EDITA: Dpto. Hidrogeología y Química Analítica UNIVERSIDAD DE ALMERÍA

International Scientific Committee

• Dr. Triantafyllos Albanis (University of Ioannina, Greece). • Dr. Ana Agüera (University of Almería, Spain). • Dr. Serge Chiron (University of Provence, France) • Dr. María de Fátima Alpendurada (University of Porto, Portugal). • Dr. Horacio R. Beldoménico (UNL, Argentina) • Dr. Sixto Malato (PSA-CIEMAT, Spain). • Dr. Sabino Bufo (University of Basilicata, Italy). • Dr. Joan Albaigés (CID-CSIC Barcelona, Spain). • Dr. Mª. Dolores Hernando (University of Almería, Spain). • Dr. George Miliadis (Banakeio Institute of Phytopatlogy, Greece). • Dr. Amadeo R. Fernández-Alba (University of Almería, Spain). • Dr. Gaël Durand (Pole Analytique des Eaux - Brest, France). • Dr. Anastasios Zouboulis (Aristotle University of Thessaloniki, Greece). • Dr. Antonio Valverde (University of Almería, Spain). • Dr. Konstantinos Poulos (University of Patras, Greece). • Dr. Silvia Lacorte (CID-CSIC -Barcelona, Spain). • Dr. Konstantinos Fytianos (Aristotle University of Thessaloniki, Greece). • Dr. Marie Claire Hennion (ESPCI Paris, France). • Dr. Milagros Mezcua (University of Almería, Spain). • Dr. Despina Tsipi (General State Laboratory of Athens, Greece). • Dr. Imma Ferrer (University of Almería, Spain). • Dr. Thierry Dagnac (CIAM A Coruña, Spain). • Dr. I.K. Konstantinou (University of Ioannina, Greece). • Dr. Marco Trevisan (University of Peruge, Italy). • Dr. Michael Thurman (University of Almería, Spain). • Dr. Dimitra Lambropoulou (University of Ioannina, Greece).

Organizing Committee Conference Chairman: Dr. Amadeo R. Fernández-Alba Co-Chairman (ENEAP): Dr. Triantafyllos Albanis Co-Chairman (IAEAC): Dr. Joan Albaigés Scientific Secretary: Dr. Ana Agüera Vocals: Dr. María Dolores Hernando Dr. Antonio Valverde Dr. Milagros Mezcua Dr. Imma Ferrer Ms. Paula Medina Ms. María Jesús Martínez Ms. María José Gómez Ms. Carmen Ferrer Mr. Antonio V. Monterreal Mr. Octavio Malato

Supporting Organizations

Ministerio de Ciencia y Tecnología

Sociedad Española de Cromatografía y Técnicas Afines (SECyTA)

Universidad de Almería

Exhibitors/Sponsors

Detailed Programme

Detailed Programme

SUNDAY 26

OPENING CEREMONY

19:00-19:15 OPENING CEREMONY

19:15-20:00

PLENARY LECTURE: The fate and input of organochlorine and polar pesticides of the Ebro River

into the NW Mediterranean Joan Albaiges

20:00 WELLCOME RECEPTION

Detailed Programme

MONDAY 27

SESSION 1

OCCURRENCE AND FATE OF PESTICIDES AND OTHER MICROCONTAMINANTS IN THE ENVIRONMENT (I)

Chairman: J. Albaiges

9:00-9:30

IL-1: Analysis and concentration level of pesticides with

endocrine disruptive activity (EDC) in European food diet Triantafyllos Albanis

9:30-9:45 O-1:

Retrieval of insecticides in streams, rivers and ground waters in Norway Gro Hege Ludvigsen

9:45-10:00

O-2: Levels of pesticides in streams, sediments and rainfall. Results from

the Swedish national pesticide monitoring program Jenny Kreuger

10:00-10:15 O-3:

Axios river pollution. Part I: The pesticides Dimitra Lambropoulou

10:15-10:30 O-4:

Input, flux, and persistence of six select pesticides in San Francisco bay, California Kathryn M. Kuivila

10:30-10:45

O-5: Monitoring study of pesticides in groundwater samples from a vulnerable zone

located in north Portugal: descriptive and multivariate statistical analysis Carlos Gonçalves

10:45-11:00

O-6: Evaluating the vulnerability of surface and coastal waters to antibiotics

on the French Mediterranean coast Juliana Felizzola

11:00-11:30 COFFEE BREAK

OCCURRENCE AND FATE OF PESTICIDES AND OTHER MICROCONTAMINANTS IN THE ENVIRONMENT (II)

Chairman: M. E. Thurman

11:30-12:00

IL-2: Occurrence and fate of endocrine disruptors in the Llobregat and

Ter river basins (Catalonia, N.E. Spain) Silvia Lacorte

12:00-12:15

O-7: Fenitrothion residues in leaves and soil of vineyard sprayed with

microencapsulate formulation Nikolaos G. Tsiropoulos

12:15-12:30 O-8:

Polycyclic aromatic nitrogen heterocycles –Analytical and distribution aspects Zdeněk Šimek

12:30-12:45

O-9: Comparison between the transport of isoxaflutole and its degradates to

triazine and acetanilide herbicides in ten Iowa rivers Michael T. Meyer

Detailed Programme

12:45-13:00

O-10: The significance of the indirect photolysis of crop protection products in natural

waters Sui Kuet

13:00-13:15

O-11: Characterization and distribution of Organochlorine pesticides in estuarine sediments

from the cantabric Coast Sonia Gómez

13:15-13:30 O-12:

Distribution of BTX in rain, surface and ground water of central India Saroj Sharma

13:30-15:00 LUNCH

OCCURRENCE AND FATE OF PESTICIDES AND OTHER MICROCONTAMINANTS IN THE ENVIRONMENT (III)

Chairman: T. Albanis

15:00-15:30 IL-3:

Occurrence, Transport and Fate of Pesticides and their Degradates in Groundwater Michael E. Thurman

15:30-15:45 O-13:

Stimulated rhizodegradation of atrazine by selected plant species R. N. Lerch

15:45-16:00 O-14:

Estrogenic Mycotoxins in Drainage Water Released from Wheat- and Corn Fields Niccolo Hartmann

16:00-16:15

O-15: Effects of Pest management and tillage practice on environmental load,

economy and farmers attitude Ole Martin Eklo

16:15-16:45 COFFEE BREAK

OCCURRENCE AND FATE OF PESTICIDES AND OTHER MICROCONTAMINANTS IN THE ENVIRONMENT (IV)

Chairman: Silvia Lacorte

16:45-17:15 IL-4:

Fate of pharmaceuticals in water-sediment systems María Ramil

17:15-17:30

O-16: Monitoring of multiple pesticide residues in different types of olive oil and preliminary

exposure assessment of Greek consumers to the pesticide residues detected Elpiniki G. Amvrazi

17:30-17:45

O-17: The effect of humic acid on the detection of pesticides at 20 parts per trillion in drinking water by LC/MS/MS using direct injection with no sample pretreatment

Manuel Lolo, Stephen J. Lock & Betram Nieland

17:45-18:00

O-18: Influence of cosolvents on the adsorption and movement of Endosulfan in Indian

soils R.P. Singh

18:00-19:00 POSTER SESSION

Detailed Programme

TUESDAY 28

SESSION 2:

ANALYTICAL TECHNIQUES APPLIED TO ENVIRONMENTAL AND FOOD ANALYSIS (I)

Chairman: Yolanda Picó

9:00-9:30

IL-5: Innovative multidimensional and comprehensive chromatography techniques for the

analysis of complex mixtures Luigi Mondello

9:30-9:45 O-19:

Strategies to control the quality of food crops used for baby food production Jana Hajslova

9:45-10:00

O-20: Determination of different classes of pesticides in processed fruits and vegetables by

Liquid Chromatography – Electrospray Ionization Tandem Mass Spectrometry Despina Tsipi

10:00-10:15

O-21: Endocrine disrupting and pharmacologically active compounds in the aquatic

environment -the contribution of immunochemical methods Rudolf J. Schneider

10:15-10:30

O-22: Advanced routine method for the analysis of pesticide residues by LV-PTV-GC-

TOFMS and LV-PTV-GCxGC-TOFMS Ralf Löscher

10:30-10:45

O-23: Sources and processes affecting the levels of pharmaceuticals, personal care

products, encocrine disruptors and feacal steroids from outfalls to coastal waters Carlos Guitart

10:45-11:00

O-24: Qualitative and quantitative analysis of polar pesticide multi residues in leave samples

with Liquid Chromatography – Ion Trap Mass Detector Céline Lesueur

11:00-11:30 COFFEE BREAK

ANALYTICAL TECHNIQUES APPLIED TO ENVIRONMENTAL AND FOOD ANALYSIS (II)

Chairman: Hans Mol

11:30-12:00

IL-6: Application of Liquid-Chromatography-Tandem Mass Spectrometry to the

determination of pesticides and their metabolites in food Yolanda Picó

12:00-12:15

O-25: Determination of new generation pesticides in complex plant matrices

by HPLC using different stationary phases Monika Michel

12:15-12:30

O-26: Screening for 927 Pesticides and Endocrine Disruptors by GC/MS with Deconvolution

Reporting Software and a New Pesticide Library Philip L. Wylie

Detailed Programme

12:30-12:45 O-27:

Carfentrazone-ethyl - Ground Application Rate Verification Experiment Audrey Chen

12:45-13:00

O-28: Fast analysis of herbicides in natural water and soil by Ultra Performance Liquid

Chromatography/Tandem Mass Spectrometry Roberto Romero

13:00-13:15

O-29: Development and implementation of fast GC combined with MS and efficient sample

preparation techniques for ultratrace pesticide residues analysis Eva Matisová

13:15-13:30

O-30: Matrix solid-phase dispersion extraction for the screening of endocrine disrupting

compounds and their metabolites residues in fruits, vegetables and juices Vasiliki I. Boti

13:30-15:00 LUNCH

ANALYTICAL TECHNIQUES APPLIED TO ENVIRONMENTAL AND FOOD ANALYSIS (III)

Chairman: L. Mondello

15:00-15:30

IL-7: Comprehensive residue/contaminant analysis: taking advantage of advanced mass

spectrometric detection Hans Mol

15:30-15:45

IL-8: Development and application of a multiresidue method for the determination of

pesticides and contaminants in food and feed using GCxGC-TOF-MS and LC-MS/MS Win Traag

15:45-16:00

O-31: Development and validation of an analytical method for the Simultaneous Determination of Endocrine Disruptors in Wastewater and Sewage Sludge

Nikolaos S. Thomaidis

16:00-16:15

O-32: Determination of PASH by various analytical techniques based on gas

chromatography-mass spectrometry. Application to biodesulfurization processes M. Mezcua

16:15-16:30

O-33: Investigation of bee hive fading away by means of multi-group pesticide

measurements in bees and associated products by on-column liquid-liquid extraction and both GC- and LC-MS/MS method Development

Laetitia Heudt

16:30-17:00

O-34: Development of a rapid and sensitive SPME-GC-ECD method for the determination of

polychlorinated biphenyls in water Katerina Tsimeli

17:00-18:00 POSTER SESSION

20:30 DINNER

Detailed Programme

WEDNESDAY 29

SESSION 3:

ENVIRONMENTAL EFFECTS, TOXICITY AND RISK (I)

Chairman: I Konstantinou

9:00-9:30 IL-9:

Low Concentrations-Significant effects Peter-Dietrich Hansen

9:30-9:45 O-35:

The role of EFSA’s Scientific PPR Panel in pesticide risk assessment. Christine Fuell

9:45-10:00 O-36:

Measuring bioavailable concentrations of pesticides in aquatic environments Jay Gan

10:00-10:15 O-37:

Quantitative determination of the influence of adjuvants on fungicide residues Bert Ryckaert

10:15-10:30 O-38:

Quantification of toxicity using bioluminescent bacteria and an instant film camera Fernando Rubio

10:30-10:45

O-39: Monitoring of pesticides and heavy metals in the western desert lakes of Egypt and

bioassaying potential toxicity of their waters Sameeh A. Mansour

10:45-11:15 COFFEE BREAK

ENVIRONMENTAL EFFECTS, TOXICITY AND RISK (II)

Chairman: Peter Hansen

11:15-11:30 O-40:

PBT characteristics and risk of lipid regulators in the environment M.D. Hernando

11:30-11:45

O-41: The attempt of mathematical simulation of dioxin-induced toxic effects

on red blood cells Anatoly G. Davidovsky

11:45-12:00 O-42:

The effects of sub- chronic exposure of rats to herbicide (glyphosate – roundup) Dürdane Kolankaya

12:00-12:15 O-43:

Studies on the response of soil microflora to the application OF fungicide fenhexamid Cristina Abbate

12:15-13:15 POSTER SESSION

13:15-15:00 LUNCH

Detailed Programme

SESSION 4:

PROTECTION AND RESTORATION TECHNIQUES

Chairman: A.R. Fernández-Alba

15:00-15:30

IL-10: Treatment of wastewater by Advances Oxidation Technologies

using Solar Energy: An overview Sixto Malato

15:30-15:45

O-44: Photocatalytic oxidation of dimethachlor Herbicide over

polyethylene glycol (PEG)-metal-modified TiO2 photocatalysts I. Konstantinou

15:45-16:00

O-45: New assessment of degradation methods for micropollutants: several

alternatives for imazethapyr detoxification Sabino A. Bufo

16:00-16:15

O-46: Application of Fenton oxidation for the degradation of atrazine and fenitrothion in

aquatic solutions Despo Fatta

16:15-16:30 O-47:

Photocatalytic oxidation of molinate in aqueous solutions Erasmia A. Bizani

16:30-16:45

O-48: Optimization of bioremediation systems for the processing

of spray losses of pesticides Tineke de Wilde

16:45-17:00

O-49: Odor and corrosion control in wastewater treatment plants:H2S photocatalytic

destruction by UV-radiation Raquel Portela

17:00-17:30 CLOSING CEREMONY

“Roland W. Frei Award”

Index

THE FATE AND INPUT OF ORGANOCHLORINE AND POLAR PESTICIDES OF THE EBRO RIVER INTO THE NW MEDITERRANEAN Anna I. Gómez, Eric Jover, Josep M. Bayona and Joan Albaigés

SESSION 1

OCCURRENCE AND FATE OF PESTICIDES AND OTHER MICROCONTAMINANTS

IN THE ENVIRONMENT IL-1. ANALYSIS AND CONCENTRATIONS LEVELS OF PESTICIDES WITH ENDOCRINE DISRUPTIVE ACTIVITY (EDC) IN EUROPEAN FOOD DIET Triantafyllos Albanis,Vasilios Sakkas, Vasiliki Boti and Vasiliki Valsamaki IL-2. OCCURENCE AND FATE OF ENDOCRINE DISRUPTORS IN THE LLOBREGAT AND TER RIVER BASINS (CATALONIA, N.E. SPAIN) Raquel Céspedes, Sílvia Lacorte, Demetrio Raldúa, Antonio Ginebreda, Damià Barceló and Benjamín Piña IL-3. OCCURENCE, TRANSPORT AND FATE OF PESTICIDES AND THEIR DEGRADATES IN GROUND WATER E. Michael Thurman, Imma Ferrer IL-4. FATE OF PHARMACEUTICALS IN WATER-SEDIMENT SYSTEMS Maria Ramil, Tarek Elaref, Dirk Loeffler and Thomas Ternes

SESSION 2

ANALYTICAL TECHNIQUES APPLIED TO ENVIRONMENTAL AND FOOD ANALYSIS IL-5. INNOVATIVE MULTIDIMENSIONAL AND COMPREHENSIVE CHROMATOGRAPHY TECHNIQUES FOR THE ANALYSIS OF COMPLEX MIXTURES Luigi Mondello, Alessandro Casilli, Enio Belotti, Rino Calori, Roberto Ferrari IL-6. APPLICATION OF LIQUID CHROMATOGRAPHY-TANDEM MASS SPECTROMETRY TO THE DETERMINATION OF PESTICIDES AND THEIR METABOLITES IN FOOD Yolanda Picó IL-7. COMPREHENSIVE RESIDUE AND CONTAMINANT ANALYSIS: TAKING ADVANTAGE OF ADVANCED MASS SPECTROMETRIC DETECTION Hans G.J. Mol, Paul Zomer, Karl Ehlert, Richard Bas, Peter Boshuis, Ruud Van Dam and Peter Hancock IL-8. DEVELOPMENT AND APPLICATION OF A MULTIRESIDUE METHOD FOR THE DETERMINATION OF PESTICIDES AND CONTAMINANTS IN FOOD AND FEED USING GCXGC-TOF-MS AND LC-MS/MS. Win Traag

SESSION 3

ENVIRONMENTAL EFFECTS, TOXICITY AND RISK

IL-9. LOW CONCENTRATIONS-SIGNIFICANT EFFECTS. Peter-Dietrich Hansen

SESSION 4

PROTECTION AND RESTORATION TECHNIQUES IL-10. TREATMENT OF WASTEWATER BY ADVANCED OXIDATION TECHNOLOGIES USING SOLAR ENERGY: AN OVERVIEW Sixto Malato

SESSION 1

OCCURRENCE AND FATE OF PESTICIDES AND OTHER MICROCONTAMINANTS IN THE

ENVIRONMENT O-1. RETRIEVAL OF INSECTICIDES IN STREAMS, RIVERS AND GROUND WATERS IN NORWAY Gro Hege Ludvigsen and Olav Lode

O-2. LEVELS OF PESTICIDES IN STREAMS, SEDIMENTS AND RAINFALL – RESULTS FROM THE SWEDISH NATIONAL PESTICIDE MONITORING PROGRAM Jenny Kreuger, Stina Adielsson

O-3. AXIOS RIVER POLLUTION. PART I: THE PESTICIDES Triantafyllos Albanis, Fokion Vosniakos, Kostas Nikolaou, Mihail Kochubovski, Dragan Gjorgjef, Blagoja Aleksoski, Dimitra Lambropoulou, Kostas Zavlaris and Presvia Selimi O-4. INPUT, FLUX, AND PERSISTENCE OF SIX SELECT PESTICIDES IN SAN FRANCISCO BAY, CALIFORNIA Kathryn M. Kuivila and Bryan E. Jennings

O-5. MONITORING STUDY OF PESTICIDES IN GROUNDWATER SAMPLES FROM A VULNERABLE ZONE LOCATED IN NORTH PORTUGAL: DESCRIPTIVE AND MULTIVARIATE STATISTICAL ANALYSIS Carlos Gonçalves; Joaquim C. G. Esteves Da Silva and Maria De Fátima Alpendurada O-6. EVALUATING THE VULNERABILITY OF SURFACE AND COASTAL WATERS TO ANTIBIOTICS ON THE FRENCH MEDITERRANEAN COAST. Juliana Felizzola and Serge Chiron O-7. FENITROTHION RESIDUES IN LEAVES AND SOIL OF VINEYARD SPRAYED WITH MICROENCAPSULATE FORMULATION. Dimitrios T. Likas and Nikolaos G. Tsiropoulos O-8. POLYCYCLIC AROMATIC NITROGEN HETEROCYCLES – ANALYTICAL AND DISTRIBUTION ASPECTS Zdeněk Šimek, Radim Švábenský, Kamila Kočí O-9. COMPARISON BETWEEN THE TRANSPORT OF ISOXAFLUTOLE AND ITS DEGRADATES TO TRIAZINE AND ACETANILIDE HERBICIDES IN TEN IOWA RIVERS Michael T. Meyer, Stephen J. Kalkhoff, and Elisabeth A. Scribner O-10. THE SIGNIFICANCE OF THE INDIRECT PHOTOLYSIS OF CROP PROTECTION PRODUCTS IN NATURAL WATERS Sui Kuet, Claire Elliot and Robin Oliver O-11. CHARACTERIZATION AND DISTRIBUTION OF ORGANOCHLORINE PESTICIDES IN ESTUARINE SEDIMENTS FROM THE CANTABRIC COAST. Sonia Gómez, Daniel Gorri; and Angel Irabien O-12. DISTRIBUTION OF BTX IN RAIN, SURFACE AND GROUND WATER OF CENTRAL INDIA Saroj Sharma and Khageshwar Singh Patel O-13. STIMULATED RHIZODEGRADATION OF ATRAZINE BY SELECTED PLANT SPECIES C. H. Lin, R. N. Lerch, R. J. Kremer, H. E. Garrett and M. F. George

O-14. ESTROGENIC MYCOTOXINS IN DRAINAGE WATER RELEASED FROM WHEAT- AND CORN FIELDS Niccolo Hartmann, Thomas D. Bucheli, Marianne Erbs, Felix E. Wettstein, Susanne Vogelgsang, Hans-Rudolf Forrer, René P. Schwarzenbach

O-15. EFFECTS OF PEST MANAGEMENT AND TILLAGE PRACTICE ON ENVIRONMENTAL LOAD, ECONOMY AND FARMERS ATTITUDE Ole Martin Eklo, Eirik Romstad and Haldor Fykse O-16. MONITORING OF MULTIPLE PESTICIDE RESIDUES IN DIFFERENT TYPES OF OLIVE OIL AND PRELIMINARY EXPOSURE ASSESSMENT OF GREEK CONSUMERS TO THE PESTICIDE RESIDUES DETECTED Elpiniki G. Amvrazi and Triantafyllos A. Albanis O-17. THE EFFECT OF HUMIC ACID ON THE DETECTION OF PESTICIDES AT 20 PARTS PER TRILLION IN DRINKING WATER BY LC/MS/MS USING DIRECT INJECTION WITH NO SAMPLE PRETREATMENT Manuel Lolo, Stephen J. Lock and Betram Nieland O-18. INFLUENCE OF COSOLVENTS ON THE ADSORPTION AND MOVEMENT OF ENDOSULFAN IN INDIAN SOILS R.P. Singh

SESSION 2

ANALYTICAL TECHNIQUES APPLIED TO ENVIRONMENTAL AND FOOD ANALYSIS O-19. STRATEGIES TO CONTROL THE QUALITY OF FOOD CROPS USED FOR BABY FOOD PRODUCTION Jana Hajslova, Tomas Cajka, Jana Ticha, Ondrej Lacina O-20. DETERMINATION OF DIFFERENT CLASSES OF PESTICIDES IN PROCESSED FRUITS AND VEGETABLES BY LIQUID CHROMATOGRAPHY – ELECTROSPRAY IONIZATION TANDEM MASS SPECTROMETRY Helen Botitsi, Pigi Kormali, Anastasios Economou, Despina Tsipi O-21. ENDOCRINE DISRUPTING AND PHARMACOLOGICALLY ACTIVE COMPOUNDS IN THE AQUATIC ENVIRONMENT - THE CONTRIBUTION OF IMMUNOCHEMICAL METHODS Rudolf J. Schneider O-22. ADVANCED ROUTINE METHOD FOR THE ANALYSIS OF PESTICIDE RESIDUES BY LV-PTV-GC-TOFMS AND LV-PTV-GCXGC-TOFMS Sabine Bergmann, Gerold Appelt, Antje Kreißel, Ralf Löscher, Sjaak de Koning, Peter Horst Tablack, Jitka Zrostlikova, Tomas Kovalczuk, Günther Kempe O-23. SOURCES AND PROCESSES AFFECTING THE LEVELS OF PHARMACEUTICALS, PERSONAL CARE PRODUCTS, ENCOCRINE DISRUPTORS AND FEACAL STEROIDS FROM OUTFALLS TO COASTAL WATERS Carlos Guitart, Trish Frickers and James W Readman O-24. QUALITATIVE AND QUANTITATIVE ANALYSIS OF POLAR PESTICIDE MULTI RESIDUES IN LEAVE SAMPLES WITH LIQUID CHROMATOGRAPHY – ION TRAP MASS DETECTOR Céline Lesueur, Michael Gartner and Maria Fuerhacker O-25. DETERMINATION OF NEW GENERATION PESTICIDES IN COMPLEX PLANT MATRICES BY HPLC USING DIFFERENT STATIONARY PHASES Monika Michel O-26. SCREENING FOR 927 PESTICIDES AND ENDOCRINE DISRUPTORS BY GC/MS WITH DECONVOLUTION REPORTING SOFTWARE AND A NEW PESTICIDE LIBRARY Philip L. Wylie O-27. CARFENTRAZONE-ETHYL - GROUND APPLICATION RATE VERIFICATION EXPERIMENT Audrey Chen, John F. Culligan Jr, Ming Xiong, Rocco Johns and John Arabinick

O-28. FAST ANALYSIS OF HERBICIDES IN NATURAL WATER AND SOIL BY ULTRA PERFORMANCE LIQUID CHROMATOGRAPHY/TANDEM MASS SPECTROMETRY Roberto Romero-González, M. Elena Hernández-Torres, Elena Pastor-Montoro, Antonio Belmonte-Vega, José Luis Martínez-Vidal and Antonia Garrido-Frenich O-29. DEVELOPMENT AND IMPLEMENTATION OF FAST GC COMBINED WITH MS AND EFFICIENT SAMPLE PREPARATION TECHNIQUES FOR ULTRATRACE PESTICIDE RESIDUES ANALYSIS Eva Matisová, Michal Kirchner, Milena Dömötörová, Andrea Hercegová, Svetlana Hrouzková, Renáta Húšková O-30. MATRIX SOLID-PHASE DISPERSION EXTRACTION FOR THE SCREENING OF ENDOCRINE DISRUPTING COMPOUNDS AND THEIR METABOLITES RESIDUES IN FRUITS, VEGETABLES AND JUICES Vasiliki I. Boti, Vasilios A. Sakkas and Triantafyllos A. Albanis O-31. DEVELOPMENT AND VALIDATION OF AN ANALYTICAL METHOD FOR THE SIMULTANEOUS DETERMINATION OF ENDOCRINE DISRUPTORS IN WASTEWATER AND SEWAGE SLUDGE Georgia Gatidou, Nikolaos S. Thomaidis,, Athanasios S. Stasinakis, Themistokles D. Lekkas O-32. DETERMINATION OF PASH BY VARIOUS ANALYTICAL TECHNIQUES BASED ON GAS CHROMATOGRAPHY-MASS SPECTROMETRY. APPLICATION TO A BIODESULFURIZATION PROCESS. Milagros Mezcua, Amadeo R. Fernández-Alba, Ana Agüera, Karina Boltes, Pedro Leton, Raul Alonso del Aguila, Antonio Rodríguez

O-33. INVESTIGATION OF BEE HIVE FADING AWAY BY MEANS OF MULTI-GROUP PESTICIDE MEASUREMENTS IN BEES AND ASSOCIATED PRODUCTS BY ON-COLUMN LIQUID-LIQUID EXTRACTION AND BOTH GC- AND LC-MS/MS METHOD DEVELOPMENT. Joëlle Widart, Kim B. Nguyen, Christelle Deleuze, Laetitia Heudt, Catherine Pirard, Eric Haubruge, Jef Focant, Edwin De Pauw O-34. DEVELOPMENT OF A RAPID AND SENSITIVE SPME-GC-ECD METHOD FOR THE DETERMINATION OF POLYCHLORINATED BIPHENYLS IN WATER Katerina TSIMELI, Dimitra DIMOTIKALI , Anastasia HISKIA

SESSION 3

ENVIRONMENTAL EFFECTS, TOXICITY AND RISK O-35. THE ROLE OF EFSA’S SCIENTIFIC PPR PANEL IN PESTICIDE RISK ASSESSMENT Christine Fuell O-36. MEASURING BIOAVAILABLE CONCENTRATIONS OF PESTICIDES IN AQUATIC ENVIRONMENTS Jay Gan, Svetlana Bondarenko, Weichun Yang, Wesley Hunter, and Frank Spurlock O-37. QUANTITATIVE DETERMINATION OF THE INFLUENCE OF ADJUVANTS ON FUNGICIDE RESIDUES Bert Ryckaert, Pieter Spanoghe, Geert Haesaert, Betty Heremans, Sofie Isebaert and Walter Steurbaut O-38. QUANTIFICATION OF TOXICITY USING BIOLUMINESCENT BACTERIA AND AN INSTANT FILM CAMERA Fernando Rubio, Meagan Mcginley, Daniel Rubio

O-39. MONITORING OF PESTICIDES AND HEAVY METALS IN THE WESTERN DESERT LAKES OF EGYPT AND BIOASSAYING POTENTIAL TOXICITY OF THEIR WATERS Sameeh A. Mansour O-40. PBT CHARACTERISTICS AND RISK OF LIPID REGULATORS IN THE ENVIRONMENT Mª Dolores Hernando, Amadeo R. Fernández-Alba O-41. THE ATTEMPT OF MATHEMATICAL SIMULATION OF DIOXIN-INDUCED TOXIC EFFECTS ON RED BLOOD CELLS Anatoly G. Davidovsky

O-42. THE EFFECTS OF SUB- CHRONIC EXPOSURE OF RATS TO HERBICIDE (GLYPHOSATE – ROUNDUP) Sinan Cağlar and Dürdane Kolankaya O-43. STUDIES ON THE RESPONSE OF SOIL MICROFLORA TO THE APPLICATION OF FUNGICIDE FENHEXAMID Daniela Borzi, Cristina Abbate, Fabrice Martin-Laurent; and Mara Gennari

SESSION 4

PROTECTION AND RESTORATION TECHNIQUES O-44. PHOTOCATALYTIC OXIDATION OF DIMETHACHLOR HERBICIDE OVER POLYETHYLENE GLYCOL (PEG)-METAL-MODIFIED TIO2 PHOTOCATALYSTS. V. Belessi, D. Lambropoulou, I. Konstantinou, V. Tzitzios, T. Albanis O-45. NEW ASSESSMENT OF DEGRADATION METHODS FOR MICROPOLLUTANTS: SEVERAL ALTERNATIVES FOR IMAZETHAPYR DETOXIFICATION. Ioannis Stathis, Dimitra Hela, Laura Scrano, Filomena Lelario and Sabino A. Bufo O-46. APPLICATION OF FENTON OXIDATION FOR THE DEGRADATION OF ATRAZINE AND FENITROTHION IN AQUATIC SOLUTIONS M. Constantinou, N. Varnava, A. E. Papadopoulos, D. Fatta O-47. PHOTOCATALYTIC OXIDATION OF MOLINATE IN AQUEOUS SOLUTIONS Erasmia A. Bizani, Konstantinos K. Fytianos, Ioannis Poulios O-48. OPTIMIZATION OF BIOREMEDIATION SYSTEMS FOR THE PROCESSING OF SPRAY LOSSES OF PESTICIDES Tineke De Wilde, Pieter Spanoghe, Walter Steurbaut, Dirk Springael, Jaak Ryckeboer and Peter Jaeken O-49. ODOR and CORROSION CONTROL IN WASTEWATER TREATMENT PLANTS: H2S PHOTOCATALYTIC DESTRUCTION BY UV-RADIATION Raquel Portela, Benigno Sánchez, Juan M. Coronado and Silvia Suárez

SESSION 1

OCCURRENCE AND FATE OF PESTICIDES AND OTHER MICROCONTAMINANTS IN THE ENVIRONMENT

P-1. CONTAMINATION OF GROUND WATER SOURCES BY ORGANOCHLORINE INSECTICIDES IN AYDIN, TURKEY. Cafer Turgut, Cengiz Gokbulut. P-2. CHARACTERIZATION OF THE FATE AND TRANSPORT OF HERBICIDES USING SWAT, A WATERSHED MODEL, IN THE BOGUE PHALIA BASIN, NORTHWESTERN MISSISSIPPI, USA Richard H. Coupe. P-3. TRANSPORT AND DEGRADATION OF GLYPHOSATE IN A MIDWESTERN TILE-DRAINED WATERSHED, SUGAR CREEK, INDIANA. Michael T. Meyer, Jeffrey W. Frey, Edward Lee, Kathryn Kuivila, and Elisabeth A. Scribner. P-4 THE ENVIRONMENT "PROTECT" BY THE BEES. HONEYBEES - BIOLOGICAL INDICATORS. Cristina Toca, Elisabeta Bianu, Daniela Nica. P-5 CLIMATIC EFFECTS ON LEACHING OF GLYPHOSATE IN NORWAY. Marit Almvik, Marianne Stenrød, Ole Martin Eklo, Randi I. Bolli, Espen Haugland, Jens Kværner, Tore Sveistrup, Christophe Moni. P-6 EFFECT OF SOIL PH ON CHANGES OF ENANTIOMERIC FRACTION OF MECOPROP AND PCB ATROPOISOMERS. Michal Oravec, Zdeněk Šimek P-7 THE DETERMINATION OF FENTHION RESIDUES IN FENTHION METAL CONTAINERS AFTER TRIPLE RINSING. Helen Karasali, Helen Anagnostopoulos and Ada Hourdakis P-8 FATE AND TRANSPORT OF GLYPHOSATE AND ITS DEGRADATION PRODUCT, AMINOMETHYLPHOSPHONIC ACID (AMPA), IN A TILE-DRAINED WATERSHED AND REGIONAL OCCURRENCE IN STREAMS. Elisabeth A. Scribner, Michael T. Meyer, Jeffrey W. Frey, and William A. Battaglin. P-9 EVALUATION OF INSECTICIDE ACTIVITY OF NEEM SEED WATER EXTRACT. Carlotta Maria Boursier, Domenico Bosco, Amadou Coulibaly, Michèle Nègre. P-10 RESIDUES OF INSECT GROWTH REGULATORS IN FRESH AND CANNED SATSUMA MANDARIN. Paula Payá, José Oliva, Alberto Barba and Miguel Ángel Cámara. P-11 FATE OF METHYL PARATHION IN NATURAL WATERS: STUDIES OF PHOTOLYSIS PROCESSES UNDER SOLAR LIGHT. Thiago M. R. De Araújo, Mariana N.N.Campos and Maria Cristina Canela. P-12 PHOTOCHEMICAL BEHAVIOR OF ZINC PYRITIONE: DEGRADATION KINETICS AND BYPRODUCT IDENTIFICATION. V.A. Sakkas, K. Shibata, Y. Yamaguchi, S. Sugasawa, T. Albanis. P-13 DISSIPATION OF FENOXYCARB AND PYRIPROXYFEN IN FIELD AND CANNING OF APRICOTS. Paula Payá, José Oliva, Alberto Barba and Miguel Ángel Cámara. P-14 OCCURRENCE OF ENDOCRINE DISRUPTORS IN WASTEWATER TREATMENT SYSTEMS OF GREECE. Athanasios S. Stasinakis, Georgia Gatidou, Nikolaos S. Thomaidis, Daniel Mamais and Themistokles D. Lekka.

P-15 THE DISSIPATION OF IMIDACLOPRID IN A CLOSED HYDROPONIC CULTIVATION SYSTEM. Dimitra Hela, Aikaterini Papavasiliou, Dimitrios Savvas, George Patakioutas and Vasilios Triantafyllidis. P-16 SOIL MOBILITY AND DISSIPATION OF MEFONOXAM AND PENDIMETHALIN IN SOIL COLUMNS TILLED WITH TOBACCO AND UNTILLED UNDER FIELD CONDITIONS. Vasilios Triantafyllidis, Dimitra Hela, Dimitrios Bilalis, George Salachas and Triantafyllos Albanis. P-17 LEVELS OF TRACE ORGANIC CONTAMINANTS AND THEIR ECOTOXICOLOGICAL IMPLICATION IN WATER AND SEDIMENTS FROM AMVRAKIKOS GULF COASTAL LAGOONS. V. Selimi, D. Barelos, T. Sakellarides, I.Konstantinou, D. Lambropoulou, T.Albanis. P-18 FATE OF DIURON AND TERBUTHYLAZINE IN SOILS AMENDED WITH AN ORGANIC RESIDUE FROM OLIVE OIL PRODUCTION INDUSTRY. Alegria Cabrera, Pilar Velarde, Lucía Cox, Juan Cornejo and William C. Koskinen. P-19 RESIDUES OF IMIDACLOPRID IN A BEAN CROP GROWN, AFTER ITS APPLICATION TO THE NUTRIENT SOLUTION, IN A CLOSED HYDROPONIC SYSTEM. George Patakioutas, Anna Karra, George Manos, Dimitrios Savvas, Theofanis Sakellaridis and Triantafyllos Albanis. P-20 OCCURRENCE OF INORGANIC AGRICULTURE POLLUTANTS IN AMBRAKIKOS GULF IN GREECE. George Karras, Vasilios Panis, Elias Kazos, George Gizas, Dimitrios Savvas, Anna Karra, Thomas Simos. P-21 RESIDUES OF NEMATICIDE FOSTHIAZATE IN LEAVES AND FRUIT OF TOMATO PLANTS. Konstantinos Liapis and Nikolaos G. Tsiropoulos. P-22 ORGANOCHLORINE PESTICIDES RESIDUES IN THE ENVIRONMENT OF PAGASSITIKOS GULF, CENTRAL GREECE. Nikolaos G. Tsiropoulos, Evangelia Golia, Panagiota Kanna and Irini Tatsi. P-23 USE SEQUENTIAL EXTRACTION FOR DETERMINATION OF ORGANIC AND INORGANIC FRACTIONS OF HEAVY METALS IN AGRICULTURAL SOILS, IN THESSALY (CENTRAL GREECE). Evangelia E. Golia, Anthoula Dimirkou, Nikolaos G. Tsiropoulos and Ioannis Mitsios. P-24 PESTICIDE LEVEL IN THE STREAMS THAT FLOW THROUGH MONTEVIDEO. Joaquín González, María Verónica Cesio, Gabriel González, Lucia Pareja, Horacio Heinzen. P-25 AXIOS RIVER POLLUTION. PART II: THE POLYCHLORINATED BIPHENYLS AND THE HEAVY METALS. Triantafyllos Albanis, Fokion Vosniakos, Kostas Nikolaou, Mihail Kochubovski, Dragan Gjorgjef, Blagoja Aleksoski, Dimitra Lambropoulou, Kostas Zavlaris and Presvia Selimi. P-26 DDT AND ITS METABOLITES IN DAIRY MILK AND MILK PRODUCTS OF AGRA CITY INDIA: A MONITORING STUDY. Anoop Kumar and P.E.Joseph. P-27 STUDY OF THE INFLUENCE OF SAMPLE PRETREATMENT AND STORAGE CONDITIONS IN THE STABILITY OF PYRETHROIDS IN WATER. Carmen Garcia-Jares, María Llompart, Vanessa Casas, Rafael Cela, María García-Chao, and Thierry Dagnac. P-28 SOIL DATA LIMITS THE PREDICTION OF CONTRIBUTING AREAS FOR DIFFUSE HERBICIDE LOSSES TO SURFACE WATERS. Martin Frey, Christian Stamm, Peter Reichert and Heinz Singer P-29 INFLUENCE OF HARVESTING METHOD AND WASHING ON THE PRESENCE OF PESTICIDE RESIDUES IN OLIVES AND OLIVE OIL. María Guardia Rubio, Antonio Ruiz Medina, Rosa Mª. Marchal López, Antonio Molina Díaz, Mª Luisa Fernández De Córdova, Mª. Isabel Pascual Reguera; and Mª. José Ayora Cañada.

P-30 EFFECT OF WASHING ON PESTICIDE RESIDUES IN OLIVES. María Guardia Rubio, Antonio Ruiz Medina, Rosa Mª. Marchal López, Antonio Molina Díaz, Mª Luisa Fernández De Córdova, Mª. Isabel Pascual Reguera; and Mª. José Ayora Cañada. P-31 NEW SIMPLE CONCEPT FOR DETERMINATION OF VOLATILIZATION AND SECONDARY DEPOSITION OF PESTICIDES

Niels Henrik Spliid, Anette Ravn Jensen, Kirsten Heinrichson P-32 DETERMINATION OF 1,4-DICHLOROBENZENE IN GREEK HONEYS BY HIGH PERFORMANCE LIQUID CHROMATOGRAPHY WITH COMBINED ULTRAVIOLET AND FLUORESCENCE DETECTION. E.K. Paleologos, S.S. Giannakopoulos and M.G. Kontominas.

SESSION 2

ANALYTICAL TECHNIQUES APPLIED TO ENVIRONMENTAL AND FOOD ANALYSIS P-33 DETERMINATION OF COPPER, CHROMIUM AND BORON BY ULTRASOUND ASSISTED EXTRACTION IN SOIL AND BIOCIDE TREATED WOOD. Ana I. García-Valcárcel and José L. Tadeo P-34 PRODUCTION OF ANTIBODIES FROM CHICKEN EGG-YOLK TO PHENYL-N-METHYLCARBAMATE INSECTICIDES FOR ANALYTICAL PURPOSES. Konstantinos P. Prousalis, Theodore Tsegenidis. P-35 SOLID-PHASE MICROEXTRACTION (SPME) FOR THE DETERMINATION OF BENZOYLUREAS IN ORANGE JUICE USING LIQUID CHROMATOGRAPHY. Ahmed R. Mughari, P. Parrilla Vázquez, M. Martínez Galera. P-36 APPLICATION OF SOLID-PHASE MICROEXTRACTION (SPME) TO DETERMINE PYRETHROIDS IN GROUND WATER USING LIQUID CHROMATOGRAPHY. Ahmed R. Mughari, P. Parrilla Vázquez, M. Martínez Galera. P-37 ANALYSIS OF PHENYLUREA AND PROPANIL HERBICIDES BY SOLID-PHASE MICROEXTRACTION AND LIQUID CHROMATOGRAPHY COMBINED WITH POST-COLUMN PHOTOCHEMICALLY INDUCED FLUORIMETRY DERIVATIZATION AND FLUORESCENCE DETECTION. P. Parrilla Vázquez, Ahmed R. Mughari, M. Martínez Galera. P-38 ANALYSIS OF TRACE LEVELS OF PESTICIDES IN RAINWATER BY SPME AND GC-TANDEM MASS SPECTROMETRY AFTER DERIVATIZATION WITH PFFBR. Anne Scheyer, Olivier Briand, Stéphane Morville, Philippe Mirabel and Maurice Millet. P-39 SIMULTANEOUS EXTRACTION AND DETERMINATION OF DI-(2-ETHYL-HEXYL)-PHTHALATE, NONYLPHENOL, NONYLPHENOL ETHOXYLATES AND POLYCHLORINATED BIPHENYLS IN SLUDGE FROM WASTEWATER TREATMENT PLANTS BY SONICATION-ASSISTED EXTRACTION AND GAS CHROMATOGRAPHY-MASS SPECTROMETRY. METHOD APPLICATION Esteban Alonso, Irene Aparicio and Juan Luis Santos. P-40 SIMULTANEOUS EXTRACTION AND DETERMINATION OF LINEAR ALKYLBENZENE SULPHONATES AND POLYCYCLIC AROMATIC HYDROCARBONS IN SLUDGE FROM WASTEWATER TREATMENT PLANTS BY SONICATION-ASSISTED EXTRACTION AND LIQUID CHROMATOGRAPHY WITH FLUORIMETRIC DETECTION. Esteban Alonso, Irene Aparicio, Juan Luis Santos, Carmen Trigo and Juan Romero. P-41 MULTIRESIDUE ANALYSIS OF FORTY FIVE PESTICIDES IN FRUITS AND VEGETABLES BY HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY/TANDEM MASS SPECTROMETRY. Martin Dušek, Petr Cuhra, Sona Baršová and Kateřina Maštovská. P-42 DEVELOPMENT OF A SENSITIVE MAGNETIC PARTICLE IMMUNOASSAY FOR PERMETHRIN AND ITS METABOLITE 3-PBA. Fernando Rubio, Carmen D. Parrotta, Lisa Kamp, Jennifer Church, Richard Slawecki, and Larry Stanker. P-43 VARIOUS GC–MS APPROACHES TO RESIDUE ANALYSIS OF FOOD CONTAMINANTS. Tomas Cajka, Jana Hajslova

P-44 OPTIMIZATION OF A SIMPLE AND SENSITIVE METHOD FOR THE DETERMINATION OF ORGANOPHOSPHORUS PESTICIDES IN MILK BY MEANS OF HEADSPACE SOLID-PHASE MICROEXTRACTION (HS-SPME) AND GAS CHROMATOGRAPHY. Charoula S. Tsoutsi, Ioannis K. Konstantinou, Dimitra G. Hela and Triantafyllos A. Albanis. P-45 DEVELOPMENT OF A METHOD FOR DETERMINING PESTICIDE RESIDUES IN FOOD BY LC-MS/MS: ADVANTAGES AND DISADVANTAGES Carla Soler, Brett Hamilton, Ambrose Furey, Kevin J. James, Jordi Mañes and Yolanda Picó. P-46 ESTIMATION ROUTINES FOR LINEAR REGRESSION BY THE LEAST SQUARE METHOD IN PESTICIDE RESIDUE DETERMINATION IN FOOD. Cristina Blasco, Imre Varga, Guillermina Font, Kornelia Kozmutza, Yolanda Pico.. P-47 MSPD FOLLOWED BY LC-MS/MS AS A NOVEL TOOL FOR THE ANALYSIS OF PESTICIDE RESIDUES IN FOOD. Carla Soler, Cristina Blasco, Guillermina Font; and Yolanda Pico. P-48 ALKYLBENZENE SULFONATES RISK ASSESSMENT: MONITORING OF LONG-CHAIN INTERMEDIATE PRODUCTS. Emilia Ferrer, Guillermina Font, Rossella Mello; Elena Gonzalez, Vicente Andreu and Yolanda Pico. P-49 QUANTIFICATION OF FLUOROQUINOLONES IN SOIL BY PRESSURIZED LIQUID EXTRACTION AND LIQUID CHROMATOGRAPHY TANDEM MASS-SPECTROMETRY. Vicente Andreu, José Luís Rubio, Emilia Ferrer, Yolanda Pico. P-50 SOLID PHASE EXTRACTION AND DETERMINATION OF CHLOROPHACINONE IN COMMERCIAL RODENTICIDE, CORN GRAINS, SOIL AND RATE SERUM BY LIQUID CHROMATOGRAPHY. Moulay-Hassane Guermouche P-51 MULTIRESIDUE METHOD FOR THE ANALYSIS OF 156 PESTICIDE RESIDUES IN STRAWBERRY Patricia Plaza-Bolaños, José Luis Fernández- Moreno, Roberto Romero-González, Antonia Garrido-Frenich, José Luis Martínez-Vidal, Manuel Mateu-Sánchez and F. Javier Arrebola Liébanas. P-52 DETERMINATION OF ORGANOCHLORINE PESTICIDES AND POLYCHLORINATED BIPHENYLS IN SOILS BASED ON GAS-CHROMATOGRAPHY-TRIPLE QUADRUPOLE DETECTION. Antonia Garrido-Frenich, José Luis Martínez-Vidal, María Ángeles Escobar-García, Inmaculada Arjona-Ruzafa, Roberto Romero-González. P-53 DETERMINATION OF POPS IN AMBIENT AIR. Roberto Romero-González, María A. Escobar-García, Inmaculada Arjona-Ruzafa, José L. Martinez-Vidal, Antonia Garrido-Frenich and Francisco J. Egea-González. P-54 MULTIRESIDUE HIGH PERFORMANCE LIQUID CHROMATOGRAPHIC DETERMINATION OF PESTICIDES IN WATERS. G. Kalampoki, D. Lambropoulou, T.Albanis. P-55 COMPARISON OF DIFFERENT SORBENTS FOR MULTIRESIDUE SOLID-PHASE EXTRACTION OF 9 PHARMACEUTICALS IN SURFACE AND WASTEWATER SAMPLES. C. Kosma, D. Lambropoulou, T. Albanis. P-56 COMPARISON OF DIFFERENT KINDS OF SORBENTS FOR THE SOLID-PHASE EXTRACTION TO OPTIMIZATION PROCEDURE OF DETERMINATION OF PESTICIDES IN WATER. Tomasz Tuzimski P-57 FRACTIONATION OF MULTICOMPONENT MIXTURES OF PESTICIDES BY ZONAL MICROPREPARATIVE PLANAR CHROMATOGRAPHY WITH DIODE ARRAY SCANNING DENSITOMETRY TO THEIR DETERMINATION IN WATER. Tomasz Tuzimski. P-58 A NEW PROCEDURE FOR THE SEPARATION OF COMPLEX MIXTURES OF PESTICIDES BY MULTIDIMENSIONAL PLANAR CHROMATOGRAPHY. Tomasz Tuzimski.

P-59 SEPARATION OF MIXTURES OF PESTICIDES BY PRESSURIZED PLANAR ELECTROCHROMATOGRAPHY. Tomasz Tuzimski, Piotr Boguta, Tadeusz H. Dzido. P-60 DEVELOPMENT AND STATISTICAL VALIDATION OF A QUANTITATIVE METHOD FOR THE DETERMINATION OF STEROID HORMONES IN WATER USING SOLID-PHASE EXTRACTION FOLLOWED BY LIQUID CHROMATOGRAPHY - TANDEM MASS SPECTROMETRY. Christophe Stavrakakis, Ronan Colin, Valérie Hequet, Catherine Faur, and Pierre Le Cloirec. P-61 DETERMINATION OF DOMOIC ACID BY HIGH PERFORMANCE LIQUID CHROMATOGRAPHY. Insaf Darmane, Bouchra. Touil and Rachid Bengueddour P-62 ANALYSIS OF PESTICIDE RESIDUES IN FRUITS USING LIQUID CHROMATOGRAPHY WITH ELECTROSPRAY TANDEM MASS SPECTROMETRY Seshaiah Kalluru and Min-Chao Wang. P-63 DETERMINATION OF NON-POLAR POLLUTANTS IN MARINE ENVIRONMENTAL USING SEMIPERMEABLE MEMBRANE DEVICES (SPMD) AND GC-MS FOR QUALITY CONTROL STRATEGY IN SEA FARMS. M.J. Martínez Bueno, M.D. Hernando O. Malato and A.R. Fernández-Alba P-64 USE OF POLAR ORGANIC COMPOUNDS INTEGRATIVE SAMPLER (POCIS) AND LC-MS/MS FOR THE MONITORING OF CHEMOTHERAPEUTANTS AND PESTICIDES IN FISH FARM CAGE SYSTEMS. M.J. Martínez Bueno, M.D. Hernando and A.R. Fernández-Alba. P-65 NEW METHODS BASED ON TWO DIFFERENT EXTRACTION STRATEGIES TO DETERMINE PYRETHROIDS IN INDOOR AIR. Ruth Barro, María Llompart, Carmen García-Jares, Rafael Cela and Thierry Dagnac. P-66 DETERMINATION OF POLYBROMINATED DIPHENYL ETHERS IN DOMESTIC DUST BY MICROWAVE-ASSISTED SOLVENT EXTRACTION AND GAS CHROMATOGRAPHY IN TANDEM MASS SPECTROMETRY . Jorge Regueiro, Thierry Dagnac, María Llompart, Carmen García-Jares, Rafael Cela. P-67 IDENTIFICATION OF PESTICIDE METABOLITES IN ENVIRONMENTAL WATER SAMPLES WITH A LTQ ORBITRAP HYBRID MASS SPECTROMETER. Heinz Singer, Kathrin Fenner, Juliane Hollender. P-68 QUANTIFICATION OF GLYPHOSATE AND AMINOMETHYLPHOSPHONIC ACID IN WATER USING SOLID PHASE EXTRACTION-LIQUID CHROMATOGRAPHY-TANDEM MASS SPECTROMETRY (SPE-LC-MS/MS). Irene Hanke, Heinz Singer, Juliane Hollender. P-69 PURGE AND TRAP GAS CHROMATOGRAPHY METHOD FOR THE EVALUATION OF THE QUALITY FLAVOUR OF TOMATOS. Yolanda Cortés, Milagros Mezcua, Maria José Gómez, Paula Medina, Amadeo R. Fernández-Alba and Mariano Contreras.

P-70 ASSESSING SUPERCRITICAL FLUID EXTRACTION FOR THE ANALYSIS OF FIPRONIL, KRESOXIM-METHYL, ACRINATRIN, AND PYRIDABEN RESIDUES IN MELON. Mourad Boulaid, Ana Aguilera, Valentina Busonera, Francisco Camacho, Antonio Valverde. P-71 MINI SOIL COLUMN TEST - A HIGH THROUGHPUT METHODOLOGY FOR SOIL MOBILITY TEST. Zhaoqiang Li, Stuart Watson and Dave Pearson. P-72 RELIABLE IDENTIFICATION OF PESTICIDES BY QUADRUPOLE MASS SPECTROMETRY AND LINEAR RETENTION INDICES Alessandro Casilli, Ennio Bellotti, Rino Calori, Roberto Ferrari, Luigi Mondello. P-73 DETERMINATION OF AZOXYSTROBIN RESIDUES IN GRAPES, MUSTS AND WINES WITH A MULTICOMMUTATED FLOW-THROUGH OPTOSENSOR IMPLEMENTED WITH PHOTOCHEMICALLY INDUCED FLUORESCENCE.

Javier López-Flores, María Luisa Fernández-De Córdova, Antonio Molina-Díaz. P-74 FLOW-THROUGH OPTOSENSING AS AN INTERESTING TOOL FOR THE ANALYSIS OF PESTICIDES IN ENVIRONMENTAL WATERS. Eulogio J. Llorent-Martínez, Juan F. García-Reyes, Bienvenida Gilbert-López, Pilar Ortega Barrales; and Antonio Molina-Díaz. P-75 IMPLEMENTATION OF MULTICOMMUTATION IN SOLID PHASE SPECTROSCOPY: A USEFUL APPROACH FOR THE DETERMINATION OF PESTICIDES IN FOOD. Eulogio J. Llorent-Martínez, Juan F. García-Reyes, Bienvenida Gilbert-López, Pilar Ortega Barrales and Antonio Molina-Díaz. P-76 DETERMINATION DETECTION OF PHOTOIRRADIATED BENZOYLUREAS BY HPLC WITH LUMINOL CHEMILUMINESCENCE DETECTION. APLICATION FOR DETERMINATION ON VEGETABLES. Rosario Santiago Valverde, María Martínez Galera and M. Dolores Gil García. P-77 SIMPLE, RAPID SOLID-PHASE EXTRACTION FOR THE DETERMINATION OF ULTRA-TRACE LEVELS OF PYRETHROIDS IN GROUND AND SEA WATER BY LC/ESI/MS. Rosario Santiago Valverde, M. Dolores Gil García, Dolores Barranco Martínez, María Martínez Galera and Piedad Parrilla Vázquez. P-78 LC/MS-MS ANALYSIS AND RESIDUAL BEHAVIOUR OF FORCHLORFENURON (CPPU) IN WATERMELON AND ZUCCHINI. Antonio Valverde, Luis Piedra, Ana Aguilera, Mourad Boulaid, Francisco Camacho. P-79 DETERMINATION OF PESTICIDES AND PCB`S IN POWDERED MILK INFANT FORMULA BY PRESSURIZED LIQUID EXTRACTION USING FAT RETAINER MATERIAL, FOLLOWED BY GAS CHROMATOGRAPHY-TANDEM MASS SPECTROMETRY. M. Mezcua, M.R. Repetti, H. R. Beldoménico, C. Ferrer and A. R. Fernández-Alba. P-80 SIMULTANEOUS ANALYSIS OF NEUTRAL AND ACIDIC PHARMACEUTICALS AND OTHER ORGANIC COMPOUNDS BY GAS CHROMATOGRAPHY-TANDEM MASS SPECTROMETRY IN WASTEWATER. M.J. Gómez, M.Mezcua, O. Malato, A. Agüera, A.R. Fernández-Alba.

SESSION 3

ENVIRONMENTAL EFFECTS, TOXICITY AND RISK P-81 SOLID PHASE MICROEXTRACTION (SPME) MEASUREMENT OF PYRETHROIDS IN SEDIMENT POREWATER. Jay Gan, Svetlana Bondarenko and Frank Spurlock P-82 HEMATOLOGIC, BIOCHEMICAL AND HISTOPATHOLOGIC EFFECTS OF THE KIDNEY, LIVER AND SPLEEN OF ADULT MALE RATS EXPOSED MATERNALLY TO 4-TERT-OCTYLPHENOL. Müfide Aydoğan, Nurhayat Barlas P-83 TESTING AND COMPARISON OF THREE PESTICIDE RISK INDICATOR MODELS UNDER NORWEGIAN CONDITIONS; A CASE STUDY IN THE SKUTERUD AND HEIABEKKEN CATCHMENTS. Marianne Stenrød, Heidi E. Heggen, Randi I. Bolli, Ole Martin Eklo. P-84 FUNGICIDES (LOW AND HIGH CONCENTRATIONS) EFFECTS ON INDICATORS BACTERIA ANTIBIOTIC RESISTANCE. Dimitra S. Dimou, Alexandra Koutsotoli, Triantafyllos Albanis, Yannis Alamanos, Vasiliki Maipa.. P-85 OXIDATIVE DAMAGES IN CHO-K1 CELLS TREATED WITH PESTICIDES. María José Ruiz, Guillermina Font, Yolanda Picó and Mónica Fernández. P-86 THE VALUE OF OUTDOOR MICROCOSM STUDIES IN AQUATIC RISK ASSESSMENT AND REGULATION OF CROP PROTECTION PRODUCT USE. Jackie Webb and Laurence Hand.

P-87 EPTC EFFECTS ON ESCHERICHIA COLI AND ENTEROCOCCUS FAECALIS. Alexandra D. Koutsotoli, Triantafyllos A. Albanis, Dimitra S. Dimou, Yannis P. Alamanos, Vassiliki E. Maipa P-88 DETERMINATION ON ACHE ACTIVITY IN BRAIN OF RUTILUS FRISI AND CYPRINUS CARPIO AS A HEALTH INDEX. Mohammad A. Ebrahimzadeh, Mahshad Bioukabadi, Mohammad Karami P-89 ANALYTICAL METHODS FOR RISK EVALUATION OF PESTICIDE CHLORDECONE IN FOOD FROM MARTINIQUE AND GUADELOUPE. François Bordet, Audrey Thieffinne, Dary Inthavong. P-90 IN VIVO AND IN VITRO DNA DAMAGING EFFECTS OF PESTICIDES IN HUMAN PERIPHERAL LYMPHOCYTES. Ülkü Ündeğer, Nurşen Başaran. P-91 UPTAKE AND ACCUMULATION OF DDT AND ITS METABOLITES IN FOOD AND FORAGE PLANTS. Hans Martin Hanslin, Hans Overgaard, Trine Eggen.

SESSION 4

PROTECTION AND RESTORATION TECHNIQUES P-92 UTILIZING VEGETATIVE BUFFER STRIPS TO REMOVE DISSOLVED AND SEDIMENT-BOUND ATRAZINE, METOLACHLOR, AND GLYPHOSATE FROM SURFACE RUNOFF. C. H. Lin, R. N. Lerch, H. E. Garrett, C. J. Gantzer, S.H. Anderson, and M. F. George. P-93 EFFECT OF SOIL SOLARIZATION ON THE DEGRADATION OF BUPROFEZIN, BROMOPROPYLATE, DICOFOL AND TETRADIFON IN A PEPPER CULTIVATION UNDER GREENHOUSE. José Fenoll, Alfredo Lacasa, Pilar Hellín, Pilar Flores, Marcos Ruíz, María V. Molina, Joaquin Navarro and Marta Miguel. P-94 DEGRADATION RATES OF S-TRIAZINE HERBICIDES IN WASTEWATER BY PHOTOCATALYSIS WITH ZnO UNDER NATURAL SUNLIGHT. Nuria Vela, Gabriel Pérez, Ginés Navarro, Misael Rangel, and Simón Navarro. P-95 EFFECT OF SOIL SOLARIZATION ON THE RATE OF LOSS OF TERBUTHYLAZINE AND ISOPROTURON. Simón Navarro, Salvador Bermejo, Nuria Vela, and Joaquín Hernández. P-96 PHOTOCATALYSIS OF ALACHLOR AND PROPANIL IN DRINKING WATER BY PHOTO-FENTON REACTION UNDER NATURAL SUNLIGHT IRRADIATION. Nuria Vela, Gabriel Pérez, Ginés Navarro, Luis Mena and Simón Navarro. P-97 REMOVAL OF INSECTICIDE AND HERBICIDE RESIDUES FROM DRINKING WATER BY USE OF FINING AND FILTER AGENTS. Nuria Vela, Gabriel Pérez, Ginés Navarro, Luis Mena and Simón Navarro. P-98 DIRECT AND INDIRECT PHOTOLYSIS OF CYHALOFOP IN WATER. Maria V. Pinna, Ilaria Braschi, Carlo E. Gessa and Alba Pusino. P-99 A FIRST APPROACH TO THE DEVELOPMENT OF AN ENVIRONMENTALLY FRIENDLY METHODOLOGY FOR THE DESTRUCTION OF PERSISTENT ORGANIC POLLUTANTS USING ENDOSULFAN AS MODEL. María Verónica Cesio, Sebastián De Paula, Gabriel González, Joaquín González, Lucia Pareja, Soledad Méndez, Rodrigo Díaz, Anisleidy Rivero-Machado, Alvaro Vázquez, Horacio Heinzen, Matilde Soubes, Maria Pía Cerdeiras. P-100 ORGANOHYDROTALCITES AS SUPPORTS FOR THE SLOW RELEASE OF THE HERBICIDES CARBETAMIDE AND METAMITRON. F. Bruna, R. Celis, C. Barriga, I. Pavlovic, M. A. Ulibarri, M. C. Hermosín, and J. Cornejo.

P-101 MINERALIZATION OF EMERGENT CONTAMINANTS BY O3/H2O2 SYSTEM. Antonio Rodriguez, Teresa Varela, Elvira Torrijos, Roberto Rosal, Jose A. Perdigon, Eloy García-Calvo, Amadeo R. Fernandez-Alba. P-102 ALLELOCHEMICALS – INCREDIBLE SOURCE OFFERING PESTICIDE ANALOGUES FOR ENVIRONMENTALLY SAFE FUTURE. Tehmina Anjum and Rukhsana Bajwa. P-103 PHOTOCHEMICAL STUDIES OF PYRETHROID INSECTICIDES BASED ON PHOTO-SPME. PART I: DIHALOGENOVINYL-SUBSTITUTED PYRETHROIDS. María Fernández-Álvarez, Marta Lores, María Llompart, Lucía Sánchez-Prado, Carmen García-Jares, Rafael Cela and Thierry Dagnac. P-104 PHOTOCHEMICAL STUDIES OF PYRETHROID INSECTICIDES BASED ON PHOTO-SPME. PART II: DOMESTIC-USE PYRETHROIDS. María Fernández-Álvarez, María Llompart, Marta Lores, Lucía Sánchez-Prado, Carmen García-Jares, Rafael Cela, and Thierry Dagnac. P-105 DESULFURIZATION OF DBT IN MODEL OIL BY RESTING CELL OF PSEUDOMONAS PUTIDA CETC5279. EFFECT OF OXYGEN. Raul Alonso Del Aguila, Karina Boltes, Pedro Leton, Antonio Rodríguez, Milagros Mezcua, Amadeo R. Fernández-Alba and Eloy Garcia-Calvo.. P-106 IMPACT OF BIOFUMIGATION WITH SOLARIZATION ON DEGRADATION OF PESTICIDES AND HEAVY METAL ACCUMULATION. Pilar Flores, Pilar Hellín, Alfredo Lacasa, Pedro Fernández and José Fenoll. P-107 DEGRADATION OF THE PHARMACEUTICAL ACTIVE INGREDIENT DIPYRONE IN WATER BY PHOTO-FENTON TREATMENT USING SOLAR ENERGY. ESTABLISHMENT OF THE DEGRADATION PATHWAY. Ana Agüera, Amadeo R. Fernández-Alba, Leónidas A. Pérez-Estrada and Sixto Malato.

P-108 PHOTODEGRADATION OF THE MALACHITE GREEN UNDER NATURAL SUNLIGHT. KINETICS AND TOXICITY OF THE DEGRADATION PRODUCTS. Leónidas A. Pérez-Estrada, Sixto Malato, Ana Agüera, M.D. Hernando and Amadeo R. Fernández-Alba. P-109 SELECTIVE MODIFICATION OF CLAY MINERALS FOR THE ADSORPTION OF HERBICIDES WIDELY USED IN OLIVE GROVES. Rafael Celis, Gracia Facenda, Carmen Trigo, Maria del Carmen Hermosín, and Juan Cornejo P-110 SORPTION AND PHOTODEGRADATION OF RIMSULFURON ON CYCLODEXTRIN AND ZEOLITE Angelica Liguori, Maurizio D’auria, Lucia Emanuele, Laura Scrano, Filomena T. Lelario and Sabino A. Bufo

LAST MINUTE POSTERS P-111 DETERMINATION OF PESTICIDE RESIDUES IN FRESH PEACHES PRODUCED IN THE REGION OF IMATHIA (GREECE) I. V. Zioris, T. G. Danis, D. T. Karagiozoglou, P.A. Pavlidis, T. A. Albanis. P-112 DEVELOPMENT OF AN ANALYTICAL METHOD FOR THE SIMULTANEOUS DETERMINATION OF TWO ANTIFOULING BOOSTER BIOCIDES AND THEIR DEGRADATION PRODUCTS IN BIOTA. Eleutheria Panagiotoglou, Georgia Gatidou, Nikolaos S. Thomaidis. P-113 SURVEY OF PAHs IN FOOD SAMPLES IN SOUTH SPAIN BY GC-MS/MS (IT) Milagros Mezcua, Yolanda Cortés, Carmen Ferrer, Paula Medina, Amadeo R. Fernández-Alba.

P-114 ESTROGENIC MICROENVIRONMENT GENERATED BY ORGANOCHLORINE RESIDUES IN ADIPOSE MAMMARY TISSUE MODULATES BIOMARKER EXPRESSION IN ERα–POSITIVE BREAST CARCINOMAS Mónica Muñoz-De-Toro, Milena Durando, Horacio R. Beldomenico, Pablo M. Beldomenico, Laura Kass, Silvia R. Garcia and Enrique H. Luque

P-115 DEVELOPMENT OF A MULTIRESIDUE PESTICIDE METHOD USING SHORT COLUMNS BY LC/MS/MS Carmen Ferrer, Mª Rosa Repetti, Maria Dolores Hernando, Imma Ferrer and Amadeo R. Fernández-Alba