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COLONIAL TERMINALS PLANT #2 SEMI-ANNUAL PROGRESS …
Transcript of COLONIAL TERMINALS PLANT #2 SEMI-ANNUAL PROGRESS …
Ramboll Environ
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Atlanta, GA 30339
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www.ramboll-environ.com
Prepared for
Colonial Terminals, Inc.
Savannah, Georgia
Georgia HSI Site No. 10098
Date
May 2016
COLONIAL TERMINALS PLANT #2
SEMI-ANNUAL PROGRESS REPORT
MAY 2016
May 2016 Semi-Annual Progress Report
Contents
1. INTRODUCTION 1 2. BACKGROUND 3 2.1 Site Geology 3 2.2 Site Hydrogeology 3 2.3 Summary of Corrective Action 4 2.4 Risk Reduction Standards 4 2.5 Vapor Intrusion 5 3. SITE ACTIVITIES – CURRENT PERIOD OF PERFORMANCE 6 3.1 Surface Water Sampling – May 2016 6 3.2 Analytical Results 6 4. SUMMARY 7 5. REFERENCES 8
LIST OF TABLES
Table 1: Summary of VOCs in Surface Water
LIST OF FIGURES
Figure 1: Site Location Map
Figure 2: Site Layout
Figure 3: Tax Parcel Location Map
Figure 4: Groundwater Monitoring Well and Surface Water Sampling Locations
Figure 5: Summary of VOC Results in Surface Water
APPENDICES
Appendix A Surface Water Sampling Logs
Appendix B Laboratory Analytical Report
May 2016 Semi-Annual Progress Report
Acronyms and Abbreviations i
Acronyms and Abbreviations
11DCE 1,1-Dichloroethene
12DCE 1,2-Dichloroethene
AST Aboveground Storage Tank
CAP Corrective Action Plan
Colonial Colonial Terminals
COPCs Constituents Of Potential Concern
CSR Compliance Status Report
ED Exposure Domain
EPD Georgia Environmental Protection Division
ERM Environmental Resources Management
ft amsl Feet Above Mean Sea Level
ft bgs Feet Below Ground Surface
ft/d Feet Per Day
HSI Hazardous Site Inventory
HSRA Hazardous Site Response Act
ISWQS Georgia In-Stream Water Quality Standards
MeCl Methylene Chloride
PCE Tetrachloroethene
REH Ramboll Environ
RPs Responsible Parties
RRS Risk Reduction Standards
SVE Soil Vapor Extraction
TCE Trichloroethene
Test America Test America Laboratories, Inc
UCL Upper Confidence Limit
UEC Uniform Environmental Covenant
USEPA United States Environmental Protection Agency
VC Vinyl Chloride
VOCs Volatile Organic Compounds
VRP Voluntary Remediation Program
May 2016 Semi-Annual Progress Report
Introduction 1
1. INTRODUCTION
The Colonial Terminals (Colonial) Plant #2 site is listed on the Georgia Environmental Protection
Division (EPD) Hazardous Site Inventory (HSI) as Site No. 10098 under the Hazardous Site Response
Act (HSRA). The site is located at 373 North Lathrop Avenue, Savannah, Chatham County, Georgia
(Figure 1). The approximately 78-acre property is comprised of six adjacent parcels of land identified
by the Chatham County Board of Assessors as Tax Parcel IDs 1-0549-01-002 (3 parcels maintain this
ID), 1-0549-01-002A, 1-0551-01-047, and 1-0550-02-004. The highly industrialized property is
bordered by the Savannah River and is improved with administrative buildings, warehouses, bulk
aboveground storage tanks (ASTs) and silos, shipping docks, truck loading racks, pipe racks, and rail
spurs (Figure 2).
The site was formerly owned and operated by Virginia-Carolina Chemical Company and Swift
Agricultural Chemicals Corporation for the manufacture of fertilizers from the late 1926 through 1972.
During that time, the site maintained two sludge-settling ponds and an adjacent sludge pile that have
been documented as likely sources of impacts at the site, and historical fertilizer production facilities
were present at various locations to the east side of the current rail yard. Since the early 1970s,
Colonial has owned and operated the site for use as a bulk storage facility for various chemicals,
petroleum, and kaolin clay. According to previous investigations and facility personnel, from 1981
through 1985 tetrachloroethylene (PCE) and trichloroethylene (TCE) were transferred from vessels to
railcars and then to trucks in the area adjacent to the two former settling ponds and the sludge pile.
From 1985 through 1990, PCE and TCE was stored in ASTs T-77 and T-78, located near the central
northern end of the site, and in the adjacent ASTs 110 through 113 from 1991 through 2009.
An investigation of the former settling ponds and sludge pile was conducted by the United States
Environmental Protection Agency (USEPA) in 1984 and identified the presence of TCE at the site.
Following an evaluation by the EPD in June 1994, the site was listed on the HSI for known releases of
metals and volatile organic compounds (VOCs) to the soil and groundwater. In addition, methylene
chloride (MeCl) and PCE degradation products 1,2-dichloroethene (12DCE); 1,1-dichloroethene
(11DCE); and vinyl chloride (VC) were identified in soil and groundwater at the site during subsequent
investigations. An initial Compliance Status Report (CSR) was submitted to EPD in 1999, and since
that time numerous revised CSRs, Corrective Action Plans (CAPs), and other reports have been
submitted that document the significant efforts that have been conducted at the site, including: the
excavation and offsite disposal of more than 24,000 tons of impacted soil; the implementation of a soil
vapor extraction system to address residual VOCs in the soil; completion of a large-scale in situ
chemical oxidation pilot test that involved the installation of 250 injection wells and injection of more
than 150,000 gallons of solution containing persulfate, lime, and caustic; and periodic groundwater
sampling of onsite monitoring wells. Colonial submitted an application to the Georgia Voluntary
Remediation Program (VRP) for the site in November 2012, and the application was approved by EPD
in May 2013. A meeting to discuss EPD’s comments and the responsible parties’ (RPs’; Colonial, BFEL
Indemnitor, Inc., and ExxonMobil Corporation) responses to those comments was held at EPD’s offices
on October 1, 2013.
Per the November 2012 VRP application (ENVIRON International Corporation, predecessor to Ramboll
Environ [REH], 2012), additional corrective action for soil, groundwater, and surface water at the site
is not warranted based on current site conditions, the exposure pathways, and the comparison of
existing data to site-specific cleanup standards. As agreed upon with EPD, annual groundwater
sampling of seven shallow and three deeper monitoring wells was to be conducted for two years to
May 2016 Semi-Annual Progress Report
Introduction 2
identify and track potential future changes related to groundwater at the site, and the last sampling
event occurred in November 2014. In addition, semi-annual surface water sampling was to be
conducted for three years to monitor the concentrations of VOCs in the Savannah River. Additionally,
an environmental covenant was to be executed on the site in conformance with O.C.G.A. 44-61-1, et
seq., the “Georgia Uniform Environmental Covenants Act.” This covenant will specify that the land use
of the site remains industrial, no drinking water wells will be installed on the site, and any future plans
for constructing new buildings on the site will be evaluated with respect to potential risks associated
with vapor intrusion. Per the VRP, semi-annual surface water sampling was conducted in May 2016.
The analytical results from the sampling event did not indicate the presence of VOCs in the Savannah
River adjacent to the site
The remainder of this Progress Report presents background site information (Section 2), site activities
since the submittal of the November 2015 Status Report (Section 3), and a summary of expected
future site activities (Section 4).
May 2016 Semi-Annual Progress Report
Background 3
2. BACKGROUND
The Colonial site is located in a highly industrial area of Savannah, Georgia, and is bordered to the
north and northeast by the Savannah River (which is in high industrial use and has been altered for
that purpose), to the southeast by Georgia Recyclers, to the south by North Lathrop Avenue (on the
other side of which is Great Dane Trailers), and to the west by Arboris, LLC and International Paper
Company’s Savannah Pulp and Paper Mill. With the exception of the earthen berms at the site that
surround the ASTs, the surface topography at the site is relatively flat and ranges from approximately
9 feet above mean sea level (ft amsl) at the southern and western property boundaries to
approximately 4 ft amsl at the northern property boundary along the Savannah River.
According to the Chatham County Board of Assessors, the site is owned and maintained by Colonial,
and consists of Tax Parcel IDs 1-0549-01-002, 1-0549-01-002A, 1-0551-01-047, and 1-0550-02-004.
The previous site owners include Virginia-Carolina Chemical Company (now Exxon Mobil Corporation)
and Swift Agricultural Chemicals Corporation (now BFEL Indemnitor, Inc.). Per EPD’s request, an
updated tax parcel location map with tax identification numbers for the entire site is provided in
Figure 3.
2.1 Site Geology
The site is located in the Barrier Island Sequence District of the Coastal Plain Physiographic Province of
Georgia. Regional soils are characterized by Pleistocene and Holocene barrier island deposits and
marsh and lagoon deposits. Pleistocene sea levels advanced and retreated several times over the
Coastal Plain to form a step-like progression of decreasing elevation toward the sea (Clark and Zisa,
1976). The area during the time of the former, higher sea levels existed as barrier island-salt marsh
environments similar to the present coast. The changes in sea level left shoreline deposit complexes
parallel to the present coastline, composed predominantly of unconsolidated sand and clayey sand
deposited during the former high sea levels.
The regional geology has been characterized as Coastal Plain strata consisting of unconsolidated to
semi-consolidated layers of sand and clay, and semi-consolidated to very dense layers of limestone
and dolomite (Clarke et al, 1990). These sediments range in age from the late Cretaceous to
Holocene periods. The strata generally strike southwest and northeast, and dip and gradually thicken
to the southeast.
Based on historical site assessment activities, the site geology from land surface to approximately 2
feet below ground surface (ft bgs) consists of sequences of sands, which are underlain by stiff sandy
clays that extend to approximately 8 to 10 ft bgs. Clayey sands with clay stringers are present from
approximately 10 ft bgs to 34 ft bgs, below which clay and silt is present to approximately 80 ft bgs.
2.2 Site Hydrogeology
The Coastal Plain is underlain by multiple aquifers. In the vicinity of the site, the surficial aquifer
consists of the Satilla Formation (Payne, Rumman, and Clarke, 2005). Beneath the surficial aquifer
are the upper and lower Brunswick aquifers, which consist of slightly phosphatic and dolomitic quartz
sands and clay confining units. The Brunswick aquifer system is approximately 80 feet thick in the
region of the site and has a higher percentage of low permeability, clayey deposits in the Savannah
area. The underlying Upper Floridan aquifer, which consists of the Ocala Limestone, is the principal
source of water in the coastal area (Clarke et al, 1990).
May 2016 Semi-Annual Progress Report
Background 4
Due to the proximity of the site to the Savannah River and Atlantic Ocean, the surficial/shallow
groundwater at the site is influenced by tidal activity, and the depth to groundwater at the site
typically ranges from approximately 3 to 12 ft bgs. Additionally, the shallow groundwater at the site
has a high saline content due to tidal influence and, as such, the groundwater in the shallow surficial
aquifer is not potable.
Slug tests were performed in three wells (MW-16, MW-18, and TW-28) on May 25 and 26, 2006, for
the purpose of evaluating the hydraulic conductivity of the shallow aquifer. Based on the results of
the tests, the average hydraulic conductivity of the shallow surficial aquifer at the site is
approximately 3.05 x 10-3 centimeters per second. Based on the site gradient, and assuming an
effective porosity of 20 percent, the groundwater flow velocity is estimated to range between 0.1 feet
per day (ft/d) and 0.2 ft/d.
2.3 Summary of Corrective Action
Corrective action has been undertaken for soil and groundwater at the site, as discussed in the 2012
VRP application and the November 2013 and May 2014 Semi-Annual Status Reports. Specifically,
corrective action has consisted of the following activities:
Excavation and offsite disposal of:
- Approximately 23,415 tons of lead and/or arsenic-impacted soil from eight distinct areas of the
site between October 2007 and December 2007.
- Approximately 812 tons of VOC-impacted soil adjacent to Tank T-88 at the southeast portion
of the site in December 2007.
- Approximately 38 tons of soil from the area surrounding historical soil boring GP-07-06 in
February and March 2009.
Operation of a soil vapor extraction (SVE) system from May 2009 through May 2013 for the
purpose of addressing VOC impacts in the vicinity of Tank 75 through Tank 78. Following removal
of approximately 6,137 pounds of total VOCs and upon meeting the shutdown criteria specified in
the Performance Monitoring Plan (Environmental Resources Management [ERM], 2009), the
system was discontinued in May 2013.
Injection of more than 150,000 gallons of a solution containing sodium persulfate, lime, and
caustic using 250 injection wells for the purpose of treating metals and VOCs in the groundwater
(ERM, 2010). In addition, a network of 34 groundwater monitoring wells were sampled annually
from 2008 through 2010 to gauge the effectiveness of the chemical injections.
2.4 Risk Reduction Standards
The site and surrounding properties are used for non-residential purposes and, therefore, Type 4 risk
reduction standards (RRS; non-residential, site-specific) for the site were submitted as part of the VRP
application. Specifically, RRS for constituents of potential concern (COPCs) in surface soil were
developed to be protective of commercial/industrial, utility, and construction workers at the site via
direct contact, and RRS for COPCs in subsurface soil were developed to be protective of utility and
construction workers via direct contact. Based on previous communication between the RPs and EPD,
the following conditions have been agreed upon regarding the RRS for the site:
The use of one exposure domain (ED) for surface soil (0 to 2 feet below ground surface) is
acceptable;
Development of Type 2 RRS is not necessary provided that the Uniform Environmental Covenant
(UEC) for the site indicates non-residential use for the site;
May 2016 Semi-Annual Progress Report
Background 5
The UEC will include language that limits construction worker scenarios to 90 days of exposure to
subsurface soil;
Trespasser scenarios are not applicable to the site because the commercial/industrial worker
exposure scenario is considered more conservative and, therefore, protective of a trespasser; and,
Exposure to groundwater does not constitute a complete exposure pathway with regards to human
health and, therefore, leaching to groundwater is not a required component of the site-specific
RRS for soil. As such, and per EPD’s request, the soil RRS will be herein referred to as Type 5
RRS.
The exposure conditions at the site have not changed since the submittal of the VRP application.
Based on discussions with the EPD, the entire site is considered to comprise one ED for the surface
soil, and three EDs were proposed for subsurface soil in the November 10, 2014, responses to EPD
comments. In those responses to comments, an area averaging approach using 95 percent Upper
Confidence Levels (UCLs) was used to determine that exposure point concentrations for arsenic and
lead in surface and subsurface soil (i.e., the two constituents for which there were individual
exceedances of the RRS) do not exceed their respective RRS.
In addition to the RRS presented in the VRP application, EPD previously approved Type 5 RRS for two
conditions at the site, as presented in the 2012 VRP application and the November 2013 and May
2014 Semi-Annual Status Reports:
Areas within 12 feet of the railroad centerline where excavations could result in a loss of structural
integrity of the tracks; and,
Deep soil adjacent to retaining walls and loading docks along the Savannah River.
The site maintains engineering and institutional controls for these Type 5 RRS areas, including a
Restrictive Covenant on the deeds for the three parcels that comprise the site.
Because there is no direct exposure to groundwater via ingestion or inhalation at or within 1,000 feet
of the site, updated RRS were not developed for groundwater.
2.5 Vapor Intrusion
Based on a comparison of the maximum detected concentrations of and 95 percent UCLs for VOCs in
soil and groundwater with vapor intrusion criteria (ENVIRON, 2012), there are two locations at the site
(GP-07-04 and GP-07-06, as presented in Figure 15 of the VRP application) that could result in
unacceptable risks associated with vapor intrusion exposures, as presented in the 2012 VRP
application and the November 2013 Semi-Annual Status Report. However, because these locations
are not under or in immediate proximity to current site structures at which workers might be exposed
to indoor air, cleanup standards have not been derived for the vapor intrusion pathway. As agreed
upon by EPD in October 2013, location-specific vapor intrusion risks will be assessed if needed and
mitigation measures, if necessary, will be implemented prior to or during future construction of
inhabited structures at the site.
May 2016 Semi-Annual Progress Report
Site Activities – Current Period of Performance 6
3. SITE ACTIVITIES – CURRENT PERIOD OF PERFORMANCE
In accordance with the agreement between the RPs and EPD under the VRP, surface water samples
were collected from three locations along the bank of the Savannah River on May 4, 2016 (the
required annual surface water sampling was completed in October 2014). A summary of these
activities is presented in the following sections.
3.1 Surface Water Sampling – May 2016
Per the approved monitoring plan presented in the VRP application, REH collected surface water
samples from three locations along the bank of the Savannah River on May 4, 2016 (Figure 4). The
surface water samples were collected from walkways to the main dock, as close to the river bank and
slope of the river bottom as possible. As requested by EPD in Comment #3 of their letter to Colonial
Terminals dated February 16, 2016, representatives from EPD were onsite during the surface water
sampling event to “assess conditions along the bank of the river in the area closest to the
groundwater impacts to determine if any modifications” could be made. While onsite on May 4, EPD
personnel did not indicate the need to modify the sampling locations.
The surface water samples were collected from approximately 1 foot above the bottom of the river at
locations where the water depth ranged from 2.1 to 4.2 feet, as follows:
SW-01R – Water Depth: 4.2 feet;
SW-02R – Water Depth: 2.9 feet; and,
SW-03R – Water Depth: 2.1 feet.
Prior to sampling at each location, surface water was withdrawn for 5 minutes with a peristaltic pump
fitted with new, disposable tubing, after which the surface water samples were collected by filling
laboratory-provided, appropriately-preserved, sample containers. Each sample container was labeled,
placed on ice, and hand-delivered to Test America Laboratories, Inc. (Test America) in Savannah,
Georgia, for analysis of VOCs by USEPA Method 8260B. The surface water samples were collected
between 1:10 pm and 2:40 pm. Low tide for that day occurred at 1:43 pm (Savannah, Georgia – Bull
Street Monitoring Station).
3.2 Analytical Results
There were no detections of VOCs in the surface water (Table 1 and Figure 5). The surface water
sampling logs are included in Appendix A, and the laboratory analytical report is provided in
Appendix B.
May 2016 Semi-Annual Progress Report
Summary 7
4. SUMMARY
Per the VRP, the final semi-annual surface water sampling was conducted on May 4, 2016. The
analytical results from the sampling event did not indicate the presence of VOCs in the Savannah
River adjacent to the site. The surface water samples were collected as close as possible along the
bank of the Savannah River, and at low tide, to provide data representative of the most conservative
conditions.
The potential exposure pathways at the site remain consistent with those defined in the VRP
application and subsequent correspondence with EPD. Specifically, “there is no direct exposure to
groundwater via ingestion or inhalation at or within 1,000 feet of the site,” and the concentrations of
VOCs in the surface water continues to be non-detect (and less than the Georgia In-Stream Water
Quality Standards).
Based on the groundwater and surface water data collected since being admitted to the VRP, and in
accordance with the schedule set forth in the VRP application and subsequent correspondence with
EPD, the next steps for the site include the development of a final CSR and UEC.
May 2016 Semi-Annual Progress Report
References 8
5. REFERENCES
Clark, William Z., and Zisa, Arnold C. 1976. Physiographic Map of Georgia. Georgia Department of Natural Resources, Geologic and Water Resources Division. 1 pl.
Clarke, John S., Hackle, Charles M., and Peck, Michael F. 1990. Geology and Ground-Water Resources of the Coastal Area of Georgia; Georgia Geologic Survey Bulletin 113. 12 pl.
Environmental Resources Management (ERM). 2009. Revised Corrective Action Plan for Volatile Organic Compounds. January.
ERM. 2010. First Corrective Action Effectiveness Report (CAER) for Groundwater 2009. January.
Payne, Dorothy F., Rumman, Malek A., and Clarke, John S. 2005. Simulation of ground-water flow in coastal Georgia and adjacent parts of South Carolina and Florida – Predevelopment, 1980, and 2000. United States Geological Survey Scientific Investigation Report 2005-5089.
Ramboll Environ, formerly ENVIRON International Corporation. 2012. Voluntary Remediation Plan and Application – Colonial Terminals Plant #2.
Table1‐SummaryofVOCsinSurfaceWaterColonialTerminalsPlant#2(HSI10098)
May2016StatusReport
Analyte PCE TCE c12DCE t12DCE VinylChlorideGAISWQS (1) 3.3 30 ‐‐ ‐‐ 2.4
Units ug/l ug/l ug/l ug/l ug/lLocation DateSampled
SW‐01 9/17/2010 < 1 < 1 < 1 < 1 < 1 12/13/2013 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 4/19/2014 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0
SW‐01R 10/28/2014 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 4/22/2015 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 10/6/2015 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0
DUP‐01 10/6/2015 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 5/4/2016 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0
DUP‐01 5/4/2016 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 SW‐02 9/17/2010 < 1 < 1 < 1 < 1 < 1
12/13/2013 1.4 < 1.0 < 1.0 < 1.0 < 1.0 4/19/2014 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0
SW‐02R 10/28/2014 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 4/22/2015 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 10/6/2015 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 5/4/2016 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0
SW‐03 9/17/2010 < 1 < 1 < 1 < 1 < 1 12/13/2013 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 4/19/2014 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0
SW‐03R 10/28/2014 1.1 < 1.0 < 1.0 < 1.0 < 1.0 4/22/2015 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 10/6/2015 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 5/4/2016 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0
Notes:(1) Georgia In‐Stream Water Quality Standards (March 2012)< ‐‐ Analyte was not detected at the laboratory reporting limit indicatedug/l ‐‐ Micrograms per liter (parts per billion)PCE ‐‐ TetrachloroetheneTCE ‐‐ Trichloroethenec12DCE ‐‐ cis‐1,2‐Dichloroethenet12DCE ‐‐ trans‐1,2‐Dichloroethene
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SITE
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CONTOUR INTERVAL 20 FEET
SITE LOCATION MAP
COLONIAL TERMINALS, INC.
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SITE LAYOUT
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SOURCE: GOOGLE EARTH PRO (JANUARY 2011).
TAX PARCEL LOCATION MAP
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SW-02
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MW-14
MW-11D
MW-6R
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MW-33
MW-27
MW-9
MW-23
MW-22
MW-28
TW-21
TW-17
MW-16
TW-12
MW-24
TW-13
TW-5
TW-6
TW-7
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TW-9
TW-19
TW-18
MW-4
MW-20
MW-29
MW-11R
MW-25
MW-11
TW-4
MW-3
MW-1
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MW-8
MW-31
TW-10
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MW-32
MW-10
MW-21
TW-25
MW-35
TW-27
TW-31
TW-32
TW-23
MW-30
TW-16
TW-28
TW-22
TW-14
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MW-26
TW-15
TW-29
MW-15
MW-18
MW-12
MW-6
MW-102D
MW-101D
SW-01R
SW-02R
SW-03R
MW-12R
SW-03
Sources: Environmental Resources Management, Drawing 1, Site Layout Map, Revised Cap for VOCs, for Colonial Terminals, Inc.,
LEGEND
EXISTING MONITORING WELL
DEEP MONITORING WELL
TEMPORARY MONITORING WELL
SURFACE WATER SAMPLE
PILOT TEST WELL
MONITORING WELL AND SURFACE
WATER SAMPLING LOCATIONS
COLONIAL TERMINALS, INC.
373 N. LATHROP AVENUE
SAVANNAH, GEORGIA
L:\Loop Project Files\00_CAD
FILES\07\Colonial Term
_2013-2014 M
onitoring 0730114D
\2015-10\04_M
W and Surface W
ater Sam
pling Locations.dw
g
DRAFTED BY:
FIGURE
DATE:CKL 10/29/15 07-30114D
4
0 200
SCALE IN FEET
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TW-6
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TW-19
TW-18
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MW-25
MW-11
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MW-10
MW-21
TW-25
MW-35
TW-27
TW-31
TW-32
TW-23
MW-30
TW-16
TW-28
TW-22
TW-14
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MW-19
MW-26
TW-15
TW-29
MW-15
MW-18
MW-12
MW-6
MW-102D
MW-101D
SW-01R
SW-02R
SW-03R
MW-12R
SW-03
Sources: Environmental Resources Management, Drawing 1, Site Layout Map, Revised Cap for VOCs, for Colonial Terminals, Inc., December 2008. Image obtained from Google Earth Pro. Photo dated January 2011.
LEGEND
EXISTING MONITORING WELL
DEEP MONITORING WELL
TEMPORARY MONITORING WELL
SURFACE WATER SAMPLE
PILOT TEST WELL
SW-01
Date PCE TCE c12DCE t12DCE VC9/17/2010 < 1 < 1 < 1 < 1 < 1
12/13/2013 < 1.0 < 1.0 < 1.0 < 1.0 < 1.04/19/2014 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0
SW-01R
Date PCE TCE c12DCE t12DCE VC10/28/2014 < 1.0 < 1.0 < 1.0 < 1.0 < 1.04/22/2015 < 1.0 < 1.0 < 1.0 < 1.0 < 1.010/6/2015 < 1.0 < 1.0 < 1.0 < 1.0 < 1.05/4/2016 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0
Notes:
PCE = Tetrachloroethylene
TCE = Trichloroethylene
c12DCE = cis-1,2-Dichloroethene
t12DEC = trans-1,2-Dichloroethene
VC = Vinyl Chloride
Bold and highlighted values indicate an exceedance of the chemical-specific Georgia ISWQS
All concentrations are in micrograms per liter (ug/L)
< Analyte was not detected at the laboratory reporting limit indicated
SW-02
Date PCE TCE c12DCE t12DCE VC9/17/2010 < 1 < 1 < 1 < 1 < 1
12/13/2013 1.4 < 1.0 < 1.0 < 1.0 < 1.04/19/2014 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0
SW-03
Date PCE TCE c12DCE t12DCE VC9/17/2010 < 1 < 1 < 1 < 1 < 1
12/13/2013 < 1.0 < 1.0 < 1.0 < 1.0 < 1.04/19/2014 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0
Georgia ISWQSPCE TCE c12DCE t12DCE VC3.3 30 N/A N/A 2.4
SUMMARY OF VOC RESULTS IN
SURFACE WATER
COLONIAL TERMINALS, INC.
373 N. LATHROP AVENUE
SAVANNAH, GEORGIA
L:\Loop Project Files\00_CAD
FILES\07\Colonial Term
_2013-2014 M
onitoring 0730114D
\2016-05\05_Sum
mary of VO
Cs in Surface W
ater.dw
g
DRAFTED BY:
FIGURE
DATE:CKL 5/13/16 07-30114D
5
0 200
SCALE IN FEET
SW-03R
Date PCE TCE c12DCE t12DCE VC10/28/2014 1.1 < 1.0 < 1.0 < 1.0 < 1.04/22/2015 < 1.0 < 1.0 < 1.0 < 1.0 < 1.010/6/2015 < 1.0 < 1.0 < 1.0 < 1.0 < 1.05/4/2016 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0
SW-02R
Date PCE TCE c12DCE t12DCE VC10/28/2014 < 1.0 < 1.0 < 1.0 < 1.0 < 1.04/22/2015 < 1.0 < 1.0 < 1.0 < 1.0 < 1.010/6/2015 < 1.0 < 1.0 < 1.0 < 1.0 < 1.05/4/2016 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0
Date Time M/D/Y HH:MM:SS Temp C SpCond uS Sal ppt DOsat % DO mg/L pH pH mV Orp mV Baro mmHg05/04/16 11:56:19 26.92 20 0.01 184.7 14.74 7.17 -17.8 195.7 764.505/04/16 11:56:24 25.82 3230 1.68 183.9 14.83 7.09 -13.3 202.6 764.505/04/16 11:56:29 25.31 3887 2.05 182.9 14.85 7.05 -11.2 203.3 764.405/04/16 11:56:34 24.98 4247 2.25 173.6 14.17 7.02 -9.7 203.7 764.405/04/16 11:56:39 24.79 4445 2.37 160.2 13.11 7.00 -8.5 203.8 764.505/04/16 11:56:44 24.68 4554 2.43 147.1 12.06 6.98 -7.6 203.9 764.405/04/16 11:56:49 24.60 4614 2.46 135.8 11.15 6.97 -6.9 203.9 764.405/04/16 11:56:54 24.54 4648 2.48 127.0 10.43 6.96 -6.3 203.9 764.505/04/16 11:56:59 24.50 4665 2.49 120.4 9.90 6.95 -5.7 203.8 764.505/04/16 11:57:04 24.45 4676 2.50 115.9 9.54 6.94 -5.2 203.7 764.505/04/16 11:57:09 24.41 4685 2.50 113.2 9.32 6.93 -4.7 203.7 764.505/04/16 11:57:14 24.37 4692 2.51 111.6 9.19 6.92 -4.3 203.6 764.505/04/16 11:57:19 24.36 4697 2.51 110.5 9.11 6.92 -4.0 203.6 764.605/04/16 11:57:24 24.36 4701 2.51 109.7 9.04 6.91 -3.7 203.5 764.605/04/16 11:57:29 24.35 4705 2.51 108.8 8.97 6.91 -3.4 203.5 764.505/04/16 11:57:34 24.33 4709 2.52 107.5 8.87 6.90 -3.2 203.5 764.505/04/16 11:57:39 24.31 4714 2.52 105.9 8.74 6.90 -3.0 203.4 764.605/04/16 11:57:44 24.28 4718 2.52 104.1 8.59 6.89 -2.8 203.3 764.605/04/16 11:57:49 24.27 4721 2.52 102.5 8.46 6.89 -2.6 203.3 764.505/04/16 11:57:54 24.26 4721 2.52 101.2 8.36 6.89 -2.4 203.2 764.505/04/16 11:57:59 24.25 4718 2.52 100.3 8.29 6.89 -2.3 203.2 764.605/04/16 11:58:04 24.26 4713 2.52 100.1 8.26 6.88 -2.2 203.1 764.505/04/16 11:58:09 24.25 4709 2.52 100.0 8.26 6.88 -2.0 203.0 764.505/04/16 11:58:14 24.25 4705 2.51 99.2 8.20 6.88 -1.9 203.0 764.505/04/16 11:58:19 24.24 4701 2.51 97.8 8.08 6.88 -1.8 202.9 764.605/04/16 11:58:24 24.24 4696 2.51 96.5 7.97 6.87 -1.7 202.9 764.505/04/16 11:58:29 24.23 4692 2.51 95.4 7.88 6.87 -1.6 202.8 764.405/04/16 11:58:34 24.23 4690 2.51 94.5 7.81 6.87 -1.5 202.7 764.405/04/16 11:58:39 24.23 4690 2.51 94.1 7.78 6.87 -1.4 202.7 764.505/04/16 11:58:44 24.23 4690 2.51 93.7 7.74 6.87 -1.3 202.6 764.505/04/16 11:58:49 24.22 4689 2.51 93.3 7.71 6.87 -1.2 202.5 764.405/04/16 11:58:54 24.19 4691 2.51 92.8 7.68 6.86 -1.1 202.5 764.405/04/16 11:58:59 24.16 4694 2.51 92.5 7.65 6.86 -1.0 202.4 764.505/04/16 11:59:04 24.13 4696 2.51 92.2 7.63 6.86 -0.9 202.4 764.405/04/16 11:59:09 24.11 4697 2.51 91.9 7.61 6.86 -0.8 202.3 764.405/04/16 11:59:14 24.07 4700 2.51 91.8 7.61 6.86 -0.7 202.2 764.405/04/16 11:59:19 24.03 4703 2.51 91.7 7.61 6.85 -0.6 202.1 764.405/04/16 11:59:24 23.99 4705 2.51 91.6 7.60 6.85 -0.5 202.1 764.405/04/16 11:59:29 23.97 4705 2.52 91.4 7.59 6.85 -0.4 202.0 764.405/04/16 11:59:34 23.94 4707 2.52 91.4 7.59 6.85 -0.4 201.9 764.405/04/16 11:59:39 23.90 4711 2.52 91.5 7.61 6.85 -0.3 201.9 764.505/04/16 11:59:44 23.86 4713 2.52 91.6 7.62 6.85 -0.3 201.8 764.4
SW-01R
Date Time M/D/Y HH:MM:SS Temp C SpCond uS Sal ppt DOsat % DO mg/L pH pH mV Orp mV Baro mmHgSW-01R
05/04/16 11:59:49 23.84 4715 2.52 91.6 7.62 6.85 -0.2 201.8 764.405/04/16 11:59:54 23.83 4716 2.52 91.6 7.62 6.85 -0.2 201.7 764.405/04/16 11:59:59 23.81 4717 2.52 91.6 7.63 6.85 -0.1 201.7 764.405/04/16 12:00:04 23.79 4719 2.52 91.6 7.63 6.84 -0.1 201.6 764.405/04/16 12:00:09 23.78 4720 2.52 91.5 7.62 6.84 -0.1 201.5 764.405/04/16 12:00:14 23.77 4720 2.52 91.4 7.61 6.84 0.0 201.4 764.405/04/16 12:00:19 23.77 4720 2.52 91.4 7.61 6.84 0.0 201.3 764.405/04/16 12:00:24 23.76 4719 2.52 91.3 7.61 6.84 0.0 201.3 764.405/04/16 12:00:29 23.75 4719 2.52 91.4 7.62 6.84 0.0 201.2 764.405/04/16 12:00:34 23.75 4718 2.52 91.7 7.64 6.84 0.1 201.1 764.405/04/16 12:00:39 23.75 4717 2.52 91.7 7.65 6.84 0.1 201.0 764.505/04/16 12:00:44 23.74 4716 2.52 91.7 7.65 6.84 0.2 201.0 764.505/04/16 12:00:49 23.73 4716 2.52 91.9 7.67 6.84 0.2 200.9 764.505/04/16 12:00:54 23.73 4717 2.52 91.9 7.67 6.84 0.3 200.8 764.505/04/16 12:00:59 23.73 4716 2.52 91.6 7.64 6.84 0.3 200.8 764.605/04/16 12:01:04 23.74 4716 2.52 91.2 7.60 6.84 0.3 200.7 764.605/04/16 12:01:09 23.74 4715 2.52 90.7 7.56 6.84 0.4 200.7 764.505/04/16 12:01:14 23.73 4715 2.52 90.3 7.53 6.84 0.4 200.6 764.505/04/16 12:01:19 23.71 4716 2.52 90.0 7.51 6.83 0.5 200.5 764.605/04/16 12:01:24 23.70 4716 2.52 89.8 7.50 6.83 0.5 200.5 764.605/04/16 12:01:29 23.69 4716 2.52 89.6 7.48 6.83 0.6 200.4 764.605/04/16 12:01:34 23.67 4718 2.52 89.5 7.48 6.83 0.7 200.3 764.605/04/16 12:01:39 23.65 4720 2.52 89.5 7.47 6.83 0.8 200.3 764.605/04/16 12:01:44 23.62 4723 2.53 89.8 7.51 6.83 0.9 200.2 764.6
Date Time M/D/Y HH:MM:SS Temp C SpCond uS Sal ppt DOsat % DO mg/L pH pH mV Orp mV Baro mmHg05/04/16 12:28:45 34.08 48 0.02 173.5 12.24 5.73 62.3 207.1 765.105/04/16 12:28:50 25.55 4006 2.12 210.8 17.04 7.17 -17.8 207.4 765.105/04/16 12:28:55 25.25 4115 2.18 212.4 17.26 7.16 -17.2 207.2 765.105/04/16 12:29:00 25.05 4165 2.21 213.2 17.38 7.14 -16.3 207.2 765.105/04/16 12:29:05 24.90 4187 2.22 213.4 17.45 7.13 -15.3 207.2 765.205/04/16 12:29:10 24.78 4196 2.22 213.7 17.51 7.11 -14.4 207.2 765.205/04/16 12:29:15 24.70 4197 2.23 213.7 17.54 7.09 -13.5 207.3 765.105/04/16 12:29:20 24.61 4196 2.23 214.0 17.59 7.08 -12.8 207.4 765.105/04/16 12:29:25 24.53 4191 2.22 214.2 17.63 7.07 -12.1 207.6 765.105/04/16 12:29:30 24.47 4187 2.22 214.0 17.63 7.06 -11.5 207.8 765.105/04/16 12:29:35 24.42 4180 2.22 213.3 17.59 7.04 -10.9 208.0 765.105/04/16 12:29:40 24.40 4174 2.21 212.7 17.55 7.03 -10.3 208.2 765.105/04/16 12:29:45 24.39 4168 2.21 212.1 17.51 7.02 -9.8 208.4 765.005/04/16 12:29:50 24.39 4161 2.21 211.6 17.46 7.02 -9.3 208.6 765.005/04/16 12:29:55 24.40 4156 2.20 211.0 17.41 7.01 -8.9 208.7 765.005/04/16 12:30:00 24.39 4153 2.20 210.5 17.38 7.00 -8.5 208.9 765.005/04/16 12:30:05 24.35 4153 2.20 210.4 17.38 6.99 -8.1 209.0 765.005/04/16 12:30:10 24.31 4151 2.20 210.2 17.38 6.99 -7.7 209.2 765.005/04/16 12:30:15 24.29 4149 2.20 210.0 17.37 6.98 -7.4 209.3 764.905/04/16 12:30:20 24.27 4147 2.20 209.7 17.34 6.97 -7.0 209.4 764.905/04/16 12:30:25 24.27 4144 2.20 209.4 17.33 6.97 -6.7 209.5 764.905/04/16 12:30:30 24.26 4144 2.20 209.2 17.31 6.96 -6.4 209.7 764.905/04/16 12:30:35 24.25 4143 2.20 208.9 17.29 6.96 -6.1 209.8 764.905/04/16 12:30:40 24.25 4143 2.20 208.6 17.26 6.95 -5.9 209.9 764.905/04/16 12:30:45 24.24 4142 2.20 208.2 17.23 6.95 -5.6 210.0 764.905/04/16 12:30:50 24.25 4141 2.20 207.8 17.20 6.94 -5.4 210.1 764.905/04/16 12:30:55 24.25 4139 2.19 207.4 17.17 6.94 -5.1 210.2 764.905/04/16 12:31:00 24.25 4137 2.19 207.2 17.15 6.93 -4.9 210.3 764.905/04/16 12:31:05 24.25 4133 2.19 206.9 17.12 6.93 -4.7 210.4 764.905/04/16 12:31:10 24.25 4130 2.19 206.5 17.09 6.93 -4.5 210.5 764.905/04/16 12:31:15 24.25 4128 2.19 206.1 17.06 6.92 -4.3 210.6 764.905/04/16 12:31:20 24.26 4126 2.19 205.8 17.03 6.92 -4.1 210.7 764.905/04/16 12:31:25 24.26 4124 2.19 205.5 17.00 6.92 -3.9 210.8 764.905/04/16 12:31:30 24.26 4123 2.19 205.2 16.98 6.91 -3.8 210.8 764.905/04/16 12:31:35 24.26 4123 2.18 205.0 16.96 6.91 -3.6 210.9 764.905/04/16 12:31:40 24.26 4122 2.18 204.8 16.94 6.91 -3.4 211.0 764.905/04/16 12:31:45 24.27 4123 2.18 204.5 16.92 6.90 -3.3 211.1 764.905/04/16 12:31:50 24.27 4124 2.19 204.6 16.93 6.90 -3.1 211.1 764.905/04/16 12:31:55 24.27 4124 2.19 205.4 16.99 6.90 -2.9 211.2 764.905/04/16 12:32:00 24.26 4123 2.19 205.1 16.97 6.90 -2.8 211.3 765.005/04/16 12:32:05 24.26 4123 2.18 204.1 16.89 6.89 -2.7 211.3 765.005/04/16 12:32:10 24.25 4123 2.18 203.1 16.80 6.89 -2.5 211.4 765.0
SW-02R
Date Time M/D/Y HH:MM:SS Temp C SpCond uS Sal ppt DOsat % DO mg/L pH pH mV Orp mV Baro mmHgSW-02R
05/04/16 12:32:15 24.25 4122 2.18 202.2 16.74 6.89 -2.4 211.5 765.005/04/16 12:32:20 24.24 4121 2.18 201.7 16.69 6.88 -2.2 211.5 765.005/04/16 12:32:25 24.24 4120 2.18 201.3 16.66 6.88 -2.1 211.6 765.005/04/16 12:32:30 24.23 4118 2.18 200.9 16.63 6.88 -1.9 211.7 765.005/04/16 12:32:35 24.23 4116 2.18 200.5 16.60 6.88 -1.7 211.8 765.005/04/16 12:32:40 24.23 4116 2.18 200.2 16.58 6.87 -1.6 212.0 765.005/04/16 12:32:45 24.22 4115 2.18 199.9 16.55 6.87 -1.4 212.2 765.005/04/16 12:32:50 24.22 4115 2.18 199.6 16.53 6.87 -1.2 212.4 765.005/04/16 12:32:55 24.22 4115 2.18 199.4 16.51 6.86 -1.1 212.4 765.005/04/16 12:33:00 24.22 4115 2.18 199.2 16.49 6.86 -1.0 212.5 765.005/04/16 12:33:05 24.22 4115 2.18 199.0 16.48 6.86 -0.9 212.5 765.005/04/16 12:33:10 24.21 4116 2.18 198.9 16.48 6.86 -0.7 212.5 765.005/04/16 12:33:15 24.20 4117 2.18 198.8 16.46 6.86 -0.7 212.6 765.005/04/16 12:33:20 24.19 4118 2.18 198.6 16.46 6.85 -0.6 212.6 765.005/04/16 12:33:25 24.18 4118 2.18 198.5 16.45 6.85 -0.5 212.6 765.005/04/16 12:33:30 24.18 4118 2.18 198.4 16.44 6.85 -0.4 212.6 765.005/04/16 12:33:35 24.17 4118 2.18 198.3 16.44 6.85 -0.3 212.6 765.005/04/16 12:33:40 24.16 4118 2.18 198.2 16.43 6.85 -0.3 212.7 765.005/04/16 12:33:45 24.14 4116 2.18 198.2 16.43 6.85 -0.2 212.7 765.005/04/16 12:33:50 24.13 4114 2.18 198.1 16.43 6.85 -0.1 212.7 765.005/04/16 12:33:55 24.13 4112 2.18 197.8 16.41 6.84 -0.1 212.7 765.005/04/16 12:34:00 24.13 4110 2.18 197.6 16.39 6.84 0.0 212.7 765.005/04/16 12:34:05 24.13 4109 2.18 197.4 16.38 6.84 0.0 212.7 765.005/04/16 12:34:10 24.13 4107 2.18 197.3 16.36 6.84 0.1 212.7 765.005/04/16 12:34:15 24.12 4106 2.18 197.1 16.36 6.84 0.2 212.7 765.005/04/16 12:34:20 24.11 4104 2.17 197.1 16.35 6.84 0.2 212.7 765.005/04/16 12:34:25 24.10 4100 2.17 197.0 16.35 6.84 0.3 212.7 765.005/04/16 12:34:30 24.10 4096 2.17 196.9 16.34 6.84 0.3 212.8 765.005/04/16 12:34:35 24.10 4093 2.17 196.8 16.33 6.84 0.4 212.8 765.105/04/16 12:34:40 24.09 4092 2.17 196.6 16.32 6.83 0.5 212.9 765.005/04/16 12:34:45 24.09 4090 2.17 196.5 16.31 6.83 0.6 212.9 765.105/04/16 12:34:50 24.09 4089 2.17 196.4 16.30 6.83 0.6 212.9 765.105/04/16 12:34:55 24.08 4087 2.17 196.3 16.29 6.83 0.7 213.0 765.105/04/16 12:35:00 24.08 4083 2.16 196.1 16.28 6.83 0.8 213.0 765.105/04/16 12:35:05 24.07 4079 2.16 196.0 16.28 6.83 0.8 213.1 765.105/04/16 12:35:10 24.07 4076 2.16 195.9 16.27 6.83 0.8 213.1 765.105/04/16 12:35:15 24.06 4073 2.16 195.7 16.26 6.83 0.9 213.0 765.005/04/16 12:35:20 24.06 4071 2.16 195.6 16.25 6.83 0.9 212.9 765.005/04/16 12:35:25 24.05 4069 2.16 195.5 16.24 6.83 1.0 212.9 765.005/04/16 12:35:30 24.05 4067 2.15 195.4 16.24 6.82 1.0 212.9 765.005/04/16 12:35:35 24.04 4066 2.15 195.3 16.23 6.82 1.1 212.8 765.105/04/16 12:35:40 24.03 4066 2.15 195.3 16.23 6.82 1.1 212.8 765.0
Date Time M/D/Y HH:MM:SS Temp C SpCond uS Sal ppt DOsat % DO mg/L pH pH mV Orp mV Baro mmHgSW-02R
05/04/16 12:35:45 24.03 4065 2.15 195.1 16.22 6.82 1.1 212.7 765.005/04/16 12:35:50 24.02 4065 2.15 195.0 16.21 6.82 1.2 212.7 765.005/04/16 12:35:55 24.01 4065 2.15 195.0 16.21 6.82 1.2 212.7 765.105/04/16 12:36:00 23.99 4064 2.15 194.9 16.21 6.82 1.2 212.7 765.105/04/16 12:36:05 23.98 4062 2.15 194.9 16.21 6.82 1.3 212.7 765.005/04/16 12:36:10 23.98 4059 2.15 194.8 16.20 6.82 1.3 212.6 765.005/04/16 12:36:15 23.98 4055 2.15 194.6 16.19 6.82 1.3 212.6 765.005/04/16 12:36:20 23.98 4048 2.14 194.4 16.18 6.82 1.3 212.6 765.005/04/16 12:36:25 23.98 4042 2.14 194.3 16.16 6.82 1.4 212.6 765.005/04/16 12:36:30 23.98 4037 2.14 194.1 16.15 6.82 1.4 212.5 765.005/04/16 12:36:35 23.98 4031 2.13 194.0 16.14 6.82 1.4 212.5 765.005/04/16 12:36:40 23.97 4027 2.13 193.8 16.13 6.82 1.5 212.5 765.005/04/16 12:36:45 23.97 4024 2.13 193.7 16.12 6.81 1.5 212.4 765.005/04/16 12:36:50 23.97 4021 2.13 193.5 16.10 6.81 1.6 212.4 765.005/04/16 12:36:55 23.97 4020 2.13 193.3 16.08 6.81 1.6 212.4 765.005/04/16 12:37:00 23.98 4019 2.13 193.1 16.07 6.81 1.7 212.5 765.005/04/16 12:37:05 23.98 4019 2.13 193.0 16.06 6.81 1.7 212.4 765.005/04/16 12:37:10 23.98 4018 2.13 192.8 16.04 6.81 1.7 212.4 765.005/04/16 12:37:15 23.98 4018 2.13 192.6 16.02 6.81 1.8 212.4 765.0
Date Time M/D/Y HH:MM:SS Temp C SpCond uS Sal ppt DOsat % DO mg/L pH pH mV Orp mV Baro mmHg05/04/16 13:24:14 31.82 65 0.03 182.6 13.38 7.12 -15.2 211.1 765.505/04/16 13:24:19 30.56 3524 1.83 182.5 13.53 7.10 -14.2 205.1 765.505/04/16 13:24:24 30.52 3614 1.88 180.8 13.41 7.10 -14.0 205.0 765.505/04/16 13:24:29 30.47 3658 1.91 179.6 13.32 7.09 -13.7 205.0 765.405/04/16 13:24:34 30.40 3677 1.92 179.4 13.32 7.09 -13.3 204.9 765.405/04/16 13:24:39 30.28 3686 1.92 180.0 13.40 7.08 -12.9 204.9 765.405/04/16 13:24:44 30.20 3687 1.92 180.6 13.46 7.07 -12.6 204.9 765.405/04/16 13:24:49 30.12 3682 1.92 181.2 13.53 7.07 -12.1 204.8 765.405/04/16 13:24:54 29.99 3675 1.92 182.4 13.65 7.06 -11.6 204.7 765.405/04/16 13:24:59 29.81 3663 1.91 184.0 13.81 7.05 -11.0 204.7 765.405/04/16 13:25:04 29.62 3652 1.91 185.5 13.97 7.04 -10.5 204.6 765.405/04/16 13:25:09 29.49 3644 1.90 186.7 14.09 7.03 -10.0 204.6 765.405/04/16 13:25:14 29.28 3639 1.90 188.4 14.27 7.02 -9.5 204.6 765.405/04/16 13:25:19 29.02 3639 1.90 190.6 14.51 7.01 -9.0 204.6 765.305/04/16 13:25:24 28.78 3640 1.90 192.7 14.72 7.00 -8.6 204.6 765.305/04/16 13:25:29 28.63 3635 1.90 193.9 14.85 6.99 -8.1 204.5 765.305/04/16 13:25:34 28.54 3628 1.90 194.7 14.94 6.99 -7.7 204.5 765.305/04/16 13:25:39 28.46 3623 1.89 195.4 15.02 6.98 -7.4 204.6 765.305/04/16 13:25:44 28.19 3625 1.90 197.8 15.27 6.97 -7.1 204.6 765.205/04/16 13:25:49 27.96 3626 1.90 200.0 15.50 6.97 -6.8 204.6 765.205/04/16 13:25:54 27.84 3621 1.89 196.0 15.23 6.96 -6.4 204.7 765.205/04/16 13:25:59 27.75 3617 1.89 173.5 13.50 6.96 -6.1 204.6 765.305/04/16 13:26:04 27.69 3615 1.89 147.3 11.47 6.95 -5.9 204.7 765.305/04/16 13:26:09 27.56 3615 1.89 128.9 10.06 6.95 -5.7 204.7 765.305/04/16 13:26:14 27.37 3614 1.89 120.4 9.43 6.95 -5.5 204.8 765.305/04/16 13:26:19 27.25 3602 1.89 116.2 9.12 6.94 -5.4 204.8 765.205/04/16 13:26:24 27.18 3597 1.88 116.3 9.14 6.94 -5.2 204.9 765.305/04/16 13:26:29 27.10 3593 1.88 118.8 9.35 6.94 -5.0 204.8 765.205/04/16 13:26:34 26.99 3585 1.88 117.9 9.30 6.93 -4.9 204.8 765.305/04/16 13:26:39 26.93 3579 1.87 112.4 8.87 6.93 -4.6 204.8 765.305/04/16 13:26:44 26.93 3575 1.87 106.9 8.44 6.93 -4.4 204.7 765.305/04/16 13:26:49 26.92 3573 1.87 99.4 7.85 6.92 -4.3 204.7 765.305/04/16 13:26:54 26.86 3567 1.87 93.4 7.38 6.92 -4.3 204.7 765.305/04/16 13:26:59 26.79 3557 1.86 89.0 7.05 6.92 -4.3 204.7 765.305/04/16 13:27:04 26.75 3553 1.86 85.6 6.78 6.92 -4.3 204.7 765.305/04/16 13:27:09 26.72 3550 1.86 83.8 6.64 6.92 -4.2 204.6 765.305/04/16 13:27:14 26.69 3539 1.85 83.9 6.66 6.92 -4.1 204.6 765.305/04/16 13:27:19 26.66 3538 1.85 84.7 6.72 6.92 -4.0 204.7 765.305/04/16 13:27:24 26.64 3537 1.85 85.8 6.81 6.91 -3.8 204.6 765.3
SW-03R
Date Time M/D/Y HH:MM:SS Temp C SpCond uS Sal ppt DOsat % DO mg/L pH pH mV Orp mV Baro mmHg
SW-03R
05/04/16 13:27:29 26.62 3536 1.85 87.2 6.93 6.91 -3.7 204.6 765.305/04/16 13:27:34 26.59 3533 1.85 88.4 7.02 6.91 -3.7 204.6 765.305/04/16 13:27:39 26.55 3528 1.85 90.5 7.20 6.91 -3.6 204.5 765.305/04/16 13:27:44 26.52 3523 1.84 93.6 7.44 6.91 -3.5 204.4 765.305/04/16 13:27:49 26.51 3519 1.84 95.6 7.61 6.91 -3.4 204.5 765.305/04/16 13:27:54 26.48 3514 1.84 96.5 7.68 6.90 -3.3 204.5 765.305/04/16 13:27:59 26.47 3508 1.84 97.8 7.79 6.90 -3.1 204.6 765.305/04/16 13:28:04 26.47 3505 1.83 99.4 7.92 6.90 -2.9 204.6 765.305/04/16 13:28:09 26.44 3499 1.83 100.5 8.00 6.90 -2.9 204.5 765.305/04/16 13:28:14 26.41 3495 1.83 100.7 8.03 6.90 -2.8 204.5 765.305/04/16 13:28:19 26.40 3493 1.83 100.7 8.03 6.89 -2.7 204.4 765.305/04/16 13:28:24 26.37 3492 1.83 102.2 8.16 6.89 -2.6 204.4 765.305/04/16 13:28:29 26.36 3488 1.82 104.1 8.31 6.89 -2.4 204.2 765.305/04/16 13:28:34 26.34 3485 1.82 106.0 8.46 6.89 -2.3 204.1 765.305/04/16 13:28:39 26.32 3483 1.82 107.7 8.60 6.88 -2.2 204.1 765.305/04/16 13:28:44 26.30 3476 1.82 109.5 8.75 6.88 -2.1 204.0 765.305/04/16 13:28:49 26.29 3473 1.82 111.0 8.87 6.88 -2.0 204.1 765.305/04/16 13:28:54 26.27 3465 1.81 111.9 8.94 6.88 -2.0 204.1 765.305/04/16 13:28:59 26.24 3466 1.81 112.5 9.00 6.88 -1.9 204.1 765.305/04/16 13:29:04 26.22 3462 1.81 114.8 9.18 6.88 -1.8 204.0 765.305/04/16 13:29:09 26.19 3458 1.81 117.6 9.42 6.88 -1.8 204.0 765.305/04/16 13:29:14 26.16 3454 1.81 120.7 9.66 6.88 -1.7 203.9 765.305/04/16 13:29:19 26.15 3450 1.80 122.6 9.82 6.87 -1.6 203.8 765.305/04/16 13:29:24 26.14 3450 1.80 125.1 10.03 6.87 -1.4 203.9 765.405/04/16 13:29:29 26.13 3449 1.80 129.8 10.40 6.87 -1.3 204.0 765.305/04/16 13:29:34 26.11 3445 1.80 135.2 10.83 6.87 -1.2 204.0 765.405/04/16 13:29:39 26.10 3445 1.80 140.7 11.28 6.86 -1.1 204.0 765.405/04/16 13:29:44 26.10 3445 1.80 144.8 11.61 6.86 -1.0 204.0 765.405/04/16 13:29:49 26.10 3442 1.80 147.6 11.84 6.86 -0.9 203.9 765.405/04/16 13:29:54 26.09 3443 1.80 149.7 12.01 6.86 -0.9 203.9 765.405/04/16 13:29:59 26.08 3442 1.80 151.3 12.13 6.86 -0.8 203.8 765.405/04/16 13:30:04 26.08 3440 1.80 152.6 12.24 6.86 -0.8 203.7 765.405/04/16 13:30:09 26.07 3436 1.80 153.7 12.33 6.86 -0.7 203.7 765.405/04/16 13:30:14 26.06 3432 1.79 154.5 12.40 6.86 -0.7 203.7 765.405/04/16 13:30:19 26.07 3428 1.79 155.1 12.44 6.86 -0.6 203.7 765.405/04/16 13:30:24 26.07 3424 1.79 155.7 12.49 6.85 -0.5 203.7 765.505/04/16 13:30:29 26.07 3420 1.79 156.2 12.53 6.85 -0.5 203.6 765.505/04/16 13:30:34 26.06 3413 1.78 156.7 12.57 6.85 -0.4 203.6 765.505/04/16 13:30:39 26.06 3409 1.78 157.1 12.61 6.85 -0.4 203.6 765.5
Date Time M/D/Y HH:MM:SS Temp C SpCond uS Sal ppt DOsat % DO mg/L pH pH mV Orp mV Baro mmHg
SW-03R
05/04/16 13:30:44 26.07 3396 1.77 157.5 12.64 6.85 -0.4 203.5 765.505/04/16 13:30:49 26.07 3387 1.77 157.9 12.67 6.85 -0.3 203.4 765.505/04/16 13:30:54 26.08 3378 1.76 158.2 12.69 6.85 -0.3 203.4 765.505/04/16 13:30:59 26.09 3371 1.76 158.3 12.70 6.85 -0.2 203.3 765.505/04/16 13:31:04 26.10 3366 1.76 158.4 12.71 6.85 -0.2 203.3 765.505/04/16 13:31:09 26.11 3361 1.75 155.9 12.50 6.85 -0.3 203.1 765.505/04/16 13:31:14 26.12 3357 1.75 141.5 11.35 6.85 -0.4 203.1 765.5
ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Savannah5102 LaRoche AvenueSavannah, GA 31404Tel: (912)354-7858
TestAmerica Job ID: 680-124858-1Client Project/Site: Colonial Terminals/0730114
For:Ramboll Environ US Corporation1600 Parkwood Circle, Suite 310Atlanta, Georgia 30339
Attn: Mr. Ryan Slakman
Authorized for release by:5/13/2016 11:25:00 AM
Michele Kersey, Project Manager I(912)[email protected]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accreditedparameters, exceptions are noted in this report. This report may not be reproduced except in full,and with written approval from the laboratory. For questions please contact the Project Managerat the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Case NarrativeClient: Ramboll Environ US Corporation TestAmerica Job ID: 680-124858-1Project/Site: Colonial Terminals/0730114
Job ID: 680-124858-1
Laboratory: TestAmerica Savannah
Narrative
CASE NARRATIVE
Client: Ramboll Environ US Corporation
Project: Colonial Terminals/0730114
Report Number: 680-124858-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.
RECEIPTThe samples were received on 5/4/2016 3:47 PM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 4.4º C.
VOLATILE ORGANIC COMPOUNDS (GC-MS)Samples SW-01R 20160504 (680-124858-1), SW-02R 20160504 (680-124858-2), SW-03R 20160504 (680-124858-3), DUP-01 20160504 (680-124858-4) and TRIP BLANK 20160504 (680-124858-5) were analyzed for Volatile Organic Compounds (GC-MS) in
accordance with EPA SW-846 Method 8260B. The samples were analyzed on 05/09/2016 and 05/12/2016.
Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with analytical batch 680-432371.
Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with analytical batch 680-432921.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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Sample SummaryTestAmerica Job ID: 680-124858-1Client: Ramboll Environ US Corporation
Project/Site: Colonial Terminals/0730114
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
680-124858-1 SW-01R 20160504 Water 05/04/16 13:10 05/04/16 15:47
680-124858-2 SW-02R 20160504 Water 05/04/16 13:42 05/04/16 15:47
680-124858-3 SW-03R 20160504 Water 05/04/16 14:40 05/04/16 15:47
680-124858-4 DUP-01 20160504 Water 05/04/16 00:00 05/04/16 15:47
680-124858-5 TRIP BLANK 20160504 Water 05/04/16 00:00 05/04/16 15:47
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Method SummaryTestAmerica Job ID: 680-124858-1Client: Ramboll Environ US Corporation
Project/Site: Colonial Terminals/0730114
Method Method Description LaboratoryProtocol
SW8468260B Volatile Organic Compounds (GC/MS) TAL SAV
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858
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Client Sample ResultsTestAmerica Job ID: 680-124858-1Client: Ramboll Environ US Corporation
Project/Site: Colonial Terminals/0730114
Lab Sample ID: 680-124858-1Client Sample ID: SW-01R 20160504Matrix: WaterDate Collected: 05/04/16 13:10
Date Received: 05/04/16 15:47
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone 11 10 ug/L 05/09/16 17:53 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 ug/L 05/09/16 17:53 1Benzene <1.0
1.0 ug/L 05/09/16 17:53 1Bromochloromethane <1.0
1.0 ug/L 05/09/16 17:53 1Bromodichloromethane <1.0
1.0 ug/L 05/09/16 17:53 1Bromoform <1.0
5.0 ug/L 05/09/16 17:53 1Bromomethane <5.0
10 ug/L 05/09/16 17:53 12-Butanone <10
2.0 ug/L 05/09/16 17:53 1Carbon disulfide <2.0
1.0 ug/L 05/09/16 17:53 1Carbon tetrachloride <1.0
1.0 ug/L 05/09/16 17:53 1Chlorobenzene <1.0
5.0 ug/L 05/09/16 17:53 1Chloroethane <5.0
1.0 ug/L 05/09/16 17:53 1Chloroform <1.0
1.0 ug/L 05/09/16 17:53 1Chloromethane <1.0
1.0 ug/L 05/09/16 17:53 1cis-1,2-Dichloroethene <1.0
1.0 ug/L 05/09/16 17:53 1cis-1,3-Dichloropropene <1.0
1.0 ug/L 05/09/16 17:53 1Cyclohexane <1.0
1.0 ug/L 05/09/16 17:53 1Dibromochloromethane <1.0
5.0 ug/L 05/09/16 17:53 11,2-Dibromo-3-Chloropropane <5.0
1.0 ug/L 05/09/16 17:53 11,2-Dibromoethane <1.0
1.0 ug/L 05/09/16 17:53 11,2-Dichlorobenzene <1.0
1.0 ug/L 05/09/16 17:53 11,3-Dichlorobenzene <1.0
1.0 ug/L 05/09/16 17:53 11,4-Dichlorobenzene <1.0
1.0 ug/L 05/09/16 17:53 1Dichlorodifluoromethane <1.0
1.0 ug/L 05/09/16 17:53 11,1-Dichloroethane <1.0
1.0 ug/L 05/09/16 17:53 11,2-Dichloroethane <1.0
1.0 ug/L 05/09/16 17:53 11,1-Dichloroethene <1.0
1.0 ug/L 05/09/16 17:53 11,2-Dichloropropane <1.0
100 ug/L 05/09/16 17:53 11,4-Dioxane <100
1.0 ug/L 05/09/16 17:53 1Ethylbenzene <1.0
10 ug/L 05/09/16 17:53 12-Hexanone <10
1.0 ug/L 05/09/16 17:53 1Isopropylbenzene <1.0
5.0 ug/L 05/09/16 17:53 1Methyl acetate <5.0
1.0 ug/L 05/09/16 17:53 1Methylcyclohexane <1.0
5.0 ug/L 05/09/16 17:53 1Methylene Chloride <5.0
10 ug/L 05/09/16 17:53 14-Methyl-2-pentanone <10
10 ug/L 05/09/16 17:53 1Methyl tert-butyl ether <10
1.0 ug/L 05/09/16 17:53 1m-Xylene & p-Xylene <1.0
1.0 ug/L 05/09/16 17:53 1o-Xylene <1.0
1.0 ug/L 05/09/16 17:53 1Styrene <1.0
1.0 ug/L 05/09/16 17:53 11,1,2,2-Tetrachloroethane <1.0
1.0 ug/L 05/09/16 17:53 1Tetrachloroethene <1.0
1.0 ug/L 05/09/16 17:53 1Toluene <1.0
1.0 ug/L 05/09/16 17:53 1trans-1,2-Dichloroethene <1.0
1.0 ug/L 05/09/16 17:53 1trans-1,3-Dichloropropene <1.0
5.0 ug/L 05/09/16 17:53 11,2,3-Trichlorobenzene <5.0
5.0 ug/L 05/09/16 17:53 11,2,4-Trichlorobenzene <5.0
1.0 ug/L 05/09/16 17:53 11,1,1-Trichloroethane <1.0
1.0 ug/L 05/09/16 17:53 11,1,2-Trichloroethane <1.0
1.0 ug/L 05/09/16 17:53 1Trichloroethene <1.0
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Client Sample ResultsTestAmerica Job ID: 680-124858-1Client: Ramboll Environ US Corporation
Project/Site: Colonial Terminals/0730114
Lab Sample ID: 680-124858-1Client Sample ID: SW-01R 20160504Matrix: WaterDate Collected: 05/04/16 13:10
Date Received: 05/04/16 15:47
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)RL MDL
Trichlorofluoromethane <1.0 1.0 ug/L 05/09/16 17:53 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 ug/L 05/09/16 17:53 11,1,2-Trichloro-1,2,2-trifluoroethane <1.0
1.0 ug/L 05/09/16 17:53 1Vinyl chloride <1.0
Toluene-d8 (Surr) 95 70 - 130 05/09/16 17:53 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr) 99 05/09/16 17:53 170 - 130
Dibromofluoromethane (Surr) 103 05/09/16 17:53 170 - 130
4-Bromofluorobenzene (Surr) 98 05/09/16 17:53 170 - 130
Lab Sample ID: 680-124858-2Client Sample ID: SW-02R 20160504Matrix: WaterDate Collected: 05/04/16 13:42
Date Received: 05/04/16 15:47
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone <10 10 ug/L 05/09/16 18:14 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 ug/L 05/09/16 18:14 1Benzene <1.0
1.0 ug/L 05/09/16 18:14 1Bromochloromethane <1.0
1.0 ug/L 05/09/16 18:14 1Bromodichloromethane <1.0
1.0 ug/L 05/09/16 18:14 1Bromoform <1.0
5.0 ug/L 05/09/16 18:14 1Bromomethane <5.0
10 ug/L 05/09/16 18:14 12-Butanone <10
2.0 ug/L 05/09/16 18:14 1Carbon disulfide <2.0
1.0 ug/L 05/09/16 18:14 1Carbon tetrachloride <1.0
1.0 ug/L 05/09/16 18:14 1Chlorobenzene <1.0
5.0 ug/L 05/09/16 18:14 1Chloroethane <5.0
1.0 ug/L 05/09/16 18:14 1Chloroform <1.0
1.0 ug/L 05/09/16 18:14 1Chloromethane <1.0
1.0 ug/L 05/09/16 18:14 1cis-1,2-Dichloroethene <1.0
1.0 ug/L 05/09/16 18:14 1cis-1,3-Dichloropropene <1.0
1.0 ug/L 05/09/16 18:14 1Cyclohexane <1.0
1.0 ug/L 05/09/16 18:14 1Dibromochloromethane <1.0
5.0 ug/L 05/09/16 18:14 11,2-Dibromo-3-Chloropropane <5.0
1.0 ug/L 05/09/16 18:14 11,2-Dibromoethane <1.0
1.0 ug/L 05/09/16 18:14 11,2-Dichlorobenzene <1.0
1.0 ug/L 05/09/16 18:14 11,3-Dichlorobenzene <1.0
1.0 ug/L 05/09/16 18:14 11,4-Dichlorobenzene <1.0
1.0 ug/L 05/09/16 18:14 1Dichlorodifluoromethane <1.0
1.0 ug/L 05/09/16 18:14 11,1-Dichloroethane <1.0
1.0 ug/L 05/09/16 18:14 11,2-Dichloroethane <1.0
1.0 ug/L 05/09/16 18:14 11,1-Dichloroethene <1.0
1.0 ug/L 05/09/16 18:14 11,2-Dichloropropane <1.0
100 ug/L 05/09/16 18:14 11,4-Dioxane <100
1.0 ug/L 05/09/16 18:14 1Ethylbenzene <1.0
10 ug/L 05/09/16 18:14 12-Hexanone <10
1.0 ug/L 05/09/16 18:14 1Isopropylbenzene <1.0
5.0 ug/L 05/09/16 18:14 1Methyl acetate <5.0
1.0 ug/L 05/09/16 18:14 1Methylcyclohexane <1.0
5.0 ug/L 05/09/16 18:14 1Methylene Chloride <5.0
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Client Sample ResultsTestAmerica Job ID: 680-124858-1Client: Ramboll Environ US Corporation
Project/Site: Colonial Terminals/0730114
Lab Sample ID: 680-124858-2Client Sample ID: SW-02R 20160504Matrix: WaterDate Collected: 05/04/16 13:42
Date Received: 05/04/16 15:47
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)RL MDL
4-Methyl-2-pentanone <10 10 ug/L 05/09/16 18:14 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10 ug/L 05/09/16 18:14 1Methyl tert-butyl ether <10
1.0 ug/L 05/09/16 18:14 1m-Xylene & p-Xylene <1.0
1.0 ug/L 05/09/16 18:14 1o-Xylene <1.0
1.0 ug/L 05/09/16 18:14 1Styrene <1.0
1.0 ug/L 05/09/16 18:14 11,1,2,2-Tetrachloroethane <1.0
1.0 ug/L 05/09/16 18:14 1Tetrachloroethene <1.0
1.0 ug/L 05/09/16 18:14 1Toluene <1.0
1.0 ug/L 05/09/16 18:14 1trans-1,2-Dichloroethene <1.0
1.0 ug/L 05/09/16 18:14 1trans-1,3-Dichloropropene <1.0
5.0 ug/L 05/09/16 18:14 11,2,3-Trichlorobenzene <5.0
5.0 ug/L 05/09/16 18:14 11,2,4-Trichlorobenzene <5.0
1.0 ug/L 05/09/16 18:14 11,1,1-Trichloroethane <1.0
1.0 ug/L 05/09/16 18:14 11,1,2-Trichloroethane <1.0
1.0 ug/L 05/09/16 18:14 1Trichloroethene <1.0
1.0 ug/L 05/09/16 18:14 1Trichlorofluoromethane <1.0
1.0 ug/L 05/09/16 18:14 11,1,2-Trichloro-1,2,2-trifluoroethane <1.0
1.0 ug/L 05/09/16 18:14 1Vinyl chloride <1.0
Toluene-d8 (Surr) 96 70 - 130 05/09/16 18:14 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr) 98 05/09/16 18:14 170 - 130
Dibromofluoromethane (Surr) 107 05/09/16 18:14 170 - 130
4-Bromofluorobenzene (Surr) 98 05/09/16 18:14 170 - 130
Lab Sample ID: 680-124858-3Client Sample ID: SW-03R 20160504Matrix: WaterDate Collected: 05/04/16 14:40
Date Received: 05/04/16 15:47
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone <10 10 ug/L 05/09/16 18:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 ug/L 05/09/16 18:34 1Benzene <1.0
1.0 ug/L 05/09/16 18:34 1Bromochloromethane <1.0
1.0 ug/L 05/09/16 18:34 1Bromodichloromethane <1.0
1.0 ug/L 05/09/16 18:34 1Bromoform <1.0
5.0 ug/L 05/09/16 18:34 1Bromomethane <5.0
10 ug/L 05/09/16 18:34 12-Butanone <10
2.0 ug/L 05/09/16 18:34 1Carbon disulfide <2.0
1.0 ug/L 05/09/16 18:34 1Carbon tetrachloride <1.0
1.0 ug/L 05/09/16 18:34 1Chlorobenzene <1.0
5.0 ug/L 05/09/16 18:34 1Chloroethane <5.0
1.0 ug/L 05/09/16 18:34 1Chloroform <1.0
1.0 ug/L 05/09/16 18:34 1Chloromethane <1.0
1.0 ug/L 05/09/16 18:34 1cis-1,2-Dichloroethene <1.0
1.0 ug/L 05/09/16 18:34 1cis-1,3-Dichloropropene <1.0
1.0 ug/L 05/09/16 18:34 1Cyclohexane <1.0
1.0 ug/L 05/09/16 18:34 1Dibromochloromethane <1.0
5.0 ug/L 05/09/16 18:34 11,2-Dibromo-3-Chloropropane <5.0
1.0 ug/L 05/09/16 18:34 11,2-Dibromoethane <1.0
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Client Sample ResultsTestAmerica Job ID: 680-124858-1Client: Ramboll Environ US Corporation
Project/Site: Colonial Terminals/0730114
Lab Sample ID: 680-124858-3Client Sample ID: SW-03R 20160504Matrix: WaterDate Collected: 05/04/16 14:40
Date Received: 05/04/16 15:47
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)RL MDL
1,2-Dichlorobenzene <1.0 1.0 ug/L 05/09/16 18:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 ug/L 05/09/16 18:34 11,3-Dichlorobenzene <1.0
1.0 ug/L 05/09/16 18:34 11,4-Dichlorobenzene <1.0
1.0 ug/L 05/09/16 18:34 1Dichlorodifluoromethane <1.0
1.0 ug/L 05/09/16 18:34 11,1-Dichloroethane <1.0
1.0 ug/L 05/09/16 18:34 11,2-Dichloroethane <1.0
1.0 ug/L 05/09/16 18:34 11,1-Dichloroethene <1.0
1.0 ug/L 05/09/16 18:34 11,2-Dichloropropane <1.0
100 ug/L 05/09/16 18:34 11,4-Dioxane <100
1.0 ug/L 05/09/16 18:34 1Ethylbenzene <1.0
10 ug/L 05/09/16 18:34 12-Hexanone <10
1.0 ug/L 05/09/16 18:34 1Isopropylbenzene <1.0
5.0 ug/L 05/09/16 18:34 1Methyl acetate <5.0
1.0 ug/L 05/09/16 18:34 1Methylcyclohexane <1.0
5.0 ug/L 05/09/16 18:34 1Methylene Chloride <5.0
10 ug/L 05/09/16 18:34 14-Methyl-2-pentanone <10
10 ug/L 05/09/16 18:34 1Methyl tert-butyl ether <10
1.0 ug/L 05/09/16 18:34 1m-Xylene & p-Xylene <1.0
1.0 ug/L 05/09/16 18:34 1o-Xylene <1.0
1.0 ug/L 05/09/16 18:34 1Styrene <1.0
1.0 ug/L 05/09/16 18:34 11,1,2,2-Tetrachloroethane <1.0
1.0 ug/L 05/09/16 18:34 1Tetrachloroethene <1.0
1.0 ug/L 05/09/16 18:34 1Toluene <1.0
1.0 ug/L 05/09/16 18:34 1trans-1,2-Dichloroethene <1.0
1.0 ug/L 05/09/16 18:34 1trans-1,3-Dichloropropene <1.0
5.0 ug/L 05/09/16 18:34 11,2,3-Trichlorobenzene <5.0
5.0 ug/L 05/09/16 18:34 11,2,4-Trichlorobenzene <5.0
1.0 ug/L 05/09/16 18:34 11,1,1-Trichloroethane <1.0
1.0 ug/L 05/09/16 18:34 11,1,2-Trichloroethane <1.0
1.0 ug/L 05/09/16 18:34 1Trichloroethene <1.0
1.0 ug/L 05/09/16 18:34 1Trichlorofluoromethane <1.0
1.0 ug/L 05/09/16 18:34 11,1,2-Trichloro-1,2,2-trifluoroethane <1.0
1.0 ug/L 05/09/16 18:34 1Vinyl chloride <1.0
Toluene-d8 (Surr) 95 70 - 130 05/09/16 18:34 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr) 99 05/09/16 18:34 170 - 130
Dibromofluoromethane (Surr) 107 05/09/16 18:34 170 - 130
4-Bromofluorobenzene (Surr) 98 05/09/16 18:34 170 - 130
Lab Sample ID: 680-124858-4Client Sample ID: DUP-01 20160504Matrix: WaterDate Collected: 05/04/16 00:00
Date Received: 05/04/16 15:47
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone <10 10 ug/L 05/09/16 18:54 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 ug/L 05/09/16 18:54 1Benzene <1.0
1.0 ug/L 05/09/16 18:54 1Bromochloromethane <1.0
1.0 ug/L 05/09/16 18:54 1Bromodichloromethane <1.0
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Client Sample ResultsTestAmerica Job ID: 680-124858-1Client: Ramboll Environ US Corporation
Project/Site: Colonial Terminals/0730114
Lab Sample ID: 680-124858-4Client Sample ID: DUP-01 20160504Matrix: WaterDate Collected: 05/04/16 00:00
Date Received: 05/04/16 15:47
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)RL MDL
Bromoform <1.0 1.0 ug/L 05/09/16 18:54 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
5.0 ug/L 05/09/16 18:54 1Bromomethane <5.0
10 ug/L 05/09/16 18:54 12-Butanone <10
2.0 ug/L 05/09/16 18:54 1Carbon disulfide <2.0
1.0 ug/L 05/09/16 18:54 1Carbon tetrachloride <1.0
1.0 ug/L 05/09/16 18:54 1Chlorobenzene <1.0
5.0 ug/L 05/09/16 18:54 1Chloroethane <5.0
1.0 ug/L 05/09/16 18:54 1Chloroform <1.0
1.0 ug/L 05/09/16 18:54 1Chloromethane <1.0
1.0 ug/L 05/09/16 18:54 1cis-1,2-Dichloroethene <1.0
1.0 ug/L 05/09/16 18:54 1cis-1,3-Dichloropropene <1.0
1.0 ug/L 05/09/16 18:54 1Cyclohexane <1.0
1.0 ug/L 05/09/16 18:54 1Dibromochloromethane <1.0
5.0 ug/L 05/09/16 18:54 11,2-Dibromo-3-Chloropropane <5.0
1.0 ug/L 05/09/16 18:54 11,2-Dibromoethane <1.0
1.0 ug/L 05/09/16 18:54 11,2-Dichlorobenzene <1.0
1.0 ug/L 05/09/16 18:54 11,3-Dichlorobenzene <1.0
1.0 ug/L 05/09/16 18:54 11,4-Dichlorobenzene <1.0
1.0 ug/L 05/09/16 18:54 1Dichlorodifluoromethane <1.0
1.0 ug/L 05/09/16 18:54 11,1-Dichloroethane <1.0
1.0 ug/L 05/09/16 18:54 11,2-Dichloroethane <1.0
1.0 ug/L 05/09/16 18:54 11,1-Dichloroethene <1.0
1.0 ug/L 05/09/16 18:54 11,2-Dichloropropane <1.0
100 ug/L 05/09/16 18:54 11,4-Dioxane <100
1.0 ug/L 05/09/16 18:54 1Ethylbenzene <1.0
10 ug/L 05/09/16 18:54 12-Hexanone <10
1.0 ug/L 05/09/16 18:54 1Isopropylbenzene <1.0
5.0 ug/L 05/09/16 18:54 1Methyl acetate <5.0
1.0 ug/L 05/09/16 18:54 1Methylcyclohexane <1.0
5.0 ug/L 05/09/16 18:54 1Methylene Chloride <5.0
10 ug/L 05/09/16 18:54 14-Methyl-2-pentanone <10
10 ug/L 05/09/16 18:54 1Methyl tert-butyl ether <10
1.0 ug/L 05/09/16 18:54 1m-Xylene & p-Xylene <1.0
1.0 ug/L 05/09/16 18:54 1o-Xylene <1.0
1.0 ug/L 05/09/16 18:54 1Styrene <1.0
1.0 ug/L 05/09/16 18:54 11,1,2,2-Tetrachloroethane <1.0
1.0 ug/L 05/09/16 18:54 1Tetrachloroethene <1.0
1.0 ug/L 05/09/16 18:54 1Toluene <1.0
1.0 ug/L 05/09/16 18:54 1trans-1,2-Dichloroethene <1.0
1.0 ug/L 05/09/16 18:54 1trans-1,3-Dichloropropene <1.0
5.0 ug/L 05/09/16 18:54 11,2,3-Trichlorobenzene <5.0
5.0 ug/L 05/09/16 18:54 11,2,4-Trichlorobenzene <5.0
1.0 ug/L 05/09/16 18:54 11,1,1-Trichloroethane <1.0
1.0 ug/L 05/09/16 18:54 11,1,2-Trichloroethane <1.0
1.0 ug/L 05/09/16 18:54 1Trichloroethene <1.0
1.0 ug/L 05/09/16 18:54 1Trichlorofluoromethane <1.0
1.0 ug/L 05/09/16 18:54 11,1,2-Trichloro-1,2,2-trifluoroethane <1.0
1.0 ug/L 05/09/16 18:54 1Vinyl chloride <1.0
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Client Sample ResultsTestAmerica Job ID: 680-124858-1Client: Ramboll Environ US Corporation
Project/Site: Colonial Terminals/0730114
Lab Sample ID: 680-124858-4Client Sample ID: DUP-01 20160504Matrix: WaterDate Collected: 05/04/16 00:00
Date Received: 05/04/16 15:47
Toluene-d8 (Surr) 94 70 - 130 05/09/16 18:54 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr) 99 05/09/16 18:54 170 - 130
Dibromofluoromethane (Surr) 109 05/09/16 18:54 170 - 130
4-Bromofluorobenzene (Surr) 96 05/09/16 18:54 170 - 130
Lab Sample ID: 680-124858-5Client Sample ID: TRIP BLANK 20160504Matrix: WaterDate Collected: 05/04/16 00:00
Date Received: 05/04/16 15:47
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone <10 10 ug/L 05/12/16 16:15 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 ug/L 05/12/16 16:15 1Benzene <1.0
1.0 ug/L 05/12/16 16:15 1Bromochloromethane <1.0
1.0 ug/L 05/12/16 16:15 1Bromodichloromethane <1.0
1.0 ug/L 05/12/16 16:15 1Bromoform <1.0
5.0 ug/L 05/12/16 16:15 1Bromomethane <5.0
10 ug/L 05/12/16 16:15 12-Butanone <10
2.0 ug/L 05/12/16 16:15 1Carbon disulfide <2.0
1.0 ug/L 05/12/16 16:15 1Carbon tetrachloride <1.0
1.0 ug/L 05/12/16 16:15 1Chlorobenzene <1.0
5.0 ug/L 05/12/16 16:15 1Chloroethane <5.0
1.0 ug/L 05/12/16 16:15 1Chloroform <1.0
1.0 ug/L 05/12/16 16:15 1Chloromethane <1.0
1.0 ug/L 05/12/16 16:15 1cis-1,2-Dichloroethene <1.0
1.0 ug/L 05/12/16 16:15 1cis-1,3-Dichloropropene <1.0
1.0 ug/L 05/12/16 16:15 1Cyclohexane <1.0
1.0 ug/L 05/12/16 16:15 1Dibromochloromethane <1.0
5.0 ug/L 05/12/16 16:15 11,2-Dibromo-3-Chloropropane <5.0
1.0 ug/L 05/12/16 16:15 11,2-Dibromoethane <1.0
1.0 ug/L 05/12/16 16:15 11,2-Dichlorobenzene <1.0
1.0 ug/L 05/12/16 16:15 11,3-Dichlorobenzene <1.0
1.0 ug/L 05/12/16 16:15 11,4-Dichlorobenzene <1.0
1.0 ug/L 05/12/16 16:15 1Dichlorodifluoromethane <1.0
1.0 ug/L 05/12/16 16:15 11,1-Dichloroethane <1.0
1.0 ug/L 05/12/16 16:15 11,2-Dichloroethane <1.0
1.0 ug/L 05/12/16 16:15 11,1-Dichloroethene <1.0
1.0 ug/L 05/12/16 16:15 11,2-Dichloropropane <1.0
100 ug/L 05/12/16 16:15 11,4-Dioxane <100
1.0 ug/L 05/12/16 16:15 1Ethylbenzene <1.0
10 ug/L 05/12/16 16:15 12-Hexanone <10
1.0 ug/L 05/12/16 16:15 1Isopropylbenzene <1.0
5.0 ug/L 05/12/16 16:15 1Methyl acetate <5.0
1.0 ug/L 05/12/16 16:15 1Methylcyclohexane <1.0
5.0 ug/L 05/12/16 16:15 1Methylene Chloride <5.0
10 ug/L 05/12/16 16:15 14-Methyl-2-pentanone <10
10 ug/L 05/12/16 16:15 1Methyl tert-butyl ether <10
1.0 ug/L 05/12/16 16:15 1m-Xylene & p-Xylene <1.0
1.0 ug/L 05/12/16 16:15 1o-Xylene <1.0
1.0 ug/L 05/12/16 16:15 1Styrene <1.0
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Client Sample ResultsTestAmerica Job ID: 680-124858-1Client: Ramboll Environ US Corporation
Project/Site: Colonial Terminals/0730114
Lab Sample ID: 680-124858-5Client Sample ID: TRIP BLANK 20160504Matrix: WaterDate Collected: 05/04/16 00:00
Date Received: 05/04/16 15:47
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)RL MDL
1,1,2,2-Tetrachloroethane <1.0 1.0 ug/L 05/12/16 16:15 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 ug/L 05/12/16 16:15 1Tetrachloroethene <1.0
1.0 ug/L 05/12/16 16:15 1Toluene <1.0
1.0 ug/L 05/12/16 16:15 1trans-1,2-Dichloroethene <1.0
1.0 ug/L 05/12/16 16:15 1trans-1,3-Dichloropropene <1.0
5.0 ug/L 05/12/16 16:15 11,2,3-Trichlorobenzene <5.0
5.0 ug/L 05/12/16 16:15 11,2,4-Trichlorobenzene <5.0
1.0 ug/L 05/12/16 16:15 11,1,1-Trichloroethane <1.0
1.0 ug/L 05/12/16 16:15 11,1,2-Trichloroethane <1.0
1.0 ug/L 05/12/16 16:15 1Trichloroethene <1.0
1.0 ug/L 05/12/16 16:15 1Trichlorofluoromethane <1.0
1.0 ug/L 05/12/16 16:15 11,1,2-Trichloro-1,2,2-trifluoroethane <1.0
1.0 ug/L 05/12/16 16:15 1Vinyl chloride <1.0
Toluene-d8 (Surr) 100 70 - 130 05/12/16 16:15 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr) 90 05/12/16 16:15 170 - 130
Dibromofluoromethane (Surr) 93 05/12/16 16:15 170 - 130
4-Bromofluorobenzene (Surr) 95 05/12/16 16:15 170 - 130
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QC Sample ResultsTestAmerica Job ID: 680-124858-1Client: Ramboll Environ US Corporation
Project/Site: Colonial Terminals/0730114
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-432371/8
Matrix: Water Prep Type: Total/NA
Analysis Batch: 432371
RL MDL
Acetone <10 10 ug/L 05/09/16 11:30 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<1.0 1.0 ug/L 05/09/16 11:30 1Benzene
<1.0 1.0 ug/L 05/09/16 11:30 1Bromochloromethane
<1.0 1.0 ug/L 05/09/16 11:30 1Bromodichloromethane
<1.0 1.0 ug/L 05/09/16 11:30 1Bromoform
<5.0 5.0 ug/L 05/09/16 11:30 1Bromomethane
<10 10 ug/L 05/09/16 11:30 12-Butanone
<2.0 2.0 ug/L 05/09/16 11:30 1Carbon disulfide
<1.0 1.0 ug/L 05/09/16 11:30 1Carbon tetrachloride
<1.0 1.0 ug/L 05/09/16 11:30 1Chlorobenzene
<5.0 5.0 ug/L 05/09/16 11:30 1Chloroethane
<1.0 1.0 ug/L 05/09/16 11:30 1Chloroform
<1.0 1.0 ug/L 05/09/16 11:30 1Chloromethane
<1.0 1.0 ug/L 05/09/16 11:30 1cis-1,2-Dichloroethene
<1.0 1.0 ug/L 05/09/16 11:30 1cis-1,3-Dichloropropene
<1.0 1.0 ug/L 05/09/16 11:30 1Cyclohexane
<1.0 1.0 ug/L 05/09/16 11:30 1Dibromochloromethane
<5.0 5.0 ug/L 05/09/16 11:30 11,2-Dibromo-3-Chloropropane
<1.0 1.0 ug/L 05/09/16 11:30 11,2-Dibromoethane
<1.0 1.0 ug/L 05/09/16 11:30 11,2-Dichlorobenzene
<1.0 1.0 ug/L 05/09/16 11:30 11,3-Dichlorobenzene
<1.0 1.0 ug/L 05/09/16 11:30 11,4-Dichlorobenzene
<1.0 1.0 ug/L 05/09/16 11:30 1Dichlorodifluoromethane
<1.0 1.0 ug/L 05/09/16 11:30 11,1-Dichloroethane
<1.0 1.0 ug/L 05/09/16 11:30 11,2-Dichloroethane
<1.0 1.0 ug/L 05/09/16 11:30 11,1-Dichloroethene
<1.0 1.0 ug/L 05/09/16 11:30 11,2-Dichloropropane
<100 100 ug/L 05/09/16 11:30 11,4-Dioxane
<1.0 1.0 ug/L 05/09/16 11:30 1Ethylbenzene
<10 10 ug/L 05/09/16 11:30 12-Hexanone
<1.0 1.0 ug/L 05/09/16 11:30 1Isopropylbenzene
<5.0 5.0 ug/L 05/09/16 11:30 1Methyl acetate
<1.0 1.0 ug/L 05/09/16 11:30 1Methylcyclohexane
<5.0 5.0 ug/L 05/09/16 11:30 1Methylene Chloride
<10 10 ug/L 05/09/16 11:30 14-Methyl-2-pentanone
<10 10 ug/L 05/09/16 11:30 1Methyl tert-butyl ether
<1.0 1.0 ug/L 05/09/16 11:30 1m-Xylene & p-Xylene
<1.0 1.0 ug/L 05/09/16 11:30 1o-Xylene
<1.0 1.0 ug/L 05/09/16 11:30 1Styrene
<1.0 1.0 ug/L 05/09/16 11:30 11,1,2,2-Tetrachloroethane
<1.0 1.0 ug/L 05/09/16 11:30 1Tetrachloroethene
<1.0 1.0 ug/L 05/09/16 11:30 1Toluene
<1.0 1.0 ug/L 05/09/16 11:30 1trans-1,2-Dichloroethene
<1.0 1.0 ug/L 05/09/16 11:30 1trans-1,3-Dichloropropene
<5.0 5.0 ug/L 05/09/16 11:30 11,2,3-Trichlorobenzene
<5.0 5.0 ug/L 05/09/16 11:30 11,2,4-Trichlorobenzene
<1.0 1.0 ug/L 05/09/16 11:30 11,1,1-Trichloroethane
<1.0 1.0 ug/L 05/09/16 11:30 11,1,2-Trichloroethane
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QC Sample ResultsTestAmerica Job ID: 680-124858-1Client: Ramboll Environ US Corporation
Project/Site: Colonial Terminals/0730114
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-432371/8
Matrix: Water Prep Type: Total/NA
Analysis Batch: 432371
RL MDL
Trichloroethene <1.0 1.0 ug/L 05/09/16 11:30 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<1.0 1.0 ug/L 05/09/16 11:30 1Trichlorofluoromethane
<1.0 1.0 ug/L 05/09/16 11:30 11,1,2-Trichloro-1,2,2-trifluoroethane
<1.0 1.0 ug/L 05/09/16 11:30 1Vinyl chloride
Toluene-d8 (Surr) 90 70 - 130 05/09/16 11:30 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
96 05/09/16 11:30 11,2-Dichloroethane-d4 (Surr) 70 - 130
106 05/09/16 11:30 1Dibromofluoromethane (Surr) 70 - 130
97 05/09/16 11:30 14-Bromofluorobenzene (Surr) 70 - 130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-432371/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 432371
Acetone 250 285 ug/L 114 60 - 154
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 50.0 48.4 ug/L 97 73 - 131
Bromochloromethane 50.0 52.4 ug/L 105 77 - 122
Bromodichloromethane 50.0 48.2 ug/L 96 77 - 129
Bromoform 50.0 44.7 ug/L 89 69 - 135
Bromomethane 50.0 52.3 ug/L 105 20 - 180
2-Butanone 250 286 ug/L 114 75 - 133
Carbon disulfide 50.0 48.2 ug/L 96 73 - 127
Carbon tetrachloride 50.0 44.3 ug/L 89 75 - 130
Chlorobenzene 50.0 49.3 ug/L 99 80 - 120
Chloroethane 50.0 58.0 ug/L 116 50 - 151
Chloroform 50.0 46.3 ug/L 93 79 - 122
Chloromethane 50.0 45.3 ug/L 91 63 - 126
cis-1,2-Dichloroethene 50.0 52.8 ug/L 106 80 - 122
cis-1,3-Dichloropropene 50.0 49.6 ug/L 99 80 - 133
Cyclohexane 50.0 49.7 ug/L 99 69 - 130
Dibromochloromethane 50.0 45.9 ug/L 92 71 - 136
1,2-Dibromo-3-Chloropropane 50.0 48.5 ug/L 97 59 - 141
1,2-Dibromoethane 50.0 51.4 ug/L 103 77 - 131
1,2-Dichlorobenzene 50.0 52.3 ug/L 105 80 - 120
1,3-Dichlorobenzene 50.0 50.9 ug/L 102 80 - 120
1,4-Dichlorobenzene 50.0 52.3 ug/L 105 80 - 120
Dichlorodifluoromethane 50.0 51.5 ug/L 103 51 - 140
1,1-Dichloroethane 50.0 52.6 ug/L 105 80 - 120
1,2-Dichloroethane 50.0 53.8 ug/L 108 75 - 130
1,1-Dichloroethene 50.0 47.2 ug/L 94 74 - 125
1,2-Dichloropropane 50.0 50.9 ug/L 102 80 - 123
1,4-Dioxane 1000 1140 ug/L 114 40 - 187
Ethylbenzene 50.0 49.6 ug/L 99 80 - 120
2-Hexanone 250 269 ug/L 108 70 - 141
Isopropylbenzene 50.0 48.5 ug/L 97 80 - 120
Methyl acetate 250 301 ug/L 120 66 - 134
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QC Sample ResultsTestAmerica Job ID: 680-124858-1Client: Ramboll Environ US Corporation
Project/Site: Colonial Terminals/0730114
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-432371/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 432371
Methylcyclohexane 50.0 45.1 ug/L 90 75 - 127
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Methylene Chloride 50.0 53.3 ug/L 107 76 - 129
4-Methyl-2-pentanone 250 273 ug/L 109 75 - 135
Methyl tert-butyl ether 50.0 53.0 ug/L 106 74 - 135
m-Xylene & p-Xylene 50.0 49.6 ug/L 99 80 - 120
o-Xylene 50.0 49.9 ug/L 100 80 - 120
Styrene 50.0 53.2 ug/L 106 80 - 122
1,1,2,2-Tetrachloroethane 50.0 53.6 ug/L 107 72 - 128
Tetrachloroethene 50.0 45.1 ug/L 90 77 - 123
Toluene 50.0 47.3 ug/L 95 80 - 122
trans-1,2-Dichloroethene 50.0 50.7 ug/L 101 78 - 123
trans-1,3-Dichloropropene 50.0 49.0 ug/L 98 74 - 140
1,2,3-Trichlorobenzene 50.0 54.4 ug/L 109 61 - 151
1,2,4-Trichlorobenzene 50.0 53.9 ug/L 108 77 - 131
1,1,1-Trichloroethane 50.0 51.7 ug/L 103 74 - 128
1,1,2-Trichloroethane 50.0 52.5 ug/L 105 79 - 125
Trichloroethene 50.0 45.0 ug/L 90 80 - 123
Trichlorofluoromethane 50.0 51.9 ug/L 104 58 - 145
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
50.0 44.9 ug/L 90 65 - 131
Vinyl chloride 50.0 49.0 ug/L 98 68 - 132
Toluene-d8 (Surr) 70 - 130
Surrogate
97
LCS LCS
Qualifier Limits%Recovery
1121,2-Dichloroethane-d4 (Surr) 70 - 130
119Dibromofluoromethane (Surr) 70 - 130
1054-Bromofluorobenzene (Surr) 70 - 130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-432371/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 432371
Acetone 250 266 ug/L 106 60 - 154 7 40
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Benzene 50.0 49.3 ug/L 99 73 - 131 2 30
Bromochloromethane 50.0 51.2 ug/L 102 77 - 122 2 20
Bromodichloromethane 50.0 47.6 ug/L 95 77 - 129 1 20
Bromoform 50.0 44.6 ug/L 89 69 - 135 0 20
Bromomethane 50.0 53.6 ug/L 107 20 - 180 2 40
2-Butanone 250 281 ug/L 112 75 - 133 2 30
Carbon disulfide 50.0 52.1 ug/L 104 73 - 127 8 20
Carbon tetrachloride 50.0 48.0 ug/L 96 75 - 130 8 20
Chlorobenzene 50.0 50.5 ug/L 101 80 - 120 2 20
Chloroethane 50.0 58.4 ug/L 117 50 - 151 1 30
Chloroform 50.0 47.3 ug/L 95 79 - 122 2 20
Chloromethane 50.0 48.0 ug/L 96 63 - 126 6 30
cis-1,2-Dichloroethene 50.0 54.0 ug/L 108 80 - 122 2 20
cis-1,3-Dichloropropene 50.0 48.9 ug/L 98 80 - 133 2 20
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QC Sample ResultsTestAmerica Job ID: 680-124858-1Client: Ramboll Environ US Corporation
Project/Site: Colonial Terminals/0730114
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-432371/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 432371
Cyclohexane 50.0 54.2 ug/L 108 69 - 130 9 30
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Dibromochloromethane 50.0 45.4 ug/L 91 71 - 136 1 20
1,2-Dibromo-3-Chloropropane 50.0 47.3 ug/L 95 59 - 141 3 30
1,2-Dibromoethane 50.0 49.7 ug/L 99 77 - 131 3 30
1,2-Dichlorobenzene 50.0 53.2 ug/L 106 80 - 120 2 20
1,3-Dichlorobenzene 50.0 52.8 ug/L 106 80 - 120 4 20
1,4-Dichlorobenzene 50.0 53.2 ug/L 106 80 - 120 2 20
Dichlorodifluoromethane 50.0 55.8 ug/L 112 51 - 140 8 40
1,1-Dichloroethane 50.0 54.1 ug/L 108 80 - 120 3 20
1,2-Dichloroethane 50.0 51.2 ug/L 102 75 - 130 5 20
1,1-Dichloroethene 50.0 54.0 ug/L 108 74 - 125 13 20
1,2-Dichloropropane 50.0 50.7 ug/L 101 80 - 123 0 20
1,4-Dioxane 1000 1070 ug/L 107 40 - 187 6 50
Ethylbenzene 50.0 52.1 ug/L 104 80 - 120 5 20
2-Hexanone 250 260 ug/L 104 70 - 141 4 40
Isopropylbenzene 50.0 51.2 ug/L 102 80 - 120 5 20
Methyl acetate 250 285 ug/L 114 66 - 134 5 30
Methylcyclohexane 50.0 48.8 ug/L 98 75 - 127 8 30
Methylene Chloride 50.0 53.9 ug/L 108 76 - 129 1 20
4-Methyl-2-pentanone 250 263 ug/L 105 75 - 135 4 30
Methyl tert-butyl ether 50.0 51.8 ug/L 104 74 - 135 2 20
m-Xylene & p-Xylene 50.0 51.9 ug/L 104 80 - 120 5 20
o-Xylene 50.0 51.5 ug/L 103 80 - 120 3 20
Styrene 50.0 53.3 ug/L 107 80 - 122 0 20
1,1,2,2-Tetrachloroethane 50.0 51.9 ug/L 104 72 - 128 3 20
Tetrachloroethene 50.0 47.3 ug/L 95 77 - 123 5 20
Toluene 50.0 48.0 ug/L 96 80 - 122 1 20
trans-1,2-Dichloroethene 50.0 52.7 ug/L 105 78 - 123 4 20
trans-1,3-Dichloropropene 50.0 47.7 ug/L 95 74 - 140 3 20
1,2,3-Trichlorobenzene 50.0 55.4 ug/L 111 61 - 151 2 40
1,2,4-Trichlorobenzene 50.0 54.5 ug/L 109 77 - 131 1 20
1,1,1-Trichloroethane 50.0 53.3 ug/L 107 74 - 128 3 20
1,1,2-Trichloroethane 50.0 51.2 ug/L 102 79 - 125 2 20
Trichloroethene 50.0 46.5 ug/L 93 80 - 123 3 20
Trichlorofluoromethane 50.0 55.3 ug/L 111 58 - 145 6 30
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
50.0 50.9 ug/L 102 65 - 131 13 30
Vinyl chloride 50.0 52.9 ug/L 106 68 - 132 8 30
Toluene-d8 (Surr) 70 - 130
Surrogate
99
LCSD LCSD
Qualifier Limits%Recovery
1091,2-Dichloroethane-d4 (Surr) 70 - 130
112Dibromofluoromethane (Surr) 70 - 130
1064-Bromofluorobenzene (Surr) 70 - 130
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QC Sample ResultsTestAmerica Job ID: 680-124858-1Client: Ramboll Environ US Corporation
Project/Site: Colonial Terminals/0730114
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-432921/9
Matrix: Water Prep Type: Total/NA
Analysis Batch: 432921
RL MDL
Acetone <10 10 ug/L 05/12/16 09:06 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<1.0 1.0 ug/L 05/12/16 09:06 1Benzene
<1.0 1.0 ug/L 05/12/16 09:06 1Bromochloromethane
<1.0 1.0 ug/L 05/12/16 09:06 1Bromodichloromethane
<1.0 1.0 ug/L 05/12/16 09:06 1Bromoform
<5.0 5.0 ug/L 05/12/16 09:06 1Bromomethane
<10 10 ug/L 05/12/16 09:06 12-Butanone
<2.0 2.0 ug/L 05/12/16 09:06 1Carbon disulfide
<1.0 1.0 ug/L 05/12/16 09:06 1Carbon tetrachloride
<1.0 1.0 ug/L 05/12/16 09:06 1Chlorobenzene
<5.0 5.0 ug/L 05/12/16 09:06 1Chloroethane
<1.0 1.0 ug/L 05/12/16 09:06 1Chloroform
<1.0 1.0 ug/L 05/12/16 09:06 1Chloromethane
<1.0 1.0 ug/L 05/12/16 09:06 1cis-1,2-Dichloroethene
<1.0 1.0 ug/L 05/12/16 09:06 1cis-1,3-Dichloropropene
<1.0 1.0 ug/L 05/12/16 09:06 1Cyclohexane
<1.0 1.0 ug/L 05/12/16 09:06 1Dibromochloromethane
<5.0 5.0 ug/L 05/12/16 09:06 11,2-Dibromo-3-Chloropropane
<1.0 1.0 ug/L 05/12/16 09:06 11,2-Dibromoethane
<1.0 1.0 ug/L 05/12/16 09:06 11,2-Dichlorobenzene
<1.0 1.0 ug/L 05/12/16 09:06 11,3-Dichlorobenzene
<1.0 1.0 ug/L 05/12/16 09:06 11,4-Dichlorobenzene
<1.0 1.0 ug/L 05/12/16 09:06 1Dichlorodifluoromethane
<1.0 1.0 ug/L 05/12/16 09:06 11,1-Dichloroethane
<1.0 1.0 ug/L 05/12/16 09:06 11,2-Dichloroethane
<1.0 1.0 ug/L 05/12/16 09:06 11,1-Dichloroethene
<1.0 1.0 ug/L 05/12/16 09:06 11,2-Dichloropropane
<100 100 ug/L 05/12/16 09:06 11,4-Dioxane
<1.0 1.0 ug/L 05/12/16 09:06 1Ethylbenzene
<10 10 ug/L 05/12/16 09:06 12-Hexanone
<1.0 1.0 ug/L 05/12/16 09:06 1Isopropylbenzene
<5.0 5.0 ug/L 05/12/16 09:06 1Methyl acetate
<1.0 1.0 ug/L 05/12/16 09:06 1Methylcyclohexane
<5.0 5.0 ug/L 05/12/16 09:06 1Methylene Chloride
<10 10 ug/L 05/12/16 09:06 14-Methyl-2-pentanone
<10 10 ug/L 05/12/16 09:06 1Methyl tert-butyl ether
<1.0 1.0 ug/L 05/12/16 09:06 1m-Xylene & p-Xylene
<1.0 1.0 ug/L 05/12/16 09:06 1o-Xylene
<1.0 1.0 ug/L 05/12/16 09:06 1Styrene
<1.0 1.0 ug/L 05/12/16 09:06 11,1,2,2-Tetrachloroethane
<1.0 1.0 ug/L 05/12/16 09:06 1Tetrachloroethene
<1.0 1.0 ug/L 05/12/16 09:06 1Toluene
<1.0 1.0 ug/L 05/12/16 09:06 1trans-1,2-Dichloroethene
<1.0 1.0 ug/L 05/12/16 09:06 1trans-1,3-Dichloropropene
<5.0 5.0 ug/L 05/12/16 09:06 11,2,3-Trichlorobenzene
<5.0 5.0 ug/L 05/12/16 09:06 11,2,4-Trichlorobenzene
<1.0 1.0 ug/L 05/12/16 09:06 11,1,1-Trichloroethane
<1.0 1.0 ug/L 05/12/16 09:06 11,1,2-Trichloroethane
TestAmerica Savannah
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QC Sample ResultsTestAmerica Job ID: 680-124858-1Client: Ramboll Environ US Corporation
Project/Site: Colonial Terminals/0730114
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-432921/9
Matrix: Water Prep Type: Total/NA
Analysis Batch: 432921
RL MDL
Trichloroethene <1.0 1.0 ug/L 05/12/16 09:06 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<1.0 1.0 ug/L 05/12/16 09:06 1Trichlorofluoromethane
<1.0 1.0 ug/L 05/12/16 09:06 11,1,2-Trichloro-1,2,2-trifluoroethane
<1.0 1.0 ug/L 05/12/16 09:06 1Vinyl chloride
Toluene-d8 (Surr) 104 70 - 130 05/12/16 09:06 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
89 05/12/16 09:06 11,2-Dichloroethane-d4 (Surr) 70 - 130
93 05/12/16 09:06 1Dibromofluoromethane (Surr) 70 - 130
94 05/12/16 09:06 14-Bromofluorobenzene (Surr) 70 - 130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-432921/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 432921
Acetone 250 188 ug/L 75 60 - 154
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 50.0 44.7 ug/L 89 73 - 131
Bromochloromethane 50.0 44.0 ug/L 88 77 - 122
Bromodichloromethane 50.0 44.5 ug/L 89 77 - 129
Bromoform 50.0 43.3 ug/L 87 69 - 135
Bromomethane 50.0 38.3 ug/L 77 20 - 180
2-Butanone 250 210 ug/L 84 75 - 133
Carbon disulfide 50.0 40.5 ug/L 81 73 - 127
Carbon tetrachloride 50.0 44.1 ug/L 88 75 - 130
Chlorobenzene 50.0 49.0 ug/L 98 80 - 120
Chloroethane 50.0 39.7 ug/L 79 50 - 151
Chloroform 50.0 41.7 ug/L 83 79 - 122
Chloromethane 50.0 36.1 ug/L 72 63 - 126
cis-1,2-Dichloroethene 50.0 44.4 ug/L 89 80 - 122
cis-1,3-Dichloropropene 50.0 44.1 ug/L 88 80 - 133
Cyclohexane 50.0 44.1 ug/L 88 69 - 130
Dibromochloromethane 50.0 45.1 ug/L 90 71 - 136
1,2-Dibromo-3-Chloropropane 50.0 44.2 ug/L 88 59 - 141
1,2-Dibromoethane 50.0 43.4 ug/L 87 77 - 131
1,2-Dichlorobenzene 50.0 48.0 ug/L 96 80 - 120
1,3-Dichlorobenzene 50.0 48.4 ug/L 97 80 - 120
1,4-Dichlorobenzene 50.0 47.1 ug/L 94 80 - 120
Dichlorodifluoromethane 50.0 40.5 ug/L 81 51 - 140
1,1-Dichloroethane 50.0 45.3 ug/L 91 80 - 120
1,2-Dichloroethane 50.0 44.9 ug/L 90 75 - 130
1,1-Dichloroethene 50.0 43.1 ug/L 86 74 - 125
1,2-Dichloropropane 50.0 43.9 ug/L 88 80 - 123
1,4-Dioxane 1000 805 ug/L 81 40 - 187
Ethylbenzene 50.0 48.2 ug/L 96 80 - 120
2-Hexanone 250 204 ug/L 82 70 - 141
Isopropylbenzene 50.0 48.1 ug/L 96 80 - 120
Methyl acetate 250 205 ug/L 82 66 - 134
TestAmerica Savannah
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QC Sample ResultsTestAmerica Job ID: 680-124858-1Client: Ramboll Environ US Corporation
Project/Site: Colonial Terminals/0730114
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-432921/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 432921
Methylcyclohexane 50.0 44.6 ug/L 89 75 - 127
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Methylene Chloride 50.0 41.9 ug/L 84 76 - 129
4-Methyl-2-pentanone 250 209 ug/L 84 75 - 135
Methyl tert-butyl ether 50.0 43.1 ug/L 86 74 - 135
m-Xylene & p-Xylene 50.0 47.5 ug/L 95 80 - 120
o-Xylene 50.0 48.9 ug/L 98 80 - 120
Styrene 50.0 49.8 ug/L 100 80 - 122
1,1,2,2-Tetrachloroethane 50.0 45.3 ug/L 91 72 - 128
Tetrachloroethene 50.0 46.5 ug/L 93 77 - 123
Toluene 50.0 45.7 ug/L 91 80 - 122
trans-1,2-Dichloroethene 50.0 42.4 ug/L 85 78 - 123
trans-1,3-Dichloropropene 50.0 45.6 ug/L 91 74 - 140
1,2,3-Trichlorobenzene 50.0 47.0 ug/L 94 61 - 151
1,2,4-Trichlorobenzene 50.0 46.4 ug/L 93 77 - 131
1,1,1-Trichloroethane 50.0 44.6 ug/L 89 74 - 128
1,1,2-Trichloroethane 50.0 43.5 ug/L 87 79 - 125
Trichloroethene 50.0 45.5 ug/L 91 80 - 123
Trichlorofluoromethane 50.0 43.7 ug/L 87 58 - 145
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
50.0 45.3 ug/L 91 65 - 131
Vinyl chloride 50.0 39.6 ug/L 79 68 - 132
Toluene-d8 (Surr) 70 - 130
Surrogate
99
LCS LCS
Qualifier Limits%Recovery
891,2-Dichloroethane-d4 (Surr) 70 - 130
93Dibromofluoromethane (Surr) 70 - 130
934-Bromofluorobenzene (Surr) 70 - 130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-432921/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 432921
Acetone 250 187 ug/L 75 60 - 154 1 40
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Benzene 50.0 45.1 ug/L 90 73 - 131 1 30
Bromochloromethane 50.0 44.0 ug/L 88 77 - 122 0 20
Bromodichloromethane 50.0 44.5 ug/L 89 77 - 129 0 20
Bromoform 50.0 43.4 ug/L 87 69 - 135 0 20
Bromomethane 50.0 39.6 ug/L 79 20 - 180 3 40
2-Butanone 250 213 ug/L 85 75 - 133 1 30
Carbon disulfide 50.0 40.3 ug/L 81 73 - 127 0 20
Carbon tetrachloride 50.0 44.2 ug/L 88 75 - 130 0 20
Chlorobenzene 50.0 50.1 ug/L 100 80 - 120 2 20
Chloroethane 50.0 39.2 ug/L 78 50 - 151 1 30
Chloroform 50.0 41.4 ug/L 83 79 - 122 1 20
Chloromethane 50.0 36.7 ug/L 73 63 - 126 2 30
cis-1,2-Dichloroethene 50.0 44.7 ug/L 89 80 - 122 1 20
cis-1,3-Dichloropropene 50.0 43.9 ug/L 88 80 - 133 0 20
TestAmerica Savannah
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QC Sample ResultsTestAmerica Job ID: 680-124858-1Client: Ramboll Environ US Corporation
Project/Site: Colonial Terminals/0730114
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-432921/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 432921
Cyclohexane 50.0 43.5 ug/L 87 69 - 130 1 30
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Dibromochloromethane 50.0 44.7 ug/L 89 71 - 136 1 20
1,2-Dibromo-3-Chloropropane 50.0 46.2 ug/L 92 59 - 141 5 30
1,2-Dibromoethane 50.0 43.1 ug/L 86 77 - 131 1 30
1,2-Dichlorobenzene 50.0 49.0 ug/L 98 80 - 120 2 20
1,3-Dichlorobenzene 50.0 49.2 ug/L 98 80 - 120 2 20
1,4-Dichlorobenzene 50.0 48.5 ug/L 97 80 - 120 3 20
Dichlorodifluoromethane 50.0 40.0 ug/L 80 51 - 140 1 40
1,1-Dichloroethane 50.0 45.3 ug/L 91 80 - 120 0 20
1,2-Dichloroethane 50.0 44.0 ug/L 88 75 - 130 2 20
1,1-Dichloroethene 50.0 43.3 ug/L 87 74 - 125 0 20
1,2-Dichloropropane 50.0 44.2 ug/L 88 80 - 123 1 20
1,4-Dioxane 1000 825 ug/L 82 40 - 187 2 50
Ethylbenzene 50.0 49.2 ug/L 98 80 - 120 2 20
2-Hexanone 250 208 ug/L 83 70 - 141 2 40
Isopropylbenzene 50.0 49.0 ug/L 98 80 - 120 2 20
Methyl acetate 250 208 ug/L 83 66 - 134 1 30
Methylcyclohexane 50.0 44.1 ug/L 88 75 - 127 1 30
Methylene Chloride 50.0 41.4 ug/L 83 76 - 129 1 20
4-Methyl-2-pentanone 250 211 ug/L 85 75 - 135 1 30
Methyl tert-butyl ether 50.0 43.6 ug/L 87 74 - 135 1 20
m-Xylene & p-Xylene 50.0 47.6 ug/L 95 80 - 120 0 20
o-Xylene 50.0 49.1 ug/L 98 80 - 120 1 20
Styrene 50.0 50.0 ug/L 100 80 - 122 0 20
1,1,2,2-Tetrachloroethane 50.0 45.8 ug/L 92 72 - 128 1 20
Tetrachloroethene 50.0 46.8 ug/L 94 77 - 123 1 20
Toluene 50.0 45.0 ug/L 90 80 - 122 2 20
trans-1,2-Dichloroethene 50.0 43.2 ug/L 86 78 - 123 2 20
trans-1,3-Dichloropropene 50.0 44.6 ug/L 89 74 - 140 2 20
1,2,3-Trichlorobenzene 50.0 48.7 ug/L 97 61 - 151 4 40
1,2,4-Trichlorobenzene 50.0 48.2 ug/L 96 77 - 131 4 20
1,1,1-Trichloroethane 50.0 45.3 ug/L 91 74 - 128 1 20
1,1,2-Trichloroethane 50.0 43.6 ug/L 87 79 - 125 0 20
Trichloroethene 50.0 45.0 ug/L 90 80 - 123 1 20
Trichlorofluoromethane 50.0 34.4 ug/L 69 58 - 145 24 30
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
50.0 44.3 ug/L 89 65 - 131 2 30
Vinyl chloride 50.0 39.8 ug/L 80 68 - 132 0 30
Toluene-d8 (Surr) 70 - 130
Surrogate
101
LCSD LCSD
Qualifier Limits%Recovery
901,2-Dichloroethane-d4 (Surr) 70 - 130
92Dibromofluoromethane (Surr) 70 - 130
954-Bromofluorobenzene (Surr) 70 - 130
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QC Association SummaryTestAmerica Job ID: 680-124858-1Client: Ramboll Environ US Corporation
Project/Site: Colonial Terminals/0730114
GC/MS VOA
Analysis Batch: 432371
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B680-124858-1 SW-01R 20160504 Total/NA
Water 8260B680-124858-2 SW-02R 20160504 Total/NA
Water 8260B680-124858-3 SW-03R 20160504 Total/NA
Water 8260B680-124858-4 DUP-01 20160504 Total/NA
Water 8260BLCS 680-432371/3 Lab Control Sample Total/NA
Water 8260BLCSD 680-432371/4 Lab Control Sample Dup Total/NA
Water 8260BMB 680-432371/8 Method Blank Total/NA
Analysis Batch: 432921
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B680-124858-5 TRIP BLANK 20160504 Total/NA
Water 8260BLCS 680-432921/4 Lab Control Sample Total/NA
Water 8260BLCSD 680-432921/5 Lab Control Sample Dup Total/NA
Water 8260BMB 680-432921/9 Method Blank Total/NA
TestAmerica Savannah
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Lab ChronicleClient: Ramboll Environ US Corporation TestAmerica Job ID: 680-124858-1
Project/Site: Colonial Terminals/0730114
Client Sample ID: SW-01R 20160504 Lab Sample ID: 680-124858-1Matrix: WaterDate Collected: 05/04/16 13:10
Date Received: 05/04/16 15:47
Analysis 8260B CAR05/09/16 17:531 TAL SAV432371
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
CMSA2Instrument ID:
Client Sample ID: SW-02R 20160504 Lab Sample ID: 680-124858-2Matrix: WaterDate Collected: 05/04/16 13:42
Date Received: 05/04/16 15:47
Analysis 8260B CAR05/09/16 18:141 TAL SAV432371
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
CMSA2Instrument ID:
Client Sample ID: SW-03R 20160504 Lab Sample ID: 680-124858-3Matrix: WaterDate Collected: 05/04/16 14:40
Date Received: 05/04/16 15:47
Analysis 8260B CAR05/09/16 18:341 TAL SAV432371
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
CMSA2Instrument ID:
Client Sample ID: DUP-01 20160504 Lab Sample ID: 680-124858-4Matrix: WaterDate Collected: 05/04/16 00:00
Date Received: 05/04/16 15:47
Analysis 8260B CAR05/09/16 18:541 TAL SAV432371
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
CMSA2Instrument ID:
Client Sample ID: TRIP BLANK 20160504 Lab Sample ID: 680-124858-5Matrix: WaterDate Collected: 05/04/16 00:00
Date Received: 05/04/16 15:47
Analysis 8260B CEJ05/12/16 16:151 TAL SAV432921
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
CMSP2Instrument ID:
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858
TestAmerica Savannah
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Login Sample Receipt Checklist
Client: Ramboll Environ US Corporation Job Number: 680-124858-1
Login Number: 124858
Question Answer Comment
Creator: White, Menica R
List Source: TestAmerica Savannah
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
N/AIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
N/AMultiphasic samples are not present.
N/ASamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica SavannahPage 23 of 24
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Certification SummaryClient: Ramboll Environ US Corporation TestAmerica Job ID: 680-124858-1
Project/Site: Colonial Terminals/0730114
Laboratory: TestAmerica SavannahAll certifications held by this laboratory are listed. Not all certifications are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
SAVLABAFCEE
A2LA DoD ELAP 399.01 02-28-17
A2LA ISO/IEC 17025 399.01 02-28-17
Alabama State Program 4 41450 06-30-16 *
Alaska (UST) State Program 10 UST-104 11-05-16
Arkansas DEQ State Program 6 88-0692 01-31-17
California State Program 9 2939 07-31-16 *
Colorado State Program 8 N/A 12-31-16
Connecticut State Program 1 PH-0161 03-31-17
Florida NELAP 4 E87052 06-30-16 *
GA Dept. of Agriculture State Program 4 N/A 06-12-17
Georgia State Program 4 803 06-30-16 *
Guam State Program 9 15-005r 04-16-16 *
Hawaii State Program 9 N/A 06-30-16 *
Illinois NELAP 5 200022 11-30-16
Indiana State Program 5 N/A 06-30-16 *
Iowa State Program 7 353 06-30-17
Kentucky (DW) State Program 4 90084 12-31-16
Kentucky (UST) State Program 4 18 06-30-16 *
Kentucky (WW) State Program 4 90084 12-31-16
Louisiana NELAP 6 30690 06-30-16 *
Louisiana (DW) NELAP 6 LA160019 12-31-16
Maine State Program 1 GA00006 09-24-16
Maryland State Program 3 250 12-31-16
Massachusetts State Program 1 M-GA006 06-30-16 *
Michigan State Program 5 9925 06-30-16 *
Mississippi State Program 4 N/A 06-30-16 *
Nebraska State Program 7 TestAmerica-Savannah 06-30-16 *
New Jersey NELAP 2 GA769 06-30-16 *
New Mexico State Program 6 N/A 06-30-16 *
New York NELAP 2 10842 03-31-17
North Carolina (DW) State Program 4 13701 07-31-16 *
North Carolina (WW/SW) State Program 4 269 12-31-16
Oklahoma State Program 6 9984 08-31-16
Pennsylvania NELAP 3 68-00474 06-30-16 *
Puerto Rico State Program 2 GA00006 12-31-16
South Carolina State Program 4 98001 06-30-16 *
Tennessee State Program 4 TN02961 06-30-16 *
Texas NELAP 6 T104704185-14-7 11-30-16
USDA Federal SAV 3-04 06-11-17
Virginia NELAP 3 460161 06-14-16 *
Washington State Program 10 C805 06-10-16 *
West Virginia (DW) State Program 3 9950C 12-31-16
West Virginia DEP State Program 3 094 06-30-16 *
Wisconsin State Program 5 999819810 08-31-16
Wyoming State Program 8 8TMS-L 06-30-16 *
TestAmerica Savannah
* Certification renewal pending - certification considered valid.
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