Descriptive analysis1 Dominique Valentin ENSBANA/CESG Université de Bourgogne...
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Transcript of Descriptive analysis1 Dominique Valentin ENSBANA/CESG Université de Bourgogne...
Descriptive analysis 1
Descriptive analysisDominique Valentin
ENSBANA/CESGUniversité de [email protected]
Descriptive analysis 2
What is descriptive analysis ?
Descriptive analysis is used to describe the sensory characteristics of a product, and to use these characteristics to quantify differences between products
Sensory profile
radar
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When should we use descriptive analysis ?
Descriptiveanalysis
Packaging
R&D
Control quality
Marketing
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Quality control
Does this product match the target specification?
What variation in quality is to be expected?
What is the normal variation in each attributes
How long can this product be stored before the Sensory quality noticeably changes?
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Research & Development
What are my product perceived sensory characteristics ?
How can it be made more like the target profile?
Have the changes brought the product closer to the target?
If the recipe/process were changed, how would quality be affected
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Marketing and Packaging
What are the attributes of products already on the market?
What are the attributes of the most and least succesfull products?
What are the key attributes to meet consumers’Expectations?
Have the changes brought the product closer to the target?
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Why should we use descriptive analysis ?
Contrary to informal product tasting, descriptive analysis limits:
Bias Subjectivity Poor control of variablesUsing wrong assessorsPatchy information
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What sort of panel is required ?
Trained panel: more capable of describing the subtle differences between samples
2 types of trained panels:Internal: within the companyExternal: outside the company
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What type of methods should we use ?
Conventional Profiling (QDA® Stone et al, 1974)Marketed by the Tragon Corporation in the USA
Free Choice profiling (Williams and Langron, 1984)
Profil Flash (Siefferman, 2000)
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Conventional Profiling
4-step process:
1. Panel selection
2. Development of a lexicon for appearance, odor, flavor, texture, mouth feel and after-taste
3. Training
4. Ratings of the products
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Panel selection
Ability to detect differences in characteristics present and in their intensities Ability to describe characteristics using verbal descriptors and scaling methods Capacity for abstract reasoning Interest in participation and availability General good health
Prescreening questionnairesAcuity testsRanking/rating testsPersonal interview
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Example of prescreening questionnaire
Time:1) Are there any weekdays that you are not available on a regular basis2) How many weeks of vacation do you plan to take this year
Health:1) Do you have any of the following
Dentures Diabetes Oral or gum disease Hypoglycemia Food allergies Hypertension
2) Do you take any medications which affect your senses, especially taste and smell?
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Flavor, fragrance and texture quiz:
1) If a recipe calls for thyme and there is none available, what would you substitute?
2) What are some other food that taste like yogurt?
3) What is the best one- or two-word description of grated Italian cheese
4) Describe some noticeable flavors in cola
5) Describe some of the textural properties of foods in general
6) What are some textural properties of potato chips
7) Describe some of the noticeable smells in a bakery
Meilgaard, Civille & Carr (1999),Sensory evaluation techniques. CRC Press
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Exemples de tests de sélection: jury bières
Matching odors / names
Descripteurs Composes Concentration (mg/L)
Banane Acétate d’isoamyle 5Amande amère Benzaldéhyde 2Citron Citral 2Vanille Vanilline 20Beurre 2,3-butanédione 5Rose Géraniol 5Eau Eau distillé – Chou Sulfure de diméthyle 0,05Fleur d’oranger Linalol 5
Chollet, 2000
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Duo-trio test : • Control sample: Kronenbourg beer•Test sample: Heineken
Identification of 4 basic tastes
Descriptors Compound Concentration (g/l)
Sweet Sucrose 8Sour Citric Acid 1Bitter Caffein 0,5Astringent Aluminum Sulfate 0,5
Exemples de tests de sélection: jury bières
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Intensity ranking: sweet taste in beer
Sample Concentration (g/l)
1 02 53 104 15
Intensity ranking: Bitterness in beer
Beer Bitterness unit (EBU)
K 4Kronenbourg 151664 21Tradition allemande 28
Selection test example: beer panel
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Odor descriptionComposés Descripteurs Concentration (mg/l)
Camphre Camphre 1Phényl acétaldéhyde jacinthe, lilas 5Acide octanoique Caprique 50Trans-2-hexenol Herbe coupée, feuille vertes 50Hexanoate d’éthyle Pomme, fruité, sucré, anisé 5-Décanolactone Pêche, abricot, noix de coco 202,5-diméthylepyrazine Céréales 20Isobutyraldéhyde Banane, amande 100Salycylate de méthyle Pharmacie, pommade 100Carvone Menthe, chlorphylle 100
Exemples de tests de sélection: jury bières
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Examples of scaling exercises
Mark on the line at the right to indicate the proportion of the area that is shaded
None All
None All
None AllMeilgaard, Civille & Carr (1999),Sensory evaluation techniques. CRC Press
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If you want to know more:
Guidelines for the selection and training of sensory panel members ASTM special technical publication 758
Sensory analysis -- General guidance for the selection, training and monitoring of assessors -- Part 1: Selected assessors, ISO 8586-1:1993, Part 2: Experts, ISO 8586-2:1994
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Conventional Profiling
4-step process:
1. Panel selection
2. Development of a lexicon for appearance, odor, flavor, texture, mouth feel and after-taste
3. Training
4. Ratings of the products
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Development of a lexicon
Goal: Describe the product category completely without overlapping
Procedure: Word generation
Reduction of the list into a working list
Choice of referents and definitions for the descriptors
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1. Collect commercially available samples which represents as many as possible of the attribute differences likely to be encountered in the product category
2. Present 4 samples to the panelists and ask them to write down independantly as many terms as they can to describe the sensory characteristics fully
3. Compile the terms given by all the panelists to form a list of descritors
Word generation
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Reduction of the list
1) Rearrange the list in family of terms (appearance, aroma, textures …)
2) Discuss with panelists to suppress:Hedonic and quantitative termsRedundant terms (synonyms)Non relevant terms
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Example of lexicon
pomme fruitpomme cuitechimiquepoirecaramelfermentécoingvert-pas mûr
cidrevanillegraspomme vertepruneaupeau pommecitroncolle blanche
List of original terms
pomme fraîchecoingcidrepomme vertecaramelvanillepruneaupoiremétalliquegras
Final list
Not discriminantNot relevant
Synonyms
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Examples of referents and definitions: Soy yogurts
Texture Thickness: consistency of the mass in the mouthRate of Melt: amount of product melted after a certain pressure of the tongueGraininess: amount of particle in massMouth coating: amount of film left on the mouth surfaces
Basic tastesSweet: SucroseSour: lactic acidBitter: caffeineSalty: sodium chloride
ArômeWater: taste like water down Flour: 1 spoon of flavor mixed in waterWood: cutting from pencil sharpening Chalk: smectaMilk: whole milk Raw pie crust: commercial raw pie crustCream: crème fraiche Hazelnut: : hazelnut powderEarthy: earth Mushroom: dry mushrooms soaked in water
TrigéminalAstringent: Shrininking or pukering of the tongue surface caused by tanins or alumn
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Procedure for manipulation of the samples
1) First compression (e.g. thickness)Place ½ spoon of sample in mouth and compress between tongue and palate
2) Manipulation (e.g. rate of melt, graininess)Compress sample several more times (2 to 3 times)
3) After feel (e.g. mouth coating)Swallow or expectorate
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Conventional Profiling
4-step process:
1. Panel selection
2. Development of a lexicon for appearance, odor, flavor, texture, mouth feel and after-taste
3. Training
4. Ratings of the products
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Training
Goal: assessors need to be able to detect and repeatedly quantify the sensory characteristicscorresponding to the lexicon
Need to be exposed to a wide range of products
Need to be familiarized with the use of the scale
Need to receive feed back to rectify any problem
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For each attribute:
1) Ranking testsPanelists receive 4 samples covering the range of differences likely to be encountered in the product category and are asked to rank them according to the attribute
Sweetness
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For each attribute:
2) Rating testsPanelists receive 4 sample and are asked to score them on an intensity scale
Start with large differences, then collect samples which represent smaller differences within the product category
Encourage panelists to refine the procedures for evaluation and terminology with definitions and references
Not sweetSweet
Very sweet
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3) Final practice
Final practice should approach the testing situation in which the panel will be used:
Same type of productsSame experimental conditionsSeveral replicates
Panelists should receive feed back on their performance compare to that of the panel
Samples Average Panelist # 1
275 6.3 5.7391 5.7 4.2856 1.2 2.3912 3.6 3.7057 2.5 1.9
Samples Average Panelist # 2
275 6.3 2.3391 5.7 1.8856 1.2 4.6912 3.6 2.4057 2.5 3.5
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Conventional Profiling
4-step process:
1. Panel selection
2. Development of a lexicon for appearance, odor, flavor, texture, mouth feel and after-taste
3. Training
4. Ratings of the products
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Pas du tout Très
Épais
Pas du tout Très
Gras
Pas du tout TrèsFondant
Code: 592
Pas du tout TrèsSucré
Pas du tout Très
Acide
Pas du tout Très
Amer
Pas du tout TrèsSalé
Pas du tout TrèsAstringent
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FAQs
How many assessors do we need ?
How many samples are there ?
How many replicates are necessary ? Normally 3 assessments per sample/assessors, however this is very expensive in time and resource. If the panel is fully trained and constantly evaluating the same type of products then a single assessment is likely to provide reliable data otherwise 1 or 2 replicates are advisable.
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How many training sessions? The number of training sessions depends on the complexity of the product, on the number of attributes to be covered, on the
requirement for validity and reliability A more experienced panel will provide greater detail with
greater reproducibility but a short version with fewer and simpler attributes is acceptable for control quality for example
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Many references exist to learn about sensory profilesThese include:
Sensory Evaluation Techniques, Third EditionMeilgaard, Morten C.Civille, Gail VanceCarr, B. ThomasCRC Press
Sensory Evaluation PracticesHerbert Stone, Joel L SidelAcademic Press
Sensory Evaluation of FoodPrinciples and PracticesHarry T. Lawless, Hildegarde HeymannAspen press