Chem 21 Schedule - Dr. Kline - Fall...

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Chem 21 Schedule - Dr. Kline - Fall 2019 Monday - Lecture Tuesday - Lab Section 4071 Wednesday - Lecture Thursday - Lab Section 4072 1 8/26 8/27 8/28 8/29 Course Information; Intro to OChem; Ch 1-Review of Genl Chem Lab and Safety Info (*); Locker Check-in Ch 2-Molecular Representations Lab and Safety Info (*); Locker Check-In 2 9/2 Labor Day Holiday 9/3 9/4 Quiz 1 9/5 Acid-Base Extraction to Separate the Components of an Analgesic Tablet (G) (*) Ch 2-cont. Acid-Base Extraction to Separate the Components of an Analgesic Tablet (G) (*) 3 9/9 9/10 9/11 Quiz 2 9/12 Ch 3-Acids & Bases Preparation of Salicylic Acid (G) (*); Finish TLC from Extraction Lab (*) Ch 3-cont. Preparation of Salicylic Acid (G) (*); Finish TLC from Extraction Lab (*) 4 9/16 9/17 9/18 Quiz 3 9/19 Ch 4-Alkanes and Cycloalkeanes, including conformations and isomers. NMR and mp of Salicylic Acid (*); Set up fermentation for Ethanol Lab (&); Lab Activity - Model Exercise I Ch 4-cont. NMR and mp of Salicylic Acid (*); Set up fermentation for Ethanol Lab (&); Lab Activity - Model Exercise I 5 9/23 9/24 9/25 Test 1 9/26 Ch 4-cont.; Sect 12.1-12.3 & 13.1-13.4 - Intro to and Naming of Alcohols and Ethers Production of Ethanol- Distillation (G) (&) Production of Ethanol- Distillation (G) (&) 6 9/30 10/1 10/2 Lab Quiz #1 (*) 10/3 Ch 5-Stereoisomerism No lab today Ch 5-cont. Lab Activity - Model Exercise II 7 10/7 10/8 10/9 10/10 Ch 6-Chemical Reactivity and Mechanisms Lab Activity - Model Exercise II Ch 6-cont. Isolation of Limonene from Orange Rinds via Steam Distillation (G) (&) 8 10/14 10/15 10/16 Quiz 4 10/17 Ch 6- finish; Ch 14-Intro to Spectroscopy Isolation of Limonene from Orange Rinds via Steam Distillation (G) (^) Ch 14-Mass Spectrometry and Infrared Spectroscopy Column Chromatography to Separate the Components of an Analgesic Tablet (G) (&) 9 10/21 10/22 10/23 Quiz 5 10/24 Ch 14-cont.; Ch 15-Nuclear Magnetic Resonance Spectroscopy Column Chromatography to Separate the Components of an Analgesic Tablet (G) (&) Ch 15-cont. Lab Activity - Identification of a Liquid Unknown by IR and NMR Spectroscopy (S)(U); Finish TLC for Column Lab (&) 10 10/28 10/29 10/30 Test 2 10/31 Ch 7-Substitution and Elimination Reactions Lab Activity - Identification of a Liquid Unknown by IR and NMR Spectroscopy (S)(U); Finish TLC for Column Lab (&) Synthesis of Butyl Benzoate (G) (^) Week 1

Transcript of Chem 21 Schedule - Dr. Kline - Fall...

Page 1: Chem 21 Schedule - Dr. Kline - Fall 2019homepage.smc.edu/kline_peggy/chem-21/chem_21_sched_f19.pdf · 2019-11-16 · 6 9/30 10/1 10/2 Lab Quiz #1 (*) 10/3 Ch 5-Stereoisomerism No

Chem 21 Schedule - Dr. Kline - Fall 2019Week Monday - Lecture Tuesday - Lab Section 4071 Wednesday - Lecture Thursday - Lab Section 4072

1 8/26 8/27 8/28 8/29Course Information; Intro to OChem; Ch 1-Review of Genl Chem

Lab and Safety Info (*); Locker Check-in

Ch 2-Molecular Representations

Lab and Safety Info (*); Locker Check-In

2 9/2 Labor Day Holiday 9/3 9/4 Quiz 1 9/5

Acid-Base Extraction to Separate the Components of an Analgesic Tablet (G) (*)

Ch 2-cont. Acid-Base Extraction to Separate the Components of an Analgesic Tablet (G) (*)

3 9/9 9/10 9/11 Quiz 2 9/12Ch 3-Acids & Bases Preparation of Salicylic Acid (G) (*);

Finish TLC from Extraction Lab (*)Ch 3-cont. Preparation of Salicylic Acid (G) (*);

Finish TLC from Extraction Lab (*)

4 9/16 9/17 9/18 Quiz 3 9/19

Ch 4-Alkanes and Cycloalkeanes, including conformations and isomers.

NMR and mp of Salicylic Acid (*); Set up fermentation for Ethanol Lab (&); Lab Activity - Model Exercise I

Ch 4-cont. NMR and mp of Salicylic Acid (*); Set up fermentation for Ethanol Lab (&); Lab Activity - Model Exercise I

5 9/23 9/24 9/25 Test 1 9/26

Ch 4-cont.; Sect 12.1-12.3 & 13.1-13.4 - Intro to and Naming of Alcohols and Ethers

Production of Ethanol- Distillation (G) (&)

Production of Ethanol- Distillation (G) (&)

6 9/30 10/1 10/2 Lab Quiz #1 (*) 10/3

Ch 5-Stereoisomerism No lab today Ch 5-cont. Lab Activity - Model Exercise II

7 10/7 10/8 10/9 10/10

Ch 6-Chemical Reactivity and Mechanisms

Lab Activity - Model Exercise II Ch 6-cont. Isolation of Limonene from Orange Rinds via Steam Distillation (G) (&)

8 10/14 10/15 10/16 Quiz 4 10/17Ch 6- finish; Ch 14-Intro to Spectroscopy

Isolation of Limonene from Orange Rinds via Steam Distillation (G) (^)

Ch 14-Mass Spectrometry and Infrared Spectroscopy

Column Chromatography to Separate the Components of an Analgesic Tablet (G) (&)

9 10/21 10/22 10/23 Quiz 5 10/24

Ch 14-cont.; Ch 15-Nuclear Magnetic Resonance Spectroscopy

Column Chromatography to Separate the Components of an Analgesic Tablet (G) (&)

Ch 15-cont. Lab Activity - Identification of a Liquid Unknown by IR and NMR Spectroscopy (S)(U); Finish TLC for Column Lab (&)

10 10/28 10/29 10/30 Test 2 10/31Ch 7-Substitution and Elimination Reactions

Lab Activity - Identification of a Liquid Unknown by IR and NMR Spectroscopy (S)(U); Finish TLC for Column Lab (&)

Synthesis of Butyl Benzoate (G) (^)

Week

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Production of Ethanol - Distillation(G) (&)
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Lab Quiz #1 (*)
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Quiz only; no electricity
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Mass Spec and IR
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H and C NMR Lecture
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Finish IR, start NMR
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H and C NMR Lecture
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Campus Closed 🔥
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(&)
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(Dr. Kline jury duty)
Page 2: Chem 21 Schedule - Dr. Kline - Fall 2019homepage.smc.edu/kline_peggy/chem-21/chem_21_sched_f19.pdf · 2019-11-16 · 6 9/30 10/1 10/2 Lab Quiz #1 (*) 10/3 Ch 5-Stereoisomerism No

11 11/4 Lab Quiz #2 (&) 11/5 11/6 Quiz 6 11/7Ch 7-cont. Synthesis of Butyl Benzoate (G) (^) Ch 7-cont. E2 Reaction of 2-Bromoheptane

(“dry” lab) (^); Analysis of Butyl Benzoate (^)

12 11/11 Veteran’s Holiday 11/12 11/13 Quiz 7 11/14

E2 Reaction of 2-Bromoheptane (“dry” lab) (^); Analysis of Butyl Benzoate (^)

Ch 8-Addition Reactions of Alkenes

Stereochemistry of Bromine Addition to trans-Cinnamic Acid (G) (^)

13 11/18 11/19 11/20 Quiz 8 11/21Ch 8-cont. Stereochemistry of Bromine

Addition to trans-Cinnamic Acid (G) (^)

Ch 8-cont. Analysis of Bromination Product (^); Lecture Material - Chapter 9- Alkynes

14 11/25 Test 3 11/26 11/27 11/28 Thanksgiving Holiday

Analysis of Bromination Product (^); Lecture Material - Chapter 9- Alkynes

Ch 9 - cont. (from lab)

15 12/2 12/3 12/4 Quiz 9 12/5

Ch 10 - Radical Reactions Lab Check-Out Ch 10 - cont. Lab Check-Out

16 12/9 Lab Quiz #3 (^) 12/10 12/11 12/12Synthesis Examples No lab today “Review” session for Final No lab today

17 12/16 Final Exam 6:45-9:45 pm 12/17 12/18 12/19

Lab notations: G=gloves worn for at least a portion of this experiment; refer to individual experiments. S=solo lab (not with lab partner). U=lab that includes the use of an unknown substance. (*), (&), and (^) refer to the information that will be included on each lab quiz.

Lecture topics may deviate from this schedule without notice. Any changes in test of quiz dates will be announced in lecture and/or via official SMC email.

Please notify the instructor by email within the first week of class if any quiz or test date conflicts with a day of religious observance.

Quizzes (~15 minutes) will be given at the end of class time. Tests (~2.25 hours) will start at the beginning of the class time.

Chapters are from the THIRD edition of the Klein Organic book.

Dr. Peggy Kline | Santa Monica College | http://homepage.smc.edu/kline_peggy/ | Last updated 7/28/2019

Monday - Lecture Tuesday - Lab Section 4071 Wednesday - Lecture Thursday - Lab Section 4072Week

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Chapter 7 - continued
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Proton NMR Examples; Start Chapter 7 (SN and E)
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11/15/2019 🤦‍♀️
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Also lecture makeup - Ch 7
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Also lecture makeup - Ch 7
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Finish Ch 7; start Ch 8
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no HVAC = no hoods
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Lecture - Ch 10 (sect 1-6); NMR examples
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Lecture - Ch 10 (sect 1-6); NMR examples
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Stereochemistry of Bromine Addition to trans-Cinnamic Acid and Analysis (G) (^)
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Stereochemistry of Bromine Addition to trans-Cinnamic Acid and Analysis (G) (^)
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Chapter 8 - continued; also sect. 10.7 and 10.10)
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Chapter 9 - Alkynes
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Ch 9- cont.
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, incl sect 10.12