CHE515 - Lesson Plan_Sept 2012 - Jan2013

LESSON PLAN CHE 515 INSTRUMENTAL

CHEMISTRY FOR ENGINEERSFACULTY OF CHEMICAL ENGINEERING

UNIVERSITI TEKNOLOGI MARA

1.0 COURSE INFORMATION

COURSE NAME : INSTRUMENTAL CHEMISTRY FORENGINEERS

COURSE CODE : CHE515PROGRAM : EH220, EH221 SEMESTER : 3/4CREDIT HOURS : 3.0CONTACT HOURS : 5.0COURSE STATUS : CORE (PASSING GRADE: C)PRE-REQUISITE : Nil

2.0 SYNOPSISThis is an advanced chemistry course. The topics covered concern the use of modern analytical methods in elucidating chemical compounds.

3.0 OBJECTIVESUpon completion of this course, students should be able to:1. Identify the most appropriate analytical method for structural determination and

environmental heavy metal pollution assessment.2. Analyze spectra and determine the functionality and structure of an unknown substance.3. Perform experiments to achieve a predetermined goal.

4.0 METHODS OF INSTRUCTIONLecture and LaboratoryLecture : 2 hours/weekLaboratory : 3 hours/week

5.0 LESSON PLAN

Week Chapter/Content Activities

1 – 2

Chapter 1:UV and Visible Spectroscopy1.1 Excitation and Absorption Laws: HOMO and LUMO 1.2 Solvent Effects1.3 Chromophores, Conjugation, Shifting1.4 Electronic Transitions1.5 Interpreting Spectra1.6 Beer-Lambert Law

Read the recommended text and reference books

Practice at the end of the chapter

Discussion

3 – 4

Chapter 2: Infrared Spectroscopy2.1 FTIR Components (Interferometer)2.2 Molecular Vibrations and Absorption Frequencies2.3 Type of Samples2.4 Interpreting Spectra 2.5 Hyphenated Methods Involving IR2.6 Applications2.7 Analysis (Quantitative and qualitative)



Discussion

5 – 6 Chapter 3: Mass Spectroscopy3.1 Ions Productions (Readily volatile and Poorly Volatile)3.2 Relative Atomic Mass (RAM)3.3 Structural Information

Read the recommended text and reference




3.4 Ion Analysis3.5 Liquid Chromatography-Mass Spectrometry, and GC-MS

books Practice at the end

of the chapter Discussion

Test 1

7 – 9

Chapter 4: Atomic Spectroscopy4.1 Atomization Methods4.2 Atomic Absorption Spectroscopy (AAS)4.3 Atomic Emission Spectroscopy (ICP)4.4 Atomic Fluorescence Spectroscopy (AFS)



Discussion

10 – 12

Chapter 5: Nuclear Magnetic Resonance5.1 Nuclear Spin and Resonance5.2 Chemical Shift 5.3 Factors Affecting Chemical Shifts5.4 1H-NMR (Splitting, Coupling, Integration of 1H-NMR

Absorption)5.5 13C-NMR



Discussion

13 – 14

Chapter 6: Chromatography6.1 Chromatographic Techniques6.2 Theory of Column Efficiency in Chromatography6.3 Thin Layer Chromatography6.4 Gas Chromatography6.5 Liquid Chromatography



Discussion

Test 2

3-12

Laboratory Work*1. Identification of organic compounds using UV-Vis and IR

spectroscopy.2. ICP determination of metal in waste water.3. AAS determination of calcium in commercial supplement

tablets.4. NMR analysis of a constitutional isomer.5. Determination of organic compound using HPLC

* Not limited to the above list but subjected to the equipment availability

Hands on experiment in the Instrumentation

Laboratory

6.0 ASSESSMENTTests and Assignments : 30%Final Examination : 50%Lab Report : 20%

7.0 TEXTBOOKS Williams, D.H. and Fleming, I., 2007. Spectroscopic Methods in Organic Chemistry. 6th ed. London: McGraw-Hill

Atkins, P. and de Paula, J., 2009. Physical Chemistry. 9th ed. Oxford: Oxford University Press.




8.0 REFERENCESYan, B., 2000. Analytical Methods in Combinatorial Chemistry. 1st ed. CRC.

Christian G. D., Analytical Chemistry, 6th Edition, John Wiley & Sons, 2009. Skoog D. A., West D. M., Holler F. J., Crouch S.R., Fundamentals of Analytical Chemistry, 8 th

Edition, Thomson Learning Inc, 2004..

9.0 ADDITIONAL INFORMATIONAttendance is compulsory. Students who fail to comply 80% of the attendance will be barred from taking the final exam. Absence from lecture, tutorial, test, presentation, etc must be supported by relevant documents.

10.0 OTHER INFORMATION/DETAILS

PREPARED BY : APPROVED BY :

SIGNATURE:

NAME: DR KAMARIAH NOOR ISMAILPOSITION: SENIOR LECTURER

DATE: 01 MAR 2013

SIGNATURE :

NAME :

POSITION :

DATE:

COURSE OUTLINECHE 515 INSTRUMENTAL CHEMISTRY

FOR ENGINEERS

FACULTY OF CHEMICAL ENGINEERINGUNIVERSITI TEKNOLOGI MARA

SEMESTER: SEPT 2012 – JAN 2013

PAGE : 4/5

Week

Chapter/Content Course Outcome Course Learning Outcomes Instructional Method

Assessment

1-2 Chapter 1: UV and Visible Spectroscopy1. Excitation and Absorption

Laws:HOMO and LUMO 2. Solvent Effects3. Chromophores, Conjugation,

Shifting4. Electronic Transitions5. Interpreting Spectra6. Beer-Lambert Law

Ability to interpret UV and Visible Spectra to elucidate the functional activity of chemical compounds

The student should be able to: Describe UV and Visible spectroscopy Analyse spectra Identify chromophores

Lectures Tutorials Laboratory

Assignment Quiz Test Examination

3-4 2.8 Infrared Spectroscopy2.9 FTIR Components

(Interferometer)2.10 Molecular Vibrations and

Absorption Frequencies2.11 Type of Samples2.12 Interpreting Spectra 2.13 Hyphenated Methods

Involving IR2.14 Applications Analysis (Quantitative and qualitative)

Ability to interpret IR Spectra The student should be able to: Describe IR spectroscopy Analyse spectra



5-6 3.6 Mass Spectroscopy3.7 Ions Productions (Readily

volatile and Poorly Volatile)3.8 RAM3.9 Structural Information3.10 Ion Analysis3.11 Liquid Chromatography-

Mass Spectrometry, and GC-MS

3.1

Ability to interpret Mass Spectra The student should be able to: Describe Mass spectroscopy Analyse spectra



7-9 4.0 Atomic Spectroscopic Methods4.1 Atomization Methods

4.2 Atomic Absorption Spectroscopy (AAS)

4.3 Atomic Emission Spectroscopy (ICP)

Ability to interpret AA, Emission, Fluorescence and ICP-AE Spectra

The student should be able to: Describe AA spectroscopy Describe Emission spectroscopy Describe Fluorescence spectroscopy



COURSE OUTLINECHE 515 INSTRUMENTAL CHEMISTRY

FOR ENGINEERS

FACULTY OF CHEMICAL ENGINEERINGUNIVERSITI TEKNOLOGI MARA

SEMESTER: SEPT 2012 – JAN 2013

PAGE : 5/5

4.4 Atomic Fluorescence Spectroscopy (AFS)

4.1

Describe ICP-AE spectroscopy Analyse spectra

10-12

5.0 Nuclear Magnetic Resonance5.1 Nuclear Spin and

Resonance5.2 Chemical Shift 5.3 Factors Affecting Chemical

Shifts 5.4 1H-NMR (Splitting, Coupling,

Integration of 1H-NMR Absorption)

5.5 13C-NMR5.1.1

Ability to interpret 1H and 13C NMR Spectra

The student should be able to : Describe NMR spectroscopy Analyse spectra



13-14

6.0 Chromatography6.6 Chromatographic Techniques6.7 Theory of Column Efficiency

in Chromatography6.8 Thin Layer Chromatography6.9 Gas Chromatography6.10 Liquid Chromatography

5.1

Ability to interpret Thin Layer, Gas and Liquid chromatographs

The student should be able to : Describe Thin Layer chromatography Describe Gas chromatography Describe Liquid chromatography Analyse spectra



1-14 Laboratory Work*6. Identification of organic compounds

using UV-Vis and IR spectroscopy.7. ICP determination of metal in waste

water.8. AAS determination of calcium in

commercial supplement tablets.9. NMR analysis of a constitutional

isomer.10. Determination of organic compound

using HPLC

* Laboratory works are not limited to the above lists, but subjected to the equipment availability

Ability to perform experiments independently and as a member of a group

The student should be able to : Develop comprehensive

experimental procedures independently

Write comprehensive and clear reports

Explain their results in a critical and constructive manner

Apply knowledge gained in the theory component of this course practically

Laboratory Experiments

Laboratory Reports

CHE515 - Lesson Plan_Sept 2012 - Jan2013

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