CONT SP-FE-0001,Rev .6 List of analysis parameters with Reference SP-DP12-0001List of... · LIST OF...

Rev. No: 6

page :1 of 23

LIST OF ANALYSIS PARAMETERS WITH REFERENCE METHODS

Dubai Central laboratory

Doc.Ref : SP-FE-0001

Issue Date :04/04/2016

CONTROLLED COPYCONTROLLED COPY

Authorized by: HOSIssued by :SQO

Note: Printed copy of this document shall be treated as ‘Uncontrolled’. Always refer the controlled version ‘Online


Rev. No: 6

page :2 of 23





S.No.Clause

AmendedDate Authorisaton

1 Heading 30/11/2011 HOS

2 All Clause 30/11/2011 HOS

3 - 30/11/2011 HOS

4 - 30/11/2011 HOS

5 Reference 30/11/2011 HOS


7 - 18/11/2012 HOS

18/11/2012 HOS

18/11/2012 HOS

18/11/2012 HOS

18/11/2012 HOS

9 18/11/2012 HOS

10 18/11/2012 HOS

22/11/2012 HOS

22/11/2012 HOS

Part 2-FCAU

Added sSOP-FE-2324 & SOP-FE-(2265,2347) & BSEN 13805:2002 to list

Part 3 -Env

8 Part 1-FMAU

Eliminated salmonella spp by Rabit technique and added 10 or as per dilution factor to solid

part of SOP-FE-3117.

Test duration (days) modified from 4 to7 days increased in SOP-FE-3105.

Added two new SOPs-FE-(1132,1133,1134) with the price in Env.unit

Modified tittle of two SOPs (3119 and 3120)

Test duration (days) incrased in Food chemical Analysis unit. Reference for

SOPs(2260,2261,2262,& 2263) replaced AOAC, 17th Edn. 2000 to AOAC, 16th Edn. 1998

11

Added three new SOPs-FE-(3122 &3123,3124) with the price in FMAU

Added Physical analysis fees

Added Government cost to list

Nature of Amendment

Change standard method 18th to 21 th

SP-DP12-0001(FE) changed to SP-FE-0001as per IMS requirement

AMENDMENT RECORD

SOPs numbring system changed from three digit number to four digit number system.

Added Chlorate(ClO30) and Chorite(Cl20) to SOP-FE-1130

Added two SOP-FE-2345 & 2346 with the price

Standard methods- 21 ST Edition instead of 18 th edition and MOOPAM 4th instead of 3rd

edition in Env list

22/11/2012 HOS

22/11/2012 HOS

22/11/2012 HOS

12 3.1 22/11/2012 HOS

13 - 22/11/2012 HOS

14 - 22/11/2012 HOS

15 20/01/2014 HOS

16 20/01/2014 HOS

17 20/01/2014 HOS

18 20/01/2014 HOS

19 Part 3 -Env 20/01/2014 HOS

20 Part 1-FMAU 09/02/2015 HOS

21 Part 2-FCAU 09/02/2015 HOS

22 Part 3 -Env 09/02/2015 HOS


24 Pari 1-FMAU 04/04/2016 HOS

25 Part2-FCAU 04/04/2016 HOS

26 Part 3 -ENVU 04/04/2016 HOS

Added new SOP-FE(3130 & 3131) with the price of tests and changed Test duation in

Yersinia entrocolitica.

Part 3 -Env

Method detection changed from 5 to 7,Changed reporting unit in SOP-FE-1124 from mg/l to

ug/L and removed waster water in sample type. Chaged method detection in SOP-FE-1128

z(Cd from 0.04 to 0.08,Zn from 0.04 to 0.05 ,Co from 0.1 to 0.12). Reduced method detection

in SOP-FE-1130 for (BrO3 from 5 to 3). TDS / EC Meter replaced of APHA-2130B in SOP-

FE-1105 for drinking water. Added sampling with price to list.

Added SOP-FE-2206 & Determination of traces elements of As*,Cd*,Hg*,Pb* by BS EN

15763:2009 with the price of tests

Added new SOPs (SOP-FE-2370 & 2371) to list

Changed the titles ,sample type and Duration time. Added Determination of salinity in water to

the list.

Added Enumeration of Legionella spp. & L pneumophila in water and wastewater by

(RT-PCR) as SOP-FE-1610 & Determination of Volatile Organic Compounds in Water

as SOP-FE-1136 & 1137.

Added detection of pork and horse as per SOP-FE-3132 &3133 ,Removed Detection of

Cronobacter sakazakii in Powdered Infant Formula for liquid.

Added Determination of Acrylamide & NSAIDS as SOP-FE-2373 &2374, corrected

standard method & input time (hrs) in the BS EN 15763:2009,pestiside residues in the

different foods as SOP-FE-2348,2349,2350 ,Determination of Residual Monomers

Migration from Food Packging into Food as SOP-FE-2450.

Added two new SOPs-FE-(1132,1133,1134) with the price in Env.unit

Added method detection of Cu -Cd ,Zn , Pb,N i,Cr & modified test duration (days) from 4 to 5

days incrased in SOP-FE-1304 in Env.unit.

Discontinuation the production of KIT from company for SOP-FE-3119

Issue By:SQO

Part 2-FCAU

Adde methosd detedtion to SOPs and replaced SOP-FE-2230 by AAS to SOP-FE-2231 by

ICPOES methods,added 3 SOP-FE-( 2231,2282,2372and 2392) to list.

Added drinking water analysis with price in ENVU

Added new SOP-FE-(3125,3126,3127,3128,3129) with the price of tests

Added SOP-FE-(1132,1133,1134,1135) with price in ENVU

Recalculated cost as 20% discount of analysis for all types of foods,drining water, animal

feed and food supplement as per law no14 year 2009.

Added remarks to list

Changed input time for Legionella from 2.2 to 2.30 hrs

11

Part 1-FMAU



Rev. No: 6

page :3 of 23





S.No.Clause

AmendedDate Authorisaton

REVIEW DATENext Review

DateAuthorisation

-03/08/2009 -

18/10/2010 18/10/2011 HOS

Outcome of Review

Nature of Amendment

Reviewed no change required

-

REVIEW RECORD

AMENDMENT RECORD

18/10/2010 18/10/2011 HOS

30/11/2011 29/11/2012 HOS

22/11/2012 21/11/2013 HOS

22/11./2013 20/11/2014 HOS

20/01/2014 20/01/2015 HOS

09/02/2015 09/02/2016 HOS

04/04/2016 04/04/2017 HOS

Changed as per requirements

Associated Document







Issue By:SQO

�� IMS-DP-12-Laboratory Work Operations



page :4 of 23

PARAMETER

TEST

METHOD

SOP-

REFERENCE SAMPLE TYPEREPORTING

UNIT

METHOD

DETECTION

INPUT

TIME

(Hrs)

ORIGINAL

COST

TEST

DURATI

ON

(Days)

REMARK

FDA (BAM on line) PPM Liquid cfu / ml 1

FDA (BAM on line) PPM Solid cfu / gm10 or as per

dilution factor

FDA (BAM on line) PPM cfu / ml 1

FDA (BAM on line) MPN cfu / ml 0.03

FDA (BAM on line) PPM cfu / gm10 or as per

dilution factor

FDA (BAM on line) MPN cfu / gm 0.3

FDA (BAM on line) MPN Liquid cfu / ml 0.03

FDA (BAM on line) MPN Solid cfu / gm 0.3

FDA (BAM on line) Liquid

Detected or

Not Detected /

ml

0.1

FDA (BAM on line) Solid

Detected or

Not Detected / 1

Enumeration of Coliforms

Bacteria

Enumeration of E.coli

Bacteria

Detection of of E.coli

Bacteria


PART 1: FOOD MICROBIOLOGY ANALYSIS UNIT

0.5

Enumeration of Mesophilic

Areobic Colony

Count(ACC)


FE-3103 * 70 2


Issue Date : 04/04/2016

FE-3104 *

Liquid

4

Solid

0.5

40.5FE-3104 *

70

70

Rev. No: 6

FDA (BAM on line) Solid Not Detected /

gm

1

FDA (BAM on line) PPM Liquid cfu / ml 1

FDA (BAM on line) PPM Solid cfu / gm10 or as per

dilution factor

FDA (BAM on line) Liquid

Detected or

Not Detected

in 25ml

1

FDA (BAM on line) Solid

Detected or

Not Detected

in 25gm

1

FDA (BAM on line.) SPM Liquid cfu / ml 1

FDA (BAM on line.) SPM Solid cfu / gm10 or as per

dilution factor

FDA (BAM on line.) SPM Liquid cfu / ml 1

FDA (BAM on line.) SPM Solid cfu / gm10 or as per

dilution factor

Enumeration of Clostridium

perfringens

FDA 1998(BAM-

8th

ed)PPMcfu / ml 1

FDA 1998(BAM-

8th

ed)MPNcfu / ml 0.03

FDA 1998(BAM-

8th

ed)PPMcfu / gm

10 or as per

dilution factor

FDA 1998(BAM-

8th

ed)MPNcfu / gm 3

FDA (BAM - 8th

ed.) MPN Liquid cfu / ml 0.3

FDA (BAM - 8th

ed.) MPN Solid cfu / gm 3

0.5 70 4

Solid

Enumeration of Vibrio

parahaemolyticus FE-3110 0.5 70 4

FE-3109*

FE-3105 *

0.5

0.5

Liquid

Enumeration of Yeasts and

Moulds

Isolation and Identification

of Salmonella Species

Enumeration of Coagulase

Positive Staphylococcus

aureus

140

Enumeration of Bacillus

cereus

5

FE-3107 *

70

FE-3106 * 1

FE-3108 *

4

5700.5

Isuue by:SQO

70

4


CONTROLLED COPY

page :5 of 23

PARAMETER

TEST

METHOD

SOP-


UNIT

METHOD

DETECTION

INPUT

TIME

(Hrs)

ORIGINAL

COST

TEST

DURATI

ON

(Days)

REMARK




Issue Date : 04/04/2016

Rev. No: 6

FDA (BAM - 8th

ed.) MPN Liquid cfu / ml 0.3

FDA (BAM - 8th

ed.) MPN Solid cfu / gm 3

FDA (BAM - 8th

ed.) Liquid

Detected or

Not Detected

in 25ml

1

FDA (BAM - 8th

ed.) Solid

Detected or

Not Detected

in 25gm

1

FDA (BAM - 8th

ed.) Liquid

Detected or

Not Detected

in 25ml

1

FDA (BAM - 8th

ed.) Solid

Detected or

Not Detected

in 25gm

1

FDA (BAM - 8th

ed.) Liquid

Detected or

Not Detected

in 25ml

1

FDA (BAM - 8th

ed.) Solid

Detected or

Not Detected

in 25gm

1

FDA (BAM - 8th

ed.) Liquid

Detected or

Not Detected

in 25ml

1Detection of Yersinia

Isolation and Identification

of E.coli O157:H7 in

Foods

Isolation of Thermophilic

Campylobacter species

from Foods

Enumeration of Vibrio

parahaemolyticus

210

1.5 5

1.5FE-3112

Method for Isolation and

Detection of Listeria

Species.

FE-3111*

FE-3110 0.5

FE-3113*

1

210

5

4

140

70

5

in 25ml

FDA (BAM - 8th

ed.) Solid

Detected or

Not Detected

in 25gm

1

Enumeration of

Pseudomonas aeruginosa

and Pseudomonas species

in Food and water

FE-3115* 1992 (APHA- 20th

ed.) Liquid cfu /250ml 1 0.5 70 4

Don Whitley SC. 1997 Liquid cfu / ml 1

Don Whitley SC. 1997 Solid cfu / gm10 or as per

dilution factor



dilution factor



dilution factor



dilution factor

Detection of Meat Species in

cooked meats and meat

products by using Enzyme

Linked Immuno Sorbant

Assay (Elisa-Technique)

FE-3120 *Bio-Kits Procedure 2002

UKSolid

Suspected or

Not Detected

in 25 g

1% 0.5 70 3

Detection of Yersinia

entrocolitica in Food

Samples

0.5

1

Analysis of Food Samples

using Rapid Automated

Bacterial Impedance

Technique (RABIT) -

( Enumeration ofMolds and

Yeasts)



Bacterial Impedance

Technique (RABIT) -

(Enumeration of Mesophilic

Aerobic Colony Count /



Bacterial Impedance

Technique (RABIT) -

(Enumeration of Coliforms)

2

2

0.5 70

70

70

0.5

FE-3117*

0.5

Issue by:SQO

3

15FE-3114

FE-3117*

FE-3117*

FE-3117* 2

140

70



Bacterial Impedance

Technique (RABIT) -

(Enumeration/ Detection of

E.coli)


CONTROLLED COPY

page :6 of 23

PARAMETER

TEST

METHOD

SOP-


UNIT

METHOD

DETECTION

INPUT

TIME

(Hrs)

ORIGINAL

COST

TEST

DURATI

ON

(Days)

REMARK




Issue Date : 04/04/2016

Rev. No: 6

Detection of Cronobacter

sakazakii in Powdered

Infant Formula

FE-3121 * FDA (BAM online) Solid

Detected or

Not detected

in 333gm

1 2 280 7

Liquid

Detected or

Not Detected

in 25ml

1

Solid

Detected or

Not Detected

in 25gm

1

USFDA- 8thed or AOAC Liquid cfu / ml 1

USFDA- 8thed or AOAC Solid cfu / gm10 or as per

dilution factor



dilution factor

USFDA- 8thed or AOAC Liquid

Detected or

not detected /

ml

1

USFDA- 8thed or AOAC Solid

Detected or

not detected /

gm

1

FE-3123*

Analysis of Food using

petriflim method 3M

( Enumeration o f

Mesophilic Areobic Colony

Count / ACC)

Detection of Salmonella

species by Using BAX

FE-3123* 2

2

70

FE-3122*AOAC Official Method

2003.092 280

0.5

2

70


petriflim method 3M

(Enumeration of Coliforms

Bacteria)

0.5

FE-3123* 0.5 2


petriflim method 3M (

Detection of E.coli Bacteria )

70gm



dilution factor



dilution factor



dilution factor



dilution factor

Solid

Detected or

Not Detected

in 25gm

1

Liquid

Detected or

Not Detected

in 25ml

1

Solid

Detected or

Not Detected

in 25gm

1

Liquid

Detected or

Not Detected

in 25ml

1

2 280FE-3126*

0.5

70

20.5

5

Enumeration of

Enterobacteriaceae in Foods FE-3124*


petriflim method 3M

( Enumeration of E.coli

Bacteria )


petriflim method 3M (

Enumeration of Yeasts and

Moulds )

FE-3123* 0.5 2

70

AOAC Official Method

2012.08


2003.092

0.5

70

FE-3123*

70 2

280

2

2


petriflim method 3M

( Enumeration of Coagulase

Positive Staphylococcus

aureus )

FE-3123*

Issue by:SQO

FE-3125*

Detection of Salmonella

spp. by VIDAS UP

Technique

Detection of Listeria

monocytogenes in Food

using BAX System


CONTROLLED COPY

page :7 of 23

PARAMETER

TEST

METHOD

SOP-


UNIT

METHOD

DETECTION

INPUT

TIME

(Hrs)

ORIGINAL

COST

TEST

DURATI

ON

(Days)

REMARK




Issue Date : 04/04/2016

Rev. No: 6

Solid

Detected or

Not Detected

in 10gm

1 ng

Liquid

Detected or

Not Detected

in 10ml

1 ng

Solid

Detected or

Not Detected

in 25gm

1

Liquid

Detected or

Not Detected

in 25ml

1

SureFood Animal ID Pork

kit (Manual S6014 Version

1.1E)

0.5%

Taqman Pork ID Kit (Pork

No. IMG-163-Rev. April

2013)

0.1%

Solid

Detected or

Not Detected 1

Detection of Pork

Contaminants in highly

processed Food and Feed by

Using Real-Time PCR

Technique

FE-3129* Solid

Detected or

Not detected

in 50-100 mg

2.5 350

FE-3128 1.5

Detection of Bacterial Enter

Toxin in food Using

TECRA Kit Method

210


993.062

2SyLab Operation Manual

BacTrac 4000 Series

FE-3127 2 280

3

Detection of Different Micro-

organisms by Using Bac

Trac Method

(Detection of Salmonella

spp)

Solid Not Detected

in 25gm

1

Liquid

Detected or

Not Detected

in 25lm

1

Solid

Detected or

Not Detected

in 25gm

1

Liquid

Detected or

Not Detected

in 25 ml

1

Detection of Pork Gelatin in

Gelatinous Food Using Real-

Time PCR Technique

FE-3132

Taqman Pork ID Kit (Pork

No. IMG-163-Rev. April

2013)

Solid

Detected or

Not detected

in 50-100 mg

0.1% 2.5 350 3

Detection of Horse

contaminant Using Real-

Time PCR Technique

FE-3133Taqman Equine ID Kit

(SKU: A15570-Rev.2013)Solid

Detected or

Not detected

in 50-100 mg

0.1% 2.5 350 3

PPM: Pour Plate Method. SPM: Spread Plate Method. MPN: Most Probable Number .

Detection of E .coli

O157:H7 in Food Using

BAX System


2009.112 280

Detection of Cronobacter

sakazakii in Baby Food

Using BAX System

280AOAC Official Method

20122FE-3131* 2

Issue by:SQO:

2


CONTROLLED COPY

page :8 of 23

PARAMETER

TEST

METHOD

SOP-


UNIT

METHOD

DETECTION

INPUT

TIME

(Hrs)

ORIGINAL

COST

TEST

DURATI

ON

(Days)

REMARK




Issue Date : 04/04/2016

Rev. No: 6

Determination of Moisture

/Total solids in Foods by

AIR-Oven methods

FE-2203 * AOAC, 17th Edn.2000 Solid / Liquid % w/w 0.02 0.4 56 4

Determination of moisture /

total solids in foods by

Vacuume -oven method

FE-2205AOAC , 17th Ed., (2000),

Gaithersburg, USA.Solid / Liquid % w/w 0.02 0.4 56 4

0.05 moisture

0.3 fat

0.5 protein

0.1 Ash

Determination of Fat content

in Foods by Ammonia

Digestion method

FE-2207 * AOAC, 17th Edn. 2000 Solid / Liquid %w/w 0.1 0.8 112 4

Determination of Fat in food

products (Meat & Cheese)FE-2208 AOAC, 15th Edn. 1990 Solid / Liquid %w/w 0.1 0.8 112 4

Determination of Total

Protein in Foods By

Kjeldahl method

FE-2210 * AOAC, 19th Ed ,2012 Solid / Liquid %w/w 0.1 0.8 112 4

Determination of Total Ash

in Foods by Incineration

method

FE-2211 * AOAC, 19th Ed ,2012 Solid / Liquid %w/w 0.05 0.7 98 4

Determination of Fat,Protein

and Acidity in selected Instrument Manual for FTIR 0.1 for Fat &


Fat Protein and ash by FT-

NIR

FE-2206*

PART 2: FOOD CHEMICAL ANALYSIS UNIT

AOAC, 17th Edn.2000 Solid / Liquid % 0.15 21 5

and Acidity in selected

foods products by FTIR

Technique

FE-2212

Instrument Manual for FTIR

milkoscan FTIR20 Analyzer

FCMS-1

Solid / Liquid %w/w

0.1 for Fat &

Protein, 0.05 for

acidity

0.4 70 3

AOAC , 19 th Ed.,2012,

Gaithersburg, USA. 2.

David Pearson, The

Chemical Analysis of

Foods, 7th Ed., 1976

Determination of pH of

foodsFE-2214* APHA 4500 B-18th Edition Solid / Liquid - 0.1 0.3 42 2

Determination of Sugars by

HPLC in HoneyFE-2216*

Leatherhead Food RA, 2nd.,

1987Liquid %w/w

Fructose &

Glucose 1% and

Sucrose 0.5%

1.5 261 4

Determination of reducing

sugar and sucrose by Lane

& Eynon's

Solid / Liquid %w/w - 1.5 210 4

Determination of Non

reducing

sugar(Sucrose),Titrimetric

method


Determination of Water-

Soluble AshFE-2218 AOAC, 15th Edn. 1990 Solid / Liquid %w/w - 1.2 168 4

Determination of Acid-

Insoluble AshFE-2219 AOAC, 15th Edn. 1990 Solid / Liquid %w/w - 1.25 175 4

Determination of Alkalinity

of Water-Soluble AshFE-2220 AOAC, 15th Edn. 1990 Solid / Liquid %w/w - 1.5 210 4

FE-2217

AOAC, 15th Edn,1990,

Journal of the Society of

Chemical Industry, by J.

Lane and L. Eynon, 42, 325

AOAC, 15th Edn. 1990

Issue by:SQO

FE-2213*Determination of total

acidity in foodsSolid / Liquid %w/w 0.05 0.3 42 3


CONTROLLED COPY

page :9 of 23

PARAMETER

TEST

METHOD

SOP-


UNIT

METHOD

DETECTION

INPUT

TIME

(Hrs)

ORIGINAL

COST

TEST

DURATI

ON

(Days)

REMARK




Issue Date : 04/04/2016

Rev. No: 6

Determination of Crude

FiberFE-2221

Pearson's Chemical Analysis

of Food, 7th Ed., 1976 Food

chemistry, by Lillian

Hoagland Mayer, CBS

Publishers & Dirtributors,

India, 1987


Determination of water

extract of tea and coffeeFE-2222 AOAC, 17th Edn.2000 Solid / Liquid %w/w - 0.55 77 4

Computationo solids not fat

and calorific value of foods

without crude Fiber

- Solid / Liquid Kcal/100g - 2.8 392 4


and calorific value of foods

with crude Fiber

Solid / Liquid Kcal/100g - 4.3 602 5


(S.N.F)Solid / Liquid %w/w 0.1 0.8 112 5

Determination of

Extraneous matter and

defects in Food grains

FE-2224 AOAC, 17th Edn.2000 Solid %w/w - 0.5 70 3

Determination of stones

(seeds) and shell content in

fruits/dried fruits and nuts.

FE-2225 - Solid / Liquid %w/w - 0.5 70 3

FE-2223

fruits/dried fruits and nuts.

Determination of Salt

content in edible Salt and

Foods

FE-2226 AOAC, 19th Ed ,2012 Solid / Liquid %w/w - 0.4 56 3

Determination of Drained

Weight in canned / Bottled

Foods

FE-2228 - Solid / Liquid %w/w - 0.25 35 3

Determination of Minerals

in Fortified Food Products

by ICPOES after Microwave

Digestion

FE-2231*J. of AOAC International,

vol 95, No. 1, 2012Solid / Liquid mg/kg As per standard 1.5 210 5

210 (Dhr)

for first

element, 32

(Dhr) per

extra

element

Detection and

Determination of Titanium

Dioxide in Food


973.36 (2012) Solid / Liquid mg/kg 10 1.5 210 5

Detection of Titanium

dioxide- AOAC OM 973.36 Solid / Liquid

Detected/Not

detected- 1 140 7

Determination of Refractive

Index of Oils and FatsFE-2260* AOAC, 17th Edn. 2000 Solid / Liquid nD - 0.25 35 4

Determination of Free Fatty

Acid (FFA) in Fats and oilsFE-2261* AOAC, 19th Ed ,2012 Solid / Liquid %w/w 0.05 0.4 56 4

Determination of Peroxide

Value of Fats and OilsFE-2262* AOAC, 19th Ed ,2012 Solid / Liquid mq/Kg 0.1 0.4 56 4

Determination of Melting

Point of FatsFE-2263* AOAC, 17th Edn. 2000 Solid / Liquid °C - 0.5 70 4

Determination of Fatty Acid

Profile of Oils & FatsFE-2264* AOAC, 17th Edn. 2000 Solid / Liquid % - 1 140 4

Issue by:SQO


CONTROLLED COPY

page :10 of 23

PARAMETER

TEST

METHOD

SOP-


UNIT

METHOD

DETECTION

INPUT

TIME

(Hrs)

ORIGINAL

COST

TEST

DURATI

ON

(Days)

REMARK




Issue Date : 04/04/2016

Rev. No: 6

AOAC, 17th Edn. 2000 Solid / Liquid % 0.2 1 140 4

Journal of AOAC

International,volume1 ,

2012. chapter 41, 27-28.

Solid / Liquid % 0.2 1 140 4

Determination of Iodine

value by FT-NIRFE-2265* AOCS cd 1e-01 Solid / Liquid

% Iodine

absoredAs per SOP 0.5 70 3

Determination of Ethanol

contents in non-alcholic I

beverage by using static

FE-2270*


986.12,2000, HALAL”

CAC/GL 24-1997

Solid / Liquid v/v % 0.001 1 140 5

Determination of

Preservatives, Artificial

sweeteners and Caffeine in

Foods by HPLC method

FE-2280 * HPLC-DAD Manual Solid / Liquid mg/Kg

Liquids: BA,SA &

Caffeine:0.5 mg/L,

APM, Ace-K &

APM-1 mg/L.

SOLIDS:BA,SA &

Caffeine:5 mg/kg,

APM, Ace-K &

APM-5 mg/kg

0.8 112 5

For one

Preservatives,

Any extra

Preservatives

will increase

the time by

0.25 hr, and

charge by 35

(Dhr)

Determination of Vitamin C

in Soft DrinksFE-2281*

British Standard: BS EN

14130:2003Solid / Liquid mg/100g 5 1.5 210 5

FE-2264*

Determination of Fatty Acid

Profile of oils and fats,

omega fatty acids in

selected foods and food

supplements

Determination of Water

Soluble Vitamins in Foods

and food supplements

FE-2282*

Official Methods of AOAC

international, 19th Edition,

2012 Solid / Liquid mg/kgRefer validation

procedure1 140 5

For one

vitamin 140

AED and

35AED for

each

additional

vitamin

Identification of water

soluble Synthetic Colours in

Foods by Paper

Chromatography

FE-2285 *Pearson's Chemical Analysis

of food, 7th Ed, 1976Solid / Liquid - - 0.5 70 2

Solid mg/Kg 1 2.15 301 5

Liquid mg/L 1 2.15 301 5

Detection & Determination

of Sulphur Dioxide FE-2290 AOAC, 17th Edn. 2000 Solid / Liquid mg/Kg 5 1 140 5

Determination of total

soluble solids (Brix°) in

foods and moisture in

Honey

FE-2294*

Instruction manual for

automatic digital

refractomer RX-

50000,AOAC Official

Methods of Analysis (2000)

– AOAC Official Method

969.38

Solid / Liquid % - 0.25 35 3

Determination of Fat in

Butter / Ghee- AOAC OM 938.06 Solid / Liquid g/100g - 0.8 112 4

Determination of Aflatoxins

(B1, B2, G1, G2) in foods

by HPLC method

FE-2320* AOAC, 17th Edn. 2000 Solid µg/kg0.3 for B1 & G1 /

0.1 for B2 & G23.5 490 4

Determination of Synthetic

Food Colours by HPLCFE-2286 AOAC, 17th Edn. 2000

Issue by:SQO


CONTROLLED COPY

page :11 of 23

PARAMETER

TEST

METHOD

SOP-


UNIT

METHOD

DETECTION

INPUT

TIME

(Hrs)

ORIGINAL

COST

TEST

DURATI

ON

(Days)

REMARK




Issue Date : 04/04/2016

Rev. No: 6

Solid 0.03 2.5 350 4

Liquid 0.003 2.5 350 4

Determination of Patulin in

Apple productsFE-2323

AOAC - BS EN

14177:2003 , BS EN

15890:2010

Solid / Liquid µg/kg 1 3.5 490 5

Determination of

Mycotoxins indifferent food

Commodities by Ultra-

Performance lquied

Chromatography and Tirple

Quadrupole Detector

FE-2324* RCM-2009; 23:1801-1809 Solid µg/kgAs per Annex-2

of SOP3.5 490 7

1-AED:490

for one toxin

2-115 for

each extra

toxins ( total

for 11 toxins

1755 Dh)

Determination of

Organochlorine and

Organophosphorous

Pisticide Residue in Cereals

(NON-Fatty dry Foods)

FE-2342 AOAC,15th Edn,1990 Cereals & Dry foods mg/KgAs per

Annex(III)of SOP 8 1120 7

Determination of N-

Methylcarbamatesin Fruits

and Vegetable Quenchers

Technique using LC-

MS/MS

FE-2343 *

AOAC 90, No. 2, 2007 In

house modified. Tripple

Quadrupole LC/MS System.Fruits & Vegetable mg/kg As per SOP 4 560 7

560 ( Dhr)

for N-

Methylcarba

matesin only


(M1, M2) in MilkFE-2321* AOAC, 15th Edn. 1990 µg/kg

MS/MS

Solid

Liquid

Multiresidue method for

analysis of pesticide residues

in fruits & Vegetables by

Acetonitrile extraction &

detection & GC-

ECD/NPD/MSD/PFPD

Detection -A QuEChERS

Approach

FE-2346*AOAC,Vol.90, No 2,2007.

In house modified. Fruits & Vegetable mg/kg

As per Annex

( I & II ) of SOP8 1120 7

Determination of N-

Methylcarbamatesin Fruits

and Vegetable Quenchers

Technique using LC-

MS/MS and Multiresidue

method for analysis of

pesticide residues in fruits &

Vegetables by Acetonitrile

extraction & detection &

GC-ECD/NPD/MSD/PFPD


Approach

FE-2343 * &

FE-2346*

AOAC 90, No. 2, 2007;In

house modified. Tripple

Quadrupole LC/MS System.Fruits & Vegetable mg/kg

10 and As per

Annex ( I &II) of

SOP

12 1680 7

For SOP-

FE-2343

(560 Dhr) +

SOP FE-

2346 (1120

(AED) =

1680

Multiresidue method for

analysis of pesticide residues

in fruits & Vegetables by

Acetonitrile extraction &

detection & GC-MSD


Approach

FE-2347*

AOAC 90, No.2, 2007 In

house modified. Single

Quadrupole GC/MS

System.

Fruits & Vegetable mg/kg As per SOP 6.75 945 7

Analysis of Pesticide

Residues in Spices by

Multiresidue Method -A

QuEChERS Approach

FE-2348*


2007.012. In house

modified. Triple

Quadrupole GC/MS

System.

Spices mg/kg As per SOP 8 1120 7

Issue by:SQO

As per Annex of

SOP4 560 7

Determination of

Organochlorine Pestiside

and Polychlorinated

Biphenyl Residue in Milk -

Quechers.

FE-2345*AOAC,Vol.88, No 2,2005

In house modified.mg/kg


CONTROLLED COPY

page :12 of 23

PARAMETER

TEST

METHOD

SOP-


UNIT

METHOD

DETECTION

INPUT

TIME

(Hrs)

ORIGINAL

COST

TEST

DURATI

ON

(Days)

REMARK




Issue Date : 04/04/2016

Rev. No: 6

Analysis of Pesticide &

PCBs Residues in Tissues

by Multiresidue Method -A

QuEChERS Approach

FE-2349*


2007.012. In house

modified. Single

Quadrupole GC/MS

System.

Tissues ng/kg As per SOP 4 560 7

Analysis of Pesticide

Residues in Honey by GC-

MSD & LC-MSMS -A

Multiresidue QuEChERS

Approach

FE-2350*

EURL-2010 In house

modified. Tripple

Quadrupole LC/MS &

Single Quadripole GC/MS

System.

Honey and Dates

syrupmg/kg As per SOP 8 1120 7

Detection of Sulfonamide

Antibacterial in Raw Milk

by Charm II Test

FE-2360

by GC/MS - Thermo

Scientific, Technical

Note:10236, 2008.

Liquid µg / L _ 1.5 210 4

Detection of Tetracycline

antibacterial in Raw Milk by

Charm II Test

FE-2361arm II Test Operator’s

Manual for Tetracyclines Liquid µg / L _ 1.5 210 4

Detection of β-Lactams

Antibacterial in Raw Milk

by CharmII Test

FE-2362

Charm II Test

TBL8MRL06,

Rev.November 2004

(Charm Sciences Inc.)

Liquid µg / L _ 1.5 210 4

Detection of Macrolide

Antibacterial in Raw & FE-2364

Charm II Test Operator’s Liquid µg / L _ 1.5 210 4

Antibacterial in Raw &

Pasteurized Milk By Charm

II Test

FE-2364Charm II Test Operator’s

Manual for Macrolides Liquid µg / L _ 1.5 210 4

Liquid µg /L Milk 0.02

Fish: 0.04

Honey: 0.07

Liquid µg /L

Solid µg /L

Liquid mg/kg

Solid mg/kg

Liquid µg /L

Solid µg /L

Determination of

Antihelmintics-

Averrmectins- Residues in

Foods by LC-MSMS

FE-2372* Agilent Application Note Solid/Liquid µg/kgAs per Appendix

of SOP5 700 5

Determination of

Chloramphenicol in Foods

by LC-MS-MS

FE-2368*

AOAC, 2005, 2006,

Commission Decision

2002/657/EC, Commission

Decision2003 /181/EC,5 700

Issue by:SQO

Determination of Melamine

and Cyanuric Acid Residues

in Foods

FE-2370*

1-FDA LIB No. 4422,

Interim Method for

Determination of Melamine

and Cyanuric Acid Residues

In Foods using LC-

0.1 5 700 5

Determination of

Sulfonamides &

Trimethoprim in Milk and

Tissues by LC-MSMS

FE-2369*

Analysis of veterinary drug

residues in shrimp, Journal

of Chromatography B, 836

(2006) 22–3

As per Appendix-

2 of SOP

5

Solid µg /kg

5 700 5

Determination of

Tetracyclines in foods by LC-

MSMS

FE-2371*

10.2 Official Methods of

Analysis, 19th Edition

(2012), Method 995.09.

As per Appendix-

1 & 2 of SOP5 700 5


CONTROLLED COPY

page :13 of 23

PARAMETER

TEST

METHOD

SOP-


UNIT

METHOD

DETECTION

INPUT

TIME

(Hrs)

ORIGINAL

COST

TEST

DURATI

ON

(Days)

REMARK




Issue Date : 04/04/2016

Rev. No: 6

Determination of

Acrylamide in Selected

Foods by LCMSMS

FE-2373*

Institue of Food safety &

health, Illinois Institue of

Technology, bedford park

Solid µg/kg 25 3 420 5

Determination of

NSAIDS(Non-Steroidal

Anti-Inflammatory Drugs)

Residues in Milk by

LCMSMS

FE-2374 Anal. Biochem 2012 Solid/Liquid µg/kgAs per Appendix

2 of SOP5 700 5

Determination of Benzo (a)

Pyrene in Oils and FatsFE-2390* BS EN ISO 25302 :2010 Solid / Liquid µg/kg 0.4 4.5 630 5

Determination of 3-MCPD

in Soy Sauce by GC-MSFE-2391* AOAC, 17th End 2000 Liquid mg/Kg 0.03 6 840 5

Determination of Polycyclic

Aromatic Hydrocarbons in

Edible Oils and fats

FE-2392*BS EN ISO 25302 :2010. In

house modified.Solid / Liquid µg/kg Refer SOP 4.5 630 5

Determination of Sudan

Dyes in Selected

Spices/Condiments &

Selected Foods

FE-2400*

Statutory Analysis

Government Chemist

Programme – LGC Limited

2006- Food Standards

Agency - information

Solid / Liquid mg / Kg 1 2 280 7

Solid Bq/kg 2.5

Liquid Bq/L 2.5

Idenfication of Rhodamine

B in Foods by paper

Chromatography

FE-2403*

David Pearson, the

Chemical Analysis of Foods

, 7th Edn, (1976),Churchill

Livingstone ,

Developments in food

colours, Vol I & II, Avi.

Publishers.

Solid / Liquid mg/kg 2 0.5 70 3

Determination of traces

elements of

As*,Cd*,Hg*,Pb* in food

stuffs by ICP-MS after

pressure digestion

-

As 15

Cd 5

Hg 15

Pb 15

Idenfication of

Rhodamine B in Foods

by paper

Chromatography

FE-2403*

David Pearson, the

Chemical Analysis of Foods

, 7th Edn, (1976),Churchill

Livingstone ,

Developments in food

colours, Vol I & II, Avi.

Publishers.

Solid / Liquid mg/kg 2 0.5 70 3

Issue by:SQO

Determination of Gamma

Radiation in Foods by using

sodium iodide gamma

Spectrometer

FE-2401*

Berthold LB 2045 Gamma

Spectrometer instruction

manual.Method for

detection of permissible

radionuclides limits in food

part 1; gamma spectrometry

analysis GSO 998-1998

1 140 2

BS EN

15763:2009BSEN 15763:2009 Solid / Liquid ug/kg 3.33 466 5

466 for one

test, more

than one test

115


CONTROLLED COPY

page :14 of 23

PARAMETER

TEST

METHOD

SOP-


UNIT

METHOD

DETECTION

INPUT

TIME

(Hrs)

ORIGINAL

COST

TEST

DURATI

ON

(Days)

REMARK




Issue Date : 04/04/2016

Rev. No: 6

Determination of Residual

Monomers Migration from

Food Packging into Food

Simulants by GC-MS

FE-2450*BSEN : 13130-1:2004,

BSEN 13130-5:2004Food contact materials µg/kg

0.5 for Benzene

&Et Benzene, 1.0

for Styrene, 1.5

for Toluene

1.5 210 5

Physical analysis SP-FE-0004 - - - - 0.3 42 1

Determination of Total Ash

in Foods by Incineration

method

FE-2211* AOAC, 17th Edn. 2000 Solid / Liquid %w/w - 0.7 98 4


(B1, B2, G1, G2) in foods

by HPLC method

FE-2320* AOAC, 17th Edn. 2000 Solid µg/kg0.3 for B1 & G1 /

0.1 for B2 & G23.5 490 4

Determination of


1-AED:490

for one toxin

ANIMAL FEED ANALYSIS


Commodities by Ultra-

Performance lquied

Chromatography and Tirple

Quadrupole Detector

FE-2324* RCM-2009; 23:1801-1809 Solid µg/kgAs per Annex-2

of SOP3.5 490 7

2-115 for

each extra

toxins ( total

for 11 toxins

1755 Dh)

*-Test is listed in DAC accreditation schedule No. LB-014 -TEST

Issue by:SQO

# -Solution basis


CONTROLLED COPY

page :15 of 23

PARAMETER

TEST

METHOD

SOP-


UNIT

METHOD

DETECTION

INPUT

TIME

(Hrs)

ORIGINAL

COST

TEST

DURATI

ON

(Days)

REMARK




Issue Date : 04/04/2016

Rev. No: 6

Water / Waste water 52 3

Drinking water 42 3

Water µS/cm 5 52 3

Drinking water µS/cm 5 42 3

Waste water mS/cm 0.01 52 3

Determination of salinity in

waterFE-1102 Salinity meter Water / Waste water ppt 5 0.3 52 3

Water / Waste water 44 3

Drinking water 35 3


Suspended Solids in water

and waste water

FE-1104 * APHA-2540 D Water / Waste water mg/L 11 0.6 104 5

0.25

Determination of

Conductivity in waterFE-1102* APHA-2510 B 0.3

Determination of Turbidity FE-1103 APHA-2130 B NTU 0.5

PART 3:ENVIRONMENT UNIT

Determination of pH in

waterFE-1101 * APHA-4500-H+ - 1 to 14 0.3

and waste water

Water mg/L 10

Waste water mg/L 51

FE-1105 TDS / EC Meter Drinking water mg/L 5 0.6 84 5


Solids in water and waste

water

FE-1106 APHA-2540 B Water / Waste water mg/L 51 0.6 104 5

Water / Waste water mg/L 5 0.5 87 3

Drinking water mg/L 5 0.5 70 3

Determination of Acidity in

water and waste waterFE-1108 APHA-2310 B Water / Waste water mg/L 5 0.5 87 3

Determination of Alkalinity

in water and waste waterFE-1109 APHA-2320 B Water / Waste water mg/L 5 0.5 87 3

Determination of Chloride FE-1110 APHA-4500-Cl- B Water / Waste water mg/L 6 0.5 87 3

Determination of Nitrogen-

Ammonia in water and

waste water

FE-1112 APHA-4500-NH3- B, C Water / Waste water mg/L 0.2 0.64 111 5

Determination of Nitrate-

Nitrogen in water

wastewater

FE-1113 APHA-4110 Water / Waste water mg/L 0.05 0.77 134 5


Nitrogen FE-1115

T.R.Parsons 2.1, 1984,

APHA 4110 BWater / Waste water mg/L 0.13 0.9 157 5


Kjeldahl NitrogenFE-1116 APHA - 4500 - Norg B, C Water / Waste water mg/L 1 1.2 209 5

Issue By:SQO

APHA-2340FE-1107


Hardness in water and

waste water


Dissolved Solids in water

and waste water

FE-1105 * APHA-2540 C 0.6 104 5


CONTROLLED COPY

page :16 of 23

PARAMETER

TEST

METHOD

SOP-


UNIT

METHOD

DETECTION

INPUT

TIME

(Hrs)

ORIGINAL

COST

TEST

DURATI

ON

(Days)

REMARK




Issue Date : 04/04/2016

Rev. No: 6

Determination of Phosphate-

phosphorousMOOPAM 4

th ED. 3.2.8-A Water / Waste water mg/L 0.02 0.64 111 5


Phosphorus in water/ waste

water

APHA - 4500 - P (B, D) Water / Waste water mg/L 0.1 0.99 172 5

Determination of Sulfide FE-1120 APHA - 4500 S2-

F Water / Waste water mg/L 1 0.5 87 5

Determination of Oil and

Grease in water and waste

water

FE-1121 * APHA - 5520 B Water / Waste water mg/L 12 1.2 209 5

Determination of

Biochemical Oxygen

Demand (BOD)

FE-1122 * APHA - 5210 B Water / Waste water mg/L 7 0.5 87 7

Determination of Chemical

Oxygen Demand (COD)FE-1123 * APHA - 5220 B Water / Waste water mg/L 12 0.44 77 5

Water ug/L 0.1 6 1044 7

drinking water ug/L 0.1 6 840 7

Determination of

Phytopigments FE-1125 T.R.Parsons (4.1,4.2), 1984 Water mg/m

3 0.5 1.2 209 5

Determination of Petroleum

Hydrocarbons in waterFE-1126

MOOPAM 4th

ED. -Section

6.6, 6.9Water / Waste water mg/L 5 0.8 139 5

Determination of

Organochlorine Pesticides in

Water By GC-ECD-Solvent

Extraction

APHA 6630 BFE-1124*

FE-1117

Hydrocarbons in waterFE-1126

6.6, 6.9Water / Waste water mg/L 5 0.8 139 5

Determination of Heavy

Metals (Cu, Cd, Pb, Ni, Zn,

Cr)*

FE 1128 APHA - 3030 E, 3111 Water / Waste water mg/Las per each

element307 7

Determination of Copper

(Cu) *Water / Waste water mg/L 0.1

Determination of Cadmium

(Cd) *Water / Waste water mg/L 0.08

Determination of Zinc (Zn)

*Water / Waste water mg/L 0.05

Determination of

Manganese (Mn)*Water / Waste water mg/L 0.05

Determination of Nickel

(Ni) * Water / Waste water mg/L 0.2

Determination of Chromium

(Cr)*Water / Waste water mg/L 0.2

Determination of Iron (Fe)* Water / Waste water mg/L 0.1

Determination of Cobalt

(Co)* Water / Waste water mg/L 0.12

Determination of Lead (Pb) * Water / Waste water mg/L 0.5

Determination of Silver (Ag)* FE-1128 APHA - 3030 E, 3111 water / waste water mg/L 0.1 0.5 87 5

0.5 87 7

87 AED for

one Element

& 44 AED

for each

extra

elements

Issue by:SQO

FE-1128 APHA - 3030 E, 3111


CONTROLLED COPY

page :17 of 23

PARAMETER

TEST

METHOD

SOP-


UNIT

METHOD

DETECTION

INPUT

TIME

(Hrs)

ORIGINAL

COST

TEST

DURATI

ON

(Days)

REMARK




Issue Date : 04/04/2016

Rev. No: 6

Determination of Fluoride (

F)* in water by Ion

chromatography

Dionex manual water mg/L 0.1

Determination of Chloride

(Cl)* in water by Ion

chromatography


Determination of Nitrate

(NO3) * in water by Ion

chromatography


Determination of Sulfate

(SO4)*in water by Ion

chromatography


Determination of Bromate

(BrO3)* in water by Ion

chromatography

Dionex manual water ug/L 3

Determination of Bromide

(Br)* in water by Ion

chromatography


Determination of Chlorite

(ClO2)in water by Ion

chromatography


Determination of

Chlorate(ClO3) in water by

Ion chromatography


5

131 AED

for one

Element &

44 AED for

each extra

elements,

DRINKING WATER (SOP-FE-1130)

FE-1130 0.75 131

Determination of Fluoride

( F)* in water by Ion

chromatography

Dionex manual Drinking water mg/L 0.1

Determination of Chloride

(Cl)* in water by Ion

chromatography


Determination of Nitrate

(NO3) * in water by Ion

chromatography


Determination of Sulfate

(SO4)*in water by Ion

chromatography


Determination of Bromate

(BrO3)* in water by Ion

chromatography

Dionex manual Drinking water ug/L 3

Determination of Bromide

(Br)* in water by Ion

chromatography


Determination of Chlorite

(ClO2)in water by Ion

chromatography


Determination of

Chlorate(ClO3) in water by

Ion chromatography



Metals (Cu, Cd, Pb, Ni, Zn,

Cr)* in water / waste water

by ICP-OES

APHA - 3030 E, 3120 Water / Waste water mg/Las per each

element131

Determination of Metals

(Cu, Fe, Zn, Ca, Mg, Na)*in

drinking water by ICP-OES

APHA - 3030 E, 3121 Drinking water mg/Las per each

element105

FE-1130 0.75 105 5

105 AED

for one

Element &

35 AED for

each extra

elements,

FE-1131 0.75 5

Issue by:SQO


CONTROLLED COPY

page :18 of 23

PARAMETER

TEST

METHOD

SOP-


UNIT

METHOD

DETECTION

INPUT

TIME

(Hrs)

ORIGINAL

COST

TEST

DURATI

ON

(Days)

REMARK




Issue Date : 04/04/2016

Rev. No: 6

water µg/L 5

Waste water mg/L 0.1

Determination of Arsenic

(As) by ICP-OES water / waste water µg/L 8

Water µg/L 2


Water µg/L 2


Water µg/L 6



(Cd*) by ICP-OES

Determination of

Manganese (Mn*) by ICP-

OES

Determination of Silver

(Ag*) by ICP-OES

FE-1131 APHA 3120 0.75 131 5

Determination of Lead (

Pb*) by ICP-OES

131 AED

for one

Element &

44 AED for

each extra

elements


Determination of Calcium

(Ca*) by ICP OESWater mg/L 0.05

Determination of

Magnesium (Mg*) by ICP-

OES

water mg/L 0.05

Determination of Iron (Fe*)

by ICP-OESWater mg/L 0.05

Determination of Zinc

(Zn*) by ICP-OESWaste water mg/L 0.05


(Ni*) by ICP-OESWaste water mg/L 0.1

Determination of

Chromium (Cr*) by ICP-

OES



(Cu*) by ICP-OESWaste water mg/L 0.05

Determination of

Molybdenum (Mo) by ICP-

OES

water µg/L 10

Determination of Sodium

(Na) by ICP-OESwater µg/L 10

Determination of

Barium(Ba) by ICP OESwater µg/L 10

Determination of

Potassium(K) by ICP OESwater µg/L 10

1131 APHA 3120 0.75 131 5

131 AED

for one

Element

&44AED

for each

extra

elements,

Issue by:SQO


CONTROLLED COPY

page :19 of 23

PARAMETER

TEST

METHOD

SOP-


UNIT

METHOD

DETECTION

INPUT

TIME

(Hrs)

ORIGINAL

COST

TEST

DURATI

ON

(Days)

REMARK




Issue Date : 04/04/2016

Rev. No: 6


(Cd*) by ICP-OES Drinking water µg/L 2

Determination of

Manganese (Mn*) by ICP-

OES

Drinking water µg/L 2

Determination of Lead (

Pb*) by ICP-OES Drinking water µg/L 6

Determination of Calcium

(Ca*) by ICP OES Drinking water mg/L 0.05

Determination of

Magnesium (Mg*) by ICP-

OES

Drinking water mg/L 0.05


(Ni*) by ICP-OES Drinking water µg/L 10

Determination of Iron (Fe*)

by ICP-OES Drinking water mg/L 0.05

Determination of Zinc

(Zn*) by ICP-OES Drinking water µg/L 10

Determination of

Chromium (Cr*) by ICP-

OES


0.75 105 5

DRINKING WATER (SOP-FE-1131)

105 AED

for one

Element

&35 AED

for each

extra

elements,

1131 APHA 3120


(Cu*) by ICP-OES Drinking water µg/L 10

Determination of

Molybdenum (Mo) by ICP-

OES


Determination of Sodium

(Na) by ICP-OES Drinking water µg/L 10

Determination of

Barium(Ba) by ICP OES Drinking water µg/L 10

Determination of

Potassium(K) by ICP OES Drinking water µg/L 10

Water Colour Units 1 0.7 122 3

Drinking water Colour Units 1 0.7 98 3

APHA - 4500 Cl -G Water mg/L 0.2 0.7 122 3

APHA - 4500 Cl -G Drinking water mg/L 0.2 0.7 98 3

APHA - 4500 Cl -G Water mg/L 0.2 0.7 122 3

APHA - 4500 Cl -G Drinking water mg/L 0.2 0.7 98 3

Determination of Carbonate

and Bicarbonate in water

by Titrimetry

FE-1134 AOAC 920.194 Water mg/L 5 0.5 87 3

FE-1133

Determination of

Monochoramine

Determination of Colour FE-1132 APHA - 2120 B

Determination of Free

Chlorine

Issue by:SQO


CONTROLLED COPY

page :20 of 23

PARAMETER

TEST

METHOD

SOP-


UNIT

METHOD

DETECTION

INPUT

TIME

(Hrs)

ORIGINAL

COST

TEST

DURATI

ON

(Days)

REMARK




Issue Date : 04/04/2016

Rev. No: 6

Drinking water ug/L 0.5 7.3 1022 7

Water ug/L 0.5 7.3 1270 7

Drinking water ug/L 0.5 4 560 7

Water ug/L 0.5 4 696 7

Determination of Volatile

Organic Compounds in

Water with Headspace Trap

GCMS

FE-1136 APHA 6200 B Drinking water ug/L As per SOP 7 890 7

Determination of total

organic carbon(TOC) in

water

FE-1137 APHA - 5310 B water / waste water mg/L 1 1 174 5


in SoilFE-1301

Chemical analysis of

polluted soils. EPA-

Publication.139-4.

Soil/ Sludge/Sediment % - 0.5 87 5

Determination of pH in

SoilFE-1302 EPA-SW-846-9045 C Soil/ Sludge/Sediment - 1 to 14 0.5 87 5


Phosphorus in Soil /

Sediment

FE-1303

Chemical analysis of

ecological materials-3,

APHA - 4500 P D

Soil / Sludge /

Sedimentmg/Kg 1 1.7 296 5

Determination of Trace

elements (Sb, As, Ba, Be, Cd,

Cr, Pb, Mn, Mo, Ni, Se, Ag, Sn,

U ) by ICP-MS

FE-1135 APHA - 3125

Determination of Trace

elements Mercury (Hg) in

by ICP-MS

FE-1135 APHA - 3125

Sediment APHA - 4500 P D

Cu-4

Cd-2

Zn-4

Pb-15

Ni-16

Cr-9


Petroleum Hydrocarbons in

Soil

FE-1305MOOPAM 4

th ED.

–Section 6.7, 6.9

Soil / Sludge /

Sedimentmg/Kg 0.2 2.1 365 7

Determination of Oil and

Grease in Soil / SludgeFE-1306 APHA - 5520 E

Soil / Sludge /

Sedimentmg/kg ** 1.1 191 7

Determination of Sludge-

Leachate test FE-1307 DM, EPSS TG-No-43

Soil / Sludge /

Sedimentmg/L - 4.55 792 7

Determination of Water

soluble chloride FE-1308

EPA,Melbourne publication

139-17Soil/ Sludge/Sediment mg/kg ** 0.6 104 5

Determination of Electrical

conductivity of soilFE-1309

EPA,Melbourne publication

139-6

Soil / Sludge /

SedimentmS/cm 0.1 0.5 87 5

Determination of Mercury

in oilFE-1310

ASTM 1992.Section

11.APHA 3111Oil ng/g ** 2.1 365 7


Metals [Copper (Cu),

Cadmium (Cd), Lead (Pb),

Zinc (Zn) ] in fish

FE-1401MOOPAM 4

th ED. - Section

5.3, 5.4

Fish / Biological

Samplemg/g ** 2.1 497 10

Determination of

Hydrocarbons in fishFE-1402

MOOPAM 4th

ED. - Section

6.8, 6.9

Fish / Biological

Samplemg/g 0.2 2.6 452 10

Issue by:SQO

10


Heavy Metals [Copper

(Cu), Cadmium (Cd),

Lead (Pb),Nickel

(Ni),Zinc (Zn), Chromium

(Cr)] in Soil / Sediment

FE-1304*

EPA-139-13

Melbourne.1981,

MOOPAM 4th

edition &

APHA -3111

Soil / Sludge /

Sedimentmg/kg 2.1 585


CONTROLLED COPY

page :21 of 23

PARAMETER

TEST

METHOD

SOP-


UNIT

METHOD

DETECTION

INPUT

TIME

(Hrs)

ORIGINAL

COST

TEST

DURATI

ON

(Days)

REMARK




Issue Date : 04/04/2016

Rev. No: 6

Organic Matter and ash in

Organic Fertilizers Growing

Media

FE-1701

AOAC, 19th

Edn (2012)

967.04 / 967.05 & British

Standard BS EN 13039 :

2000

Organic Fertilizers % - 0.5 87 5

Water/waste water CFU/100 mL 1/100 ml 0.35 61 3

Drinking water CFU/100 mL 1/100 ml 0.35 49 3

Water/waste water CFU/ mL 1/1ml 0.35 61 4

Drinking water CFU/ mL 1/1ml 0.35 49

Water/waste water CFU/100 mL 1 /100ml 104

Drinking water CFU/250 mL 1 /250ml 84

Detection and Enumeration

of Legionella species FE-1605*

BSI BS 6068 section 4.12

:1998Water /Waste water CFU/L 1 /L 2.3 400 16


of Coliforms and E.ColiFE-1601* APHA - 9223 B

APHA - 9215 A & BFE-1603*Enumeration of Aerobic

Colony Count


of Pseudomonas aeruginosa FE-1604*


:19890.6 5




of Sulphite reducing

clostridia in drinking water

FE-1609*BSEN 26461 Part 2 1993

water quality detectionDrinking water CFU/250 mL 1 /250ml 0.6 84 5

Detection & Enumeration of

Legionella spp. & L

pneumophila in water and

wastewater by

(RT-PCR)

FE-1610


Legionella spp. & L

pneumophila (BIO-RAD

manual)

Water /Waste water UG/L 1 2.8 487 3

1Hr 174

Determination of Mercury

in oilFE-1310

ASTM 1992.Section

11.APHA 3111Oil ng/g ** 2.1 365 7


Metals [Copper (Cu),

Cadmium (Cd), Lead (Pb),

Zinc (Zn) ] in fish

FE-1401MOOPAM 4

th ED. - Section

5.3, 5.4

Fish / Biological

Samplemg/g ** 2.1 497 10

Determination of

Hydrocarbons in fishFE-1402

MOOPAM 4th

ED. - Section

6.8, 6.9

Fish / Biological

Samplemg/g 0.2 2.6 452 10

Organic Matter and ash in

Organic Fertilizers Growing

Media

FE-1701

AOAC, 19th

Edn (2012)

967.04 / 967.05 & British

Standard BS EN 13039 :

2000

Organic Fertilizers % - 0.5 87 5

Detection and Enumuration

of Faecal StreptococciFE-1606*


:19890.6 5

Sampling NA NA NA NA NA NA

Issue by:SQO


CONTROLLED COPY

page :22 of 23

PARAMETER

TEST

METHOD

SOP-


UNIT

METHOD

DETECTION

INPUT

TIME

(Hrs)

ORIGINAL

COST

TEST

DURATI

ON

(Days)

REMARK




Issue Date : 04/04/2016

Rev. No: 6

Drinking water 0.35 49 3

Water/waste water/ 0.35 61 3

Drinking water 0.35 49

Water/waste water 0.35 61 4

Water/waste water CFU/100 mL 1 /100ml 0.6 104

Drinking water CFU/250 mL 1 /250ml 0.6 84


of Legionella species FE-1605*


:1998Water /Waste water CFU/L 1 /L 2.3 400 16


of Coliforms and E.ColiCFU/100 mL 1/100 mlFE-1601* APHA - 9223 B

Enumeration of Aerobic

Colony Count FE-1603* APHA - 9215 A & B CFU/ mL 1/1ml


of Pseudomonas aeruginosa FE-1604*


:19895

Issue by:SQO




of Sulphite reducing

clostridia in drinking water

FE-1609*BSEN 26461 Part 2 1993

water quality detectionDrinking water CFU/250 mL 1 /250ml 0.6 84 5


Legionella spp. & L

pneumophila in water and

wastewater by

(RT-PCR)

FE-1610


Legionella spp. & L

pneumophila (BIO-RAD

manual)

Water /Waste water UG/L 1 2.8 500 3

1Hr 174

2Hr 348

3 Hr 522

Issue by:SQO

NA NA NA NA

** The method detection limit will be calculated during the analysis depending on the

type and weight of sample.

Detection and Enumuration

of Faecal StreptococciFE-1606*


:19890.6 5

Sampling NA NA


CONTROLLED COPY

page :23 of 23

PARAMETER

TEST

METHOD

SOP-


UNIT

METHOD

DETECTION

INPUT

TIME

(Hrs)

ORIGINAL

COST

TEST

DURATI

ON

(Days)

REMARK




Issue Date : 04/04/2016

Rev. No: 6

Prepared By:

S. No. Employee No.

1 1447

3 465

2 -

Reviewed By:

S. No. Employee No.

1 1789

TECHICAL APPOVALS

Makeya Abdulrahman AlRais

Name

Dr.Hamed Mohammed Ibrahim

Signature

Lilly George

Dr.Alamuri Gopalakrishnamacharyulu

Name Signature

This procedure was Prepared, Reviewed and Approved for technical content by the following Staff:

1 1789

2 9394

3 16064

4 5426

5 6262

6 13871

S. No. Employee No.

1 9550

2 5426

3 4762

Issue by:SQO

Shaikha Khalfan AlJallaf

Aisha Ibrahim Al Beshr

Name

Farida Mohammed Alamadi

Approved By HOUs( Food Chemical Analysis , Food Microbiology Analysis and Environment Unit)

Signature

Makeya Abdulrahman AlRais

Majida Mohammed AlHarmoodi

Wedad Saeed AbdulRahman

Shaikha Khalfan Al Jallaf

Vaidehi Garimella

Fatma Hassan AlObaidly


CONTROLLED COPY

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