ETC-TOXICONJuly 13, 1988

0 2 3

Environmental Testingand Certification Corp.ETC-TOXICON3213 Monterrey BoulevardBaton Rouge, LA 7081~504-925-5012

Mr. Russell D. HartRemedial Project ManagerCES-MI/WI UnitU.S. Environmental Protection AgencyRegion 5230 South Dearborn StreetChicago, Illinois 60604

RE: Request for Information Dated June 22,1988

Dear Mr. Hart:

The residential well samples analyzed for Rollins Field Services were run in accordancewith Statement of Work for Organic Analysis Multi-Media, Multi-Concentration OrganicsGC/MS Techniques 7/85 Revision (SOW 785), Office of Solid Waste and EmergencyResponse, Washington, D.C., August, 1985.

Instrument Detection Limits were calculated as (° n-1) standard deviation of three 20 ug/Lstandards calibrated against a 50 ug/L standard.

A copy of the data subset has been included for your perusal.

If you havej^x^aesnqhslripase feel free to call me at (504) 925-5012.

Since

Michael D. CrouchPresident

MDC/ecc

EPA Region S Records Ctr.

232427

Initial Calibration DataVolatile HSL Compounds

Case No: Region:

Contractor: Tnyionn I nhnrafcories. Inc.

Contract M»68-01-7026

Instrument I O: FJNN2

Calibration Date:. I "2.-Z-- 67

Minimum AT for SPCC is 0.300(O.25 for Bromoform)

Maximum % RSO for CCC is 30%

I Laboratory ID

I Compound ^"20 RF150 «F200 RTCCC-

pRSO I SPCC-

IChloromethane 1/006 I 3.t>ooiBromomethane . 3/3

Chloride 0.3?7IChloroethaneIMethylene Chloride 3l. <?/.?*/(Acetone yT-733 /.T.47/I Carbon Oisulfide 0./7Q1. 1-Oichloro«thene

1.1 -O«ch(oro«thane[Trans-1. 2-OichtofoetheneI Chloroform

1. 2-Oichloroethane 33?|2-Butanone //. 362. 9. OS"/ /,/t.O1.1. 1-Trichloroeihane

(Cartoon Tetrachloride

I Vinyl Acetate /9.Q8/ I /y.S-67I Bromodichlorometharve

. 2-O«chk>ropropane /9.ra/-1. 3-Dichloropfopenel

I Trichloroethene \jo.off I /y.r«/7Dibfomochloromethane Q.TS31.1. 2-Trichloro«thane ?. 3o/

IBenzene

|cis-1.3-0ichtofopfopeoe|2.Chlofoethy«vinytethefI Bromoform

14-Methyf-2-Pentanone 79. 2,^0812-HenanoneI Tetrachloroethene

1. 1. 2. 2-Tetrachloroethar 0.3/2-OMo'sToluene

IChlorobenxene

IStyrene[Total Xyfones

HF -ResponM Factor (cubccript is lh« Amount of ug/L)fiF -Av«r«oe Re*pon«« Factor

-Percent RaUftve Sundird O««Mtion

CCC -Calibration Check Compounds (.JSPCC -System Performance Check Compounds (-.»

Form VI

GC/MS TUNING AND MASS CALIBRATION

Bromofluorobenzene (BFB)

Case No.

Instrument ID

Lab ID

Contractor Toxicon Laboratories. Incnnmran No. 60-01 -O

Date Q/ ~ #-<^ -*y "7 Time.

Data Release Authorized By:

m/e ION ABUNDANCE CRITERIA XRELATIVE ABUNDANCE

50

75

95

96

173

174

175

176

177

15.0 - 40.0% of the base peak

30.0 • 60.0% of the base peak

Base peak. 100% relative abundance

5.0 • 9.0% of the bate peak

Less than 1.0% of the base peak

Greater than 50.0% of the base peak

5.0 - 9.0% of mass 174

Greater than 95.0%. but leu than 101.0% of mats 174

5.0- 9.0% of mass 176

c?0.</

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THJS PERFORMANCE TUNE APPLIES TO THE FOLLOWINGSAMPLES. BLANKS AND STANDARDS.

Value in parenthesis is % mas< 174.Value in parenthesis is % mass 176.

SAMPLE ID LAB ID DATE OF ANALYSIS TIME OF ANALYSIS

01 -

i MM. ii •••»

MASS SPECTRUM01/22/8? 8:36:96 + 4:51SAMPLE: 56NG 4-BFB,1-52-1,1.6ULCOHOS.: DESCBF, 1550U,6'SPIMQ,FIHH82,ETC-TOX1COH,LOW WATER

- #90 - #10635

DATA: BF81228?A #97CALI: BF012287A #3

BASE M/Z: 95RIC: 144896.

r 3564S.

174

t-la-s List Data: BF012287A # 9701/22/87 8:36:OO + 4:51 Call: BFO12287A * 3hf.afT-rj le: SONG 4-BFD, 1-52-1, 1. OULConds : DESCBF, 1550V, 6 'SP1OOO; FINN02* ETC-TCX ICON. I.QU WA7£F:

Bate ir./z: 95RIC: 144896.

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RIC DATA: US012287F #101/22>'37 13:59:88 CALI: VS012287F #3SAMPLE: 20PPB UOA STD. ,3-22-L5.8ML, IS&SSCONDS.: DESCUP,1550"J,6'SP1000,FINN02,ETC-TOXICON,LOW WATER

SCANS 19 TO

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D4-1,2-DICHLOROETHANE SS1DS-TOLUENE S3?4-BROMOFLUOROBENZENE SS3CHLOROMETHANE <**)BROMOMETHANEVINYL CHLORIDE (*)CHLOROETHANEMETHYLENE CHL OR IDEACETONECARBON DISULFIDE1,1-DICHLOROETHENE (*)1,1 DICHLOROETHANE <**)TRANS-1,2-DICHLOROETHENECHLOROFORM (*)1,2-DICHLORQETHANE2--BUTANONEi,I,1-TR1CHLOROETHANECARBON TETRACHLORIDEVINYL ACETATEBROMODICHLOROMETHANE1,2-DICHLOROPRQPANE (*)TRANS-1,3-DICHLOROPROPENETRICHLOROETHYLENED1 BROriOCHLOROMETHANE1.1,2-TRICHLOROETHANEBENZENECIS-1.3-DICHLOROPROPENE2-CHLOROETHYLVINYL ETHEREROMOFORM (**)4-METHYL-2-PENTANONE2-HEXANONE1122-TETRACLETHANE (**)TETRACHLOROETHYLENETOLUENE <*>CHLOROBENZENE («•*)ETHYLBENZENE <*)STYRENETOTAL XYLENES

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> Amount50.50.5O.47.49.48.18.18.19.19.21.14.2019.19.19.20.17.10.19.21.19.19.19.19.19.18.19.20.IS17.17.19.21.19.19.19.19.19.19.19.

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RIC DATA: US812237I #1 SCAMS 19 TO 60901/22/37 17:30:00 CALI: US812287I #3SAMPLE: 20PPB UOA STD.,3-22-1,5.8ML,IS&SSCONDS.: DESCVP,1550U,6'SP1000,FINN92, ETC-TOXICON,LOW WATERRANGE: G 1, 608 LABEL: N 0.- 4.0 QUAN: A 0, 1.8 J 8 BASE: U 20. 3

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Area(Hght) Amount67939.385568.306365.33037.363396.278053.28743.9O04.45886.24513.60726.6087.

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