
-ND ,
5.0
5.0
2.0
5.0
0.30
0.30
0.10
1.7
ug/L:
ug/L
ug/L
ug/L
1
1
1
1
Run 1 Acceptance % Recovery Limits
1,2-Dichloroethane-d4
Bromofluorobenzene Toluene-d8
112
98
108
70-130
70-130
70-130
PQL = Practical quantitation limit B = Detected in the method blank ND = Not detected at or above the MDL ., J = Estimated result < PQL and ; MDL V tiere applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range P = The,RPD between two GC columns'exceeds 40% N = Recovery is out of criteria H = iDut of holding time
Shealy Environmental Services, Inc. 106 Vantage Point Drive WestColumbia.SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 18 of 63 Level 1 Report v2.1
AR000310
Volatile Organic Compounds by GC/MS ClientARCADIS
Description: MW-14D060110
Date Sampled:06/0i/2010 1030
Date Received:06/03/2010
Laboratory ID: LF03012-008
Matrix: Aqueous
Run 1
Prep Method 5030B
Analytical Method 82608
Dilution Analysis Date 1 06/10/2010 1907
Analyst LBS
Prep Date Batch 35556
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Acetone
Benzene
Bromodichloromethane
"Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulf ide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichloroben2ene
1,3-Dichlorobenzene
1,4-Dichloroben2ene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloro6thene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
' ( Styrene \
^ 1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene •
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,2,4-Trichlorob6nzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
67-64-1
71^3-2
75-27-4
75-25-2
74-83-9
78-93-3 -
75-15-0 56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7 •
96-12-8
124-48-1
106-93-4
95-50-1
541-73-1
106-46-7
75-71-8^
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
108-10-1
108-87-2
, 75-09-2
100-42-5
79-34-5
127-18-4
108-88-3
76-13-1
120-82-1
71-55-6
79-00-5
- 8260B
8260B
8260B
8260B
82608
82608
8260B
82608
82608
8260B
82608
82608
82608
82608
8260B
82608
82608
82608
8260B
82608
'82608
82608
82608
82608
82608
82608
82608 •
8260B
8260B
8260B
82608
82608
82608
82608
82608
82608
8260B
8260B 82608
8260B
82608
82608
82608
82608
ND
ND
ND
ND
ND
ND
0.42
•ND
ND
ND
ND
ND
ND
ND
ND ND
ND
ND
ND
ND ' '
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
20
5.0
5.0
5.0
5.0
10 "
J 5.0
5.0
5.0
5.0
5.0
5.0
5:0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0 ,
5.0
5.0
10 .
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
6.7 ,
0.20
1.7
0.40 ,
0.80
1.8
0.30 0.40
1.7
0.50
1.7
0.30
0.98
0.60
1.7
0.30
1.7
1.7
1.7
0.20
0.30
0.30 '
0.50
0.20
0.40
0.30,
0.30
0.30
1.7
1.0
1.0
0.72
0.40
0.80
0.95
1.7
0.10
0.40
0.40
'. 1.7
0.30
1.7
0.20
0.30
ug/L' 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1 ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1 ug/L 1
ug/L 1
• ug/L • 1
. ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L ^ 1
ug/L 1
ug/L • 1
ug/L 1
ug/L 1
ug/L • 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
> ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank
ND = Nol detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation ot compound exceeded the calibration range
P = The RPD fcielween two GC columns exceeds 40%
N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services. Inc. 106 Vantage Point Drive WestColumbia.SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 19 of 63 Level 1 Report v2.1
AR000311
Client:ARCADIS
Description: MW-14D060110
Date Sampled:06/01/2010 1030
Date Received:06/03/2010
Volatile Organic Compounds by GC/MS Laboratory ID: LF03012-008
^ Matrix: Aqueous
Run l '
Prep Method 5030B
Analyt ical Method 8260B
Dilution Analysis Date Analyst 1 06/10/2010 1907 LBS
Prep Date Batch 35556
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run .
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
79-01-6
75-69-4
75-01-4
1330-20-7
8260B
8260B
8260B
8260B
ND
ND
ND
ND
5.0 •
5.0
2.0
5.0
0.30
0.30
0.10
. 1.7
ug/L
ug/L
ug/L
ug/L ,
1
1
1
1
Run 1 Acceptance % Recovery Limits
1,2-Dichloroethane-d4
Bromofluorobenzene Toluene-d8
102
101 99
70-130
70-130
-70-130
PQL = Practical quantitation limit B = Detected in the method blank
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services. Inc. 106Vantage Point Drive WestColumbia.SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 20 of 63 Level 1 Report v2.1
AR000312
Client: ARCADIS
Description: FB-060110
Date Sampled:06/01/2010 1630
Date Received:06/03/2010
Volatile Organic Compounds by GC/MS '
Laboratory ID: LF03012-009
Matrix: Aqueous
Run 1
Prep Method 50308
Analytical Method ' 82608
Dilution Analysis Date ' Analyst Prep Date . Batch 1 06/10/2010 1929 LBS 35556
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
• 2-Butanone (MEK)
Carbon disulf ide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform " >
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane.
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,2-Trichlbro-1,2,2-Trifluoroethane-
1,2,4-Trichlorobenzene
1,1,1 -Trichloroethane
1,1,2-Trich)oroethane
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3 •
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1
106-93-4
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2 75-35-4
156-59-2
156-60-5 '
78-87-5
10061-01-5
10061-02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4 ^
108-10-1
108-87-2
75-09-2 ,
100-42-5
79-34-5
127-18-4
108-88-3
76-13-1
120-82-1
71-55-6
79-00-5
82608
82608
8260B
8260B
82608
82608
8260B
82608
• 82608
82608
82608
82608
82608
82608
82608
82608
, 8260B
8260B
82608
.82608
82608
,82608
82608
8260B
82608
82608
8260B
82608 '.
82608
82608
8260B
8260B
8260B
8260B
8260B
82608
82608
82608
8260B
. 8260B
8260B
82608
82608
8260B
ND
ND
,ND
ND
ND
ND
0.35
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
. ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
20
5.0
5.0
5.0
5.0
10
J 5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
. 5.0 5.0
5.0
5.0
5.0'
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0 -
5.0
10
5.0
5.0'
5.0
10
5.0
5.0
5.0 -
5,0
5.0
5.0
5.0
5.0
5.0
5.0
6.7
0.20
1.7
0.40
0.80
1.8
0.30
0.40
1.7
0.50
1.7
0.30
0.98
0.60
1.7
0.30
1.7
1.7
1.7
0.20
0.30-
0.30
0.50
0.20
0.40
. 0.30
0.30
0.30 •
1.7 •
1.0
r.o 0.72
0.40
0.80
0.95
1-7 0.10
0.40
0.40
1.7
0.30
1.7
0.20
0.30
ug/L 1
ug/L 1
ug/L 1
ug/L '. 1
ug/L 1
ug/L' 1
ug/L 1
ug/L 1
ug/L • 1
ug/L 1
ug/L ' 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1 1 ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L . 1 ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L ^ 1
ug/L ' 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
• ug/L 1
ug/L 1
•ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L : 1
ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank •
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unfess flagged with a "W"
E = Quantitation of compound exceeded the calibration range
. P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803)791-9700 Fax (803) 791-9111 ' wvw.sheajylab.com
Page; 21 of 63 Level 1 Report v2.1
AR000313
Volatile Organic Compounds by GC/MS Client: ARCADIS
Description: FB-060110
Date Sampled:06/01/2010 1630
Date Received: 06/03/2010
Laboratory ID: LF03012-009
Matrix: Aqueous
Run 1
Prep Method 50308
Analyt ical Method 82608
Dilution Analysis Date 1 06/10/2010 1929
Analyst LBS
Prep Date Batch 35556
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
79-01-6
75-69-4
75-01-4 •
1330-20-7
8260B
8260B •
8260B •
8260B
ND
ND
ND
ND
5.0
5.0
2.0
5.0
0.30
0.30
0.10
1.'7.
ug/L
ug/L
ug/L
ug/L
1
1
1
1
Run 1 Acceptance % Recovery Limits
1,2-Dichloroethane-d4
Bromofluorobenzene Toluene-d8
103
102 105
70-130
70-130
70-130
PQL = Practical quantitation limit B = Detected in the mettiod blank ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL Wtiere applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40% ' N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services. Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 wviw.shealylab.com
Page: 22 of 63 Level 1 Report v2 1
AR000314
Client:ARCADIS
Description: MW-UNS-060110
Date Sampled:06/02/2010 1340
Date Received:06/03/2010
Volatile Organic Compounds by GC/MS / Laboratory ID: LF03012-010
Matrix: Aqueous
• • • . '
Run 1
Prep Method 50308
Analyt ical Method 8260B-
Dilution Analysis Date 1 06/10/2010 1952
Analyst LBS
Prep Date Batch 35556
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Acetone
Benzene . _ ^
Bromodichloromethane
Bromoform '
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichloroben2ene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene '
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1.1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
67-64-1.
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7 .
75-00-3'
67-66-3 ,
74-87-3
110-82-7
96-12-8
124-48-1
106-93-4
95-50-1
541-73-1
106-46-7 '
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4 ,
591-78-6
98-82-8
79-20-9
1634-04-4.
108-10-1
108-87-2
75-09-2
100-42-5
79-34-5 127-18-4.
108-88-3
• 76-13-1
120-82-1
71-55-6 ~
79-00-5
8260B
82608
82608
82608
8260B
8260B
8260B
82608
82608
• 82608
82608
82608
8260B
8260B .
8260B
8260B
8260B
8260B
82608
82608
82608
8260B
8260B
8260B
82608
8260B
82608
82608
8260B
8260B
82608
82608
82608
82608
8260B
8260B
8260B 1
8260B
82608
82608 •
82608
82608
8260B .
8260B
ND
ND
ND
ND
, ND
ND
ND '
. ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
20
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5,0
5.0
5.0
. 5.0
5.0
5.0
5.0
5.0
5.0
5.0 '
5.0
5.0 .
5.0
5.0
' 5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0 .
- 5.0
• 5.0
5.0
5.0 1
5.0
6.7
0.20
1.7
0.40
0.80
'1.8
0.30
0.40
1.7
0.50
1.7
0.30
0.98
0.60
1.7
0.30
1.7
1.7
1.7
0.20
0.30
0.30 0.50
0.20
0.40
0.30
0.30
0.30
. 1 .7
10 .
10 0.72
0.40
0.80
0.95
1.7
0.10
0.40
0.40
1.7
0.30
1.7
0.20
0.30
ug/L 1
ug/L - 1
ug/L 1
ug/L 1
ug/L 1
ug/L. 1
ug/L 1
• ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
„ ug/L 1
ug/L 1
ug/L - 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L • ' 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
. ug/L • 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L ' 1
PQL = Practical quantitation limit B = Detected in the method blanK ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagge'd with a 'V^
. E = Quantitation of compound exceeded the calibration range P = Ttie RPD between two GC columns exceeds 40% N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services. Inc. 106 Vantage Point Drive WestColumbia.SC 29172 (803)791-9700 Fax (803) 791-9111 vww.shealylab.com
Page: 23 of 63 Level 1 Report v2.1
AR000315
Volatile Organic Compounds by GC/MS ClientARCADIS
Description: MW-UNS-060110
Date Sampled:06/02/2010 1340
Date Received: 06/03/2010
Laboratory ID: LF03012-010
Matrix: Aqueous
Run • 1
Prep Method 50308
Analytical Method 82608
Dilution Analysis Date Analyst 1 06/10/2010 1952 LBS
Prep Date Batch 35556
Parameter CAS
Number
Analyt ical
Method 1.
Result PQL MDL Units Run
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
79-01-6
75-69-4
75-01-4
1330-20-7
8260B
8260B
8260B
8260B
ND
. ND
ND^
ND
5.0
5.0
2.0
5.0
0.30
0.30
0.10
1.7
ug/L
ug/L
ug/L
ug/L
1
.1
1
1
Run 1 Acceptance % Recovery Limits
1,2-Dichloroethane-d4
Bromofluorobenzene Toluene-d8
104
101 104
70-130
70-130
70-130
/
PQL = Practical quantitation limit B = Detected in the method blanl<
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services. Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803)79.1-9700 Fax (803) 791-9111 www.shealylab.com
Page: 24 of 63 Level 1 Report v2.1
AR000316
Client: ARCADIS
Description: MW-13S060210
Date Samp!ed:06/02/2010 1100
Date Received: 06/03/2010
Volatile Organic Compounds by GC/MS ,, Laboratory ID: LF03012-011
Matrix: Aqueous
Run 1
Prep Method 50308
Analytical Method 8260B
Dilution Analysis Date Analyst 1 06/10/2010 2014 LBS
Prep Date Batch 35556
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Acetone
Benzene
Bromodichloromethane
( Bromoform '
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
. Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
-1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane -
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroetherie
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,,2,4-Trichlorobenzene
1,1,1 -Trichloroethane
1,1,2-Trichloroethane
67-64-1'
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0.• "56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1
106-93-4
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
• 107-06-2
75-35-4
156-59-2,
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
108-10-1
108-87-2 .•
• 75-09-2
100-42-5
79-34-5
127-18-4
108-88-3
76-13-1
120-82-1
71-55-6
79-00-5
82608
82608
8260B
8260B
82608
82608
82608
82608
.82608
8260B
8260B
8260B
82608
82608
82608
82608
8260B
8260B
82608
82608
82608
82608
.8260B
82608
82608
8260B
8260B
82608
82608
82608
82608
82608
8260B
8260B
82608
82608
82608
82608
8260B
8260B
• 82608
82608
82608
82608
ND
ND
ND
ND
ND
ND
ND ND '
ND
ND
ND
ND
ND
ND
. ND •' •
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
. ND
ND
ND
ND' ND
ND
ND
ND
ND
ND
ND
' ND
20
5.0
5.0
5.0
5.0
10
5.0 5.0
5.0
. 5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0 ' 5.0
5.0
5.0
5.0
5.0
' 5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0 •
5.0
5:0
5.0
5.0
5.0
6.7
0.20
1.7
0.40
0.80
1.8
0.30
0.40
1.7
0.50
1.7
0.30
0.98
0.60
1.7
0.30
1.7
1.7
1.7
0.20
0.30
0.30
0.50
0.20
0.40
0.30
0.30
0.30
1.7
- 1.0
1 0
0.72
0.40
0.80
0.95
1.7
0.10
0.40
0.40
1.7
0.30
1.7
0.20
0.30
ug/L 1
ug/L 1
ug/L 1
• ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L : 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L ' 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L . 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L , 1
ug/L 1
ug/L 1
ug/L • 1
ug/L 1
ug/L 1
•ug/L 1
ug/L 1
ug/L 1
ug/L ' l
ug/L 1
ug/L 1
ug/L . 1
ug/L 1
- ug/L 1
ug/L 1
ug/L 1
ug/L 1
PQL = Practical quantitation limit B = Detected in the mettiod blank
ND = Nol detected at or above the MDL J = Estimated result < PQL and > MDL
VVhere applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "V^
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria H = Out of holding time
Shealy Environmenlal Services. Inc. 106 Vantage'Point Drive West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 25 of 63 Level 1 Report v2.1
AR000317
Volatile Organic Compounds by GC/MS Client: ARCADIS
Description: MW-13S060210
Date Sampled:06/02/2010 1100
Date Received:06/03/2010
Run Prep Method 1 5030B
Parameter N
Trichloroethene
Trichlorofluoromethane .
Vinyl chloride
Xylenes (total)
Surrogate
Analyt ical Method 82608
Q
1
,
Dilution Analysis Date 1 06/10/2010 2014
Analyst LBS
CAS Analyt ical
Number Method
79-01-6
75-69-4
75-01-4
1330-20-7
Run 1 Acceptance % Recovery Limits
8260B
82608
82608
82608
\
Prep Date
Result
ND
ND
ND
ND
Laboratory ID
Matrix:
Batch 35556
Q PQL
5.0
5.0
2.0
5.0 N
LF03012-011
Aqueous
\
MDL
0.30
0.30
0.10
1.7
Units
ug/L
ug/L
ug/L
ug/L
. -
Run
1
1
1
1 .
1,2-Dichloroethane-d4
Bromofluorobenzene Toluene-d8
105
102 106
70-130
70-130
70-130
PQL = Practical quantitation limit . B = Detected in the method blank
ND = Not detected al or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "V^
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services, Inc -106 Vantage Point Drive WestColumbia.SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 26 of 63 Level 1 Report v2.1
AR000318
Client: ARCADIS
Description: MW-13M060210
Date Sampled:06/02/2010 0920
Date Received:06/03/2010
Volatile Organic Compounds by GC/MS Laboratory ID: LF03012-012
) Matrix: Aqueous
~- . .
Run, 1
Prep Method 50308
Analyt ical Method 8260B
Dilution Analysis Date Analyst 1 06/10/2010 2227 DLB
Prep Date Batch 35610
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethan6 (EDB)
1,2-Dichlor;obenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,2-Trichloro-1,2,2-Trifluoroethahe
1,2,4-Trichloroben2ene
1,1,1 -Trichloroethane
1,1,2-Trichloroethane
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1 106-93-4
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2 75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
108-10-1
108-87-2
75-09-2
100-42-5'
79-34-5
127-18-4
108-88-3.
76-13-1
120-82-1
71-55-6
79-00-5
8260B
8260B
, 82608 .
82608
82608
8260B
82608
82608
82608
82608
8260B
8260B
82608
82608
82608
82608
82608
82608
• 82608
8260B
8260B
82608 •
82608
82608
8260B
• 8260B
8260B
8260B
8260B
8260B
82608
8260B
82608
. 82608
82608
8260B
82608
8260B
8260B
• 82608 •'
82608
82608
82608
8260B
ND
ND
ND
ND
ND
ND
ND •
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND.
ND ND
ND
ND
ND
ND '
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND .
ND
ND
ND
ND
ND
ND
ND
20
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0 •
5.0
5.0
5.0
5.0 5.0
5.0
5.0
5.0
5,0
5.0
5.0
10
5.0
.5.0
5.0 .
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
6.7
• 0.20
1.7
0.40
0.80
1.8
0.30 •
0.40
1.7
0.50
1.7
0.30
0.98
0.60
1.7
0.30
1 7
1.7
1.7
0.20
0.30-
0.30
0.50
0.20
0.40
0.30
0.30
0.30
1.7 .
1.0
1.0
• 0.72
0.40
0.80
0.95
1.7
0.10
0.40
0.40
17
. 0.30
. 1.7
0.20
0.30
ug/L 1
.ug/L . 1
. ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
- ug/L . 1
ug/L 1
ug/L 1
. ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L . 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L . 1
ug/L 1
^ ug/L . 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
. ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L , 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
. ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L ' 1
PQL = Practical quantitation limit 8 = Detected in the method blank
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services. Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 wv/w.shealylab.com
Page: 27 of 63 Level 1 Report v2.1
AR000319
Volatile Organic Compounds by GC/MS Client: ARCADIS
Description: MW-13M060210
Date Sampled:06/02/2010 0920
Date Received: 06/03/2010
Laboratory ID: LF03012-012
Matrix: Aqueous
Run Prep Method 1 5030B
Analytical-Method 8260B
Dilution Anjalysis Date Analyst r 06/10/2010 2227 . DLB
Prep Date Batch 35610
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total) ,
Surrogate
79-01-6
75-69-4
75-01-4
1330-20-7
82608
8260B
8260B
8260B
•ND
ND
ND
ND
5.0
' 5 .0
2.0
5.0
0.30
0.30
0.10
1.7 •
ug/L
ug/L
ug/L
ug/L
1
1
1
1
Run 1 Acceptance % Recovery Ljmits
1,2-Dichloroethane-d4
Bromofluorobenzene Toluene-d8
109
99
113
70-130
70-130
70-130
PQL = Practicalquantitation limit B = Detected in tlie mettiod blank ND = Notdeteaedatorabovethe MDL J = Estimated result < PQL and > MDL Where applicable, all soil sample analysis are reported on a dry'weight basis unless flagged with a "V^
E - Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40% N = Recovery is out of cnteria H = Out of holding time
Shealy Environmental Services, Inc. 106 Vantage Point Drive WestColumbia.SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 28 of 63 Level 1 Report v2.1
AR000320
^
Client:ARCADIS
Description: MW-12M060210
Date Sampled:06/02/2010 0850
Date Received:06/03/2010
Volatile Organic Compounds by GC/MS Laboratory ID: LF03012-013
Matrix: Aqueous
Run ,1
Prep Method 5030B
Analyt ical Method 82608
Dilution Analysis Date Analyst 1 06/10/2010 2249 DLB
Prep Date Batch 35610
Parameter CAS
Number Analyt ical
Method Result PQL MDL Units Run
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide) '
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane'
1,2-pibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlbrobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-DichlDroethane
1,1-DichlDroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-,Tetrachloroethane
Tetrachloroethene
Toluene
1,1,2-Trichloro-1,2,2-Trifiuoroethane
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1
i06-93-4
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
'107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
loa-io-i 108-87-2
75-09-2
100-42-5
, 79-34-5 127-18-4
108-88-3
76-13-1
120-82-1
71-55-6
79-00-5
8260B
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
8260B
8260B
8260B
82608
82608
82608
8260B
8260B
82608
8260B
82608
82608
82608
82608
82608
82608
8260B
8260B
8260B
82608
82608
82608
82608
82608
82608
82608
8260B
8260B
82608
82608
82608
82608
82608
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND'
ND
ND
ND
- ND
ND
ND
" ND
ND
ND
ND
ND
ND
ND
ND
ND
ND ND
ND
ND .
ND
ND
ND
20
5.0
5.0 .
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0 •
5.0
5.0
5.0
5.0
5.0
5.0
5.0.
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
6.7
0.20
.1.7
0.40
0.80
1.8
.0.30
0.40
1.7
0.50 '
1.7
0.30 •
0.98
0.60-
1.7
0.30
1.7
1.7
1.7
0.20
0.30
0.30
0.50
0.20
0.40
0.30. '
0.30
0.30
1.7
1.0
1.0
0.72
0.40
0.80
0.95
1.7
0.10
0.40
0.40
1.7
0.30
1.7
0.20
0.30
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L • 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
. ug/L 1
ug/L 1
'ug/L 1
ug/L 1
ug/L 1
ug/L, 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
. ug/L 1
ug/L 1
' ug/L 1
ug/L . 1
ug/L 1
ug/L 1
ug/L- 1
ug/L 1
. ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank ND = f>lot detected at or above the MDL J = Estimated result < PQL and > MDL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40% N = Recovery is out of critena H = Out of holding time
Shealy Environmental Services. Inc. 106 Vantage Point Drive WestColumbia.SC 29172 (803)791-9700 Fax (803) 791-9111 vww.shealylab.com
Page: 29 of 63 Level 1 Report v2.1
AR000321
Client:ARCADIS
Description: MW-12M060210
Date Sampled:06/02/2010 0850
Date Received: 06/03/2010
Volatile Organic Compounds by GC/MS Laboratory ID: LF03012-013 _
Matrix: Aqueous
Run / I
Prep Method '' 50308
Analyt ical Method 82608
Dilution Analysis Date Analyst 1 06/10/2010 2249 DLB
Prep Date Batch 35610
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total) /
Surrogate
79-01-6
75-69-4
75-01-4
1330-20-7
82608
82608
82608
82608
ND
ND
ND
ND
5.0
5.0
• 2.0
5.0
0.30
^0.30
0.10
1-7
ug/L
ug/L
ug/L
_ug/L
1
1
1
1
Run 1 Acceptance % Recovery Limits
1,2-Dichloroethane-d4
Bromofluorobenzene Toluene-d8
108
99
107
70-130
70-130 70-130
PQL = Practical quantitation limit ' B = Detected in the method blanit
NO = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40% . s,
N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services, Inc. 106 Vantage Point Drive WestColumbia.SC 29172 (803)791-9700 Fax (803) 791-9111 vww.shealylab.com
Page: 30 of 63 Level 1 Report v2.1
AR000322
I
Cl ientARCADIS
Description: MW-12D060210
Date Sampled:06/02/2010 1030 -
Date Received: 06/03/2010
Volatile Organic Compounds by GC/MS . •• , Laboratory ID: LF03012-014
Matrix: Aqueous
. • '
Run 1
Prep Method 5030B
Analyt ical Method 82608
Dilution Analysis Date 1 06/10/2010 2312
Analyst DLB
Prep Date Batch 35610
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-8utanone (MEK)
Carbon disulf ide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane-
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dlchloroefhene .
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-H6xanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane .
Tetrachloroethene
Toluene
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,2,4-Trichlorobenzene'
1,1,1-Trichloroethane
1,1,2-Trichloroethane
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3 '
74-87-3
'110-82-7
96-12-8
124-48-1 ,
106-93-4
95-50-1
541-73-1
106-46-7
75-71,-8
75-34-3
107-06-2 75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4
591-78-6
98-82-8
79-20-9
.1634-04-4
108-10-1
108-87;2
75-09-2
100-42-5
79-34-5
127-18-4
108-88-3
76-13-1
120-82-1
71-55-6
79-00-5
8260B
82608
82608
82608
82608
8260B
8260B
8260B
8260B
8260B -
82608
82608
82608
82608 •
8260B -
8260B
8260B
8260B
82608
82608
82608
82608
8260B
8260B
82608
82608
82608
82608
82608
82608
8260B
82608
- 82608
82608
82608
82608
. . 8260B -
8260B
82608
82608
82608
82608
8260B
82608
ND
ND
ND
ND
ND
ND
0.48
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND • ND
ND-
. ND
ND
ND
ND
ND
ND
ND
ND
ND
ND .
•.' ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
' 20
5.0
5.0
5.0
5.0
10
J 5.0
5.0
5.0
5.0
5.0
• 5.0
5.0
5.0
. 5.0
5.0
5.0
5.0
5.0'
-5.0
5.0
5.0 5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0 5.0
5.0
5.0
5.0
5.0
5.0
6.7
0.20
1.7
0.40
0.80
1.8
0.30
0.40
^1.7
0,50
1.7
0.30
0.98
0.60
1.7
0.30
1.7
1.7
1.7
0.20
, 0.30
0.30
0.50
0.20
0.40
0.30
0.30
0.30
1.7
1.0
1-0 0.72
0.40
0.80
0.95
. 1.7-
0.10
0.40
0.40
1.7
0.30
1.7
0.20
0.30
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
• ug/L . 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L ' 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L . 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L • 1
ug/L 1
ug/L 1 ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
PQL = Practical quantitation limit B = Detected in ttie method blank ND = Not detected at or above ttie MDL J = Estimated result < PQL and > MDL Whfere applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range P = The RPD between two GC column3,exceeds 40% N = Recovery is out of criteria H = Out of holding time
Shealy Environmenlal Services. Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 31 of 63 Level 1 Report v2.1
AR000323
'
Client:ARCADIS
Description: MW-12D060210
Date Sampled:06/02/2010 1030
Date Received:06/03/2010
Volatile Organic Compounds by GC/MS Laboratory ID: LF03012-014
Matrix: Aqueous '
Run Prep Method 1 5030B
Analytical Method Dilution Analysis Date Analyst 8260B 1 06/10/2010 2312. DLB
Prep Date Batch 35610
Parameter CAS
Number
Analyt ical Result PQL MDL Units Run
Trichloroethene
Trichlorofluoromethane
Vinyl chloride v
Xylenes (total)
Surrogate
- 79-01-6
75-69-4
75-01-4
1330-20-7
8260B .-
82608
8260B
82608
ND
ND
ND
ND
5.0
5.0
2.0
• 5.0
0.30
0.30
0.10
1.7
ug/L
ug/L
Ug/L
ug/L
1
1
1
1
Run 1 . Acceptance % Recovery Limits
1,2-DichlorQethane-d4
Bromofluorobenzene Toluene-d8
110
99
109
70-130
70-130
70-130
^- ( •
PQL = Practical quantitation limit B = Detected in the method blank
, ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "V^
E ~ Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services, Inc. " . 106 Vantage Point Drive • West Columbia, SC 29172 {803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 32 of 63 Level 1 Report v2.1
AR000324
ClientARCADIS
Description: MW-13D060210
Date Sampled:06/02/2010 1320
Date Received: 06/03/2010
Volatile Organic Compounds by GC/MS Laboratory ID: LF03012-015
' Matrix: Aqueous
'
Run Prep Method 1 5030B
Analyt ical Method 8260B
Dilution Analysis Date Analyst 1 06/10/2010 2334 ' DLB
Prep Date Batch 35610
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform •*
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,2-Trichloro-1,2,2-Triflubroethane
1,2,4-Trichlorob6nzene
1.1,1-Trichloroethane
1,1,2-Trichloroethane
67-64-1
71-43-2
75-27-4 r
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1 106-93-4
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2 75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
108-10^1
108-87-2
75-09-2
100-42-5
79-34-5
127-18-4
108-88-3
76-13-1
120-82-l '
71-55-6
79-00-5
82608
82608
82608
8260B
82608
82608
82608
82608
8260B
8260B
8260B
8260B
. 82608
82608
82608
82608
8260B
82608
82608
82608
82608
82608
8260B
8260B
82608 /
8260B 1
82608
8260B
8260B .
82608
82608
82608
82608
82608
' 82608
8260B
82608
82608
82608
8260B
• 82608
82608
82608
8260B
ND
ND
ND
ND
ND.
, ND
ND
ND
. ND
ND
ND
ND
ND
ND .
ND ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
'ND ND
ND
ND
ND
ND
ND
ND
ND
ND
, . ND-. ND
, ND
ND
ND
ND
ND
20
5.0 ..
5.0 .
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5;o^ 5.0
5.0
5.0 5.0
. 5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0 ..
5.0
5.0
5.0
5.0
5.0.
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0 •
5.0
5.0'
6.7
0.20
1.7
0.40
0.80
1.8
0.30 0.40
.1.7
0.50
1-7
0.30
0.98
0.60
1.7
0.30
1.7
1.7
1.7
0.20
' 0.30
. 0.30
0.50,
0.20
0.40
0.30 •
0.30
0.30
1.7
1.0
1.0
0.72
0.40
0.80
0.95
1.7
0.10
0.40 .
0.40
1.7
0.30
1.7
0.20
0.30
ug/L 1
• ug/L 1
ug/L i ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L ' 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L ^ i ug/L ' 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L • 1
ug/L • 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L". 1
ug/L 1
ug /L 1
ug/L 1
ug/L 1
ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank
ND = Not detected at or above the tJIDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E =.Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services. Inc. 106 Vantage Point Drive WestColumbia.SC 29172 (803) 791-9700 . Fax (803) 791-9111 www.shealylab.com
Page: 33 of 63 Level 1 Report v2.1
AR000325
. •
Client: ARCADIS
Description: MW-13D060210
Date Sampled:06/02/2010 1320
Date Received: 06/03/2010
Volatile.Organic Compounds by GC/MS
Laboratory ID: LF03012-015
Matrix: Aqueous
Run 1
Prep Method 50308'
Analytical Method 82608
Dilution Analysis Date Analyst • l ' 06/10/2010 2334 DLB
Prep Date Batch 35610
Parameter CAS
Number
Analyt ical
Method Result P Q L M D L Units R u n
TrichloroetJiene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
79-01-6
75-69-4
75-01-4
1330-20-7
82608
82608
82608
8260B
ND
ND
ND
ND
5.0
,5.0
2.0
5.0
0.30
0.30
o:io 1.7
ug/L
• ug/L
ug/L""
ug/L
1
1
1
1
R u n 1 A c c e p t a n c e % R e c o v e r y L i m i t s
1 ,2 -D ich lo roe thane-d4
B r o m o f l u o r o b e n z e n e
To luene -d8
108
100
106
7 0 - 1 3 0
7 0 - 1 3 0
•70 -130
PQL = Practical quantitation limit B = Detected in the method blanii
ND = Not dstected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "VV"
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria • H = Out of holding time
Shealy Environmental Services, Inc. 106 Vantage Point Drive WestColumbia.SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 34 of 63 Level 1 Report v2.1
AR000326
Client:ARCADIS
Description: FB-060210
Date Sampled:06/02/2010 1405.
Date Received: 06/03/2010
Volatile Organic Compounds by GC/MS Laboratory ID: LF03012-016^
Matrix: Aqueous
J • . • •
Run 1
Prep Method 5030B
Analytical Method 82608
Dilution Analysis Date Analyst 1 06/10/2010 2357 DLB
Prep Date Batch 35610
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromo6thane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
DichlorodifiuororfTethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1.2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-l-lexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE) -
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chjoride
Styrene
1,1,2,2-Tetrachloroethane ^
Tetrachloroethene
Toluene
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,2,4-Trichlorbbenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78T93 -3
'75-15-0 56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1. 106-93-4
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
•107-06-2 75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
108-10-1
108-87-2
75-09-2
100-42-5
79-34-5 . 127-18-4
108-88-3
76-13-1
120-82-1
71-55-6
79-00-5
82608
82608
82608
82608
8260B
82608
82608
8260B
82608
82608
82608
82608
8260B
8260B
82608 82608
82608
8260B
8260B
82608
82608
82608
82608
82608
8260B
82608
8260B
8260B
8260B
82608
82608
82608
82608
82608 .
82608
8260B
8260B
82608
82608
82608
8260B
82608
82608
82608
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
^ ND
ND
ND
ND
ND
ND
ND
ND
ND
ND ,
ND
ND
• ND-
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND •
ND
ND
ND
ND
ND ND
ND
. ND .
ND
ND
ND'
20
5.0
5.0
5.0
- 5.0
10
5.0
5.0
5.0
5.0
5:0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0 ' 5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0 '
5.0
10
5.0
-5.0
5.0
5.0
5.0
5.0
5 . 0 .
5.0
5.0
5.0
6.7
0.20
1.7
, .0.40
0.80
1.8
0.30
0.40
1.7
• 0.50
, 1.7
0.30
0.98
0.60
1.7
0.30
1.7
1.7
1.7
0.20 .
0.30
0 . 3 0 ^
0.50
0.20
0.40
0.30
0.30
0.30
1.7
1.0
1.0
0.72
0.40
0.80
0.95
1.7
., 0.10
0.40
0.40
1.7
0.30
1.7
0.20
0.30
ug/L. 1
ug/L 1
' ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1 ug/L , 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L • 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
'ug/L 1
ug/L 1
ug/L 1
ug/L • 1
ug/L - 1
ug/L 1
ug/L 1
ug/L 1
ug/L - 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1 ug/L 1
ug/L 1
~ ug/L 1
ug/L 1
ug/L 1
ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank
ND = Not detected al or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of alteria H = Out of holding time
Shealy Environmental Services. Inc.
106 Vantage Point Drive WestColumbia.SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 35 of 63 Level 1 Report v2.1
AR000327
Client:ARCADIS
Description: FB-060210
Date Sampled:06/02/2010 1405
Date Received:06/03/2010
Volatile Organic Compounds by GC/MS Laboratory ID: LF03012-016
Matrix: Aqueous
• ' ' . ' i '
Run 1
Prep Method , 50308
Analyt ical Method 82608
Dilution . Analysis Date Analyst 1 06/10/2010 2357 DLB
Prep Date Batch 35610
Parameter CAS
Number
Analyt ical
Method Result PQL MDL Units Run
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
79-01-6
75-69-4
75-01-4
1330-20-7
8260B
82608
82608
82608
ND
ND
ND
ND
5.0
5.0 ,
2:0
5.0
0.30
0.30
0.10
1.7
ug/L
ug/L
ug/L
ug/L.
1
1
1
1
Run 1 Acceptance % Recovery Limits
1,2-Dichloroethane-d4
Bromofluorobenzene Toluene-d8
109
99
108
70-130
70-130 70-130
PQL = Practical quantitation limit B = Detected in the method blanl<
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria H = Out oT holding time
Stiealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 36 of 63 Level 1 Report v2.1
AR000328
Client: ARCADIS
Description: Trip Blank
Date Sampled:06/03/2010
Date Received: 06/03/2010
Volatile Organic Compounds by GC/MS . Laboratory ID: LF03012-017
Matrix: Aqueous
Run 1
Prep Method 5030B
Analyt ical Method , 82608
Dilution' Analysis Date Analyst 1 06/11/2010 0019 DLB
Prep Date Batch 35610
Parameter CAS
Number
Analyt ical
Methgd Result PQL MDL Units Run
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane - -
Chloroform i
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-pichloroethene_
1,2-Dichloropropane
cisri ,3-Dichloropropene
trans-1.3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,2-TrichioroTl,2,2-Trifluoroethane
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
67-64-1
71-43-2
75-27-4
75-25-2
• 74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1 106-93-4
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
10061-01-5
10061-02-6
•100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
108-10-1
10'8-87-2
75-09-2
100-42-5
79-34-5
127-18-4
108-88-3
76-13-1
120-82-1
71-55-6
79-00-5
8260B
82608
82608
82608
82608
82608
82608
8260B
8260B
8260B
82608
82608
• 8260B
8260B
8260B
8260B
82608
8260B
8260B
8260B
8260B
- 8 2 6 0 8 .
82608
82608
8260B
8260B
8260B
8260B
82608
82608
82608
82608
8260B
8260B
8260B
82608
82608
82608
8260B
82608 .
82608
82608
82608
8260B
ND
ND
ND^
ND
ND
ND
ND ND'
ND
ND^
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
. ND
^ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND -
ND
ND
20
5.0
5.0
5.0
5.0
10
5:0 5.0
• 5.0
5.0
5.0
5.0
5.0
5.0
5:0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5..0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0.
5.0
5.0
6.7
0.20
• 1.7
0.40
0.80
1.8
.0.30
0.40
1.7
0.50
1.7
0.30
0.98
0.60
1.7
0.30
1.7
1.7
1.7
0.20
0.30
0.30
• 0.50
0.20
0.40
0.30
0.30
0.30
1.7
1.0
1.0
0.72
0.40
0.80
0.95
1.7 •
0.10
0.40
, 0.40
1.7
0.30
1-7,
0.20
0.30
ug/L , 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L. , 1
ug/L 1
ug/L . 1
ug/L 1
ug/L 1
, ug/L 1
ug/L 1
ug/L 1
ug/L 1
. ug/L 1
ug/L ' 1
ug/L • 1
ug/L 1
ug/L 1
ug/L • 1
ug/L 1
ug/L' .1
ug/L • 1
ug/L 1
ug/L 1
. ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L 1
. ug/L 1
ug/L 1
ug/L 1
ug/L 1
. ug/L 1
ug/L 1
ug/L 1
ug/L 1
ug/L -. 1
ug/L 1
ug/L 1
ug/L . 1
PQL = Practical quantitation limit B = Detected in the method blank ND = Not detected at or above the MDL J = Estimated result < PQL and > rviDL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W
E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services. Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 wvw.shealylab.com
Page: 37 of 63 Level 1 Report v2.1
AR000329
Client:ARCADIS
Description: Trip Blank
Date Sampled:b6/03/2010
Date Recelved:06/03/2010
Volatile Organic Compounds by GC/MS Laboratory ID: LF03012-017
Matrix: Aqueous
• '
Run 1
Prep Method 50308
Analytical Method Dilution ' Analysis Date Analyst 82608 1 06/11/2010 0019 DLB
Prep Date Batch 35610
Parameter CAS
Number
Analyt ical
Method Result P Q L M D L Units R u n
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
79-01-6
75-69-4
75-01-4
1330-20-7
82608
82608
8260B
8260B
ND
ND
ND
ND
5.0
5.0
2.0
5.0
0.30
0.30
0.10
1.7
ug/L
ug/L
ug/L
^ ug/L
. 1
1
1
1
Run 1 Acceptance % Recovery Limits
1,2-Dichloroethane-d4
Bromofluorobenzene Toluene-d8
114
97
113
70-130
70-130
70-130
PQL = Practical quantitation limit B = Detected in the method blank
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
N = Recovery Is out of criteria H = Out of holding time
Shealy Environniental Services! Inc. 106 Vantage Point Drive WestColumbia.SC 29172 (803)791-9700 Fax (603) 791-9111 www.shealylab.com
Page: 38 of 63 Level 1 Report v2.1
AR000330
QC Summary
Shealy Environmental Services. Inc. ,, Page: 39 of 63 106 Vantage Point Drive West Columbia, SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com Level i Report v2.i
AR000331
Volatile Organic Compounds by GC/MS - MB
Sample ID: LQ35427-001
Batch: 35427
Analyt ical Method: 8260B
Matrix: Aqueous
Prep Method: 50308
Parameter Result Dil PQL MDL Units Analysis Date
Acetone ND
Benzene ND
Brohnodich|ororhethane ND
Bromoform ND
Bromomethane (Methyl bromide) ND
2-8utanone (MEK) ND
Carbon disulfide ND
Carbon tetrachloride ND
Chlorobenzene ND
Chloroethane • ND
Chloroform ND
Chloromethane (Methyl chloride) ND
Cyclohexane ND
1,2-Dibromo-3-chloropropane (DBCP) ND
Dibromochloromethane ND
1,2-Dibromoethane (EDB) ND
1.,4-Dichlorobenzene ND
1,3-Dichlorobenzene ND
1,2-Dichlorobenzene , ND
Dichlorodifluoromethane .ND
1,1-Dichloroethane . • ND
1,2-Dichloroethane ND
cis-1,2-Dichloroethene ND
1,1-Dichloroethene ND
trans-1,2-Dichloroethene ND
1,2-Dichloropropane ND
cis-1,3-Dichloropropene ND
trans-1,3-Dichloropropene ND
Ethylbenzene ND
2-Hexanone ND
Isopropylbenzene ND
Methyl acetate ND
Methyl tertiary butyl ether(MT8E) ND
4-Methyl-2-pentanone ND
Methylcyclohexane ND
Methylene chloride ND
Styrene ' ND
1,1,2.2-Tetrachloroethane ND
Tetrachloroethene ND
Toluene ND
1,1,2-Trichloro-1,2,2-Trifluoroethane ND
1,2,4-Trichlorobenzene ND
1,1,2-Trichloroethane ND
1,1,1-Trichloroethane ND
20
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5,0
5.0
5.0 •
5.0
5.0
5.0
5.0 -*
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
6.7
0.20
1.7 .
0.40
0.80 •
1.8
0.30 1
• 0.40
1.7
0.50
1.7
0.30
0.98
0.60
1.7
0.30
1.7
1.7
1.7
0.20
0.30 • '
0.30
0.20 0.50
0.40
0.30
0.30
0.30
i.7 1.0
1.0
0.72
0.40
0.80
0.95
1.7
0.10
0.40
0.40 •
1.7
0.30 ^.
1.7
0.30
0.20
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
• ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
. 'ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
' ug/L
ug/L
ug/L •
ug/L
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/2010 1620
06/08/20101620
' 06/08/2010 1620
06/08/2010 1620
PQL = Practical quantitation limit P = The RPD between tA'o GC columns exceeds 40%
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, alt soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
N - Recovery is out of criteria
• - RPD is out of criteria
Shealy Environmental Services. Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 40 of 63 Level 1 Report v2.1
AR000332
Volatile Organic Compounds by GC/MS - MB
Sample ID: LQ35427-001
Batch: 35427
Analyt ical Method: 82608
Matrix: Aqueous
Prep Method: 50308
Parameter Result
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
ND
ND
ND
ND
Dil PQL MDL Units
% Rec
1
1
1 , 1
Acceptance Limit
Analysis Date
5.0
5.0,
2.0
5.0
0.30
0.30
0.10
1.7
ug/L
ug/L
ug/L
ug/L
06/08/2010 1620
06/08/20101620
06/08/2010 1620
06/08/2010 1620
Bromofluorobenzene
1.2-Dichloroethane-d4
Toluene-d8
102
104
112
70-130
70-130
70-130
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40%
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
N - Recovery is out of criteria
+ - RPD IS out of criteria
Shealy Environmental Services. Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803)791-9700 Fax (803) 791-9111 vrtvw.shealylab.com
Page:,41 of 63 Level 1 Report v2.1
AR000333
Volatile Organic Compounds by GC/MS r LCS
, Sample ID: LQ35427-002
Batch: 35427
Analyt ical Method: 8260B
Matrix: Aqueous
Prep Method: 50308
Parameter
Spike Amount (ug/L)
Result .(ug/L) Dil % Rec
% Rec Limit Analysis Date
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-8utanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropahe (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,4-Dichlorobenzene
1,3-Dichlorobenzene
1,2-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
cis-1,2-Dichloroethene
1,1-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichlcjropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone :
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene Toluene
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,2,4-Trichlorobenzene
1,1,2-Trichloroethane
1,1,1-Trichloroethane ',
100
50
50
50
' 50
100
50
50
50
5 0 .
50
50
50
50
50
50
50
50
50
50
50
50
. 50 . 50
50
50
50
50
50
100
50
50
50
100
50
50
50
50
50
50 •
50
50 - ,
50 •
50
110
55
55
49
48
110
58
48
52
36
53
46
42
52
54
55
54
56
55
43
52
53
55
.53
54
53
52
51
58
110
55
59
59
100
38
54
55
55
54
^ 58
39
53
51
50
1 - 105
1 110
1 110
1 98
1 V 95 '
1 107
1 116
1 96
1 • 105
1 72
1 105
1 92
1 83
1 103
1 109
1 . I l l , 1 108
1 113
1 109
1 86
1- 105
1 107 •
1 110 1 107
1 109
1 106
1 ' 104
1 101
1 116 •
1 107
1 109
1 118
1 . 118
1 . ' 105
1 76
1 108
1 109
1 111
1 108
1 117
1 77
1 106
1 102
1 • . 100
46-153
72-127
71-143
65-131
36-168
60-140
60-140
37-166
78-129
42-163
63-123
20-158
70-130 ,
70-130
74-134
70-130
70-130
70-130
70-130
10-158
69-132
59-143
70-130
50-132
70-130
71-126
69-130
73-131
79-132
60-140
70-130
15-128
70-130
60-140
70-130
69-129
70-130
60-155
70-130
75-125
70-130
70-130
77-132
77-132
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
. 06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
06/08/2010 1416
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40%
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged v th a 'W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
N - Recovery is out of critena
+ - RPD is out of criteria
Shealy Environmental Services. Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 42 of 63 Level 1 Report 2.1
AR000334
Volatile Organic Compounds by GC/MS - LCS
Sample ID: LQ35427-002
Batch: 35427
Analyt ical Method: 82608
Parameter
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
Bromofluorobenzene
1,2-Dichloro6thane-d4
Toluene-d8
-
Spike Amount (ug/L)
50
50
50
100
Q % Rec
109
101 •
112
/
Result (ug/L) Q
54
43
43
110,
Acceptance Limit
70-130
70-130
. 70-130
Matrix:
Prep Method:
Dil
1
1
1
1
Aqueous
50308
'
% Rec
108
86
87
113
% R e c Limit
73-124
41-173
29-159 '
70-130
' Analysis Date
06/08/2010 1416
06/08/2010 1416
. 06/08/2010 1416
06/08/2010 1416
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40%
ND = Not detected at or above the MDL J = Estimated result < PQL and iMDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a ' W
Note: Calculations are performed before rounding to avoid round-off errors in calctj iated results
N - Recovery is out of criteria
+ - RPD is out of criteria
Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172' (803).791-9700 Fax (803)791-9111 www.shealylab.com
Page: 43 of 63 Level 1 Report v2.1
AR000335
Volatile Organic Compounds by GC/MS < LCSD
Sample ID
Batch
Analyt ical Method:
Parameter
LQ35427-003
35427 • f
82608
Spike Amount
(ug/L) Result (ug/L) Q
Matrix: Aqueous
Prep Method: 50308
Dil % Rec % RPD % Rec Limit
% RPD Limit
1
Analysis Date
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-8utanon6 (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,4-Dichlorobenzene
1,3-Dichlorobenzene
1,2-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
cis-1,2-Dichloroethene
1,1-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-pichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,2-Trichloro-1,2,2-Trinuoroethane
1,2,4-Trichlorobenzene
1,1,2-Trichloroethane
1,1,1-Trichloroethane
100 50
50
50
50 100
50 50
50
50
50
50
50
50
50 50 50
50
50 50
50
50
50 50
50
50
50 50
50
100
50
50 50
100
50
50
50
50
50 50
50
50
50
50
83
56 55
47
• 47
93 61 49
54
45
52
47
46 47
53 52
54 58
55
46
53 51
, 55 ' 57
56 54
53
50
60 98
57
46
57
99
40
57
56 54
55 60
41 53
49
51
1 83 .
1 113 ^
1 110
1 93
1 94
1 93
1 122
1 • 99
1 107
1 90
1 105
1 94
1 . 9 2
1 94
1 107 1 105
1 109
1 115
1 110
1 91
1 105
1 103
1 111
1 113
1 112
1 108
1 105
1 100
1 120
1 98
1 115,
1 91
1 . 114
1 99
1 80
1 114
1 111
1 107
1 - 111
1 120
1 82
1 ^ 105
1 99
1 102
24-
2.1
0.47
4.7
1.6
15
4.8
3.1
2.2
22
0.65
2.6
11
9.5
1-8 5.7
1.0
2.2
0.75
5.7
0.32
3.8
0.54.
5.9
3.4
1.5 •
1.1
1.2
3.7
8.2
4.9
26
4.2
, 5.9
4.4
5.6
1.9
3.6
3.0
2.5
6.2
0.55
3.3
2.5
46-153
72-127
-' 71-143
65-131
36-168
60-140
60-140 .37-166
78-129
' 42-163-
-63-123
20-158
70-130
70-130
74-134 70-130
70-130
70:130
70-130
10-158 •
69-132
59-143
70-130 ^
50-132
70-130 ,
71-126
69-130
73-131
79-132
60-140
70-130
15-128
70-130
60-140
70-130
69-129
70-130
60-155
70-130
75-1,25
70-130
70-130
77-132
77-132
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
- 20
20
20
20
20
20
20
20
20
20
20
20
20^
20
20
20
20
20
20
20
20
20
20
20
20
20
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438 06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
. PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40%
ND = Not detected at or above the MDL J = Estimated result < PQL and >_MDL
Wiiere applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
N - Recovery is out of criteria
+ - RPD is out of critena
Shealy Environmental Services. Inc. / ' 106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 vrtvw.shealylab.com
Page: 44 of 63 Level 1 Report V2.1
AR000336
Volatile Organic Compounds by GC/MS - LCSD
Sample ID: LQ35427-003
Batch: 35427
Analy t ica lMethod: 82608
Parameter
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
Bromcjfluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
Spike Amount (ug/L)
50
• 50
50
100
, Q % Rec
109.
98
118
Resi J It (ug/L)
55
45
46
120
'
Q
Acceptance Limit
70-130
70-130
70-130
Prep
Dil
1
1
1
1
Matrix: Aqueous
Method: 5030B
% Rec % RPD
110 - 2.5
90 3.9 .
91 5.0
116 2.8
% Rec Limit
73-124
41-173
29-159
70-130
% RPD Limit
20
20 .
20
20
Analysis Date
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
06/08/2010 1438
(
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40%
ND = Not detected at or above the MDL J = Estimated result < PQL and >.MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a 'W"
Note: CalcuJations are performed before rounding to avoid round-off errors in calculated results
N - Recovery is out of critena
+ - RPD is out of criteria
Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 {803)791-9700 Fax (803) 791-9111 vmw.shealylab.com
Page: 45 of 63 Level 1 Report v2.1
AR000337
Volatile Organic Compounds by GC/MS - MB
Sample ID: LQ35556-001
Batch: 35556
Analyt ical Method: 82608
Matrix: Aqueous
Prep Method: 50308
Parameter Result Dil PQL MDL Units Analysis Date
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-8utanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chlorornethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,4-Dichlorobenzene
1,3-Dichlorobenzene
1.2-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
cis-1,2-Dichlorpethene.
trans-1,2-Dichloroethene
1,1-Dichloroethene
1,2-Dichloropropane
cis-1.3-Dichloropropen6
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1.2-Trichloro-1,2,2-Trifluoroethane
1,2',4-Trichlorobenzene
1,1,2-Trichloroethane
1,1.1 -Trichloroethane
/
ND' ND -ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
20
5.0
5.0
5.0 '
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0 5.0
5.0
5.0 •
5.0
5.0
5.0
5.0
5.0 5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
6.7
0.20
1.7
0.40
0.80
1.8
0.30
0.40
1.7
0.50
1.7
0.30-
0.98
0.60
1.7
0.30
1.7
1.7
1.7
0.20
0.30
0.30
.0.20
0.40
0.50
0.30
0.30
0.30
1.7
1.0
1.0
0.72
0.40
0.80
0.95
- 1.7
0.10
0.40
0.40
1-7
0.30
1.7
0.30 •
0.20
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
. ug/L
ug/L
ug/L .
ug/L
ug/L . ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L I ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
•ug /L
ug/L
ug/L
ug/L
ug/L
06/10/2010 1618'
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618,
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618 06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618'
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
PQL = Practical quantitation limit P = Tlie RPD between two GC columns exceeds 40%
ND = Not detected at or above the MDL J = Estimated result < PQL and >. MDL
Wtiere applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a 'W
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
N - Recovery is out ot criteria
+ - RPD is out ot criteria
Shealy Environmental Services. Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 vAvw.shealylab.com
Page: 46 of 63 Level 1 Report v2.1
AR000338
Volatile Organic Compounds by GC/MS - MB
Sample ID: LQ35556-001
Batch: 35556
Analyt ical Method: 8260B
Matrix: Aqueous
Prep Method: 50308
Parameter Result Dil PQL MDL Units Analysis Date
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate "*
ND
ND
ND
ND
Q
,
% Rec
106
92
98
1
1
1
1
Acceptance Limit
70-130
70-130
70-130
5.0
5.0
2.0
5.0
0.30
0.30
0.10
1.7
.. ug/L .
ug/L
ug/L
ug/L
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
Bromofluorobenzene
1.2-Dichloroethane-d4
Toluene-d8
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40%
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weigtit basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
N - Recovery is out of criteria
+ - RPD is out of criteria
Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia. SC. 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com.
Page: 47 of 63 Level 1 Report v2 1
AR000339
Volatile Organic Compounds by GC/MS - LCS
Sample ID: LQ35556-002
Batch': 35556
Analyt ical Method: 82608
Matrix: Aqueous
Prep Method: 5030B
Parameter
Spike Amount
(ug/L) Result (ug/L) Dil % Rec
% Rec Limit Analysis Date
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromornethane (Methyl bromide)
2-8utanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1.2-Dibromoethane (EDB)
1,4-Dichlorpbenzene
1,3-Dichlorobenzene
1,2-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichl6roethane
1,2-Dichloroethane
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,1-Dichloroethene
1,2-Dichloropropane
cis-1.3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene .
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
.1,1,2-Trichloro-1,2,2-Trifluoroethane
1,2,4-Trichlorobenzene
1,1,2-Trichloroethane
1,1,1 -Trichloroethane
100 50
50
50
50
100
50 50 50
50
50 50
50
50
50 50
50
50
50
50
50
50
50. ' 50 50
50
50
50
50
100 50
50
50
100
50 50
50
50
50 . 50
50
50 50
50
97 47
51
42
47
100
56 47
46
48
50 47
53
52
44 49
47
48
47
• 49
. 4 9
50 49 48
49
49
•'47
46
48
100 50
53
49
110
53 48
45
52 49 49
61
50
47
52
1 97
1 95
1 102
1 83
1 - 9 4
1 ioi 1 112
1 93
1 93
1 • • - 9 7
1 99
1 93
1 .106
1 . 103
.1 . 88
1 98
1 95
1 96 \ ,
1 95
1 99
1 99
1 100
1 99
1 97
1 97
1 • 98 '
1 95
1 ' 93
1 . 96 .
1 , 1 0 4
1 99
1 105
1 97
1 106 •
1 105
1 96
1 9b
1 104
1 • 97
1 98
1 . 123
1 100
1 94
1 103
,46-153
• 72-127
71-143
65-131
36-168
60-140
60-140
37-166
78-129
42-163
63-123
20-158
70-130
70-130
74-134
70-130
70-130,
70-130
70-130
10-158'
69-132
59-143
70-130
70-130
50-132
71-126
69-130
73-131'
79-132.
60-140
70-130
15-128
70-130
60-140
70-130
69-129
70-130
60-155
70-130 75-125
70-130
'70-130
,77-132
77-132
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
V P = The RPD between two GC columns exceeds 40% PQL = Practical quantitation limit
ND = Not detected at or above the MDL J = Estimated result < PQL and >MDL
Where applicable, all soil sample analysis are reported on a dry Weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
N - Recovery is out of criteria
+ - RPD is out of criteria
Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 48 of 63 Level 1 Report v2.1
AR000340
Volatile Organic Compounds by GC/MS - LCS
Sample ID: LQ35556-002
• Batch: 35556
Analyt ical Method: 8260B
Parameter
. Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate '
Bromofluorobenzene
1,2-Dichlqroethane-d4
Toluene-d8
Spike Amount (ug/L)
50
50
50
100
Q % Rec
107
97
100
Result (ug/L) Q
47
51 •
49
97
Acceptance Limit
70-130
70-130
70-130
, Matrix:
Prep Method:
Dil
1 .
1
1 . .
1
Aqueous
50308
% Rec
95
102
97
97
.
% Rec Limit
73-124
41-173
29-159
70-130
'
1
Analysis Date
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
06/10/2010 1445
,
/
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40%
ND = Not detected at or above the MDL j = Estimated result < PQL and ^ MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
N - Recovery is out of criteria
+ - RPD is out of cnteria
Shealy Environrnental Services, Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 49 of 63 Level 1 Report v2.1
AR000341
Volatile Organic Compounds by GC/MS - LCSD
Sample ID:
Batch
Analyt ical Method:
Parameter
LQ35556-003
35556
82608
Spike Amount
(ug/L) Result (ug/L) Q
Matrix: Aqueous
Prep Method: 50308
Dil % Rec % RPD % Rec' L imit
I
% RPD Limit
)
Analysis Date
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chloroberizene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,4-Dichlorobenzene
1,3-Dichlorobenzene
1,2-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,1-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,2,4-Trichlorobenzene
1,1,2-Trichloroethane
' 1,1,1-Trichloroethane
100 50
50
50
50-
100
50 50
50
50 50
50
50.-
50
50 50
50 50
50
50
50 50
50 50
50
50
50
50
50
100
50
50
50
100
50 50
50
50
50 50 50
50
50
50
87 47
50
41
45
92
53 45
46
46
48
44
50 50
44 48
47 47
. 47
45
47
48 47 . 46 46
48
46
- 45
47
98
49
48
46
100
51
46.
44 50
48 - 48
59
49 46
49
1 87
1 94
1 100 •
1 82
1 89
1 92
1 107
1 90
1 92
1 91
1 95
1 87
1 • '100
1 100
1 , 87 1 97
1 94
1 94
1 94
1 91
1 94 .
1 ,96
1 , 95
r 93
1 93
1 95
1 93
1 91
1 95
1 98
1 99
1 95
1 9 2 .
1 100
1 103
1 91
1 88
1 100
1 96-1 96
1 118
1 98
1 93^
1 . 98
10
0;72
1.9
1.3
4.9
8.8
4.4
4.2
1.2
5.7
4.3
6.6
6.3
3.4
0.84
1.8
1.3
1.8
0.86
8.2
5.4
4.9
4 . 1 - ' ,
4.2
4.8
2.3
2.2
2.3
1.2
5.9
0.84
9.6
' 5.6
6.0
2.3
5.2
2.2
3.8
1.6 '
1.7
' 4.2
1.6
0.89
5.0
46-153
72-127
71-143 ,
65-131
36-168
60-140
60-140.
37-166
78-129
42-163
63-123
20-158
70-130
70-130
74-134
70-130
70-130
70-130
70-130
10-158
69-132
59-143
70-130 70-130
50-132
,71-126
69-130
73-131
. 79-132
60-140
^ 70-130
15-128
70-130
60-140
70-130
69-129
70-130
60-155
' 70-130
75-125
• 70-130
70-130
77-132
77-132
20
20
2,0
20
20
20
20
20
20
20
20
20
. 20
20
20
20
20
. 20
20
>• 20
20
20
20
20
20
20
20
20
20
.20
20
20
20
20
20
20
20
20
20
20
20
20
20 .
20
06/10/2010 1508
•06/10/2010 1508
06/10/20101508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
,06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/20101508
06/10/2010 1508
PQL = Practical quantitation limit ^ P = The RPD between two GC columns exceeds 40%
ND = Not detected at or above thfe MDL J = Estimated result < PQL and >_ MDL
Where applicable, all soil sample analysis are reported pn a dry weight basis unless nagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
N - Recovery is out of criteria
+ - RPD is out of criteria
Shealy Environmental Services, Inc. 106 Vantage Point Drive- WestColumbia.SC 29172 (803)791-9700 Fax (803) 791-9111 vww.shealylab.com
Page: 50 of 63 Level 1 Report v2.1
AR000342
. J Volatile Organic Compounds by GC/MS - LCSD
Sample ID: LQ35556-003
Batch: 35556
Analyt ical Method: 8260B
Matrix: Aqueous
Prep Method: 50308
Parameter
Spike Amount (ug/L)
Result (ug/L) Dil % Rec % RPD
% Rec. % RPD Limit Limit Analysis Date
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
50
50
50
100
k Rec
107
93
100
47
48
45
95
Acceptance Limit
70-130
70-130 '
70-130
1
1
1
1
95
95
91
95
0.29
7.1
6.6
1.9 .
73-124
41-173
29-159
70-130
20
20
20
20
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
06/10/2010 1508
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
' PQL =. Practical quantitation limit P = The RPD between two GC columns exceeds 40%
ND = Not detected afor above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
N - Recovery is out of critena
+ - RPD is out of criteria
Shealy Environmental Services. Inc. 106 VantagePoint Drive West Columbia, SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 51 of 63 Level 1 Report v2.1
AR000343
Volatile Organic Compounds by GC/MS - MB
Sample ID: LQ35603-001
Batch: 35603
Analytical Method: 82608
Matrix: Aqueous
Prep Method: 50308 .
Parameter Result Dil PQL
20
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0 •
5.0
5.0
5.0 '
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10 .
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0 "
5.0
MDL
6.7
0.20
1.7
0.40
0.80
1.8
0.30 0.40
1.7
0.50
1.7
0.30
0.98
0.60
1.7
0.30
1.7
1.7
1.7
0.20
0.30
0.30
0.40
0.20
0.50'
0.30
0.30
0.30
1.7
1.0 ''
.1.0
0.72
0.40
0.80
0.95
1.7
0.10
0.40
.0.40 1.7
0.30
1.7
0.30
0.20
Units
' • ug/L
-,ug/L
ug/L
ug/L
ug/L
ug/L .
ug/L
ug/L
ug/L
ug/L^
ug/L
.ug/L
ug/L
ug/L
ug/L
ug/L
• ug/L
ug/L
ug/L
.ug/L
ug/L
ug/L
. ug /L- .
. ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Analysis Date
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
' 06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/20100959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/.10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 095?
06/10/2010 0959
Acetone ND
Benzene ND
Bromodichloromethane ND
Bromoform ND
Bromomethane (Methyl bromide) ND
2-Butanone (MEK) ND
Carbon disulfide N ND
Carbon tetrachloride ND
Chlorobenzene ND
Chloroethane ND
Chloroform ND
Chloromethane (Methyl chloride) ND
Cyclohexane ND
1,2-Dibrorino-3-chloropropane (DBCP) ND
Dibromochloromethane ND
1,2-Dibromoethane (EDB) ND
1,4-Dichlorobenzene ND
1,3-Dichlorobenzene ND
1.2-Dichlorobenzene ND
Dichlorodifluoromethane ND
1,2-Dichloroethane ND
1,1-Dichloroethane ND
trans-1,2-Dichloroethene ND
cis-1,2-Dichloroethene 'ND
1;1-Dichloroethene ND
1,2-Dichloropropane ND
trans-1,3-Dichloropropene ND
cis-1,3-Dichloropropene ND
Ethylbenzene ND
2-Hexanone ND
Isopropylbenzene . ND
Methyl acetate ND
Methyl tertiary butyl ether (MTBE) • ND
4-Methyl-2-pentanone ND
Methylcyclohexane i ND
Methylene chloride ND
Styrene , ND
1,1,2.2-Tetrachloroethane ND
Tetrachloroethene ND
Toluene ND
1,1.2-Trichloro-1,i2,2-Trifluoroethane ND
1,2,4-Trichlorobenzene 2.3
1,1,2-Trichloroethane ND
1,1,1-Trichloroethane ( . ND
r
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40%
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
N - Recovery is out of critena
+ - RPD is out of criteria
Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 52 of 63 Level 1 Report v2 1
AR000344
Volatile Organic Compounds by GC/MS - MB
Sample ID: LQ35603-001
Batch; 35603
Analyt ical Method: 82608
Matrix: Aqueous
Prep Method: 50308
Parameter r
Result Dil PQL MDL Units Analysis Date
Trichloroethene
Trichlorofluoronnethane
Vinyl chloride
Xylenes (total)
Surrogate
ND
ND
ND
ND
Q % Rec
99
107
106
1
1
1
1
Acceptance Limit
70-130
70-130
70-130
5.0
5.0
2.0
5.0
• - .
0.30
0.30 .
0.10 .
1.7
ug/L
ug/L
ug/L
ug/L .,
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
06/10/2010 0959
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
PQL! = Practical quantitation limit P = Tfie RPD between two GC columns exceeds 40%
ND = Not detected at or above the MDL J = Estimated result < POL and MDL
Where applicable, atl soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in'calculated results
N - Recovery is out of criteria
+ - RPD is out of criteria
Shealy Environmental Services. Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 vmw.shealylab com
Page: 53 of 63 Level 1 Report v2.1
AR000345
Volatile Organic Compounds by GC/MS - LCS
Sample ID: LQ35603-002
Batch: 35603
Analyt ical Method: 82608
Matrix: Aqueous
Prep Method: .5030B
Parameter
Spike Amount
(ug/L) Result (ug/L) Dil % Rec
% Rec Limit Analysis Date
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-8utanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,4-DichlQrobenzene
1,3-DichlQrobenzene
1,2-Dichlorobenzene
Dichlorodifluoromethane
1,2-Dichloroethane
1,1-Dichloroethane
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
1,1-Dichloroethene
1,2-Dichloropropane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene '
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,2,4-Trichlorobenzene
1,1,2-Trichloroethane
1,1,1-Trichloroethane
40
20
20
20
20
40
20
20
20
20
20
20 •
20
20
20
20
20 _
20
20
20
20
20
20
20
20
20
20
20
20
40
20
20
20
40
20
20
20
20
20
20
20 /
20 20
20
52
19
18
22
18
•45
3.6
21
18
18
19
21
23
20
20 19
19
19
19
21
15
20
. 20
19 21
18
19
20
19
37
15
22
20
37
21
18
17
19
19
20
24
17
18
21
1 131
1 94
1 92
1 111
1 92
1 112
1 18
1 104
1 91
1 90
1 ' 9 6
1 105
1 114
1 100
1 100
1 -.93
1 ' 94
1 95
1 94
1 107
1 76
1 98
1 101
1 • '96
1 106
1 92
1 96
1 98
1 , 97,
1 92
^• 73
1 111 .
1 100
1 92
1 104
1 92
1 83
r 94
1 95
1 100
1 120
1 • 86 '
1 88
1 105
46-153
72-127
71-143
65-131
36-168
60-140
60-140
37-166
78-129
42-163
63-123
• 20-158
70-130
70-130
74-134
70-130
70-130
70-130
70-130
10-158
59-143
69-132
70-130
70-130
50-132
71-126
73-131
69-130
79-132
60-140 •
70-130
15-128
70-130
60-140
70-130
69-129
70-130
60-155
70-130
75-125
70-130
70-130
• 77-132
77-132
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010;p855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
. 06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855 06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
(
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40%
ND = Not detected al or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
N - Recovery is out of critena
+ - RPD IS out of criteria
Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 vrtvw.shealylab.com
Page: 54 of 63 Level 1 Report v2.1
AR000346
Volatile Organic Compounds by GC/MS - LCS
Sample ID: LQ35603-002
Batch: 35603
Analyt ical Method: 82608
Parameter
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
Spike Amount
(ug/L)
, 20
20
20
40
Q ' '/o Rec
104 '
106
108
Result (ug/L) Q
18
23
21 •.
36
Acceptance Limit
70-130
70-130
70-130
Matrix:
Prep Method:
Dil
1
1
1
1,
Aqueous
50308
% Rec
92
113
103
90
'
% Rec Limit
73-124
41-173
29-159
70-130
Analysis Date
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
06/10/2010 0855
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40%
ND = Not detected at or above the MDL . J = Estimated resulK PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
N - Recovery is out of criteria
+ - RPD is out of criteria
Shealy Environmental Services. Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 55 of 63 Level 1 Report v2.1
AR000347
Volatile Organic Compounds by GC/MS - LCSD
Sample ID: LQ35603-003
Batch: 35603
Analytical Method: 62608
Matrix: Aqueous
-Prep Method: 50308
Parameter
Spike Amount
(ug/L) Result (ug/L) Dil % Rec % RPD
% Rec Limit
% RPD Limit Analysis Date
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-8utanone (MEK) '
Carbon disulflde
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (D8CP)
Dibromochloromethane
T,2-Dibromoethane (EDB)
1,4-Dichlorobenzene
1,3-Dichlorobenzene
1,2-Dichlorobenzene
Dichlorodifluoromethane
1,2-Dichloroethane
1,1-Dichloroethane
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
1,1-Dichloroethene
1,2-Dichloropropane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,2,4-Trichlorobenzene
1,1,2-Trichloroetharie
1,1,1-Trichloroethane
40
20
20
20
20
40
20
20
20
20
20
20
20
20
20
20'
20
20
20
20
2 0 .
20
20
20
20 '
20
20
20
20
40
20
20
20
40
20
20
20
20
20
20
20
20
20
20
56
20
20
21
22
47
23
22
20
20 '
20
21-
24
21
- 20
20
20
21
21
21
17
21
21
21
23
> 20
20
21
21
41
17
23
22
41
22
19
18
.21
21
22
25
19
• 19
23
1 139
1 102
1 98
1 103
1 111
1 . . 117
1 117
1 112
1 99
1 102
1 102
1 104
1 121
1 105
1 99
1 100
1 101
1 . 103
1 103
1 104
1 86
1 105
1 106
1 104 ,
1 114
1 . 100
1 100
1 103
1 105
1 .103
1 83
1 114
1 108
1 102
1 111
1 95 •
1 92
1 103 ' _
1 • 104 '
1 108
1 124
1 - 96
1 97
1 113
6.1
7.9
5.9
7.3
18
4.3-
150
6.6
8.5
12
. 6 . 5
1.4
6.1
5.5
1.6
8.1
• 7.7
7.8
9.2
2.5
12
7.1.
5.2
8.1
7.6
8.3
4.8
5.5
7.7
11 12
2.4
8.0
10
6.4
3.9
9.6
9.1
. 9.7 7.8
3.1 '
11
9.7
7.6
46-153
72-127
71-143
65-131
36-168
60-140
60-140
37-166
78-129
42-163
63-123
20-158
70-130
70-130
74-134
70-130
70-130
70-130
70-130
10-158
59-143
69-132
70-130
70-130
50-132
71-126
73-131
69-130'
79-132
60-140
70-130
15-128
70-130
60-140
70-130
• 69-129
70-130
60-155
70-130
75-125
70-130
70-130
77-132
77-132
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
_ 06/10/2010 0916
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916 06/10/2010 0916
06/,10/2010 0916
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916
06/10/201.0 0916
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916
06/10/20100916
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916 (
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916' '
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40%
ND = Not detected at or above the MDL J = Estimated result < PQL and >_MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged wilh a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
N - Recovery is out of critena
+ - RPD is out of criteria
Shealy Environmental Services. Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 56 of 63 Level 1 Report v2.1
AR000348
Volatile Organic Compounds by GC/MS - LCSD
Sample ID: LQ35603-003
Batch: 35603
Analyt ical Method: 8260B
Parameter
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
Spike Amount (ug/L)
20
20
20
40
Q % Rec
Result (ug/L)
20
23
24
39
Q
Acceptance Limit
Prep
Dil
1
1
1
1
Matrix: Aqueous
Method: 5030B
% R e c % R P D
101 8.9
117 3.5
118 14
98 8:7
% Rec Limit
73-124
41-173
29-159
70-130
% RPD Limit
20
20
20
20
Analysis Date
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916
06/10/2010 0916
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d6
106
106
109
70-130
70-130
70-130
PQL = Practical quantitation limit P = Ttie RPD between two GC columns exceeds 40%
ND = Not detected al or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
N - Recovery is out of critena
+ - RPD is out of cntena
Shealy Environmental Services. Inc. 106 Vantage Point Drive. West Columbia. SC 29172 (803)791-9700 Fax(803) 791-9111 www.shealylab.com
Page: 57 of 63 Level 1 Report v2.1
AR000349
Volatile Organic Compounds by GC/MS - MB
Sample ID: LQ35610-001
Batch: 35610
Analyt ical Method: 82608
Matrix: Aqueous
Prep Method: 50308
Parameter Result Dil PQL MDL Units Analysis Date
Acetone ND
Benzene ND
Bromodichloromethane ND
Bromoform • ND
Bromomethane (Methyl bromide) ND
2-Butanone (MEK) ND
Carbon disulfide ND
Carbon tetrachloride ND
Chlorobenzene ND
Chloroethane ND
Chloroform ND
Chloromethane (Methyl chloride) -ND
Cyclohexane ND
1,2-Dibromo-3-chloropropane (DBCP) ND
Dibromochloromethane ND
1,2-Dibromoethane (EDB) ND
1,4-Dichlorobenzene ND
1,3-Dichlorobenzene ND
1,2-Dichlorobenzene ND
Dichlorodifluoromethane ND
1,2-Dichloroethahe ND
1,1-Dichloroethane ND
trans-1,2-Dichloroethene ND
cis-1,2-Dichloroethene ND
1,1-Dichloroethene ND
1,2-Dichloropropane ND
trans-1,3-Dichloropropene ' • , ND
cis-1,3-Dichloropropene ND
Ethylbenzene ND
2-Hexanqne ND
Isopropylbenzene ND
Methyl acetate ND
Methyl tertiary butyl ether (MTBE) ND
4-Methyl-2-pentanone ND
Methylcyclohexane ND
Methylene chloride ND
Styrene ND
1,1,2,2-Tetrachloroethane ND
Tetrachloroethene . ND
Toluene ND •
1,1,2-Trichloro-1,2,2-Trifluoroethane ND
1,2,4-Trichlorobenzene ND
1,1,2-Trichloroethane ND
1,1,1-Trichloroethane ND
20
5.0
5.0 ,
5.0 '
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0 •
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0.
5.0
5.0
5.0
5.0
6,7 0.20
1.7 0.40
0.80
1.8 0.30 0.40
1.7 0.50
1.7 0.30
0.98
0.60
1.7 0.30
1.7 1.7
,1.7
0.20
0.30
0.30
0.40 0.20
0.50
. 0.30
0.30
0.30
1.7,
. 1.0
1.0 0.72
0.40
0.80
0.95
1.7 0.10
0.40
0.40
1-7.
0.30
1.7 0.30
0.20
ug/L
ug/L
ug/L
ug/L
ug/L ug/L
ug/L ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L ug/L
ug/L
ug/L
ug/L
, ,ug/L
ug/L
ug/L
ug/L ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L ug/L
ug/L
ug/L
1 ug/L ug/L
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
. 06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010-1725_
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
PQL = Practical quantitation limit r P = Ttie RPD between two GC columns exceeds 40%
ND = Not detected at or above the MDL ' • J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations.are performed before rounding to avoid i-ound-off errors in calculated results
N - Recovery is out of criteria
+ - RPD is out ot criteria
Shealy Environmental Services. Inc. , 106 Vantage Point Drive West Columbia, SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 58 of 63 Level 1 Report v2.1
AR000350
Volatile Organic Compounds by GC/MS - MB
Sample ID: LQ35610-001
Batch: 35610 '
Analyt ical Method: 82608
Matrix: Aqueous
Prep Method: 50308
Parameter Result Dil PQL MDL Units Analysis Date
Trichloroetherie
Trichlorofluoromethane
Vinyl chloride
Xylenes (total)
Surrogate
ND
ND
ND
ND
% Rec
1
1
1
1,
Acceptance Limit
5.0
5.0
2.0
5.0
0.30
0.30
0.10
1.7
ug/L
ug/L
ug/L
ug/L
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
06/10/2010 1725
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
102
108
108
70-130
70-130
70-130
PQL = Practical quantitation limit P = Ttie RPD between two GC columns exceeds 40%
ND = Not detected at or above the MDL J = Estimated result < PQL and >^MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
N - Recovery is out of criteria
+ - RPD is out of criteria '•
Shealy Environmental Services. Inc. - , 106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 59 of 63 Level 1 Report v2.1
AR000351
Volatile Organic Compounds by GC/MS - LCS
Sample ID: LQ35610-002
Batch: 35610
Analyt ical Method: 82608
Matrix: Aqueous
Prep Method: 50308
Parameter
Spike Amount
(ug/L) Result (ug/L) Dil % Rec
% Rec Limit Analysis Date
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-8utanone (MEK) •
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dib'romoethane (EDB) '
1,4-Dichlorobenzene
1,3-Dichlorobenzene
1,2-Dichlorobenzene
Dichlorodifluoromethane
1,2-Dichloroethane
1,1-Dichloroethane
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene . ( .
1,1-Dichloroethene
1,2-Dichloropropane (
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,2,4-Trichlorobenzene
1,1,2-Trichloroethane .
1,1,1 -Trichloroethane
100
50
50
50
50
100
50
50 •'
50
50
50
50
50
50 •
50 50
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
50
50
100
50
50
50
50
50
50
50
50
50
50 "
170
49
51
51
49
140
56
52
- 48
44
50
46
52
52
48
52
48
50
49
49
52
,50
50
50
53
49
47
.49
51
120
50
62
59
120
49
, 47
49
52
48
52
59
48
49
52
1 ^.
.1
166
98
102
101
98
143
113
105
95
88
99
92
105
104
96
i05
97
100
98
98
104
100
99
101 .
106
99
95
98
103
119
99
124
• 118 . .
119 ,.
98
93
97
105
96
105
117
96
97
104
46-153
72-127
71-f43
65-131
"36-168
60-140
60-140
37-166
78-129
42-163
63-123
20-158
70-130
70-130
74-134
70-130
70-130
70-130
70-130
10^158
59-143
. 69-132
70-130
70-130
50-132
71-126
73-131
69-130
79-132 .
60-140
.70-130
15-128
70-130
60-140
70-130
69-129
70-130
60-155
70-130
75-125
70-130
70-130
77-132
77-132
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
1 06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010^556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
. 06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
P = The RPD between two GC columns exceeds 40% f
N - Recovery is out of critena
+ - RPD is out of criteria
PQL = Practical qua'ntitation limit
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W^ ^
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services. Inc. , 106 Vantage Point Drive' West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 v™w.shealylab.com
Page: 60 of 63 Level 1 Report v2.1
AR000352
Volatile Organic Compounds by GC/MS - LCS
Sample ID: LQ35610-002
Batch: 35610
Analyt ical Method: 8260B
Parameter
Trichloroethene
Trichlorofhjoronriethane
Vinyl chloride
Xylenes (total)
Surrogate
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8'
—
Spike Amount
(ug/L)
50
50
50
100
Q % Rec
106
107
109
Result . (ug/L) Q
48
51
50 '
99
Acceptance Limit
70-130
70-130
^ 70-130
Matrix:
Prep Method:
Dil
1
1
1
1
Aqueous
50308-
% Rec
96
101
. 100
99
% R e c Limit
73-124
41-173
29-159
70-130
V
(
Analysis Date.
- 06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
06/10/2010 1556
PQL = Practical quantitation limit P = Ttie RPD between two GC columns exceeds 40%
ND = Not detected at or above the MDL J = Estimated result < PQL and >_MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a r w
Note: Calculations are performed before rounding to avoid round-off errors In calculated results
N - Recovery is out of criteria
+ - RPD is out of criteria
Shealy Environmental Services, Inc. 106 Vantage Point Drive WestColumbia.SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 61 of 63 Level 1 Report v2.1
AR000353
Volatile Organic Compounds by GC/MS - LCSD
Sample ID
Batch
Analyt ical Method:
Parameter
LQ35610-003
35610
82608
Spike Amount (ug/L)
Result (ug/L) Q
Matrix: Aqueous
Prep Method: 5030B
Dil % Rec % RPD % Rec Limit
% RPD Limit Analysis Date
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,4-Dichlorobenzene
1,3-Dichlorobenzene
1,2-Dichlorobenzene
Dichlorodifluoromethane
1,2-Dichloroethane
^ 1,1-Dichloroethane
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
1,1-Dichloroethene
1,2-Dichloropropane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,2-Trichloro-1,2,2-Trifluoroethane
1,2,4-Txichlorobenzene
1,1,2-Trichloroethane
1,1,1-Trichloroethane
100
50
50
50 >
50
100
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50 -
50
50
50
50
50
50
100
50
50
50
100
50
50
50
50
50
50
50
50
50
50
110
48
50
47
49
110
58 51
48
49
48
46
58
47
46
50
49
51
49
, 51
49
48
50
48
54
49
46
48
53
110
51
45
49
110
50
47
48
51
49
52
57
43
47
51
1 . 106
1 96
1 99
1 95
1 .98
1 112
1 115
1 102
1 96
1 98
1 96
1 92
1 116
1 93
1 92
1 99
1 98 .
1 103
1 99
1 102
1 98
1 95
1 . 99 1 97
1 109
1 98
1 . 93
1 97
1 105
1 112
1 102
1 ' ' 90 ,
1 99
1 .110
1 100
1 94
1 97
1 102
1 99
1- 105
1 115 .
1 87
1 94
1 101
45
1.7
2.1
6.9
0.43
24
2.1
2.6
0.25
11
3.2
0.34
11 11
4.5
5.5
1.8
2.2
0.36
3.9
6.7
5.0
0.052 3.9
2.5
. 1.4
2.5
1 J
2.0
5.8
3.2
31
18 .
7.9
2.0
0.89
0.52
2.1
2.7
0.36
2.2
9.9
3.4
. 2.8
46-153
72-127
71-143
65-131
36-168
60-140 ^
60-140
37-166
78-129
42-163
63-123
20-158
70-130
70-130
74-134
70-130
70-130
70-130
70-130
i 0-158 .
59-143
69-132
70-130
70-130
50-132
71-126
73-131
69-130
-79-132
60-140 ,
70-130
15-128
70-130
60-140
70-130
69-129
70-130
60-155
70-130
75-125
70-130
70-130
77-132
77-132
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20,
20
20
20
20
20
20
20
20
20
20
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 -1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/20101618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
PQL = Practic:al quantitatioii limit P = Ttie RPD between two GC columns exceeds 40% I.
ND = Not detected al or above the MDL J = Estimated result < PQL and i MDL
Where applicable, all soil sample analysis are reporied on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
N - Recovery is out of criteria
+ - RPD is out of criteria
Shealy Environmental Services. Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 vww.shealylab.com
Page: 62 of 63 Level 1 Report v2.1
AR000354
Volatile Organic Compounds by GC/MS - LCSD
Sample ID: LQ35610-003
Batch: 35610
Analy t ica lMethod: 8260B
Parameter .
Trichloi-oethene '
Trichlorofluoromethane
Vinyl chloride'.
Xylenes (total)
Surrogate
, Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
J
Spike Amount
(ug/L)
50
50
50 •
100
Q % Rec
106
98
111
Result (ug/L)
49
53
52
100
'
Q
'
)
y
Acceptance Limit
70-130
70-130 •
70-130
Prep
Dil
1
. 1
1 ,
1
Matrix: Aqueous
Method: 5030B
% Rec
98
106
103
100 .
• '
% RPD
1.2
' 5.1
2.9
0.38
% Rec Limit
73-124
41-173
29-159
70-130
; - •
% RPD Limit
20
20 .
. 2 0
20
-
,
>
Analysis Date
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
06/10/2010 1618
r -
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40%
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged v^th a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
N - Recovery is out of critena
+ - RPD is out of critena
Shealy Environmental Services. Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803)791-9700 Fax (803) 791-9111 www.shealylab.com
Page: 63 of 63 Level 1 Report v2.1
AR000355
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