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Transcript of Development of YAG:Dy Thermographic Phosphor … · Development of YAG:Dy Thermographic Phosphor...
Development of YAG:Dy Thermographic Phosphor Coatings for Turbine Engine Applications
J.I. Eldridge NASA Glenn Research Center
Cleveland,OH
T.P. Jenkins Metrolaser, Inc.
Irvine, CA
S.W. Allison Oak Ridge National Laboratory
Oak Ridge, TN
D. E. Wolfe Penn State University University Park, PA
E. H. Jordan University of Connecticut
Storrs, CT
58h International Instrumentation Symposium San Diego, CA June 5-8, 2012
N~.··· . . . , ... ~ '. . . . . -' ~.
https://ntrs.nasa.gov/search.jsp?R=20120016798 2018-08-30T08:33:01+00:00Z
AFRL Versatile Affordable Advanced Turbine Engines (VAATE) Project Gas Turbine Engine Sensor and Instrumentation Development
Project 1: TBC Health & Component Temperatures of Turbine Blades & Vanes
NASA GRC High-HeatFlux Laser Facility -Proof-of-concept with easy optical access, no radiative background, no probe heating issues.
Demonstrated to 1360°C . ./
Williams International Combustor Burner Rig -Address probe/TP survivability & ability to "see" through flame.
Demonstrated to >1400°C . ./
-Probe/translate through afterburner flame. -Opportunity to test excitation/collection integrated probe.
Goal: Demonstrate thermographic phosphor (TP) based temperature measurements to 1300°C on TP/TBC-coated HPT stator on Honeywell TECH7000 demonstrator engine.
Deca
y Ti
me
(µs)
Inte
nsity
(V)Basis for Selection of YAG:Dy
• Advantages of YAG:Dy (at least in powder form produced at high temperature) 1. Excellent temperature sensitivity from 1100° to 1700°C.
2. Higher upper temperature limit than other thermographic phosphors.
3. Short-wavelength emission at 456 nm reduces interference from background thermal radiation.
4. Nearly single exponential decay for simple, robust decay time determination.
Oe~~}' Time VS. Tern erature Calibration for YAG:Oy
100 +---------+--~---I
10 1--------~-~--1
o 200 400 600 800 1000 1200 1400 1600 1800
Temperature (0C)
Lu 11;1} n, e;....:s....;;.c....:...e _nc..:....e,-O_ e..:....c.:....;;a-",---C,-u,-rv_ e..:....s,-f;....:o_r_y'_'A....;;.G-,: Oy
Nearly monoexponential
- 15C
- 393C
- 590C
- 787C
0.01 ~_----------I
0.001 +----~~~~~----I
0.0001 +--------,-------,-------,----=:11.0.~
0.001 0.002 0.003 0.004
Time {sed
Decay Time vs. Temperature 10,000
1,000
100 -(/') :l. ----
10
1
0.1
0.01
° 400 800 1 ,200 1,600 2,000 Temperature (Kelvin)
But, will YAG:Dy coatings exhibit these desirable attributes because temperatures of coating processing restricted to much lower temperatures «1200°C) than powder processing?
Coating Deposition Methods Investigated
• Binder-Based Paint Application 1. Mixture of YAG:Dy powder and ZAP binder (ZYP Coatings, Oak Ridge, TN)
2. Air-brush or paint brush application.
3. Fire to produce coating consisiting of YAG:Dy powder particles in AIP04 matrix.
- Simple, fast, & inexpensive.
- Incorporates fully crystallized phosphor powder.
• Electron-Beam Physical Vapor Deposition (EB-PVD) - E-beam evaporation of YAG:Dy ingot at Penn State.
- Most compatible for in-line industrial thermal barrier coating (TBC) deposition.
- Excellent thickness control.
- Desirable microstructure.
• Solution Precursor Plasma-Spray (SPPS) - Injection of atomized solution into plasma jet.
- Low-cost alternative to EB-PVD and conventional plasma-spray.
- Easily tailorable composition.
ZAP YAG:Dy on Plasma-Sprayed YSZ
or
+
3hr @1000°C
Coating consists of YAG:Dy powder particles in aluminum phosphate matrix.
Inte
nsity
Multi-Ingot EB-PVD Chamber at Penn State
HV De! WD Mdg - ::'00f.Jm-::'00 kV S:-;D q q mm ",000)
® Guns • Thermocouple Ingots (Trans-Tech):
G-v • Airfoil -Undoped 7YSZ Crucibles + Ingots • Ion Source -YAG:Dy
~~ Oxygen Supply Path • Graphite heating plate
Inte
nsit
y
Effect of Heat Treatment on EB-PVD YAG:Dy
450
amorphous
YAP:Dy YAG:Dy
Time-Averaged Luminescence Emission Excitation at 355 nm
- no heat
- 24hr@1163C
- 2hr laser Ts = 1300C
-YAG:Dy slurry coating
• x XRD after 2hr I ser
•
10 20 30 40
28
470 490 510
Wavelength nm
so
Amorphous ~ YAP + a-A120 3 + 8-A120 3 ~ YAP + a-A120 3 (no YAG)
VAG is difficult to achieve due to non-congruent evaporation from ingot.
60
• YAP )( a-A1203
• t-YSZ
70 80
Inte
nsity
(V)
Inte
nsity
(V)
Inte
nsit
y
Effect of Heat Treatment on SPPS YAG:Dy
450
Time-Averaged Luminescence Emission 4F9/2 ~ 6H 15/2 Excitation at 355 nm
10
500 550 600
Wavelength nm
- no heat treat
-YAG:Dy slurry
XRD spps· 0 heat treat • YAG + YAP
• DYAM • t-YSZ
20 30 40 so 60
28
650 700
SPPS YAG:Dy coating exhibits desired YAG:Dy emission spectrum.
70 80
Inte
nsit
yIn
tens
ity
Inte
nsity
(V)
Inte
nsity
(V)
Inte
nsity
(V)
Inte
nsity
(V)
- 50ns, 1 Ous wide
- 1ms, 100us wide
470 475 480 485 490 495 500
Wavelength nm
Inte
nsity
(V)
Inte
nsity
(V)