CLOSURE PLAN WASTE MANAGEMENT UNITSClosure Plan Waste Management Units Project No. 4014 1-1...

CLOSURE PLAN

WASTE MANAGEMENT UNITS

FOR

CES GRIGGS ROAD VCP SITE

VCP NO. 2751

HOUSTON, HARRIS COUNTY, TEXAS 77021

CUSTOMER NO. CN604824904 REGULATED ENTITY NO. RN108370644

PREPARED BY:

PASTOR, BEHLING, & WHEELER, LLC 11231 RICHMOND AVENUE, D104

HOUSTON, TEXAS PROJECT NO. 4014

SEPTEMBER 2016

CES Griggs Road VCP Site

Closure Plan Waste Management Units

Project No. 4014 i September 2016

TABLE OF CONTENTS

1.0 INTRODUCTION ....................................................................................................................... 1-1

1.1 Site History ............................................................................................................................ 1-1

1.2 Previous Removal Actions .................................................................................................... 1-2

1.3 Analytical Methods and Closure Criteria ............................................................................... 1-3

2.0 CLOSURE ACTIVITIES FOR NOTICE OF REGISTRATION (NOR) UNITS ........................... 2-1

2.1 Container Storage Areas ....................................................................................................... 2-1

2.2 Miscellaneous Storage Containers ....................................................................................... 2-1

2.3 Sumps .................................................................................................................................... 2-2

2.4 Tanks ..................................................................................................................................... 2-2

3.0 OTHER WASTE UNITS ............................................................................................................ 3-1

3.1 Sumps and Trenches ............................................................................................................ 3-1

3.2 Tanks ..................................................................................................................................... 3-2

4.0 CLOSURE ACTIVITIES ............................................................................................................. 4-1

4.1 Safety ..................................................................................................................................... 4-1

4.2 Pressure Washing ................................................................................................................. 4-2

4.3 CSA Cleaning and Documentation ....................................................................................... 4-2

4.4 Sump / Trench Cleaning and Documentation ....................................................................... 4-2

4.5 Tank Cleaning and Decontamination .................................................................................... 4-3

4.6 Storage, Transportation and Disposal ................................................................................... 4-4

4.7 Backfill ................................................................................................................................... 4-4

4.8 Analytical Data ....................................................................................................................... 4-4

4.9 Reporting ............................................................................................................................... 4-5

5.0 REFERENCES .......................................................................................................................... 5-1

LIST OF TABLES

Table 1 RCRA Waste Codes Associated with Hazardous Waste Management Units Table 2 Notice of Registration (NOR) Waste Management Units Table 3 Sump and Trench Dimensions Table 4 Summary of Nonhazardous and Hazardous Waste Classification for Tanks Table 5 Summary of Waste Liquid Data



Project No. 4014 ii September 2016

Table 6 Summary of Waste Sludge Data

LIST OF FIGURES

Figure 1 On-Site Property Map Figure 2 Stormwater Pollution Prevention Plan Map Figure 3 Site Plan Suttles Truck Leasing

ATTACHMENTS

Attachment 1 March 6, 2012 CES Environmental Services Notice of Registration Attachment 2 TCEQ Closure Report Checklist Attachment 3 Notice of Registration Units Photolog Attachment 4 Other Waste Management Units Photolog

Attachment 5 30 TAC 335.521(a)(1) Texas Class 2 Regulatory Levels



Project No. 4014 1-1 September 2016

1.0 INTRODUCTION

This document provides a closure plan for waste units located at the CES Environmental Services Voluntary Cleanup Program (VCP) Site (the “Site”). The project consists of the decontamination of waste units and does not include demolition activities. This plan describes the procedures and protocols to close units listed on the CES Environmental Services Solid Waste Registration (SWR) Notice of Registration (NOR) (Attachment 1) and to decontaminate other units such as sumps, trenches, and above ground storage tanks (ASTs) that may have held waste materials but are not listed on the NOR. These procedures were prepared based on guidance in the waste management unit (WMU) Closure Report Checklist developed by the Texas Commission on Environmental Quality (TCEQ) Remediation Division (Attachment 2).

1.1 Site History

The Site is a former industrial cleaning, waste recycling, and waste disposal facility located at 4904 Griggs Road, Houston, Harris County, Texas. The Site consists of three properties: 4904 Griggs Road, 5910 Wayland Street, and 4900 Griggs Road Street (Figure 1).

The Younger family purchased the 4904 Griggs Road property in the early 1940’s. According to the Harris County Appraisal District Records (HCAD, 2015), the following companies owned the 4904 Griggs Road Property:

• Younger Transportation to December 31, 1988

• Younger Brothers, Inc. to August 18, 1998

• Suttles Truck Leasing, Inc. to June 11, 2002

• CES Environmental Services

Younger Brothers, Inc. operated the facility as a tank truck terminal (WCM, 1996). Operations included dispatch, storage, routine maintenance, and internal and external washing of tank trucks that hauled a variety of petrochemical substances. CES cleaned truck trailers, roll-off boxes, totes and other transportation equipment. Materials within the equipment included petroleum products, paint thinners, solvents, and acids. CES also recycled motor oil and solvents such as acetone, methyl ethyl ketone, and methylene chloride. The company processed sodium sulfide, sodium hydroxide, and naphthenic acid solutions and treated industrial wastewater at the Site (TCEQ, 2014). On August 13, 2010, CES filed for Chapter 11 bankruptcy and operations appear to have ceased at that time. The property is owned by CES Environmental Services but is under the control of a Chapter 7 bankruptcy trustee.

Waste handling activities for Younger Brothers, Suttles, and CES were authorized under SWR 30900. The NOR lists 49 waste units and 45 waste codes. The table below summarizes the permit and authorization status.




Program Identification Number Status

IHW Corrective Action Solid Waste Registration 30900 Inactive

Industrial and Hazardous Waste Registration TXD008950461 Active

Industrial and Hazardous Waste Permit 39048 Cancelled*

Sludge Registration 23198 Cancelled

Used Oil Identification TXD008950461 Active

Used Oil Registration A85775 / C87443 Inactive * The Chapter 7 Bankruptcy Trustee relinquished operating permits for the Site to enable Site cleanup.

Closure activities are not planned for the 4900 Griggs Road and 5910 Wayland Street properties as waste units have not been identified at these two properties. The only entity associated with 4900 Griggs Road in the TCEQ Central Registry records is Tony’s Bar Supply Company (CN600996201). An underground storage tank (UST) was registered to Tony’s Bar Supply and, according to the TCEQ Central Registry, the UST was removed in 1989. A ground penetrating radar search was conducted during the affected property assessment and an UST was not located.

The Younger family utilized the 5910 Wayland Street property for tank truck trailer and tractor parking, as well as storage of flat bed and tank trucks and staging of offices in small temporary buildings (WCM, 1996). The entities listed below are associated with 5910 Wayland Street in the TCEQ Central Registry records (TCEQ, 2015).

• Bluebonnet Petrochemical (CN603776758)

• J&J Container Manufacturing (CN601491210)

• SKS Stricker LLC (CN603578022)

• Tornado Waste (CN603021577)

An active registration, SWR 88933, was identified in the TCEQ Central Registry records as an authorization for Bluebonnet Petrochemical to operate as a 10-day transfer station starting in September 2009. The metal warehouse on the 5910 Wayland Street property is labeled as field services and various containers were stored on the property prior to and through CES ownership. However, no waste units or waste codes associated with SWR 88933 have been identified.

In addition, this closure work plan does not address the former USTs located in the northern portion of 4904 Griggs Road. The 10,000-gallon diesel UST was permanently removed from the ground on August 27, 1998 (TCEQ, 2016a). The removal was certified by Dodie Sterling of Younger Brothers on September 16, 1998. The 12,000-gallon UST was permanently removed from service in January 1976 by filling the tank with an inert material. This was certified by James Longaker on May 6, 1986.

1.2 Previous Removal Actions

The Bankruptcy Trustee consolidated and disposed of laboratory chemicals, bulk process chemicals, and profile samples. In addition, the Trustee removed wastes that were dumped on the ground during the March 2014 theft, as well as one vacuum box and one roll-off box of waste materials. In September




2014, EPA and their emergency response contractor, mobilized to initiate the removal and disposal of hazardous wastes and substances contained in approximately 22 ASTs, two roll-off boxes, 12 frac tanks, 11 vacuum boxes, two tanker trailers, 224 totes/drums, and other containers located at the Site. In addition, EPA and TCEQ cleaned secondary containments, sumps, the truck and loading bays in the main processing building, the equipment and fleet maintenance warehouse, and the oil/water separator to remove debris and hydrocarbons. Visibly contaminated soils were removed to eliminate sheen on stormwater. The waste removal action was completed in June 2015. The table below summarizes the estimated volume of waste removed by EPA and TCEQ (EPA, 2015b).

Disposal Volume Units RCRA Waste Code Hazardous waste incineration 607,850 pounds D001, D002, D003, D007, D008, D018, D020,

D023, D024, D025, D026, D027, D030, D032, D033, D034, D036, D037, D038, D042, D043

Hazardous waste landfill 140 cubic yards D020, D023, D024, D026, D032 Hazardous waste fuel blending or wastewater treatment or landfill stabilization

185,062 gallons D002, D004, D006, D007, D008, D010, D011, D018, D019, D023, D026, D027, D028, D033, D034, D036, D040, D042, D043

Non-hazardous waste landfill solids Class 1 or Class 2 285 cubic yards

Non-hazardous waste landfill Class 1 4.9 tons Non-hazardous waste landfill (liquids for solidification) Class 1 or waste water treatment or deep well injection

421,1576 gallons

1.3 Analytical Methods and Closure Criteria

Table 1 lists the Environmental Protection Agency (EPA) RCRA waste codes for the materials handled in the hazardous waste units. Table 2 summarizes general information about the NOR units and includes a list of soil borings completed during the affected property assessment that were associated with each unit. Figure 1 shows the buildings located at the Site. Figure 2 shows the location of units documented in the CES Compliance Investigation #707324 (TCEQ, 2009). Figure 3 shows the locations of WMU 002 to WMU 008 from the Suttles Compliance Evaluation Inspection (TNRCC, 1998). The location of WMU 001 (sump) was identified from the 1985 facility drawings in the TCEQ Central Files accessed on May 20, 2016. Attachment 3 contains photographs of the current conditions of most of the waste units listed on the NOR. Attachment 4 contains photographs of other units (sumps, trenches, and tanks) that may have held waste materials but are not listed on the NOR.

The closure analytical suite for each WMU was determined by reviewing TCEQ waste codes listed on the NOR (Attachment 1) and EPA waste data (Tables 4 through 6). If the TCEQ waste code ended in “H” OR if the EPA waste data indicated the presence a RCRA hazardous constituent above the regulatory levels (40 CFR 261.24), then the rinsate samples will be analyzed for the RCRA waste code parameters. Conversely, if the TCEQ waste code ended in “1” or “2” AND if the EPA waste data did not indicate the presence a RCRA hazardous constituent above the regulatory levels, then the rinsate samples will be analyzed for the constituents listed on either Table 5 or Table 6. Rinsate samples will be analyzed for constituents listed on Tables 5 and 6 which had concentrations exceeding the Texas Class 2 Regulatory Levels (30 TAC 335.521 (a)(1)) (Attachment 5).




In the example below, WMU 119 (Tank T10) managed TCEQ waste codes 9019519H, 90185191, and 90171142. The corresponding waste information for TCEQ code 9019519H (precipitated hazardous sludge) was reviewed to identify the RCRA codes. The waste information section of the NOR states that 9019519H was hazardous for characteristics, D004 (arsenic), D005 (barium), D006 (cadmium), D007 (chromium), D008 (lead), D009 (mercury), and D011 (silver). Rinsate samples from WMU 119 (or other units with TCEQ code 90919519H) would be analyzed for RCRA metals.

If waste samples were not analyzed during the EPA/TCEQ removal action, the NOR waste codes were reviewed. As an example, the Class 1 (90185191) and Class 2 (90171142) waste codes shown below do not provide specific waste descriptions. However, TCEQ code 90185191 provides sufficient information to designate an analytical suite. It is described as inorganic sludge generated from treatment of water with dissolved metals or acid/base solution. Appropriate analyses for rinsate samples from units that managed waste with a TCEQ code of 90185191 are RCRA metals and pH. In contrast, TCEQ code 90171142 is described as treated Class 2 wastewater discharged to a POTW and as aqueous waste with low dissolved solids. No analytical suite would be identified for this type of TCEQ code. Total petroleum hydrocarbons (TPH) and pH are the appropriate analtyical parameters for waste units with insufficient information to identify an analytical suite.




2.0 CLOSURE ACTIVITIES FOR NOTICE OF REGISTRATION (NOR) UNITS

This describes the closure activities planned for the container storage areas (CSA), miscellaneous storage containers (MSC), sumps and tanks listed on the NOR for SWR 30900. Table 1 summarizes the RCRA waste codes for units handling hazardous waste. Table 2 provides information for the NOR waste units. Figure 1 shows the location of the buildings associated with the WMUs. Figures 2 and 3 show the locations of the WMUs. Attachment 3 contains photographs of the WMUs or the former location of the WMUs.

2.1 Container Storage Areas

This section describes the closure process for the CSAs listed on the NOR (Table 2). The CSAs will be cleaned as described in Section 4.3. Samples will be collected from the final rinsates in each CSA for the analytes listed in the table below. A closure report will be prepared with the general information listed on the Closure Report Checklist (Attachment 2) and analytical data from the rinsate analyses.

NOR Unit Facility ID Location Analytical Suite

003 Old Wash Rack

Current Safe Wash area Acetone, naphthalene, toluene, xylene; TPH (See Table 1)

105 Hazardous Waste CSA

South side Equipment and Fleet Maintenance Building

Flashpoint, pH, reactivity, RCRA Metals, RCRA VOCs, and RCRA SVOCs, acetone, 1,2-dichlorobenzene, ethylbenzene,

methyl isobutyl ketone, methylene chloride, 1,1,1-trichloroethane, 1,1,2-trichloroethane, 1,1,2-trichloro-

1,2,2-trichloroethane, trichlorofluoromethane, xylenes (See Table 1)

106 Permit Unit No. 1

South part of Main Processing Building; include trenches pH, TPH

107 Permit Unit No. 2

Middle portion of Main Processing Building; include trenches pH, TPH

Hazardous waste management units

2.2 Miscellaneous Storage Containers

This section describes the closure process for the MSCs listed on the NOR (Table 2). These units are no longer present at the Site. The exact location of WMU 009 is unknown. The closure report will be prepared with the general information listed on the Closure Report Checklist, photographs of the areas showing the absence of the MSC, and a description of the EPA/TCEQ removal action.

NOR Unit Facility ID Original Location Analytical Suite

002 None South side of Equipment & Fleet Maintenance Building None; not present at Site

005 Dumpster Located corner of Wayland Street right of way and 5910 Wayland Street None; not present at Site

009 CSA Unknown; held used oil filters and rags None; not present at Site

103 Sludge box Located in Safe Wash Building. Close by cleaning trenches in Safe Wash area as described in Section 4 and by analyzing rinsate pH, TPH

104 Open top box Roll-off south of Drum Cleaning Building None; not present at Site Hazardous waste management units




2.3 Sumps

This section describes the closure process for sumps listed on the NOR. Wastes were removed from the sumps during the EPA emergency removal action and the sumps were rinsed (Moore, 2015). Table 3 summarizes the sump dimensions, where known. The sumps will be cleaned as described in Section 4.4. Samples will be collected from the final rinsates for the analytes listed in the table below. Sumps and trenches will be backfilled as described in Section 4.7. In addition, solids within metal bars of grates (Photo 44, Attachment 4) will also be removed by pressure washing.

A closure report will be prepared with the general information listed on the Closure Report Checklist, analytical data from the rinsate analyses. Soil sample data are required for release determination and closure of WMUs that are below ground or in direct contact with the ground surface. The table below also lists soil borings that will be used for the release determination.

NOR Unit Facility ID Location Boring

Locations Analytical Suite

001 Sump Between Safe Wash and Drum Cleaning Buildings

4904-SB04 / MW-01

RCRA VOCs, and RCRA SVOCs, acetone, 1,2-dichlorobenzene, ethylbenzene, methyl isobutyl ketone,

methylene chloride, 1,1,1-trichloroethane, 1,1,2-trichloroethane, 1,1,2-trichloro-1,2,2-trichloroethane,

trichlorofluoromethane, xylenes (See Table 1)

006 Oil/water separator

Between Safe Wash and Drum Cleaning Buildings

4904-SB04 / MW-01 TPH

130 Concrete containment

Inside Equipment/Fleet Maintenance Building

4904-SB22 / 4904-SB23 pH, TPH

131 Concrete containment

Inside Drum Cleaning Building

4904-SB04 / MW-01 pH, TPH


2.4 Tanks

This section describes the closure process for tanks listed on the NOR. Wastes were removed from the tanks during the EPA emergency removal action and the tanks were rinsed (Moore, 2015). Section 1.2 describes the methodology for determining the analytical suite for the closure analyses. The tanks will be cleaned as described in Section 4.5. Samples will be collected from the final rinsates for the analytes listed in the table below. A closure report will be prepared with the general information listed on the Closure Report Checklist and analytical data from the rinsate analyses. NOR Unit Facility ID Location Analytical Suite

004 Steel tank Inside Equipment & Fleet Maintenance Building (north side)

Not present. Close by cleaning concrete floor and trenches 1 and 2. Analyze rinsates for pH, TPH

007 pH adjustment unit Inside Safe Wash Building Not present. Close by cleaning concrete floor and trenches.

Analyze rinsates for pH, TPH

008 2 50-gal Inside Truck Maintenance Building (southeast corner) Close by cleaning concrete floor. No analytical

101 Vacuum box South side of Equipment & Fleet Maintenance Building Not present; no analytical





102 Wastewater Two plastic tanks south of

Equipment & Fleet Maintenance Building

pH, TPH

108 Wastewater treatment plant

North end of Main Processing Building

Flashpoint, RCRA VOCs, benzene, tetrachloroethene, methylene chloride, trichloroethene, 1,1,1-trichloroethane, chlorobenzene, 1,1,2-trichloro-1,2,2-trifluoroethane, 1,2-

dichlorobenzene, trichlorofluoromethane, 1,1,2-trichloroethane, xylene, acetone, ethylbenzene, methyl

isobutyl ketone (Table 1); TPH

109 Wastewater Treatment Plant

Neutralization tank between Safe Wash and Drum Cleaning Building

Not present; Close by cleaning concrete flow and trenches in Safe Wash building area. Analyze rinsates for pH, TPH

110 Tank T1 WWTP – north end Main Processing Building pH, TPH (See WWT 1/4/5 + Vat on Tables 4 and 5)

111 Tank T2 WWTP – north end Main Processing Building pH, TPH (no EPA data)

112 Tank T3 WWTP – north end Main Processing Building pH, TPH (See WWT3 on Tables 4 and 5)



115 Tank T6 WWTP – north end Main Processing Building pH, TPH (See WWT 6/7/8 on Tables 4 and 5)



118 Tank T9 WWTP – north end Main Processing Building

Arsenic, barium, cadmium, chromium, lead, mercury, silver (See Table 1) (See WWT 9/10/12 on Tables 4 and 5)



120 Tank T11 WWTP – north end Main

Processing Building Arsenic, barium, cadmium, chromium, lead, mercury, silver

(See Table 1) (See WWT 9/10/12 on Tables 4 and 5)



122 Water Solids

Separator (WSS1)

WWTP – north end Main Processing Building

Arsenic, barium, cadmium, chromium, lead, mercury, silver, TPH (See Table 1) (Labeled as “vat” on Tables 4 and 5)

123 Tank wash West side of Equipment and Fleet Maintenance Building Benzene, mercury, TPH (See WMU-123 on Tables 4 and 5)

126 Clarification / Settling Tank

Outside Main Processing Building adjacent to interior WWTP pH, TPH (See FT-1001 on Tables 4 and 5)


Outside Main Processing Building adjacent to interior WWTP

2-Methylphenol, 3&4-methylphenol, pH, TPH (See FT-1004 on Tables 4 and 6)


Outside Main Processing Building adjacent to interior WWTP pH, TPH (See FT-1002 on Tables 4 and 5)





129 Wastewater tank Unknown Not present; None

132 Clarification / Settling Tank Unknown Not present; None







139 Never Built Unknown Not present; None 140 Never Built Unknown Not present; None





3.0 OTHER WASTE UNITS

This section discusses the closure process for sumps, trenches, and tanks that may have been in contact with waste materials but were not listed on the NOR. Attachment 4 contains the photolog for the remaining waste units that are not listed on the NOR.

3.1 Sumps and Trenches

Sumps were numbered during Site reconnaissance activities and are not associated with any regulatory document. Table 3 summarizes the sump dimensions (where known). Sumps and trenches will be cleaned as described in Section 4.4. Rinsate samples will be analyzed for pH and TPH. Sumps and trenches will be backfilled as described in Section 4.7. Soil sample data are required for release determination and closure of WMUs that are below ground or in direct contact with the ground surface. The table below also lists sample locations from the affected property assessment associated with each sump that will be used for the release determination.

Sump Sump Location Sample Location Boring Location

2 Safe Wash 4904-SB04 MW-01 Between Safe Wash and Drum Cleaning Building

3 Safe Wash 4904-SB04 MW-01 Between Safe Wash and Drum Cleaning Building

5 Inside Drum Cleaning Building 4904-SB04 MW-01 Inside Drum Cleaning Building

6 Drive in front Drum Cleaning Building 4904-SB05 Southeast of drum cleaning building between sumps 6 and 7

7 Drive in front Drum Cleaning Building 4904-SB05 Southeast of drum cleaning building between sumps 6 and 7

9 Equipment/Fleet Maintenance 4904-SB23 Between equipment/fleet maintenance building and WMU 123

10 Between Drum/Tote area and South Tank Farm 4904-SB15 North side of drum/tote area / south side of south tank farm

12 Outside west side Main Processing building WWTP 4904-SB24 Outside west side of Main Processing Building

13 Outside west side Main Processing building WWTP 4904-SB24 Outside west side of Main Processing Building

14 Main Processing Building WWTP 4904-SB02 In north bay at Trench 6 inside Main Processing Building

16 Welding Shop 4904-SB10 West of sump in ramp near southwestern corner of Site

17 East side adjacent to Drum Tote area 4904-SB14 East side of drum/tote storage area

18 East side Drum/Tote area inside 4904-SB14 East side of drum/tote storage area

19 West side Drum/Tote area inside 4904-SB13 West side of drum/tote storage area

20 Between North and South Tank Farm 4904-SB18 North side of south tank farm and south of north tank farm

21 Inside North Tank Farm 4904-SB18 North side of south tank farm and south of north tank farm

22 Inside South Tank Farm 4904-SB18 North side of south tank farm and south of north tank farm

23 Outside southwest side Main Processing Building None None




3.2 Tanks

Waste samples were collected from tanks during the EPA emergency removal action. Tables 5 and 6 summarize the EPA waste data. Section 1.2 describes the methodology for determining the analytical suite for the closure analyses. The tanks will be cleaned as described in Section 4.5. Samples will be collected from the final rinsates for the analytes listed in the table below. A closure report will be prepared with the general information listed on the Closure Report Checklist and analytical data from the rinsate sample analyses.

Facility ID Tank Analytical Suite North Tank Farm OT1 pH, TPH (No EPA data) North Tank Farm OT2 Benzene, mercury, TPH (See OT-2 on Tables 4 and 5) North Tank Farm OT3 1,2-Dichloroethane, benzene, TPH (See OT-3 on Tables 4 and 5) North Tank Farm OT4 Benzene, TPH (See OT 4/5 on Tables 4 and 5) North Tank Farm OT5 Benzene, TPH (See OT 4/5 on Tables 4 and 5) North Tank Farm OT6 Benzene TPH (See OT6 on Tables 4 and 5) North Tank Farm OT7 Hazardous: Benzene, mercury, TPH (See N. Tank 7 on Tables 4 and 5) North Tank Farm OT8 Hazardous: Benzene, pyrene TPH (See N. Tank 8 on Tables 4 and 6) North Tank Farm OT9 Hazardous: Benzene, lead, TPH (See N. Tank 9/10 on Tables 4 and 6)

Tanker Trailer 407 Next to North Tank Farm TPH (See CES-CS-Tank 407 on Tables 4 and 5)

Tanker Trailer 408 Next to North Tank Farm Chromium, lead TPH (See CES-CS-Tank 408 on Tables 4 and 5)

South Tank Farm South Tank 1 Hazardous: pH, chromium, lead, mercury, benzene; TPH (See S. Tank 1/3/6 on Tables 4, 5 and 6)

South Tank Farm South Tank 2 Hazardous: benzene; tetrachloroethene, trichloroethene, TPH (See S. Tank 2 on Tables 4 and 5)


South Tank Farm South Tank 4 pH, TPH (No EPA data) South Tank Farm South Tank 5 Benzene, TPH (See S. Tank 5 on Tables 4, 5, and 6)


South Tank Farm South Tank 7 Hazardous: pH; antimony, benzene; lead, mercury, TPH (See Tables 4 and 5) South Tank Farm South Tank 8 Benzene, TPH (See S. Tank 8 on Tables 4 and 5) South Tank Farm South Tank 9 pH, TPH (No EPA data) Main Processing

Building Lime Tank pH, TPH (No EPA data)

Main Process Building

Unnumbered Poly Tanks pH, TPH (No EPA data)

Office Building FT5180 pH, TPH (See FT5180 on Table 4)




4.0 CLOSURE ACTIVITIES

This section describes the field and reporting activities for closing the WMUs in accordance with the guidance in the Closure Report Checklist. Upon completion of this project, the WMUs will be free of waste and cleaned to allow, in conjunction with soil data developed during the affected property assessment, regulatory closure. The objectives are to sufficiently clean container storage areas, sumps, and trenches such that future contact storm water would not expected to be contaminated and to allow tanks to be sold or demolished by the trustee. The pressure washing and associated waste removal will be performed by a contractor selected by the CES Griggs Road PRP Group.

4.1 Safety

A health and safety plan (HASP) specific to the activities of this closure project will be prepared by the contractor prior to mobilization. The contractor will be provided with a copy of this closure plan, including the analytical data, to aid in HASP preparation. At a minimum, the contractor’s HASP for the cleaning and sampling activities will need to address OSHA requirements in accordance with 29 CFR 1910.120, including but not limited to:

1. Level of personal protective equipment (PPE) for tasks

2. Working at heights

3. Confined space entry

4. Air monitoring

All site workers shall be trained to the appropriate level according to 29 CFR 1910.120 for their job functions and responsibilities.

At a minimum, the PPE should include Level D PPE protection (i.e., hardhat, safety glasses, steel toe shoes, earplugs, and long sleeve shirt/pants). The criteria for upgrading PPE to Level C shall- be included in the HASP. Personnel SHALL have a functional personal hydrogen sulfide monitor worn in the breathing space. PPE will be upgraded to Level C as needed based on readings from the 4-gas meters and hydrogen sulfide monitors. Stop work will be employed if monitoring indicates the need for OSHA Level B PPE.

To the extent possible, all cleaning and sampling activities will be performed at ground level. If the tanks cannot be accessed from the ground, personnel will use a man lift or scaffolding with appropriate fall protection. Existing ladders and railings will not be relied on to access tanks.

Tank cleaning and sampling activities will be considered confined space entries. The contractor’s HASP shall provide the criteria for non-permit and permit confined space entries. Continuous air monitoring of confined space entries will be performed using a 5-gas meter.

At a minimum, air monitoring with a 5-gas meter and photoionization detector (PID) will be performed by the contractor after breaking bolts but prior to opening manways or sampling points (if tank does not have an existing opening). The air monitoring will be repeated immediately after removing the manway or sample point. Air monitoring will also be performed at the edge of existing tank openings prior to cleaning. Routine air quality monitoring of the work area will be performed using a 5-gas meter (carbon dioxide, methane, oxygen, carbon monoxide, and hydrogen sulfide) and a PID for volatile organic




compounds. The contractor should review existing information to evaluate the need for additional air monitoring / sampling activities.

In addition to worker health and safety monitoring, perimeter monitoring air monitoring with PID along the nearest fenceline will be conducted periodically. If sustained readings (more than one minute) of 10 ppmv or higher are measured at the perimeter monitoring locations, work activities upwind of that location will cease. Monitoring will be performed at the location every five minutes for 15 minutes. If readings continue to be greater than or equal to 10 ppmv, all activities will stop until the elevated readings are reduced to less than 10 ppm (sustained). PID readings will be recorded in the daily field records.

4.2 Pressure Washing

Following the removal of liquids and waste materials, the contractor will pressure wash the storage areas, sumps, tanks, and piping as described below. Tanks and other equipment will be pressure washed from existing openings. CSAs, sumps, and trenches will be pressure washed at ground surface. Pressure washing consists of two passes of a greater than 3,000 psig pressure washer and lance. Personnel performing the washing will wear a minimum of OSHA Level D PPE with the addition of a face shield. The HASP will specify conditions for upgrading PPE and the contractor is responsible for monitoring conditions.

4.3 CSA Cleaning and Documentation

CSAs will be cleaned prior to rinsate sampling using the process described below. In addition, this procedures will be used to clean the concrete floors in the warehouses.

1. Remove debris, piping or trash from CSA and stage as designed by oversight personnel.

2. Photograph and document the condition (stains, cracks, etc.) of the CSA prior to cleaning.

3. Pressure wash the CSA to remove surficial materials.

4. Containerize wash water for disposal in “Aqueous Liquid” frac tank.

5. Photograph and document the condition of the CSA after cleaning.

6. Lightly wash the CSA and collect rinsate samples for the analyses specified in Section 2.

4.4 Sump / Trench Cleaning and Documentation

Table 3 summarizes the dimensions (where known) of the sumps and trenches. The order of cleaning will be based on location and presumed order of drainage (i.e. south to north). In order to provide a collection point for rinsate water, sumps will be cleaned and closed last in each area.

According to EPA, sumps and trenches were pressure washed at the end of the emergency removal action (Moore, 2015). Sumps and trenches will be cleaned prior to rinsate sampling using the following process.

1. Photograph sump or trench and surface of liquids.




2. Place a small amount of the liquid from the surface of the sump or trench into a test tube. Add water to check miscibility of waste liquid with water. Check pH of the liquid.

3. Pump liquids out and place in frac tank.

a. If the waste liquid is miscible with water and pH greater than 2 or less than 12.5 units, place waste liquid in the “Aqueous Liquid” frac tank.

b. If the waste liquid is not miscible with water, place waste liquid in the “Non-aqueous Liquid” container.

c. If the pH of the waste liquid is less than 2 or greater than 12.5 units, place waste liquid in the “Acidic Liquid” or “Caustic Liquid” container, respectively.

4. Photograph and document the condition of the sump or trench (stains, cracks, etc.). Document the presence (approximate size and location) or absence of piping exiting the sump. Plug piping exiting the sump or trench.

5. Pressure wash the sump or trench. If the liquids in the sump or trench were miscible with water and the pH greater than 2 or less than 12.5 units, place rinsates water in the “Aqueous Liquid” frac tank.

6. Repeat step 2 to determine appropriate storage container for rinsates if the liquids in the sump or trench were not miscible with water or the pH was less than 2 or greater than 12.5 units. If rinse liquids are not miscible or pH is less than 2 or greater than 12.5 units, repeat process until rinse liquids are miscible and/or pH is between 2 and 12.5.

7. Re-rinse the sump and collect a rinsates sample for the analyses specified in Sections 2 or 3.

8. Cover outdoor sumps to prevent the accumulation of storm water.

9. Upon receipt of acceptable analytical data, backfill the sump or trench as described in Section 4.4

4.5 Tank Cleaning and Decontamination

According to EPA, tanks were pressure washed at the end of the emergency removal action (Moore, 2015). However, piping remains attached to many of the tanks and may contain waste materials. Prior to tank cleaning, accumulated liquids will be removed from the containment areas to a depth of less than 1-inch. Tanks will be cleaned prior rinsate sampling by the process described below.

1. Remove piping.

2. Pressure wash the interior of the piping.

3. Pressure wash the interior of the tank.

4. Collect a sample for the analyses specified in Sections 2 or 3.

5. Place the excess rinsate in the “Aqueous Liquid” frac tank.

6. Record physical characteristics of rinsates (color, odor, etc.).




4.6 Storage, Transportation and Disposal

Liquid and solids wastes will be segregated by media. Oily wastes will be segregated from other aqueous or solid materials. Samples will be collected from the liquids contained in the frac tanks and characterized for disposal. Liquid and solid waste analyses will include RCRA metals plus antimony, beryllium, and nickel, RCRA VOCs, and TPH.

Hazardous wastes will be stored in tanks or containers and disposed of within 90 days of generation. Upon receipt of the analytical results, the contractor will prepare a waste profile and obtain approval for shipment of the wastes to the designated disposal facility. In addition, the contractor shall complete a TCEQ One-Time Shipment Request for Texas Waste Code for Shipment of Hazardous and Class 1 Waste (TCEQ Form 0757) and/or other applicable forms.

Waste materials will be transported to the designated disposal facility by the contractor. Transportation will comply with applicable state and federal regulations, including U.S. Department of Transportation (DOT) regulations in 49 CFR 173 and 179 and placarded requirements in 40 CFR 172. The contractor shall use only permitted waste haulers.

Aqueous wastes will be sent to the Intergulf facility in Pasadena, Texas. Used PPE and debris generated by the project will be collected in a roll-off box for shipment to the Waste Management Coastal Plains Landfill in Alvin, Texas. Alternatively, the Seabreeze Environmental Landfill in Angleton, Texas or the Waste Management Conroe Landfill in Conroe, Texas may be acceptable. The contractor will review the analytical data and recommend an appropriate disposal facility for the PRP group approval.

Manifests and bills of lading will be provided to the group in the monthly invoices. The contractor shall notify the group if the disposal facility copy of the signed manifests is not returned within 30 days. Certificates of destruction/treatment are required from any disposal facilities utilizing treatment or destruction technologies.

4.7 Backfill

Common fill will be obtained from an off-site source. Common fill typically has a high clay content and is used in applications that do not have an engineering specification. Prior to use, a sample from the fill source will be analyzed for metals, volatile organic compounds (VOCs), semivolatile organic compounds (SVOCs), and TPH. In order to be acceptable for use as fill, analyte concentrations must be less than the commercial/industrial PCLs. The sump or trench will be photographed after backfilling.

4.8 Analytical Data

Rinsate samples will be collected from the WMUs as described above. Analyte concentrations less than the commercial/industrial PCLs for the ingestion of groundwater (GWGWIng) will demonstrate that all waste has been removed from the WMU.

As discussed in the Closure Report Checklist (Attachment 1), soil data generated during the affected property assessment (CES, 2016) will be used to demonstrate that a release from the WMU to the environment has not occurred. Soil data will be compared to the 0.5-acre residential PCLs, as described in the memorandum “Determining which Releases are Subject to TRRP” (TCEQ, 2010), to determine if the WMU had a release subject to TRRP.




4.9 Reporting

Closure reports will be prepared for submitted to the TCEQ Remediation Division and Region 12. It is anticipated that two closure reports will be submitted. One closure report will include the rinsate and soil data for WMUs which do not have a release to the environment as defined in the guidance memorandum “Determining which Releases are Subject to TRRP” (TCEQ, 2010). The second closure report will include the rinsates and soil data for WMUs which had releases to the environment. Based on soil concentrations from the APAR data exceeding the 0.5-acre residential standard, the WMUs with a potential release to the environment are listed below.


Locations Chemical of Concern

108 Wastewater treatment plant North end of Main Processing Building 4904-SB02 TPH

110 Tank T1 WWTP – north end Main Processing Building 4904-SB02 TPH












None Sump 14 WWTP – north end Main Processing Building 4904-SB02 TPH

006 Oil/water separator Between Safe Wash and Drum Cleaning Buildings

4904-SB04 / MW-01 Chlorinated VOCs

131 Concrete containment Inside Drum Cleaning Building 4904-SB04 / MW-01 Chlorinated VOCs

None Sump 1 Safe Wash 4904-SB04 MW-01 Chlorinated VOCs






Locations Chemical of Concern


None Sump 5 Inside Drum Cleaning Building 4904-SB04 MW-01 Chlorinated VOCs

None Sump 10 North side of drum/tote area / south side of south tank farm 4904-SB15 TPH


Both closure reports will contain the following information:

1. Owner/operator information and NOR;

2. Location of facility;

3. Map of the facility showing the WMU location;

4. Description of the WMU, including NOR number, construction, condition, operational history and wastes managed (to the extent that information is available from TCEQ documents), waste characterization results (if available from EPA removal action), waste spill(s) and cleanup response(s) (to the extent that information is available for a specific WMU);

5. Reason for WMU closure;

6. Demonstration of how WMU was closed and demonstrated to not have released to the environment (using data gathered during the affected property assessment and closure work);

7. Photographs with descriptions of the WMU before, during, and following closure;

8. Description of rinsates samples, laboratory reports, and summary table of analytical results; and

9. Description of the WMU waste disposition (from closure), including copies waste manifests.

The closure reports will also include the relevant APAR data for the soil borings drilled adjacent to the sumps.




5.0 REFERENCES

CES Griggs Road PRP Group. (CES). 2016. Affected Property Assessment Report (APAR) for CES Griggs Road VCP Site. 4900 Griggs Road, 4904 Griggs Road, and 5910 Wayland Street (VCP No. 2751; CN604824904; RN108370644)

Harris County Appraisal District. 2015. Record for Account Number. http://www.hcad.org/records.

Moore, Gary (Moore). 2015. Email communication from Gary Moore (EPA On-Scene Coordinator) to Brenda Basile (PBW). Progress report dated June 3, 2015.

Texas Commission on Environmental Quality (TCEQ). 2009. CES Environmental Services Compliance Investigation 707234. November 5, 2008 to June 30, 2009.

Texas Commission on Environmental Quality (TCEQ). 2010. Determining Which Releases are Subject to TRRP. November 19, 2010. https://www.tceq.texas.gov/assets/public/remediation/trrp/releasesTRRPrev.pdf

Texas Commission on Environmental Quality (TCEQ). 2011. TCEQ Remediation Division Closure Report Checklist Revised July 28, 2011. https://www.tceq.texas.gov/assets/public/remediation/corrective_action/ENCLOSURE%20-%20Closure%20Report%20Checklist.pdf

Texas Commission on Environmental Quality (TCEQ). 2012. Notice of Registration dated March 6, 2012. http://www15.tceq.texas.gov/crpub/index.cfm?fuseaction=iwr.viewdocument&doc_name=IHW%5FNOR%5FFACREG30900&doc_id=345336232012075&format_cd=PDF. Retrieved August 15, 2015.

Texas Commission on Environmental Quality (TCEQ). 2014. Justification Assessment for State Funded Cleanup. September 26, 2014.

Texas Commission on Environmental Quality (TCEQ). 2015. TCEQ Central Registry Query – Regulated Entity Information. Query Dated September 12, 2015.

Texas Commission on Environmental Quality (TCEQ). 2016a. Petroleum Storage Tanks Registration 32061 1986-1998. Retrieved by TCEQ Central Files on February 19, 2016.

Texas Commission on Environmental Quality (TCEQ). 2016b. Protective Concentration Levels. March 4, 2016. http://www.tceq.state.tx.us/remediation/trrp/trrppcls.html.

Texas Natural Resource Conservation Commission (TNRCC). 1998. Suttles Truck Leasing Compliance Evaluation Inspection. June 23, 1998.

TGE Resources, Inc. (TGE). 2011. Phase II Environmental Site Assessment, Holiday Place Townhome Lots, East of Calhoun Road and South of Griggs Road, Houston, Harris County, Texas. January 4, 2011.

The WCM Group (WCM). 1996. Phase I and Limited Phase II Environmental Site Assessment for the Evaluation of Recognized Environmental Conditions at Younger Brothers, Inc. Truck Terminal. September 27, 1996.



Project No.4014 September 2016

TABLES




Table 1 RCRA Waste Codes Associated with Hazardous Waste Management Units

RCRA Waste Code Parameter NOR

001 NOR 002

NOR 003

NOR 105

NOR 108

NOR 119

NOR 120

NOR 121

NOR 122

D001 Flammability √ √ D002 Corrosivity √ √ D003 Reactivity √ D004 Arsenic √ √ √ √ √ D005 Barium √ √ √ √ √ D006 Cadmium √ √ √ √ √ D007 Chromium √ √ √ √ √ D008 Lead √ √ √ √ √ D009 Mercury √ √ √ √ √ D010 Selenium √ D011 Silver √ √ √ √ √ D012 Endrin √ D013 Lindane (g-BHC) √ D014 Methoxychlor √ D015 Toxaphene √ D016 2,4-D √ D017 2,4,5-TP √ D018 Benzene √ √ D020 Chlordane √ √ √ D021 Chlorobenzene √ √ √ D022 Chloroform √ √ √ D023 o-Cresol √ D024 m-Cresol √ D025 p-Cresol √ D026 Total Cresol √






001 NOR 002

NOR 003

NOR 105

NOR 108

NOR 119

NOR 120

NOR 121

NOR 122

D027 1,4-Dichlorobenzene √ √ √ D028 1,2-Dichloroethane √ √ √ D029 1,1-Dichloroethene √ √ √ D030 2,4-Dinitrotoluene √ D031 Heptachlor (and epoxide) √ √ √ D032 Hexachlorobenzene √ √ √ D033 Hexachlorobutadiene √ √ √ D034 Hexachloroethane √ √ √ D035 Methyl ethyl ketone (2-Butanone) √ D036 Nitrobenzene √ D037 Pentachlorophenol √ √ √ D038 Pyridine √ D039 Tetrachloroethene √ √ √ D040 Trichloroethene √ √ √ D041 2,4,5-Trichlorophenol √ √ √ D042 2,4,6-Trichlorophenol √ √ √ D043 Vinyl chloride √

F001 Spent halogenated solvents: tetrachloroethene, trichloroethene, methylene chloride, 1,1,1-trichloroethane, carbon tetrachloride, chlorinated fluorocarbons √ √ √

F002 Spent halogenated solvents: tetrachloroethene, methylene chloride, trichloroethene, 1,1,1-trichloroethane, chlorobenzene, 1,1,2-trichloro-1,2,2-trifluoroethane, 1,2-dichlorobenzene,

trichlorofluoromethane, 1,1,2-trichloroethane √ √ √ √

F003 Spent non-halogenated solvents: xylene, acetone, ethyl acetate, ethylbenzene, ethyl ether, methyl isobutyl ketone (4-methyl-2-pentanone), n-butanol, cyclohexanone, methanol √ √ √ √

F004 Spent non-halogenated solvents: cresols and cresylic acid, nitrobenzene √ √ √






001 NOR 002

NOR 003

NOR 105

NOR 108

NOR 119

NOR 120

NOR 121

NOR 122

F005 Spent non-halogenated solvents: toluene, methyl ethyl ketone (2-butanone), carbon disulfide, isobutanol, pyridine, benzene, 2-ethoxyethanol, 2-nitropropane √ √ √

F034 Wastewaters, process residuals, preservative drippage, and spent formulations from wood preserving processes generated at plants that use or used chlorophenolic formulations √

U002 Acetone √ U031 n-Butanol √ U037 Chlorobenzene √ U118 Ethyl methacrylate √ U154 Methanol √ U162 Methyl methacrylate √ U165 Naphthalene √ U220 Toluene √ U223 Toluene diisocyanate √ U239 Xylene √ U359 2-Ethoxyethanol √




Table 2 Notice of Registration (NOR) Waste Management Units

NOR Unit

Unit Type Facility ID Process Waste Codes Volume

or Area Soil Boring Original Location/Comment

001 Sump None Status date 1/22/1991 (Younger); Texas hazardous waste code 9014206H (halogenated hydrocarbons) See Table 1 4.6 ft3 4904-SB04 4904-SB26

Between Equipment Cleaning/Drum Cleaning Building and New Shop/Truck Maintenance Building (Figure 3)

002 MSC None (Hazardous Waste) Closure request 1/8/2007; storage bulking; waste codes 9014206H, 0004102H See Table 1; Class 1 250 ft2 4904-SB22 South side of Equipment & Fleet Maintenance Building (Figure 3)

003 CSA Old Wash Rack Closure request 8/24/2006; Waste management unit for miscellaneous 55-gallon drums; Texas hazardous waste code 0016219H See Table 1; Class 1 2,500 ft2 4904-SB04

4904-SB26 Northwest corner of Safe Wash Area (Figure 3)

004 Tank Steel tank Closure request 8/24/2006; steel tank; non-hazardous waste oil, spent diesel fuel; lube oils and additives Class 1; TPH 500 gal 4904-SB22 Inside Equipment & Fleet Maintenance Building; not present; capacity 6/17/2011 NOR

005 MSC Dumpster Closure request 8/24/2006; 7 – 15 cubic yard dumpster; non-hazardous plant refuse and oil/water separator solids Class 1; Class 2 15 cy TSB-3 TGE 2011 West of Wayland Street right of way; no dumpsters currently at Site

006 Sump Oil/water separator Closure request 8/24/2006; non-hazardous oil/water separator solids Class 1 Unknown 4904-SB04 4904-SB26 Between Safe Wash and Drum Cleaning Buildings

007 Tank pH adjustment unit Closure request 8/24/2006; nonhazardous first flush from tank washes Class 1; Class 2 2,500 ft2 4904-SB04 4904-SB26 Inside Safe Wash Building (Figure 3)

008 Tank 2 50-gal Closure request 8/24/2006; non-hazardous used oil Class 1; TPH 2x50 gal 4904-SB22 Southeast corner of Truck Maintenance Building; no 50-gallon tanks at Site (Figure 3)

009 MSC CSA Closure request 8/24/2006; non-hazardous used oil filters and rags contaminated with petroleum products Class 1; TPH Unknown

101 Tank Vacuum box Located in tank wash; non-hazardous first flush from tank washes Class 1 1,000 4904-SB21 South of Equipment & Fleet Maintenance Building; no vacuum boxes currently at Site; location of 2 tanker trailers; capacity 6/17/2011 NOR

102 Tank Wastewater Closure request 1/8/2007; non-hazardous wastewater tank; non-RCRA rinse water of RCRA empty containers Class 1 4,000 4904-SB21 South of Equipment & Fleet Maintenance Building; volume based on 6/17/2011 NOR(non-hazardous wastewater tank)

103 MSC Sludge box Non-hazardous sludge removed from tanks and totes Class 1 25 cy 4904-SB04 Safe Wash Area; no sludge boxes at Site; capacity 6/17/2011 NOR

104 MSC Open top box Open top box for plant trash Class 2 40 cy Roll-off south of Drum Cleaning Building; no roll-offs at Site; capacity 6/17/2011 NOR

105 CSA Hazardous waste CSA Removal of unused products from tank/tote management services and solids from cleaning totes, tanks roll-off

boxes, vacuum boxes, and tanker trucks; Texas hazardous waste codes: 9005609H, 9010609H, 9011110H, 9012105H, 9013409H, 9014206H, 9015519H, 9025403H, 9029319H

See Table 1 250 ft2 4904-SB22 Outside Equipment and Fleet Maintenance Building

106 CSA Permit Unit No. 1 Storage and processing nonhazardous waste in drums or other containers; 50 ft.x70 ft. area within 210 ft. x70 ft. metal building; capacity 500 55-gallon drums Class 1; Class 2 3,500 ft2

27500 gal 4904-SB03 South part of Main Processing Building

107 CSA Permit Unit No. 2 Storage and processing nonhazardous waste in roll-off boxes or other containers; 122 ft. x 70 ft. area within 210 ft. x70 ft. metal building; capacity four 25-cy rolloffs Class 1; Class 2 1,540 ft2

100 cy 4904-SB02 4904-SB03 Middle portion of Main Processing Building

108 Tank Permit Unit No. 3 Tank in wastewater treatment system consisting of tank, filter presses, ion-exchange unit, reverse osmosis, and

sumps. 38 ft. x 70 ft. area within 210 ft. x70 ft. metal building. Texas hazardous waste codes: 9027207H, 9030601H

See Table 1; Class 1; Class 2 6,500 gal 4904-SB04

4904-SB26 North end of Main Processing Building; capacity 6/17/2011 NOR

109 WWTP WW treatment system consisting of flow equalization, free oil removal, precipitation, and pH adjustment; tank truck cleaning Class 1; Class 2 4900-SB03

4904-SB02 Neutralization tank between Safe Wash and Drum Cleaning

110 Tank Tank T1 Oil recovery, phase separation, and neutralization – industrial wastewater treatment Class 1 4900-SB03 4904-SB02 WWTP – north end Main Processing Building

111 Tank Tank T2 Oil recovery, phase separation, and clarification – industrial wastewater treatment Class 1; Class 2 4900-SB03 4904-SB02 WWTP – north end Main Processing Building







Table 2 Notice of Registration (NOR) Waste Management Units

NOR Unit

Unit Type Facility ID Process Waste Codes Volume

or Area Soil Boring Original Location/Comment


116 Tank Tank T7 Oxidation, biotreatment, organic separation from water – industrial wastewater treatment None 4900-SB03 4904-SB02 WWTP – north end Main Processing Building



119 Tank Tank T10 Precipitation dissolved metals, neutralization acids/bases, settling suspended solids – industrial wastewater treatment; Texas hazardous waste code 9019519H

See Table 1; Class 1; Class 2 4900-SB03

4904-SB02 WWTP – north end Main Processing Building







122 Tank Water Solids Separator Phase separation, clarification, and solids settling – industrial wastewater treatment; Texas hazardous waste code 9019519H



123 Tank Tank wash Tank wash sump water None 20,000 gal 4904-SB23 Tank west of Equipment/Fleet Maintenance Building; capacity 6/17/2011 NOR

126 Tank Clarification / Settling Tank Frac tank FT1001 Class 1; Class 2 4904-SB01 Outside Main Processing Building adjacent to interior WWTP; current location south of office building

127 Tank Clarification / Settling Tank Frac tank FT1002 Class 1; Class 2 4904-SB01 Outside Main Processing Building adjacent to interior WWTP; current location south of office building

128 Tank Clarification / Settling Tank Frac tank FT 1004 Class 1; Class 2 4904-SB01 Outside Main Processing Building adjacent to interior WWTP; current location south of office building

129 Tank Wastewater tank Class 1; Class 2 Unknown

130 Sump Concrete containment Concrete containment area with sump that holds truck wash rinse water Class 1; Class 2 4,500 gal 4904-SB22 4904-SB23

Inside Equipment/Fleet Maintenance Building; capacity based on 6/17/2011 NOR

131 Sump Concrete containment Concrete containment area with sump that holds drum cleaning wash water Class 1 1,500 gal 4904-SB04 4904-SB26 Inside Drum Cleaning Building; capacity based on 6/17/2011 NOR

132 Tank Clarification / Settling Tank Class 1; Class 2 20,000 gal Capacity based on 6/17/2011 NOR 133 Tank Clarification / Settling Tank Class 1; Class 2 20,000 gal Capacity based on 6/17/2011 NOR 134 Tank Clarification / Settling Tank Class 1; Class 2 20,000 gal Capacity based on 6/17/2011 NOR 135 Tank Clarification / Settling Tank Class 1; Class 2 20,000 gal Capacity based on 6/17/2011 NOR 136 Tank Clarification / Settling Tank Class 1; Class 2 20,000 gal Capacity based on 6/17/2011 NOR 137 Tank Clarification / Settling Tank Class 1; Class 2 20,000 gal Capacity based on 6/17/2011 NOR 138 Tank Clarification / Settling Tank Class 1; Class 2 20,000 gal Capacity based on 6/17/2011 NOR 139 Tank Clarification / Settling Tank Class 1; Class 2 20,000 gal Frac tank not used; sent back to rental company 140 Tank Clarification / Settling Tank Class 1; Class 2 20,000 gal Frac tank not used; sent back to rental company

See Attachment 3 for unit photographs. CSA – Container storage area MSC – Miscellaneous storage container WWTP – Wastewater treatment plant

Table 3

Sump and Trench Dimensions


Identification Location

Length

(in)

Width

(in)

Depth

(in)

Diameter

(in)

Volume

(ft3)NOR ID Boring

Comment

Sump 14 03‐Main Processing Building 28 28 20 9 108 4904‐SB02

Trench 1 03‐Main Processing Building 390 22 15 74 106 4904‐SB03

Trench 2 03‐Main Processing Building 591 21 21.75 156 107 4904‐SB03

Trench 3 03‐Main Processing Building 318 21 11.5 44 107 4940‐SB02

Trench 4 03‐Main Processing Building 432 21.5 17 91 108 4904‐SB02

Trench 5 03‐Main Processing Building 282 21.5 12 42 None 4904‐SB03

Trench 6 03‐Main Processing Building 306 21.5 12 46 None 4904‐SB02

Sump 11 03‐Main Processing Building Outside Northwest 8.5 None None

Sump 15 03‐Main Processing Building Outside Southwest 8.5 None None

Sump 23 03‐Main Processing Building Back Outside South 62 18 1.0 None

Sump 12 03‐Main Processing Building Back Outside WWTP 27.5 27.5 39 17 None 4904‐SB24 Round

Sump 13 03‐Main Processing Building Back Outside WWTP 21 22 32 8.6 None 4904‐SB24

OWS 04‐Safe Wash No measurements 006 4904‐SB04 Oil/Water Separator

Sump 1 04‐Safe Wash 95 53 4.6 None 4904‐SB04 Round

Sump 2 04‐Safe Wash 23 23 19 5.8 None 4904‐SB04

Sump 3 04‐Safe Wash 72 48 48 96 None 4904‐SB04

Trench 1 04‐Safe Wash 243 14 12 24 103 4904‐SB04

Trench 2 04‐Safe Wash 154 14.75 12 16 103 4904‐SB04

Trench 3 04‐Safe Wash 244 14.75 12 25 103 4904‐SB04

Trench 4 04‐Safe Wash 70 14.75 12 7.2 103 4904‐SB04

Trench 5 04‐Safe Wash 60 12 22 9.2 103 4904‐SB04

Sump 4 05‐Drum Cleaning 112 108 25 175 131 4904‐SB04

Sump 5 05‐Drum Cleaning 27.5 27.5 39 17 None 4904‐SB04

Sump 6 05‐Drum Cleaning Front Outside 21 21 32 8.2 None 4904‐SB05

Sump 7 05‐Drum Cleaning Front Outside 21 21 31 7.9 None 4904‐SB05

Sump 8A 07‐Equipment & Fleet Maintenance 37 101 84 182 130 4904‐SB23

Sump 8B 07‐Equipment & Fleet Maintenance 36.5 101 84 179 130 4904‐SB23

Sump 8C 07‐Equipment & Fleet Maintenance 37 101 84 182 130 4904‐SB23

Trench 1 07‐Equipment & Fleet Maintenance 458 15.25 11 44 None 4904‐SB23



Trench 4 07‐Equipment & Fleet Maintenance 458 15 15 60 105 4904‐SB22

Trench 5 07‐Equipment & Fleet Maintenance 144 15.5 12 16 105 4904‐SB22

Trench 6 07‐Equipment & Fleet Maintenance 457 15.5 15 61 105 4904‐SB22

Sump 9 07‐Equipment & Fleet Maintenance Front Outside 21 21 32 8.2 None 4904‐SB23

Sump 21 08‐North Tank Farm (inside) No measurements None 4904‐SB18

Sump 20 08‐North Tank Farm and 09‐South Tank Farm No measurements None 4904‐SB18

Sump 22 09‐South Tank Farm (inside) No measurements None 4904‐SB18

Sump 19 10‐Drum/Tote Storage ‐ SB13 inside No measurements None 4904‐SB13

Sump 17 10‐Drum/Tote Storage ‐ SB14 No measurements None 4904‐SB14

Sump 18 10‐Drum/Tote Storage ‐ SB14 inside No measurements None 4904‐SB14

Sump 10 10‐Drum/Tote Storage ‐ SB15 27 27 50 21 None 4904‐SB15

Sump 16 11‐ Welding Shop 18.5 18.5 12 2.4 None 4904‐SB10

SUM 1779

Length

(ft)

Width

(ft)

Depth

(ft)

Volume

(ft3)

08‐North Tank Farm Containment 80 55 2.5 11000 4904‐SB19/20/18 82000 gallons

09‐South Tank Farm Containment 55 55 3 9075 4904‐SB15/16/17/18 68000 gallons

Appears to be sanitary

sewer cleanouts

Building locations are shown on Figure 1. 1 Table 3 Sump and Drain Measurements.xlsx: Sheet1

Table 4Summary of Nonhazardous and Hazardous Waste Classification for Tanks - EPA Emergency Removal Action


Container Consistency Classification

Volume Estimate RCRA Codes

RCRA Codes Due to Matrix Interference

RCRA Codes Eliminated

Based Upon Totals Data

RCRA Codes Eliminated by EPA Houston

Lab

RCRA Code Eliminated by

Generator Knowledge

FT1001 Water Non HazardousFT1002 Water Non Hazardous D032 D032

FT1004 Oil HazardousD023, D024, D025, D026 D030, D032 D030, D032

FT5180 Oil/Oily WaterTT407 Non HazardousTT408 Non HazardousWMU123 Non Hazardous Sludge - Residual

NTank7 Hazardous D018NTank8 Hazardous D018 D032 D032NTank9_10 Comp Hazardous D018 D032 D032OT2 (Liquid Disposed) Non Hazardous Sludge - 1692OT3 Non Hazardous Sludge - ResidualOT4_OT5 Comp Non Hazardous D032 D032OT6 Non Hazardous Sludge - Residual

Non Hazardous D020 D020

Stank1 (STank1_3_6 Comp - Water/SludgHazardousD002(1.25/1.75),

D007, D018D020, D030, D032, D033

D020, D030, D032, D033

STank2 Hazardous D018 D032 D032

STank3 (split from 1,3,6 Comp) Hazardous D018 D020, D030, D032, D033

D002, D007, D032, D033

STank5 (Liquid Disposed) Non Hazardous Sludge - 12684

Stank6 (STank1_3_6 Comp - Water/SludgHazardousD002(1.25/1.75),

D007, D018D020, D030, D032, D033

D020, D030, D032, D033

STank7 Hazardous D002 (13.07)STank8 Non Hazardous D030, D032 D030, D032

WWT13 Non Hazardous 5637 D032 D032WWT3 Non Hazardous 5750WWT9_10_12 Comp Non Hazardous 18867 D032 D032WWT6_7_8 Comp Non Hazardous 18603 D032 D032WWT1_4_5_Vat Comp Non Hazardous 17702

Reference: EPA Removal Action Communication from Gary Moore

South AST Containment (Combined with FT 506/5180/1001)

Frac Tanks, Tanker Trailers, and Other Tanks

North Tank Farm

South Tank Farm

Wastewater Treatment Plant

1 Table 4 to 6 CES Data Waste Data.xlsx: Waste Classification

Table 5Summary of Waste Liquid Data

EPA Emergency Removal Action CES Griggs Road VCP Site

Texas Class 2 CES-CS-Tank 407

CES-CS-Tank 408 FT-1001 FT-1002 N-Tank 7 N. Tank

9/10 OT-2 OT-3 OT 4/5 OT-6 S. Tank 1/3/6 S. Tank 2 S. Tank 5 S. Tank 7 S. Tank 8 WMU-123 WWT 1/4/5

+ VAT WWT-3 WWT 6/7/8

WWT 9/10/12 WWT-13

Levels (mg/L 8/7/14 8/7/14 8/28/14 8/29/14 9/23/14 9/26/14 9/24/14 9/23/14 ###### 9/23/14 10/1/14 9/25/14 9/25/14 9/24/14 9/25/14 9/24/14 10/2/14 10/1/14 10/2/14 10/2/14 10/1/14

1,2,4-Trimethylbenzene NA NA NA 0.163 0.0032 J 46.3 2.28 18.6 62.5 9.09 15 17.9 33.7 3.83 3.64 58.1 4.10 < 0.0032 0.0669 < 0.0032 <0.0064 0.0102 J1,2-Dichloroethane 0.5 <0.018 <0.018 < 0.0018 <0.0018 <0.035 <0.018 <0.035 2.98 <0.0070 <0.034 <0.035 <0.088 <0.018 <0.034 <0.070 <0.035 < 0.0035 <0.0070 < 0.0035 <0.0070 <0.00701,3,5-Trimethylbenzene NA NA NA 0.0375 <0.0017 6.22 0.605 4.14 14.4 2.98 4.07 4.02 8.74 0.799 0.964 16.5 1.20 < 0.0035 0.0202 < 0.0035 <0.0069 <0.00692-Hexanone NA <0.130 <0.130 <0.013 <0.013 <0.260 <0.130 <0.260 <1.3 <0.051 <0.260 <0.260 <0.640 <0.130 <0.260 <0.510 <0.260 < 0.026 <0.051 < 0.026 0.0522 J <0.0514-Methyl-2-pentanone 200 <0.110 <0.110 < 0.011 <0.011 <0.220 0.399 J 3.79 <1.1 0.363 1.06 1.20 2.49 J 1.87 <0.220 9.94 <0.220 < 0.022 0.0480 J < 0.022 0.309 0.114 JAcetone 400 17.1 30.9 < 0.050 0.168 J 18.2 11.1 8.92 7.81 J 2.59 2.92 J 201 19.8 25.5 8.10 36.6 <1.0 0.152 <0.200 0.358 2.78 17.9Benzene 0.5 0.0319 J <0.017 0.019 <0.0017 34.2 15.7 4.92 23.7 0.737 7.04 2.99 8.76 0.830 0.285 2.02 0.931 < 0.0034 0.0115 J < 0.0034 <0.0068 <0.0068Carbon disulfide 400 <0.018 <0.018 < 0.0018 0.0045 J 0.0471 J <0.018 0.0481 J <0.180 0.098 0.106 <0.036 0.198 J <0.018 0.0447 J 37 <0.036 < 0.0036 <0.0072 0.0523 <0.0072 <0.0072Chlorobenzene 70 <0.013 <0.013 < 0.0013 <0.0013 <0.027 <0.013 0.0486 J 2.96 <0.0053 <0.027 <0.027 0.297 0.110 <0.027 20.1 <0.027 < 0.0027 <0.0053 < 0.0027 <0.0053 <0.0053Chloroform 6 <0.017 <0.017 < 0.0017 <0.0017 0.137 <0.017 0.179 1.13 0.229 5.33 0.420 2.09 <0.017 <0.035 <0.069 <0.035 < 0.0035 <0.0069 < 0.0035 0.0118 J <0.00692-Chlorotoluene NA NA NA < 0.0018 < 0.0018 < 0.0036 <0.018 < 0.036 < 0.18 < 0.0073 < 0.036 < 0.036 < 0.091 < 0.018 < 0.036 < 0.073 < 0.036 < 0.0036 <0.0073 < 0.0036 <0.0073 <0.0073Ethylbenzene 400 0.154 0.127 0.181 0.0033 J 11.7 3.19 50.4 27.3 2.93 11.4 15.8 33 2.00 49.6 48.5 3.73 < 0.0032 0.0168 J < 0.0032 <0.0065 <0.0065Isopropylbenzene NA NA NA 0.0116 <0.0020 4.58 0.186 41 5.33 0.511 2.85 1.41 5.16 0.329 1.19 6.69 0.834 < 0.0040 <0.0080 < 0.0040 <0.0080 <0.0080Methyl chloride NA <0.032 <0.032 < 0.0032 <0.0032 <0.063 <0.032 <0.063 0.363 J <0.013 <0.063 <0.063 <0.160 <0.032 <0.063 <0.130 <0.063 < 0.0063 <0.013 < 0.0063 <0.013 <0.013Methyl ethyl ketone 200 8.13 2.48 < 0.014 0.0471 J 21.3 4.95 18.6 1.93 J 0.593 6.53 56.7 42.2 23.2 12.5 <0.540 <0.270 0.0771 0.104 J 0.119 1.16 2.14Methyl tert-butyl ether NA NA NA < 0.0015 <0.0015 7.89 8.39 1.56 0.67 0.124 1.32 1.53 23.0 0.328 3.81 0.414 0.0817 J < 0.0030 0.0238 < 0.0030 <0.0060 0.0175 JMethylene chloride 50 <0.081 <0.081 < 0.0081 <0.0081 <0.160 <0.081 <0.160 <0.810 0.108 <0.160 0.182 J <0.410 <0.081 <0.160 <0.320 <0.160 < 0.016 <0.032 < 0.016 0.0413 J <0.032Naphthalene NA NA NA 0.172 0.0085 J 217 2.42 17 56.4 5.01 7.95 18.9 17.1 2.45 8.65 16.3 4.09 < 0.016 <0.031 < 0.016 <0.031 <0.031n-Butylbenzene NA NA NA 0.0212 <0.0020 2.62 0.313 5.54 14.4 1.04 1.52 <0.039 5.79 1.32 1.38 8.03 <0.039 < 0.0039 <0.0078 < 0.0039 <0.0078 <0.0078n-Propylbenzene NA NA NA 0.0179 <0.0018 3.54 0.343 2.27 9.10 1.41 2.13 2.19 4.68 0.373 0.452 6.93 0.324 < 0.0035 0.0070 J < 0.0035 <0.0070 <0.0070p-Isopropyltoluene NA NA NA 0.0034 <0.0018 0.752 0.0458 J 0.844 6.11 0.282 0.362 5.71 1.26 0.122 0.171 <0.073 0.70 < 0.0036 0.0093 J < 0.0036 <0.0073 <0.0073sec-Butylbenzene NA NA NA 0.003 <0.0023 1.01 0.0576 1.25 8.34 0.359 0.459 0.674 1.40 0.129 0.129 <0.091 0.202 < 0.0045 <0.0091 < 0.0045 <0.0091 <0.0091Styrene 700 0.129 <0.015 < 0.0015 0.0023 J 13.8 0.901 7.48 21.8 1.97 1.47 <0.029 6.33 0.396 <0.029 2.15 <0.029 < 0.0029 <0.0059 < 0.0029 <0.0059 <0.0059Tetrachloroethene 0.7 <0.023 <0.023 < 0.0023 <0.0023 0.124 <0.023 0.503 <0.230 0.123 0.186 0.165 1.14 0.028 J <0.046 <0.092 <0.046 < 0.0046 <0.0092 < 0.0046 <0.0092 <0.0092Toluene 1000 0.375 1.97 0.454 0.023 171 16 133 233 10.1 37.1 158 221 4.23 1.84 87.1 0.47 < 0.0033 0.0539 < 0.0033 0.0108 J <0.0065Trichloroethene 0.5 <0.024 <0.024 < 0.0024 <0.0024 <0.049 <0.024 0.0865 J 0.840 0.0122 J 0.0858 J <0.049 0.606 <0.024 <0.049 <0.098 <0.049 < 0.0049 <0.0098 < 0.0049 <0.0098 <0.0098Xylenes (Total) 7000 0.862 0.688 0.989 0.0157 35.5 14.2 263 105 13.4 52.6 99.2 204 10.5 270 349 12.4 < 0.0087 0.0885 < 0.0087 <0.017 <0.017

1-Methylnaphthalene NA NA NA 0.0258 0.0146 J 6.33 0.777 7.82 1.12 31.2 3.05 0.610 J 10.20 4.46 0.858 J 0.66 J 3.32 < 0.0043 <0.027 < 0.011 <0.022 <0.0542,4,6-Trichlorophenol 2.0 <0.016 <0.023 < 0.0023 0.551 0.0669 J <0.110 <0.450 <0.011 <0.560 1.18 <0.220 0.60 J <0.270 0.741 J <0.270 <0.090 < 0.0045 0.0571 J 0.816 0.200 <0.0572,4-Dichlorophenol 10 <0.016 <0.022 < 0.0022 0.0508 J <0.044 <0.110 <0.440 <0.011 <0.560 0.473 <0.220 <0.220 <0.270 0.488 J <0.270 <0.089 0.0108 <0.028 0.0734 0.0914 J <0.0562,4-Dimethylphenol 70 <0.015 0.175 < 0.0021 6.66 3.23 6.56 3.57 3.97 6.67 6.25 0.428 J 1.30 <0.250 39.8 J <0.250 0.546 0.0059 0.142 0.0871 0.140 0.124 J2-Chlorophenol 20 < 0.014 < 0.019 < 0.0019 <0.010 <0.038 <0.096 <0.380 <0.0096 <0.480 0.050 J <0.190 <0.190 <0.230 0.533 J <0.230 <0.077 < 0.0039 <0.024 0.0273 0.0553 J <0.0482-Methylnaphthalene NA 0.0758 0.209 0.0382 0.0152 J 8.64 1.13 12.4 1.65 50.6 4.77 1.06 16.10 7.24 1.08 J 1.16 J 4.60 < 0.0050 <0.031 < 0.012 <0.025 <0.0622-Methylphenol 200 0.039 0.326 < 0.0019 11.9 3.04 11.6 5.92 10.4 11.1 15.4 2.85 1.19 0.423 J 47.7 <0.230 0.285 J < 0.0039 0.157 0.198 0.328 0.2543&4-Methylphenol 200 0.117 1.89 0.0087 8.63 12.9 10.8 3.78 8.40 10.6 13.2 3.08 2.93 1.2 42.2 <0.260 <0.086 < 0.0044 <0.027 0.290 2.09 0.5704-Chloro-3-methylphenol 7000 0.302 1.08 < 0.0023 0.0238 J 1.14 0.515 3.24 <0.012 3.00 7.97 3.13 2.93 <0.280 0.859 J <0.280 0.880 0.0258 2.50 < 0.012 0.393 0.958Acenaphthene 210 < 0.017 <0.024 < 0.0024 <0.013 0.822 <0.120 0.520 J 0.0761 2.60 0.154 <0.240 0.603 J <0.290 <0.480 <0.290 0.427 < 0.0048 <0.030 < 0.012 <0.024 <0.061Acenaphthylene NA < 0.017 <0.024 < 0.0024 <0.012 0.714 <0.120 <0.470 <0.012 <0.590 <0.023 <0.230 <0.230 <0.280 <0.470 <0.280 0.182 J < 0.0047 <0.030 < 0.012 <0.024 <0.059Aniline 60 NA NA < 0.0026 <0.014 <0.052 <0.130 <0.520 <0.013 <0.650 <0.026 <0.260 <0.260 <0.310 <0.520 <0.310 <0.100 0.0062 <0.033 < 0.013 0.0393 J <0.065Anthracene 1050 < 0.020 <0.028 < 0.0028 <0.015 0.433 <0.140 <0.560 0.0476 J 1.40 0.125 <0.280 0.327 J <0.340 <0.560 <0.340 0.221 J < 0.0057 <0.035 < 0.014 <0.028 <0.071Benzo(a)anthracene NA < 0.021 <0.030 < 0.0030 <0.016 0.172 J <0.150 <0.600 <0.015 <0.750 0.0453 J <0.300 <0.300 <0.360 <0.600 <0.360 0.134 J < 0.0060 <0.038 < 0.015 <0.030 <0.075Benzo(a)pyrene NA < 0.019 <0.027 < 0.0027 <0.014 0.0677 J <0.130 <0.540 <0.013 <0.670 <0.027 <0.270 <0.270 <0.320 <0.540 <0.320 <0.110 < 0.0054 <0.034 < 0.014 <0.027 <0.068Benzo(b)fluoranthene NA < 0.017 <0.024 < 0.0024 <0.013 0.0506 J <0.120 <0.480 <0.012 <0.600 <0.024 <0.240 <0.240 <0.290 <0.480 <0.290 <0.095 < 0.0048 <0.030 < 0.012 <0.031 <0.060Benzoic acid NA 9.85 11.1 < 0.020 <0.110 <0.400 <1.0 <4.0 <0.100 <5.0 <0.200 3.44 J <2.0 <2.4 <4.0 <2.4 <0.800 < 0.040 <0.250 < 0.100 <0.200 17.6Benzyl alcohol NA 0.10 0.163 < 0.0018 <0.0093 <0.035 <0.088 <0.350 <0.0088 <0.440 <0.018 1.13 2.19 1.75 <0.350 <0.210 <0.070 < 0.0035 <0.022 0.329 <0.018 1.34bis(2-Ethylhexyl)phthalate 30 < 0.021 <0.030 0.0564 <0.016 0.306 0.386 J 1.20 J 0.0381 J 0.871 J 0.366 <0.290 2.19 6.73 <0.590 <0.350 2.18 < 0.0059 0.101 J < 0.015 <0.030 <0.074Carbazole NA < 0.020 <0.028 < 0.0028 <0.015 0.165 J <0.140 <0.560 0.0358 J 0.986 J 0.129 <0.280 <0.280 <0.330 <0.560 <0.330 <0.110 < 0.0056 <0.035 < 0.014 <0.028 <0.070Chrysene NA < 0.022 <0.032 < 0.0032 <0.017 0.320 <0.160 <0.630 <0.016 <0.790 0.513 <0.310 <0.310 <0.380 <0.630 <0.380 <0.130 < 0.0063 <0.040 < 0.016 <0.032 <0.079Dibenzofuran NA < 0.018 <0.025 < 0.0025 <0.013 0.227 <0.130 <0.500 0.0491 J <0.630 0.135 <0.250 <0.250 <0.300 <0.500 <0.300 <0.100 < 0.0051 <0.032 < 0.013 <0.025 <0.064Diethyl phthalate 3000 < 0.020 <0.028 < 0.0028 <0.015 <0.055 <0.140 <0.550 <0.014 <0.690 0.147 <0.280 0.963 J 0.766 J <0.550 0.658 J <0.110 < 0.0056 <0.035 < 0.014 <0.028 <0.070Di-n-butyl phthalate 400 < 0.019 <0.027 < 0.0027 <0.014 <0.054 <0.130 <0.540 <0.013 <0.670 0.0369 J <0.270 <0.270 1.14 J <0.540 1.02 J <0.110 < 0.0054 <0.034 < 0.014 <0.027 <0.068Fluoranthene 140 < 0.020 <0.028 < 0.0028 <0.015 0.224 <0.140 <0.560 0.0233 J <0.700 0.0621 J <0.280 <0.280 <0.330 <0.560 <0.330 0.263 J < 0.0056 <0.035 < 0.014 <0.028 <0.070Fluorene 140 < 0.017 0.0414 J 0.0046 <0.013 1.35 0.136 J 0.929 J 0.189 4.26 0.381 <0.250 1.22 0.582 J <0.490 <0.300 0.506 < 0.0050 <0.031 < 0.012 <0.025 <0.062Naphthalene NA 0.0441 0.132 0.166 <0.011 21.3 3.30 27.4 0.640 13.8 5.91 6.04 25.80 21.9 3.18 1.89 4.49 < 0.0042 <0.026 < 0.010 0.0316 J <0.052N-Nitrosodiphenylamine 70 < 0.020 <0.029 < 0.0029 <0.015 <0.041 <0.140 2.34 <0.010 <0.710 <0.021 <0.280 4.49 8.81 <0.410 7.25 <0.082 < 0.0057 <0.036 < 0.014 <0.029 <0.072Phenanthrene NA 0.0247 0.109 0.0092 <0.016 2.35 0.217 J 2.02 0.473 10.6 0.493 <0.300 3.41 0.703 J 0.631 J <0.360 1.24 < 0.0060 <0.038 < 0.015 <0.030 <0.075Phenol 2000 0.643 2.86 < 0.0029 1.68 6.04 2.94 1.27 J 2.70 2.96 4.45 15 3.19 1.05 J 24 <0.350 <0.120 < 0.0059 <0.037 0.424 0.962 0.605

Analyte

SVOCS by Method 8270

VOCs by Method 8260

2 Table 4 to 6 CES Data Waste Data.xlsx: Tank Liquids

Table 5Summary of Waste Liquid Data

EPA Emergency Removal Action CES Griggs Road VCP Site

Texas Class 2 CES-CS-Tank 407

CES-CS-Tank 408 FT-1001 FT-1002 N-Tank 7 N. Tank

9/10 OT-2 OT-3 OT 4/5 OT-6 S. Tank 1/3/6 S. Tank 2 S. Tank 5 S. Tank 7 S. Tank 8 WMU-123 WWT 1/4/5

+ VAT WWT-3 WWT 6/7/8

WWT 9/10/12 WWT-13

Levels (mg/L 8/7/14 8/7/14 8/28/14 8/29/14 9/23/14 9/26/14 9/24/14 9/23/14 ###### 9/23/14 10/1/14 9/25/14 9/25/14 9/24/14 9/25/14 9/24/14 10/2/14 10/1/14 10/2/14 10/2/14 10/1/14AnalytePyrene 5.9 < 0.020 0.0345 J 0.0041 <0.015 0.697 <0.140 0.584 J 0.139 2.37 0.303 <0.290 0.735 J <0.340 <0.570 <0.340 0.549 < 0.0058 <0.036 < 0.014 <0.029 <0.072Pyridine 4.0 NA NA < 0.0025 < 0.013 < 0.050 < 0.130 < 0.50 < 0.013 < 0.63 < 0.025 < 0.25 < 0.25 < 0.30 < 0.50 < 0.30 < 0.10 < 0.0051 <0.032 0.0148 <0.025 <0.054

Aluminum NA 20.1 300 0.0825 J 2.02 7.99 3.14 33 4.71 48.0 10.5 794 42.0 47.9 21.2 49.9 1.10 0.190 J 2.29 0.184 J 0.0426 J 4.77Antimony 1.0 0.323 0.765 0.0023 J 0.0033 J 0.0212 J 0.0344 0.197 0.0230 0.0869 0.0698 0.325 0.132 0.0972 1.25 0.0551 0.0262 0.0029 J 0.0061 0.0173 0.0082 0.0717Arsenic 1.8 0.0721 0.547 < 0.0047 0.0126 0.0482 0.108 0.0344 0.0637 0.0303 0.0225 0.306 0.107 0.0249 J 1.76 0.0435 0.0148 0.0438 0.0170 0.0365 0.0208 0.0218Barium 100 2.60 136 0.0501 J 0.0486 J 1.15 0.375 3.58 0.625 21.2 2.85 1.04 4.61 3.93 2.07 3.45 0.123 J 0.0198 J 0.159 J 0.0315 J 0.0437 J 0.352 JBeryllium 0.08 0.0026 J 0.0345 J < 0.00018 0.00040 J <0.00090 0.00024 J 0.00087 J 0.00029 J 0.0011 J 0.00035 J 0.0368 0.0027 J 0.0023 J <0.00090 <0.00090 <0.00018 < 0.00018 <0.00018 < 0.00018 <0.00018 <0.00036Cadmium 0.5 0.0101 J 0.0507 J < 0.00023 0.00038 J <0.0012 0.0054 0.0051 0.0012 J 0.0115 0.0059 0.286 0.0147 J 0.0126 J 0.0039 J 0.0030 J 0.00025 J < 0.00023 0.00031 J 0.00090 J <0.00023 <0.00046Chromium 5.0 1.18 33.6 0.0017 J 0.0109 0.142 0.141 0.183 0.0572 0.284 0.108 24.3 1.05 0.485 0.374 0.198 0.0464 0.0566 0.114 0.115 0.0640 0.145Cobalt NA 0.115 J 0.184 J 0.00072 J 0.0077 J 0.156 J 0.0215 J 0.0417 J 0.0082 J 0.0085 J 0.0166 J 3.20 0.224 J 0.21 J 0.0716 J 0.0400 J 0.0192 J 0.0084 J 0.0790 0.0341 J 0.0435 J 0.0271 JCopper NA 1.59 35.2 0.0043 J 0.0278 0.464 0.431 2.30 0.190 2.17 1.13 11.9 6.51 3.28 1.64 1.14 0.289 0.0056 J 0.0403 0.0659 <0.0029 0.0152 JIron NA 575 3,070 3.96 21.9 640 28.9 92.1 75 89.3 115 15,600 655 835 110 78.0 12.1 2.39 16.5 35.6 286 470Lead 1.5 0.208 9.33 0.0017 J 0.0136 0.184 3.15 0.354 0.07 0.385 0.437 6.29 0.985 0.505 0.366 0.134 0.0166 0.0011 J 0.0240 0.0063 0.0026 J 0.0211Manganese NA 12.8 8.89 0.227 0.517 11.7 0.476 2.54 1.29 3.16 1.55 122 12.8 12.5 1.48 3.34 1.04 0.237 0.656 1.33 4.10 5.76Mercury 0.2 0.00065 0.0022 0.0745 0.000089 J 2.56 0.0153 0.816 0.0043 0.0067 0.0944 0.389 0.668 0.0603 0.250 0.00013 J 0.50 0.000066 J 0.000071 J < 0.000050 <0.000050 <0.000050Nickel 70 1.42 3.53 0.0118 J 0.0476 2.46 0.318 0.431 0.0893 0.492 0.195 33.6 3.44 2.59 1.23 8.81 0.32 0.434 0.263 1.78 1.56 2.38Selenium 1.0 0.0614 0.256 J 0.0034 J 0.0036 J <0.012 0.0109 0.0077 0.0046 J 0.0056 0.0058 <0.12 0.0740 0.0247 J 0.0470 <0.012 <0.0024 < 0.0024 0.0040 J 0.0035 J <0.0024 <0.0048Silver 5.0 < 0.0024 <0.040 < 0.00059 <0.00059 0.0065 J 0.0012 J 0.0041 J 0.0013 J 0.0031 J 0.0028 J 0.0433 J 0.0103 J 0.0123 J <0.0030 2.24 <0.00059 < 0.00059 <0.00059 < 0.00059 <0.0059 <0.0012Thallium NA < 0.0078 < 0.13 < 0.0021 < 0.0021 < 0.010 < 0.010 < 0.010 < 0.0021 < 0.0021 < 0.0021 < 0.10 < 0.021 < 0.010 < 0.041 < 0.010 < 0.0021 < 0.0021 < 0.0021 < 0.010 < 0.010 < 0.010Vanadium 30 0.249 J 1.78 J 0.00063 J 0.0068 J 0.0605 J 0.0499 J 0.102 0.016 J 0.0575 0.0549 3.48 0.407 0.577 0.157 J 0.0294 J 0.0132 J 0.0185 J 0.0105 J 0.0074 J 0.0156 J 0.0351 JZinc NA 42.8 78 0.0233 0.698 18.1 3.80 12.1 11.6 12.0 3.20 641 40.1 62.3 7.33 8.05 2.19 0.0522 0.663 2.17 0.0444 4.37

TPH (C6-C12) NA 748 313 6.02 14.1 2,710 335 4080 421 1,980 2,000 603 310 792 1,100 8,410 563 < 0.77 6.57 J 5.16 6.63 229TPH (>C12-C28) NA 9,720 15,600 29.1 108 22,300 1,240 19,100 2,880 8,970 14,000 1,190 1,520 5,030 6,260 65,400 4,400 2.14 621 18.7 12.5 379TPH (>C28-C35) NA 3,620 4,780 15.2 23.8 8,240 801 10,500 231 2,690 8,470 605 415 3,610 2,470 13,300 1,620 < 0.83 113 3.73 <0.83 211TPH (C6-C35) 1500 14,100 20,700 50.3 146 33,300 2,380 33,700 3,530 13,600 24,500 2,390 2250 9,430 9,830 87,100 6,580 2.14 741 27.6 19.1 819

2,4-D 10 0.0154 0.0046 J < 0.0002 < 0.00022 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA2,4,5-TP (Silvex) 1.0 < 0.0002 < 0.0002 < 0.0004 < 0.000044 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA

gamma-BHC (Lindane) 0.3 0.000064 < 0.00017 < 0.00087 < 0.00094 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NAalpha-Chlordane 0.03 0.00012 < 0.00011 < 0.00055 < 0.00059 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA

Notes:Concentrations presented in milligrams per Liter (mg/L) < - Analyte reported as non-detect by laboratory at associated method detection limit (MDL)Bolded values are concentrations detected above the MDL J - Reported concentration is estimatedNA - Not analyzedPink shaded values exceed TCEQ Class 2 regulatory level (30 TAC 335.521(a)(1))

Pesticides by Method 8081

Herbicides by Method 8151

Total Petroleum Hydrocarbons by TX 1005

Metals by Method 6010

3 Table 4 to 6 CES Data Waste Data.xlsx: Tank Liquids

Table 6Summary of Waste Sludge DataEPA Emergency Removal Action

CES Griggs Road VCP SiteTexas Class 2 FT-1004 N-Tank 8 S. Tank 5 S. Tank 1/3/6

Levels (mg/kg) 8/29/2014 9/23/2014 9/25/2014 10/1/2014

1,2,4-Trimethylbenzene NA 1.11 229 75.6 6371,3,5-Trimethylbenzene NA 0.271 74.6 17 1114-Methyl-2-pentanone 2000 <0.32 <62 <6.2 10.7 JAcetone 8000 3.02 <99 <9.9 57.3Benzene 10 < 0.034 1,540 12.5 73.7Carbon disulfide 8000 0.983 <5.8 <0.580 3.69 JChlorobenzene 1400 < 0.047 <9.2 3.83 J <0.930Chloroform 120 < 0.022 <4.3 <0.430 9.62Ethylbenzene 8000 0.311 326 58.2 654Isopropylbenzene NA 0.0753 18.3 J 10.7 43.3Methyl ethyl ketone 4000 0.477 <50 8.77 J 46.4Methyl tert-butyl ether NA < 0.025 33.1 J <0.500 <0.510Naphthalene NA 1.11 2,020 107 911n-Butylbenzene NA < 0.022 11.8 J 24.8 135n-Propylbenzene NA 0.130 76.8 10.2 69.0p-Isopropyltoluene NA 0.0859 <13 2.56 J 18.0sec-Butylbenzene NA 0.100 19.8 J 2.70 J 18.7Styrene 14000 < 0.046 656 15.1 <0.920Tetrachloroethene 14 < 0.051 <10 <1.0 4.18Toluene 20000 0.253 1,070 108 3,800Trichloroethene 10 < 0.023 <4.6 <0.460 0.946 JXylenes (Total) 140000 2.88 510 299 3,370

1-Methylnaphthalene NA 1.95 1,570 8.86 J 264 J2-Chlorophenol 400 0.493 < 35 < 7.2 < 1402,4,6-Trichlorophenol 40 3.02 <21 <4.3 <842,4-Dimethylphenol 1400 275 350 <5.7 <1102-Methylnaphthalene NA 3.17 2,000 14.2 J 4652-Methylphenol 4000 824 249 <7.2 165 J3&4-Methylphenol 4000 551 1,040 <7.2 146 J4-Chloro-3-methylphenol 140000 < 0.23 <27 10.4 J <110Acenaphthene 4200 < 0.24 232 <4.7 <91Acenaphthylene NA < 0.23 243 <4.5 <86Anthracene 21000 < 0.28 110 <4.2 <81Benzoic acid NA < 2.0 <130 58.8 J <510Benzyl alcohol NA < 0.18 <31 13.8 J <130Chrysene NA < 0.31 35.7 J <7.1 <140Dibenzofuran NA < 0.25 36.5 J <5.4 <100bis(2-Ethylhexyl)phthalate 600 < 0.29 <64 17.3 <260Fluoranthene 2800 < 0.28 59.3 J <5.5 <110Fluorene 2800 < 0.25 383 <4.9 <95Naphthalene NA 4.03 7,280 45.6 2,510N-Nitrosodiphenylamine 1400 < 0.28 57.5 J 17.4 <91Phenanthrene NA 0.526 598 <4.7 <91Phenol 40000 364 586 12.1 J 321Pyrene 118 0.331 131 <7.4 <140

Analyte

VOCs by Method 8260

SVOCS by Method 8270

4 Table 4 to 6 CES Data Waste Data.xlsx: Tank Solids

Table 6Summary of Waste Sludge DataEPA Emergency Removal Action

CES Griggs Road VCP SiteTexas Class 2 FT-1004 N-Tank 8 S. Tank 5 S. Tank 1/3/6

Levels (mg/kg) 8/29/2014 9/23/2014 9/25/2014 10/1/2014Analyte

Aluminum NA 5.9 J 528 1,190 2,710Antimony 20 < 0.16 1.6 1.2 13.7Arsenic 36 < 0.16 2.1 0.44 4.4Barium 2000 0.28 J 106 601 1,030Beryllium 1.6 < 0.062 <0.035 <0.034 0.050 JCadmium 10 0.024 J 0.22 0.26 1.6Calcium NA 255 J 1,600 1,710 3,170Chromium 100 0.41 J 11.7 7.7 50.4Cobalt NA 0.86 J 3.3 0.95 J 7.1Copper NA 0.23 J 107 48.8 579Iron NA 39.5 3,530 1,650 7,030Lead 30 < 0.20 19.6 7.1 134Magnesium NA 11.3 J 465 77.6 J 96.8 JManganese NA 4.0 28.7 12.7 40.4Mercury 4.0 0.049 0.70 0.77 91.9Nickel 1400 2.4 J 73.3 10.5 41.3Potassium NA 200 J 102 J 67.6 J 1,370Selenium 20 0.20 J 0.38 0.12 J 0.93Silver 100 < 0.063 0.12 J 0.30 J 1.1Sodium NA 14,200 809 832 1,310Vanadium 600 0.12 J 4.7 2.0 J 36.2Zinc NA 2.1 205 623 519

TPH (C6-C12) NA 2,470 574 581 J 76,700TPH (>C12-C28) NA 9,500 1,020 2,480 150,000TPH (>C28-C35) NA 868 301 1,660 73,300TPH (C6-C35) 1500 12,800 1,900 4,720 303,000

Notes:Concentrations presented in milligrams per kilogram (mg/kg) < - Analyte reported as non-detect by laboratory at associated method detection limit (MDL)Bolded values are concentrations detected above the MDL J - Reported concentration is estimatedPink shaded values exceed TCEQ regulatory level (30 TAC 335.521(a)(1)) adjusted for 20-fold preparation factor

Metals by Method 6010

TPH by TX 1005

5 Table 4 to 6 CES Data Waste Data.xlsx: Tank Solids



Project No. 4014 September 2016

FIGURES

Figure 1 On-Site Property Map (CES, 2016)

Figure 2 Stormwater Pollution Prevention Plan Map (TCEQ, 2008)

Figure 3 Site Plan Suttles Truck Leasing (TNRCC, 1998)

01

11

12

14

13

10

17

18

16

09

19

20

21

23

08

07

01

22

15

02

03

4900 Griggs Rd.

4904 Griggs Rd.

5910 Wayland St.

01

03

04

02

06

05

06

04

05

03

02

24

25

26

27

28

29

30

29A

14

18

13

12

10

17

11

03A

16

15

07

04A

09

08

MW-02

MW-01

MW-05

MW-04

MW-03

12

3

4

5

6

7

8

9

1011

12

14

13

120600

Scale in Feet

DATE:

PROJECT:

PASTOR, BEHLING & WHEELER, LLC

CONSULTING ENGINEERS AND SCIENTISTS

REVISIONS

CHECKED:

BY:

Figure 1

AJD

BBMARCH, 2016

4020

CES GRIGGS ROAD VCP SITE

HOUSTON, TEXAS

Approx. Property Boundary

PBW Sample Location - Phase I

PBW Sample Location - Phase II

PBW Monitoring Well Location

Source:

Imagery taken from www.tnris.gov, Harris County, TX 2013 photography.

Office Building

Training Center/Locker Room (2008)/

Administrative (2010)

Industrial Waste Processing & Storage (2008)/

Main Processing (2010)

Old Cleaning Rack (1996)/

Tank Trucking Cleaning (2008)/Safe Wash (2010)

Equipment Cleaning (2008)/

Drum Cleaning (2010)

New Shop (1996)/Truck Maintenance (2008)

Cleaning Rack (1996)/Tank Truck Cleaning (2008)/

Equipment & Fleet Maintenance (2015)

Oil/Water Separating Tanks (2010)/

North Tank Farm (2015)

Oil/Water Separating Tanks (2010)/

South Tank Farm (2015)

Welding Shop

Fuel Storage Shed

WMU 126-128 (Frac Tanks)

Former Mechanic Shop (2010)/Field Services (2015)

1

2

3

4

5

6

7

8

9

11

12

13

14

Hot Oil Heat System (2008)/

Drum-Tote Storage (2015)

10

Figure 2

Figure 3

Sump WMU 001

brenda basile

Rectangle

brenda basile

Rectangle

brenda basile

Rectangle

brenda basile

Oval

brenda basile

Line




Attachment 1 March 6, 2012 CES Environmental Services Notice of Registration

*** TEXAS COMMISSION ON ENVIRONMENTAL QUALITY ***Notice of Registration

Industrial and Hazardous Waste

CES ENVIRONMENTAL SERVICES30900

Page: 1

Date: 03/15/2012

Solid Waste Registration Number: 30900 EPA Id: TXD008950461

CES ENVIRONMENTAL SERVICES INC Region: 12 Initial Registration Date: 02/18/1977Company Name:

CES ENVIRONMENTAL SERVICES County: 101 HARRIS Last Amendment Date: 03/06/2012Site Name:

Site Location: 4904 Griggs Rd, Houston, TX Land Type: Private Last Date NOR Computer update: 03/06/2012Primary Contact: THANGUDU, PRABHAKAR Title: MGR Phone: 713-676-1460

Mailing Address: 4904 GRIGGS RD Site Street Address: 4904 GRIGGS RD

HOUSTON, TX 77021-3208 HOUSTON, TX 77021

Registration Status: Inactive Reporting Method: PAPERRegistration Type: Generator Receiver Transporter Transfer Facility

Generator Type: Industrial Hazardous Waste Generation Status: Large Quantity GeneratorReceiver Type: Commercial

Transporter Type: FOR HIRE TRANSPORT OWN WASTE

Transport Wst Class: H 2 1

Business Description: Operation of a nonhazardous industrial solid waste processing and storage facility. Filed Chapter 7 Bankruptcy

NAICS Code: 562219 Other Nonhazardous Waste Treatment and DisposalTax Identification #: 17605929854

Handler Status:

Operator Information Owner Information:

CES ENVIRONMENTAL SERVICES INC713-676-1460 4904 GRIGGS RDHOUSTON, TX 77021-3208

Name:

Phone:

Address:

CES ENVIRONMENTAL SERVICES INC713-676-1460 4904 GRIGGS RDHOUSTON, TX 77021-3208

Name:

Phone:

Address:

Billing Contact: Title: Phone:

Billing Address:201 KINGWOOD MEDICAL DR STE A200KINGWOOD, TX 77339-6011

Other Contact: Manager, Environmental Role: IHW: Owner Contact Phone: 713-676-1460Mailing Address: 4904 GRIGGS RD

HOUSTON, TX 77021-3208

Other Contact: THANGUDU, PRABHAKAR Role: IHW: Steers Contact Phone: 713-676-1460Mailing Address: 4904 GRIGGS RD

HOUSTON, TX 77021-3208

As of 03/06/2012 -the next unassigned sequence number for UNITS is 141the next unassigned sequence number for WASTES is 9031 and




Page: 2

Date: 03/15/2012

**** WASTE INFORMATION ****

Texas

Waste

Code

Waste

ClassStatus

Date of

Status

Managed

Onsite/

Offsite

Radio-

active

TCEQ Audit

Complete

** No Longer Generated Wastes **

00022061 1 Inactive 03/06/2012 On-site No No

Description from Generator: Waste oil currently generated through general vehicle maintenance operations.

Texas Form Code: 206 Waste oilOrigin Code: 1 Generated on-site from a product process or service activity

Current Management Units: None

0004102H H Inactive 03/06/2012 On-site No No

Description from Generator: Mixed organics (<4%), inorganic caustic (<1%) & water (>95%). Currently generated through cleaning "RCRA empty" containers (tank trucks).

Texas Form Code: 102 Aqueous waste with low other toxic organicsEPA Form Code: W101 Very dilute aqueous waste containing more than 99% water

Origin Code: 1 Generated on-site from a product process or service activitySource Code: G01 Dip, flush or spray rinsingNAICS Code: 488490 Other Support Activities for Road Transportation

EPA Hazardous Waste Numbers: D002



Description from Generator: Used oil filters currently generated through general vehicle maintenance operations. This waste is recycled by being sent to a recycling facility in Mexia, Texas.

Texas Form Code: 310 Spent solid filters or adsorbentsOrigin Code: 1 Generated on-site from a product process or service activity



Description from Generator: Plant production refuse currently generated during normal facility & office operations.

Texas Form Code: 901Origin Code: 1 Generated on-site from a product process or service activity



Description from Generator: Mixed organics (<1%), inorganic caustic (<1%) & water (>98%). "Final internal &external rinsewaters" are currently generated through cleaning "RCRA empty" containers (tank trucks).

Texas Form Code: 119 Other inorganic liquidsOrigin Code: 1 Generated on-site from a product process or service activity



Description from Generator: Generated through a routine cleaning of a tank washing process vat as a result of cleaning "RCRA empty" containers (tank trucks).

Texas Form Code: 319 Other waste inorganic solidsOrigin Code: 1 Generated on-site from a product process or service activity





Page: 3

Date: 03/15/2012

Texas

Waste

Code

Waste

ClassStatus

Date of

Status

Managed

Onsite/

Offsite

Radio-

active

TCEQ Audit

Complete



Description from Generator: Petroleum (oils & greases) contaminated rags currently generated during generalvehicle maintenance operations.

Texas Form Code: 489 Petroleum contaminated solidsOrigin Code: 1 Generated on-site from a product process or service activity



Description from Generator: "Petroleum contaminated solids" absorbents (>99%) & miscellaneous organic chemicals (<1%). This waste stream is currently generated during general "housekeeping" maintenance

operations.




Description from Generator: Oil/water separator solids currently generated during internal & external washing of "RCRA empty" containers (tank truck).

Texas Form Code: 519 Other inorganic sludgesOrigin Code: 1 Generated on-site from a product process or service activity



Description from Generator: Pretreated effluent discharged to the City of Houston's wastewater treatment system. Effluent meets the criteria of a class 2 waste under Subchapter R requirements & this waste code is being

added as a companion to waste code 00091191, final internal & external rinsewaters, to avoid confusion on the exempt status of the annual generator fee for waste code 00091191




Description from Generator: This is a first flush from internal tank washes. This stream goes to on site storage for transport to off site treatment.

Texas Form Code: 219 Other organic liquidsOrigin Code: 3 Derived from on-site management of a nonhazardous waste



Description from Generator: This material is flammable "heel" drummed from transport trailers before first flush.

Texas Form Code: 219 Other organic liquidsEPA Form Code: W219 Other organic liquid

Origin Code: 5 Residual from on-site treatment, disposal or recycling of hazardous wasteSource Code: G09 Other production or service-related processesNAICS Code: 811211 Consumer Electronics Repair and Maintenance

EPA Hazardous Waste Numbers: U002 U031 U118 U154 U162 U165 U220 U239 U359





Page: 4

Date: 03/15/2012

Texas

Waste

Code

Waste

ClassStatus

Date of

Status

Managed

Onsite/

Offsite

Radio-

active

TCEQ Audit

Complete



Description from Generator: Supplemental plant production refuse and cleaned cut up hoses.

Texas Form Code: 902 Class 2 supplemental plant production refuseOrigin Code: 1 Generated on-site from a product process or service activity



Description from Generator: Lube oils and additives

Texas Form Code: 219 Other organic liquidsOrigin Code: 1 Generated on-site from a product process or service activity



Description from Generator: Used engine oil generated from maintenance operations.




Description from Generator: Spent diesel fuel contaminated with lub oil and petroleum distillates.

Texas Form Code: 203 Non-halogenated solventOrigin Code: 1 Generated on-site from a product process or service activity



Description from Generator: Rags contaminated with petroleum products




Description from Generator: Petroleum Wax




Description from Generator: Aqueous waste with low other toxic organ

Texas Form Code: 102 Aqueous waste with low other toxic organicsOrigin Code: 1 Generated on-site from a product process or service activity





Page: 5

Date: 03/15/2012

Texas

Waste

Code

Waste

ClassStatus

Date of

Status

Managed

Onsite/

Offsite

Radio-

active

TCEQ Audit

Complete



Description from Generator: Non RCRA regulated rinse water. Generating process: Rinsing w/ pressure washerof RCRA Empty containers. Date of generation 6-30-2002




Description from Generator: Non RCRA regulated waste sludge. Generating process: Removal of non haz from tanks and totes before destruction. Date of generation: 7-1-2002

Texas Form Code: 519 Other inorganic sludgesOrigin Code: 3 Derived from on-site management of a nonhazardous waste


90032191 1 Inactive 03/06/2012 No No

Description from Generator: This is a first flush from internal tank washes. Date of generation: 7-1-02.




Description from Generator: Plant trash generated from on-site activities. Date of generation: 7-1-02.

Texas Form Code: 999 Class 2 plant trashOrigin Code: 1 Generated on-site from a product process or service activity



Description from Generator: Flammable sludge. Generating process: removal of unused products from tank/tote management services. Date of generation: 7-1-02.

Texas Form Code: 609 Other organic sludgesEPA Form Code: W609 Other organic sludge

Origin Code: 1 Generated on-site from a product process or service activitySource Code: G09 Other production or service-related processesNAICS Code: 236220 Commercial and Institutional Building Construction

EPA Hazardous Waste Numbers: D001 D002 D018 F005



Description from Generator: Flammable/corrosive sludge. Generating process: Removal of unused product fromtank/tote management services. Date of generation: 7-1-02.

Texas Form Code: 609 Other organic sludgesEPA Form Code: W609 Other organic sludge


EPA Hazardous Waste Numbers: D001 D002





Page: 6

Date: 03/15/2012

Texas

Waste

Code

Waste

ClassStatus

Date of

Status

Managed

Onsite/

Offsite

Radio-

active

TCEQ Audit

Complete



Description from Generator: Corrosive sludge alkaline. Generating process: Removal of unused products fromtank/tote management services. Date of generation: 7-1-02.

Texas Form Code: 110 Caustic aqueous wasteEPA Form Code: W110 Caustic aqueous waste without cyanides





Description from Generator: Corrosive Sludge acidic. Generating process: Removal of unused products from tank /tote management services. 7-1-2002

Texas Form Code: 105 Acidic aqueous wasteEPA Form Code: W105 Acidic aqueous wastes less than 5% acid





Description from Generator: Hazardous Waste Solids from the cleaning of totes, tanks, Roll-off boxes, VacuumBoxes, and tanker trucks.

Texas Form Code: 409 Other non-halogenated organic solidsEPA Form Code: W409 Other organic solids

Origin Code: 1 Generated on-site from a product process or service activitySource Code: G13 Cleaning out process equipmentNAICS Code: 236220 Commercial and Institutional Building Construction

Company's Internal Code(s): HAZ WASTE SOLIDSEPA Hazardous Waste Numbers: D004 D005 D006 D007 D008 D009 D010 D011 D012 D013 D014

D015 D016 D017 D018 D021 D023 D024 D025 D026 D030 D035D036 D038 D043 U037



Description from Generator: Halogenated Hydrocarbon and water mixture

Texas Form Code: 206 Waste oilEPA Form Code: W206 Waste oil

Origin Code: 1 Generated on-site from a product process or service activitySource Code: G19 Other one-time or intermittent processesNAICS Code: 236220 Commercial and Institutional Building Construction

Company's Internal Code(s): HAL HYDROCARB H2OEPA Hazardous Waste Numbers: D020 D021 D022 D027 D028 D029 D031 D032 D033 D034 D037

D039 D040 D041 D042 F001 F002 F003 F004 F005





Page: 7

Date: 03/15/2012

Texas

Waste

Code

Waste

ClassStatus

Date of

Status

Managed

Onsite/

Offsite

Radio-

active

TCEQ Audit

Complete



Description from Generator: Generated from rinsing and removing residues from tank trailers, totes and vacuum boxes

Texas Form Code: 519 Other inorganic sludgesEPA Form Code: W519 Other inorganic sludges


Company's Internal Code(s): METAL SLUDGESEPA Hazardous Waste Numbers: D004 D005 D006 D007 D008 D009 D010



Description from Generator: Rinse water from tank cleaning process discharged to local POTW


Company's Internal Code(s): POTW DISCHARGE WATER



Description from Generator: Treated Class 2 Wastewater discharged to a POTW from wastewater treatment facility used to treat industrial wastewater.

Texas Form Code: 114 Other aqueous waste with low dissolved solidsOrigin Code: 1 Generated on-site from a product process or service activity

Company's Internal Code(s): WATER TO POTW



Description from Generator: Inorganic sludge generated from treatment of water with dissolved metals, or acid/base solutions.

Texas Form Code: 519 Other inorganic sludgesOrigin Code: 1 Generated on-site from a product process or service activity

Company's Internal Code(s): INORGANIC SLUDGE



Description from Generator: Precipitated hazardous sludge from the treatment of water with dissolved metals,and acid/base solutions.

Texas Form Code: 519 Other inorganic sludgesEPA Form Code: W105 Acidic aqueous wastes less than 5% acid

Origin Code: 5 Residual from on-site treatment, disposal or recycling of hazardous wasteSource Code: G23 Wastewater treatment (sludge, filter cake, etc.)NAICS Code: 562211 Hazardous Waste Treatment and Disposal

Company's Internal Code(s): INORGANIC SLUDGE HAZEPA Hazardous Waste Numbers: D004 D005 D006 D007 D008 D009 D011





Page: 8

Date: 03/15/2012

Texas

Waste

Code

Waste

ClassStatus

Date of

Status

Managed

Onsite/

Offsite

Radio-

active

TCEQ Audit

Complete



Description from Generator: Generated from the consolidation of various non-hazardous, Class-1 sludges per permit ISWP No. 39048.

Texas Form Code: 609 Other organic sludgesOrigin Code: 4 Received from off-site and was not recycled or treated on-site

Company's Internal Code(s): NON-HAZARDOUS SLUDGE



Description from Generator: Generated from the consolidation of various non-hazardous, class-2 sludges per permit No. 39048.

Texas Form Code: 609 Other organic sludgesOrigin Code: 4 Received from off-site and was not recycled or treated on-site

Company's Internal Code(s): NON-HAZ CLASS2 SLUDG



Description from Generator: Generated from the consolidation of various non-hazardous, class-1 solids per permit No. 39048. Per a notification dated September 27, 2005, this waste is recycled by being used as road

base material.

Texas Form Code: 409 Other non-halogenated organic solidsOrigin Code: 4 Received from off-site and was not recycled or treated on-site

Company's Internal Code(s): CLASS 1 NON-HAZ SOLI



Description from Generator: Generated from the consolidation of various non-hazardous, Class II solids per Permit No. 39048.

Texas Form Code: 409 Other non-halogenated organic solidsOrigin Code: 4 Received from off-site and was not recycled or treated on-site

Company's Internal Code(s): CLASS II SOLIDS



Description from Generator: Water-soluble liquids and oily waters with low solids. Generating Process: Non-hazardous waste in drums, roll-off boxes, or other containers.

Texas Form Code: 119 Other inorganic liquidsOrigin Code: 3 Derived from on-site management of a nonhazardous waste

Company's Internal Code(s): INORGANIC LIQUIDS





Page: 9

Date: 03/15/2012

Texas

Waste

Code

Waste

ClassStatus

Date of

Status

Managed

Onsite/

Offsite

Radio-

active

TCEQ Audit

Complete



Description from Generator: Removal of heels from trailers/containers.

Texas Form Code: 403 Solids resins or polymerized organicsEPA Form Code: W403 Solid resins, plastics or polymerized organics

Origin Code: 1 Generated on-site from a product process or service activitySource Code: G14 Removal of tank sludge, sediments or slagNAICS Code: 236220 Commercial and Institutional Building Construction

Company's Internal Code(s): WASTE TDIEPA Hazardous Waste Numbers: D003 F034 U223



Description from Generator: Water-soluble liquids and oily waters with low solids and includes alcohols at amaximum of 23% by volume. Generating Process: Non-hazardous waste in drums, roll-off boxes, or other

containers.

Texas Form Code: 119 Other inorganic liquidsOrigin Code: 3 Derived from on-site management of a nonhazardous waste

Company's Internal Code(s): INORGANIC LIQUIDS



Description from Generator: Concentrate from R/O unit generated from wastewater treatment facility used to treat industrial wastewater and recyclable oily/gassy water.

Texas Form Code: 207 Concentrated aqueous solution of other organicsEPA Form Code: W205 Oil-water emulsion or mixture

Origin Code: 3 Derived from on-site management of a nonhazardous wasteSource Code: G09 Other production or service-related processesNAICS Code: 562219 Other Nonhazardous Waste Treatment and Disposal

Company's Internal Code(s): R O CONCENTRATEEPA Hazardous Waste Numbers: D001 D018



Description from Generator: Centrifuge sludge

Texas Form Code: 603 Oily sludgeOrigin Code: 1 Generated on-site from a product process or service activity

Company's Internal Code(s): CENTRIFUGE SLUDGE





Page: 10

Date: 03/15/2012

Texas

Waste

Code

Waste

ClassStatus

Date of

Status

Managed

Onsite/

Offsite

Radio-

active

TCEQ Audit

Complete



Description from Generator: Removal of sludge/solids from pressing caustic

Texas Form Code: 319 Other waste inorganic solidsEPA Form Code: W519 Other inorganic sludges

Origin Code: 1 Generated on-site from a product process or service activitySource Code: G07 Product and by-product processingNAICS Code: 562219 Other Nonhazardous Waste Treatment and Disposal

Company's Internal Code(s): HAZ-WASTE SOLIDSEPA Hazardous Waste Numbers: D018



Description from Generator: Still bottoms

Texas Form Code: 601 Still bottoms of halogenated (e.g., chlorinated) solvents or other organicsEPA Form Code: W319 Other inorganic solids

Origin Code: 5 Residual from on-site treatment, disposal or recycling of hazardous wasteSource Code: G07 Product and by-product processingNAICS Code: 562219 Other Nonhazardous Waste Treatment and Disposal

Company's Internal Code(s): STILL BOTTOMSEPA Hazardous Waste Numbers: D001 F002 F003


As of 03/06/2012, the next unassinged sequence number for WASTES is 9031




Page: 11

Date: 03/15/2012

**** UNITS AT THIS SITE MANAGING WASTE ****Unit

Number

Unit

Type

Unit

Status

Date of

Status

Classes of Waste

Managed in Unit

Onsite / Offsite

Unit

Permit

Number

Unit #

on

Permit

Regulatory

Status

Deed Recording

Needed/Date

112 Tank ACTIVE 05/10/2005 NA / H12 NA NA08 RCRA Permit exempt-waste

water treatment unitYES /

Description from Company: Tank T3 is used for oil recovery, phase separation, and clarification. The tank is part of an industrial wastewater treatment plant with

discharge water fl owing to a POTW.

System Types: 135 Discharge to sewer/POTW or NPDES (with prior storage - with or without treatment) 039 Other recovery or reclamation for reuse including acid regeneration, organics recovery, etc. 124 Phase

separation

Wastes Previously Managed at Unit: 90241191 Water-soluble liquids and 90261191 Water-soluble liquids and 90171142 Treated Class 2 Wastewater




discharge water f lowing to a POTW.

System Types: 135 Discharge to sewer/POTW or NPDES (with prior storage - with or without treatment) 124 Phase separation 039 Other recovery or reclamation for reuse including acid regeneration, organics

recovery, etc.






System Types: 135 Discharge to sewer/POTW or NPDES (with prior storage - with or without treatment) 039 Other recovery or reclamation for reuse including acid regeneration, organics recovery, etc. 124 Phase

separation







recovery, etc.




Description from Company: Tank T7 is used for oxidation, biotreatment, and separation of organics from wat er. The tank is part of an indusrtial wastewater

treatment facility with d ischarge water flowing to a POTW.

System Types: 135 Discharge to sewer/POTW or NPDES (with prior storage - with or without treatment) 075 Chemical oxidation 081 Biological treatment with or without precipitation



Description from Company: Tank T8 is used for oxidation, biotreatment, and separation of organics from wat er. The tank is part of an industrial wastewater


System Types: 135 Discharge to sewer/POTW or NPDES (with prior storage - with or without treatment) 081 Biological treatment with or without precipitation 075 Chemical oxidation




Page: 12

Date: 03/15/2012

Unit

Number

Unit

Type

Unit

Status

Date of

Status

Classes of Waste

Managed in Unit

Onsite / Offsite

Unit

Permit

Number

Unit #

on

Permit

Regulatory

Status

Deed Recording

Needed/Date



Description from Company: Tank T9 is used for oxidation, biotreatment, and separation of organics from wat er. The tank is part of an industrial wastewater


System Types: 135 Discharge to sewer/POTW or NPDES (with prior storage - with or without treatment) 075 Chemical oxidation 081 Biological treatment with or without precipitation



Description from Company: Tank T10 is used for precipitation of dissolved metals, neutralization of acids/ bases, and settling of suspended solids from water.

The tank is part of an industrial wastewater treatment facility with discharge water flowing to a POTW.

System Types: 135 Discharge to sewer/POTW or NPDES (with prior storage - with or without treatment) 077 Other chemical precipitation with or without pre-treatment 123 Settling or clarification

Wastes Previously Managed at Unit: 9019519H Precipitated hazardous 90185191 Inorganic sludge generated 90171142 Treated Class 2 Wastewater



Description from Company: Tank T11 is used for precipitation of dissolved metals, neutralization of acids/ bases, settling of suspended solids from water. The

tank is part of an ind ustrial wastewater treatment facility with discharge water flowing to a POT W.

System Types: 135 Discharge to sewer/POTW or NPDES (with prior storage - with or without treatment) 123 Settling or clarification 077 Other chemical precipitation with or without pre-treatment

Wastes Previously Managed at Unit: 9019519H Precipitated hazardous 90171142 Treated Class 2 Wastewater 90185191 Inorganic sludge generated



Description from Company: Tank T12 is used for precipitation of dissolved metals, neutralization of acids/ bases, settling of suspended solids from water. The

tank is part of an ind ustrial wastewater treatment facility with discharge water flowing to a POT W.

System Types: 135 Discharge to sewer/POTW or NPDES (with prior storage - with or without treatment) 077 Other chemical precipitation with or without pre-treatment 123 Settling or clarification

Wastes Previously Managed at Unit: 90185191 Inorganic sludge generated 90171142 Treated Class 2 Wastewater 9019519H Precipitated hazardous



Description from Company: The water solids separator is used for phase separation, clarification, and soli ds settling. The unit is part of an industrial wastewater

treatment facili ty with discharge water flowing to a POTW. The unit is identified as WSS1.

System Types: 135 Discharge to sewer/POTW or NPDES (with prior storage - with or without treatment) 124 Phase separation 123 Settling or clarification

Wastes Previously Managed at Unit: 90185191 Inorganic sludge generated 9019519H Precipitated hazardous 90171142 Treated Class 2 Wastewater

123 Tank ACTIVE 11/23/2009 NA / NA NA NA08 RCRA Permit exempt-waste


Description from Company: Tank wash sump water

System Types: 135 Discharge to sewer/POTW or NPDES (with prior storage - with or without treatment)

126 Tank ACTIVE 12/13/2007 1 / NA NA NA08 RCRA Permit exempt-waste


Description from Company: Clarification and settling tank

System Types: 129 Other treatment 124 Phase separation 123 Settling or clarification

Wastes Previously Managed at Unit: 90216092 Generated from the 90241191 Water-soluble liquids and 90161192 Rinse water from tank 90261191 Water-soluble liquids and90171142 Treated Class 2 Wastewater 90206091 Generated from the 90011191 Non RCRA regulated rinse




Page: 13

Date: 03/15/2012

Unit

Number

Unit

Type

Unit

Status

Date of

Status

Classes of Waste

Managed in Unit

Onsite / Offsite

Unit

Permit

Number

Unit #

on

Permit

Regulatory

Status

Deed Recording

Needed/Date





Wastes Previously Managed at Unit: 90171142 Treated Class 2 Wastewater 90261191 Water-soluble liquids and 90161192 Rinse water from tank 90241191 Water-soluble liquids and90011191 Non RCRA regulated rinse 90206091 Generated from the 90216092 Generated from the





Wastes Previously Managed at Unit: 90261191 Water-soluble liquids and 90171142 Treated Class 2 Wastewater 90206091 Generated from the 90216092 Generated from the90011191 Non RCRA regulated rinse 90161192 Rinse water from tank 90241191 Water-soluble liquids and

129 Tank ACTIVE 12/13/2007 1 / NA NA NA13 RCRA Pmt Exempt -

Accumulation TimeYES /

Description from Company: Wastewater tank


Wastes Previously Managed at Unit: 90025191 Non RCRA regulated waste 90011191 Non RCRA regulated rinse 90161192 Rinse water from tank

130 Sump ACTIVE 10/01/2009 12 / NA NA NA 05 Non-Hazardous Regulated YES /

Description from Company: Concrete containment area w/sump that holds truck wash rinse water


Wastes Previously Managed at Unit: 90161192 Rinse water from tank 90011191 Non RCRA regulated rinse

131 Sump ACTIVE 10/01/2009 1 / NA NA NA 05 Non-Hazardous Regulated YES /

Description from Company: Concrete containment are w/sump that holds drum cleaning washwater


Wastes Previously Managed at Unit: 90025191 Non RCRA regulated waste

132 Tank ACTIVE 11/06/2009 NA / 12 NA NA08 RCRA Permit exempt-waste


Description from Company: Clarification and settling

System Types: 123 Settling or clarification

Wastes Previously Managed at Unit: 90241191 Water-soluble liquids and 90261191 Water-soluble liquids and 90011191 Non RCRA regulated rinse 90171142 Treated Class 2 Wastewater90216092 Generated from the 90161192 Rinse water from tank 90206091 Generated from the





Wastes Previously Managed at Unit: 90206091 Generated from the 90261191 Water-soluble liquids and 90216092 Generated from the 90241191 Water-soluble liquids and90011191 Non RCRA regulated rinse 90161192 Rinse water from tank 90171142 Treated Class 2 Wastewater




Page: 14

Date: 03/15/2012

Unit

Number

Unit

Type

Unit

Status

Date of

Status

Classes of Waste

Managed in Unit

Onsite / Offsite

Unit

Permit

Number

Unit #

on

Permit

Regulatory

Status

Deed Recording

Needed/Date





Wastes Previously Managed at Unit: 90206091 Generated from the 90216092 Generated from the 90241191 Water-soluble liquids and 90261191 Water-soluble liquids and90011191 Non RCRA regulated rinse 90161192 Rinse water from tank 90171142 Treated Class 2 Wastewater





Wastes Previously Managed at Unit: 90171142 Treated Class 2 Wastewater 90161192 Rinse water from tank 90261191 Water-soluble liquids and 90216092 Generated from the90011191 Non RCRA regulated rinse 90206091 Generated from the 90241191 Water-soluble liquids and





Wastes Previously Managed at Unit: 90216092 Generated from the 90261191 Water-soluble liquids and 90011191 Non RCRA regulated rinse 90161192 Rinse water from tank90171142 Treated Class 2 Wastewater 90241191 Water-soluble liquids and 90206091 Generated from the





Wastes Previously Managed at Unit: 90171142 Treated Class 2 Wastewater 90216092 Generated from the 90241191 Water-soluble liquids and 90206091 Generated from the90161192 Rinse water from tank 90261191 Water-soluble liquids and 90011191 Non RCRA regulated rinse





Wastes Previously Managed at Unit: 90206091 Generated from the 90171142 Treated Class 2 Wastewater 90011191 Non RCRA regulated rinse 90161192 Rinse water from tank90241191 Water-soluble liquids and 90261191 Water-soluble liquids and 90216092 Generated from the

139 Tank NEVER BUILT 11/23/2009 NA / 12 NA NA08 RCRA Permit exempt-waste


Description from Company: Clarification and settling. Frac tank were never used. Sent back to rental company.


Wastes Previously Managed at Unit: 90216092 Generated from the 90206091 Generated from the 90241191 Water-soluble liquids and 90171142 Treated Class 2 Wastewater90161192 Rinse water from tank 90261191 Water-soluble liquids and 90011191 Non RCRA regulated rinse




Page: 15

Date: 03/15/2012

Unit

Number

Unit

Type

Unit

Status

Date of

Status

Classes of Waste

Managed in Unit

Onsite / Offsite

Unit

Permit

Number

Unit #

on

Permit

Regulatory

Status

Deed Recording

Needed/Date

140 Tank NEVER BUILT 11/23/2009 NA / 12 NA NA08 RCRA Permit exempt-waste


Description from Company: Clarification and settling. Frac tank were never used. Sent back to rental company.


Wastes Previously Managed at Unit: 90216092 Generated from the 90206091 Generated from the 90241191 Water-soluble liquids and 90011191 Non RCRA regulated rinse90161192 Rinse water from tank 90171142 Treated Class 2 Wastewater 90261191 Water-soluble liquids and

001 Sump INACTIVE 01/22/1991 H / NA NA NA 06 YES /

Description from Company:

Wastes Previously Managed at Unit: 9014206H Halogenated Hydrocarbon

002 Miscellaneous storage containers CLOSURE REQUEST 01/08/2007 1 / NA NA NA 06 YES /

Description from Company:

System Types: 141 Storage, bulking, and/or transfer off site - no treatment/recovery, fuel blending or disposal at this site.

Wastes Previously Managed at Unit: 00152191 This is a first flush from 0004102H Mixed organics (<4%), 9014206H Halogenated Hydrocarbon 00251021 Aqueous waste with low

003 Container storage area CLOSURE REQUEST 08/24/2006 1 / NA NA NA13 RCRA Pmt Exempt -


Description from Company: This facility's "old wash rack" has been designated a waste management unit for miscellaneous 55 gallon drums. This area is covered

& inspected weekly for possible hazards.


Wastes Previously Managed at Unit: 00202191 Lube oils and additives 00244891 Petroleum Wax 00073101 Used oil filters currently 00114891 Petroleum (oils & greases)0016219H This material is flammable 00103191 Generated through a routine 00222031 Spent diesel fuel 00124891 "Petroleum contaminated

004 Tank (surface) CLOSURE REQUEST 08/24/2006 1 / NA NA NA 05 Non-Hazardous Regulated YES /

Description from Company: Steel tank


Wastes Previously Managed at Unit: 00022061 Waste oil currently 00222031 Spent diesel fuel 00202191 Lube oils and additives

005 Miscellaneous storage containers CLOSURE REQUEST 08/24/2006 12 / NA NA NA 05 Non-Hazardous Regulated YES /

Description from Company: 7-15 cubic yard dumpster


Wastes Previously Managed at Unit: 00199022 Supplemental plant 00135191 Oil/water separator solids 00089012 Plant production refuse

006 Sump CLOSURE REQUEST 08/24/2006 1 / NA NA NA 05 Non-Hazardous Regulated YES /

Description from Company: Subsurface sumps or oil/water separator basins unit.

System Types: 124 Phase separation

Wastes Previously Managed at Unit: 00152191 This is a first flush from 00135191 Oil/water separator solids




Page: 16

Date: 03/15/2012

Unit

Number

Unit

Type

Unit

Status

Date of

Status

Classes of Waste

Managed in Unit

Onsite / Offsite

Unit

Permit

Number

Unit #

on

Permit

Regulatory

Status

Deed Recording

Needed/Date

007 Tank (surface) CLOSURE REQUEST 08/24/2006 1 / NA NA NA08 RCRA Permit exempt-waste


Description from Company: ph adjustment unit

System Types: 121 Neutralization only

Wastes Previously Managed at Unit: 00152191 This is a first flush from 00091191 Mixed organics (<1%), 00141192 Pretreated effluent

008 Tank (surface) CLOSURE REQUEST 08/24/2006 1 / NA NA NA 05 Non-Hazardous Regulated YES /

Description from Company: 2 - 50 gallon surface tanks

System Types: 061 Fuel blending prior to energy recovery at another site

Wastes Previously Managed at Unit: 00212191 Used engine oil generated

009 Miscellaneous storage containers CLOSURE REQUEST 08/24/2006 1 / NA NA NA13 RCRA Pmt Exempt -


Description from Company: Container Storage Area


Wastes Previously Managed at Unit: 00073101 Used oil filters currently 00234891 Rags contaminated with

101 Tank ACTIVE 06/18/2002 1 / NA NA NA 05 Non-Hazardous Regulated YES /

Description from Company: Vacuum box located in tank wash for the first flush. The first flush is ei ther vacuumed or collected in a container and transferred to

thish first fl ush tank.


Wastes Previously Managed at Unit: 90032191 This is a first flush from 90011191 Non RCRA regulated rinse

102 Tank CLOSURE REQUEST 01/08/2007 1 / NA NA NA13 RCRA Pmt Exempt -


Description from Company: Non Hazardous wastewater tank


Wastes Previously Managed at Unit: 90011191 Non RCRA regulated rinse

103 Miscellaneous storage containers ACTIVE 06/18/2002 1 / NA NA NA 05 Non-Hazardous Regulated YES /

Description from Company: Non Hazrdous sludge box.


Wastes Previously Managed at Unit: 90025191 Non RCRA regulated waste 90286031 Centrifuge sludge

104 Miscellaneous storage containers ACTIVE 06/18/2002 2 / NA NA NA 05 Non-Hazardous Regulated YES /

Description from Company: 40 cubic yard open top box for plant trash.


Wastes Previously Managed at Unit: 90049992 Plant trash generated from




Page: 17

Date: 03/15/2012

Unit

Number

Unit

Type

Unit

Status

Date of

Status

Classes of Waste

Managed in Unit

Onsite / Offsite

Unit

Permit

Number

Unit #

on

Permit

Regulatory

Status

Deed Recording

Needed/Date

105 Container storage area ACTIVE 06/18/2002 H / NA NA NA13 RCRA Pmt Exempt -


Description from Company: Hazardous waste container storage area


Wastes Previously Managed at Unit: 9011110H Corrosive sludge alkaline. 9012105H Corrosive Sludge acidic. 9010609H Flammable/corrosive 9015519H Generated from rinsing and9025403H Removal of heels from 9005609H Flammable sludge. 9013409H Hazardous Waste Solids 9014206H Halogenated Hydrocarbon9029319H Removal of sludge/solids

106 Container storage area ACTIVE 06/18/2003 NA / 12 001 NA12 Permitted Nonhazardous

Industrial UnitYES /

Description from Company: This is Permit Unit No. 1 under Industrial Solid Waste Permit No. 39048 whi ch is a Container Storage Area for storage and

processing of nonhazardous w aste in drums or other containers.


Wastes Previously Managed at Unit: 90224091 Generated from the 90234092 Generated from the 90241191 Water-soluble liquids and 90261191 Water-soluble liquids and90206091 Generated from the 90216092 Generated from the

107 Container storage area ACTIVE 06/29/2004 NA / 12 002 NA12 Permitted Nonhazardous


Description from Company: This is Permit Unit No. 2 under Industrial Solid Waste Permit No. 39048 whi ch is a Container Storage Area for storage and

processing of nonhazardous w aste in roll-off boxes or other containers.


Wastes Previously Managed at Unit: 90011191 Non RCRA regulated rinse 90206091 Generated from the 90224091 Generated from the 90234092 Generated from the90216092 Generated from the 90241191 Water-soluble liquids and 90161192 Rinse water from tank 90261191 Water-soluble liquids and

108 Tank ACTIVE 05/10/2005 NA / 12 003 NA12 Permitted Nonhazardous


Description from Company: Wastewater treatment system permitted under ISWP No. 39048 consisting of 65 00 gallon tank, filter presses, ion exchange unit, R/O,

and the sumps that are used to introduce waste into the system.

System Types: 129 Other treatment 123 Settling or clarification 124 Phase separation

Wastes Previously Managed at Unit: 90206091 Generated from the 90224091 Generated from the 90234092 Generated from the 90261191 Water-soluble liquids and90241191 Water-soluble liquids and 9027207H Concentrate from R/O unit 9030601H Still bottoms 90216092 Generated from the

109 Waste water treatment plant ACTIVE 05/10/2005 12 / NA NA NA08 RCRA Permit exempt-waste


Description from Company: Wastewater treatment system consisting of flow equalization, free oil removal, p recipitation, and pH adjustment for tank truck

cleaning operation which dis charges to a POTW.

System Types: 123 Settling or clarification 121 Neutralization only 135 Discharge to sewer/POTW or NPDES (with prior storage - with or without treatment)

Wastes Previously Managed at Unit: 90011191 Non RCRA regulated rinse 90161192 Rinse water from tank



Description from Company: Tank T1 is used for oil recovery, phase separation, and neutralization. The tan k is part of an industrial wastewater treatment plant

with discharge water flowing to a POTW.


recovery, etc.

Wastes Previously Managed at Unit: 90261191 Water-soluble liquids and 90241191 Water-soluble liquids and




Page: 18

Date: 03/15/2012

Unit

Number

Unit

Type

Unit

Status

Date of

Status

Classes of Waste

Managed in Unit

Onsite / Offsite

Unit

Permit

Number

Unit #

on

Permit

Regulatory

Status

Deed Recording

Needed/Date



Description from Company: Tank T2 is ued for oil recovery, phase separation, and clarification. The tank is part of an industrial wastewater treatment plant with

discharge water fl owing to a POTW.


recovery, etc.

Wastes Previously Managed at Unit: 90171142 Treated Class 2 Wastewater 90261191 Water-soluble liquids and 90241191 Water-soluble liquids and

As of 03/06/2012, the next unassinged sequence number for UNITS is 141




Attachment 2 TCEQ Closure Report Checklist

Texas Commission on Environmental Quality Remediation Division

Closure Report Checklist (Revised July 28, 2011)

Title 30 of the Texas Administration Code (TAC) §335.8, establishes the obligation for persons to perform closure of waste management units (WMUs) used to store industrial solid waste or municipal hazardous waste. Closure is the act of permanently taking a WMU out of service. In order to close a WMU, a person must remove all waste from the WMU and demonstrate that a release from the WMU to the environment has not occurred. If a release has occurred, refer to 30 TAC 350 and the guidance memo, “Determining Which Releases are Subject to TRRP”.

The Texas Commission on Environmental Quality (TCEQ), Remediation Division developed this checklist to assist persons in preparing a closure report for units listed on the facilities Notice of Registration(NOR). This checklist should not be used for Resource Conservation and Recovery Act (RCRA) units (permitted or interim status). Persons/Facilities that are in the TCEQ’s Corrective Action (CA) or Voluntary Cleanup Program (VCP) should close/transfer all WMUs for properties which will change ownership. Persons/Facilities that are in CA or VCP which will remain active should investigate land base WMUs for possible releases. Closure reports submitted to the Remediation Division should include the following general information:

Owner / operator information and hard copy of the Notice of Registration (NOR),

Location of facility (address, city), Description of the WMU, including NOR No., construction,

condition, operational history, waste(s) managed, waste characterization results (process knowledge or analytical results), and any waste spill(s) and cleanup response(s),

Reason for the WMU closure (for example, facility closing, TCEQ inspection),

A map of the facility showing the WMU location, Description of how the WMU was closed and demonstrated to not

have released to the environment, Photographs with descriptions of the WMU before, during, and

following closure, and a Description of the WMU and waste dispositions, including copies of

waste manifest, if applicable.

Other supporting documentation may include completed facility inspection logs and maintenance reports.

TCEQ Remediation Division Closure Report Checklist Page 2 of 2

For less-than 90 day containers, also provide a discussion that demonstrates the container(s) was empty in accordance with 40 Code of Federal Regulations §261.7.

For less-than 90 day tanks, also provide a discussion of the decontamination process including analytical results for rinsate or wipe samples.

If any samples were collected, submit the following:

Description of sample (rinsate, soil, etc.), Reports of chemical analyses, chain of custody forms and QA/QC

data, Summary table of analytical results, and a Map that shows the sampling locations.

For WMUs which are below ground or in direct contact with the ground surface (for example, surface impoundments, landfills, underground storage tanks, sumps) soil samples are required for release determination and closure. Closure reports submitted to the Remediation Division should include the following:

Soil sample depths and description of soil surrounding WMU, Table of analytical results. Investigation sample results should be

compared to the appropriate regulatory values (e.g. residential assessment level or background),

Map that shows borings or sampling locations demonstrating extent of COCs, if any,

Depth and construction details of WMU, and Reports of chemical analyses, chain of custody forms and QA/QC

data.

Additional guidance on the closure process may be found in Closure of Waste-Management Units Subject to TRRP (RG-366/TRRP-2A) and TRRP Compatibility with RCRA (RG–366/TRRP-3). These guidance documents may be obtained from the TCEQ’s TRRP Guidance and Forms page at http://www.tceq.texas.gov/remediation/trrp/guidance.html.

An original and one copy of the closure report should be submitted to the Texas Commission on Environmental Quality, Remediation Division (MC-127), P. O. Box 13087, Austin, TX 78711-3087, and one copy of the closure report should be submitted to your local TCEQ Regional Office.




Attachment 3 Notice of Registration Units Photolog

1 160516 CES NOR Units Photolog.Doc

PHOTOGRAPHIC LOG

Client Name: CES Griggs Road PRP Group

Site Location: CES Environmental Services, 4904 Griggs Road, Houston, Texas

Project No. 4014

Photo No. 1

Date: 6/4/15

Description: NOR 001 Unit Type: Sump Description from Company: None Located between the Safe Wash and Drum Cleaning Buildings. Verified with 1985 Younger facility layout (Figure 3).

Photo No. 2

Date: 6/4/15

Description: NOR 002 Unit Type: Miscellaneous Storage Containers Description from Company: None Located on south side of Equipment Fleet Maintenance Building per 1998 Suttles Site Plan (Figure 3). Picture of south side of Equipment Fleet Maintenance Building after EPA/TCEQ removal action. Tanks are NOR 102 and metal storage area is NOR 105.


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 3

Date: 4/26/16

Description: NOR Unit 003 Unit Type: Container Storage Area Description from Company: Old Wash Rack designated as a waste management unit for miscellaneous 55-gallon drums Location in northwest corner per 1998 Suttles Site Plan. Photo shows location of Old Wash Rack (Safe Wash Building) after EPA/TCEQ removal action.

Photo No. 4

Date: 6/4/15

Description: NOR Unit 004 Unit Type: Tank Description from Company: Steel tank Located inside Equipment and Fleet Maintenance Building (north side) per 1998 Suttles Site Plan. Picture of NOR area after EPA/TCEQ removal action.


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 5

Date: 9/27/14

Description: NOR Unit 005 Unit Type: Miscellaneous Storage Container Description from Company: Dumpster (7-15 cy) Located west of Wayland Street right of way per 1998 Suttles Site Plan (Figure 3).

Photo No. 6

Date: 6/4/15

Description: NOR Unit 006 Unit Type: Sump Description from Company: Subsurface sumps or oil/water separator basins unit Oil/Water Separator located between the Safe Wash and Drum Cleaning Buildings. Verified with 1998 Suttles Site Plan (Figure 3).


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 7

Date: 4/26/16

Description: NOR Unit 007 Unit Type: Tank Description from company: pH Adjustment Unit Located inside Safe Wash Building per 1998 Suttles Site Plan (Figure 3). Picture of Safe Wash building area after EPA/TCEQ removal action.

Photo No. 8

Date: 5/18/16

Description: NOR Unit 008 Unit Type: Tank Description from Company: 2 x 50-gallon tanks Located inside Truck Maintenance Building per 1998 Suttles Site Plan (Figure 3). Picture of Truck Maintenance Building after EPA/TCEQ removal action.


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 9

Date: 6/14/15

NO PICTURE AVAILABLE

Description: NOR Unit 009 Unit Type: Miscellaneous Storage Containers Description from Company: Container Storage Area Location Unknown

Photo No. 10

Date: 11/4/14

Description: NOR Unit 101 Unit Type: Tank Description from Company: Vacuum box in tank wash for first flush Shown on July 18, 2008 Stormwater Pollution Prevent Plan (SWPPP) map (Figure 2) as next to southwest corner of Equipment/Fleet Maintenance Building Photo of vacuum boxes in Equipment/Fleet Maintenance Building during EPA/TCEQ removal action. No vacuum boxes currently located at Site.


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 11

Date: 6/4/15

Description: NOR Unit 102 Unit Type: Tank Description from Company: Non-hazardous Wastewater tank Shown on July 18, 2008 SWPPP map (Figure 2) as two tanks adjacent to south wall of Equipment/Fleet Maintenance Building. Picture of two fiberglass tanks next to Equipment and Fleet Maintenance Building.

Photo No. 12

Date: 4/26/16

Description: NOR Unit 103 Unit Type: Miscellaneous Storage Containers Description from Company: Non-hazardous sludge box Shown on July 18, 2008 SWPPP map (Figure 2) in Tank Truck Cleaning Building (Safe Wash Building). Photo of Safe Wash Area; no sludge boxes located at Site.


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 13

Date: 9/17/15

Description: NOR Unit 104 Unit Type: Miscellaneous Storage Containers Description from Company: 40 cubic yard open top box for plant trash Shown on July 18, 2008 SWPPP map (Figure 2) adjacent to Equipment Cleaning Building (Drum Cleaning). Drum Cleaning Building removed during 3rd party demolition; no open top boxes located at Site.

Photo No. 14

Date: 4/26/16

Description: NOR Unit 105 Unit Type: Container Storage Area Description from Company: Hazardous Waste Container Storage Area Shown on July 18, 2008 SWPPP map (Figure 2) as area adjacent to south wall inside Equipment/Fleet Maintenance Building. Photo showing empty area after EPA/TCEQ removal action. Signs for TCEQ Unit #105 can be seen next to mailbox and on metal wall on right side of picture.


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 15

Date: 2/14/16

Description: NOR Unit 106 Unit Type: Container Storage Area Description from Company: Permit Unit 1 under ISW Permit 39048 Container Storage Area for storage and processing of non-hazardous waste in drums or other containers. Photo showing empty area after EPA/TCEQ removal action.

Photo No. 16

Date: 2/14/16

Description: NOR Unit 107 Unit Type: Container Storage Area Description from Company: Permit Unit 2 under ISW Permit 39048 container Storage Area for storage and processing of non-hazardous waste in roll-off boxes or other containers. Photo after EPA/TCEQ removal action.


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 17

Date: 2/14/16

Description: NOR Unit 108 Unit Type: Tank Description from Company: WW treatment system under ISW Permit 39048 with 6,500 gallon tank, filter presses, ion exchange unit, R/O and sumps. Photo of tank with TCEQ Unit #108 label.

Photo No. 18

Date: 2/14/16

Description: NOR Unit 109 Unit Type: Wastewater Treatment Plant Description from Company: WW Treatment system consisting of flow equalization, free oil removal, precipitation and pH adjustment for tank truck cleaning operation. Photo of shed with TCEQ Unit #109 sign.


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 19

Date: 2/14/16

Description: NOR Unit 110 Unit Type: Tank Description from Company: Tank T1 for oil recovery, phase separation, and neutralization. Part of industrial waste water treatment plant.

Photo No. 20

Date: 5/18/16

Description: NOR Unit 111 Unit Type: Tank Description from Company: Tank T2 for oil recovery, phase separation, and clarification. Part of industrial waste water treatment plant.


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 21

Date: 2/14/16


Photo No. 22

Date: 2/14/16



PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 23

Date: 2/14/16


Photo No. 24

Date: 2/14/16



PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 25

Date: 2/14/16

Description: NOR Units 116 and 118 Unit Type: Tank Description from Company: Tanks T7 and T9 for oxidation, biotreatment and separation of organics from water. Part of industrial waste water treatment plant.

Photo No. 26

Date: 2/14/16

Description: NOR Unit 117 Unit Type: Tank Description from Company: Tank T8 for oxidation, biotreatment and separation of organics from water. Part of industrial waste water treatment plant.


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 27

Date: 2/14/16

Description: NOR Unit 119 Unit Type: Tank Description from Company: Tank T10 for precipitation of dissolved metals, neutralization of acids/bases, settling of suspended solids from watr. Part of industrial waste water treatment plant.

Photo No. 28

Date: 2/14/16

Description: NOR Unit 120 Unit Type: Tank Description from Company: Tank T11 for precipitation of dissolved metals, neutralization of acids/bases, settling of suspended solids from water. Part of industrial waste water treatment plant.


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 29

Date: 2/14/16

Description: NOR Unit 121 Unit Type: Tank Description from Company: Tank T12 for precipitation of dissolved metals, neutralization of acids/bases, settling of suspended solids from water. Part of industrial waste water treatment plant.

Photo No. 30

Date: 5/18/16

Description: NOR Unit 122 Unit Type: Tank Description from Company: Water solids separator phase separation, clarification, and solids setting. Part of industrial waste water treatment plant.


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 31

Date: 4/26/16

Description: NOR Unit 123 Unit Type: Tank Description from Company: Tank Wash Sump Water.

Photo No. 32

Date: 4/26/16

Description: NOR Units 126, 127, and 128 Unit Type: Tank Description from Company: 20,000-gallon Clarification and Settling Tanks. FT1001 (WMU 126) on left; FT1002 (WMU 128) third from left; FT1004 (WMU 127) on right. Green frac tank is FT5180.


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 33

Date:


Description: NOR Unit 129 Unit Type: Tank Description from Company: Clarification and Settling Location unknown

Photo No. 34

Date: 11/4/14

Description: NOR Unit 130 Unit Type: Sump Description from Company: Concrete containment area with sump that holds truck wash rinse water. Condition after EPA/TCEQ removal action.


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 35

Date: 11/4/14

Description: NOR Unit 131 Unit Type: Sump Description from Company: Concrete containment area with sump that holds drum cleaning wash water. Condition after EPA/TCEQ removal action; building removed by 3rd party.

Photo No. 36

Date:




PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 37

Date:



Photo No. 38

Date:




PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 39

Date:



Photo No. 40

Date:




PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 41

Date:



Photo No. 42

Date:




PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 43

Date:


Description: NOR Unit 139 Unit Type: Tank Description from Company: Clarification and Settling. Frac tank never used. Sent back to rental company Location unknown

Photo No. 44

Date:


Description: NOR 140 Unit Type: Tank Description from Company: Clarification and Settling. Frac tank never used. Sent back to rental company Location unknown




Attachment 4 Other Waste Management Units Photolog

1 160516 CES Other Unit Photolog Original.Docx

PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 1

Date: 6/4/15

Description: Main Processing Building looking south from 4904 Griggs Road Entrance. Truck Maintenance building can be seen in background and FT1001 can be seen on left side of picture.

Photo No. 2

Date: 6/14/15

Description: Main Processing Building – Sump 14 Wastewater Treatment Plant


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 3

Date: 6/4/15

Description: Main Processing Building – Trench 1 North end looking south to vehicle ramp

Photo No. 4

Date: 6/14/15

Description: Main Processing Building – Trench 2 South end looking north to wastewater treatment plant (WWTP)


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 5

Date: 6/15/15

Description: Main Processing Building – Trench 3 Looking southeast

Photo No. 6

Date: 6/15/15

Description: Main Processing Building – Trench 4 Looking south to WWTP


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 7

Date: 2/14/16

Description: Main Processing Building – Trench 5 Looking northwest at SB-02

Photo No. 8

Date: 2/14/16

Description: Main Processing Building – Trench 6 looking north. SB-03 is located east of Trench 6 and marked with pink pin flag.


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 9

Date: 4/26/16

Description: Main Processing Building – West Side of Building looking south along Wayland Street.

Photo No. 10

Date: 4/26/16

Description: Main Processing Building – Sump 11 Located outside, northwest corner of the building under wood cover (Round)


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 11

Date: 2/14/16

Description: Main Processing Building – Sump 12 Located outside, west of the building.

Photo No. 12

Date: 2/14/16

Description: Main Processing Building – Sump 13 Located outside, west of the building.


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 13

Date: 2/14/16

Description: Main Processing Building – Sump 15 Located outside and south of the building.

Photo No. 14

Date: 4/26/16

Description: Main Processing Building – Sump 23 Located outside on west side of building behind NOR 106.


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 15

Date: 6/28/16

Description: Lime tank

Photo No. 16

Date: 4/26/16

Description: Safe Wash Area Looking northwest (located south of Main Processing Building).


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 17

Date: 6/14/15

Description: Safe Wash – Oil/Water Separator Contents are unknown.

Photo No. 18

Date: 6/4/15

Description: Safe Wash – Sump 2 Located adjacent to MW-01.


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 19

Date: 6/4/15

Description: Safe Wash – Sump 3 Located west of Oil/Water Separator

Photo No. 20

Date: 2/14/16

Description: Safe Wash – Trench 1 through 5


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 21

Date: 5/18/16

Description: Drum Cleaning – Sump 4 Example of grates with solids to be removed

Photo No. 22

Date: 4/26/16

Description: Drum Cleaning (after removal of metal building by 3rd party)


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 23

Date: 11/4/14

Description: Drum Cleaning – Sump 5

Photo No. 24

Date: 6/14/15

Description: Drum Cleaning – Sump 6 Adjacent to SB-05 in drive near Drum Cleaning Building


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 25

Date: 6/14/15

Description: Drum Cleaning – Sump 7 Adjacent to SB-05 in drive near Drum Cleaning Building

Photo No. 26

Date: 6/10/15

Description: Frac tanks behind Admin building


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 27

Date: 8/29/15

Description: Equipment & Fleet Maintenance Building

Photo No. 28

Date: 11/4/14

Description: Equipment & Fleet Maintenance Building – Sumps 8A through 8C. Vacuum box removed by EPA/TCEQ in 2014/2015 Removal Action.


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 29

Date: 6/4/15

Description: Equipment & Fleet Maintenance Building – Trench 1 and 2

Photo No. 30

Date: 4/26/16

Description: Equipment & Fleet Maintenance Building – Trenches 3, 4, 5, and 6


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 31

Date: 4/26/16

Description: Equipment & Fleet Maintenance Building – Sump 9

Photo No. 32

Date: 3/16/16

Description: Looking northeast towards North and South Tank Farm


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 33

Date: 6/4/15

Description: North and South Tank Farm – Sump 20

Photo No. 34

Date: 6/4/15

Description: North Tank Farm - Sump 21


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 35

Date: 6/4/15

Description: South Tank Farm – Sump 22

Photo No. 36

Date: 9/15/15

Description: Drum/Tote Storage


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 37

Date: 4/26/16

Description: Drum/Tote Storage – Sump 10 Located adjacent to SB-15

Photo No. 38

Date: 6/4/15

Description: Drum/Tote Storage – Sump 17 Located adjacent to SB-14


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 39

Date: 6/4/15

Description: Drum/Tote Storage – Sump 18 Located adjacent to SB-14 inside of containment

Photo No. 40

Date: 6/4/15

Description: Drum/Tote Storage – Sump 19 Located adjacent to SB-13 inside of containment


PHOTOGRAPHIC LOG



Project No. 4014

Photo No. 41

Date: 3/13/16

Description: Welding Shop

Photo No. 42

Date: 6/4/15

Description: Welding Shop – Sump 16




Attachment 5 30 TAC 335.521(a)(1) Texas Class 2 Regulatory Levels

Constituents of Concern and Their Maximum Leachable Concentrations.

Values are based on information contained in Federal Registers Vol. 55 / Friday, July 27, 1990; Vol. 56 / June 7, 1991; and Integrated Risk Information Systems, U.S. Environmental Protection Agency, and 40 CFR 264 Appendix 9.

Concentration Compound CAS No. (mg/l)

Acenaphthene 83-32-9 210 Acetone 67-64-1 400 Acetonitrile 75-05-8 20 Acetophenone 98-86-2 400 Acrylamide 79-06-1 0.08 Acrylonitrile 107-13-1 0.6 Aniline 62-53-3 60 #Anthracene 120-12-7 1050 Antimony 7440-36-0 1 Arsenic 7440-38-2 1.8 Barium 7440-39-3 100.0 Benzene 71-43-2 0.50 Benzidine 92-87-5 0.002 Beryllium 7440-41-7 0.08 Bis(2-chloroethyl)ether 111-44-4 0.3 Bis(2-ethylhexyl) 117-81-7 30 phthalate -- -- Bromodichloromethane 75-27-4 0.3 Bromomethane 74-83-9 5 Butylbenzyl phthalate 85-68-7 700 Cadmium 7440-43-9 0.5 Carbon disulfide 75-15-0 400 Carbon tetrachloride 56-23-5 0.50 Chlordane 57-74-9 0.03 Chlorobenzene 08-90-7 70 Chloroform 67-66-3 6.0 #Chloro-m-cresol, p 59-50-7 7000 2-Chlorophenol 95-57-8 20 Chromium 7440-47-3 5.0 m-Cresol 108-39-4 200.0* o-Cresol 95-48-7 200.0* p-Cresol 106-44-5 200.0* DDD 72-54-8 1 DDE 72-55-9 1 DDT 50-29-3 1 Dibutyl phthalate 84-74-2 400 1,4-Dichlorobenzene 106-46-7 7.5 3,3-Dichlorobenzidine 91-94-1 0.8 1,2-Dichloroethane 107-06-2 0.50 Dichlorodifluoromethane 75-71-8 700 1,1-Dichloroethylene 75-35-4 0.6 1,3-Dichloropropene 542-75-6 1 2,4-Dichlorophenol 120-83-2 10 2,4-Dichlorophenoxy- 94-75-7 10.0 acetic acid (2,4-D) -- -- Dieldrin 60-57-1 0.02 Diethyl phthalate 84-66-2 3000 Dimethoate 60-51-5 70 #2,4-Dimethylphenol 105-67-9 70 #2,6-Dimethylphenol 576-26-1 21 m-Dinitrobenzene 99-65-0 0.4 2,4-Dinitrophenol 51-28-5 7 2,4 -Dinitrotoluene 602-01-7 0.13 (and 2,6-, mixture) -- -- #Dinoseb 88-85-7 3.5 1,4-Dioxane 123-91-1 30 Dioxins (Poly chlorinated dibenzo-p-dioxins) 2,3,7,8-TCDD 1746-01-6 0.005 1,2,3,7,8-PeCDD 0321-76-4 0.010 1,2,3,4,7,8-HxCDD 57653-85-7 0.050 1,2,3,6,7,8-HxCDD 34465-46-8 0.050 1,2,3,7,8,9-HxCDD 0.050 Diphenylamine 122-39-4 90 1,2-Diphenylhydrazine 122-66-7 0.4 Disulfoton 298-04-4 0.1 Endosulfan 959-98-8 0.2 Endrin 72-20-8 0.02 #2-Ethoxyethanol 110-80-5 1400 Ethylbenzene 100-41-4 400 Ethylene dibromide 106-93-4 0.004 #Ethylene Glycol 107-21-1 7000 #Fluoranthene 206-44-0 140 #Fluorene 86-73-7 140 Furans (Polychlorinated dibenzo furans) 2,3,7,8-TCDF 51207-31-9 0.050 1,2,3,7,8-PeCDF 0.100 2,3,4,7,8-PeCDF 0.010 1,2,3,4,7,8-HxCDF 0.050 1,2,3,6,7,8-HxCDF 0.050 1,2,3,7,8,9-HxCDF 0.050 Heptachlor 76-44-8 0.008 (and its hydroxide) -- -- Heptachlor epoxide 1024-57-3 0.04 Hexachlorobenzene 118-74-1 0.13 Hexachloro-1,3-butadiene 87-68-3 0.4 Hexachlorocyclopentadiene 77-47-4 20 Hexachloroethane 67-72-1 3.0 Hexachlorophene 70-30-4 1

10/2/2016https://texreg.sos.state.tx.us/fids/30_0335_0521-1.html

Isobutyl alcohol 78-83-1 1000 Isophorone 78-59-1 90 Lead 7439-92-1 1.5 Lindane 58-89-9 0.3 Mercury 7439-97-6 0.2 Methacrylonitrile 126-98-7 0.4 Methomyl 16752-77-5 90 Methoxychlor 72-43-5 10.0 #2-Methoxyethanol 109-86-4 14.0 Methyl ethyl ketone 78-93-3 200.0 Methyl isobutyl ketone 108-10-1 200 Methylene chloride 75-09-2 50 Methyl parathion 298-00-0 0.9 #Mirex 2385-85-5 0.7 Nickel 7440-02-0 70 Nitrobenzene 98-95-3 2.0 N-Nitroso-di-n-butylamine 924-16-3 0.06 N-Nitrosodiphenylamine 86-30-6 70 N-Nitrosomethylethylamine 10595-95-6 0.02 N-Nitroso-n-propylamine 621-64-7 0.05 N-Nitrosopyrrolidine 930-55-2 0.2 p-Phenylene diamine 106-50-3 20 Parathion 56-38-2 20 Pentachlorobenzene 608-93-5 3 Pentachloronitrobenzene 82-68-8 10 Pentachlorophenol 87-86-5 100.0 Phenol 108-95-2 2000 Pronamide 23950-58-5 300 #Pyrene 129-00-0 5.9 Pyridine 110-86-1 4 Selenium 7782-49-2 1.0 Silver 7440-22-4 5.0 Styrene 100-42-5 700 1,1,1,2-Tetrachloroethane 630-20-6 10 1,1,2,2-Tetrachloroethane 79-34-5 2 Tetrachloroethylene 127-18-4 0.7 2,3,4,6-Tetrachlorophenol 58-90-2 100 Toluene 108-88-3 1000 Toxaphene 8001-35-2 0.3 trans-1,3-Dichloro- 542-75-6 1 propene -- -- Tribromomethane 75-25-2 70 (Bromoform) 1,2,4-Trichlorobenzene 120-82-1 70 1,1,1-Trichloroethane 71-55-6 300 Trichloroethylene 79-01-6 0.5 1,1,2-Trichloroethane 79-00-5 6 Trichlorofluoromethane 75-69-4 1000 2,4,5-Trichlorophenoxy- 93-72-1 1.0 propionic acid -- -- (2,4,5 TP or Silvex) 1,2,3-Trichloropropane 96-18-4 20 2,4,5-Trichlorophenol 95-95-4 400.0 2,4,6-Trichlorophenol 88-06-2 2 Vanadium Pentoxide 1314-62-1 30 Vinyl chloride 75-01-4 0.2 Xylenes (all isomers) 1330-82-1 7000

---------------------------------------------------------------- # Constituent added since original rule publication. * If o-, m-, and p-Cresol concentrations cannot be differen- tiated, the total cresol concentration is used. The Maximum Concentration for total cresol is 200.0 mg/l.

10/2/2016https://texreg.sos.state.tx.us/fids/30_0335_0521-1.html

CLOSURE PLAN WASTE MANAGEMENT UNITSClosure Plan Waste Management Units Project No. 4014 1-1...

Documents

Transcript of CLOSURE PLAN WASTE MANAGEMENT UNITSClosure Plan Waste Management Units Project No. 4014 1-1...