Enclosure 20 to TN E-28034, Scavuzzo, R.J., Lam, P.C., Gau ...

Enclosure 20 to TN E-28034

Scavuzzo, R. J., Lam, P. C., Gau, J. S., "Buckling Tests of FusionWelded Composite Stainless Steel Aluminum Plates," Dept. ofMechanical Engineering, The University of Akron, May, 1990

(associated with RAI 2-7 and RAI 2-13)

Test Report

Buckling Tests of Fusion Welded Composite Stainless Steel

* Aluminum Plates

May 1990

R. J. Scavuzzo

P. C. Lam

J. S. Gau

Department of Mechanical Engineering

The University of Akron

Akron, Ohio 4.43.25-3903

This work was sponsored by UST&D Inc. and waswitnessed under UST&D!s QA program

CONTENTS

PAGE

INTRODUCTION 1

TEST DESCRIPTION & RESULTS 1-7

TEST CONCLUSIONS 7

TABLES#1#2

Load vs. Deflection Date - Specimens Al, B1 & ClLoad vs. Deflection at Temp. Data - Specimens Dl, A2, B2 & C2

FIGURES#1 Sketches of Plate Test Specimens A, B, C & D#1A Buckling of the Steel Plates of Specimen Al Due to Initial Load

(Photo)#2 Specimen Being Mounted on Baldwin Compression Machine (Photo)#3 Specimen Being Mounted on Tinius Olsen Universal Test Machine

(Photo)#4 Specimen Being Aligned (Photo)#5 Electric Chromalox Heaters Being Installed on Specimen (Photo)#6 Controller for Electric Chromalox Heaters#7 Insulation of Specimen (Photo)#8 Installation of LVDT (Photo)#9 Compression Machine Load Indicator (Photo)#10 Initial Reading of the LVDT (Photo)#11 Initial Reading of the Thermocouple (Photo)#12 Room Temperature Buckling Testing of Composite Panel Al Using

Baldwin Compression Machine#13 Room Temperature Buckling Testing of Composite Panel Al Using

Tinius Olsen Universal Test Machine#14 Room Temperature Buckling Testing of Composite Panel B1 Using

Tinius Olsen Universal Test Machine (Graph)#15 Room Temperature Buckling Testing of Composite Panel Cl Using

Tinius Olden Universal Test Machine (Graph)#16 Panel Al After Buckling (Photo)#17 Panel B1 After Buckling (Photo)#18 Panel Al, B1 and Cl After Buckling (Photo)#19 High Temperature Buckling Testing of Composite Panel D1 Using

Baldwin Compression Machine (Graph)#20 High Temperature Buckling Testing of Composite Panel A2 Using

Baldwin Compression Machine (Graph)#21 High Temperature Buckling Testing of Composite Panel B2 Using

Baldwin Compression Machine#22 High Temperature Buckling Testing of Composite Panel C2 Using

Baldwin Compression Machine

APPENDIX A - Calibration of Equipment Certification

APPENDIX B - Test Certifications

APPENDIX C - Materials Documentation

1

Test Report

Introduction

The objective of the test was to load composite plate

specimens in compression to determine the buckling load and

post buckling behavior. Tests were conducted at room

temperature and at elevated temperatures (z400*F at-the corner

of the specimen). Different fusion weld configurations were

tested.

Testing was conducted in two phases. In Phase I three

specimen. were tested at room temperature. The test results are

listed in Table 1. In-the secondphase, Phase II, tests were

conducted at elevated ....temperatures such that the minimum

temperature was 40:GF. This minimum temperature occurred at

the corner of the specimen. At the center, temperatures were

approximately 500,F and .varied with each specimen. Details are

in Table 2.

Test Specimen Description

Three 24" long, 8.05" high and 0.72"' thick composite plate

specimens with four, six and eight fusion welds respectively

were tested. Sketches of the plate specimens are provided on

Figure 1.

The plates are composed of two inner 6061-T6 aluminum

plates, each 0.25" thick and two outside 304 SS plates, each

0.11" thick. The steel plates were wider than the aluminum

plates by about a 1/161" on both sides. Thus, the loading was

2

first applied to the outer steel plate until they were

compressed to the width of the aluminum plates. Then the

compressive load was .shared by both the aluminum and steel

plates. This initial load cause buckling of the steel plates

(Figure 1A), prior to buckling of the aluminum.

Calibration:

Prior to any testing on the Baldwin Compression Tester, the

machine was calibrated by C&M Calibration Service, 230 Haymond

Dr. P.O. Box 149, Gibsonia, Pa. 15044 on April 13, 1990.

The LVDT (linear variable displacement transformer) was

also calibrated prior to use as indicated in Appendix A. A

LVDT calibration instrument was used for this purpose. This

device consists of a fixture to hold the LVDT and a micrometer

at one end. The voltage read-out versus deflections is

obtained. The micrometer was checked against standard gage

blocks. The calibration data is provided in Appendix A.

For the high temperature work, the three thermocouples and

digital read out devices were calibrated using newly purchasedelectronic devices specifically for these instruments. In

addition, the thermocouples and read-out devices were checked

against the boiling point and freezing point of water. These

results are also provided in Appendix A.

Phase I Room Temperature TestinQ:r

The first specimen with 4 fusion welds spaced in pairs at

12" apart was tested in a 300,000 lb Baldwin compression test

3

machine (Figure.2) at University of Akron. However, this

machine did not have enough force capacity to buckle the

specimen. This preloaded specimen (Specimen Al) and two other

specimens with 6 and 8 welds respectively (Specimens Bi and CI)

were tested in a 1.2 million pound Tinius Olsen Universal Test

Machine (Figure 3) at the Pittsburgh. Testing Laboratory. All

the tests were conducted at room temperature.

Specimen Al

The top of the fixture was mounted to the Baldwin

compression test machine with a bolt at its center. The bottom

fixture was braced with two wood planks to prevent lateral

slipping if buckling should be initiated. Care was taken to

align the specimen vertically (Figure 4). A brass circular bar

on both the top and bottom support plates provided a pin type

support. A grove was milled into each. circular brass bar to

support the plate test specimen in the lateral directions

(Figure 4).

A compressed load was applied in 20,000 Ibs increments from

0 to 280,000 lbs. The maximum load was 290,000 lbs. The last

load increment was 10,000 lbs. The load rate was applied at

0.2"/min. Lateral and top support plate deflections were

measured with dial indicators and recorded at the 20,000 lb

increments.

Specimens Al, BI & Cl: Preloaded Four, Six, Eight Fusion Welds

Additional tests were run to buckle the room temperature

4

specimens: Al, Bi, and C1. These. tests were run at thePittsburgh Testing Laboratory to obtain a higher test capacity.

The test of specimen 1A., originally loaded on the Baldwin

Compression Machine, was retested on. the 1.2 million pound

Tinius Olsen compression machine. The top of the fixture was

mounted to the Tinius Olsen test machine with a single bolt.

The bottom fixture was braced with two steel plates to prevent

lateral slipping once the specimen buckled. Other specimens

were supported ::in the same manner as. Specimen 1A of the

previous test. A compressed load was applied with a head

travel rate of 0.2',/min. Load and deflections were recorded.

with a load cell and LVDT. Load-Deflection curves were

automatically plotted during the tests.

Phase II Elevated Temperature Testing.:

In this phase of testi ng, all tests were conducted on the

Baldwin Compression-Machine at the Civil Engineering

Laboratory, University of Akron. Electric Chromalox heaters

and controller (Figures 5 & 6) were used to heat each specimen

while installed the Baldwin Compression Tester. Each specimen

was wrapped in a blanket insulator after being installed in the

Tester (Figure 7). In order to reduce heat conduction to the

top of the Tester, there was a gap between the top edge of the

specimen and brass bar. A fiber glass sheet was used to reduce

heat conduction to the bottom platen of the Tester.

In the first specimen (Specimen Dl with 12 welds), two

Chro-malox heaters were used to elevate the temperature.

5

Approximately. 4 hours, were needed to reach a minimum

temperature of 400F. ..The last three6specimens A2, 12 and C2

were heated with four Chromalox heaters and one controller

(Figure 5).

Two thermocouples were used to measure the temperature of

the specimen: one was located at :the center and one at the

outer edge of the-speimen. The edge thermocouple was located

1" above the bottom support and: 1/2" from the side. The

difference between these temperature measurements, when the

minimum edge temperature-reached 400-°F, was about 100°F. The

third thermocouple monitored the pl.at.en temperature of the test

machine, ,as a safety precaution against overheating.

Test. Procedure Phase II

1. Install the test panel on compression test machine.2. Install the strip heaters on the test panel.

3. Install t hermostat sensor bulb in the end of the panel.

4. Cover the panel with insulating blankets.

5. Attach thermocouples at the center and edge of the panel..

6. Set the thermostat for 550 9 F and heat the test panel until

corner thermocouplep: reading is above 4000F.

7. Install the LVDT between the load patterns (Figure 8).

8. Zero out the compression machine load dial indicator

(Figure 9)

9. Record initial reading of LVDT and Thermocouples (Figure 1.0

and 11).

10. Start loading the test coupon and fixture at a rate of

6

0.2."/mi~n. Continue loading and .recording load and vertical

deflection: data: for every 20,-000lb increments.

ii. Mark.and record the highest load obtained prior to load

decreasing. Continue the 0.2,./min loading rate until the

load fallsof f to 50%. of the maximum value obtained. Then

stop the. loading.

12. Record the final LVDT, load, and temperature readings

obtained at the stop position.

13. Unload..the ýýcompression machine and remove the test panel.

Repeat setup. and steps 1-13 for. each test panel.

Results

Phaseg I Room. Temperature Tests:

For the: first test on specimen Al, containing four fusion

welds. and using. the :Baldwin. compression test machine, measureddeflections: were..plottedon Figure 12 and recorded on Table: ...

The specimen did not buckle at a load 290,000 lbs at room.

temperature (75.F). However, because .the width of the two 304

SS plates were. larger than. the 0.25"1: aluminum plates, there was

some bulging of the outer. cladding (see. Figure 1A).

Using. the Tinius Olsen compression test machine, measured

load-deflection curves were. plotted. and are shown in Figures 13

to 15 for the four, six and eight fusion welds specimens.

Maximum loads .for the tested specimens- are listed in Table 1.

Specimens buckled. at an average load of about 330,000 lb.

From these test results, the failure:. mode indicated that the

two aluminum, plates and one steel. plate buckled in one

7

direction while the. other steel plate buckled in the opposite

direction, (Figure .117. and 18).

Only one fusion weld failed during all of the testing

(specimen Bl), and this was attributed to very large lateral

deflections well1 past the buckling point. For this case,

vertical deflections were :off scale (Figure 14)ý and exceeded

0.45". Photographs of the buckleidill: specimens are shown on

Figures 16, 17 and 18. Post buckling loads are listed in

Table 1.

Phase II Elevated Temperature Tests:

Deflection versus load results. are shown on Figures 19 to

22. Numerical resu.lts. are- tabulated in Table 2. Temperature

measurements at the start of the test are also listed in Table

2. The average maximum load for *specimens A2, B2 and C2 is

260,300 pounds: which is 79% of the r6oom temperature value.

Conclusions.

From the test results the following i•conclusions can be made:

1. The same buckling failure mode was observed in allspecimens.

2. Except for the weld -pattern: 5establishing the bucklingspan, the fusiion: weld. patternsi tested: had no effects. onbuckling load at either temperature.

3. Weld failure did not occur in.any specimen in which theedge deflection was less than 0.45",.

4. By increasing the temperature to a minimum value of4 00 0 F. et buhe buch. kling. load is erduced to 79% of the roomtemperature value.

5. At, both temperatures:, substantial post bucklingstrength can.be expecte. :This is shown by the_ load-deflec.ti .on: cu rves ..as thde .graduali s!opetý after reachingthe buc k i..ng load., in :Figures. 13,714 & 15.

Table 1: :Load vs. Deflec n for Panel Buckling Test.,

Load Disp(1;).. Disp(2). : Disp.(3)(lb)ý (in* 10-3)'(in* 10-3) (...* 1 0-3)

20000 .:63 20. 35:40000 7 :79,: 44: :.o6760000 :. 89 .:.. '64: 100::80000 98......79 39"

100000 1.06 . 0 16:::0

.80;o , 0 •6 :, .0..3o " .1

1.20000 113 140." 187:140000 120 170 2081160000 17 195, . 22,9180000 ý134 218 250:200000 1I40 '. ý238 i271

22000 146. 258, 292ý240000 153 275: 309.:260000 159ý 292 329:-280000 1:65, 308, .347:ý2900010 168 36l 357

Specimen Al (1) B1 C.Load Disp 4W Disp6W.. Disp W.

(Ib) (i* 10-3) (irl 10-3) (.•* 10-3)

00 0 0.200o:: 4.0 4 5040000 45. 42: 54:60000 . 46.: '43.. 56:80000" ... 47 57:

1 00000 48 : -458..120000 49 46 59140000 4:49 47 61.160000 49 48 6.2,::180000. .49: 50:. 63.200000 49. 56' 64:.

220049 58 6.5.:240000 50 60 .66::.260000 :51 : 61 68:280000 51 :62 *69300000 52,. ::862 72:

,..320000 ,iŽ 52 63 765

-340000-- 54 ________

320000 60 70 76-300000 66 80 83 1:280000 73 92 -90 1260000 82. :104 . 97

240095 11:4 106:2 20000 9110 .1..: 1 :105:n20000 1:32 1424 121::1'80000. 160 1!: 162::160000.. 175. .. 1 :76- " .: ._

1.40000.:. 256. 21::21:,.12000.0 .. : 270p

l~o100000i " ____ 380 4._" __

(1) Retest. o Specimen Al.:Note: :Load Pace =.0.2"/min

All:Deflections in Lateral Direction

1,333~

(1) Lateral Deflection

(2) Transverse Deflection of the Right Panel

(3) Transverse Deflection .of the Left Panel

Note:. Load Pace =0.211/min

U of Akron BaldwinCompression:Machine.Specimen.Al,. (4: Fusi.on Weld: Panel):

:Pitt sburgh Testing Lab Tinius :Olsen Universa• Test MNlac•.h e.Specimens Al:..B1 and Cl.(4, ý6 and 8 Fusion.Welds. Panel)

Table 2: Load vs Deflection for Elevated TemperaturePanel Buckling Test.:Using BaldwinCompression Test Machine

SPecimenDD1 " SpecimenA2 Specimen B2 Specimen C2• Load .Disp : Tern/C TemtE Dis T Te isp Tern/C Tern/E Disp Ter/C Tern/E

(Ib) (in). (F) (F) (in) " () (F) (in) (F) (F) (in) (F) (F)

0 0 485 405 0.000000 629 408" 0.00000 504. 410 ý0.000009 425 403.

2o0o000 0.0110o85 0, 0.036308 0.045154 0.052989: ....40000 0.01 43047_ 0.037912 _! _ 0.047973, 0.054933:l:60000 0.015362 - 0.038982 04 :0 9042 ___, 0.05668380000 0.015654 0.039614 0.050306 . 0.058384

i00000 0015799. 0.040051 0.051327 __ I_ 0,05989 1i:200000 0.0158979 0..... .. 0.040294 0.051813 ...... 0.0609192 _ _

1:40000 0.015945 __ 0.040488 0.052007. 0.061786 __

160000 0. o 15994 _•._ 0.040634 :0.052056 0.062613180000 0. 015994 0.040683D '_ .052105: 0,063342:%200o000 .o016042:. .:04040731 0..0521205 0. ".:063876 1220000 0.016091 ,:0.040780 ":0., 0.052105 .... .064362: , ._

:240000 0.01614.0. 0.0140780: ___0.052153- t__ __ .649 __ _

:253000 0.01W6334.. _ 0.040780m : 1 0.052199 0.065338 ._ "

.261•500 0.016460: _. __ .. 06.052229: 0065626: 5 •

266000:: 0.016528.11 ===___=_= _____=== 0.052245. : _ _, ."...267250 ____t __ ____ __1_ 0.05225:: . '2400,00 _____.. 0.045751 .... -0.0571I64. _____ 0.066060:

220000 __" :1 0.053399 :.0.060771:i:: 010.6466411.200000 0,0610416 0.064378 0.066868:1.80000 0,___ O 068694 0.067986 0.067271:

160000 .0,0763.4111 ." _,. . :0.071593 :,__" 0.067675:.1:40000 0.083989 :,0.075200 0.068079 _

132500. 0.0-086857 0.0 76553.: 405. 285 0.068230:'

13.1.5001_: 0.087239: _0,068251 415 2691... i25000 "____ _ ....... . _ 0.089725: 629 5 246 __... ' " _"... . '" " " I " • .

Note: Load :Pace = 0.24/min

i-s; I0r,

Ty,=ý I QL

~47- 0f4

4,

A / 7~7/~( -

00

~,,'T/l-- /

Figure 1. Sketches of Plate Test Specimens A, B, C and D.

Figure lA. Buckling of the Steel Plates of the Specimen Al due to Initial Load.

.Figure 2. Specimen being:Mounted on Badwin Compression Machine.• ~ ~ ~ ~ ~ ~ ~ o n e • ..... .o ... ....:Ba ... :: . . . .. ..... .. V.a• .....

Figure3. Specimen beinglMounted on Tinius Qlsen U niversal:Test Machine.

Figure 4. Specimen being Aligned.

\.

Figure 5. Electric Chromalox Heaters being lnstalled on: Specimen.

Figure 7. Insulation of Specimen.

ilgure.6. Controller for Electric AChrm l t.!:: .. : ,. ." .a: . .

Srk

Figure 9. Zero.out the .Compression Machine: Load Dial.Indicator.

Figure: 8. Installation ofLVDT.

FigU re. 10..•. Initial Reading of the: LVDT.

Figure 1. linitial Reading of the Thermocouple.

Figure 12. Room Temperature Buckling Testing of CompositePanel.Al Using Baldwin Compression Machine.

400

350

7'O

0

b-

C)

z0

I--

:w_.

300

250

200

150

100

50

00 50000 1 0000 0 150000 200000 250000 300000

LOAD (LBWS)

Figure 13. Room Temperature Buckling Testing of Composite:Panel Al Using Tinius Olsen Universal.Test Machine.

Plý ...

iilillilili

I CI Ill~-e9Q• ~ I

1 4 1

I Iii

I IIiU)

.0

V

0-J

Deflection (in * 5E-3)

Figure 14. Room Temperature Buckling Testing of CompositePanel B1 Using Tinius Olsen Universal Test Machine.

~/~7~ZV

JC~T~2

C',

0

A A A

Iii~I I

Ii

•tiiii

RA

lee-, erw-, I, II

F 1

Al hAil !IAj /

Deflection (in * 5E-3)

Figure 15. Room TemperatureBUckling, Testing of Composite

Panel.c1 Using Tinius&Olsen Universal Test Machine.

!Ho

1. I . • • . .. .. • • ,1 I H I

CIS.0

i 1

i! l I}' ,1 I IIII •i'

! 1 ' ' I.,[ [ I i ; .i . ! : :

I': .I

' . t I .!i" :

V I Ii. 0O . .- . - ,- • ...• ! -....'..... ....: ' • .. ..'- "/ . ,:: ' .... •" • r ,"" ..• ' . ! ~ i i

Deflection (in *5E-3)

Figure 16. Panel Al :after Buckling.

Figure 17. Panel BI after Buckling.,

Figur -18. Panel.Al:, Bi and.C after:Bucklingc.

Figure 19. High Temperature Buckling Testing of CompositePanel Dl Using Baldwin Compression Machine.

2580000

0Q

0-il

240000

200000:-

160000-

12000:0-

80.000-

40000-

0

0

0

0

K I00

!

Ut

0.000 0.020I .i

0.040 0.060Deflection (in)

0.080 0.100

Deflection :as Measured by LVDT model :E 5:00 S/N 2044

Figure 20. High Temperature Buckling Testing: of'CompositePanel e : AUsing Baldwin Cmp:ression Machine.

28.0000

240000

2000:00

0-JýO,

1 60000

120000-

80000

40000

00.000 0.020 0.040. 0.060 0.080 0

Deflection (in)Deflection as Measured by LVDT model E 500 S/N 2044

.100

Figure 21. High Temperature Buckling Testing of Composite

Panel B2 Using Baldwin Compression: Machine.

2800:00

240000-

200000-

160000-

0-A

0

00

0

0I

0

I.0I

0I0/,,,

120000+n

80000-

40000+

tI' I !

C

I *d)~~'-.1 1 I I ,I

).000 0.020 0.040 0. 060 0.080Defl .ection (in)

Deflection as Measured by LVDT model E 500 S/N

0.100

2044

Figure 22. High Temperature Buckling Testing of CompositePanel C2 Using Baldwin Compression Machine.

0.0-J

280000-

240000-

200000-

160000-

120000-

80000-

40000-

I

0

10

01

0I

0I

00

0I

0/

0/0/

0/

n A.-

C-' , - i I

).000 0.02:0 0.040 0.060Deflection (in)

Deflection as Measured by LVDT model

0.080 0.100

E 500 S/N 2044

Appendix A

... .hc.----------

Department or ,Mechanical Engineering 2-16) 375-7731College of Engineering:Akron, OH 44325-3903

CALIBRATION OF THERMOCOUPLES

Three high temperature thermocouples using ANSI Type J high

temperature wire (wire code CG-J-20-SEE) with a model OMEGA

115 distal thermocouple readout. The temperature range for

this wire is from -100 0 C to 720 0 C (-1000F to 1400'F). Each

digital system (Serial No.'s 0091154, 0091155 and 0091159)

was calibrated using the OMEGA calibrator Model CL-307 by

C. Bailey, Electronics Technician, Dept. of Mechanical Engin-

eering, during the week of April 23, 1990. In addition, the

systems were checked at the freezing and boiling points of

water. An accuracy of t 2°F is obtained.

J. (. ~u, Ph.D.

F IDate

EngineeringfUTURE

The Uniwiv nL t.Akrn is An Equal Eduat-on And Enmp;-mrent Insiut~n-

700-Calibration of 0091159 at the Freezing and

D600iBoiling Point of WaterY - 1.239 + 0.98944 X

5004-

4-00

-_300

0

o 200E :

100-

0 100 200 300 400 500 600 700

Temperature of Water (0 F)

700 Calbration of 0091154 Using OMEGA CL-307

y Y -0.053732 + 1.0025 XJ

f

7'-7

0

0

C-)

E

500-

400-

300-

200

100

7,

,07-

7,7-

LL

KK 7

x

or

0 !

0I0 J I I ,I

200 300 400 500Calibration Device Reading (OF)

Calibration of Thermocouple

600 700

700ICalbration of 0091155 at Freezing and Boiling Point,.,-

2600 of Water-Y 0.25902 + 0.98944 X

n 500- .-

®400

-00u000

1~-00 -

0

o200 100

Tca 000 I---H ]-----i --- h- -

0 10O0 200 300 400 500 600 700Temperature of Water (0 F)

700

cr_

Li)0-

:30

0

0

600-

500-

400-

300-

200-

100-

Calbration of 0091155 Using OMEGA CL-307

Y = -0.63457 + 1.0044 X

J 7

;-7

7A

7

70

0

00 100 200 300 400 500 600 700

Calibration Device Reading (OF)Calibration of Thermocouple

700 lCalbration of 0091159 at Freezing and Boiling Point

2•EL 600 of Water0nY= -0.93941 + 0.995 X

4o -

0

o 4001

• -3001

00o 200-E-1 100% +

0 -/ t- +--t----I-----t-

0 100 200 3O0 400 500 600 700Temperature of Water (OF)

700-7 Calbration of 0091159 Using OMEGA CL-307

C" 600 Y = -1.0431 + 1.0049 X0

S5.000

Qo400

0-n300--0

0 200EI-Q)-C 100I--

0 I .lz0 100 200 300 400 50.0 600 700


lihe.i'f •lvers1tv _ _ _ __

Department of Mechanirc. Engineering 216) 375-7731.College o( EngineerinpAkron, OH 44325-3903

CALIBRATION OF THE BALDWIN COMPRESSION MACHINE

The compression test machine was calibrated on April 13, 1990-

prior to the start of the test series by C&M Collins Calibration

Service.

Attached is a plot of the calibration data for the compression

machine and the data taken by C&M Collins Calibration Service.

VJ. S. Ga.4, Ph.D.

Date

75ANNIVERSARY

Engineering

FUTURE

The. UrnivrrsfY. of Akron is -0 E~ual Edo-tion and Enmploymantn 1115tuItion

~0

c

00

0

C)

300000

250000

200000

150000

100000

50000

00 50000 100000 150000 200000 250000 300000

Calibration Device Reading (Qb)Calibration of Load Cell of Baldwin Compression Machine

C&M COLLINS CALIBRATION SERVIC.€ETHIS IS TO CERTIFY that the following dlescri bed testing machine h:as been calibrated by C&M CALI-BRATION and the loading range(s) shown below found: to be within a maximum tolerance of

/, %.

MACHINE __ _ _ _ _ _ _ _ _ _ _ __,_ _TYPE. o ,-r

LOCATION (... i ; V e-S-,' o /r ,, CAPACITY 30coo' 6/&r

i-ir',Lo,4- ,..A;& 32.S SERIALNO, 3COCT -.. oi .

DATE O:F VERIFICATION A '. .. 3. /f?9oMethod of verification and below recorded data it ln accordance with A S.T.M. E-4 cc-. . The testing device(s) used forthis calibration have certifications traceable to-.the National Institute of Standards Technology.

Machine Readings .2 Pounds.C. Newtops.0 Kilograms Readings temperature corrected for .71., 'F.MACHINF CALISRA71ON DEVICE MACHINE ERROR C.0

READING READING t ." N01

S C2 I )2a. 4-+(.? . ,

_ _.o _,. ,t? .- / _ z

7209 7 4-j.o . ' 1

16.00 0___ __ o -SIo S.3 ?

,:_____ IJ909 .'-l .:7667[ 6000 -7, ,1?OO0 3e.•77- + .e3I? .If O .o 0•~ - o .

3. .o , ii ' 3,Y 5

6oIooo ] - 4I o .- 7 5

MACHINE . CALIBRATION DEVICE mADNINE ERROR D.READING READING / ,'t. "4 NO.

?....... U P .7 go. . ... _= 00oo0 ee _ _.__/ . t/

'2 Y...0 o 00 0e 3 s-o K 0•9. ./"

?O:Oo 9. 9 •Te 9 q•o /. .70 3

L ."' . _._ __._.' ' +.1.

_________"HF' ....

CALIBRATION APPARATUS - Morehouse.Proving RIngs, Staln.sense load cells & Troemner Dead Weights. Verificationstraceable to .the National Instilute.of".Standards Technoloay; in accordance with A.S.T.M. latest speciftcations.C. .. SEIRIAL NO. LO.0ADINiG RANGE CALIB. NATIONAL INSTITUTE OF STANDARDS TECHNOLOGY LA: NO. TEMP.CODE CLASSAVALUE DATE OFC.D.

*2 3 7-( 63?2-10h f6 !;?7 k 97 731_7_Y_ý

2 2R2t to ii l&oO 5t. 9# -?5'-ty S J-7- 0/ 2 1- -7 7___3 ' _.. .'_ .' _ ,. .. " _"'" '_ _.. ._.. . . . ._ _ __" '_ _'_ _'_ _'" '_ . .. _m _ _ _ _ ___

. , . i . , , . ,. . . . ,, ,

MACHINE RANGE LOADING:RANGE

/ -- o6 o ('c 18o - 160oo lW

30.. - 00o 1 h

O - ho0 t•!, 20.i -3..oof /•

Primary Load Indicating Device___.T - L,- e,..r• .....

C & M COLLINS CALIBRATION SERVICE230 Haymont Dr., Box 149, Gibsonia, PA 15044

(412). 443-7631

ý- 7-- rZýBy:.1 SERVICE ENGINEER)

%Yilnessed By.:

She.j" l]versitv

Department of Mechanical Engineering ý216) 375-7731College of EngineeringAkron. OH 44325-3903

CALIBRATION OF THE LVDT

The LVDT calibrator is a micrometer device on a fixture. Both

the calibration device and LVDT, model E 500 S/N 2044, were

calibrated using the model DJR 450 digital transducer readout.

(a) Calibration Device

The micrometer of the calibration device was calibrated

on May 2, 1990, using Johansson Gage Blocks. Attached is

a plot of this calibration, The accuracy is t 0.001".

(b) Calibration of the LVDT

The LVDT was calibrated during the week of April 16, using

the calibration device. A plot of the calibration is

attached. Measurements are within t 0.010.

oi I I" ý0I ;, N rt:i I,(,

75 JS u, Ph.D.

ANNIVERSARY

Engineering 6 C)ETU.T-U RE Date

Th. Un-vnnty o0 Akron is an Equal Eduction and Employent lnsotfution

'~ ~,

0

Q)

L.Q

4-,ci)E0

1.000-

0.900-

0.800-

0.700-

0.600-

0.500-

0.400-

0.300-

0.200-

0.100-

Calbration of Micrometer (No 262) onLVDT Transducer E 500 S/N 2044Using JOHANSSON GAGE BLOCK 1 ASerial No 10008 lJ

Y = -0.0001 2236 + 0.99943 X

K

- I --- !

7-

A 7 -

n nnr)

0.000--- , 1

I I I

0.200 0.400 0,600Thickness of Gage Block (in)

Calibration of Micrometer

0.800 1.000

2.000E4

1.500E4-

1.000E4'

05000.000-

C: 0.000-

-5000.000-

- 1 .000E4-

- 1.500E4-

LVDT Transducer E 500 S/N 2044DTR-450 Digital Transducer Readout (0083971)Y = 10888 - 20574 X

)

-2.000E4 I0.000

00.200 1 1

0.400 0.600Displacement (in)

Calibration of LVDT

00.800 1.000

APPENDIX B

TEST CERTIFICATION

# --us, L),

CERTIFICATE OF CONFORMANCE

THIS IS TO CERTIFY THAT THE LOAD TESTING OF THE STAINLESS STEEL/ALUMINUM

COMPOSITE PANEL WAS SATISFACTORILY PERFORMED IN ACCORDANCE WITH THE

REQUIREMENTS OF TRANSNUCLEAR SPECIFICATION E-11586 AND UST&D CONTRACT

SPECIFIC PROCEDURE CSP-89-011-1, Rev. 1.

UST&D QUALITY ASSU RA NCE MANAGER DAT 5 -7

UNIVERSITY OF AKRON REPRESENTATIVE DATE______

*SEE ATTATCHED INSPECTION SUMMARY REPORT FOR DEVIATIONS FROM

THE REFERENCED PROCEDURE.

J

IUST&D, )Ntuclem" lo'uct~cs

Inspection Summary ReportProject 89-011-1

The following composite panel load tests were conductedin accordance with QC procedure CSP-89-011-1 Rev. 1 with thefollowing exceptions:

1). Panels A-2, B-2 and C-2 were initially heated with4 heaters prior to test. A-2 had 2 heaters removed justprior to testing. The other 2 heaters were left installedduring the test. B-2, all 4 heaters were used and operatingduring the entire test. C-2, 4 heaters were installed duringthe entire test, however power was disconnected at the startof the test.

2). All test panels were heated to at least 4000 at thestart of the test. Thermostat was set at maximum setting toobtain at least 4000 at both the center and edge of testpanel. The temperature readings prior to testing at centerof panel varied from 4250 to 6290.

UST&D Quality Representative/QC Manager

Engineering Concurrence

UST& VP En eering

I 75 Butler StreetPittsburgh, PA 15223412-784-7225

LJST\ 1), --

F- ý 1; ",4; A"'ý 'ýc sýý *-'ý-' 'V ý"

COMPOSITE PANEL LOAD TEST DATA SHEET

START OF TEST DATA

a) TEMPERATURE

b) LOAD ________,

c) VERTICAL DEFLECTION

d) TEST PANEL ID# Ae) No. OF PANEL WELDS .

f) DATE & TIME o .• ,

AT MAXIMUM LOAD READING

a) TEMPERATURE .9'e',dJ"• z7os, deb ) LOAD . . .. . !2.,

c) VERTICAL DEFLECTION .o•07

END OF TEST (50% of mqx. od)

a) TEMPERATURE _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _

b) LOAD , .

c) VERTICAL DEFLECTION , _"_,._ _,,,

d) TIME ,o; ".

EQUIPMENT DATA

a) TYPE

b)

c)

MODEL No.

RANGE a!' ice, -ZcOA r - Oo I90 06F

47/3 ZT

-300 CT-- 01I

C0 0o 0, L&0.I4d) DATE CALIBRATED

e) CALIBRATED BY

University of Akron Test Operator

UST&D Test Supervisor (Engineer)

UST&D Quality Representative

Transnuclear Witness (if required) - _..._ _ __/_ _...... .

\1

High Temperature Buckling Testing of Composite Panel A2

280000

240000

200000-

160000-

120000-

"Q

0_j

0

0

/0

/

80000+

40000-

n I

C.J 7I a a

).000 0.020 0.040 0.060 0.080 0Deflection (in)

Deflection as Measured by LVDT model E 500 S/N 2044

,100

UST\I)\\~I~ A U

COMPOSITE PANEL LOAD TEST DATA SHEET Z,

START OF TEST DATA

a) TEMPERATURE 1 ,1fJq/ ~~;eb) LOAD __

c) VERTICAL DEFLECTION ,)d) TEST PANEL IDO 132-

e) No. OF PANEL WELDS

f) DATE & TIME 9 0


a) TEMPERATURE L/-,50.1JIe sij

b) LOAD ?6 7 2-5c.

C) VERTICAL DEFLECTION

ND OF TST (50% of max. oad)

a) TEMPERATURE _____ ____ ___d__11____ ____

b) LOAD 3 Z, 67..

c) VERTICAL DEFLECTION ,, 7 (76__ _........ . ....

cl) TIME

EQUIPMENT DATA

a)b)

d)e)

TYPE

MODEL No.RANGE

DATE CALIBRATED

CALIBRATED BY

D rf? Zria-m, 1/60, 6 0ý

0 10 ý o z390ý64* 1c) q C'Lr1 1-,Z.90 I



UST&D Quality Representative

Transnuclear Witness (if required)

r• I I .. .~. ., .,. .i .. ... . ...

High Temperature Buckling Testing of Composite Panel B2

280000

240000

200000

0-j

160000t

120000'-

800001

40000--

0C).000 0.020 0.040 0.060 0.080 0

Deflection (in)Deflection as Measured by LVDT model E 500 S/N 2044

.100

r tiS'LX1) ~/. ~

'XV, A '!'-,"1-'V "4." 1ý"Xý 41

COMPOSITE PANEL LOAD TEST DATA SHEET

START OF TEST DATA

a) TEMPERATURE 2- Z5 7 l;'/e Ic 3 ,db) LOAD

c) VERTICAL DEFLECTION 0_

d) TEST PANEL ID# C Ze) No. OF PANEL WELDS

f) DATE & TIME 3 0


a) TEMPERATURE 7- 6 ,9

b) LOAD 2 '/ 5c0

C) VERTICAL DEFLECTION - .

END OF TEST (50% of max. load)

a) TEMPERATURE -3 32Z r.1;(/e 9 c9 c4L s*sde

b) LOAD

c) VERTICAL DEFLECTION 4'4 S Z 5/d) TIME '4.4"/- O,,N..E . .. .,,, .. .

EQUIPMENT DATA

a)

b)c)

d)

e)

TYPE -nay~~ n0- /MODEL No. ).•ri.5o,.S,,zO.M r, - 3_OC_-_1,6

RANGE o-,oi g " A,,1,, - - F- C43 1 0oo ..bs.DATE CALIBRATED -.. /1 1, . /goCALIBRATED BY p. 42i&Jo,, " CoI,.S



UST&D Quality Representative ___..-._.....

Transnuclear Witness (if required)

\1

High Temperature Buckling Testing of Composite Panel C2

£2

00

-j

280000-

240000-

200000-

160000-

120000-

80000-

40000-

0.,0

I

0

0

0

00

/

0/

0

0$ .C).000 0.020 0.040 0.060

Deflection (in)Deflection as Measured by LVDT model

i

0.080 0.100

E 500 S/N 2044

1C.

Of r01,1[Departmecnt of N'1tc~han ical Enginee~ringC~ollege of EngineeringAkron, 01-1 4,1325-3903

(216) 375-7731

CALIBRATION OF THE BALDWIN COMPRESSION MACHINE

The compression test machine was calibrated on April 13, 1990

prior to the start of the test series by C&M Collins Calibration

Service.

Attached is a plot of the calibration data for the compression

machine and the data taken by C&M Collins Calibration Service.

Ge , Ph.D.

Date

'. 0 . LI (; 1 0 F1F N Cý I N EF h RF N t,

*\NNIVUSAI(Y

En)4ineerin).F Ui T Ui R E

The Univem~ity, of *Axron 4,a Fqu~ poyetI.looanft , nPloymvni Insmution

-Q

Q)a:V

C)C

300000

250000

200000

150000

100000

50000

00 50000 100000 150000 200000 250000 300000

Calibration Device Reading (Ib)Calibration of Load Cell of Baldwin Compression Machine

SSeport & (Tertificai e of erifiratiouC&M COLLINS CALIBRATION SERVICE

THIS IS TO CERTIFY that the following described testing machine has been calibrated by C&M CALI-* BRATION and the loading range(s) shown below found to be within a maximum tolerance of

/1 %.

MACHINE TYPE

LOCATION "/) ; V ej,^.r I' I L_' CAPACITY 30Oo00/4j

CA; o) SERIAL NO. 10oCT -,/o/,_(

DATE OF VERIFICATION .. pr,'l /3 ,'?90Method of verification and below recorded data Is In accordance with A.S.T.M. 2-4 8 .3. The testing device(s) used forthis calibration have certifications traceable to the National Institute of Standards Technology.

Machine Readings U] Pounds El Newtons 0 Kilograms Readings temperature corrected for 72. Y 'F.

MACHINE CALIBRATION DEVICE MACHINE ER OR C.0READING READING %NO

2iL ~ C/ 4- ,7

-7 0 0 _ -71____o 4-13.0 .j I

12 00 0 1 1 og -e- / .76 e

1.6000 e a .17 3

36oooo 3 y t - o .71 3

MACHINE CALIBRATION DEVICE MACHINE ERROR c..

READING READING q 6," . NO,

. C 000 to/?' /Y , 3

12 0000 //9_____

/8100o0 /71Žo5 f79 9 .' 3

00000 Z 9790 9 o??/ ,70 .

CALIBRATION APPARATUS - Morehouse Proving Rings, StaInsense load cells & Troemner Dead Weights. Verificationstraceable to the National Institute of Standards Technology, in accordance with A.S.T.M. latest specifications.,C.D. SERIAL NO. LOADING RANGE CALIB. NATIONAL INSTITUTE OF STANDARDS TECHNOLOGY LAB NO. TEMP.CODE CLASS AVALUE DATE OF CD,

1__ 3914!t'-6 612-IOA 16s !S-27-kY 7X 2'?! 1 Ž7 S 5 I?2 R o j?3?al •to S.T70Fr -// I1o? 1.-7 7e

3 ?'5lC?3 4Z I..rgo-o¢ ....g- S-?1-9 SIT7o0 // /o0, 2,,,7 7__1

4

5 __________ _______ ______

MACHINE RANGE LOADING RANGE

6 000o 161 (,,ooo -6ooov c r

0-~~ O?-d IotJo 1jk

Primary L.•ad Indicating Device

C & M COLLINS CALIBRATION SERVICE

230 Haymont Dr., Box 149, Gibsonia, PA 15044(412) 443-7631

By:(RENE(SERVICE ENGINEEFR)

W•tnessed

By:

Witnessed By:

o r L I 11VCrI.

, ~plrsit\

[)epartinent at o Med:)anical Engineering (216) 375-7731C.ollege o(f EngineeringAkron, OH 44325-3903

CALIBRATION OF THE LVDT

The LVDT calibrator is a micrometer device on a fixture. Both

the calibration device and LVDT, model E 500 S/N 2044, were

calibrated using the model DJR 450 digital transducer readout.

(a) Calibration Device

The micrometer of the calibration device was calibrated

on May 2, 1990, using Johansson Gage Blocks. Attached is

a plot of this calibration. The accuracy is ± 0.001".

(b) Calibration of the LVDT

The LVDT was calibrated during the week of April 16, using

the calibration device. A plot of the calibration is

attached. Measurements are within ± 0.010.

0;! N-b. S. au, Ph.D.ANNIVE RSA Y

Fngineering U R -DFUTURE Date

The Univonity 4' Akron i. an ' luction -a. Iinplovrnrt In51.titai

C:

0"0

E0

0)

1.000-

0.900-

0.800-

0.700-

0.600-

0.500-

0.400-

Calbration of Micrometer (No 2632']LD rasueLVDT Transducer E 500 S/N 2044Using JOHANSSON GAGE BLOCK 1 ASerial No 10008Y = -0.00012236 + 0.99943 X j-

I I I

flm

0.300 -

0.200-0.100-

n' n' t"•I t"•

0.000I I I

0.200 0.400 0.600Thickness of Gage Block (in)

Calibration of Micrometer

0.800 1.000

2.000E4

1.500E4

1.000E4

05000.000

LVDT Transducer E 500 S/N 2044DTR-450 Digital Transducer Readout (0083971)Y = 10888 - 20574 X

0.000

-5000.000-

-1.000E4 -

- 1.500E4+

-2.000E4 10.000

I ! Ii i -

0.200I i

0.400 0.600Displacement (in)

Calibration of LVDT

0.800 1.000

ro•

[)epartment of Mechacnical Engineering (216) 375-7731College of Engineering.Akron, OH 44325-3903

CALIBRATION OF THERMOCOUPLES

Three high temperature thermocouples using ANSI Type J high

temperature wire (wire code CG-J-20-SEE) with a model OMEGA

115 distal thermocouple readout. The temperature range for

this wire is from -100 0 C to 720 0 C (-100°F to 1400'F). Each

digital system (Serial No.'s 0091154, 0091155 and 0091159)

was calibrated using the OMEGA calibrator Model CL-307 by

C. Bailey, Electronics Technician, Dept. of Mechanical Engin-

eering, during the week of April 23, 1990. In addition, the

systems were checked at the freezing and boiling points of

water. An accuracy of t 2'F is obtained.

S. u, Ph.D.

75 Date

ANNI\ERSARY

Engineering

F U T U R E

Thv.Uniw~rfty of ~At, - iý anF, ioppene tno ;

7 0 0 i

Calbration of 0091154 Using OMEGA CL-307

2" 600± Y = -0.033732 + 1.0025 X

% 5100-j04-

400

'I)-3000020 200E Tci)

_ 100H1--

0 100 200 300 400 500 600 700


700- 7 Calbration of 0091154 at Frezzing and Boiling PointL600-of Water

o Y =1.239 + 0.98944 X

500±0

400

-300000 200E

_c100F-

00 100 200 300 400 500 600 700

Temperature Of Water (OF)

7 0 0 Calbration of 0091155 at Frezzing and Boiling Point~-~ 6 ~jof Water

0 Ty = 0.23902 + 0.98944 X -

:3 5000

Q400

3-3000

0200E-

0

0 100 200 300 400 50 600 7600Temperature of Water (OF)


o600- Y =-0.63457 + 1.0044 X

o5004-0 0t

-0

02E

4.00I- 300-

0

0c 1001

0 100 200 300 400 500 600 700Calibration Device Reading (OF)


(.

700-,Calbration of 0091159 at Frezzing and Boiling Point

i 600o"of Water0 Y= -0.93941 + 0.995 X

4o-

D 400--

Q)~- 3000

o 200-7E

-c100 +

0 -- 4----------- I -I

0 100 200 300 400 500 600 700Temperature of Water (OF)


QL 600 Y = -1.0431 + 1 .0049 X0

5000

Q400

c,300:30

E

£100

0--

0 100 200 300 400 500 600 700Calibration Device Reading (OF)


APPENDIX C

MATERIALS DOCUMENTATION

1\cý

DOCUMENTATION CHBCKLI8T

CUSTOMERDOCUMENTS PAGE PAGE REVIEW & REMARKS

QTY. NO. RELEASE

DOCUMERNTATION CHECKLIST17.2 1 1

SHOP BILL OF MATERIALS 8.... ..8.3 1 2 __ __ __ _ _. . . ..___ __ _

MATERIAL LOG8.1 3 3- 5

ýMATERIAL TEST REPORTS & 5 6-11CERTIFICATES OF CONFORMANCEWELD EXAMINATION RECORDS

10.5 12 12-13

DIMENSIONAL DATA RECORD 1 14

.FINAL INSPECTION CHECKLIST 1 1510.4

CUSTOMER P.O. NO. UST&D PART NO. PART DESCRIPTION QUANTITY4-Phase I

NA Drawing 89-011-1 CASK INTERNALS 4-Phase II

UST&D CERTIFIES'THAT THE LISTED WORK AND REQUIRED DOCUMENTS MEET THEREQUIREMENTS OF THE PROCUREMENT DOCUMENTS.

UST&D' QA/QC DATE

WORK WAS RELEASED ON SATISFACTORY COMPLETION OF INSPECTION AND REVIEWOF DOCUMENTATION.

CUSTOMER REPRESENTATIVE DATE

CUSTOMER TRANSNUCLEAR PROJECT UNIVERSITY OF AKRON

UST&D PROJECT NO. 89-011 SHIPMENT NO. ONE

form 17.2

PA E.W OfJ

L/iw/ ProductsF-dyI"O UTX)L ! * L,4 5c04 s _

A

H PC. HK , QUA DECITO "tI=d =Q1¢ RETMARKS

2-. -_7 :L ? " Ji....• S 0 ______

;24 46041

_______ /(~, ~ £ O • . .. _ _ _ _ _ _

-4--

. .. . . .. 3. i . . . . .j i .4.

- _ ___ ___ ___ ______ ___ 2

4 S S. p

4 9-9 9 .1 t

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-. . .. ..a. .'

USTOMER .. ... f .. ... i JDWG REV.ROJECT SHOP al LL REV. 07Y , PRoJ. NGR. PAI ._ OF .

V

QCP Form 8.3

PAGE OF .2L

v,--1ý UST& D

U. S. TOOL & DIE, INC.

MATERIAL LOG

FOR AqLUMINUMP.O0. Heat -Lot - Da te Submit

MIC # Description Numnber Batch # Source Cert. Doc.

A-J6 644 1 TroALUM 83-11S97 So7PNE .16_____31"y211 Z G)( G4 I pe 83 _ ________ _____PAN__Y

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Form 8.1

PAGE 3 . F•_P

-. UST&DU. S. TOOL & DIE, INC.

MATERIAL LOG

P..O. Heat -Lot - Da te Submit

MIC # Description Number Batch #t Source Cert. Doc,

5-1010 ff7-~V~T 6'0-7O'W 272Z14\N HUB INC.214 -

_7__ -70 91Jk Iboq HUBIC in. -21-88

S-1012 I/2sX.IXL 67-70 q/ 17I1147W HUB INIC 2.8

S71013 iyZ?-Aq. lay,..q.16 87-70q/4 1.1 q 7 W I1UB INC. -.- 8 __

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~~~~ LtEI 855~ 04 .X~BO~ 888o2~ '5 ______ ___ ____

Form 8. 1 Page S-1oiPAU-~ L

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I- I I . ~ _______--

PAGE ~9OF .,., 7& ________ J___________ A__________ _ __ __ __ ____

Page ..

QCP 7.5 Att.3.2

CERTIFIED INSPECTION REPORT %,t .- LUM I.INUIVI %IVIr'MI T+ ± r- I . A LC O A ""

N K INC .48939-99-ST.90-E0.O NO./GOVT. CONTRACT NO.

~jr t1 ¶1YI TSBURGH PAA'ýHIPPED FROM: OAVENPORT,l ,OWA

»'PAGE 00 .V0

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Uupt 1 II . 51 iS213 We hweby carily thaith z" aton~al c.oveed by I1ES ieport has been .nspocteij ., aCcotdarce .1111, an~ajjýsbee fo..nc to ,neT. the *PP6,.tI. eer-oaCnbed hawe~fl. "nclodmr, any lipeclfýIIUon lomni.rg a "A ol the 06encflt~n andl thti~ Sat'pies tspresahlatne GI Mm ,naloteal.tna the COtnPo.tton Itints pne

the ntýhancal oy~Ie.,a 61to,, On Sae fae. of tt,, sheet Pe

INVOICE NO INVOICE DATE CODE Q'2 2 t.. UAIJTY

2256583? 89/10/23 1163 974"820 MANSAGCER

ALCOA NO. SHIP DATE VIA

UR 32797 89/.10/-23 IACE DORAN _ _ _ _ _ _ _ _ _ _ _

4-

[i~ ~vaj:I U.4. ~}4 ~ '~'

PRODUCT LDESCiIPTION

DLATE IB/LNO. 'GROSS WEIGHT

§68 4486ALLOY-TEMPER

6061 T651

V

ITEM DESCRIPTION OUANTIrY SHIPPED Of TIEST (D TEST (DT T ( TEST D TE TEST ib TES-

PCs..FT..1ETC POUNDS .. -O _ !

.2500 IN Ti x 36.5.0u IN LJ X -431•99- UTS1 TYS1 EL4D96.560 IN L;N '!ZAT 0 1243.'• (N) AT OQT-288963 T6.%l -L.T MAX 43.4 3:8.0 15.5-6061-T651 TYPE 200 WROQUGHT 26 K M IN 42.4 3 7.j-fA.~-TUOLING PLATE MILL FINISH PER . f-'QQ-A-250'/11 RE.U F & (EX. M1-;PK) "OT-28896 14 -).5,LT. T_ MAX 43.4 38.2:. M'S4027 .REU K & (.EX. MARK) ... 23Pc "' "• .. ,-" .. I MIN 43.1 38.0 '_". -"-'_.... ',.;. .. •• |::;"

ASTMi6209 REV 88 (EX. MAR~K) ,-.. -

MlL-1-45208 REV A AM 1 ((MARYED)L . - •INTRtlEAVED SKID WGT: 4000 L8 .. -

- UA J~VOL +/-10 b. ýfCQR 0003220 REU 01 ). 4".- ...- :.

PACKAGE LOT N0 ;I 7 ..-. .-301398B 288963.301398 288961 WM-& &, - "

QIA.A AR -. ?Q

OCT 2519

flChemicalComposition SI FE CU MN MG -R 21N TI OTHER OTHER ALUrMINUMI

Max. 0.8 .7 0.4,0 0.15 1.2 0.35 0.25 0.15 0.05 0.15 REMAINDERN.uAloy C . •.1 Min. 0.400.1', 0.e 0. 04 EACH .TOTAL

I-Chemical:Compositon

.1 MaxI-..Mmn.

(.IJ 1. WHEN 2 OR MORE TESTS PER LOT ARE MADE. THE HIGHEST AND LOWEST VALUES ARE REPORTED FOR EACH PROPERTY DETERMINED.

2. SE7 -,,:'-ST ABBREVIATION EXPLANATION ON THE BACK OF THIS SHEET. -' . .-

- . . ;.

11 9•"&U11 IL "L

certification'ýDcA 0ý_

4*00 Ryersona subsidiary ofInland Steel Industries, Inc.

U.S. Tool & Die Inc.4030 RTE 8Allison Park, Pa. 15101

DATE OUR ORDER NO,

2/29/88 11 738437

YOUR ORDER N

88 80215

HEAT NIJMBERITEM DESCRIPTION

60 SHTS STNLS TYPE 304 L 12 GA X 48 x 9610 CFR 21 APPLIESASTM A 240

835499TEST # A379'

This material has been supplied in accordance with our QualityAssurance Program, Rev 8 dated May 1987.

)4ý

UST&DREVIE&JAPPROVAIC

uTY ASSURANCE

A survey of our material sources has indicated that neither mercury nor radioactive substances is introduced into t1products, or is used in any of their processes. While we make no independent tests for mercury or radiation, ther,nothing in Ryerson's system which could be expected to introduce contamination of either type.This document certifies that the material described above was shipped on your order and that the attached data is a tcopy of the test report firnished by the producer with said material. PAG E -OF

JOSEPH T. RYERSON & SON, ID•

By (iuhrd Aj

- COPYT4 .OSEPH T. RYERSON A SONFORM 230.44 2 Rov

9-102..IPA~ *.~LOF

NOT ICk&VOHIMENTf

DM9WONOiFmURLHUJOLUM:fl&tCAJONm~axAmma uAtroQaaAur s

AL 3SG-5' logo

CERTIFICATE OF TEST

c u s m . & . . 'm m o m -C C C 2 Ya - c. m C Sý & . . -s .

U3AK 3692 b7/i7/8371 783505 I NEWd CASTLE, IN. L)7ý5404 3012000 13-77/881i~i '

021565-1 I 11124 ImEmd CASTLE N 7ý540A S LD TO :PR IME SEC. SHIP TO

JOSEPH 'W *YERSON AMD SON INC. DEW DSO JOSEPH T RYERSON AND SON INC . sbPO BOX 8000-A 28 DRITE LINE DOOR 13 - K SPANCHICAGO IL 6"80 2558 WEST 16TH STREET

CHICAGO IL 60406U?

GRADE AND SPECIFICATIONS FRT CHG - PPD ADD CARRIER - KAPLAN TRUCKING41-EG, ENY STAINLESS STEEL TYPE 304-L SHEET C R COILS ANWEALED 29 FIN 3 EDGE RYER SPEC (751t-FlIASTM-A-240-6") LAT/DUPONT (S1-300-M) LAT/ LAT CONW A EXCEPT MARKING (ANS 5511E) LAT EXCEPT MARKING/SUIT-Ar TO LGTH LINE (ASHE-SA-240-A6) (ASTM-A-480-85) (08/09/85 EXCEPTIONS TO 75"1-F) (ASTDI-A-262-86 PRZ/.CREEN PR A)-----

l £.'rEM PCS DIMENSIONS WI/G/L

438 1 48./.t*5/COILAV.&A. .102C CUST IDENTITY CC 741125

i COIL

HEAT # COIL #

835499 1 0"27M4050

TEST 0 GROSS TARE NET THED TAG 0/ CID SKID 4

A3792 22162 22162

22162

588171 A5

io'loyo22162

.AtDEREMARKS: PAPER WRAPPED-NO SKID-LOAD ONLY BRITE LINE MATL ON SAME-TRK AIM LRG AS POSS-CDPRD CORE 1/2"

MIN THKNSDIST: ACK TO SOLD TO ATTN: MDSE DEPTi I S/N TO SOLD TO ATTN: R.T. DESK; ¶ CPY T/R TO RYERSON ATTIN:

JEAN MALEC, PO BOX 8263, CHICAGO, IL 60680

TYPE HEAT/TESTADLE 835499

ýEM-)3BD

02.-M.. --

> .02 1.81 .E

m• YIELD TENSILEI F41000"./ 89500.I PSI '/

011i * Y-S- BY O.2X OFF

-P- ..-- 5--.138 .00)2

TEST NOA3792

Z ELONG CORROSIONIN 2:/ ZXR/A HARDNESS BEMD A 262 PR E

58. MR 83.HRBV/ T PASS PASS83.HR w

SET METHOD UST&DEV.IEV lAPPROVAl

. .ý 3:1'

18.07 .4t .37 .08

GRAINSIZEMR

HAR•DE•BILITYMR

..j i

NR = DATA NOTI' REQUIRED

PAGE 01 OF CONTINUED ON NEXT PAGE Ii 'vu,, .1/10/87 14:17:14-w - ' • I ,

I 'A now 0. o/

NOTICE OF SHIPMENTALLEG11E9t: -MUQM STEE

W0tSKWE4NAU.EGI-VfriEN.L4COUC0WA~tN

AL 6164.-t IC

CERTIFICATE OF TEST

-4

.33AK3692 07/17/871 783505 NEW CASTLE,

"W-0 1 11 I ý 1- a -1 565-IjSOLD TO PRIME SEC.

JOSEPH T. RYERSON AND SON INC. DSO DSOPO BOX 8000-A 28CHICAGO IL 6068e

I

I. r754-4 I30201 6~0O 0-077-298 109/87

I124 INEWICASTLE - IN 7540.4SHIP TO

JOSEPH T RYERSON AND SON INCBRITE LINE DOOR 13 - K SPAN2558 4UEST 16TH STREETCHICAGO IL 60606

-1

GRADE AND SPECIFICATIONS FRT CHiG - PPD ADD CARRIER - KAPLAN TRUCKINGALLEGHENY STAINLESS STEEL TYPE 304-L SHEET C R COILS ANNEALED 2B FIN 3 EDGE RYER SPEC (7511-F).C4STM-A-249--86) LAT/DUPONT (SM-300-M) LAT/ LAT COND A EXCEPT MARKING (AMS 5511E) LAT EXCEPT MARKING/SUIT FGLtT TO LGTH LINE (AS,.E-SAr-240-A6) (ASTM-A-480-85) (08/09/85 EXCEPTIONS TO 7511-F) (ASTM-A-262-86 PR1ECREEN PR A) - -

AI•STENITIC STAINLESS STEELS ARE SOLUTION ANNEALED AT 1990 DEGREES FAHIENHEIT MINIMUM ANDAi-TIIDLY COOLED TO DEVELOP THE SPECIFIED PROPERTIES. EVIDENCE OF CONFORMNCE IS PROVIDED BY THE

4I0LITY OF THE MATERIAL TO MEET THESE SPECIFIED MECHANICAL AMI CORROSION REQUIREMENMTS

I-iLEGHENY LUDLUM DOES NOT TEST FOR MERCURY OR RADIOACTIVITY AS PART OF ITS QUALITY ASSURANCE PROGRAM.MIWVER, WE DO NOT SPECIFY EITHER MERCURY OR RADIOACTIVE MATERIAS AS INGREDIENTS IN OUR STEELS NOR DOWJE USE THEM IN PRODUCTION OPERATIONS EXCEPT IN DEVICES SUCH AS THERMOMETERS, BAROMETERS, MANWOETERS,EIZ. •CHEMICAL ANALYTICAL EQUIPMENT AND NON-CONTACTING GAUGING DEVICES FOR THE MEASUREMEIT OF

1THICKNESS, ETC.SINCE THESE MATERIALS EXIST IN NAT1JRAL BACKGROUND LEVELS THROUGHOUT THE EARTH, IT IS NOT POSSIBLE FORUS TO CERTIFY TOTAL FREEDOM. WE CAN ONLY INDICATE THAT SUCH MATERIALS ARE NEITHER A KNOWN INGREDIENTPN OUR PRODUCT COMPOSITIONS NOR ARE THEY USED IN MANMUACTURING OPERATIONS IN ANY DELIBERATE FASHIONMHICH WOULD RESULT IN THEIR PRESENCE.

REFERENCED SPECS MODIFIED BY CUSTOMER SPECS.

2'tRROSIOM PERFORMED PER ASTM-A-262 PRACTICE E SCREENED IN ACCORDANCE WITH PRACTICE A.

UST& D

m REVIEWIAPPROVA"

-I 2-k-FLITY ASSURANCE

C4

PAG 02OF22 REPRINTI - w~w*"%-m=lfw

11/19/87 14:18:50

IL A S

CASTLE MET

£ 14ý 5/1AL~ SPECIALTY'S! dIWPa&10N 05,"2' 1 0 9 1517ARMCO0 A .buba~isry of AsrGm oo. Inc. PACKING LIP A

ALS vP.O. Box 1697. Balumwa,. Matyland 2 1203 CIRTINICATI Of CH*1

IBMICAL ANALYSIS AND TESTS-B020 I IV" i 0-70445 2 6" 2 0511-15/139 c"

'2000136309'020 /B/ -80028I, oto CASTLE METALS 80.51o CASTLE METALS, CTO FUR DEFT to 26800 MILES RD

3,100 N WOLF ROAD BEDFORD, HGTS 44146FRANKLIN FARK, IL 60131

40 ROUTING C9 CAR INITIAIL AND NO.

GEORGE TRANSFER / . Rom MO L

O0VNN'AGt GROS WEl~w~ I'Il*Ht "to~l $10p o, •e 11 Poo •J ... ...... P O C.$rt... ,Goimt( i t

X4 ( 2 2 .242 3.6000i

1f0• HEAT ,I BDL . . -. ' .

pIoouciTh Li " SNL2 TYPE 304 SMOOTH TURNED gCSTE 41? 4,.h,0 AM' S39E.'ASME $A,179 '86ED/BSAI}D 304A ASTM A484"ISME 5A182 *ADD ANAL ONLY-l•%ril A276-87 COND A ASTM A479-87TB 304A •$TM A182-B7A ANAL_ ONLY ASTri1IA193-87 CL i ANAL + MECH PROPS ONLrQQS 763E COND A EX iT TRT iMIL-H-687

iVD 69241 '4 iR4 XI M00` \YC 514 SF' '3- __) 1 _ _ __ _CUST No 4, ) 6 ; 7 CA

901 a,2413.062 . B~9' '•924,13 CU .42A ;' 'MPLE TAKE F 1-.'

•924'3 066 .03''92413 CU .420

I-) T: 1 INC HE -EBYA M.AT:RIA 14Y

)1(:.:CT Co4NEC ED MOR IERCUR -IN -LASor1-I rEST:IN ' HA (A)h|fMATRIAL qOR B) RHFý'q MATEF AL IEEN

6924,13 BI1Ni 49

,0360025 A,68118.56 ?.00 MO .25N .06, CO .i1i A EIAR F TAE A1i)VE H.AT WAS AN )LYZED.029.028 .7010.51 8.96 MO .25N .065 CO .ii

:ERTEFIE' TH•T IN THE 'RODUCTION OR TESTING OF THE-NRMC IN.. 40 AL "HA EiITTING RA3IATION DEVICESKRCU•Y M.NOMT'TERS MER URY VACUU4 PUMPS MERCURY SEALSSTH:'RMO4ETEM$ HAVE BE EN USED N]R IN SUCH PRODUCTIONMEKjURY BEE HANDLED IN THE IMMZDIATE VICINITY OF SUCH

IDIO[CTI E M TERIýL BEEN APPLIED TO ITS SURFACE; NOR (C):ONT•MIN TED BY N RCUR LEAD RBI)IUM OR ALPHA SOURCL"3

111. OU V I,

8,400 47OF /ý

-I0-REE FROM CONTINUOUS CARBIDE NKTWORK---MACRO ETCH TEST SATISFACTORY INTERGRANULAR CORROSION TEST 01< FER ASTH 1i2621,-MATERIAL ANNEALED 1950 LV. F 1/2 HR WATER QUENCH CASTLE METALS-CLV

USTaD DT ED b5$OVAL REC'D FROM

A... ASSR A.A11111 AND Affm v It N11 COuld At CONv0, "V " " •--*$'I NO sw TIS 'MAYrd I 189 E.T'AMULAR~O, cERT

I"T rakic THIS CJRFTIFIEO TEST REPORT HAS 44 OfIVERED TO A CONSIGNEE OF MATERIALPUACAS10 FRM AMCOINC. TO AVOID THE POISSIOILIY 0f it$ MISU~if. ON ITHEREIIEYOF THIS REPORT TO A T"IMhl PARTY 11 MV31 So ECLtIPIEU UY AND

UNDER THE NAMAS OF SUCH CON011CINES4.

3w1374

u SL INCNuclem-ProductsWELD EXAMINATION RECORD

-WELD DATAW E L D ID . . . ._ _ _ . . . . . .. _ ._. . ..WELD-TYPEWELD PROC.

WELD PPOC, ____ ___

WELDER ID. ... 6

FILLER ICCC ACCEPT -

S T i • i I CD Ii .. . 1EI 111 -.2

Drawing 89011-1TypeA

Item 1 to item 3(8 places) WPS-531)

2) Item 1 to item

3) Item 1 to item

4) Item 1 to item

Type B3(12 places) WPS-53

Type C3(16 places) WPS-53

Type D3(24 places) WPS-53

PAGE_ . OF

PROJECT- TRANSNUCLEAR-INC. PROJECT NUMBER 8901,

Test jLate Mock" 's ASSEMBLY DWG NO& 8901.-IIINSPECTO, --. FINAL INSP. DATE' ..• PC, MK .....

WtLUINU VLU(tkiUUMtI .bwIHCjATI

u•t U.6. TOOL & DIE, INC.• FORM 9.1

WflS NO, 53

REV NO. 2

PAGE . OF - -I U. I

SUPPORTING POR'S:

NO. 5E REV. 2 --

NO. 5F REV. 2NO. __ REV.

NO -REV. __

REFERENCE TO%

AS&E IX UASME III imASME VIIIAPPENDIX

14 - 10

PROCESS:

GTAW U WELD - THROUGHARC SPOT FUSION WELDTYPE:AUTOMATIC TIMED ARC

POSITION(S):

FLAT

HORZ 03VERT 3

OVERbID 0

CHARPY QUALIFIE

ASME IX 0ASME I11 0NONE N/AWr

a aDESIGN: SPOT WELD OF LAPPED MEMBERS

PENETRATION: FULL U1 PARTIAL 13 N/A 03BACKING: NO 03 YES 02 FUSING r1 NON-FUSING 13

OTHER: WITH COPPER BACKING

SHIELDING GAS ARGON OXYGEN HELIUM CO

LOWRATECFH. 7- 7o-92-TO 30 COMP -_" , __

P NO. 8...GROUP L1.ASME - SA240TYPE 304

TOIP. NO. .-L GROUP 4

ASME - Sa 240TYPE 304

BACKING GAS 0 YES 13 NO TRAILING GAS 03 YES Cl N(N/ACOMPOSITION & FLOW RATE

THICKNESS RANGE:

CURRENT: AC 0 OCE

POLARITY: STRAIGHT 13 REVERSE 0AMPS * VOLTS *BASE METAL *t MEMBER TO *t MEMBER

DEPOSITED WELD METAL THROUGH t AND INTO tTO OBTAIN A MINIMUM NUGýT DIAMETER'AT THE FAYING SURFACE - 1/2".

at *AMPS *VOLTS *ARC TIME

.0 l~.9G:o •'18 18-3 2S•f_.J~ ~U u'.U- -C 2 5E

I ~ l cpS)BEAD: STRINGER 0 WEAVE 0 BOTH (3 N/A

MULTIPLE 10 OR SINGLE M PASS PER SIDE SUPPLEMENTAL FILLER N/A

CONSUMABLE INSERT DELETED

RETAINERS DELETED

IMr•T qs __

MAXIMUM PASS THICKNESS t 1 , 2 £JJU, £U.*. -

THRU IN t2 MEMBER WHICH IS NOT EXCESSIVE.

FILLER METAL ** PEL,=EDMINIMUM PREHEAT TEMP. 50p F

FILLER SFA NO. _ _ _ AWS NO. **

F. NO. -_ _ CHEMISTRY OR A NO. .

WIRE/FILLER METAL SIZE __ _ _ _,,,,,,,,

MAXIMUM INTERPASS TEMP.

POSTWELD HEAT TREATMENT NONE

1/8"

AUTO OSCILLATION: NO!0- WIDTH N/A

FREOUENCY NLA .DWELL TIME N/A

MULTIPLE ELECTRODE N/A SPACING N/AELECTRODE SIZE

TYPE ELECTRODE 2% TBORIATED TUNGSTEN

N/ACONTACT TUBE TO WORK DIST.?•4 "€ ,,,•, ....

ORIFICE OR GAS CUP Size _ -, 3 .1L. - ..ELECTRODE TIP TO bW DISTANCE~--.150o

BACK GOUGING METHOD

PUENING. YES 0l NOW

N/A

INITIAL AND INTERPASS&ECIANING: STAINLESS STEEL WIRE BRUSHING OR GRINDING

NOTE: PRIOR TO WLDING USING THIS P , A WORKMANSHIP WELD SAMPLE SHALL BE MADEFROM EACH WELDING MACHINE ON MATERIAL OF THE SAME THICKNSS, SPECIFICATIONAND GRADE AS TO BE USED IN CONSTRUCTION3 AND BE REPRESENTATIVE OF THE PRACTICEEMPLOYED IN FABRICATION AND TO BE USED FOR THE PRODUCTION WELDS.

PAGE/:- F O ,/N

USE 1)PROJECT NO. 89011

TEST PLATE MOCK-UP DATA RECORD (STORAGE CASK INTERNALS)

(REF.UST&D DWG. 89011-1)

PHASE Ia -

TYPE A TYPE B TYPE C TYPX D

A ...1 ...0 ..... 4 •. .

B ,2-zs •____

C •.266 .____ 2 55 .25•

D

E .7317- . ql .I4.-

PHASE II

TYPE A TYPE B TYPE C TYPE D

A . o //Io0

B 2 (

B 75(3z• 2& 5

D , //0 l ./) /09

E -75E ,¢- .743. 3

-AFTER WELDING

---- ~~~~Ik\\\ \\ '-•[

I'-tQINSTRWtNT USED 6-I

/27

09 3 2a 90INSPkOR DATE

PAGE/ 2OF '\1 i

US11&ID,

FINAL INSPECTION CHECKLIST

INSPECTION

1. DIMENSIONAL VERIFICATION

2. MIC # CERTIFICATION

3. VISUAL WELD INSPECTION

4. CLEAN (Per Proc. 13.2)

5. MARKINGS

CUSTOMER SPECIAL INSPECTIONS

7. DIMENSIONAL DATA RECORD

8.

9.

1.

2.

3.

4.

5.

6/9

INSPECTION

Dimensions are to be verified and be within the tolerances shown on theShop Drawings.

Material Inventory Control numbers marked on the material are to be inaccordance with those shown on the Documentation Shop Bill of Material.

Visual Weld Inspection is to be performed, accepted, and documented per thecriteria established in Procedure 10.5

The finished piece is to be inspected for cleanliness per the requirementsof Procedure 13.2.

Markings on the finished piece are to be in accordance with Procedure 13.3and the Client's Specification.

List and perform all special Client inspections and record acceptance perwritten procedures.

PROJECT UNIVERSITY OF AKRON

CASK INTERNALS

INSPECTOR .2? ... FINAL I

PROJECT NUMBER 89-011

ASSEMBLY DRAWING NO. 89-011-1,2

NSP. DATE 3, :2 2-9) PI ECEMARK Cask ,nt,

P AGE ., -(OF/j ,Form 10.4

--st ~3"3"

7k (9'

/ 33" .

3'. 1

I-*3"

'. .. .... . .... ..

... • 3"":': .... ........... ' .......

,.j f.. ir.• .... 'CA...... .... •.•.• ...••. ....3.3:: • 1• •••.•'•• .. -,'''.-" :... •.•...........4...:,9..&. .h.. /....... ... /1<

" 7-,i -•;5:""u;;L.-:: """7•'" •:[-":": '7:•:.,•: .............:,,,•• ....... ••• ........ >.........: ..........

3 7(.3

.222".3 7 4,33

- $7 "/9%

I472.,33LŽ& *'~~/~ 3#

e~Q~ 1)"it,

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3 -c!4~rrAtt ~k~7

fl "4?> ....... ~ / -- 3-.3 77 x33"'~ -fi

- - "3 - - 33? r

1$

Enclosure 21 to TN E-28034

Public versions of Enclosures 5, 9, 15, 16, and 17, as follows:

5 RAI Responses (proprietary items)

9 TN Technical Report No. E-25768, Rev. 0, "Evaluation of Creep of NUHOMS BasketAluminum Components under Long Term Storage Conditions," November 2007

15 Transnuclear, Inc. Calculation 10421-024



• r .

Non-Proprietary Version

RAIs and Responses

6.0 CRITICALITY

Enclosure 5 to E-28034

6-1

Proprietary Information WithheldPursuant to 10 CFR 2.390Response to 6-1

6-3

Page 1 of 3


RAIs and Responses Enclosure 5 to E-28034

6-4

Page 2 of 3


RAIs and Responses Enclosure 5 to E-28034

Response to 6-4

6-5

Proprietary Information WithheldPursuant to 10 CFR 2.390

Response to 6-5

Page 3 of 3

Technical Report

For

Evaluation of Creep of NUHOMS® Basket AluminumComponents under Long Term Storage Conditions

Proprietary Information Withheld per 10 CFR 2.390

Transnu-clear, Inc 7135 Minstrel Way - Suite 300 Columbia Maryland 21045

Enclosure 20 to TN E-28034, Scavuzzo, R.J., Lam, P.C., Gau ...

Documents

Transcript of Enclosure 20 to TN E-28034, Scavuzzo, R.J., Lam, P.C., Gau ...