CV4

ABIETIC ACID

Submitted by: G. C. Harris and T. F. Sanderson Checked by: R. T. Arnold and K. L. LindsayPublished in Org. Synth. 1952, 32, 1 Org. Synth. 1963, Coll. Vol. 4, 1

3-ACETAMIDO-2-BUTANONE

Submitted by: Richard H. Wiley and O. H. Borum Checked by: R. S. Schreiber and B. D. AspergrenPublished in Org. Synth. 1953, 33, 1 Org. Synth. 1963, Coll. Vol. 4, 5

N-( p - ACETYLAMINOPHENYL)RHODANINE

Submitted by: R. E. Strube Checked by: John D. Roberts and Stanley L. ManattPublished in Org. Synth. 1959, 39, 1 Org. Synth. 1963, Coll. Vol. 4, 6

9-ACETYLANTHRACENE

Submitted by: Charles Merritt, Jr and Charles E. Braun Checked by: William S. Johnson and Ralph F. HirschmannPublished in Org. Synth. 1950, 30, 1 Org. Synth. 1963, Coll. Vol. 4, 8

α-ACETYL-δ-CHLORO-γ-VALEROLACTONE

Submitted by: G. D. Zuidema, Eugene E. van Tamelen, and G. Van Zyl Checked by: William S. Johnson and Herbert I. Hadler

1 | P a g e

http://www.orgsyn.org/orgsyn/pdfs/CV4P0001.pdf





Published in Org. Synth. 1951, 31, 1 Org. Synth. 1963, Coll. Vol. 4, 10

1-ACETYLCYCLOHEXANOL

Submitted by: Gardner W. Stacy and Richard A. Mikulec Checked by: John C. Sheehan, George A. Mortimer, and Norman A. NelsonPublished in Org. Synth. 1955, 35, 1 Org. Synth. 1963, Coll. Vol. 4, 13

2- p -ACETYLPHENYLHYDROQUINONE

Submitted by: George A. Reynolds and J. A. VanAllan Checked by: R. S. Schreiber and A. H. NathanPublished in Org. Synth. 1954, 34, 1 Org. Synth. 1963, Coll. Vol. 4, 15

δ-ACETYL- n -VALERIC ACID

Submitted by: J. R. Schaeffer and A. O. Snoddy Checked by: Richard T. Arnold and H. W. TurnerPublished in Org. Synth. 1951, 31, 3 Org. Synth. 1963, Coll. Vol. 4, 19

ACROLEIN ACETAL

Submitted by: J. A. VanAllan

2 | P a g e





Checked by: T. L. Cairns and R. E. BensonPublished in Org. Synth. 1952, 32, 5 Org. Synth. 1963, Coll. Vol. 4, 21

ALLOXAN MONOHYDRATE

Submitted by: A. V. Holmgren and Wilhelm Wenner Checked by: T. L. Cairns and R. W. UpsonPublished in Org. Synth. 1952, 32, 6 Org. Synth. 1963, Coll. Vol. 4, 23

ALLOXANTIN DIHYDRATE

Submitted by: R. Stuart Tipson Checked by: T. L. Cairns and F. S. FawcettPublished in Org. Synth. 1953, 33, 3 Org. Synth. 1963, Coll. Vol. 4, 25

2-AMINO-4-ANILINO-6-(CHLOROMETHYL)- s -TRIAZINE

Submitted by: C. G. Overberger and Francis W. Michelotti Checked by: B. C. McKusick and F. W. StaceyPublished in Org. Synth. 1958, 38, 1 Org. Synth. 1963, Coll. Vol. 4, 29

p -AMINOBENZALDEHYDE

Submitted by: E. Campaigne, W. M. Budde, and G. F. Schaefer Checked by: Cliff S. Hamilton and R. C. RupertPublished in Org. Synth. 1951, 31, 6 Org. Synth. 1963, Coll. Vol. 4, 31

3 | P a g e





2-AMINOBENZOPHENONE

Submitted by: H. J. Scheifele, Jr and D. F. DeTar Checked by: R. T. Arnold and John D. JonesPublished in Org. Synth. 1952, 32, 8 Org. Synth. 1963, Coll. Vol. 4, 34

ε-AMINOCAPROIC ACID

Submitted by: Cal Y. Meyers and Leonard E. Miller Checked by: Richard T. Arnold and William R. Hasek

4 | P a g e




2-AMINO-3-NITROTOLUENE

Submitted by: John C. Howard Checked by: Charles C. Price and Joseph D. BermanPublished in Org. Synth. 1955, 35, 3 Org. Synth. 1963, Coll. Vol. 4, 42

3-AMINOPYRIDINE

Submitted by: C. F. H. Allen and Calvin N. Wolf Checked by: Cliff S. Hamilton and Marjorie DebrunnerPublished in Org. Synth. 1950, 30, 3 Org. Synth. 1963, Coll. Vol. 4, 45

p -AMINOTETRAPHENYLMETHANE

Submitted by: Benjamin Witten and E. Emmet Reid Checked by: Richard T. Arnold and Jerome J. Rosenbaum

5 | P a g e





ARYLUREASI. CYANATE METHODp -BROMOPHENYLUREA

Submitted by: Frederick Kurzer Checked by: Richard T. Arnold and Lester C. KroghPublished in Org. Synth. 1951, 31, 8 Org. Synth. 1963, Coll. Vol. 4, 49

ARYLUREASII. UREA METHODp -ETHOXYPHENYLUREA

Submitted by: Checked by: Published in Org. Synth. 1951, 31, 11 Org. Synth. 1963, Coll. Vol. 4, 52

DL-ASPARTIC ACID

Submitted by: M. S. Dunn and B. W. Smart Checked by: H. T. Clarke and W. PearlmanPublished in Org. Synth. 1950, 30, 7 Org. Synth. 1963, Coll. Vol. 4, 55

ATROLACTIC ACID

Submitted by: Ernest L. Eliel and Jeremiah P. Freeman Checked by: Arthur C. Cope, William F. Gorham, and Roscoe A. PikePublished in Org. Synth. 1953, 33, 7 Org. Synth. 1963, Coll. Vol. 4, 58

6 | P a g e





AZELANITRILE

Submitted by: Arthur C. Cope, Robert J. Cotter, and Leland L. Estes Checked by: N. J. Leonard and R. W. FulmerPublished in Org. Synth. 1954, 34, 4 Org. Synth. 1963, Coll. Vol. 4, 62

1,1'-AZO- bis -1-CYCLOHEXANENITRILE

Submitted by: C. G. Overberger, Pao-tung Huang, and M. B. Berenbaum Checked by: N. J. Leonard and E. H. MottusPublished in Org. Synth. 1952, 32, 16 Org. Synth. 1963, Coll. Vol. 4, 66

BENZENEBORONIC ANHYDRIDE

Submitted by: Robert M. Washburn, Ernest Levens, Charles F. Albright, and Franklin A. Billig

Checked by: B. C. McKusick and H. C. MillerPublished in Org. Synth. 1959, 39, 3 Org. Synth. 1963, Coll. Vol. 4, 68

BENZHYDRYL β-CHLOROETHYL ETHER

Submitted by: Shigehiko Sugasawa and Kunio Fujiwara Checked by: N. J. Leonard, P. D. Thomas, and L. A. MillerPublished in Org. Synth. 1953, 33, 11 Org. Synth. 1963, Coll. Vol. 4, 72

7 | P a g e





BENZOFURAZAN OXIDE

Submitted by: F. B. Mallory, P. A. S. Smith, and J. H. Boyer Checked by: T. L. Cairns, H. E. Simmons, Arthur C. Cope, David J. Marshall, and Douglas S. SmithPublished in Org. Synth. 1957, 37, 1 Org. Synth. 1963, Coll. Vol. 4, 74

BENZOGUANAMINE

Submitted by: J. K. Simons and M. R. Saxton Checked by: T. L. Cairns and A. K. SchneiderPublished in Org. Synth. 1953, 33, 13 Org. Synth. 1963, Coll. Vol. 4, 78

BENZOYLACETANILIDE

Submitted by: C. F. H. Allen and W. J. Humphlett Checked by: Max Tishler and R. ConnellPublished in Org. Synth. 1957, 37, 2 Org. Synth. 1963, Coll. Vol. 4, 80

BENZOYLCHOLINE IODIDE AND CHLORIDE

Submitted by: A. H. Ford-Moore Checked by: R. L. Shriner and Calvin N. WolfPublished in Org. Synth. 1950, 30, 10 Org. Synth. 1963, Coll. Vol. 4, 84

3-BENZOYLPYRIDINE

Submitted by: Frank J. Villani and Mary S. King Checked by: Max Tishler and Matthew A. KozlowskiPublished in Org. Synth. 1957, 37, 6

8 | P a g e






Org. Synth. 1963, Coll. Vol. 4, 88

2-BENZYLAMINOPYRIDINE

Submitted by: Yaïr Sprinzak Checked by: Max Tishler and Matthew A. KozlowskiPublished in Org. Synth. 1958, 38, 3 Org. Synth. 1963, Coll. Vol. 4, 91

3-BENZYL-3-METHYLPENTANOIC ACID

Submitted by: F. S. Prout, R. J. Hartman, E. P.-Y. Huang, C. J. Korpics, and G. R. Tichelaar Checked by: James Cason, K. C. Dewhirst, E. J. Gauglitz, Jr, and William G. DaubenPublished in Org. Synth. 1955, 35, 6 Org. Synth. 1963, Coll. Vol. 4, 93

BENZYLTRIMETHYLAMMONIUM ETHOXIDE

Submitted by: W. J. Croxall, Marion F. Fegley, and H. J. Schneider Checked by: John C. Sheehan and M. Gertrude HowellPublished in Org. Synth. 1958, 38, 5 Org. Synth. 1963, Coll. Vol. 4, 98

BISCHLOROMETHYL ETHER

9 | P a g e





Submitted by: Saul R. Buc Checked by: Charles C. Price, Frederick V. Brutcher, and Jerome CohenPublished in Org. Synth. 1956, 36, 1 Org. Synth. 1963, Coll. Vol. 4, 101

N-BROMOACETAMIDE

Submitted by: Eugene P. Oliveto and Corinne Gerold Checked by: Richard T. Arnold and Carl G. KrespanPublished in Org. Synth. 1951, 31, 17 Org. Synth. 1963, Coll. Vol. 4, 104

β-BROMOETHYLPHTHALIMIDE

Submitted by: T. O. Soine and M. R. Buchdahl Checked by: Cliff S. Hamilton and John D. SculleyPublished in Org. Synth. 1952, 32, 18 Org. Synth. 1963, Coll. Vol. 4, 106

4-BROMO-2-HEPTENE

Submitted by: F. L. Greenwood, M. D. Kellert, and J. Sedlak Checked by: John D. Roberts and A. T. BottiniPublished in Org. Synth. 1958, 38, 8 Org. Synth. 1963, Coll. Vol. 4, 108

p -BROMOMANDELIC ACID

Submitted by: J. J. Klingenberg Checked by: R. T. Arnold and C. D. WrightPublished in Org. Synth. 1955, 35, 11 Org. Synth. 1963, Coll. Vol. 4, 110

10 | P a g e





2-BROMO-3-METHYLBENZOIC ACID

Submitted by: J. F. Bunnett and M. M. Rauhut Checked by: John D. Roberts and Marc S. SilverPublished in Org. Synth. 1958, 38, 11 Org. Synth. 1963, Coll. Vol. 4, 114

n -BUTYLACETYLENE

Submitted by: Kenneth N. Campbell and Barbara K. Campbell Checked by: R. S. Schreiber, M. F. Murray, and A. C. OttPublished in Org. Synth. 1950, 30, 15 Org. Synth. 1963, Coll. Vol. 4, 117

sec -BUTYL α- n -CAPROYLPROPIONATE

Submitted by: Kenneth L. Rinehart Checked by: John C. Sheehan and J. IannicelliPublished in Org. Synth. 1955, 35, 15 Org. Synth. 1963, Coll. Vol. 4, 120

n -BUTYL GLYOXYLATE

Submitted by: Frank J. Wolf and John Weijlard Checked by: N. J. Leonard and L. A. MillerPublished in Org. Synth. 1955, 35, 18 Org. Synth. 1963, Coll. Vol. 4, 124

11 | P a g e





tert -BUTYL HYPOCHLORITE

Submitted by: H. M. Teeter and E. W. Bell Checked by: Charles C. Price and T. C. SchwannPublished in Org. Synth. 1952, 32, 20 Org. Synth. 1963, Coll. Vol. 4, 125

2-BUTYN-1-OL

Submitted by: P. J. Ashworth, G. H. Mansfield, and M. C. Whiting Checked by: John C. Sheehan, George Buchi, and Walfred S. SaariPublished in Org. Synth. 1955, 35, 20 Org. Synth. 1963, Coll. Vol. 4, 128

BUTYRCHLORAL

Submitted by: Gus A. Ropp, W. E. Craig, and Vernon Raaen Checked by: T. L. Cairns and H. N. CrippsPublished in Org. Synth. 1953, 33, 15


β-CARBETHOXY-γ,γ-DIPHENYLVINYLACETIC ACID

Submitted by: William S. Johnson and William P. Schneider Checked by: Arthur C. Cope and Malcolm ChamberlainPublished in Org. Synth. 1950, 30, 18 Org. Synth. 1963, Coll. Vol. 4, 132

β-( o -CARBOXYPHENYL)PROPIONIC ACID

12 | P a g e





Submitted by: G. A. Page and D. S. Tarbell Checked by: William S. Johnson, Shirley Rosenberg, and Robert D. EberhardtPublished in Org. Synth. 1954, 34, 8 Org. Synth. 1963, Coll. Vol. 4, 136

CETYLMALONIC ESTER

Submitted by: Don E. Floyd and Sidney E. Miller Checked by: James Cason and George A. GilliesPublished in Org. Synth. 1954, 34, 13 Org. Synth. 1963, Coll. Vol. 4, 141

CHLOROACETONITRILE

Submitted by: D. B. Reisner and E. C. Horning Checked by: R. L. Shriner and Calvin N. WolfPublished in Org. Synth. 1950, 30, 22


3-( o -CHLOROANILINO)PROPIONITRILE

Submitted by: S. A. Heininger Checked by: John C. Sheehan and Alma M. BostonPublished in Org. Synth. 1958, 38, 14 Org. Synth. 1963, Coll. Vol. 4, 146

CHLORO- p -BENZOQUINONE

Submitted by: R. E. Harman Checked by: N. J. Leonard and R. W. FulmerPublished in Org. Synth. 1955, 35, 22 Org. Synth. 1963, Coll. Vol. 4, 148

13 | P a g e






N-CHLOROBETAINYL CHLORIDE

Submitted by: B. Vassel and W. G. Skelly Checked by: John C. Sheehan and J. IannicelliPublished in Org. Synth. 1955, 35, 28 Org. Synth. 1963, Coll. Vol. 4, 154

trans -2-CHLOROCYCLOPENTANOL

Submitted by: Hugh B. Donahoe and Calvin A. Vanderwerf Checked by: Arthur C. Cope and Elbert C. HerrickPublished in Org. Synth. 1950, 30, 24 Org. Synth. 1963, Coll. Vol. 4, 157

1-CHLORO-2,6-DINITROBENZENE

Submitted by: F. D. Gunstone and S. Horwood Tucker Checked by: Arthur C. Cope, David J. Marshall, and Ronald M. PikePublished in Org. Synth. 1952, 32, 23 Org. Synth. 1963, Coll. Vol. 4, 160

2-CHLORO-2-METHYLCYCLOHEXANONE and 2-METHYL-2-CYCLOHEXENONE

14 | P a g e





Submitted by: E. W. Warnhoff, D. G. Martin, and William S. Johnson Checked by: M. S. Newman, G. R. Kahle, and D. E. ReidPublished in Org. Synth. 1957, 37, 8 Org. Synth. 1963, Coll. Vol. 4, 162

2-CHLORONICOTINONITRILE

Submitted by: E. C. Taylor, Jr and Aldo J. Crovetti

Checked by: Charles C. Price and Walter A. SchroederPublished in Org. Synth. 1957, 37, 12 Org. Synth. 1963, Coll. Vol. 4, 166

α-CHLOROPHENYLACETIC ACID

Submitted by: Ernest L. Eliel, Milton T. Fisk, and

Thomas Prosser Checked by: James Cason, Lois J. Durham, and Gerhard J. FonkenPublished in Org. Synth. 1956, 36, 3 Org. Synth. 1963, Coll. Vol. 4, 169

o -CHLOROPHENYLCYANAMIDE

Submitted by: Frederick Kurzer Checked by: Cliff S. Hamilton and David B. CappsPublished in Org. Synth. 1951, 31, 19 Org. Synth. 1963, Coll. Vol. 4, 172

α-(4-CHLOROPHENYL)-γ-PHENYLACETOACETONITRILE

Submitted by: Stephen B. Coan and Ernest I. Becker Checked by: Charles C. Price and G. Venkat RaoPublished in Org. Synth. 1955, 35, 30

15 | P a g e






1-( p -CHLOROPHENYL)-3-PHENYL-2- PROPANONE

Submitted by: Stephen B. Coan and Ernest I. Becker Checked by: Charles C. Price and G. Venkat RaoPublished in Org. Synth. 1955, 35, 32 Org. Synth. 1963, Coll. Vol. 4, 176

p -CHLOROPHENYL SALICYLATE

Submitted by: Norman G. Gaylord and P. M. Kamath Checked by: R. T. Arnold and J. John BrezinskiPublished in Org. Synth. 1952, 32, 25 Org. Synth. 1963, Coll. Vol. 4, 178

o -CHLOROPHENYLTHIOUREA

Submitted by: Frederick Kurzer Checked by: Cliff S. Hamilton and David B. Capps


2-CHLOROPYRIMIDINE

Submitted by: Irving C. Kogon, Ronald Minin, and C. G. Overberger Checked by: Charles C. Price and T. L. V. UlbrichtPublished in Org. Synth. 1955, 35, 34 Org. Synth. 1963, Coll. Vol. 4, 182

2-CHLORO-1,1,2-TRIFLUOROETHYL ETHYL ETHER

16 | P a g e






Submitted by: Bruce Englund Checked by: R. S. Schreiber and Burris D. TiffanyPublished in Org. Synth. 1954, 34, 16 Org. Synth. 1963, Coll. Vol. 4, 184

β-CHLOROVINYL ISOAMYL KETONE

Submitted by: Charles C. Price and Joseph A. Pappalardo Checked by: R. S. Schreiber, Wm. Bradley Reid, Jr, and R. W. JacksonPublished in Org. Synth. 1952, 32, 27 Org. Synth. 1963, Coll. Vol. 4, 186

Δ 4 -CHOLESTEN-3,6-DIONE

Submitted by: Louis F. Fieser Checked by: William S. Johnson and David G. MartinPublished in Org. Synth. 1955, 35, 36 Org. Synth. 1963, Coll. Vol. 4, 189

Δ 4 -CHOLESTEN-3-ONE

Submitted by: Jerome F. Eastham and Roy Teranishi Checked by: James Cason, James Jiu, and Elmer J. ReistPublished in Org. Synth. 1955, 35, 39 Org. Synth. 1963, Coll. Vol. 4, 192

CHOLESTEROL, Δ 5 -CHOLESTEN-3-ONE, AND Δ 4 -CHOLESTEN-3-ONE

Submitted by: Louis F. Fieser Checked by: William S. Johnson and David G. MartinPublished in Org. Synth. 1955, 35, 43 Org. Synth. 1963, Coll. Vol. 4, 195

17 | P a g e





COUMALIC ACID

Submitted by: Richard H. Wiley and Newton R. Smith Checked by: C. F. H. Allen and George A. ReynoldsPublished in Org. Synth. 1951, 31, 23 Org. Synth. 1963, Coll. Vol. 4, 201

CREOSOL

Submitted by: R. Schwarz and H. Hering Checked by: R. L. Shriner and C. L. Furrow, JrPublished in Org. Synth. 1953, 33, 17 Org. Synth. 1963, Coll. Vol. 4, 203

N-2-CYANOETHYLANILINE

Submitted by: J. Cymerman-Craig and M. Moyle Checked by: William S. Johnson and Duff S. Allen, JrPublished in Org. Synth. 1956, 36, 6 Org. Synth. 1963, Coll. Vol. 4, 205

CYANOGEN IODIDE

Submitted by: B. Bak and A. Hillebert Checked by: R. T. Arnold and H. E. FritzPublished in Org. Synth. 1952, 32, 29

18 | P a g e






3-CYANO-6-METHYL-2(1)-PYRIDONE

Submitted by: Raymond P. Mariella Checked by: Arthur C. Cope, James E. Krueger, and David J. MarshallPublished in Org. Synth. 1952, 32, 32 Org. Synth. 1963, Coll. Vol. 4, 210

1-CYANO-3-PHENYLUREA

Submitted by: Frederick Kurzer and J. Roy Powell Checked by: John C. Sheehan and Ernest R. GilmontPublished in Org. Synth. 1956, 36, 8 Org. Synth. 1963, Coll. Vol. 4, 213

Top of Form

1,2-CYCLODECANEDIOL

Submitted by: A. T. Blomquist and Albert Goldstein Checked by: N. J. Leonard and F. H. OwensPublished in Org. Synth. 1956, 36, 12 Org. Synth. 1963, Coll. Vol. 4, 216

CYCLODECANONE

Submitted by: Arthur C. Cope, John W. Barthel, and Ronald Dean Smith Checked by: N. J. Leonard and J. C. LittlePublished in Org. Synth. 1956, 36, 14 Org. Synth. 1963, Coll. Vol. 4, 218

19 | P a g e





CYCLOHEPTANONE

Submitted by: Hyp J. Dauben, Jr, Howard J. Ringold, Robert H. Wade, David L. Pearson, Arthur G. Anderson, Jr, Th. J. de Boer, and H. J. Backer Checked by: Arthur C. Cope, Warren N. Baxter, Robert J. Cotter, James Cason, John B. Rogan, and Wm. G. DaubenPublished in Org. Synth. 1954, 34, 19 Org. Synth. 1963, Coll. Vol. 4, 221

1,2-CYCLOHEXANEDIONE DIOXIME

Submitted by: Clifford C. Hach, Charles V. Banks, and Harvey Diehl Checked by: R. T. Arnold and Philip N. GordonPublished in Org. Synth. 1952, 32, 35 Org. Synth. 1963, Coll. Vol. 4, 229

CYCLOHEXENE SULFIDE

Submitted by: Eugene E. van Tamelen Checked by: Charles C. Price and Paul F. KirkPublished in Org. Synth. 1952, 32, 39 Org. Synth. 1963, Coll. Vol. 4, 232

CYCLOHEXYLIDENECYANOACETIC ACID AND 1-CYCLOHEXENYLACETONITRILE

Submitted by: Arthur C. Cope, Alfred A. D'Addieco, Donald Edward Whyte, and Samuel A. Glickman Checked by: T. L. Cairns and R. E. HeckertPublished in Org. Synth. 1951, 31, 25 Org. Synth. 1963, Coll. Vol. 4, 234

20 | P a g e





CYCLOPENTADIENE AND 3-CHLOROCYCLOPENTENE

Submitted by: Robert Bruce Moffett Checked by: R. T. Arnold and George P. ScottPublished in Org. Synth. 1952, 32, 41 Org. Synth. 1963, Coll. Vol. 4, 238

DIACETYL- d -TARTARIC ANHYDRIDE

Submitted by: R. L. Shriner and C. L. Furrow, Jr Checked by: N. J. Leonard and R. R. SauersPublished in Org. Synth. 1955, 35, 49 Org. Synth. 1963, Coll. Vol. 4, 242

2,5-DIAMINO-3,4-DICYANOTHIOPHENE

Submitted by: W. J. Middleton Checked by: James Cason and Ralph J. FessendenPublished in Org. Synth. 1959, 39, 8 Org. Synth. 1963, Coll. Vol. 4, 243

2,4-DIAMINO-6-HYDROXYPYRIMIDINE

Submitted by: J. A. VanAllan Checked by: Cliff S. Hamilton and John D. SculleyPublished in Org. Synth. 1952, 32, 45 Org. Synth. 1963, Coll. Vol. 4, 245

DIAMINOURACIL HYDROCHLORIDE

Submitted by: Wm. R. Sherman and E. C. Taylor, Jr

21 | P a g e






Checked by: T. L. Cairns and D. S. AckerPublished in Org. Synth. 1957, 37, 15 Org. Synth. 1963, Coll. Vol. 4, 247

DIAZOMETHANE

Submitted by: Th. J. de Boer and H. J. Backer Checked by: James Cason, Max J. Kalm, and R. F. PorterPublished in Org. Synth. 1956, 36, 16 Org. Synth. 1963, Coll. Vol. 4, 250

DIBROMOACETONITRILE

Submitted by: James W. Wilt and James L. Diebold Checked by: B. C. McKusick and H. E. KnipmeyerPublished in Org. Synth. 1958, 38, 16


4,4'-DIBROMOBIPHENYL

Submitted by: Robert E. Buckles and Norris G. Wheeler Checked by: R. S. Schreiber, Wm. Bradley Reid, Jr, and Robert W. JacksonPublished in Org. Synth. 1951, 31, 29 Org. Synth. 1963, Coll. Vol. 4, 256

DI- n -BUTYLDIVINYLTIN

Submitted by: Dietmar Seyferth Checked by: Melvin S. Newman and S. RamachandranPublished in Org. Synth. 1959, 39, 10 Org. Synth. 1963, Coll. Vol. 4, 258

22 | P a g e





DI- tert -BUTYL MALONATE

Submitted by: Allen L. McCloskey, Gunther S. Fonken, Rudolph W. Kluiber, William S. Johnson, and Chittaranjan Raha Checked by: James Cason, Gerhard J. Fonken, William G. Dauben, William S. Johnson, and Rudolph W. KluiberPublished in Org. Synth. 1954, 34, 26 Org. Synth. 1963, Coll. Vol. 4, 261

4,4'-DICHLORODIBUTYL ETHER

Submitted by: Kliem Alexander and H. V. Towles Checked by: Arthur C. Cope, Malcolm Chamberlain, and Mark R. KinterPublished in Org. Synth. 1950, 30, 27 Org. Synth. 1963, Coll. Vol. 4, 266

1,1-DICHLORO-2,2-DIFLUOROETHYLENE

Submitted by: J. C. Sauer Checked by: Charles C. Price and Maseh OsganPublished in Org. Synth. 1956, 36, 19 Org. Synth. 1963, Coll. Vol. 4, 268

2,2-DICHLOROETHANOL

Submitted by: C. E. Sroog and H. M. Woodburn Checked by: R. S. Schreiber and C. J. Lintner, JrPublished in Org. Synth. 1952, 32, 46 Org. Synth. 1963, Coll. Vol. 4, 271

1,1'-DICYANO-1,1'-BICYCLOHEXYL

Submitted by: C. G. Overberger and M. B. Berenbaum Checked by: N. J. Leonard and E. H. MottusPublished in Org. Synth. 1952, 32, 48 Org. Synth. 1963, Coll. Vol. 4, 273

1,2-DI-1-(1-CYANO)CYCLOHEXYLHYDRAZINE

Submitted by: C. G. Overberger, Pao-tung Huang, and M. B. Berenbaum Checked by: N. J. Leonard and E. H. MottusPublished in Org. Synth. 1952, 32, 50

23 | P a g e








DICYANOKETENE ETHYLENE ACETAL

Submitted by: C. L. Dickinson and L. R. Melby Checked by: James Cason, Edwin R. Harris, and William T. MillerPublished in Org. Synth. 1959, 39, 13 Org. Synth. 1963, Coll. Vol. 4, 276

DICYCLOPROPYL KETONE

Submitted by: Omer E. Curtis, Jr, Joseph M. Sandri, Richard E. Crocker, and Harold Hart Checked by: V. Boekelheide, R. Taber, and D. S. TarbellPublished in Org. Synth. 1958, 38, 19 Org. Synth. 1963, Coll. Vol. 4, 278

1-DIETHYLAMINO-3-BUTANONE

Submitted by: Alfred L. Wilds, Robert M. Nowak, and Kirtland E. McCaleb Checked by: William S. Johnson and Duane ZinkelPublished in Org. Synth. 1957, 37, 18 Org. Synth. 1963, Coll. Vol. 4, 281

N,N'-DIETHYLBENZIDINE

Submitted by: Rip G. Rice and Earl J. Kohn Checked by: Max Tishler, W. H. Jones, and W. F. BenningPublished in Org. Synth. 1956, 36, 21 Org. Synth. 1963, Coll. Vol. 4, 283

24 | P a g e





DIETHYL BENZOYLMALONATE

Submitted by: John A. Price and D. S. Tarbell Checked by: T. L. Cairns and C. L. DickinsonPublished in Org. Synth. 1957, 37, 20 Org. Synth. 1963, Coll. Vol. 4, 285

DIETHYL 1,1-CYCLOBUTANEDICARBOXYLATE

Submitted by: Raymond P. Mariella and Richard Raube Checked by: William S. Johnson, William DeAcetis, and Herbert TitlePublished in Org. Synth. 1953, 33, 23 Org. Synth. 1963, Coll. Vol. 4, 288

DIETHYL Δ 2 - CYCLOPENTENYLMALONATE

Submitted by: Robert Bruce Moffett Checked by: R. T. Arnold and George P. ScottPublished in Org. Synth. 1952, 32, 52 Org. Synth. 1963, Coll. Vol. 4, 291

DIETHYL ETHYLIDENEMALONATE

Submitted by: William S. Fones Checked by: Arthur C. Cope, Harris E. Petree, and E. R. TrumbullPublished in Org. Synth. 1952, 32, 54 Org. Synth. 1963, Coll. Vol. 4, 293

DIETHYL MERCAPTOACETAL

Submitted by: William E. Parham and Hans Wynberg Checked by: Max Tishler and George Purdue

25 | P a g e







DIETHYL METHYLENEMALONATE

Submitted by: Wayne Feely and V. Boekelheide Checked by: Max Tishler, Barbara P. Birt, and Arthur A. PatchettPublished in Org. Synth. 1958, 38, 22 Org. Synth. 1963, Coll. Vol. 4, 298

DIETHYL γ-OXOPIMELATE

Submitted by: W. S. Emerson and R. I. Longley, Jr

Checked by: William S. Johnson and I. A. DavidPublished in Org. Synth. 1953, 33, 25 Org. Synth. 1963, Coll. Vol. 4, 302

DIETHYL cis -Δ 4 - TETRAHYDROPHTHALATE AND DIETHYL cis -HEXAHYDROPHTHALATE

Submitted by: Arthur C. Cope and Elbert C. Herrick Checked by: Charles C. Price and George A. CypherPublished in Org. Synth. 1950, 30, 29 Org. Synth. 1963, Coll. Vol. 4, 304

DIETHYLTHIOCARBAMYL CHLORIDE

Submitted by: R. H. Goshorn, W. W. Levis, Jr, E. Jaul, and E. J. Ritter Checked by: T. L. Cairns and H. E. CuperyPublished in Org. Synth. 1955, 35, 55 Org. Synth. 1963, Coll. Vol. 4, 307

26 | P a g e





3,4-DIHYDRO-2-METHOXY-4-METHYL-2H-PYRAN

Submitted by: Raymond I. Longley, Jr, William S. Emerson, and Albert J. Blardinelli Checked by: T. L. Cairns and T. E. YoungPublished in Org. Synth. 1954, 34, 29 Org. Synth. 1963, Coll. Vol. 4, 311

9,10-DIHYDROPHENANTHRENE

Submitted by: Donald D. Phillips Checked by: William S. Johnson and David C. RemyPublished in Org. Synth. 1954, 34, 31 Org. Synth. 1963, Coll. Vol. 4, 313

9,10-DIHYDROXYSTEARIC ACID

Submitted by: Daniel Swern, John T. Scanlan, and

Geraldine B. Dickel Checked by: John D. Roberts and Edgar F. KieferPublished in Org. Synth. 1959, 39, 15 Org. Synth. 1963, Coll. Vol. 4, 317

1,4-DIIODOBUTANE

Submitted by: Herman Stone and Harold Shechter Checked by: Cliff S. Hamilton and R. C. RupertPublished in Org. Synth. 1950, 30, 33 Org. Synth. 1963, Coll. Vol. 4, 321

1,6-DIIODOHEXANE

Submitted by: Herman Stone and Harold Shechter Checked by: T. L. Cairns, B. C. McKusick, and G. V. MockPublished in Org. Synth. 1951, 31, 31 Org. Synth. 1963, Coll. Vol. 4, 323

27 | P a g e






DIISOPROPYL METHYLPHOSPHONATE

Submitted by: A. H. Ford-Moore and B. J. Perry Checked by: William S. Johnson and James AckermanPublished in Org. Synth. 1951, 31, 33 Org. Synth. 1963, Coll. Vol. 4, 325

2,3-DIMETHOXYCINNAMIC ACID

Submitted by: J. Koo, M. S. Fish, G. N. Walker, and J. Blake Checked by: T. L. Cairns and A. E. BarkdollPublished in Org. Synth. 1951, 31, 35 Org. Synth. 1963, Coll. Vol. 4, 327

DIMETHYL ACETYLENEDICARBOXYLATE

Submitted by: E. H. Huntress, T. E. Lesslie, and J. Bornstein Checked by: T. L. Cairns and M. J. HogsedPublished in Org. Synth. 1952, 32, 55 Org. Synth. 1963, Coll. Vol. 4, 329

p -DIMETHYLAMINOBENZALDEHYDE

Submitted by: E. Campaigne and W. L. Archer Checked by: N. J. Leonard and R. W. FulmerPublished in Org. Synth. 1953, 33, 27 Org. Synth. 1963, Coll. Vol. 4, 331

β-DIMETHYLAMINOETHYL CHLORIDE HYDROCHLORIDE

Submitted by: Luther A. R. Hall, Verlin C. Stephens, and J. H. Burckhalter Checked by: Richard T. Arnold and William LeePublished in Org. Synth. 1951, 31, 37 Org. Synth. 1963, Coll. Vol. 4, 333

28 | P a g e






2-(DIMETHYLAMINO)PYRIMIDINE

Submitted by: C. G. Overberger, Irving C. Kogon, and Ronald Minin Checked by: Charles C. Price and T. L. V. UlbrichtPublished in Org. Synth. 1955, 35, 58 Org. Synth. 1963, Coll. Vol. 4, 336

4,6-DIMETHYLCOUMALIN

Submitted by: Newton R. Smith and Richard H. Wiley Checked by: R. S. Schreiber and H. H. FallPublished in Org. Synth. 1952, 32, 57 Org. Synth. 1963, Coll. Vol. 4, 337

N,N-DIMETHYLCYCLOHEXYLMETHYLAMINE

Submitted by: Arthur C. Cope and Engelbert Ciganek Checked by: William E. Parham and Robert KoncosPublished in Org. Synth. 1959, 39, 19 Org. Synth. 1963, Coll. Vol. 4, 339

DIMETHYLFURAZAN

Submitted by: Lyell C. Behr and John T. Brent Checked by: T. L. Cairns and J. E. CarnahanPublished in Org. Synth. 1954, 34, 40 Org. Synth. 1963, Coll. Vol. 4, 342

β,β-DIMETHYLGLUTARIC ACID

Submitted by: Walter T. Smith and Gerald L. McLeod Checked by: William S. Johnson and Donald D. CameronPublished in Org. Synth. 1951, 31, 40 Org. Synth. 1963, Coll. Vol. 4, 345

29 | P a g e






DIMETHYLKETENE

Submitted by: C. W. Smith and D. G. Norton Checked by: T. L. Cairns and J. C. SauerPublished in Org. Synth. 1953, 33, 29 Org. Synth. 1963, Coll. Vol. 4, 348

5,5-DIMETHYL-2- n - PENTYLTETRAHYDROFURAN

Submitted by: J. Colonge and R. Marey Checked by: V. Boekelheide and H. KaempfenPublished in Org. Synth. 1958, 38, 25 Org. Synth. 1963, Coll. Vol. 4, 350

3,5-DIMETHYLPYRAZOLE

Submitted by: Richard H. Wiley and Peter E. Hexner Checked by: William S. Johnson and Robert J. HighetPublished in Org. Synth. 1951, 31, 43 Org. Synth. 1963, Coll. Vol. 4, 351

2,2-DIMETHYLPYRROLIDINE

Submitted by: Robert Bruce Moffett Checked by: N. J. Leonard and J. W. CurryPublished in Org. Synth. 1953, 33, 32 Org. Synth. 1963, Coll. Vol. 4, 354

30 | P a g e





5,5-DIMETHYL-2-PYRROLIDONE

Submitted by: R. B. Moffett Checked by: N. J. Leonard, W. E. Smith, and B. L. RyderPublished in Org. Synth. 1952, 32, 59 Org. Synth. 1963, Coll. Vol. 4, 357

N,N-DIMETHYLSELENOUREA

Submitted by: Frank Bennett and Ralph Zingaro Checked by: C. F. H. Allen and K. C. KennardPublished in Org. Synth. 1956, 36, 23


asym -DIMETHYLUREA

Submitted by: Frederick Kurzer Checked by: William S. Johnson and William T. TsatsosPublished in Org. Synth. 1952, 32, 61 Org. Synth. 1963, Coll. Vol. 4, 361

2,6-DINITROANILINE

Submitted by: Harry P. Schultz Checked by: Arthur C. Cope and Douglas S. SmithPublished in Org. Synth. 1951, 31, 45 Org. Synth. 1963, Coll. Vol. 4, 364

31 | P a g e





p,p'-DINITROBIBENZYL

Submitted by: Herbert O. House Checked by: John C. Sheehan and J. IannicelliPublished in Org. Synth. 1954, 34, 35 Org. Synth. 1963, Coll. Vol. 4, 367

1,4-DINITROBUTANE

Submitted by: Henry Feuer and Gerd Leston Checked by: John C. Sheehan and J. IannicelliPublished in Org. Synth. 1954, 34, 37 Org. Synth. 1963, Coll. Vol. 4, 368

3,4-DINITRO-3-HEXENE

Submitted by: D. E. Bisgrove, J. F. Brown, Jr, and L. B. Clapp Checked by: John C. Sheehan, Richard L. Wasson, and Herbert O. HousePublished in Org. Synth. 1957, 37, 23 Org. Synth. 1963, Coll. Vol. 4, 372

DIPHENYLACETALDEHYDE

Submitted by: Donald J. Reif and Herbert O. House Checked by: M. S. Newman and W. H. PowellPublished in Org. Synth. 1958, 38, 26 Org. Synth. 1963, Coll. Vol. 4, 375

DIPHENYLACETYLENE

Submitted by: Arthur C. Cope, Douglas S. Smith, and Robert J. Cotter Checked by: Charles C. Price and Thomas F. McKeon, JrPublished in Org. Synth. 1954, 34, 42 Org. Synth. 1963, Coll. Vol. 4, 377

32 | P a g e






1,4-DIPHENYL-5-AMINO-1,2,3-TRIAZOLE AND 4-PHENYL-5-ANILINO-1,2,3-TRIAZOLE

Submitted by: Eugene Lieber, Tai Siang Chao, and C. N. Ramachandra Rao Checked by: T. L. Cairns and E. L. MartinPublished in Org. Synth. 1957, 37, 26 Org. Synth. 1963, Coll. Vol. 4, 380

N,N'-DIPHENYLBENZAMIDINE

Submitted by: Arthur C. Hontz and E. C. Wagner Checked by: R. S. Schreiber and Wm. Bradley Reid, JrPublished in Org. Synth. 1951, 31, 48


α,β-DIPHENYLCINNAMONITRILE

Submitted by: Stanley Wawzonek and Edwin M. Smolin Checked by: Arthur C. Cope and Malcolm ChamberlainPublished in Org. Synth. 1951, 31, 52 Org. Synth. 1963, Coll. Vol. 4, 387

DIPHENYL SUCCINATE

Submitted by: Guido H. Daub and William S. Johnson Checked by: James Cason, Robert A. Wessman,

33 | P a g e





and William G. DaubenPublished in Org. Synth. 1954, 34, 44 Org. Synth. 1963, Coll. Vol. 4, 390

2,3-DIPHENYLSUCCINONITRILE

Submitted by: R. B. Davis, J. A. Ward, Jr, J. A. McRae, and R. A. B. Bannard Checked by: B. C. McKusick, R. L. Morgan, R. T. Arnold, and Stuart W. FentonPublished in Org. Synth. 1952, 32, 63 Org. Synth. 1963, Coll. Vol. 4, 392

p -DITHIANE

Submitted by: Richard G. Gillis and A. B. Lacey Checked by: B. C. McKusick and R. J. HarderPublished in Org. Synth. 1959, 39, 23 Org. Synth. 1963, Coll. Vol. 4, 396

trans -2-DODECENOIC ACID

Submitted by: C. Freeman Allen and Max J. Kalm Checked by: William S. Johnson and Alan D. LouriePublished in Org. Synth. 1957, 37, 29 Org. Synth. 1963, Coll. Vol. 4, 398

ETHANEDITHIOL

Submitted by: A. John Speziale Checked by: R. S. Schreiber and R. W. KratzPublished in Org. Synth. 1950, 30, 35

34 | P a g e






ETHOXYACETYLENE

Submitted by: E. R. H. Jones, Geoffrey Eglinton, M. C. Whiting, and B. L. Shaw Checked by: Arthur C. Cope and Ronald M. PikePublished in Org. Synth. 1954, 34, 46 Org. Synth. 1963, Coll. Vol. 4, 404

ETHYL α-ACETYL-β-(2,3-DIMETHOXYPHENYL)-PROPIONATE

Submitted by: E. C. Horning, J. Koo, M. S. Fish, and G. N. Walker Checked by: T. L. Cairns and Charles W. ToddPublished in Org. Synth. 1951, 31, 56 Org. Synth. 1963, Coll. Vol. 4, 408

ETHYL AZODICARBOXYLATE

Submitted by: J. C. Kauer Checked by: William G. Dauben and Robert L. Cargill


ETHYL BENZOYLACETATE

Submitted by: J. M. Straley and A. C. Adams

35 | P a g e





Checked by: Max Tishler and M. A. KozlowskiPublished in Org. Synth. 1957, 37, 32 Org. Synth. 1963, Coll. Vol. 4, 415

ETHYL tert -BUTYL MALONATE

Submitted by: R. E. Strube Checked by: William S. Johnson and Duff S. Allen, JrPublished in Org. Synth. 1957, 37, 34 Org. Synth. 1963, Coll. Vol. 4, 417

Bottom of FormTop of FormBottom of Form

Top of Form

N-ETHYL- p -CHLOROANILINE

Submitted by: Royston M. Roberts and Paul J. Vogt Checked by: James Cason and Milton FingerPublished in Org. Synth. 1958, 38, 29 Org. Synth. 1963, Coll. Vol. 4, 420

ETHYL CHLOROFLUOROACETATE

Submitted by: Bruce Englund Checked by: R. S. Schreiber and Burris D. TiffanyPublished in Org. Synth. 1954, 34, 49 Org. Synth. 1963, Coll. Vol. 4, 423

ETHYL DIAZOACETATE

36 | P a g e





Submitted by: N. E. Searle Checked by: Melvin S. Newman, G. F. Ottmann, and C. F. GrundmannPublished in Org. Synth. 1956, 36, 25 Org. Synth. 1963, Coll. Vol. 4, 424

ETHYL DIETHOXYACETATE

Submitted by: Robert Bruce Moffett Checked by: Charles C. Price and Charles E. ScottPublished in Org. Synth. 1955, 35, 59 Org. Synth. 1963, Coll. Vol. 4, 427

ETHYL ENANTHYLSUCCINATE

Submitted by: Tracy M. Patrick, Jr and Floyd B. Erickson Checked by: T. L. Cairns and R. D. CramerPublished in Org. Synth. 1954, 34, 51 Org. Synth. 1963, Coll. Vol. 4, 430

ETHYLENIMINE

Submitted by: C. F. H. Allen, F. W. Spangler, and E. R. Webster Checked by: R. S. Schreiber, A. C. Ott, and M. F. MurrayPublished in Org. Synth. 1950, 30, 38 Org. Synth. 1963, Coll. Vol. 4, 433

2-ETHYLHEXANONITRILE

Submitted by: John A. Krynitsky and Homer W. Carhart Checked by: H. R. Snyder and Richard S. ColgrovePublished in Org. Synth. 1952, 32, 65 Org. Synth. 1963, Coll. Vol. 4, 436

ETHYL ISOCYANIDE

Submitted by: H. L. Jackson and B. C. McKusick

37 | P a g e






Checked by: N. J. Leonard and L. E. Coleman, JrPublished in Org. Synth. 1955, 35, 62 Org. Synth. 1963, Coll. Vol. 4, 438

β-ETHYL-β-METHYLGLUTARIC ACID

Submitted by: H. H. Farmer and Norman Rabjohn Checked by: Melvin S. Newman and Robert HarperPublished in Org. Synth. 1956, 36, 28 Org. Synth. 1963, Coll. Vol. 4, 441

4-ETHYL-2-METHYL-2-OCTENOIC ACID

Submitted by: Kenneth L. Rinehart and Edward G. Perkins Checked by: Melvin S. Newman and Joseph H. ManhartPublished in Org. Synth. 1957, 37, 37 Org. Synth. 1963, Coll. Vol. 4, 444

5-ETHYL-2-METHYLPYRIDINE

Submitted by: Robert L. Frank, Frederick J. Pilgrim, and Edward F. Riener

38 | P a g e




Checked by: R. S. Schreiber and T. L. AldersonPublished in Org. Synth. 1950, 30, 41 Org. Synth. 1963, Coll. Vol. 4, 451

ETHYL α-NITROBUTYRATE

Submitted by: Nathan Kornblum and Robert K. Blackwood Checked by: James Cason, Joanne Facaros, and William G. DaubenPublished in Org. Synth. 1957, 37, 44 Org. Synth. 1963, Coll. Vol. 4, 454

ETHYL ORTHOCARBONATE

Submitted by: John D. Roberts and Robert E. McMahon Checked by: William S. Johnson and William E. LoebPublished in Org. Synth. 1952, 32, 68 Org. Synth. 1963, Coll. Vol. 4, 457

ETHYL β,β-PENTAMETHYLENEGLYCIDATE

Submitted by: Richard H. Hunt, Leland J. Chinn, and William S. Johnson Checked by: N. J. Leonard and F. P. Hauck, JrPublished in Org. Synth. 1954, 34, 54 Org. Synth. 1963, Coll. Vol. 4, 459

ETHYL PHENYLCYANOACETATE

Submitted by: E. C. Horning and A. F. Finelli Checked by: William S. Johnson and H. WynbergPublished in Org. Synth. 1950, 30, 43 Org. Synth. 1963, Coll. Vol. 4, 461

ETHYL (1-PHENYLETHYLIDENE)CYANOACETATE

Submitted by: S. M. McElvain and David H. Clemens Checked by: W. E. Parham, Perry W. Kirklin, Jr, and Wayland E. NolandPublished in Org. Synth. 1959, 39, 25

39 | P a g e







ETHYL N-PHENYLFORMIMIDATE

Submitted by: Royston M. Roberts and Paul J. Vogt Checked by: T. L. Cairns and J. J. DrysdalePublished in Org. Synth. 1955, 35, 65 Org. Synth. 1963, Coll. Vol. 4, 464

ETHYL α-(1-PYRROLIDYL)PROPIONATE

Submitted by: Robert Bruce Moffett Checked by: N. J. Leonard and S. GelfandPublished in Org. Synth. 1953, 33, 35 Org. Synth. 1963, Coll. Vol. 4, 466

ETHYL PYRUVATE

Submitted by: J. W. Cornforth Checked by: Charles C. Price, Kenneth N. Campbell, and John WarnkePublished in Org. Synth. 1951, 31, 59 Org. Synth. 1963, Coll. Vol. 4, 467

1,1'-ETHYNYLENE- bis -CYCLOHEXANOL

Submitted by: G. Forrest Woods and Louis H. Schwartzman Checked by: Richard T. Arnold and Stuart W. FentonPublished in Org. Synth. 1952, 32, 70 Org. Synth. 1963, Coll. Vol. 4, 471

FERROCENE

Submitted by: G. Wilkinson and G. Wilkinson Checked by: N. J. Leonard, Kenneth L. Rinehart, Donald J. Casey, Sung Moon, N. J. Leonard, Kenneth L. Rinehart, and Peter WooPublished in Org. Synth. 1956, 36, 31 Org. Synth. 1963, Coll. Vol. 4, 473

40 | P a g e






FLAVONE

Submitted by: T. S. Wheeler Checked by: R. L. Shriner and Donald A. ScottPublished in Org. Synth. 1952, 32, 72 Org. Synth. 1963, Coll. Vol. 4, 478

9-FLUORENECARBOXYLIC ACID

Submitted by: Henry J. Richter Checked by: Richard T. Arnold, B. C. W. Hummel, and W. J. Wolf


5-FORMYL-4-PHENANTHROIC ACID

Submitted by: R. E. Dessy and M. S. Newman Checked by: J. D. Roberts and D. I. SchusterPublished in Org. Synth. 1958, 38, 32 Org. Synth. 1963, Coll. Vol. 4, 484

FUMARONITRILE

Submitted by: David T. Mowry and John Mann Butler Checked by: Charles C. Price and Richard D. GilbertPublished in Org. Synth. 1950, 30, 46 Org. Synth. 1963, Coll. Vol. 4, 486

41 | P a g e





FURFURAL DIACETATE

Submitted by: R. T. Bertz Checked by: James Cason, William G. Dauben, W. B. Fearing, and B. P. SummererPublished in Org. Synth. 1953, 33, 39 Org. Synth. 1963, Coll. Vol. 4, 489

2-FURFURYL MERCAPTAN

Submitted by: Helmer Kofod Checked by: Richard T. Arnold and Erich MarcusPublished in Org. Synth. 1955, 35, 66 Org. Synth. 1963, Coll. Vol. 4, 491

2-FUROIC ACID

Submitted by: R. J. Harrisson and M. Moyle Checked by: James Cason and W. N. BaxterPublished in Org. Synth. 1956, 36, 36 Org. Synth. 1963, Coll. Vol. 4, 493

GLUTARIC ACID AND GLUTARIMIDE

Submitted by: G. Paris, L. Berlinguet, R. Gaudry, J. English, Jr, and J. E. Dayan Checked by: James Cason, Edwin R. Harris, Arthur C. Cope, and Mark R. KniterPublished in Org. Synth. 1957, 37, 47 Org. Synth. 1963, Coll. Vol. 4, 496

42 | P a g e





GUANYLTHIOUREA

Submitted by: Frederick Kurzer Checked by: John C. Sheehan, George Buchi, and David KnutsonPublished in Org. Synth. 1955, 35, 69 Org. Synth. 1963, Coll. Vol. 4, 502

D-GULONIC-γ-LACTONE

Submitted by: J. V. Karabinos Checked by: R. T. Arnold, Fred Smith, and Bertha LewisPublished in Org. Synth. 1956, 36, 38 Org. Synth. 1963, Coll. Vol. 4, 506

HEMIMELLITENE

Submitted by: W. R. Brasen and C. R. Hauser Checked by: William S. Johnson, Donald W. Stoutamire, and A. L. WildsPublished in Org. Synth. 1954, 34, 56 Org. Synth. 1963, Coll. Vol. 4, 508

HENDECANEDIOIC ACID

Submitted by: Lois J. Durham, Donald J. McLeod, and James Cason Checked by: N. J. Leonard, D. H. Dybvig, and K. L. Rinehart, JrPublished in Org. Synth. 1958, 38, 34 Org. Synth. 1963, Coll. Vol. 4, 510

43 | P a g e





n -HEPTAMIDE

Submitted by: J. L. Guthrie and Norman Rabjohn Checked by: William S. Johnson and Duane ZinkelPublished in Org. Synth. 1957, 37, 50 Org. Synth. 1963, Coll. Vol. 4, 513

3- n -HEPTYL-5-CYANOCYTOSINE

Submitted by: Barbara B. Kehm and Calvert W. Whitehead Checked by: M. S. Newman and K. G. IhrmanPublished in Org. Synth. 1957, 37, 52 Org. Synth. 1963, Coll. Vol. 4, 515

HEXAHYDRO-1,3,5-TRIPROPIONYL- s - TRIAZINE

Submitted by: W. O. Teeters and M. A. Gradsten Checked by: Arthur C. Cope and Mark R. KinterPublished in Org. Synth. 1950, 30, 51 Org. Synth. 1963, Coll. Vol. 4, 518

HEXAMETHYLBENZENE

Submitted by: N. M. Cullinane, S. J. Chard, and C. W. C. Dawkins Checked by: T. L. Cairns and D. C. EnglandPublished in Org. Synth. 1955, 35, 73 Org. Synth. 1963, Coll. Vol. 4, 520

44 | P a g e





HEXAMETHYLENE DIISOCYANATE

Submitted by: Mark W. Farlow Checked by: R. L. Shriner and Robert C. JohnsonPublished in Org. Synth. 1951, 31, 62 Org. Synth. 1963, Coll. Vol. 4, 521

n -HEXYL FLUORIDE

Submitted by: Arthur I. Vogel, James Leicester, and William A. T. Macey Checked by: T. L. Cairns and C. W. TullockPublished in Org. Synth. 1956, 36, 40 Org. Synth. 1963, Coll. Vol. 4, 525

4-HYDROXY-1-BUTANESULFONIC ACID SULTONE

Submitted by: A. O. Snoddy

Checked by: T. L. Cairns and W. R. BrasenPublished in Org. Synth. 1957, 37, 55 Org. Synth. 1963, Coll. Vol. 4, 529

6-HYDROXYNICOTINIC ACID

Submitted by: J. H. Boyer and W. Schoen Checked by: T. L. Cairns and W. J. LinnPublished in Org. Synth. 1956, 36, 44 Org. Synth. 1963, Coll. Vol. 4, 532

3-HYDROXYTETRAHYDROFURAN

Submitted by: Hans Wynberg and A. Bantjes Checked by: John C. Sheehan and Gregory L. Boshart

45 | P a g e







INDAZOLE

Submitted by: C. Ainsworth Checked by: Max Tishler, George Gal, and G. A. SteinPublished in Org. Synth. 1959, 39, 27 Org. Synth. 1963, Coll. Vol. 4, 536

INDOLE-3-ALDEHYDE

Submitted by: Philip N. James and H. R. Snyder Checked by: Virgil Boekelheide and Richard N. KnowlesPublished in Org. Synth. 1959, 39, 30 Org. Synth. 1963, Coll. Vol. 4, 539

IODOCYCLOHEXANE

Submitted by: Herman Stone and Harold Shechter Checked by: T. L. Cairns and V. A. EngelhardtPublished in Org. Synth. 1951, 31, 66 Org. Synth. 1963, Coll. Vol. 4, 543

2-IODOTHIOPHENE

Submitted by: Henry Y. Lew and C. R. Noller Checked by: Cliff S. Hamilton and Frank A. BowerPublished in Org. Synth. 1950, 30, 53 Org. Synth. 1963, Coll. Vol. 4, 545

4-IODOVERATROLE

Submitted by: Donald E. Janssen and C. V. Wilson

Checked by: Max Tishler and George PurduePublished in Org. Synth. 1956, 36, 46 Org. Synth. 1963, Coll. Vol. 4, 547

46 | P a g e






ISODEHYDROACETIC ACID AND ETHYL ISODEHYDROACETATE

Submitted by: Newton R. Smith and Richard H. Wiley Checked by: R. S. Schreiber and H. H. FallPublished in Org. Synth. 1952, 32, 76 Org. Synth. 1963, Coll. Vol. 4, 549

ISOPHORONE OXIDE

Submitted by: Richard L. Wasson and Herbert O. House Checked by: James Cason and Ralph J. FessendenPublished in Org. Synth. 1957, 37, 58 Org. Synth. 1963, Coll. Vol. 4, 552

ITACONYL CHLORIDE

Submitted by: Henry Feuer and Stanley M. Pier Checked by: William S. Johnson and Ernest F. SilversmithPublished in Org. Synth. 1953, 33, 41 Org. Synth. 1963, Coll. Vol. 4, 554

6-KETOHENDECANEDIOIC ACID


β-KETOISOÖCTALDEHYDE DIMETHYL ACETAL

Submitted by: Charles C. Price and Joseph A. Pappalardo

47 | P a g e






Checked by: R. S. Schreiber, Wm. Bradley Reid, Jr, and R. W. JacksonPublished in Org. Synth. 1952, 32, 79 Org. Synth. 1963, Coll. Vol. 4, 558

LAURONE

Submitted by: J. C. Sauer Checked by: William S. Johnson and H. C. DehmPublished in Org. Synth. 1951, 31, 68 Org. Synth. 1963, Coll. Vol. 4, 560

LAURYLMETHYLAMINE

Submitted by: C. V. Wilson and J. F. Stenberg Checked by: N. J. Leonard and C. W. SchimelpfenigPublished in Org. Synth. 1956, 36, 48 Org. Synth. 1963, Coll. Vol. 4, 564

2-MERCAPTO-4-AMINO-5-CARBETHOXYPYRIMIDINE AND 2-MERCAPTO-4-HYDROXY-5-CYANOPYRIMIDINE

Submitted by: T. L. V. Ulbricht, Takuo Okuda, and Charles C. Price Checked by: B. C. McKusick and Stephen ProskowPublished in Org. Synth. 1959, 39, 34 Org. Synth. 1963, Coll. Vol. 4, 566

2-MERCAPTOBENZIMIDAZOLE

Submitted by: J. A. VanAllan and B. D. Deacon Checked by: Cliff S. Hamilton and Yao-Hua WuPublished in Org. Synth. 1950, 30, 56 Org. Synth. 1963, Coll. Vol. 4, 569

48 | P a g e





METHANESULFONYL CHLORIDE

Submitted by: Peter J. Hearst and C. R. Noller Checked by: R. S. Schreiber, B. D. Aspergren, and R. V. HeinzelmannPublished in Org. Synth. 1950, 30, 58 Org. Synth. 1963, Coll. Vol. 4, 571

o -METHOXYPHENYLACETONE

Submitted by: R. V. Heinzelman Checked by: M. Tishler and H. L. SlatesPublished in Org. Synth. 1955, 35, 74 Org. Synth. 1963, Coll. Vol. 4, 573

p -METHOXYPHENYLACETONITRILE

Submitted by: Kurt Rorig, J. Derland Johnston, Robert W. Hamilton, and Thomas J. Telinski Checked by: William S. Johnson, Stanley Seltzer, and Peter YatesPublished in Org. Synth. 1956, 36, 50 Org. Synth. 1963, Coll. Vol. 4, 576

METHYL p -ACETYLBENZOATE

Submitted by: William S. Emerson and George F. Deebel Checked by: Arthur C. Cope and Warren N. BaxterPublished in Org. Synth. 1952, 32, 81 Org. Synth. 1963, Coll. Vol. 4, 579

o -METHYLBENZYL ALCOHOL

Submitted by: W. R. Brasen and C. R. Hauser Checked by: William S. Johnson, Donald W. Stoutamire, and A. L. WildsPublished in Org. Synth. 1954, 34, 58 Org. Synth. 1963, Coll. Vol. 4, 582

49 | P a g e






2-METHYLBENZYLDIMETHYLAMINE

Submitted by: W. R. Brasen and C. R. Hauser Checked by: William S. Johnson, Mary E. Mills, and A. L. WildsPublished in Org. Synth. 1954, 34, 61 Org. Synth. 1963, Coll. Vol. 4, 585

O-METHYLCAPROLACTIM

Submitted by: Richard E. Benson and Theodore L. Cairns Checked by: Charles C. Price, Kenneth N. Campbell, and Richard McbridePublished in Org. Synth. 1951, 31, 72


3-METHYLCOUMARONE

Submitted by: Werner R. Boehme Checked by: James Cason and Kenneth L. RinehartPublished in Org. Synth. 1953, 33, 43 Org. Synth. 1963, Coll. Vol. 4, 590

50 | P a g e




METHYL CYCLOPENTANECARBOXYLATE

Submitted by: D. W. Goheen and W. R. Vaughan Checked by: N. J. Leonard, M. J. Konz, W. H. Pittman, and K. L. Rinehart, JrPublished in Org. Synth. 1959, 39, 37 Org. Synth. 1963, Coll. Vol. 4, 594

METHYL CYCLOPROPYL KETONE

Submitted by: George W. Cannon, Ray C. Ellis, and Joseph R. Leal Checked by: R. S. Schreiber, Wm. Bradley Reid, Jr, and R. D. BirkenmeyerPublished in Org. Synth. 1951, 31, 74 Org. Synth. 1963, Coll. Vol. 4, 597

2-METHYL-2,5-DECANEDIOL

Submitted by: J. Colonge and R. Marey Checked by: V. Boekelheide and H. KaempfenPublished in Org. Synth. 1958, 38, 41 Org. Synth. 1963, Coll. Vol. 4, 601

51 | P a g e




N-METHYL-2,3-DIMETHOXYBENZYLAMINE

Submitted by: Don M. Balcom and C. R. Noller Checked by: Homer Adkins and Walter W. GilbertPublished in Org. Synth. 1950, 30, 59 Org. Synth. 1963, Coll. Vol. 4, 603

N-METHYL-1,2-DIPHENYLETHYLAMINE AND HYDROCHLORIDE

Submitted by: Robert Bruce Moffett Checked by: N. J. Leonard and L. A. MillerPublished in Org. Synth. 1954, 34, 64 Org. Synth. 1963, Coll. Vol. 4, 605

trans -2-METHYL-2-DODECENOIC ACID

Submitted by: C. Freeman Allen and Max J. Kalm Checked by: William S. Johnson and H. W. Whitlock, JrPublished in Org. Synth. 1958, 38, 43 Org. Synth. 1963, Coll. Vol. 4, 608

52 | P a g e




METHYLENECYCLOHEXANE AND N,N-DIMETHYLHYDROXYLAMINE HYDROCHLORIDE

Submitted by: Arthur C. Cope and Engelbert Ciganek Checked by: William E. Parham and Robert KoncosPublished in Org. Synth. 1959, 39, 40 Org. Synth. 1963, Coll. Vol. 4, 612

2-METHYLENEDODECANOIC ACID

Submitted by: C. Freeman Allen and Max J. Kalm Checked by: William S. Johnson and Kenneth L. WilliamsonPublished in Org. Synth. 1958, 38, 47 Org. Synth. 1963, Coll. Vol. 4, 616

1-METHYL-3-ETHYLOXINDOLE

Submitted by: M. W. Rutenberg and E. C. Horning

Checked by: William S. Johnson and C. A. EricksonPublished in Org. Synth. 1950, 30, 62 Org. Synth. 1963, Coll. Vol. 4, 620

53 | P a g e




9-METHYLFLUORENE

Submitted by: Kurt L. Schoen and E. I. Becker Checked by: William S. Johnson and V. B. HaarstadPublished in Org. Synth. 1959, 39, 43 Org. Synth. 1963, Coll. Vol. 4, 623

5-METHYLFURFURYLDIMETHYLAMINE

Submitted by: Ernest L. Eliel and Milton T. Fisk Checked by: James Cason, Mary S. Nakata, and William G. DaubenPublished in Org. Synth. 1955, 35, 78 Org. Synth. 1963, Coll. Vol. 4, 626

3-METHYL-2-FUROIC ACID AND 3-METHYLFURAN

Submitted by: D. M. Burness Checked by: James Cason and Robert B. HutchisonPublished in Org. Synth. 1959, 39, 46 Org. Synth. 1963, Coll. Vol. 4, 628

β-METHYLGLUTARIC ANHYDRIDE

Submitted by: James Cason Checked by: B. C. McKusick, R. D. Smith, and W. R. HatchardPublished in Org. Synth. 1958, 38, 52 Org. Synth. 1963, Coll. Vol. 4, 630

54 | P a g e





METHYLGLYOXAL-ω-PHENYLHYDRAZONE

Submitted by: George A. Reynolds and J. A. VanAllan Checked by: T. L. Cairns and C. T. HandyPublished in Org. Synth. 1952, 32, 84 Org. Synth. 1963, Coll. Vol. 4, 633

METHYL HYDROGEN HENDECANEDIOATE


4-METHYL-6-HYDROXYPYRIMIDINE

Submitted by: H. M. Foster and H. R. Snyder Checked by: R. T. Arnold and P. E. ThrockmortonPublished in Org. Synth. 1955, 35, 80 Org. Synth. 1963, Coll. Vol. 4, 638

1-METHYLISOQUINOLINE

Submitted by: J. Weinstock and V. Boekelheide Checked by: N. J. Leonard, Terry W. Milligan, and William R. Sherman

55 | P a g e






METHYLISOUREA HYDROCHLORIDE

Submitted by: Frederick Kurzer and Alexander Lawson Checked by: William S. Johnson and William T. TsatsosPublished in Org. Synth. 1954, 34, 67 Org. Synth. 1963, Coll. Vol. 4, 645

METHYL 3-METHYL-2-FUROATE

Submitted by: D. M. Burness

Checked by: James Cason and Robert B. HutchisonPublished in Org. Synth. 1959, 39, 49 Org. Synth. 1963, Coll. Vol. 4, 649

METHYL γ-METHYL-γ-NITROVALERATE

Submitted by: R. B. Moffett Checked by: N. J. Leonard and B. L. RyderPublished in Org. Synth. 1952, 32, 86 Org. Synth. 1963, Coll. Vol. 4, 652

3-METHYL-4-NITROPYRIDINE-1-OXIDE


Checked by: Max Tishler and Henry B. LangePublished in Org. Synth. 1956, 36, 53 Org. Synth. 1963, Coll. Vol. 4, 654

56 | P a g e





3-METHYLOXINDOLE

Submitted by: Abraham S. Endler and Ernest I. Becker Checked by: James Cason and Warren N. BaxterPublished in Org. Synth. 1957, 37, 60 Org. Synth. 1963, Coll. Vol. 4, 657

3-METHYL-1,5-PENTANEDIOL

Submitted by: Raymond I. Longley, Jr and William S. Emerson Checked by: T. L. Cairns and John F. Harris, JrPublished in Org. Synth. 1954, 34, 71 Org. Synth. 1963, Coll. Vol. 4, 660

β-METHYL-β-PHENYL-α,α'-DICYANOGLUTARIMIDE

Submitted by: S. M. McElvain and David H. Clemens Checked by: W. E. Parham, Perry W. Kirklin, Jr, and Wayland E. NolandPublished in Org. Synth. 1959, 39, 52 Org. Synth. 1963, Coll. Vol. 4, 662

β-METHYL-β-PHENYLGLUTARIC ACID

Submitted by: S. M. McElvain and David H. Clemens

57 | P a g e





Checked by: W. E. Parham, Perry W. Kirklin, Jr, and Wayland E. NolandPublished in Org. Synth. 1959, 39, 54 Org. Synth. 1963, Coll. Vol. 4, 664

1-METHYL-3-PHENYLINDANE

Submitted by: Milton J. Rosen Checked by: R. T. Arnold and William K. WitsiepePublished in Org. Synth. 1955, 35, 83 Org. Synth. 1963, Coll. Vol. 4, 665

METHYL 2-THIENYL SULFIDE

Submitted by: J. Cymerman-Craig and J. W. Loder

Checked by: Charles C. Price and E. A. DudleyPublished in Org. Synth. 1955, 35, 85 Org. Synth. 1963, Coll. Vol. 4, 667

METHYL β-THIODIPROPIONATE

Submitted by: Edward A. Fehnel and Marvin Carmack Checked by: Arthur C. Cope and James J. RyanPublished in Org. Synth. 1950, 30, 65 Org. Synth. 1963, Coll. Vol. 4, 669

3-METHYLTHIOPHENE

Submitted by: R. F. Feldkamp and B. F. Tullar Checked by: Cliff S. Hamilton, Y. H. Wu, and William J. RaichPublished in Org. Synth. 1954, 34, 73 Org. Synth. 1963, Coll. Vol. 4, 671

58 | P a g e





METHYL p -TOLYL SULFONE

Submitted by: L. Field and R. D. Clark Checked by: John C. Sheehan and M. Gertrude HowellPublished in Org. Synth. 1958, 38, 62 Org. Synth. 1963, Coll. Vol. 4, 674

β-METHYL-δ-VALEROLACTONE

Submitted by: Raymond I. Longley, Jr and William S. Emerson Checked by: T. L. Cairns and W. W. GilbertPublished in Org. Synth. 1955, 35, 87 Org. Synth. 1963, Coll. Vol. 4, 677

MONOBENZALPENTAERYTHRITOL

Submitted by: C. H. Issidorides and R. Gulen Checked by: M. S. Newman and Arlen B. MeklerPublished in Org. Synth. 1958, 38, 65


MONOBROMOPENTAERYTHRITOL

Submitted by: S. Wawzonek, A. Matar, and C. H. Issidorides Checked by: Charles C. Price and G. Venkat RaoPublished in Org. Synth. 1958, 38, 68 Org. Synth. 1963, Coll. Vol. 4, 681

MONOVINYLACETYLENE

Submitted by: G. F. Hennion, Charles C. Price, and Thomas F. McKeon, Jr Checked by: Max Tishler and John E. AllegrettiPublished in Org. Synth. 1958, 38, 70 Org. Synth. 1963, Coll. Vol. 4, 683

MUCOBROMIC ACID

Submitted by: G. A. Taylor Checked by: B. C. McKusick, E. L. Martin, and

59 | P a g e







W. R. Brasen


1-NAPHTHALDEHYDE

Submitted by: S. J. Angyal, J. R. Tetaz, and J. G. Wilson Checked by: R. S. Schreiber and Paul E. MarlattPublished in Org. Synth. 1950, 30, 67 Org. Synth. 1963, Coll. Vol. 4, 690

NAPHTHALENE-1,5-DISULFONYL CHLORIDE

Submitted by: P. D. Caesar Checked by: R. T. Arnold and George P. ScottPublished in Org. Synth. 1952, 32, 88 Org. Synth. 1963, Coll. Vol. 4, 693

1,5-NAPHTHALENEDITHIOL

Submitted by: P. D. Caesar Checked by: Richard T. Arnold, W. E. Parham, and R. M. ScribnerPublished in Org. Synth. 1953, 33, 47 Org. Synth. 1963, Coll. Vol. 4, 695

1,4-NAPHTHOQUINONE

Submitted by: E. A. Braude and J. S. Fawcett Checked by: Charles C. Price, R. S. Schreiber, R. D. Birkenmeyer, Paul F. Kirk, and William Bradley Reid, JrPublished in Org. Synth. 1953, 33, 50 Org. Synth. 1963, Coll. Vol. 4, 698

60 | P a g e





α-NAPHTHYL ISOTHIOCYANATE

Submitted by: J. Cymerman-Craig, M. Moyle, and R. A. White Checked by: N. J. Leonard and F. H. OwensPublished in Org. Synth. 1956, 36, 56 Org. Synth. 1963, Coll. Vol. 4, 700

NEOPHYL CHLORIDE

Submitted by: W. T. Smith, Jr and J. T. Sellas Checked by: N. J. Leonard and R. O. KerrPublished in Org. Synth. 1952, 32, 90 Org. Synth. 1963, Coll. Vol. 4, 702

NICOTINAMIDE-1-OXIDE


Checked by: Charles C. Price and Walter A. SchroederPublished in Org. Synth. 1957, 37, 63


NICOTINONITRILE

Submitted by: Peyton C. Teague and William A. Short Checked by: Arthur C. Cope, John C. Sheehan, and Louis A. CohenPublished in Org. Synth. 1953, 33, 52 Org. Synth. 1963, Coll. Vol. 4, 706

o -NITROACETOPHENONE

Submitted by: George A. Reynolds and Charles R. Hauser Checked by: Cliff S. Hamilton and Yao-Hua WuPublished in Org. Synth. 1950, 30, 70 Org. Synth. 1963, Coll. Vol. 4, 708

61 | P a g e






9-NITROANTHRACENE

Submitted by: Charles E. Braun, Clinton D. Cook, Charles Merritt, Jr, and Joseph E. Rousseau Checked by: William S. Johnson, George N. Sausen, and Paul R. ShaferPublished in Org. Synth. 1951, 31, 77 Org. Synth. 1963, Coll. Vol. 4, 711

o - AND p -NITROBENZALDIACETATE

Submitted by: Tamio Nishimura Checked by: T. L. Cairns and R. E. FosterPublished in Org. Synth. 1956, 36, 58 Org. Synth. 1963, Coll. Vol. 4, 713

m -NITROBENZAZIDE

Submitted by: Jon Munch-Petersen Checked by: William S. Johnson and W. David WoodPublished in Org. Synth. 1953, 33, 53 Org. Synth. 1963, Coll. Vol. 4, 715

m -NITROBIPHENYL

Submitted by: C. E. Kaslow and R. M. Summers

62 | P a g e





Checked by: James Cason and B. H. WalkerPublished in Org. Synth. 1953, 33, 56 Org. Synth. 1963, Coll. Vol. 4, 718

o -NITROCINNAMALDEHYDE

Submitted by: Robert E. Buckles and M. Peter Bellis Checked by: Richard T. Arnold and James D. GrovesPublished in Org. Synth. 1953, 33, 60 Org. Synth. 1963, Coll. Vol. 4, 722

1-NITROÖCTANE

Submitted by: N. Kornblum and H. E. Ungnade

Checked by: John C. Sheehan and M. Gertrude HowellPublished in Org. Synth. 1958, 38, 75 Org. Synth. 1963, Coll. Vol. 4, 724

1-( p -NITROPHENYL)-1,3-BUTADIENE

Submitted by: Gus A. Ropp and Eugene C. Coyner

Checked by: Arthur C. Cope and David J. MarshallPublished in Org. Synth. 1951, 31, 80 Org. Synth. 1963, Coll. Vol. 4, 727

trans - o -NITRO-α-PHENYLCINNAMIC ACID

Submitted by: DeLos F. DeTar Checked by: Charles C. Price and J. D. BermanPublished in Org. Synth. 1955, 35, 89

63 | P a g e






m -NITROSTYRENE

Submitted by: Richard H. Wiley and Newton R. Smith Checked by: Richard T. Arnold, William E. Parham, and Darwin D. DavisPublished in Org. Synth. 1953, 33, 62 Org. Synth. 1963, Coll. Vol. 4, 731

6-NITROVERATRALDEHYDE

Submitted by: Charles A. Fetscher Checked by: Richard T. Arnold, W. E. Parham, and Donald A. LeisterPublished in Org. Synth. 1953, 33, 65 Org. Synth. 1963, Coll. Vol. 4, 735

NORBORNYLENE

Submitted by: J. Meinwald and N. J. Hudak Checked by: J. D. Roberts, C. M. Sharts, and W. G. WoodsPublished in Org. Synth. 1957, 37, 65 Org. Synth. 1963, Coll. Vol. 4, 738

OLEOYL CHLORIDE

Submitted by: C. F. H. Allen, J. R. Byers, and W. J. Humphlett Checked by: Max Tishler and R. ConnellPublished in Org. Synth. 1957, 37, 66 Org. Synth. 1963, Coll. Vol. 4, 739

PARABANIC ACID

Submitted by: Joseph I. Murray Checked by: M. S. Newman and Tadamichi FukunagaPublished in Org. Synth. 1957, 37, 71

64 | P a g e







1,4-PENTADIENE

Submitted by: R. E. Benson, B. C. McKusick, Oliver Grummitt, E. P. Budewitz, and C. C. Chudd

Checked by: N. J. Leonard, A. G. Cook, William S. Johnson, E. Saito, and Donald J. ReifPublished in Org. Synth. 1958, 38, 78 Org. Synth. 1963, Coll. Vol. 4, 746

PENTAERYTHRITYL TETRABROMIDE

Submitted by: Hershel L. Herzog Checked by: T. L. Cairns and D. W. WoodwardPublished in Org. Synth. 1951, 31, 82 Org. Synth. 1963, Coll. Vol. 4, 753

4-PENTYN-1-OL

Submitted by: E. R. H. Jones, Geoffrey Eglinton, and M. C. Whiting Checked by: Arthur C. Cope and Ronald M. PikePublished in Org. Synth. 1953, 33, 68 Org. Synth. 1963, Coll. Vol. 4, 755

PHENANTHRENEQUINONE

Submitted by: Ray Wendland and John LaLonde Checked by: William S. Johnson and Sol ShulmanPublished in Org. Synth. 1954, 34, 76 Org. Synth. 1963, Coll. Vol. 4, 757

65 | P a g e





PHENYLACETAMIDE

Submitted by: Wilhelm Wenner Checked by: William S. Johnson and Robert E. IrelandPublished in Org. Synth. 1952, 32, 92 Org. Synth. 1963, Coll. Vol. 4, 760

PHENYLACETYLENE

Submitted by: Kenneth N. Campbell and Barbara K. Campbell Checked by: R. S. Schreiber and H. E. CuperyPublished in Org. Synth. 1950, 30, 72 Org. Synth. 1963, Coll. Vol. 4, 763

γ-PHENYLALLYLSUCCINIC ACID

Submitted by: Christian S. Rondestvedt, Jr Checked by: Charles C. Price and Wm. J. BelangerPublished in Org. Synth. 1951, 31, 85 Org. Synth. 1963, Coll. Vol. 4, 766

N-PHENYLBENZAMIDINE

Submitted by: F. C. Cooper and M. W. Partridge Checked by: T. L. Cairns, R. E. Benson, and V. J. WebersPublished in Org. Synth. 1956, 36, 64 Org. Synth. 1963, Coll. Vol. 4, 769

trans -1-PHENYL-1,3-BUTADIENE

Submitted by: Oliver Grummitt and Ernest I. Becker Checked by: Charles C. Price and T. L. PattonPublished in Org. Synth. 1950, 30, 75 Org. Synth. 1963, Coll. Vol. 4, 771

66 | P a g e






α-PHENYL-α-CARBETHOXYGLUTARONITRILE


α-PHENYLCINNAMIC ACID

Submitted by: Robert E. Buckles and Keith Bremer Checked by: T. L. Cairns and J. C. LorenzPublished in Org. Synth. 1953, 33, 70 Org. Synth. 1963, Coll. Vol. 4, 777

2-PHENYLCYCLOHEPTANONE

Submitted by: C. David Gutsche and Herbert E. Johnson Checked by: N. J. Leonard and F. P. Hauck, JrPublished in Org. Synth. 1955, 35, 91 Org. Synth. 1963, Coll. Vol. 4, 780

PHENYLDICHLOROPHOSPHINE

Submitted by: B. Buchner and L. B. Lockhart, Jr Checked by: Cliff S. Hamilton and P. J. VanderhorstPublished in Org. Synth. 1951, 31, 88 Org. Synth. 1963, Coll. Vol. 4, 784

67 | P a g e





4-PHENYL- m -DIOXANE

Submitted by: R. L. Shriner and Philip R. Ruby Checked by: Richard T. Arnold, W. E. Parham, and John E. FranzPublished in Org. Synth. 1953, 33, 72 Org. Synth. 1963, Coll. Vol. 4, 786

o -PHENYLENE CARBONATE

Submitted by: R. S. Hanslick, W. F. Bruce, and A. Mascitti Checked by: Arthur C. Cope, Harris E. Petree, and Elmer R. TrumbullPublished in Org. Synth. 1953, 33, 74 Org. Synth. 1963, Coll. Vol. 4, 788

α-PHENYLGLUTARIC ANHYDRIDE


1-PHENYL-1-PENTEN-4-YN-3-OL

Submitted by: Lars Skattebøl, E. R. H. Jones, and Mark C. Whiting Checked by: Melvin S. Newman and Raymond E. DessyPublished in Org. Synth. 1959, 39, 56 Org. Synth. 1963, Coll. Vol. 4, 792

1-PHENYLPIPERIDINE

Submitted by: A. N. Bourns, H. W. Embleton, and Mary K. Hansuld Checked by: R. T. Arnold, William E. Parham, and Carl SerresPublished in Org. Synth. 1954, 34, 79 Org. Synth. 1963, Coll. Vol. 4, 795

68 | P a g e






3-PHENYL-1-PROPANOL

Submitted by: R. L. Shriner and Philip R. Ruby Checked by: Richard T. Arnold, W. E. Parham, and Hans WynbergPublished in Org. Synth. 1953, 33, 76 Org. Synth. 1963, Coll. Vol. 4, 798

PHENYLPROPARGYLALDEHYDE DIETHYL ACETAL

Submitted by: B. W. Howk and J. C. Sauer Checked by: N. J. Leonard and S. W. BlumPublished in Org. Synth. 1959, 39, 59 Org. Synth. 1963, Coll. Vol. 4, 801

PHENYLSUCCINIC ACID

Submitted by: C. F. H. Allen and H. B. Johnson Checked by: H. R. Snyder, D. J. Mann, and Leonard E. Miller


o -PHTHALALDEHYDE

Submitted by: J. C. Bill and D. S. Tarbell Checked by: Arthur C. Cope and Harris E. PetreePublished in Org. Synth. 1954, 34, 82 Org. Synth. 1963, Coll. Vol. 4, 807

α-PHTHALIMIDO- o -TOLUIC ACID

Submitted by: J. Bornstein, P. E. Drummond, and S. F. Bedell Checked by: John C. Sheehan and Y. L. YehPublished in Org. Synth. 1958, 38, 81 Org. Synth. 1963, Coll. Vol. 4, 810

69 | P a g e






PROPIOLALDEHYDE

Submitted by: J. C. Sauer Checked by: John C. Sheehan and E. R. GilmontPublished in Org. Synth. 1956, 36, 66 Org. Synth. 1963, Coll. Vol. 4, 813

PSEUDOPELLETIERINE

Submitted by: Arthur C. Cope, Hugh L. Dryden, Jr, and Charles F. Howell Checked by: N. J. Leonard, D. F. Morrow, and W. D. SmartPublished in Org. Synth. 1957, 37, 73 Org. Synth. 1963, Coll. Vol. 4, 816

PUTRESCINE DIHYDROCHLORIDE

Submitted by: Peter A. S. Smith Checked by: James Cason and Wm. DeAcetisPublished in Org. Synth. 1956, 36, 69 Org. Synth. 1963, Coll. Vol. 4, 819

2,3-PYRAZINEDICARBOXYLIC ACID

Submitted by: Reuben G. Jones and Keith C. McLaughlin Checked by: H. R. Snyder and R. E. HeckertPublished in Org. Synth. 1950, 30, 86

70 | P a g e






PYRIDINE-N-OXIDE

Submitted by: Harry S. Mosher, Leslie Turner, and Allan Carlsmith Checked by: N. J. Leonard and E. D. SutorisPublished in Org. Synth. 1953, 33, 79 Org. Synth. 1963, Coll. Vol. 4, 828

2-PYRROLEALDEHYDE

Submitted by: Robert M. Silverstein, Edward E. Ryskiewicz, and Constance Willard Checked by: Max Tishler and George PurduePublished in Org. Synth. 1956, 36, 74 Org. Synth. 1963, Coll. Vol. 4, 831

71 | P a g e



Top of Form

2-(1-PYRROLIDYL)PROPANOL

Submitted by: Robert Bruce Moffett Checked by: N. J. Leonard and S. GelfandPublished in Org. Synth. 1953, 33, 82 Org. Synth. 1963, Coll. Vol. 4, 834

QUINACETOPHENONE MONOMETHYL ETHER

Submitted by: G. N. Vyas and N. M. Shah Checked by: William S. Johnson and R. T. KellerPublished in Org. Synth. 1951, 31, 90 Org. Synth. 1963, Coll. Vol. 4, 836

SEBACIL

Submitted by: A. T. Blomquist and Albert Goldstein Checked by: N. J. Leonard and J. C. LittlePublished in Org. Synth. 1956, 36, 77 Org. Synth. 1963, Coll. Vol. 4, 838

72 | P a g e




SEBACOIN

Submitted by: Norman L. Allinger Checked by: N. J. Leonard, J. C. Little, and F. H. OwensPublished in Org. Synth. 1956, 36, 79 Org. Synth. 1963, Coll. Vol. 4, 840

SODIUM NITROMALONALDEHYDE MONOHYDRATE

Submitted by: Paul E. Fanta Checked by: Cliff S. Hamilton and Philip J. VanderhorstPublished in Org. Synth. 1952, 32, 95 Org. Synth. 1963, Coll. Vol. 4, 844

SODIUM β-STYRENESULFONATE AND β-

STYRENESULFONYL CHLORIDE

Submitted by: Christian S. Rondestvedt, Jr and F. G. Bordwell Checked by: T. L. Cairns and H. E. WinbergPublished in Org. Synth. 1954, 34, 85 Org. Synth. 1963, Coll. Vol. 4, 846

STEAROLIC ACID

Submitted by: N. A. Khan, F. E. Deatherage, and J. B. Brown Checked by: Max Tishler, W. J. Paleveda, and E. F. SchoenewaldtPublished in Org. Synth. 1957, 37, 77 Org. Synth. 1963, Coll. Vol. 4, 851

STEARONE

Submitted by: A. G. Dobson and H. H. Hatt Checked by: R. L. Shriner and Philip R. RubyPublished in Org. Synth. 1953, 33, 84 Org. Synth. 1963, Coll. Vol. 4, 854

73 | P a g e






cis -STILBENE

Submitted by: Robert E. Buckles and Norris G. Wheeler Checked by: T. L. Cairns and J. C. LorenzPublished in Org. Synth. 1953, 33, 88 Org. Synth. 1963, Coll. Vol. 4, 857

trans -STILBENE OXIDE

Submitted by: Donald J. Reif and Herbert O. House Checked by: Melvin S. Newman and Donald K. PhillipsPublished in Org. Synth. 1958, 38, 83 Org. Synth. 1963, Coll. Vol. 4, 860

α-SULFOPALMITIC ACID

Submitted by: J. K. Weil, R. G. Bistline, Jr, and A.

J. Stirton Checked by: James Cason and Gerhard J. FonkenPublished in Org. Synth. 1956, 36, 83 Org. Synth. 1963, Coll. Vol. 4, 862

SYRINGIC ALDEHYDE

Submitted by: C. F. H. Allen and Gerhard W. Leubner Checked by: R. S. Schreiber, Wm. Bradley Reid, Jr, and R. W. JacksonPublished in Org. Synth. 1951, 31, 92 Org. Synth. 1963, Coll. Vol. 4, 866

TETRAACETYLETHANE

Submitted by: Robert G. Charles Checked by: Virgil Boekelheide and Henry FleischerPublished in Org. Synth. 1959, 39, 61 Org. Synth. 1963, Coll. Vol. 4, 869

74 | P a g e






dl -4,4',6,6'-TETRACHLORODIPHENIC ACID

Submitted by: Edward R. Atkinson, Donald M. Murphy, and James E. Lufkin Checked by: R. S. Schreiber, Wm. Bradley Reid, Jr, and R. D. BirkenmeyerPublished in Org. Synth. 1951, 31, 96 Org. Synth. 1963, Coll. Vol. 4, 872

TETRACYANOETHYLENE

Submitted by: R. A. Carboni Checked by: James Cason and Edwin R. HarrisPublished in Org. Synth. 1959, 39, 64 Org. Synth. 1963, Coll. Vol. 4, 877

TETRAETHYLTIN

Submitted by: G. J. M. Van Der Kerk and J. G. A. Luijten Checked by: M. S. Newman and L. L. WoodPublished in Org. Synth. 1956, 36, 86 Org. Synth. 1963, Coll. Vol. 4, 881

1,2,3,4-TETRAHYDROCARBAZOLE

Submitted by: Crosby U. Rogers and B. B. Corson Checked by: Charles C. Price, Kenneth N. Campbell, and Robert P. KanePublished in Org. Synth. 1950, 30, 90 Org. Synth. 1963, Coll. Vol. 4, 884

75 | P a g e





ar -TETRAHYDRO-α-NAPHTHOL

Submitted by: C. David Gutsche and Hugo H. Peter Checked by: John C. Sheehan, George H. Buchi, and Dwain M. WhitePublished in Org. Synth. 1957, 37, 80 Org. Synth. 1963, Coll. Vol. 4, 887

cis -Δ 4 -TETRAHYDROPHTHALIC ANHYDRIDE

Submitted by: Arthur C. Cope and Elbert C. Herrick Checked by: Charles C. Price, Kenneth N. Campbell, and Robert P. KanePublished in Org. Synth. 1950, 30, 93 Org. Synth. 1963, Coll. Vol. 4, 890

TETRAHYDROTHIOPHENE

Submitted by: J. Keith Lawson, William K. Easley, and William S. Wagner Checked by: William S. Johnson and W. David WoodPublished in Org. Synth. 1956, 36, 89 Org. Synth. 1963, Coll. Vol. 4, 892

TETRALIN HYDROPEROXIDE

Submitted by: H. B. Knight and Daniel Swern Checked by: John C. Sheehan and Curt W. BeckPublished in Org. Synth. 1954, 34, 90 Org. Synth. 1963, Coll. Vol. 4, 895

α-TETRALONE

Submitted by: Cecil E. Olson, Alfred R. Bader, and G. Dana Johnson

76 | P a g e






Checked by: James Cason, Gerhard J. Fonken, William G. Dauben, James Cason, William G. Dauben, Bradford H. Walker, and Charles E. StehrPublished in Org. Synth. 1955, 35, 95 Org. Synth. 1963, Coll. Vol. 4, 898

β-TETRALONE

Submitted by: M. D. Soffer, M. P. Bellis, Hilda E. Gellerson, and Roberta A. Stewart Checked by: N. J. Leonard and R. C. FoxPublished in Org. Synth. 1952, 32, 97 Org. Synth. 1963, Coll. Vol. 4, 903

2,2,6,6-TETRAMETHYLOLCYCLOHEXANOL

Submitted by: Harold Wittcoff Checked by: R. S. Schreiber, Wm. Bradley Reid, Jr, and John L. WhitePublished in Org. Synth. 1951, 31, 101 Org. Synth. 1963, Coll. Vol. 4, 907

TETRAPHENYLARSONIUM CHLORIDE HYDROCHLORIDE

Submitted by: R. L. Shriner and Calvin N. Wolf Checked by: Cliff S. Hamilton and Yao-Hua WuPublished in Org. Synth. 1950, 30, 95 Org. Synth. 1963, Coll. Vol. 4, 910

TETRAPHENYLETHYLENE

Submitted by: Robert E. Buckles and George M. Matlack Checked by: T. L. Cairns and C. J. AlbisettiPublished in Org. Synth. 1951, 31, 104 Org. Synth. 1963, Coll. Vol. 4, 914

77 | P a g e





2-THENALDEHYDE

Submitted by: Arthur W. Weston and R. J. Michaels, Jr Checked by: Cliff S. Hamilton and Joe R. WillardPublished in Org. Synth. 1951, 31, 108 Org. Synth. 1963, Coll. Vol. 4, 915

3-THENALDEHYDE

Submitted by: E. Campaigne, R. C. Bourgeois, and W. C. McCarthy Checked by: Charles C. Price and E. A. DudleyPublished in Org. Synth. 1953, 33, 93 Org. Synth. 1963, Coll. Vol. 4, 918

3-THENOIC ACID

Submitted by: E. Campaigne and William M. LeSuer Checked by: Charles C. Price and E. A. DudleyPublished in Org. Synth. 1953, 33, 94 Org. Synth. 1963, Coll. Vol. 4, 919

3-THENYL BROMIDE

Submitted by: E. Campaigne and B. F. Tullar Checked by: Charles C. Price and E. A. DudleyPublished in Org. Synth. 1953, 33, 96 Org. Synth. 1963, Coll. Vol. 4, 921

THIOBENZOIC ACID

Submitted by: Paul Noble, Jr and D. S. Tarbell Checked by: William S. Johnson and Robert A. KlossPublished in Org. Synth. 1952, 32, 101 Org. Synth. 1963, Coll. Vol. 4, 924

78 | P a g e






THIOBENZOPHENONE

Submitted by: B. F. Gofton and E. A. Braude Checked by: Charles C. Price and J. Frank GillespiePublished in Org. Synth. 1955, 35, 97 Org. Synth. 1963, Coll. Vol. 4, 927

THIOLACETIC ACID

Submitted by: E. K. Ellingboe Checked by: Arthur C. Cope and Malcolm ChamberlainPublished in Org. Synth. 1951, 31, 105 Org. Synth. 1963, Coll. Vol. 4, 928

o -TOLUALDEHYDE

Submitted by: H. B. Hass and Myron L. Bender

Checked by: Arthur C. Cope and Malcolm ChamberlainPublished in Org. Synth. 1950, 30, 99 Org. Synth. 1963, Coll. Vol. 4, 932

p -TOLUENESULFENYL CHLORIDE

Submitted by: Frederick Kurzer and J. Roy Powell Checked by: Richard S. Schreiber and Fred KaganPublished in Org. Synth. 1955, 35, 99 Org. Synth. 1963, Coll. Vol. 4, 934

p -TOLUENESULFINYL CHLORIDE

Submitted by: Frederick Kurzer Checked by: Richard S. Schreiber and Fred KaganPublished in Org. Synth. 1954, 34, 93 Org. Synth. 1963, Coll. Vol. 4, 937

p -TOLUENESULFONIC ANHYDRIDE

Submitted by: L. Field and J. W. McFarland Checked by: William S. Johnson, Raymond R. Hindersinn, and A. G. Fisher

79 | P a g e








p - TOLYLSULFONYLMETHYLNITROSAMIDE

Submitted by: Th. J. de Boer and H. J. Backer Checked by: James Cason, John B. Rogan, and Wm. G. DaubenPublished in Org. Synth. 1954, 34, 96 Org. Synth. 1963, Coll. Vol. 4, 943

2,4,6-TRIBROMOBENZOIC ACID

Submitted by: Michael M. Robison and Bonnie L. Robison Checked by: N. J. Leonard and Kenneth ConrowPublished in Org. Synth. 1956, 36, 94 Org. Synth. 1963, Coll. Vol. 4, 947

TRICHLOROMETHYLPHOSPHONYL DICHLORIDE

Submitted by: Kenneth C. Kennard and Cliff S. Hamilton Checked by: John C. Sheehan and J. L. YehPublished in Org. Synth. 1957, 37, 82 Org. Synth. 1963, Coll. Vol. 4, 950

p -TRICYANOVINYL-N,N- DIMETHYLANILINE

Submitted by: B. C. McKusick and L. R. Melby Checked by: James Cason and Ralph J. FessendenPublished in Org. Synth. 1959, 39, 68 Org. Synth. 1963, Coll. Vol. 4, 953

80 | P a g e





TRIETHYL PHOSPHITE

Submitted by: A. H. Ford-Moore and B. J. Perry Checked by: William S. Johnson and James AckermanPublished in Org. Synth. 1951, 31, 111 Org. Synth. 1963, Coll. Vol. 4, 955

2,4,4-TRIMETHYLCYCLOPENTANONE

Submitted by: George D. Ryerson, Richard L. Wasson, and Herbert O. House Checked by: James Cason and Ralph J. Fessenden


α,β,β-TRIPHENYLPROPIONIC ACID

Submitted by: C. P. Krimmel, L. E. Thielen, E. A. Brown, and W. J. Heidtke Checked by: William S. Johnson, A. L. Wilds, and J. S. JellinekPublished in Org. Synth. 1953, 33, 98 Org. Synth. 1963, Coll. Vol. 4, 960

α,α,β-TRIPHENYLPROPIONITRILE

Submitted by: C. R. Hauser and W. R. Dunnavant Checked by: Virgil Boekelheide and Donald R. ArnoldPublished in Org. Synth. 1959, 39, 73 Org. Synth. 1963, Coll. Vol. 4, 962

TRIPTYCENE

Submitted by: George Wittig Checked by: John D. Roberts, M. C. Caserio, E. S. Johnson, and L. SkattebølPublished in Org. Synth. 1959, 39, 75 Org. Synth. 1963, Coll. Vol. 4, 964

81 | P a g e






TRITHIOCARBODIGLYCOLIC ACID

Submitted by: R. E. Strube Checked by: John D. Roberts and Stanley L. ManattPublished in Org. Synth. 1959, 39, 77 Org. Synth. 1963, Coll. Vol. 4, 967

10-UNDECYNOIC ACID

Submitted by: N. A. Khan Checked by: T. L. Cairns and D. H. SmithPublished in Org. Synth. 1952, 32, 104 Org. Synth. 1963, Coll. Vol. 4, 969

VANILLIC ACID

Submitted by: Irwin A. Pearl and Irwin A. Pearl Checked by: R. L. Shriner, Calvin N. Wolf, R. L. Shriner, and Robert C. JohnsonPublished in Org. Synth. 1950, 30, 101 Org. Synth. 1963, Coll. Vol. 4, 972

82 | P a g e





2-VINYLTHIOPHENE

Submitted by: W. S. Emerson and T. M. Patrick, Jr

Checked by: Max Tishler, P. Tishler, and F. W. BollingerPublished in Org. Synth. 1958, 38, 86 Org. Synth. 1963, Coll. Vol. 4, 980

o -XYLYLENE DIBROMIDE

Submitted by: Emily F. M. Stephenson Checked by: William S. Johnson, C. W. Taylor, and William DeAcetisPublished in Org. Synth. 1954, 34, 100 Org. Synth. 1963, Coll. Vol. 4, 984

83 | P a g e



CV4

Documents

Transcript of CV4