Emissions to Atmosphere Report No: 5290/M54 Industrial … · Report for the Periodic Monitoring of...

Gypsum Industries LimitedKingscourt, Co Cavan

5290/M54

Emissions to AtmosphereReport No:

Report Date:

Fitz Scientific

Unit 35, Boyne Business Park, Drogheda, Co Louth

Phone: +353 41 98 45440

03/12/2018

Industrial Emissions Licence: P0519-03

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Fitz Scientific

Kingscourt, Co Cavan

Gypsum Industries Limited

Visit No: 2Year: 2018

Report for the Periodic Monitoring of Emissions to Air

Executive Summary

Licence / Permit Number:

Job Quote Number:

P0519-03

Y17Q19107

Operator Name:

Installation:

Phone:

Contact Name:



0 86 836 4510

Conor Dolan

Monitoring Dates:

Monitoring Organisation: Fitz Scientific

Unit 35, Boyne Business Park, Drogheda, Co. Louth, Ireland

Phone: +353 41 98 45440 / Fax: +353 41 98 46171

email: [email protected]

UKAS Registration number 2802

Report Date: 03/12/2018

Signed: ____________________________ Signed: ____________________________

-1

P0519-03Industrial Emissions Licence

Report created using QRSys version

5290/M54

01/11/2018

02/11/2018

Adrian Gaughan

MM14 1287

Level 2

Technician

TE1, TE2, TE3, TE4

Written By:

MCERTS Reg:

Competency:

Function:

Endorsements:

Aadil Khan

MM11 1120

Level 2

Field Services Manager

TE1, TE2, TE3, TE4

Approved By:

MCERTS Reg:

Competency:

Function:

Endorsements:

3.11 October 2018

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Contents

1.- Part 1

1.1.- Monitoring Objectives

1.2.- Special Monitoring Requirements

1.3.- Monitoring Results

1.4.- Operational Information

1.5.- Monitoring Deviations

1.6.- Monitoring Procedures and Deviations

2.- Part 2

Appendix 1: General Information

Appendix 2: Monitoring Information

Fitz Scientific




P0519-03Industrial Emissions Licence5290/M54

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1.- Part 1

1.1.- Monitoring Objectives

The monitoring was carried out as requested by the management of the company above mentioned. The customer has chosen not to sample to the requirements of BS EN 15259:2007 for the substances monitored at the emission points listed below as stated in the Confirmation Form received from the customer.

AE10

Parameter Result

NOx 4.5 mg/m3

O2 20.4 %

Particulates 15.4 mg/m3

Volumetric flow 19366.7 m3/h

AE8

Parameter Result

NOx 70.2 mg/m3

O2 14.1 %

Particulates <0.2 mg/m3


AE9

Parameter Result

NOx 12.5 mg/m3

O2 19.6 %



BE1

Parameter Result

CO 163.4 mg/m3

NOx 42.3 mg/m3

O2 15.21 %



BE4

Parameter Result

NOx 71.4 mg/m3

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1.2.- Special Monitoring Remarks

All the sampling points were obtainable Yes

All parameters were sampled Yes

BE6 not in operation.

Opinions and interpretations expressed in this report are outside the scope of any claimed ISO 17025 accreditation.

Additional information

NOx conversion efficiency: 95.7% tested on 20/08/2018

O2 15.9 %



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1.3.- Monitoring Results

Analysis information

Emission Point

ReferenceSubstance to be Monitored ELV Result

Uncert (+/-) Units

Date of sampling

Start - End

Times Reference Method Accr.velocity

(m/s)LOD

AE10 NOx 4.5 0.47 02/11/2018 08:50-09:20

US EPA CTM-034 No10.42n/a mg/m350 mg/m3

AE10 O2 20.4 0.82 02/11/2018 08:50-09:20

US EPA CTM-034 No10.42n/a %

AE10 Particulates 15.4 5.61 02/11/2018 09:16-09:50

BS EN 13284-1:2017 Yes10.420.1 mg/m320 mg/m3

AE10 Volumetric flow 19366.7 546.1 02/11/2018 09:16-09:50

BS EN 16911-1:2013 MCERTS10.42n/a m3/h25000 m3/h

AE8 NOx 70.2 4.41 01/11/2018 10:15-10:45


AE8 O2 14.1 0.81 01/11/2018 10:15-10:45


AE8 Particulates <0.2 0.01 01/11/2018 10:39-11:09

BS EN 13284-1:2017 Yes9.990.2 mg/m350 mg/m3



AE9 NOx 12.5 0.96 01/11/2018 15:35-16:05


AE9 O2 19.6 0.82 01/11/2018 15:35-16:05


AE9 Particulates <0.2 0.04 01/11/2018 15:58-16:28

BS EN 13284-1:2017 Yes14.690.2 mg/m350 mg/m3



BE1 CO 163.4 51.5 02/11/2018 12:22-12:52

BS EN 15058:2017 Yes12.830.18 mg/m3n/a mg/m3

BE1 NOx 42.3 10.9 02/11/2018 12:22-12:52

BS EN 14792:2017 MCERTS12.830.04 mg/m3130 mg/m3

BE1 O2 15.21 0.24 02/11/2018 12:22-12:52

BS EN 14789:2017 MCERTS12.830.01 %n/a

BE1 Particulates <0.2 0.01 02/11/2018 13:45-14:21

BS EN 13284-1:2017 Yes12.830.2 mg/m3n/a mg/m3

BE1 Volumetric flow 47047.2 1325.8 02/11/2018 13:45-14:21


BE4 NOx 71.4 4.49 01/11/2018 13:40-14:10


BE4 O2 15.9 0.82 01/11/2018 13:40-14:10


BE4 Particulates <2.6 0.6 01/11/2018 14:11-14:41

BS EN 13284-1:2017 Yes3.452.6 mg/m3n/a mg/m3

BE4 Volumetric flow 1036.2 196.5 01/11/2018 14:11-14:41


CO Fitz Scientific

NOx Fitz Scientific

Particulates-blank 0.1 0.05 02/11/2018 08:55-08:57

BS EN 13284-1:2017 Yes0.1 mg/m3AE10

Particulates-blank <0.2 0.01 01/11/2018 10:27-10:29

BS EN 13284-1:2017 Yes0.2 mg/m3AE8


BS EN 13284-1:2017 Yes0.2 mg/m3AE9


BS EN 13284-1:2017 Yes0.2 mg/m3BE1


BS EN 13284-1:2017 Yes2.6 mg/m3BE4

Sampling stage carried out as per MCERTS requirementsNo*:

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O2 Fitz Scientific

Particulates Fitz Scientific

Volumetric flow Fitz Scientific

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Additional information

* The reported uncertainty is based on a standard uncertainty multiplied by a coverage factor k=2, providing a level of confidence of approximately 95%

** Results reported at following Reference Conditions

Reference Conditions

Abatement system and process load

Emission Point Reference Temperature (K) Pressure (KPa) Moisture (%) Oxygen (%)

Monitoring Result Reference Conditions

AE10 273 101.3 no correctionno correction



BE1 273 101.3 no correctionDry

BE4 273 101.3 no correctionno correction

Abatement system In Operation Fuel type and LoadLocation

None n/a As NormalBE4 Natural Gas

None n/a1200 x 12.5 Fire Line

BE1 Natural Gas

None n/a As NormalAE9 Natural Gas



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1.4.- Operating Information

Emission Point Reference Date Process Type

ProcessDuration Substance CEMS PR Units

AE10 02/11/2018 n/a 4.5NOxExpanders Continuous mg/m3

AE10 02/11/2018 n/a 20.4O2Expanders Continuous %

AE10 02/11/2018 n/a 15.4ParticulatesExpanders Continuous mg/m3

AE10 02/11/2018 n/a 19366.7Volumetric flowExpanders Continuous m3/h

AE8 01/11/2018 n/a 70.2NOxKettle Continuous mg/m3

AE8 01/11/2018 n/a 14.1O2Kettle Continuous %

AE8 01/11/2018 n/a <0.2ParticulatesKettle Continuous mg/m3

AE8 01/11/2018 n/a 28660.3Volumetric flowKettle Continuous m3/h

AE9 01/11/2018 n/a 12.5NOxMill Continuous mg/m3

AE9 01/11/2018 n/a 19.6O2Mill Continuous %

AE9 01/11/2018 n/a <0.2ParticulatesMill Continuous mg/m3

AE9 01/11/2018 n/a 19331.9Volumetric flowMill Continuous m3/h

BE1 02/11/2018 n/a 163.4CODryer Exhaust Continuous mg/m3

BE1 02/11/2018 n/a 42.3NOxDryer Exhaust Continuous mg/m3

BE1 02/11/2018 n/a 15.21O2Dryer Exhaust Continuous %

BE1 02/11/2018 n/a <0.2ParticulatesDryer Exhaust Continuous mg/m3

BE1 02/11/2018 n/a 47047.2Volumetric flowDryer Exhaust Continuous m3/h

BE4 01/11/2018 n/a 71.4NOxCalcining Continuous mg/m3

BE4 01/11/2018 n/a 15.9O2Calcining Continuous %

BE4 01/11/2018 n/a <2.6ParticulatesCalcining Continuous mg/m3

BE4 01/11/2018 n/a 1036.2Volumetric flowCalcining Continuous m3/h

* CEMS: Continuous Emission Monitoring System Results

* PR: Periodic Monitoring Results

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1.5.- Monitoring Deviations

Monitoring carried out as per Standard Methods. No deviations were recorded

Isokinetic conditions were outside the requirements of BS EN 13284-1 section 9.5.

Due to the high velocity in the duct a smaller nozzle size was used than required by BS EN 13282-1 section 7.2.3 (8mm) to carry out isokinetic sampling.

Emission monitoring point does not have required number of ports as per AG1 section 2.1/2.2 (per M1 Figure A2.5).

The ELV is such that the LOD for the analysis does not allow for the requirement of >10% ELV to be achieved (for ELV >5 mg/m3).

The ELV is such that the LOD for the analysis does not allow for the requirement of >20% ELV to be achieved (for ELV <5 mg/m3)

Negative flow was found (BS EN 13284-1 Annex D).

The stack flow direction doesn’t meet the minimum requirement of 15 degrees with regard the axis of the stack. (BS EN 13284-1 Annex D).

The ratio of highest to lowest local gas velocity is outside (higher than 3:1) of BS EN 13284-1 Annex D) requirements.

Emission point does not meet the requirements of BS EN 15259:2007 Section 6.2.1 NOTE 4 and AG1 section 2.1/2.2 (per M1 Annex 1) - The measurement plane is not in a section of duct that is at least 5 hydraulic diameters of straight duct upstream of the sampling plane and 2 hydraulic diameters downtream (5 hydraulic diameters from the top of the stack)

Sampling port size is too small for velocity, temperature and pressure measurements to be carried out as per AG1 section 2.1/2.2 (M1 Annex 1).

Differential pressure lower than 5Pa measured with pitot tube (BS EN 13284-1 Annex D).

SO2/NH3 Impinger efficiency is lower than the requirements of 95% total of concentration in the first impinger (BS EN 14791:2017 section 6.6.1)

NOx calibration drift is higher than 2% of the span value. Results are corrected to drift. (BS EN 14792:2017 Section 9.4.3)

The blank reading does not meet the required target of <10% of the daily limit value or 0.5 mg/m3, whichever is the greater (BS EN 13284-1 section 5(g).

AE10Emission Point NOxParameter

NOx overall uncertainty calculated is outside requirement of <10% at the daily ELV, or the lowest limit value assigned by the local authorities, expressed on dry basis before correction to O2 reference concentration as per Section 8 BS EN 14789:2017

CO overall uncertainty calculated is outside requirement of <6% at the daily ELV expressed on dry basis before correction to O2 reference concentration as per 7.3 BS EN 15058:2017.

O2 overall uncertainty calculated is outside requirement of <6% of the value expressed on dry basis, or 0.3% expressed as a volume concentration as per Section 8 BS EN 14789:2017

CO calibration drift is higher than 2% of the span value. Results are corrected to drift. (BS EN 15058:2017 Section 9.4.3)

O2 calibration drift is higher than 2% of the span value. Results are corrected to drift. (EN 14789:2017 Section 9.4.3)

TVOC calibration drift is higher than 2% of the span value. Results are corrected to drift. (BS EN 12619:2013 Section 6.2.3)

HCl Impinger efficiency is lower than the requirements of 95% total of concentration in the first impinger (BS EN 1911:2010 section 5.2.1.2.2)

HF Impinger efficiency is lower than the requirements of 95% total of concentration in the first impinger (BS ISO 15713:2006 section 6.4).

Homogeneity test is required for this stack as per BS EN 15259:2007 but customer did not require it in the Confirmation Form

The measurement values are invalid as the corresponding blank result is greater than the requirement identified in CEN/TS 13649:2014 section 10 (c) (must be <10% of the limit values)

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AE10Emission Point O2Parameter











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AE10Emission Point ParticulatesParameter











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AE10Emission Point Volumetric flowParameter











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BE1Emission Point COParameter











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BE1Emission Point NOxParameter











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BE1Emission Point O2Parameter











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BE1Emission Point ParticulatesParameter











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BE1Emission Point Volumetric flowParameter











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BE4Emission Point NOxParameter











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BE4Emission Point O2Parameter











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Port cap on second port seized.















BE4Emission Point ParticulatesParameter











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BE4Emission Point Volumetric flowParameter











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Licence / Permit Number:

Job Quote Number:

P0519-03

Y17Q19107

Operator Name:

Installation:

Phone:

Contact Name:



Conor Dolan

0 86 836 4510

Monitoring Dates:

Monitoring Organisation: Fitz Scientific


Phone: +353 41 98 45440 / Fax: +353 41 98 46171

email: [email protected]

2.- Part 2

Supporting information

01/11/2018

02/11/2018

Laboratory details

CO

Address Contact email Phone Acc. Number


Geoff Fitzpatrick

[email protected] +353 41 98 45440 - ext 2

UKAS 2802Fitz Scientific

NOx



Geoff Fitzpatrick



O2



Geoff Fitzpatrick



Particulates


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Geoff Fitzpatrick



Volumetric flow



Geoff Fitzpatrick



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Appendix 1:

Sampling personnel used

Substances Monitored

Equipment Checklist References

As an accredited organisation Fitz scientific have implemented procedures to ensure that the requirements of TPS 63 (UKAS Policy on Deviating Samples) are met with regard to samples taken and tested for chemical analysis. As such all samples, when applicable, have been transported in containers, and in an environment, that meet the relevant standard requirements where applicable

Substance Fitz SOPMethod used for Monitoring

CO BS EN 15058:2017 161

NOx BS EN 14792:2017 161

O2 BS EN 14789:2017 161

Particulates BS EN 13284-1:2017 101

Volumetric flow BS EN 16911-1:2013 122

Stack: AE10

n/a

n/a

n/a

n/a

n/a

n/a

n/a n/a

n/a

n/a

n/a

EM214 n/a

n/a

n/a

TCR

Nozzles

Impingers

Probe

Pitot tube

Weights

Caliper Filters

Horiba

FID

FTIR

Testo Gases

Handheld pumps

Tubes

O2Parameter:

EM207

Set1

Set D

Probe2

EM077

EM201 (a

EM389 EM4053/EM4055

n/a

n/a

n/a

n/a n/a

n/a

n/a

TCR

Nozzles

Impingers

Probe

Pitot tube

Weights

Caliper Filters

Horiba

FID

FTIR

Testo Gases

Handheld pumps

Tubes

ParticulatesParameter:

01/11/2018 Technician Name Position Qualification TEs MCERTS no

Adrian Gaughan Team Leader Level 2 TE1, TE2, TE3, TE4

Aadil Khan Team Leader Level 2 TE1, TE2, TE3, TE4

MM14 1287

MM11 1120

02/11/2018 Technician Name Position Qualification TEs MCERTS no

Adrian Gaughan Team Leader Level 2 TE1, TE2, TE3, TE4

Aadil Khan Team Leader Level 2 TE1, TE2, TE3, TE4

MM14 1287

MM11 1120

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EM207

n/a

n/a

Probe2

EM077

n/a

n/a n/a

n/a

n/a

n/a

n/a n/a

n/a

n/a

TCR

Nozzles

Impingers

Probe

Pitot tube

Weights

Caliper Filters

Horiba

FID

FTIR

Testo Gases

Handheld pumps

Tubes

Volumetric flowParameter:

n/a

n/a

n/a

n/a

n/a

n/a

n/a n/a

n/a

n/a

n/a

EM214 n/a

n/a

n/a

TCR

Nozzles

Impingers

Probe

Pitot tube

Weights

Caliper Filters

Horiba

FID

FTIR

Testo Gases

Handheld pumps

Tubes

NOxParameter:

Stack: AE8

n/a

n/a

n/a

n/a

n/a

n/a

n/a n/a

n/a

n/a

n/a

EM214 n/a

n/a

n/a

TCR

Nozzles

Impingers

Probe

Pitot tube

Weights

Caliper Filters

Horiba

FID

FTIR

Testo Gases

Handheld pumps

Tubes

NOxParameter:

n/a

n/a

n/a

n/a

n/a

n/a

n/a n/a

n/a

n/a

n/a

EM214 n/a

n/a

n/a

TCR

Nozzles

Impingers

Probe

Pitot tube

Weights

Caliper Filters

Horiba

FID

FTIR

Testo Gases

Handheld pumps

Tubes

O2Parameter:

EM207

Set1

Set D

Probe2

EM077

EM201 (a

EM389 EM4052/EM4047

n/a

n/a

n/a

n/a n/a

n/a

n/a

TCR

Nozzles

Impingers

Probe

Pitot tube

Weights

Caliper Filters

Horiba

FID

FTIR

Testo Gases

Handheld pumps

Tubes


EM207

n/a

n/a

Probe2

EM077

n/a

n/a n/a

n/a

n/a

n/a

n/a n/a

n/a

n/a

TCR

Nozzles

Impingers

Probe

Pitot tube

Weights

Caliper Filters

Horiba

FID

FTIR

Testo Gases

Handheld pumps

Tubes


Stack: AE9

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Fitz Scientific





EM207

n/a

n/a

Probe2

EM077

n/a

n/a n/a

n/a

n/a

n/a

n/a n/a

n/a

n/a

TCR

Nozzles

Impingers

Probe

Pitot tube

Weights

Caliper Filters

Horiba

FID

FTIR

Testo Gases

Handheld pumps

Tubes


n/a

n/a

n/a

n/a

n/a

n/a

n/a n/a

n/a

n/a

n/a

EM214 n/a

n/a

n/a

TCR

Nozzles

Impingers

Probe

Pitot tube

Weights

Caliper Filters

Horiba

FID

FTIR

Testo Gases

Handheld pumps

Tubes

NOxParameter:

EM207

Set1

Set D

Probe2

EM077

EM201 (a

EM389 EM4048/EM4050

n/a

n/a

n/a

n/a n/a

n/a

n/a

TCR

Nozzles

Impingers

Probe

Pitot tube

Weights

Caliper Filters

Horiba

FID

FTIR

Testo Gases

Handheld pumps

Tubes


n/a

n/a

n/a

n/a

n/a

n/a

n/a n/a

n/a

n/a

n/a

EM214 n/a

n/a

n/a

TCR

Nozzles

Impingers

Probe

Pitot tube

Weights

Caliper Filters

Horiba

FID

FTIR

Testo Gases

Handheld pumps

Tubes

O2Parameter:

Stack: BE1

n/a

n/a

n/a

n/a

n/a

n/a

n/a n/a

EM209

n/a

n/a

n/a DX51LHG

n/a

n/a

TCR

Nozzles

Impingers

Probe

Pitot tube

Weights

Caliper Filters

Horiba

FID

FTIR

Testo Gases

Handheld pumps

Tubes

COParameter:

n/a

n/a

n/a

n/a

n/a

n/a

n/a n/a

EM209

n/a

n/a

n/a DX51LHG

n/a

n/a

TCR

Nozzles

Impingers

Probe

Pitot tube

Weights

Caliper Filters

Horiba

FID

FTIR

Testo Gases

Handheld pumps

Tubes

NOxParameter:

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Fitz Scientific





n/a

n/a

n/a

n/a

n/a

n/a

n/a n/a

EM209

n/a

n/a

n/a n/a

n/a

n/a

TCR

Nozzles

Impingers

Probe

Pitot tube

Weights

Caliper Filters

Horiba

FID

FTIR

Testo Gases

Handheld pumps

Tubes

O2Parameter:

EM207

Set1

Set D

Probe2

EM077

EM201 (a

EM389 EM4056/EM4059

n/a

n/a

n/a

n/a n/a

n/a

n/a

TCR

Nozzles

Impingers

Probe

Pitot tube

Weights

Caliper Filters

Horiba

FID

FTIR

Testo Gases

Handheld pumps

Tubes


EM207

n/a

n/a

Probe2

EM077

n/a

n/a n/a

n/a

n/a

n/a

n/a n/a

n/a

n/a

TCR

Nozzles

Impingers

Probe

Pitot tube

Weights

Caliper Filters

Horiba

FID

FTIR

Testo Gases

Handheld pumps

Tubes


Stack: BE4

EM207

n/a

n/a

Probe2

EM077

n/a

n/a n/a

n/a

n/a

n/a

n/a n/a

n/a

n/a

TCR

Nozzles

Impingers

Probe

Pitot tube

Weights

Caliper Filters

Horiba

FID

FTIR

Testo Gases

Handheld pumps

Tubes


n/a

n/a

n/a

n/a

n/a

n/a

n/a n/a

n/a

n/a

n/a

EM214 n/a

n/a

n/a

TCR

Nozzles

Impingers

Probe

Pitot tube

Weights

Caliper Filters

Horiba

FID

FTIR

Testo Gases

Handheld pumps

Tubes

NOxParameter:

n/a

n/a

n/a

n/a

n/a

n/a

n/a n/a

n/a

n/a

n/a

EM214 n/a

n/a

n/a

TCR

Nozzles

Impingers

Probe

Pitot tube

Weights

Caliper Filters

Horiba

FID

FTIR

Testo Gases

Handheld pumps

Tubes

O2Parameter:

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Fitz Scientific





EM207

Set1

Set D

Probe2

EM077

EM201 (a

EM389 EM4057/EM4051

n/a

n/a

n/a

n/a n/a

n/a

n/a

TCR

Nozzles

Impingers

Probe

Pitot tube

Weights

Caliper Filters

Horiba

FID

FTIR

Testo Gases

Handheld pumps

Tubes


37 of 113

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Fitz Scientific





Appendix 2:

Monitoring Information

2

4

10.42

101.421

63.91

0.9

23872.0

19366.7

19366.7

273

101.3

-0.17

20.4

n/a

Number of Ports

Number of Points

Average Velocity v'a (m/s)

Average Pressure (KPa)

Average Temperature (ºC)

Stack Diameter (m)

Actual Moisture Flow rate (m3/h)

Moisture Flow rate at STP (m3/h)

Dry Flow rate at STP, Ref O2 (m3/h)

T reference (Deg K)

P reference (KPa)

Isokinetic condition (%)

Oxygen measured (%)

Water vapor (%)

Wet Stack (yes/no) No

Probe Temperature (°C) n/a

Impinger efficiency (%) n/a

Size of Nozzle 8

AE10Stack Parameter: Volumetric Flow, Particulates, NOx, O2

Max Flow Rate in Licence (m3/h): 25000

1

6

9.99

99.712

140.71

1.25

44124.1

28660.3

20463.4

273

101.3

-0.94

14.12

n/a

Number of Ports

Number of Points




Stack Diameter (m)




T reference (Deg K)

P reference (KPa)


Oxygen measured (%)

Water vapor (%)

Wet Stack (yes/no) Yes



Size of Nozzle 8



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Fitz Scientific





2

4

14.69

100.167

79.79

0.78

25264.7

19331.9

19022.0

273

101.3

-1.51

19.58

n/a

Number of Ports

Number of Points




Stack Diameter (m)




T reference (Deg K)

P reference (KPa)


Oxygen measured (%)

Water vapor (%)




Size of Nozzle 6



1

12

12.83

100.541

155.35

1.76

112351.9

71068.7

47047.2

273

101.3

-1.59

15.21

33.85

Number of Ports

Number of Points




Stack Diameter (m)




T reference (Deg K)

P reference (KPa)


Oxygen measured (%)

Water vapor (%)

Wet Stack (yes/no) Yes



Size of Nozzle 8

BE1Stack Parameter: Volumetric Flow, Particulates, NOx, O2, CO


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1

4

3.45

99.994

240.57

0.45

1974.7

1036.2

1036.2

273

101.3

9.09

n/a

n/a

Number of Ports

Number of Points




Stack Diameter (m)




T reference (Deg K)

P reference (KPa)


Oxygen measured (%)

Water vapor (%)




Size of Nozzle 4

BE4Stack Parameter: Volumetric Flow, Particulates, NOx, O2


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Diagram of Sampling Location (not to scale)

X

X

X

X X X

X

X

A

B

AE10Circular

2

4

ports

points

Point % of Diameter Location (cm) Velocity (m/s) Temperature (ºC)

Traverse Length 0.9 m

Line

1 6.70 6 9.27 60.391

2 25.00 22.5 10.2 60.451

3 75.00 67.5 9.27 60.551

4 93.30 84 9.98 60.71

1 6.70 6 9.86 60.872

2 25.00 22.5 9.49 60.922

3 75.00 67.5 9.38 60.932

4 93.30 84 9.29 60.942

41 of 113

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X

X X X

A

X

X

AE8Circular

1

6

ports

points



Line

1 4.40 5.5 8.59 138.471

2 14.60 18.3 8.83 138.21

3 29.60 37 8.96 138.141

4 70.40 88 9.52 138.321

5 85.40 106.8 8.55 138.381

6 95.60 119.5 8.72 138.481

42 of 113

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X

X

X

X X X

X

X

A

B

AE9Circular

2

4

ports

points



Line

1 6.70 5.2 13.66 78.541

2 25.00 19.5 14.19 78.561

3 75.00 58.5 13.86 78.581

4 93.30 72.8 13.4 78.671

1 6.70 5.2 13.28 78.72

2 25.00 19.5 13.89 78.652

3 75.00 58.5 14.01 78.562

4 93.30 72.8 13.8 78.412

43 of 113

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X

X X X

A

X

X X

X X X X X

BE1Circular

1

12

ports

points



Line

1 2.10 3.7 13.23 152.771

2 6.70 11.8 13.47 152.91

3 11.80 20.8 13.1 152.831

4 17.70 31.2 13.82 153.261

5 25.00 44 13.31 153.611

6 35.60 62.7 12.88 153.571

7 64.40 113.3 13.15 153.731

8 75.00 132 12.74 154.311

9 82.30 144.8 13.34 154.131

10 88.20 155.2 12.72 154.491

11 93.30 164.2 12.53 154.231

12 97.90 172.3 12.89 154.151

44 of 113

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X

X X X

A

BE4

Circular

1

4

ports

points



Line

1 6.70 3 3.44 238.681

2 25.10 11.3 3.7 238.791

3 75.10 33.8 3.44 238.961

4 93.30 42 3.13 239.051

45 of 113

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Monitoring result calculations and uncertainty calculations

46 of 113

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EPA Export 18-08-2019:03:54:54

Fitz Scientific5290/M54Yar: 2018 Visit no: 2________________________________________________________________________________________________________________________

Gypsum Industries LimitedIndustrial Emissions Licence P0519-03

Volumetric Flowrate Correction Template BS EN 16911-1:2013Company Gypsum Industries Limited Date of Test 02/11/2018Site Kingscourt, Co Cavan Reference No M54Plant Identification BE1 Operator Id MM14 1287Test carried out by Adrian Gaughan TE's TE1, TE2, TE3, TE4

5290/M54

Stack information:

Stack dimensions

m Stack Area m2 No ports / No pointsSuitable ports

(Y/N)?

Comply with 5 Up / 2 Down?

(Y/N) Pressure kPa Temperature K Moisture % Oxygen %

Circular Stack 1.76 2.432849351 1 Yes NoReference Condition 101.3 273 0 15.21

Rectangular stack 0.00 0.00 0.00 12Stack Conditions 100.5 428.4 33.9 15.21

Actual Value: 2.432849351

PointVelocity m/s (v'a)

Temp degC (ta) Temp K Presssure kPa (Pa)

Flow Rate m3/sec:

Actual Flow rate m3/hr

Moisture Flow rate at STP m3/hr Moisture

Flow rate at STP, Dry m3/hr O2 %

Flow Rate at STP, Dry, Ref O2 m3/hr

1 12.83 155.35 428.35 101 31.2 112351.9 71068.7 33.9 47011.6 15.21 47047.2Volumetric flow 12.83 155.35 428.35 100.541 31.2 112351.9 71068.7 33.9 47011.6 15.21 47047.2Uncertainty 155.35 428.35 100.541 3166.0 2002.7 33.9 1324.8 15.21 1325.8

Maximum volumetric flow as per Licence 138600.0 m3/h

Report Number :

Calculation spreadsheet v.5547 of 113

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EPA Export 18-08-2019:03:54:54

Fitz Scientific5290/M54Yar: 2018 Visit no: 2_________________________________________________________________________________________________________________________


v1.4 Oct-16Enter data in orange cells onlyConstantsGas constant 8.314 J/(K.mol)

1990 Pa0.01 Pa

2 % of value0.2 % of range between calibrations

PITOT 0.04 % of rangeSampling probe: Probe2 1.00 Pa

Pitot EM077 Water vapour me 1.14 % relativePitot coefficient, K 0.86 0.61 °C CO content meas 31.52 % relativeExpanded uncertainty (95%, k=2) 0.02 1016.3 Pa CO2 content mea 0.24 % relative

0.50 % O2 content measu 1.57 % relative

Duct dimensions Circular RectangularDiameter 1.76 m a mArea 2.4 m2 b m

Area 0.00 m2Uncertainty (%) 0.500568182 Uncertainty (%) 0.00116889

All Pressures should be entered in Pascals, Pa

Measurement Point Atmospheric Pressure, PaStack Pressure, Pa Static Pressure, Pa meas1, Pa meas2, Pa meas3, Pa meas4, Pa meas5, Pa Delta P, Pa Stack Temperature, C

Water Vapour Content, % CO, ppm CO2, % N2, % O2, % dry molecular wt, g/mol stack molecular wt, g/mol

1 101330 100541 79.744 79.74 155.35 33.85 130.83 3.52261109 81.3 15.21 29.17 25.392 33.85 130.83 3.52261109 81.3 15.21 29.17 25.393 33.85 130.83 3.52261109 81.3 15.21 29.17 25.394 33.85 130.83 3.52261109 81.3 15.21 29.17 25.395 33.85 130.83 3.52261109 81.3 15.21 29.17 25.396 33.85 130.83 3.52261109 81.3 15.21 29.17 25.397 33.85 130.83 3.52261109 81.3 15.21 29.17 25.398 33.85 130.83 3.52261109 81.3 15.21 29.17 25.399 33.85 130.83 3.52261109 81.3 15.21 29.17 25.39

10 33.85 130.83 3.52261109 81.3 15.21 29.17 25.3911 33.85 130.83 3.52261109 81.3 15.21 29.17 25.3912 33.85 130.83 3.52261109 81.3 15.21 29.17 25.3913 33.85 130.83 3.52261109 81.3 15.21 29.17 25.3914 33.85 130.83 3.52261109 81.3 15.21 29.17 25.3915 33.85 130.83 3.52261109 81.3 15.21 29.17 25.3916 33.85 130.83 3.52261109 81.3 15.21 29.17 25.3917 33.85 130.83 3.52261109 81.3 15.21 29.17 25.3918 33.85 130.83 3.52261109 81.3 15.21 29.17 25.3919 33.85 130.83 3.52261109 81.3 15.21 29.17 25.3920 33.85 130.83 3.52261109 81.3 15.21 29.17 25.39

Mean 101330 100541 #DIV/0! 79.74 #DIV/0! #DIV/0! #DIV/0! #DIV/0! 79.74 155.35 33.85 130.8 3.5 81.3 15.2 29.17 25.39

Circular duct Rectangular ductMean velocity 12.83 m/sec Flow rate (stack conditions) 112352 m3/hour 0 m3/hour

Standard uncerta 0.16 m/sec 1.3 % of value Vol. flow rate expanded uncertain 3166 m3/hour #DIV/0! m3/hour

Mean density 0.717 kg/m3 Expanded uncert 0.33 m/sec 2.6 % of value Vol. flow rate expanded uncertain 2.8 % of value #DIV/0! % of value

Developed for the STA by David Butterfield & Chris Dimopoulos, NPL

Uncertainty in duct area measurement

Dry gas basis

Uncertainty in stack gas compositionUncertainty in Delta P transducer Enter uncertainties as (95%,k=2) where relevant

Uncertainty in temperature readout systemUncertainty in atmospheric pressure transducer

Enter uncertainties as (95%,k=2) where relevant

Repeatability of Delta P transducerDrift of Delta P transducerLack of fit of measurement system

Uncertainty calculation for Velocity and Volume Flow Rate Measurement by Pitot tube EN ISO 16911‐1

Characteristics of pressure sensor used for Delta PEnter uncertainties as (95%,k=2) where relevant

Range of Delta P transducerResolution of Delta P transducer


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Fitz Scientific5290/M54Yar: 2018 Visit no: 2_______________________________________________________________________________________________________________________


Velocity associated uncertainties

Pitot Tube CoefficientExpanded uncertainty (95%, k=2) 0.02Standard uncertainty (Dimensionless) 0.01

Table 1

Delta P Standard uncertanites^2 Measurement Point SD of the mean of the DP measurements (Standard uncertainty Delta P)^2 u2(Dpi)Velocity (m/s) Standard uncertainty velocity m/s

Sigma DP See Table 1 1 1.6 2.9 3E‐04 12.8 0.28Resolution uncertainty 0.00 2Calibration uncertainty 0.25 3Lack of fit 0.21 4Drift 5.28 5

67

Molar Mass 8u(H2O) 0.192805119 9(O2)wet 10.1 10u(O2)wet 0.08 11(CO2)wet 2.3 12u(CO2)wet 0.01 13(CO)wet 0.0 14u(CO)wet 0.00 15Oxygen sensitivity 4.00E‐05 16Water sensitivity 1.00E‐04 17CO2 sensitivity 1.60E‐04 18CO sensitivity 4.00E‐08 19

20standard uncertainty 0.000020 kg/mol 0.08 % of value Average 1.59 2.87814365 3E‐04 12.83 0.283002278

Temperaturestandard uncertainty 0.31 K 0.07 % of value

Stack static pressurestandard uncertainty 0.0 Pa #DIV/0! % of value

Stack pressurestandard uncertainty 1016.3 Pa 1.01 % of value

Stack gas densitystandard uncertainty 0.0073 kg/m3 1.02 % of value

Standard uncertainty of velocity 0.16 m/sec 1.3 % of value

Expanded uncertainty in velocity 0.33 m/sec 2.6 % of value


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Volume flow rate associated uncertainties

Circular duct Rectangular ductArea uncertainty 0.01 m2 #DIV/0! m2

Flow rate standard uncertainty 1583 m3/h #DIV/0! m3/h

Volume flow rate expanded uncertainty 3166 m3/h #DIV/0! m3/h

Volume flow rate expanded uncertainty 2.8 % of value #DIV/0! % of value

Calculation spreadsheet v.55 50 of 113

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EPA Export 18-08-2019:03:54:54



Lookup tables

Factor Loading Function

Number of measurments dn2 0.8853 0.5914 0.4865 0.436 0.3957 0.378 0.3519 0.337

10 0.32511 0.31512 0.30715 0.28820 0.26825 0.25430 0.24540 0.22750 0.22260 0.21680 0.206

100 0.199


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EPA Export 18-08-2019:03:54:54



Swirl Test Record BS EN 16911-1:2013Company Gypsum Industries Limited Date of Test 02/11/2018Site Kingscourt, Co Cavan Reference No M54Plant Identification BE1 Operator Id MM14 1287Test carried out by Adrian Gaughan TE's TE1, TE2, TE3, TE4

Sampling Line APoint Distance to duct (cm) Diff. Pressure (Pa) Temp oC Velocity (m/s) Angle of Swirl

1 3.70 86.38 152.77 13.23 <152 11.80 89.55 152.90 13.47 <153 20.80 84.72 152.83 13.10 <154 31.20 94.17 153.26 13.82 <155 44.00 87.22 153.61 13.31 <156 62.70 81.75 153.57 12.88 <157 113.30 85.16 153.73 13.15 <158 132.00 79.75 154.31 12.74 <159 144.80 87.58 154.13 13.34 <15

10 155.20 79.56 154.49 12.72 <1511 164.20 77.18 154.23 12.53 <1512 172.30 81.77 154.15 12.89 <15

Average 84.57 153.67 13.10Min 77.18 152.77 12.53Max 94.17 154.49 13.82

Sampling Line BPoint Distance to duct (cm) Diff. Pressure (Pa) Temp oC Velocity (m/s) Angle of Swirl

123456789

101112

Average #DIV/0! #DIV/0! #DIV/0! #DIV/0!Min 0 0 0 0Max 0 0 0 0


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Moisture Content BS EN 14790:2017Company Gypsum Industries Limited 02/11/2018Site Kingscourt, Co Cavan M54Plant Identification BE1 MM14 1287Test carried out by Adrian Gaughan TE1, TE2, TE3, TE4Report Number : 5290/M54

Dry at Gas Meter: (Vg) 0.55310 m3Gas Meter Temperature: (tg) 24.24000 297.24 K EM No. Volume:orrection Fact Calibration Date:Ambient Pressure Measured:(Pa) 101.33000 kPa EM036 0.5 0.9987 15/03/2018Gas Volume STP (Vgn) 0.508144992 m3 1 1.0007Gas Volume Factor Correction: 0.9873 taken from this table --> 1.5 1.0045Corrected Volume STP 0.501691551 m3 2 1.0133

2.5 1.0185Before EM003 0.5 1.0051 08/05/2017

Readings: Line Impinger 1 Impinger 2 Impinger 3 Impinger 4 Sum: 1 1.01161 442.2 628.5 568.8 384.2 699.1 2722.8 1.5 1.01972 442.2 628.5 568.8 384.2 699.1 2722.8 2 1.02873 442.2 628.5 568.8 384.2 699.1 2722.8 2.5 1.03824 442.2 628.5 568.8 384.2 699.1 2722.8 EM207 0.5 0.9920 09/02/20185 442.2 628.5 568.8 384.2 699.1 2722.8 1 0.98736 442.2 628.5 568.8 384.2 699.1 2722.8 1.5 0.99067 442.2 628.5 568.8 384.2 699.1 2722.8 2 0.99828 442.2 628.5 568.8 384.2 699.1 2722.8 2.5 1.00169 442.2 628.5 568.8 384.2 699.1 2722.8 EM402 0.72 0.9822 09/10/2017

10 442.2 628.5 568.8 384.2 699.1 2722.8 1.44 0.9811Standard Deviation: 0.0 0.0 0.0 0.0 0.0 0.0 2.16 0.9861

Average: 442.2 628.5 568.8 384.2 699.1 2722.8 2.88 0.99193.6 0.9963

After: EM423 0.72 0.9858 15/05/2018Readings: Line Impinger 1 Impinger 2 Impinger 3 Impinger 4 Sum: 1.44 0.9909

1 442.9 759.8 605.3 400.6 720.5 2929.1 2.16 0.99842 442.9 759.8 605.3 400.6 720.5 2929.1 2.88 1.00383 442.9 759.8 605.3 400.6 720.5 2929.1 3.6 1.01614 442.9 759.8 605.3 400.6 720.5 2929.15 442.9 759.8 605.3 400.6 720.5 2929.16 442.9 759.8 605.3 400.6 720.5 2929.17 442.9 759.8 605.3 400.6 720.5 2929.18 442.9 759.8 605.3 400.6 720.5 2929.19 442.9 759.8 605.3 400.6 720.5 2929.1

10 442.9 759.8 605.3 400.6 720.5 2929.1Standard Deviation: 0.0 0.0 0.0 0.0 0.0 0.0

Average: 442.9 759.8 605.3 400.6 720.5 2929.1

Difference in weigh of impingers after and before measurements: 206.3 g

411.21 g/m3

15.21 %15.21 %

33.9 %33.8 %

Weights: Before Sampling: After Sampling: Difference:Silca trap: 699.1 720.5 21.4 g

Efficiency: 97.0 %

Corrected to O2ref:

Referenced oxygen:Meas oxygen:

Water vapour content on STP basis:

Water vapour content in % on wet basis:

Correction Factors for Volume:

TE's

Date of TestReference NoOperator Id

Calculation spreadsheet v.55

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Moisture Uncertainty Calculations

Measured concentration 33.9 % (at STP)

Measured Quantities Symbol Value Standard uncertainty UnitsSampled Volume Vm 0.501691551 uVm 0.001 m3Sampled gas Temperature Tm 428.35 uTm 2 kSampled gas Pressure ρm 100.541 uρm 1 kPaEfficiency Ɛ 97.03 %Oxygen content O2,m 15.21 uO2,m 0.1 % by volumeWater collected in condensation stage 699.10Water collected in adsorption stage 21.4Wate collected in addidional unit 21.40Water collected in trapping m 720.50 um 0.00 gIntermediate calculationsVwc 150.169155 ^2

0.1 0.0 Efficiency uncertain 0.00-0.5 0.3 support 0.00-0.7 0.5 calculations -0.13

√water in trapping unit 26.8

water in adsorption stage 4.6Uncertainty Efficiency^2 0.3Volume ^2 0.7Sensityvity coefficiency 0.6Uncertainty efficiency 0.08

Repatability standard devWeight in the field st 0.0 0.0Sampled Volume 0.002 0.0Sampled gas Temperature 0.02 0.0Sampled gas Pressure 0.3 0.2

Combined measurement uncertainty 0.19 %

Expanded uncertainty as percentage of measured value 1.14 % measured of value expressed with a level of confidence of 95%(Using a coverage factor k=2)

Expanded uncertainty in units of measuremen 0.39 % of water vapour

Overall uncertainty should be less than +/-20% of the measured concentration.


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Flue gases O2 BS EN 14789:2017, NOx BS EN 14792:2017, CO BS EN 15058:2017, CO2 ISO 12039:2001Company Gypsum Industries Limited Date of TestSite Kingscourt, Co Cavan Reference NoPlant Identification BE1 Operator IdTest carried out by Adrian Gaughan TE'sReport Number : 5290/M54

No. O2 % CO2 % CO ppm NOx ppm SO2 ppm1 15.21 3.52 130.83 20.63 -

Flue Gas parameter Concentration UnitRef O2 Value 15.21 % If no correction for oxygen use the same value as for measured oxygen.Meas O2 Value O2 15.21 % Deviation?Uncertainty 0.24 % FALSENOx 20.63 ppmConvert to NO2 mg/Nm3 42.3 Nmg/m3Corrected to ref. O2 % NOx 42.3 Nmg/m3 Deviation?Uncertainty 10.9 Nmg/m3 FALSEMass concentration STP, dry, Ref O2 2.0 kg/hrUncertainty 0.0 kg/hrCO 130.83 ppmConvert to mg/m3 163.5 Nmg/m3Corrected to ref. O2 % CO 163.4 Nmg/m3 Deviation?Uncertainty 51.5 Nmg/m3 #VALUE!Mass concentration STP, dry, Ref O2 7.7 kg/hrUncertainty 0.0 kg/hrCO2Meas CO2 Value CO2 3.5 %Uncertainty 6.9 %

Flow Rate STP,dry,RefO2 47047.17 m3/hr

Calibration Cylinder No: Concentration ppm Concentration mg/m3NO DX51LHG 191.05 391.6525CO DX51LHG 200.3 250.375

Concentration%CO2 DX51LHG 15.01O2 Ambient Air 21Drift Calculations NO ppm CO ppm SO2 ppm O2 % CO2

Sampling time 30 30 30 30Span expected Value 191.05 200.3 21 15.01Zero expected result 0 0 0 0Zero reading before 1 0 0.53 -0.05 0Span reading before measurement 191.73 200.33 21.05 15.013Zero reading before 2 0.4 0.93 -0.07 0.02Zero reading after 0.133 0.967 0.01 0.01Span reading after measurement 192.6 199.5 21.07 14.95

Span adjustment 0.996 1.003 0.995 1.000Span Check 0.993 1.009 0.997 1.005Deviation -0.004 0.006 0.002 0.005Drift/Min -0.000127188 0.00021326 6.3011E-05 0.00016284

Zero adjustment 1 0 -0.5313263 0.04976303 0Zero Adjustment 2 -0.398581338 -0.9323273 0.06966825 -0.019996Zero check 1 -0.132020814 -0.9756066 -0.0099715 -0.0100469Zero Check 2 -0.132020814 -0.9756066 -0.0099715 -0.0100469Deviation 1 0.132020814 0.44428025 0.05973454 0.01004685Deviation 2 -0.266560524 0.04327925 0.07963976 -0.0099491Drift/min 1 0.004400694 0.01480934 0.00199115 0.0003349Drift/min 2 -0.008885351 0.00144264 0.00265466 -0.0003316Drift -0.521088651 0.66138532 0.5682703 0.42224004Actual measured Concentration 20.63 130.83 15.21 3.52Corrected concentration for drift 20.63 130.83 15.21 3.52Deviation FALSE FALSE FALSE FALSE

If the span or zero are higher than 2% of the spanvalue, it is necessary to correct result for zero andspan drifts. The results shal be rejected if the drift

in zero or span gas is higher than 5%

TE1, TE2, TE3, TE4

02/11/2018M54

MM14 1287


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Uncertainty calculation for Gaseous Measurement Oxygen EN14789V2.2 Jul-08

Limit value n/a %vol Calibration gas 21 %volMeasured concentration 15.21 %vol Full Scale 25 %vol

Performance characteristic Value specificationResponse time 56 seconds < 200 sLogger sampling interval 15 seconds 0.00 % volMeasurement period 30 minutes 0.00 % valueNumber of readings in measurement 30 Assuming 1 minute collected over 1 hourRepeatability at zero 0.03 % by volume stdev <0.2 % rangeRepeatability at span level 0.02 % by volume stdev <0.4 % rangeDeviation from linearity 0.1 % vol +/- <0.3 % volumeZero drift (during measurement period) 6.30111E-05 % vol at zero level +/- <2% of volume / 24hrSpan drift (during measurement period) 6.30111E-05 % vol at span level +/- <2% volume/24hr min max value at calibvolume or pressure flow dependence 0.1 % of fs / 10l/h +- 5 l/h <1% range flow 5 15 10 l/hatmospheric pressure dependence 0.19 % of fs/kPa +- 2kPa < 1.5 % range pressure 99.00 101 100 kPaambient temperature dependence -0.21 % by volume /10K +- 15K <0.3% volume 10 K temp 280 285 285 KCO2 (% vol) 15 0.07 % by volume per 15 CO2 range 8 15 0 % volNO (mg/m3) 300 0.02 % by volume per 300 NO range 100 150 0 mg/m3NO2 (mg/m3) 30 0 % by volume per 30 NO2 range 5 7.5 0 mg/m3Combined interference 0.56 % range <2% range Voltage 105 115 110 VDependence on voltage 0.02 % by volume /10V +- 5% < 0.1%vol /10 voltLosses in the line (leak) 0.27 % of value < 2% of valueUncertainty of calibration gas 0.5 % of value

Performance characteristic Uncertainty Value of uncertainty quantity % volStandard deviation of repeatability at zero ur0 for mean Only use rep at spanStandard deviation of repeatability at span level urs for mean 0.00Lack of fit ufit 0.06Drift u0dr 0.00volume or pressure flow dependence uspres 0.01atmospheric pressure dependence uapres 0.03ambient temperature dependence utemp -0.06CO2 0.05 Use largest of sum of all positive or all negative influencesNO 0.01 0.06 all +ves CriteriaNO2 0.00 0 all -ves sum <2% valueCombined interference (from mcerts) 0.08 0.06 largest 0.304114dependence on voltage uvolt 0.01 Value to use for intereference uncertaintylosses in the line (leak) uleak 0.02 unit 0.06Uncertainty of calibration gas ucalib 0.04

Measurement uncertainty 15.21 %volCombined uncertainty 0.12 %vol% of value 0.79 %Coverage factor k = 2Expanded uncertainty expressed with a level of confidence of 95% 1.57 % of valueExpanded uncertainty expressed with a level of confidence of 95% 0.24 % vol

Requirement for SRM is that Uncertaitny should be < 6% of value, on a dry gas basis, or 0.3% expressed as a volume concentration

Effect of drift

range of variation from conditions at calibration


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Uncertainty calculation for Gaseous Measurement NOxv4

Limit value 130 mg.m-3 (corrected) NOGas NO Correction for reference conditionsFull Scale 250 ppm O2, % Moisture, %Pressure, Temperature, K

Measured concentration 20.63 ppm Cal gas conc 191.05 ppm ref 15.21 0.00 101.30 273.00Measured concentration 42.29 mg.m-3 (273K, 101.3kPConversion 2.05 measured 15.21 33.85 100.54 428.35Ratio NO/NO2 5.00 Full Scale 512.5 mg.m-3 (NO2) Factors 1.00 1.51 1.01 1.57

Cal gas conc 391.6525 mg.m-3 (NO2) Correction Factor 2.39

Performance characteristic Value specification Effect of driftResponse time 55 seconds 180.000 -0.05 mg/m3Number of readings in measurement 120 -0.11 % valueRepeatability at zero 0 % full scale 0.200Repeatability at span level 0.1 % full scale 2.000Deviation from linearity 0.75 % of value 2.000 rangesZero drift -0.008885351 % full scale 2.000 min max value at calibSpan drift -0.000127188 % full scale 2.000 flow 0.3 0.5 0.4volume or pressure flow dependence 0.02 % of full scale/kPa 0.033 pressure 101.30 101.5 101.3atmospheric pressure dependence 0.1 % of value/kPa 0.750 temp 283 289 283ambient temperature dependence 0.01 % full scale/10K 0.300 NH3 range 0 0 0NH3 (20 mg/m3) 1.2 mg/m3 CO2 range 0 0.5 0CO2 (15%) 1.2 % by vol H2O range 0 0.5 0H2O (30%) 1.2 % by vol 4.000 Instrument Voltage Rating 110dependence on voltage -0.23 % full scale/10V 2%fs/10V Voltage 104.5 115.5 110converter efficiency 95 % 95%losses in the line (leak) 0.29 % of value 2% of valueUncertainty of calibration gas 2 % of value

Measurement performance related to stationary conditionsPerformance characteristic UncertaintyStandard deviation of repeatability at zero ur0 for mean use rep at spanStandard deviation of repeatability at span level urs for mean 0.01 Use largest negative or positive interferent effectLack of fit ufit 2.22 0 0.00Drift u0dr -0.03 0 0.02volume or pressure flow dependence uspres 0.00 0 0.01atmopsheric pressure dependence uapres 0.06 0 0.03ambient temperature dependence utemp 0.00 Interference uncertainty 0.03NH3 (20 mg/m3) uinterf 0.00CO2 (15%) 0.02H2O (30%) 0.01

Dependence on voltage uvolt -0.07Converter efficiency uceff 0.06losses in the line (leak) uleak 0.07Uncertainty of calibration gas ucalib 0.49

Measurement uncertainty Result 42.29 mg/m3

Combined uncertainty 2.28 mg/m3

Expanded uncertainty k = 2 4.55 mg/m3

Uncertainty corrected to std conds 10.87 mg.m-3 (corrected)Expanded uncertainty expressed with a level of confidence of 95% 8.36 % ELVExpanded uncertainty expressed with a level of confidence of 95% 10.87 mg.m-3 at ELV

Requirement in standard is for uncertainty to be < 10% at ELV, or the lowest limit value assigned by the local authorities, expressed on a dry basis before correction to O2 reference concentration

Value of uncertainty quantity


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Uncertainty calculation for Gaseous Measurement COV2 Jul-08

Limit value n/a mg/m3 (corrected) SOCal gas conc 250.375 mg.m-3 Correction for reference conditionsO2, % Moisture, %Pressure, Temperature, K

Measured concentration 163.54 mg/m3 Full Scale mg/m3 ref 15.21 0.00 101.30 273.00Measured concentration 163.4 mg/m3 (Corrected) measured 15.21 33.85 100.54 428.35

Uncert 0.35 1.00 0.00 1.00Factors 1.00 1.51 1.01 1.57Uncertainty in factor 0.06 0.02 0.00 0.00Correction Factor 2.39 uf 0.07

Performance characteristic Value specification Effect of driftResponse time 57 seconds 180.000 0.01 mg/m3Logger sampling interval 15 seconds 0.01 % valueMeasurement period 30 minutesNumber of readings in measurement 30Repeatability at zero 0.1 % full scale <1 % rangeRepeatability at span level 0.2 % full scale <2 % rangeDeviation from linearity 0.61 % of value <2 % rangeZero drift 0.014809342 % full scale <2% range / 24hr rangesSpan drift 0.000213259 % full scale <2% range/24hr min max value at calibvolume or pressure flow dependence 0.02 % of full scale/3 kPa <2 % / 3 kPa flow 0.3 0.5 0.4 l/hratmospheric pressure dependence 0.22 % of full scale/2 kPa <3% / 2 kPa pressure 100.76 100.92 100.88 kPaambient temperature dependence -0.2 % full scale/10K <3% range / 10 K temp 287 288.5 287.5 K N2O (mg/m3) 40 1.2 mg/m3 N2O range 0 0 0 mg/m3CO2 (% vol) 15 1.2 mg/m3 CO2 range 0 40 0 %volCH4 (mg/m3) 57 1.2 mg/m3 CH4 range 0 57 0 mg/m3H2O (% vol) 30 1.2 mg/m3 H2O range 0 1 0 %voldependence on voltage -0.35 % full scale/10V <2% range Voltage 93 121 110 Vlosses in the line (leak) 0.53 % of value < 0.1%vol /10 voltUncertainty of calibration gas 1.07 % of value < 2% of value

Performance characteristic Uncertainty Value of uncertainty quantityStandard deviation of repeatability at zero ur0 for mean use rep at spanStandard deviation of repeatability at span level urs for mean 0.04Lack of fit ufit 0.00Drift u0dr 0.01volume or pressure flow dependence uspres 0.00atmopsheric pressure dependence uapres 0.00ambient temperature dependence utemp 0.00N2O (mg/m3) uinterf 0.00 Use largest of sum of all positive or all negative influencesCO2 (% vol) uinterf 1.85 2.56 all +ves CriteriaCH4 (mg/m3) uinterf 0.69 0 all -ves sum <4% rangeH2O (% vol) uinterf 0.02 2.56 largest 3.270715Dependence on voltage uvolt 0.00 Value to use for intereference uncertaintylosses in the line (leak) uleak 0.50 unit 2.56Uncertainty of calibration gas ucalib 1.01Uncertianty in factor uf 10.73

Measurement uncertainty 163.41 mg/m3Combined uncertainty 10.78 mg/m3Expanded uncertainty k = 2 21.57 mg/m3

Uncertainty corrected to std conds 51.51 mg/m3Expanded uncertainty expressed with a level of confidence of 95% #VALUE! % ELVExpanded uncertainty expressed with a level of confidence of 95% 51.51 mg.m-3

Expanded uncertainty expressed with a level of confidence of 95% 31.5 % value

Requirement in standard is for uncertainty to be < 10% at ELV at standard conditions


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Uncertainty calculation for Gaseous Measurement CO2V2.2 Jul-08

Limit value n/a %vol Calibration gas 15.01 %volMeasured concentration 3.52 %vol Full Scale 25 %vol

Performance characteristic Value specificationResponse time 60 seconds < 200 sLogger sampling interval 60 seconds 0.00 % volMeasurement period 30 minutes 0.01 % valueNumber of readings in measurement 30 Assuming 1 minute collected over 1 hourRepeatability at zero 0 % by volume stdev <0.2 % rangeRepeatability at span level 0.1 % by volume stdev <0.4 % rangeDeviation from linearity 0.13 % vol +/- <0.3 % volumeZero drift (during measurement period) 0.000334895 % vol at zero level +/- <2% of volume / 24hrSpan drift (during measurement period) 0.000162841 % vol at span level +/- <2% volume/24hr min max value at calibvolume or pressure flow dependence 0 % of fs / 10l/h +- 5 l/h <1% range flow 5 15 10 l/hatmospheric pressure dependence 0.3 % of fs/kPa +- 2kPa < 1.5 % range pressure 99.00 101 100 kPaambient temperature dependence -0.07 % by volume /10K +- 15K <0.3% volume 10 K temp 280 285 285 KCO2 (% vol) 15 0.07 % by volume per 15 CO2 range 8 15 0 % volNO (mg/m3) 300 0.02 % by volume per 300 NO range 100 150 0 mg/m3NO2 (mg/m3) 30 0 % by volume per 30 NO2 range 5 7.5 0 mg/m3Combined interference 0.56 % range <2% range Voltage 105 115 110 VDependence on voltage 0.1 % by volume /10V +- 5% < 0.1%vol /10 voltLosses in the line (leak) 2 % of value < 2% of valueUncertainty of calibration gas 0.5 % of value

Performance characteristic Uncertainty Value of uncertainty quantity % volStandard deviation of repeatability at zero ur0 for mean Only use rep at spanStandard deviation of repeatability at span level urs for mean 0.02Lack of fit ufit 0.08Drift u0dr 0.00volume or pressure flow dependence uspres 0.00atmospheric pressure dependence uapres 0.04ambient temperature dependence utemp -0.02CO2 0.05 Use largest of sum of all positive or all negative influencesNO 0.01 0.06 all +ves CriteriaNO2 0.00 0 all -ves sum <2% valueCombined interference (from mcerts) 0.08 0.06 largest 0.070452dependence on voltage uvolt 0.03 Value to use for intereference uncertaintylosses in the line (leak) uleak 0.04 unit 0.06Uncertainty of calibration gas ucalib 0.01

Measurement uncertainty 3.52 %volCombined uncertainty 0.12 %vol% of value 3.45 %Coverage factor k = 2Expanded uncertainty expressed with a level of confidence of 95% 6.91 % of valueExpanded uncertainty expressed with a level of confidence of 95% 0.24 % vol

Requirement for SRM is that Uncertaitny should be < 6% of value, on a dry gas basis

range of variation from conditions at calibration

Effect of drift


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Date / Time CO (ppm) CO2 (%) NOx (ppm) O2 (%)02/11/2018 12:22 120.60 3.52 21.17 15.3002/11/2018 12:22 122.30 3.54 21.30 15.2402/11/2018 12:22 123.37 3.54 20.97 15.2102/11/2018 12:22 123.93 3.54 20.80 15.1902/11/2018 12:23 127.07 3.52 20.37 15.2002/11/2018 12:23 128.87 3.53 20.20 15.2002/11/2018 12:23 129.13 3.53 20.17 15.1902/11/2018 12:23 128.37 3.53 20.13 15.1702/11/2018 12:24 129.23 3.52 20.13 15.1902/11/2018 12:24 128.27 3.56 20.27 15.1402/11/2018 12:24 129.37 3.54 20.23 15.1602/11/2018 12:24 130.30 3.54 20.37 15.1802/11/2018 12:25 130.87 3.53 20.27 15.1802/11/2018 12:25 131.50 3.54 20.33 15.1602/11/2018 12:25 132.70 3.54 20.30 15.1702/11/2018 12:25 135.20 3.52 20.13 15.2102/11/2018 12:26 136.17 3.52 20.17 15.2102/11/2018 12:26 136.70 3.51 20.10 15.2202/11/2018 12:26 136.87 3.51 20.13 15.2202/11/2018 12:26 138.00 3.51 20.17 15.2202/11/2018 12:27 138.20 3.51 20.33 15.2302/11/2018 12:27 138.10 3.51 20.50 15.2002/11/2018 12:27 138.13 3.50 20.37 15.2302/11/2018 12:27 139.57 3.49 20.37 15.2602/11/2018 12:28 140.77 3.47 20.17 15.2902/11/2018 12:28 139.13 3.51 20.33 15.2302/11/2018 12:28 139.77 3.48 20.37 15.2602/11/2018 12:28 138.77 3.48 20.17 15.2702/11/2018 12:29 139.07 3.48 20.13 15.2702/11/2018 12:29 139.97 3.49 20.07 15.2602/11/2018 12:29 140.03 3.48 19.90 15.2702/11/2018 12:29 140.07 3.47 19.87 15.2802/11/2018 12:30 140.07 3.48 20.00 15.2702/11/2018 12:30 140.80 3.48 19.83 15.2802/11/2018 12:30 139.43 3.49 20.07 15.2502/11/2018 12:30 139.70 3.48 20.00 15.2702/11/2018 12:31 139.73 3.49 20.10 15.2402/11/2018 12:31 139.67 3.49 20.07 15.2702/11/2018 12:31 139.10 3.50 20.17 15.2302/11/2018 12:31 139.53 3.48 20.07 15.2702/11/2018 12:32 139.20 3.49 20.17 15.2602/11/2018 12:32 137.40 3.48 20.10 15.2602/11/2018 12:32 135.77 3.50 20.30 15.2402/11/2018 12:32 134.70 3.50 20.37 15.2402/11/2018 12:33 133.53 3.51 20.43 15.2402/11/2018 12:33 133.47 3.49 20.43 15.2502/11/2018 12:33 132.00 3.52 20.60 15.2102/11/2018 12:33 132.60 3.50 20.47 15.2402/11/2018 12:34 130.93 3.51 20.60 15.2202/11/2018 12:34 131.60 3.52 20.63 15.2202/11/2018 12:34 132.03 3.50 20.57 15.2402/11/2018 12:34 131.03 3.51 20.57 15.2302/11/2018 12:35 130.57 3.53 20.67 15.2002/11/2018 12:35 131.20 3.52 20.70 15.2002/11/2018 12:35 130.90 3.52 20.60 15.2202/11/2018 12:35 130.17 3.50 20.57 15.2302/11/2018 12:36 129.63 3.52 20.63 15.2102/11/2018 12:36 129.37 3.52 20.53 15.2202/11/2018 12:36 128.43 3.52 20.70 15.2002/11/2018 12:36 128.13 3.53 20.77 15.1902/11/2018 12:37 128.30 3.52 20.73 15.2102/11/2018 12:37 129.23 3.52 20.60 15.2102/11/2018 12:37 128.50 3.54 20.83 15.1802/11/2018 12:37 128.97 3.51 21.13 15.2202/11/2018 12:38 129.43 3.51 20.67 15.22


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Date / Time CO (ppm) CO2 (%) NOx (ppm) O2 (%)02/11/2018 12:38 129.20 3.52 20.63 15.2102/11/2018 12:38 129.53 3.51 20.60 15.2202/11/2018 12:38 128.70 3.51 20.63 15.2202/11/2018 12:39 128.53 3.51 20.67 15.2202/11/2018 12:39 128.60 3.52 20.73 15.2102/11/2018 12:39 127.80 3.53 20.83 15.2002/11/2018 12:39 128.37 3.53 20.83 15.2002/11/2018 12:40 127.87 3.53 20.83 15.1902/11/2018 12:40 127.80 3.54 20.87 15.1702/11/2018 12:40 128.73 3.55 21.00 15.1702/11/2018 12:40 127.97 3.55 20.97 15.1602/11/2018 12:41 127.57 3.55 20.90 15.1602/11/2018 12:41 127.83 3.54 20.87 15.1902/11/2018 12:41 127.63 3.54 20.87 15.1802/11/2018 12:41 128.03 3.53 20.80 15.1902/11/2018 12:42 128.63 3.53 20.80 15.2002/11/2018 12:42 128.77 3.55 20.93 15.1802/11/2018 12:42 128.90 3.55 20.90 15.1802/11/2018 12:42 128.50 3.53 20.87 15.2002/11/2018 12:43 128.40 3.52 20.80 15.2102/11/2018 12:43 127.73 3.54 20.97 15.1902/11/2018 12:43 128.93 3.53 20.97 15.1902/11/2018 12:43 129.00 3.53 20.90 15.2002/11/2018 12:44 129.80 3.52 20.80 15.2202/11/2018 12:44 129.37 3.52 20.77 15.2202/11/2018 12:44 128.23 3.54 20.97 15.1802/11/2018 12:44 127.47 3.54 20.90 15.1802/11/2018 12:45 127.07 3.53 20.90 15.1902/11/2018 12:45 127.07 3.53 20.87 15.2002/11/2018 12:45 126.83 3.55 20.97 15.1602/11/2018 12:45 126.77 3.53 21.00 15.1802/11/2018 12:46 127.60 3.54 21.00 15.1802/11/2018 12:46 127.60 3.54 20.93 15.1902/11/2018 12:46 127.23 3.55 20.97 15.1602/11/2018 12:46 127.00 3.55 21.03 15.1602/11/2018 12:47 125.80 3.55 21.07 15.1602/11/2018 12:47 126.00 3.54 21.00 15.1802/11/2018 12:47 127.00 3.54 20.97 15.1902/11/2018 12:47 125.83 3.56 21.20 15.1402/11/2018 12:48 125.73 3.53 21.03 15.1802/11/2018 12:48 125.77 3.55 21.13 15.1602/11/2018 12:48 127.57 3.54 21.07 15.1802/11/2018 12:48 128.20 3.55 21.07 15.1502/11/2018 12:49 127.53 3.54 21.00 15.1802/11/2018 12:49 127.37 3.53 20.97 15.1902/11/2018 12:49 128.17 3.52 20.90 15.2102/11/2018 12:49 128.17 3.53 20.90 15.1902/11/2018 12:50 127.13 3.55 21.03 15.1602/11/2018 12:50 126.73 3.55 21.03 15.1602/11/2018 12:50 127.10 3.55 20.97 15.1702/11/2018 12:50 127.30 3.54 21.03 15.1802/11/2018 12:51 128.30 3.53 20.87 15.1802/11/2018 12:51 127.77 3.54 20.97 15.1802/11/2018 12:51 126.17 3.56 21.00 15.1502/11/2018 12:51 125.23 3.57 21.23 15.12

Average 130.83 3.52 20.63 15.21


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02/11/2018 12:14 02/11/2018 12:21 02/11/2018 12:28 02/11/2018 12:36 02/11/2018 12:43 02/11/2018 12:50 02/11/2018 12:57

BE1 ‐ Raw Flue Gas Results

CO (ppm) CO2 (%) NOx (ppm) O2 (%)


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Particulates BS EN 13284-1:2017Company Gypsum Industries Limited Date of Test 02/11/2018Site Kingscourt, Co Cavan Reference No M54Plant Identification BE1 Operator Id MM14 1287Test carried out by Adrian Gaughan TE's TE1, TE2, TE3, TE4

Report Number: 5290/M54

Particulate ConcentrationsLab Results g Certificate Number: Laboratory: Accreditation status: Analytical Method Date of AnalysisFilter #1 0.00006 0620/800/05 Fitz Scientific ISO 17025 Gravimetry 30/11/2018Rinse 0.00005 0620/800/06 Fitz Scientific ISO 17025Filter Blank 0.00006 0620/800/07 Fitz Scientific ISO 17025Rinse Blank 0.00005 0620/800/08 Fitz Scientific ISO 17025LOD Filter 0.00006 n/aLOD Nozzle Wash 0.00005 n/aTotal Particulate g mg Deviation?LOD 0.00011 0.11 Nozzle 8 FALSERun 0.00011 0.11 Isokinetic Ratio -1.59 FALSEBlank 0.00011 0.11 5 up / 2 down (Y/N?) No TRUE

No of ports 1 TRUERequirements:

Dry at Gas Meter: (Vg) 0.55310 m3 Blank < 10% ELV #VALUE!Gas Meter Temperature: (tg) 24.24000 297.24 K ELV>5mg/m3 --> LOD<10%ELV #VALUE!Ambient Pressure Measured:(Pa) 101.33000 KPa ELV<=5mg/m3 --> LOD<20%ELV FALSEGas Volume STP (Vgn) 0.508144992 m3Gas Volume Factor Correction: 0.98730Corrected Volume STP 0.501691551 m3

Resultsmg/Nm3 @ STP Dry Gas

mg/Nm3 @ STP Dry Gas Ref Oxygen Uncertainty mg/m3 kg/h Uncertainty Kg/h

LOD 0.2 0.2 n/a 0.010 n/aRun 0.2 0.2 0.01 0.010 0.001Blank 0.2 0.2 0.01 0.010 0.001

O2 meas = 15.20569441 %O2 Reference = 15.21 %

Flow Rate as reference conditions 47047.17 m3/hr

Before Blank : After Blank: Before Sample After SampleLeak Test Results: -50 -50 -50 -50 cc/min


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Run CalculationsUncertainty calculation for EN 13284 Determination of low range mass concentration of dust, Manual Gravimetric Methodv14 Measurement EquationLimit value (ELV) n/a mg.m-3 Reference oxygen 15.21 % by volumeMeasured concentration 0.2 mg.m-3 (at reference conditions)

Measured Quantities Symbol Value Standard uncertainty Units Uncertainty as percentage Uncertainty aRequirement of stdSampled Volume Vm 0.501691551 uVm 0.001 m3 0.20 <=2%Sampled gas Temperature Tm 428.35 uTm 2 k 0.47 <=1%Sampled gas Pressure ρm 100.541 uρm 1 kPa 0.99 <=1%Sampled gas Humidity Hm 33.85047071 uHm 1 % by volume 2.95 <=1%Oxygen content O2,m 15.20569441 uO2,m 0.1 % by volume 0.66 <=5%Mass particulate m 0.11 um 0.00 mg 0.00 #VALUE! <5% of limit valueNote - Sampled gas humidity, temperature and pressure are values at the gas meterLeak L -0.597976983 % -0.60 <=2%Uncollected Mass UCM 0 mg 0 <=10%(Instack filter - no rinse)Intermediate calculationsFactor for std conds fs 0.42uncertainty components symbol sensitivity coeff u (in units of fs)

ρm 0.004 0.004Hm 0.006 0.006Tm 0.001 0.002ufs 0.008 1.87

Corrected volume V 0.21 uV 0.004 m3 1.93

Factor for O2 correction fc 1.00uncertainty components symbol sensitivity coeff u

O2,m 0.18 0.018Factor for O2 Correction ufc 1.00 0.018 1.76

Parameter Value Units Sensitivity coeff Uncertainty contribution Uncertainty as %Corrected Volume (standard V 0.21 m3 1.04 0.00 mg.m-3 1.93 %Mass m 0.11 mg 1.99 0.00 mg.m-3 0.00 %Factor for O2 Correction fc 1.00 0.22 0.00 mg.m-3 1.76 %Leak L 0.00 mg.m-3 1.00 0.00 mg.m-3 -0.35 %Uncollected mass UCM 0.00 mg 1.99 0.00 mg.m-3 0.00 %Combined measurement uncertainty 0.01 mg.m-3


Expanded uncertainty in units of measurement 0.01 mg.m-3

Expanded uncertainty as percentage of limit value #VALUE! % ELV


sm fVV

m

refc O

Of

,2

,2

2121

cfVmc

3.101273

100)100( m

m

ms T

Hf


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Blank CalculationsUncertainty calculation for EN 13284 Determination of low range mass concentration of dust, Manual Gravimetric Methodv14

Measurement EquationLimit value (ELV) #VALUE! mg.m-3 Reference oxygen 15.21 % by volumeMeasured concentration 0.2 mg.m-3 (at reference conditions)

Measured Quantities Symbol Value Standard uncertainty Units Uncertainty as percentage Uncertainty aRequirement of stdSampled Volume Vm 0.501691551 uVm 0.001 m3 0.20 <=2%Sampled gas Temperature Tm 428.35 uTm 2 k 0.47 <=1%Sampled gas Pressure ρm 100.541 uρm 1 kPa 0.99 <=1%Sampled gas Humidity Hm 33.85047071 uHm 1 % by volume 2.95 <=1%Oxygen content O2,m 15.20569441 uO2,m 0.1 % by volume 0.66 <=5%Mass particulate m 0.11 um 0.00 mg 0.00 #VALUE! <5% of limit valueNote - Sampled gas humidity, temperature and pressure are values at the gas meterLeak L -0.597976983 % -0.60 <=2%Uncollected Mass UCM 0 mg 0 <=10%(Instack filter - no rinse)Intermediate calculationsFactor for std conds fs 0.42uncertainty components symbol sensitivity coeff u (in units of fs)

ρm 0.004 0.004Hm 0.006 0.006Tm 0.001 0.002ufs 0.008 1.87







Expanded uncertainty as percentage of limit value #VALUE! % ELVNote:

sm fVV

m

refc O

Of

,2

,2

2121

3.101273

100)100( m

m

ms T

Hf

cfVmc


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Volumetric Flowrate Correction Template BS EN 16911-1:2013Company Gypsum Industries Limited Date of Test 01/11/2018Site Kingscourt, Co Cavan Reference No M54Plant Identification BE4 Operator Id MM14 1287Test carried out by Adrian Gaughan TE's TE1, TE2, TE3, TE4

5290/M54

Stack information:

Stack dimensions


(Y/N)?








Flow Rate m3/sec:







Report Number :


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1990 Pa0.01 Pa










1 99690 99994 5.393 5.39 240.57 0.00 0.00 0 84.1 15.94 28.64 28.642 0.00 0.00 0 84.1 15.94 28.64 28.643 0.00 0.00 0 84.1 15.94 28.64 28.644 0.00 0.00 0 84.1 15.94 28.64 28.645 0.00 0.00 0 84.1 15.94 28.64 28.646 0.00 0.00 0 84.1 15.94 28.64 28.647 0.00 0.00 0 84.1 15.94 28.64 28.648 0.00 0.00 0 84.1 15.94 28.64 28.649 0.00 0.00 0 84.1 15.94 28.64 28.64

10 0.00 0.00 0 84.1 15.94 28.64 28.6411 0.00 0.00 0 84.1 15.94 28.64 28.6412 0.00 0.00 0 84.1 15.94 28.64 28.6413 0.00 0.00 0 84.1 15.94 28.64 28.6414 0.00 0.00 0 84.1 15.94 28.64 28.6415 0.00 0.00 0 84.1 15.94 28.64 28.6416 0.00 0.00 0 84.1 15.94 28.64 28.6417 0.00 0.00 0 84.1 15.94 28.64 28.6418 0.00 0.00 0 84.1 15.94 28.64 28.6419 0.00 0.00 0 84.1 15.94 28.64 28.6420 0.00 0.00 0 84.1 15.94 28.64 28.64











Dry gas basis





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Table 1


Sigma DP See Table 1 1 0.1 2.3 0.047 3.4 0.75Resolution uncertainty 0.00 2Calibration uncertainty 0.02 3Lack of fit 0.21 4Drift 5.28 5

67

Molar Mass 8u(H2O) 0 9(O2)wet 15.9 10u(O2)wet 0.00 11(CO2)wet 0.0 12u(CO2)wet 0.00 13(CO)wet 0.0 14u(CO)wet 0.00 15Oxygen sensitivity 4.00E‐05 16Water sensitivity 1.00E‐04 17CO2 sensitivity 1.60E‐04 18CO sensitivity 4.00E‐08 19

20standard uncertainty 0.000000 kg/mol 0.00 % of value Average 0.11 2.34927667 0.047 3.45 0.752461766








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Lookup tables



10 0.32511 0.31512 0.30715 0.28820 0.26825 0.25430 0.24540 0.22750 0.22260 0.21680 0.206

100 0.199


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Swirl Test Record BS EN 16911-1:2013Company Gypsum Industries Limited Date of Test 01/11/2018Site Kingscourt, Co Cavan Reference No M54Plant Identification BE4 Operator Id MM14 1287Test carried out by Adrian Gaughan TE's TE1, TE2, TE3, TE4

Sampling Line APoint Distance to duct (m) Diff. Pressure (Pa) Temp oC Velocity (m/s) Angle of Swirl

1 3.0 5.84 238.68 3.44 <152 11.3 6.74 238.79 3.70 <153 33.8 5.82 238.96 3.44 <154 42.0 4.83 239.05 3.13 <1556789

101112

Average 5.81 238.87 3.43Min 4.83 238.68 3.13Max 6.74 239.05 3.70

Sampling Line BPoint Distance to duct (m) Diff. Pressure (Pa) Temp oC Velocity (m/s) Angle of Swirl

123456789

101112



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Moisture Content BS EN 14790:2017Company Gypsum Industries Limited 01/11/2018Site Kingscourt, Co Cavan M54Plant Identification BE4 MM14 1287Test carried out by Adrian Gaughan TE1, TE2, TE3, TE4Report Number : 5290/M54


2.5 1.0185Before EM003 0.5 1.0051 08/05/2017



Average: 443.0 626.9 567.0 385.0 698.5 2720.4 2.88 0.99193.6 0.9963


1 442.8 626.8 567.1 384.7 699.0 2720.4 2.16 0.99842 442.8 626.8 567.1 384.7 699.0 2720.4 2.88 1.00383 442.8 626.8 567.1 384.7 699.0 2720.4 3.6 1.01614 442.8 626.8 567.1 384.7 699.0 2720.45 442.8 626.8 567.1 384.7 699.0 2720.46 442.8 626.8 567.1 384.7 699.0 2720.47 442.8 626.8 567.1 384.7 699.0 2720.48 442.8 626.8 567.1 384.7 699.0 2720.49 442.8 626.8 567.1 384.7 699.0 2720.4


Average: 442.8 626.8 567.1 384.7 699.0 2720.4


0.00 g/m3

15.94 %15.94 %

0.0 %0.0 %


Efficiency: 99.9 %


TE's


Corrected to O2ref:





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0.0 0.0 Efficiency uncertain 0.000.0 0.0 support 0.00

-1.1 1.2 calculations -0.14√

water in trapping unit 26.4water in adsorption stage 0.7

Uncertainty Efficiency^2 0.1Volume ^2 0.2Sensityvity coefficiency 0.2Uncertainty efficiency 0.01



Expanded uncertainty as percentage of measured value #DIV/0! % measured of value expressed with a level of confidence of 95%(Using a coverage factor k=2)




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Particulates BS EN 13284-1:2017Company Gypsum Industries Limited Date of Test 01/11/2018Site Kingscourt, Co Cavan Reference No M54Plant Identification BE4 Operator Id MM14 1287Test carried out by Adrian Gaughan TE's TE1, TE2, TE3, TE4


Particulate ConcentrationsLab Results g Certificate Number: Laboratory: Accreditation status: Analytical Method Date of AnalysisFilter #1 0.00006 0620/800/13 Fitz Scientific ISO 17025 Gravimetry 30/11/2018Rinse 0.00005 0620/800/14 Fitz Scientific ISO 17025Filter Blank 0.00006 0620/800/15 Fitz Scientific ISO 17025Rinse Blank 0.00005 0620/800/16 Fitz Scientific ISO 17025LOD Filter 0.00006 n/aLOD Nozzle Wash 0.00005 n/aTotal Particulate g mg Deviation?LOD 0.00011 0.11 Nozzle 4 TRUERun 0.00011 0.11 Isokinetic Ratio 9.09 FALSEBlank 0.00011 0.11 5 up / 2 down (Y/N?) No TRUE


Dry at Gas Meter: (Vg) 0.04800 m3 Blank < 10% ELV #VALUE!Gas Meter Temperature: (tg) 26.94000 299.94 K ELV>5mg/m3 --> LOD<10%ELV #VALUE!Ambient Pressure Measured:(Pa) 99.69000 KPa ELV<=5mg/m3 --> LOD<20%ELV FALSEGas Volume STP (Vgn) 0.042994376 m3Gas Volume Factor Correction: 0.99200Corrected Volume STP 0.042650421 m3






Before Blank : After Blank: Before Sample After SampleLeak Test Results: 50 50 -50 -50 cc/min


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Run CalculationsUncertainty calculation for EN 13284 Determination of low range mass concentration of dust, Manual Gravimetric Methodv14 Measurement EquationLimit value (ELV) n/a mg.m-3 Reference oxygen 15.94 % by volumeMeasured concentration 2.6 mg.m-3 (at reference conditions)

Measured Quantities Symbol Value Standard uncertainty Units Uncertainty as percentage Uncertainty aRequirement of stdSampled Volume Vm 0.042650421 uVm 0.001 m3 2.34 <=2%Sampled gas Temperature Tm 513.57 uTm 2 k 0.39 <=1%Sampled gas Pressure ρm 99.994 uρm 1 kPa 1.00 <=1%Sampled gas Humidity Hm 0 uHm 1 % by volume 1.00 <=1%Oxygen content O2,m 15.94 uO2,m 0.1 % by volume 0.63 <=5%Mass particulate m 0.11 um 0.00 mg 0.00 #VALUE! <5% of limit valueNote - Sampled gas humidity, temperature and pressure are values at the gas meterLeak L -7.033928261 % -7.03 <=2%Uncollected Mass UCM 0 mg 0 <=10%(Instack filter - no rinse)Intermediate calculationsFactor for std conds fs 0.52uncertainty components symbol sensitivity coeff u (in units of fs)

ρm 0.005 0.005Hm 0.005 0.005Tm 0.001 0.002ufs 0.008 1.47




Parameter Value Units Sensitivity coeff Uncertainty contribution Uncertainty as %Corrected Volume (standard V 0.02 m3 115.24 0.12 mg.m-3 4.70 %Mass m 0.11 mg 23.45 0.00 mg.m-3 0.00 %Factor for O2 Correction fc 1.00 2.58 0.05 mg.m-3 2.02 %Leak L -0.10 mg.m-3 1.00 -0.10 mg.m-3 -4.06 %Uncollected mass UCM 0.00 mg 23.45 0.00 mg.m-3 0.00 %Combined measurement uncertainty 0.17 mg.m-3



Expanded uncertainty as percentage of limit value #VALUE! % ELV


sm fVV

m

refc O

Of

,2

,2

2121

cfVmc

3.101273

100)100( m

m

ms T

Hf


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Measurement EquationLimit value (ELV) #VALUE! mg.m-3 Reference oxygen 15.94 % by volumeMeasured concentration 2.6 mg.m-3 (at reference conditions)

Measured Quantities Symbol Value Standard uncertainty Units Uncertainty as percentage Uncertainty aRequirement of stdSampled Volume Vm 0.042650421 uVm 0.001 m3 2.34 <=2%Sampled gas Temperature Tm 513.57 uTm 2 k 0.39 <=1%Sampled gas Pressure ρm 99.994 uρm 1 kPa 1.00 <=1%Sampled gas Humidity Hm 0 uHm 1 % by volume 1.00 <=1%Oxygen content O2,m 15.94 uO2,m 0.1 % by volume 0.63 <=5%Mass particulate m 0.11 um 0.00 mg 0.00 #VALUE! <5% of limit valueNote - Sampled gas humidity, temperature and pressure are values at the gas meterLeak L 7.033928261 % 7.03 <=2%Uncollected Mass UCM 0 mg 0 <=10%(Instack filter - no rinse)Intermediate calculationsFactor for std conds fs 0.52uncertainty components symbol sensitivity coeff u (in units of fs)

ρm 0.005 0.005Hm 0.005 0.005Tm 0.001 0.002ufs 0.008 1.47




Parameter Value Units Sensitivity coeff Uncertainty contribution Uncertainty as %Corrected Volume (standard V 0.02 m3 115.24 0.12 mg.m-3 4.70 %Mass m 0.11 mg 23.45 0.00 mg.m-3 0.00 %Factor for O2 Correction fc 1.00 2.58 0.05 mg.m-3 2.02 %Leak L 0.10 mg.m-3 1.00 0.10 mg.m-3 4.06 %Uncollected mass UCM 0.00 mg 23.45 0.00 mg.m-3 0.00 %Combined measurement uncertainty 0.17 mg.m-3



Expanded uncertainty as percentage of limit value #VALUE! % ELVNote:

sm fVV

m

refc O

Of

,2

,2

2121

3.101273

100)100( m

m

ms T

Hf

cfVmc


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Flue Gases O2 US EPA CTM-034, NOx US EPA CTM-034, CO US EPA CTM-034, SO2 US EPA CTM-6cCompany Gypsum Industries Limited Date of TestSite Kingscourt, Co Cavan Reference NoPlant Identification BE4 Operator IdTest carried out by Adrian Gaughan TE'sReport Number : 5290/M54

No. Temp oC O2 % CO2 % CO ppm NO ppm NO2 ppm NOx ppm SO2 ppm1 240.57 16 2.84 3 352 15.96 2.85 2 353 15.99 2.85 3 354 15.97 2.85 3 355 15.94 2.85 3 356 15.96 2.85 3 347 15.95 2.86 3 348 15.97 2.87 2 349 15.95 2.87 2 34

10 15.94 2.85 3 3411 15.95 2.86 3 3412 15.93 2.87 2 3413 15.92 2.87 2 3514 15.93 2.88 2 3515 15.92 2.88 3 3516 15.91 2.89 2 3617 15.93 2.87 2 3518 15.94 2.88 2 3519 15.9 2.87 3 3520 15.91 2.89 3 3521 15.91 2.87 2 3522 15.93 2.88 3 3523 15.92 2.88 2 3524 15.91 2.89 2 3525 15.89 2.89 3 3526 15.93 2.87 2 3627 15.92 2.88 2 3528 15.93 2.89 3 3529 15.94 2.87 3 3630 15.93 2.87 3 35

Flue Gas parameter Concentration UnitRef O2 Value 15.94 % If no correction for oxygen use the same value as for measured oxygen.

Meas O2 Value 15.94 %

Temperature 240.57 oC

NOx 34.87 ppmNO #DIV/0! ppmConvert to NO2 mg/Nm3 71.5 Nmg/m3Corrected to ref. O2 % 71.4 Nmg/m3Mass concentration STP, dry, Ref O2 0.1 kg/hr

CO 2.53 ppmConvert to mg/m3 3.2 Nmg/m3Corrected to ref. O2 % 3.2 Nmg/m3Mass concentration STP, dry, Ref O2 0.0 kg/hr

SO2 #DIV/0! ppmConvert to mg/Nm3 #DIV/0! Nmg/m3Corrected to ref. O2 % #DIV/0! Nmg/m3Mass concentration STP, dry, Ref O2 #DIV/0! kg/hrCO2Meas CO2 Value 2.869666667 %


Value Unit Value Unit Value UnitOxygen 0.1 % 0.82 %CO ppm 6 % 1.15 ppm 1.44 mg/m3

NO2 ppm 6 % 2.19 ppm 4.49 mg/m3SO2 ppm 6 % #DIV/0! ppm #DIV/0! mg/m3NO ppm 6 % 3.09 ppm 4.14 mg/m3

Temp 0.3 DegCPressure 0.3 hPa

Note: Overall uncertainty values taken from calibaration certificate dated 09/10/2018

The overall uncertainty of the measurements was estimated not to exceed:

01/11/2018M54

MM14 1287TE1, TE2, TE3, TE4


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EPA Export 18-08-2019:03:54:54



Volumetric Flowrate Correction Template BS EN 16911-1:2013Company Gypsum Industries Limited Date of Test 01/11/2018Site Kingscourt, Co Cavan Reference No M54Plant Identification AE8 Operator Id MM14 1287Test carried out by Adrian Gaughan TE's TE1, TE2, TE3, TE4

5290/M54

Stack information:

Stack dimensions


(Y/N)?



Circular Stack 1.25 1.22718463 1 Yes NoReference Condition 101.3 273 28.6 14.12





Flow Rate m3/sec:







Report Number :


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1990 Pa0.01 Pa










1 99330 99712 49.937 49.94 140.71 28.60 0.00 0 85.9 14.12 28.56 25.542 28.60 0.00 0 85.9 14.12 28.56 25.543 28.60 0.00 0 85.9 14.12 28.56 25.544 28.60 0.00 0 85.9 14.12 28.56 25.545 28.60 0.00 0 85.9 14.12 28.56 25.546 28.60 0.00 0 85.9 14.12 28.56 25.547 28.60 0.00 0 85.9 14.12 28.56 25.548 28.60 0.00 0 85.9 14.12 28.56 25.549 28.60 0.00 0 85.9 14.12 28.56 25.54

10 28.60 0.00 0 85.9 14.12 28.56 25.5411 28.60 0.00 0 85.9 14.12 28.56 25.5412 28.60 0.00 0 85.9 14.12 28.56 25.5413 28.60 0.00 0 85.9 14.12 28.56 25.5414 28.60 0.00 0 85.9 14.12 28.56 25.5415 28.60 0.00 0 85.9 14.12 28.56 25.5416 28.60 0.00 0 85.9 14.12 28.56 25.5417 28.60 0.00 0 85.9 14.12 28.56 25.5418 28.60 0.00 0 85.9 14.12 28.56 25.5419 28.60 0.00 0 85.9 14.12 28.56 25.5420 28.60 0.00 0 85.9 14.12 28.56 25.54







Dry gas basis









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Table 1



67










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Lookup tables



10 0.32511 0.31512 0.30715 0.28820 0.26825 0.25430 0.24540 0.22750 0.22260 0.21680 0.206

100 0.199


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EPA Export 18-08-2019:03:54:54



Swirl Test Record BS EN 16911-1:2013Company Gypsum Industries Limited Date of Test 01/11/2018Site Kingscourt, Co Cavan Reference No M54Plant Identification AE8 Operator Id MM14 1287Test carried out by Adrian Gaughan TE's TE1, TE2, TE3, TE4

Sampling Line APoint Distance to duct (m) Diff. Pressure (Pa) Temp oC Velocity (m/s) Angle of Swirl

1 5.5 45.12 138.47 8.59 <152 18.3 47.70 138.20 8.83 <153 37 49.08 138.14 8.96 <154 88 55.07 138.32 9.52 <155 106.8 44.67 138.38 8.55 <156 119.5 46.02 138.48 8.72 <15789

101112

Average 47.94 138.33 8.86Min 44.67 138.14 8.55Max 55.07 138.48 9.52

Sampling Line BPoint Distance to duct (m) Diff. Pressure (Pa) Temp oC Velocity (m/s) Angle of Swirl

123456789

101112



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EPA Export 18-08-2019:03:54:54



Moisture Content BS EN 14790:2017Company Gypsum Industries Limited 01/11/2018Site Kingscourt, Co Cavan M54Plant Identification AE8 MM14 1287Test carried out by Adrian Gaughan TE1, TE2, TE3, TE4Report Number : 5290/M54


2.5 1.0185Before EM003 0.5 1.0051 08/05/2017



Average: 442.9 481.0 558.6 375.1 694.2 2551.8 2.88 0.99193.6 0.9963


1 443.0 626.9 567.0 385.0 698.5 2720.4 2.16 0.99842 443.0 626.9 567.0 385.0 698.5 2720.4 2.88 1.00383 443.0 626.9 567.0 385.0 698.5 2720.4 3.6 1.01614 443.0 626.9 567.0 385.0 698.5 2720.45 443.0 626.9 567.0 385.0 698.5 2720.46 443.0 626.9 567.0 385.0 698.5 2720.47 443.0 626.9 567.0 385.0 698.5 2720.48 443.0 626.9 567.0 385.0 698.5 2720.49 443.0 626.9 567.0 385.0 698.5 2720.4


Average: 443.0 626.9 567.0 385.0 698.5 2720.4


321.83 g/m3

14.12 %14.12 %

28.6 %28.6 %


Efficiency: 99.4 %

Corrected to O2ref:





TE's



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Particulates BS EN 13284-1:2017Company Gypsum Industries Limited Date of Test 01/11/2018Site Kingscourt, Co Cavan Reference No M54Plant Identification AE8 Operator Id MM14 1287Test carried out by Adrian Gaughan TE's TE1, TE2, TE3, TE4




Dry at Gas Meter: (Vg) 0.5626 m3 Blank < 10% ELV FALSEGas Meter Temperature: (tg) 12.18 285.18 K ELV>5mg/m3 --> LOD<10%ELV FALSEAmbient Pressure Measured:(Pa) 99.33 KPa ELV<=5mg/m3 --> LOD<20%ELV FALSEGas Volume STP (Vgn) 0.52809773 m3Gas Volume Factor Correction: 0.99200Corrected Volume STP 0.523872948 m3






Before Blank : After Blank: Before Sample After SampleLeak Test Results: -50 -50 0 0 cc/min


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Run CalculationsUncertainty calculation for EN 13284 Determination of low range mass concentration of dust, Manual Gravimetric Methodv14 Measurement EquationLimit value (ELV) 50 mg.m-3 Reference oxygen 14.12 % by volumeMeasured concentration 0.2 mg.m-3 (at reference conditions)

Measured Quantities Symbol Value Standard uncertainty Units Uncertainty as percentage Uncertainty aRequirement of stdSampled Volume Vm 0.523872948 uVm 0.001 m3 0.19 <=2%Sampled gas Temperature Tm 413.71 uTm 2 k 0.48 <=1%Sampled gas Pressure ρm 99.712 uρm 1 kPa 1.00 <=1%Sampled gas Humidity Hm 28.59714551 uHm 1 % by volume 3.50 <=1%Oxygen content O2,m 14.12 uO2,m 0.1 % by volume 0.71 <=5%Mass particulate m 0.11 um 0.00 mg 0.00 0.00 <5% of limit valueNote - Sampled gas humidity, temperature and pressure are values at the gas meterLeak L 0 % 0.00 <=2%Uncollected Mass UCM 0 mg 0 <=10%(Instack filter - no rinse)Intermediate calculationsFactor for std conds fs 0.46uncertainty components symbol sensitivity coeff u (in units of fs)

ρm 0.005 0.005Hm 0.006 0.006Tm 0.001 0.002ufs 0.008 1.79







Expanded uncertainty as percentage of limit value 0.0 % ELV


sm fVV

m

refc O

Of

,2

,2

2121

cfVmc

3.101273

100)100( m

m

ms T

Hf


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EPA Export 18-08-2019:03:54:54




Measurement EquationLimit value (ELV) 5 mg.m-3 Reference oxygen 14.12 % by volumeMeasured concentration 0.2 mg.m-3 (at reference conditions)

Measured Quantities Symbol Value Standard uncertainty Units Uncertainty as percentage Uncertainty aRequirement of stdSampled Volume Vm 0.523872948 uVm 0.001 m3 0.19 <=2%Sampled gas Temperature Tm 413.71 uTm 2 k 0.48 <=1%Sampled gas Pressure ρm 99.712 uρm 1 kPa 1.00 <=1%Sampled gas Humidity Hm 28.59714551 uHm 1 % by volume 3.50 <=1%Oxygen content O2,m 14.12 uO2,m 0.1 % by volume 0.71 <=5%Mass particulate m 0.11 um 0.00 mg 0.00 0.00 <5% of limit valueNote - Sampled gas humidity, temperature and pressure are values at the gas meterLeak L -0.572657934 % -0.57 <=2%Uncollected Mass UCM 0 mg 0 <=10%(Instack filter - no rinse)Intermediate calculationsFactor for std conds fs 0.46uncertainty components symbol sensitivity coeff u (in units of fs)

ρm 0.005 0.005Hm 0.006 0.006Tm 0.001 0.002ufs 0.008 1.79







Expanded uncertainty as percentage of limit value 0.2 % ELVNote:

sm fVV

m

refc O

Of

,2

,2

2121

3.101273

100)100( m

m

ms T

Hf

cfVmc


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Flue Gases O2 US EPA CTM-034, NOx US EPA CTM-034, CO US EPA CTM-034, SO2 US EPA CTM-6cCompany Gypsum Industries Limited Date of TestSite Kingscourt, Co Cavan Reference NoPlant Identification AE8 Operator IdTest carried out by Adrian Gaughan TE'sReport Number : 5290/M54

No. Temp oC O2 % CO2 % CO ppm NO ppm NO2 ppm NOx ppm SO2 ppm1 140.71 14.22 3.85 85 332 140.71 14.19 3.89 76 343 140.71 14.11 3.91 90 344 140.71 14.1 3.9 81 345 140.71 14.09 3.91 92 356 140.71 14.05 3.95 99 357 140.71 14.09 3.92 87 348 140.71 14.04 3.94 91 349 140.71 14.06 3.91 77 34

10 140.71 14.07 3.92 76 3411 140.71 14.08 3.93 80 3412 140.71 14.08 3.93 103 3513 140.71 14.09 3.91 98 3414 140.71 14.1 3.92 81 3415 140.71 14.12 3.9 78 3516 140.71 14.14 3.89 83 3417 140.71 14.13 3.9 87 3418 140.71 14.15 3.88 74 3419 140.71 14.16 3.9 77 3420 140.71 14.14 3.89 81 3521 140.71 14.15 3.88 90 3422 140.71 14.13 3.9 96 3523 140.71 14.09 3.9 90 3424 140.71 14.16 3.87 80 3425 140.71 14.17 3.86 82 3426 140.71 14.16 3.89 92 3427 140.71 14.15 3.87 90 3428 140.71 14.16 3.87 75 3429 140.71 14.19 3.87 80 3430 140.71 14.15 3.88 81 35













01/11/2018M54

MM14 1287TE1, TE2, TE3, TE4


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5290/M54

Stack information:

Stack dimensions


(Y/N)?



Circular Stack 0.78 0.477836243 2 Yes NoReference Condition 101.3 273 1.6 19.58





Flow Rate m3/sec:







Report Number :


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1990 Pa0.01 Pa










1 10006 100167 142.740 142.74 79.79 1.60 0.00 0 79.1 20.90 28.84 28.662 1.60 0.00 0 79.1 20.90 28.84 28.663 1.60 0.00 0 79.1 20.90 28.84 28.664 1.60 0.00 0 79.1 20.90 28.84 28.665 1.60 0.00 0 79.1 20.90 28.84 28.666 1.60 0.00 0 79.1 20.90 28.84 28.667 1.60 0.00 0 79.1 20.90 28.84 28.668 1.60 0.00 0 79.1 20.90 28.84 28.669 1.60 0.00 0 79.1 20.90 28.84 28.66

10 1.60 0.00 0 79.1 20.90 28.84 28.6611 1.60 0.00 0 79.1 20.90 28.84 28.6612 1.60 0.00 0 79.1 20.90 28.84 28.6613 1.60 0.00 0 79.1 20.90 28.84 28.6614 1.60 0.00 0 79.1 20.90 28.84 28.6615 1.60 0.00 0 79.1 20.90 28.84 28.6616 1.60 0.00 0 79.1 20.90 28.84 28.6617 1.60 0.00 0 79.1 20.90 28.84 28.6618 1.60 0.00 0 79.1 20.90 28.84 28.6619 1.60 0.00 0 79.1 20.90 28.84 28.6620 1.60 0.00 0 79.1 20.90 28.84 28.66











Dry gas basis





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Table 1



67










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EPA Export 18-08-2019:03:54:54



Lookup tables



10 0.32511 0.31512 0.30715 0.28820 0.26825 0.25430 0.24540 0.22750 0.22260 0.21680 0.206

100 0.199


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1 5.20 130.29 78.54 13.66 <152 19.50 140.54 78.56 14.19 <153 58.50 134.01 78.58 13.86 <154 72.80 125.39 78.67 13.40 <1556789

101112

Average 132.56 78.59 13.78Min 125.39 78.54 13.40Max 140.54 78.67 14.19


1 5.20 123.13 78.70 13.28 <152 19.50 134.57 78.65 13.89 <153 58.50 137.07 78.56 14.01 <154 72.80 133.01 78.41 13.80 <1556789

101112

Average 131.95 78.58 13.75Min 123.13 78.41 13.28Max 137.07 78.70 14.01


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2.5 1.0185Before EM003 0.5 1.0051 08/05/2017



Average: 442.8 626.8 567.1 384.7 699.0 2720.4 2.88 0.99193.6 0.9963


1 443.1 631.4 568.6 384.9 699.5 2727.5 2.16 0.99842 443.1 631.4 568.6 384.9 699.5 2727.5 2.88 1.00383 443.1 631.4 568.6 384.9 699.5 2727.5 3.6 1.01614 443.1 631.4 568.6 384.9 699.5 2727.55 443.1 631.4 568.6 384.9 699.5 2727.56 443.1 631.4 568.6 384.9 699.5 2727.57 443.1 631.4 568.6 384.9 699.5 2727.58 443.1 631.4 568.6 384.9 699.5 2727.59 443.1 631.4 568.6 384.9 699.5 2727.5


Average: 443.1 631.4 568.6 384.9 699.5 2727.5


13.09 g/m3

19.58 %19.58 %

1.6 %1.6 %


Efficiency: 99.9 %


TE's


Corrected to O2ref:





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EPA Export 18-08-2019:03:54:54





Particulate ConcentrationsLab Results g Certificate Number: Laboratory: Accreditation status: Analytical Method Date of AnalysisFilter #1 0.00006 0620/800/17 Fitz Scientific ISO 17025 Gravimetry 30/11/2018Rinse 0.00005 0620/800/18 Fitz Scientific ISO 17025Filter Blank 0.00006 0620/800/19 Fitz Scientific ISO 17025Rinse Blank 0.00005 0620/800/20 Fitz Scientific ISO 17025LOD Filter 0.00006 n/aLOD Nozzle Wash 0.00005 n/aTotal Particulate g mg Deviation?LOD 0.00011 0.11 Nozzle 6 TRUERun 0.00011 0.11 Isokinetic Ratio -1.51 FALSEBlank 0.00011 0.11 5 up / 2 down (Y/N?) No TRUE

No of ports 2 FALSERequirements:







Before Blank : After Blank: Before Sample After SampleLeak Test Results: 0 0 -50 -50 cc/min


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Measured Quantities Symbol Value Standard uncertainty Units Uncertainty as percentage Uncertainty aRequirement of stdSampled Volume Vm 0.54230008 uVm 0.001 m3 0.18 <=2%Sampled gas Temperature Tm 352.79 uTm 2 k 0.57 <=1%Sampled gas Pressure ρm 100.167 uρm 1 kPa 1.00 <=1%Sampled gas Humidity Hm 1.603154467 uHm 1 % by volume 62.38 <=1%Oxygen content O2,m 19.58 uO2,m 0.1 % by volume 0.51 <=5%Mass particulate m 0.11 um 0.00 mg 0.00 0.00 <5% of limit valueNote - Sampled gas humidity, temperature and pressure are values at the gas meterLeak L -0.553199255 % -0.55 <=2%Uncollected Mass UCM 0 mg 0 <=10%(Instack filter - no rinse)Intermediate calculationsFactor for std conds fs 0.75uncertainty components symbol sensitivity coeff u (in units of fs)

ρm 0.008 0.008Hm 0.008 0.008Tm 0.002 0.004ufs 0.012 1.53









sm fVV

m

refc O

Of

,2

,2

2121

cfVmc

3.101273

100)100( m

m

ms T

Hf


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EPA Export 18-08-2019:03:54:54





Measured Quantities Symbol Value Standard uncertainty Units Uncertainty as percentage Uncertainty aRequirement of stdSampled Volume Vm 0.54230008 uVm 0.001 m3 0.18 <=2%Sampled gas Temperature Tm 352.79 uTm 2 k 0.57 <=1%Sampled gas Pressure ρm 100.167 uρm 1 kPa 1.00 <=1%Sampled gas Humidity Hm 1.603154467 uHm 1 % by volume 62.38 <=1%Oxygen content O2,m 19.58 uO2,m 0.1 % by volume 0.51 <=5%Mass particulate m 0.11 um 0.00 mg 0.00 0.00 <5% of limit valueNote - Sampled gas humidity, temperature and pressure are values at the gas meterLeak L 0 % 0.00 <=2%Uncollected Mass UCM 0 mg 0 <=10%(Instack filter - no rinse)Intermediate calculationsFactor for std conds fs 0.75uncertainty components symbol sensitivity coeff u (in units of fs)

ρm 0.008 0.008Hm 0.008 0.008Tm 0.002 0.004ufs 0.012 1.53








sm fVV

m

refc O

Of

,2

,2

2121

3.101273

100)100( m

m

ms T

Hf

cfVmc


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EPA Export 18-08-2019:03:54:54




No. Temp oC O2 % CO2 % CO ppm NO ppm NO2 ppm NOx ppm SO2 ppm1 79.79 19.54 0.83 3 62 79.79 19.51 0.85 4 63 79.79 19.5 0.85 4 64 79.79 19.47 0.89 4 65 79.79 19.48 0.87 4 66 79.79 19.48 0.86 4 67 79.79 19.51 0.85 3 68 79.79 19.52 0.83 3 69 79.79 19.56 0.83 3 6

10 79.79 19.62 0.77 2 611 79.79 19.66 0.74 2 612 79.79 19.73 0.72 2 613 79.79 19.74 0.71 2 614 79.79 19.77 0.7 2 615 79.79 19.79 0.68 2 516 79.79 19.79 0.68 2 617 79.79 19.75 0.72 2 618 79.79 19.68 0.75 2 619 79.79 19.64 0.77 2 620 79.79 19.59 0.82 3 621 79.79 19.53 0.85 3 622 79.79 19.49 0.86 4 723 79.79 19.49 0.87 4 624 79.79 19.47 0.87 4 725 79.79 19.44 0.88 4 726 79.79 19.46 0.86 4 727 79.79 19.48 0.85 4 628 79.79 19.5 0.84 3 629 79.79 19.52 0.83 3 630 79.79 19.55 0.8 3 6













01/11/2018M54

MM14 1287TE1, TE2, TE3, TE4


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EPA Export 18-08-2019:03:54:54




5290/M54

Stack information:

Stack dimensions


(Y/N)?








Flow Rate m3/sec:







Report Number :


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EPA Export 18-08-2019:03:54:54




1990 Pa0.01 Pa










1 101220 101421 74.466 74.47 63.91 0.00 0.00 0 100.0 0.00 28.00 28.002 0.00 0.00 0 100.0 0.00 28.00 28.003 0.00 0.00 0 100.0 0.00 28.00 28.004 0.00 0.00 0 100.0 0.00 28.00 28.005 0.00 0.00 0 100.0 0.00 28.00 28.006 0.00 0.00 0 100.0 0.00 28.00 28.007 0.00 0.00 0 100.0 0.00 28.00 28.008 0.00 0.00 0 100.0 0.00 28.00 28.009 0.00 0.00 0 100.0 0.00 28.00 28.00

10 0.00 0.00 0 100.0 0.00 28.00 28.0011 0.00 0.00 0 100.0 0.00 28.00 28.0012 0.00 0.00 0 100.0 0.00 28.00 28.0013 0.00 0.00 0 100.0 0.00 28.00 28.0014 0.00 0.00 0 100.0 0.00 28.00 28.0015 0.00 0.00 0 100.0 0.00 28.00 28.0016 0.00 0.00 0 100.0 0.00 28.00 28.0017 0.00 0.00 0 100.0 0.00 28.00 28.0018 0.00 0.00 0 100.0 0.00 28.00 28.0019 0.00 0.00 0 100.0 0.00 28.00 28.0020 0.00 0.00 0 100.0 0.00 28.00 28.00











Dry gas basis





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Table 1



67

Molar Mass 8u(H2O) 0 9(O2)wet 0.0 10u(O2)wet 0.00 11(CO2)wet 0.0 12u(CO2)wet 0.00 13(CO)wet 0.0 14u(CO)wet 0.00 15Oxygen sensitivity 4.00E‐05 16Water sensitivity 1.00E‐04 17CO2 sensitivity 1.60E‐04 18CO sensitivity 4.00E‐08 19









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Lookup tables



10 0.32511 0.31512 0.30715 0.28820 0.26825 0.25430 0.24540 0.22750 0.22260 0.21680 0.206

100 0.199


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1 6.00 65.03 60.39 9.27 <152 22.50 78.56 60.45 10.20 <153 67.50 65.87 60.55 9.27 <154 84.00 74.84 60.70 9.98 <1556789

101112

Average 71.08 60.52 9.68Min 65.03 60.39 9.27Max 78.56 60.70 10.20


1 6.00 73.31 60.87 9.86 <152 22.50 68.40 60.92 9.49 <153 67.50 66.85 60.93 9.38 <154 84.00 65.48 60.94 9.29 <1556789

101112

Average 68.51 60.92 9.51Min 65.48 60.87 9.29Max 73.31 60.94 9.86


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2.5 1.0185Before EM003 0.5 1.0051 08/05/2017



Average: 443.1 631.4 568.6 384.9 699.5 2727.5 2.88 0.99193.6 0.9963


1 442.2 628.5 568.8 384.2 699.1 2722.8 2.16 0.99842 442.2 628.5 568.8 384.2 699.1 2722.8 2.88 1.00383 442.2 628.5 568.8 384.2 699.1 2722.8 3.6 1.01614 442.2 628.5 568.8 384.2 699.1 2722.85 442.2 628.5 568.8 384.2 699.1 2722.86 442.2 628.5 568.8 384.2 699.1 2722.87 442.2 628.5 568.8 384.2 699.1 2722.88 442.2 628.5 568.8 384.2 699.1 2722.89 442.2 628.5 568.8 384.2 699.1 2722.8


Average: 442.2 628.5 568.8 384.2 699.1 2722.8

Difference in weigh of impingers after and before measurements: -4.7 g

-6.11 g/m3

20.35 %20.35 %

-0.8 %-0.8 %

Weights: Before Sampling: After Sampling: Difference:Silca trap: 699.5 699.1 -0.4 g

Efficiency: 100.1 %


TE's


Corrected to O2ref:





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Measured concentration -0.8 % (at STP)

Measured Quantities Symbol Value Standard uncertainty UnitsSampled Volume Vm 0.769459838 uVm 0.001 m3Sampled gas Temperature Tm 336.91 uTm 2 kSampled gas Pressure ρm 101.421 uρm 1 kPaEfficiency Ɛ 100.06 %Oxygen content O2,m 20.35 uO2,m 0.1 % by volumeWater collected in condensation stage 699.50Water collected in adsorption stage -0.4Wate collected in addidional unit -0.40Water collected in trapping m 699.10 um 0.00 gIntermediate calculationsVwc 176.945984 ^2



water in adsorption stage #NUM!Uncertainty Efficiency^2 #NUM!Volume ^2 0.9Sensityvity coefficiency #NUM!Uncertainty efficiency #NUM!


Combined measurement uncertainty #NUM! %

Expanded uncertainty as percentage of measured value #NUM! % measured of value expressed with a level of confidence of 95%(Using a coverage factor k=2)

Expanded uncertainty in units of measuremen #NUM! % of water vapour



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No of ports 2 FALSERequirements:







Before Blank : After Blank: Before Sample After SampleLeak Test Results: 0 0 0 0 cc/min


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Measured Quantities Symbol Value Standard uncertainty Units Uncertainty as percentage Uncertainty aRequirement of stdSampled Volume Vm 0.769459838 uVm 0.001 m3 0.13 <=2%Sampled gas Temperature Tm 336.91 uTm 2 k 0.59 <=1%Sampled gas Pressure ρm 101.421 uρm 1 kPa 0.99 <=1%Sampled gas Humidity Hm 0 uHm 1 % by volume 1.00 <=1%Oxygen content O2,m 20.35 uO2,m 0.1 % by volume 0.49 <=5%Mass particulate m 11.83 um 0.00 mg 0.00 0.00 <5% of limit valueNote - Sampled gas humidity, temperature and pressure are values at the gas meterLeak L 0 % 0.00 <=2%Uncollected Mass UCM 0 mg 0 <=10%(Instack filter - no rinse)Intermediate calculationsFactor for std conds fs 0.81uncertainty components symbol sensitivity coeff u (in units of fs)

ρm 0.008 0.008Hm 0.008 0.008Tm 0.002 0.005ufs 0.012 1.52









sm fVV

m

refc O

Of

,2

,2

2121

cfVmc

3.101273

100)100( m

m

ms T

Hf


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Measured Quantities Symbol Value Standard uncertainty Units Uncertainty as percentage Uncertainty aRequirement of stdSampled Volume Vm 0.769459838 uVm 0.001 m3 0.13 <=2%Sampled gas Temperature Tm 336.91 uTm 2 k 0.59 <=1%Sampled gas Pressure ρm 101.421 uρm 1 kPa 0.99 <=1%Sampled gas Humidity Hm 0 uHm 1 % by volume 1.00 <=1%Oxygen content O2,m 20.35 uO2,m 0.1 % by volume 0.49 <=5%Mass particulate m 0.11 um 0.00 mg 0.00 0.00 <5% of limit valueNote - Sampled gas humidity, temperature and pressure are values at the gas meterLeak L 0 % 0.00 <=2%Uncollected Mass UCM 0 mg 0 <=10%(Instack filter - no rinse)Intermediate calculationsFactor for std conds fs 0.81uncertainty components symbol sensitivity coeff u (in units of fs)

ρm 0.008 0.008Hm 0.008 0.008Tm 0.002 0.005ufs 0.012 1.52








sm fVV

m

refc O

Of

,2

,2

2121

3.101273

100)100( m

m

ms T

Hf

cfVmc


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No. Temp oC O2 % CO2 % CO ppm NO ppm NO2 ppm NOx ppm SO2 ppm1 63.91 20.35 24 22 63.91 20.37 28 23 63.91 20.33 24 24 63.91 20.37 28 25 63.91 20.35 24 26 63.91 20.34 27 27 63.91 20.38 27 28 63.91 20.35 25 29 63.91 20.39 25 2

10 63.91 20.34 26 311 63.91 20.36 27 212 63.91 20.35 24 213 63.91 20.37 25 214 63.91 20.32 24 215 63.91 20.39 27 216 63.91 20.33 25 217 63.91 20.36 27 218 63.91 20.34 23 219 63.91 20.35 27 220 63.91 20.36 28 221 63.91 20.32 25 322 63.91 20.34 29 223 63.91 20.34 27 224 63.91 20.37 28 325 63.91 20.33 26 326 63.91 20.36 25 327 63.91 20.37 25 228 63.91 20.34 26 229 63.91 20.34 25 230 63.91 20.37 26 2






SO2 #DIV/0! ppmConvert to mg/Nm3 #DIV/0! Nmg/m3Corrected to ref. O2 % #DIV/0! Nmg/m3Mass concentration STP, dry, Ref O2 #DIV/0! kg/hrCO2Meas CO2 Value #DIV/0! %







02/11/2018M54

MM14 1287TE1, TE2, TE3, TE4


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Emissions to Atmosphere Report No: 5290/M54 Industrial … · Report for the Periodic Monitoring of...

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