D8 ADVANCE Pre-Installation Guide (2)

8/19/2019 D8 ADVANCE Pre-Installation Guide (2)

1/13M88-E04046 18 February 2009

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Bruker AXS

D8 ADVANCEX-ray Diffractometer

Pre-installation Guide(North America)

Purpose

This Pre-installation Guide will aid you and any requiredpersonnel in site preparation prior to installation of the

D8 ADVANCE X-ray diffractometer.

Read these instructions carefully and thoroughly to

prepare for the installation of your D8 ADVANCE. Proper

site planning will ensure optimum efficiency,

maintenance access, proper instrument performance,

and avoidance of unnecessary delays during installation.

Responsibility

The customer is responsible for making certain that thebasic site requirements for the D8 ADVANCE are

fulfilled. These instructions are to be followed by the

customer and by personally contracted tradespeople,

except where otherwise noted.

When the basic site requirements are fulfilled, it is the

customer’s responsibility to complete the attached Pre-

installation Checklist and return it to Bruker AXS via fax.

System Requirements

The following specifications are general system

requirements. Use this information to make an initial

decision on the suitability of your proposed site. Refer to

later sections of this Pre-installation Guide for more

details.

Power (pages 4 - 5)

System 208-240V, 60Hz, 1-phase, 40A

Computer/peripherals 100-120V, 60Hz, 1-phase, 15A

Haskris R100C water

recirculator

208-240V, 60Hz (isolated),

1-phase, 15A

Cooling Capacity 3850W (13125 btu/hr) or greater

Temperature 50-68°F ±2°F (10-20°C ±1°C)

Pressure 60-90 psi (4-6 bar)

Quantity* 6 gal (23 L)

*Quantity specified is for Haskris R100C. Use distilled water.

Communications (Figure 2 and Table 5)

Optional RJ-11 line near system for voice connection

Ethernet network connection (Table 5)

Table 1. Pre-installation Overview

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D8 ADVANCE Dimensions

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D8 ADVANCE Dimensions Shipping Dimensions

The D8 ADVANCE shipment includes two large boxes

from Bruker AXS factories (Table 3). To account for

variation in box size, maximum dimensions are given in

the Table. Additional small boxes may arrive with the

shipment, given the configuration of the system.

Figure 1. D8 ADVANCE dimensions

D8 ADVANCE

dimensions

and weight

Height 82.5” (209.5 cm)

Width 55.1” (140.0 cm)

Depth 49.4” (125.5 cm)

Weightapprox. 1190 lbs

(540 kg)

Floor load

capacity

146.9 lbs/ft2 (717.0 kg/m2) minimum. The floor

should be level and as rigid as possible to avoid

vibration.

Doorway

clearance

required

Largest sub-assembly

(unboxed/uncrated), if

mounted parts are

removed

36.0” (91.4 cm)

Wall-to rear ofinstrument

clearance

27.5” (70.0 cm)

minimum

Although the

instrument has

wheels, it should be

accessible from all

sides for proper

servicing and airflow.

Table 2. Actual instrument dimensions, weights, and clearances

Base Box (on pallet) Top Box (on pallet)

Height 58.3” (148 cm) 44.5” (113 cm)

Width 57.1” (145 cm) 43.3” (110 cm)

Depth 66.1” (168 cm) 55.1” (140 cm)

Weight 1030 lbs (467 kg) 710 lbs (322 kg)

Table 3. Maximum dimensions of instrument boxes from factory

46.7" (118.7 cm)

3.1"(8 cm)

82.5"(209.5 cm)

46.3" (117.7 cm)(side panels removed*)

35.1"

Dolly - 2.4"

(6.0 cm)

(89.2 cm)

55.1" (140.0 cm)

33.7" (85.6 cm)(front and rear panels removed*)

46.0"(116.8 cm)

33.3" (84.7 cm)

Side View

(enclosure rear removed*)

Front View43.6"

(111 cm)(light bar

removed*)

*NOTE: Dimensions with portions temporarily removed for transportation

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Environmental Considerations

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Environmental Considerations

Figure 2. Typical D8 ADVANCE floor plan

Room/Instrument Requirements

Optimal room temperature 75.2°F (24.0°C)

Room operation-range temperature 57.2 - 93.2°F (14.0 - 34.0°C)

Maximum temperature gradient 1.8°F (1°C) per hour for highest stabil ity of measuring values

Relative humidity 20%-80%, non-condensing

Heat dissipation to the air by the

diffractometer (with temperature stabilizer,

electronics measuring, X-ray generator, and

vacuum pump).

This configuration assumes that an external

water recirculator is installed in a separate

room.

1.0 kW (3412 btu/hr) maximum

Dissipated heat must be removed by a ventilation or air conditioning system. Cooling air

should flow around the instrument without restriction. If possible, locate the air conditioning

and heating ducts so that their airflow is not aimed directly at the instrument.

NOTE: We recommend a clean, dust-free environment.

Static electricity elimination (to avoid adverse

effects on instrument electronics)

Any carpeting in the area should be of a conductive variety. If the area is carpeted with non-

conductive carpet, we recommend that you place anti-static mats over the conventional

carpeting in the area around the instrument.

Table 4. Environmental considerations

Table (not factory-supplied)

(70 cm)27.5"

External water recirculator

(Haskris R100C)

(70 cm)

27.5"Generator

Electronics

Minimumclearance

28' (8.5 m) maximum

cable distance between

instrument and computer.

Allow for routing of cables

along baseboards.

(70 cm)27.5"

RJ-11 jack

for voice

connection

(optional)

RJ-45 jack

for internet

connection

(optional)

NOTE: For plumbing and electrical details,see the other Figures and Tables inthis Pre-installation Guide.


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Communications

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Communications

We strongly recommend that you install a telephone

connection (for voice communications) near the

instrument.

NOTE: Bruker AXS’ Remote Diagnosis features are nowavailable over the internet (i.e., WebEx). Checkwith your IT administrator to find out howRemote Diagnosis may affect your IT policy.

Electrical Power

■ See Table 6 for power requirements for the D8

ADVANCE (including the computer and peripherals).

Note the lengths of the various cables.

■ On the wall behind the instrument, connect powerfrom the building mains to a plug-type wall outlet or

to a direct-wired circuit breaker/disconnect box, so

that power to the instrument can be interrupted if

necessary.

NOTE: Outlet and plug not factory-supplied.

NOTE: If the power line voltage at your site fluctuatesoutside the values in Table 6, a compatible linevoltage conditioner or regulator may benecessary. Check with your site’s electricalcoordinator.

■ Wire the room air conditioner and any external

pumps to a different electrical circuit than that used

for the instrument. High starting currents from their

motors may adversely affect line voltage stability.

Additionally, provide a separate electrical power cir-

cuit for the Haskris water recirculator (if purchased).

Figure 3. D8 ADVANCE electrical connections

Connection Connector Purpose

Telephone

(optional)RJ-11

Voice connection near

instrument

Internet

connectionRJ-45 (Ethernet)

Remote diagnosis over

the internet

Table 5. Communications: connections

Generator

Electronics

Haskris

R100C

water

recirculator

Ground cable

(factory-supplied)

208 VAC, 40A

Circuit breaker, disconnect box, or

outlet for plug (not factory-supplied).

Secure to wall.

208 VAC, 15A

(isolated from system)

110 VAC, 15A

six-outlet power strip

(included)

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Electrical Power

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Figure 4. D8 ADVANCE electrical connections (schematic)

L1

L2

Fuse or

breaker40 A (2)

Electronics & Generator

Cable to

chassis ground

(factory-supplied)

3-conductor, 8-gauge

power cable (factory-supplied).Cable is 20 feet (6.1 m) long,

4 feet (1.5 m) of which areenclosed inside the instrument.

Electrical Box

House Power208 VAC

Instrument(left side)

Earth Ground

Component Current rating Voltage and frequency Power cable lengths

D8 ADVANCE diffractometer

unit40A† 208-240V, 60Hz, 1-phase

8-gauge, 3-conductor power cable

(factory-supplied), about 15 ft (4.6 m)*

Computer and peripherals 15A 100-120V, 60Hz, 1-phase6 ft (1.8 m)**

Data cables: about 28 ft (8.5 m)

External water recirculator,

Haskris R100C

15A 208-240V, 60Hz, 1-phase About 8 ft (2.4 m)***

* Customer supplies plug to match wall receptacle (if used).

** Factory-supplied 6-position AC outlet strip (110V).

*** For the recommended Haskris model (R100C), customer supplies plug to match wall receptacle (if used).

† If fuses are used, use slow-blow fuses.

Table 6. D8 ADVANCE electrical specifications


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Cooling Requirements

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An external cooling-water system is required to

dissipate heat produced by the D8 ADVANCE. The

cooling-water system must be fed with a closed-circuit

cooling system.

To minimize difficulties with cooling water (e.g.,

suspended solids, low pressure, and extreme water

temperature variations), we recommend installing a

Haskris R100C closed-circuit water recirculator as

shown in Figures 5 and 6. Other cooling system

arrangements are not recommended as they will

inevitably fail to minimize the aforementioned difficulties

and result in cooling problems.

NOTE: If you do not wish to install a Haskris closed-circuit water recirculator, contact Bruker AXS for

more information.

CAUTION

The X-ray tube’s warranty does not cover damageresulting from improper cooling water.

Install two 3/4” copper lines, each maximum length of

48 ft (15m), with a shut-off valve near each end of each

pipe. Install 1/2” barbed fittings (not supplied) at each

end of the pipes. These copper lines are intended for

transporting the cooling water over long distances. The

barbed fittings at the end of the pipes will connect to the

short, factory-supplied hoses attached to the instrument.

During installation, the Bruker AXS Field Service

Engineer will connect factory-supplied 1/2” (12mm)

inside diameter hoses between the Haskris R100C and

piping, and then between the piping and instrument (the

unit and instrument having customer-supplied barbed

fittings). The Engineer will then fasten the water hoses

to the barbed fittings with hose clamps.

NOTE: The Haskris R100C needs supply water and adrain to remove heat that it emits. However, it

keeps water consumption to a minimum using awater valve that opens and closes as required.

NOTE: To protect the Haskris R100C, ensure that thewater is free of suspended matter. Also, ensurethat water hardness does not exceed 300 mg/ liter CaO, while remaining at neutral pH (7).

Technical

features

Cooling capacity

when water source

is 65°F (18°C):

3850W (13125 btu/hr)

Water pump

capacity3.7 gal/min (14.1 L/min)

Water reservoir

volume6 gal (23 L)

Temperature

stability±2°F (1.1°C)

Refrigerant R134a

Unit weight

325 lbs (148 kg)

(approximate shipping

weight without water in

the tank)

Unit dimensions 31”H × 21”W × 29”D(79 cm × 53 cm × 74 cm)

Coolant required

Clean, potable, distilled

water. Do not use

deionized water.

Condensercooling water

requirements

When temp. is:

65°F (18°C)

75°F (24°C)

85°F (29°C)

Flow rate required is:

1.0 gal/min (3.8 L/min)



Minimum required

pressure differential

from condenser

water inlet to outlet:

25 psi (1.7 bar)

Maximum pressure

differential from

condenser water

inlet to outlet:

60 psi (4.1 bar)

Maximum

condenser water

inlet pressure:

125 psi (8.6 bar)

Location

Must be installed in

a clean, indoor

environment. Ifpossible, install the

Haskris in a

separate room to

minimize noise and

heat emission.

We recommend access to

the:

TOP for routine

maintenance, such aschanging water in the

reservoir.

FRONT for visibility of

controls and readouts.

ONE SIDE for convenient

servicing should a spare

part be required.

Table 7. Haskris R100C recirculator specifications

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Figure 5. Haskris R100C recirculator specifications

Figure 6. Cooling water with the Haskris R100C closed-circuit water recirculator

Haskris Model R100CTECHNICAL SPECIFICATIONS

1. Power Requirements: 208/230V-1-60Hz

2. F.L.A. Rating: 9.9A

3. Recommended Fuse Size: 15A (time delay)

REAR

VIEWNOT DRAWN

TO SCALE

3"

2.5"

2.5"

City Water "IN"3/8" FPT Brass

City Water "OUT"

3/8" FPT Brass

SUPPLY

RETURN

21"24"

2.25"

18.5"

POWER CORD (7 ft., no plug furnished)

Note:

Supply and return connections are

1/2" Hand Valves with 1/2" Hose Barbs.

DEPTH = 29.0"

(73.7 cm)

21.0"

(53.3 cm)

31.0"

(78.7 cm)

FRONT

VIEWNOT DRAWN

TO SCALE

Unit ON/OFF

Switch

Power

Indicator

Water Level

Indicator

Flowmeter

Leveling Legs

(adjustable from 1/2" To 2")

Ventilation grille

Water Temp

Control & Display

65

MENU

FULL

Generator Electronics

Reinforced industrial water hose

3/4" copper tubing

Shut-off valves (wall-mounted)

1/2" barbed fitting

Water supply

Supply to

instrument

Return from

instrument

R100C

HaskrisDrain

NOTE: 25’ (7.6 m) of water hose comeswith the Haskris R100C.

65’ (20.0 m) of usable waterhose comes with the D8ADVANCE.


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Plumbing Requirements

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Plumbing Requirements

Gas Specifications

Position-sensitive Detector Gas Supply(optional—for MBraun PSD only)

■ If an MBraun PSD (position-sensitive detector) is

used with the D8 ADVANCE, install a P10 gas cylin-

der and regulator as noted in Table 9.

■ Install a cylinder of gas with a two-stage regulator

(for the flow counter) as noted in Table 9. We recom-

mend indoor installation of the gas cylinder.

■ Ensure that the cylinder is securely mounted to avoid

tipping. Observe all safety regulations for flammable

gases. We recommend that you keep a reserve cylin-

der.

■ Install as short a line as possible from the gas cylin-

der to the instrument. Use factory-supplied Viton tub-

ing (length as noted in Table 8). If your supply line

must exceed the supplied length, use oxygen-free

(high-purity) copper or stainless-steel piping. Ensure

that the lines are clean and free of water, solvents,

and particulate matter. Avoid exposing the gas linesto extreme temperatures (such as heating vents).

■ Operate the flow counters only with a commercial-

grade mixture of P10 gas (i.e., 90% Argon, 10%

methane, impurities less than 0.5% by volume).

■ Install a separate exhaust line leading to an outside

discharge for the spent gas.

Helium Supply (optional)

■ For equipment with a helium or nitrogen flush option

(required for liquid or loose powder analysis), install a

helium or nitrogen cylinder with a two-stage regula-

tor as noted in Table 9.

■ Secure the cylinder with a mounting support to avoid

accidental tipping.

Material supplied with D8ADVANCE

Tubing/hose ID sizes forbarbed fittings

Tubing/hose lengths

Counter tube gas

(P10—for MBraun position-

sensitive detector only)

Inlet: Black Viton tubing 0.125” (0.32cm) 23 ft (7m)

Outlet: Blue polymer tubing 0.25” (0.64cm) 23 ft (7m)

Helium Blue Polymer tubing 0.125” (0.32cm) 23 ft (7m)

Cooling water hoses Pressure water hose 0.5” (1.27cm) 65 ft (20.0m)

Vacuum exhaust* Plastic hose 0.5” (1.27cm) 17 ft (5.2m)

* Mist elimination is installed; exhausting vacuum is an option. You must provide an outlet for the vacuum exhaust (see Figure 2).

Table 8. Tubing and hose sizes for supplied barbed fittings on D8 ADVANCE and Haskris R100C water recirculator

GasCylinder/Regulator(not factory-supplied)

P10

Compressed-gas cylinder with T-size

cylinder filling pressure, 2900 psi (180

bar), with regulator such as AGA model

SGVHPT272B-350 or equivalent.*

Helium or nitrogen

(optional; use if

ordered)

Compressed-gas cylinder with T-size

cylinder filling pressure, 2900 psi (180

bar), with regulator such as AGA model

SGVHPT270B-580 or equivalent.*

* Securely mount the cylinders to a wall or table. Observe safety

regulations for all flammable gases.

Table 9. Gas specifications

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Bruker AXS Inc.

5465 East Cheryl Parkway

Madison, WI 53711-5373 USA

Phone +1 (800) 234-XRAY [9729]

Fax +1 (608) 276-3006

E-mail: [email protected]

www.bruker-axs.com

Bruker BioSciences

40 Manning Road

Billerica, MA USA

Phone +1 (978) 663-3660

Fax: +1 (978) 667-5993


www.bruker-biosciences.com

Final Check

Final Check

You, the customer, are responsible for meeting all

applicable building and safety codes. Once the pre-

installation utilities are connected, get certification (from

an approved authority) that the installation meets all

local building and safety codes.

When all pre-installation work is finished, complete the

attached D8 ADVANCE Pre-installation Checklist and fax

it to Bruker AXS.

Fax: 1 (608) 276-9162 or 1 (608) 276-3015

Also, contact the Bruker AXS Service Department by

telephone to confirm that your site is ready forinstallation.

Tel: 1 (800) 234-XRAY [9729] or 1 (608) 276-3087

Upon receiving confirmation that your site is ready,

Bruker AXS personnel will schedule the instrument

installation.

When the System Arrives

■ When the system arrives, check it for damage with

the delivery driver. Contact the carrier’s office and

Bruker AXS immediately if you find any damage.

■Compare the packing list (i.e., the number of boxesreceived) with your order invoice and contact Bruker

AXS if you find any discrepancies.

■ Move boxes or crates to the installation site (if possi-

ble) to facilitate timely installation. Wait until a Bruker

AXS Field Service Engineer opens the boxes to

check their contents against your invoice. Do not

open or uncrate any boxes.

■ If uncrating is required, call Bruker AXS for authoriza-

tion at 1 (800) 234-XRAY [9729] extension 3087. If

you are authorized to uncrate the shipment, save all

packing material until the Bruker AXS Field Service

Engineer completes the installation.

■ Installation must be performed by a Bruker AXS Field

Service Engineer.

■ Save all packing materials for the system until the

Bruker AXS Field Service Engineer has completed

the installation.

NOTE: Installation of the system typically requires threeto four working days. Optional attachmentsrequire additional time for installation andtesting.


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D8 ADVANCE Pre-installation Checklist

M88-E04046


Please complete the checklist below and fax it to the Bruker AXS Service Department:

FAX

FROM: TO:

Bruker AXS,

Attn: Service Dept.

1 (608) 276-9162 or

1 (608) 276-3015

Contact Name Phone

Company/Organization Fax

Email

Component YES/NO Value/remark Initial/date

Room Location

Floor load capacity exceeds 146.9 lbs/ft2 (717.0 kg/m2)(see Table 2)

Room height exceeds 82.5” (209.5 cm) (see Table 2)

Floor space for D8 ADVANCE free of equipment and clean (see

Figures 1 and 2, Table 2)

Doors and hallways from loading dock to location have adequate

clearance for moving the D8 ADVANCE in its shipping crates;

freight elevator available (see Table 3)

Clearance on all sides of uncrated unit exceeds 27.5” (70.0 cm)

(see Figure 2, Table 2)

Computer table within 13.0’ (4.0 m) of instrument

Environment (see Table 4)

System is not exposed to direct sunlight

Temperature between 57.2 - 93.2°F (14.0 - 34.0°C)

Temperature gradient less than 1.8°F (1°C) per hour

Heat removal capacity exceeds 1.0 kW (3412 btu/hr)

Relative humidity between 20% - 80%, no condensation

Carpeted rooms: anti-static carpeting or mats installed

Communications (see page 4)

Optional voice line (near instrument)

Internet connection for remote diagnostics

Electrical Power (see Figure 4, Table 6)

208 VAC, 60 Hz ± 3 Hz, 40A (D8 ADVANCE)

208 VAC, 60 Hz ± 3 Hz, 15A (Haskris R100C)

110 VAC, 60 Hz ± 3 Hz, 15A (Computer and peripherals)

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M88-E04046

All electrical power for the system must be isolated from circuits

that have high starting currents (e.g., air conditioners, pumps,

furnaces)

Electrical connection of instrument to mains power supply is

provided with automatic circuit breakers for all phases

It is possible to disconnect the D8 ADVANCE completely from the

mains power supply, using either a labeled switch or a circuit

breaker located near the system

Power cable connected directly to switchboard

Socket outlet according to DIN49462, VDE 0623, IEC 309-1

(Approved plug connector supplied by customer)

Cooling Requirements (see page 6)

Closed cooling system (Haskris R100C recommended)

(see Figures 2 and 6)

Plumbing/piping complete

(for recommended Haskris unit)

Customer-supplied cooling system (not recommended)

The Haskris R100C water recirculator meets the cooling water requirements of the system. If you provide your own water supply, it must

meet the following requirements.

Flow rate greater than 1 gal/min (3.6 L/min). Recommended rate:


Pressure 60-110 psi (4-7.5 bar) and pressure-free drain

Temperature 59-68°F (15-20°C). Room temperature must be high

enough to avoid condensation.

Bruker AXS recommends the use of distilled or reverse osmosis (RO) water for cooling the X-ray tube and generator. Use of deionized water

is NOT recommended. If building water is used, it must meet the following requirements.

Hardness less than:

300mg/L CaO, or

30° CaO (German scale), or

53.7° CaO (French scale), or

37.5° CaO (UK scale)

pH of 7.0 ± 1

Adequate filtering to remove suspended solids ( 50 m)

Plumbing Requirements (see page 8)

Distance to water supply less than 26’ (8 m), less than 48’ (15 m)

if Haskris used

Shutoff valves installed on both lines (not required if discharginginto drain)

Elevation difference between Haskris and instrument less than 20’

(6 m)

NW ½” hose barb fittings for supply and return of cooling water

Supply Gases (the optional helium mode requires helium gas cylinders and regulators, not factory-supplied) (see

Tables 9 and 8, Figure 2)


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Bruker AXS Inc.

5465 East Cheryl Parkway

Madison, WI 53711-5373 USA

Phone +1 (800) 234-XRAY [9729]

Fax +1 (608) 276-3006


Bruker BioSciences

40 Manning Road

Billerica, MA USA

Phone +1 (978) 663-3660

Fax: +1 (978) 667-5993



P10 Gas (for MBraun PSD only):

Commercial-grade P10 gas (90% Argon, 10% methane, less than

0.5% impurities by volume) in T-size gas cylinder, e.g., 50 L, 200

bar (2900 psi)

Cylinder/regulator securely mounted to wall within 6’ (2 m) of theD8 ADVANCE

If mounted further away than the supplied hose length, correct

tubing/piping line installed (see Table 8)

Local safety requirements for flammable gases fulfilled

Exhaust gas vents to the outside, or a fume hood is present

(if mandated by local safety requirements)

Helium Gas (if applicable):

Cylinder/regulator securely mounted to wall within 6’ (2 m) of the

D8 ADVANCE

If mounted farther away than the supplied hose length, correcttubing/piping line installed (see Table 8)

Vacuum

Exhaust to outside (optional)

Final Check

All local safety codes are met

Fax a copy of this form to: Bruker AXS, Attention: Service

Department 1 (608) 276-9162

Call for installation: 1 (800) 234-XRAY [9729] extension 3087

When system arrives: Check packing crates for shipping damage. If there is damage, contact your Carrier’s Office and Bruker AXS. Compare

the packing list (the number of boxes) with your invoice. If possible, move boxes (crates) to installation site or storage area.

Do not open crates or boxes. If uncrating is required, call Bruker AXS for authorization at 1 (800) 234-XRAY [9729] extension 3087.

If authorized to uncrate, save all packing material until the Bruker AXS Field Service Engineer completes installation.


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D8 ADVANCE Pre-Installation Guide (2)

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Transcript of D8 ADVANCE Pre-Installation Guide (2)