Capillary Accessories · 2009-10-08 · Capillary Accessories ACCESSORIES Universal Guard Column...

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Contact your Alltech office or distributor for current or local prices. © Copyright 2004 Alltech Associates, Inc. 385 6021 6628 5717 0017 Capillary Accessories ACCESSORIES CONNECTORS DESCRIPTION QTY . PART NO. PRICE Straight Connectors Fused Silica Universal Straight Connector 5 20400 Universal Straight Connector 25 20401 Angled Universal Connector 5 20694 Angled Universal Connector 25 20695 Borosilicate Universal Straight Connector 5 20490 Universal Straight Connector 25 20492 Y-Connectors Fused Silica Universal Y-Connector 1 20405 Angled Universal Y-Connector 1 20500 Borosilicate Universal Y-Connector 1 20480 Universal Y-Connector 5 20482 Accessories Polyimide Sealing Resin 5g 5825 Universal Capillary Connectors • One size fits tubing from 0.25mm i.d. to 0.53mm i.d. • Available in straight or Y configurations Capillary connectors form a gas-tight seal when heated to typical GC temperatures. The angled connectors conform to the curvature of a fused silica capillary column. To create a permanent seal, add a small amount of polyimide resin to the outside of the capillary tube before inserting. Order under "Accessories" below. Universal Straight Connector Featherweight Capillary Union • Lightweight • High temperature Vespel ® construction • Accommodates all tubing sizes FEATHERWEIGHT CAPILLARY UNION DESCRIPTION PART NO. PRICE Featherweight Union with 2 Nuts* 28990 Vespel ® Ferrules for Use with Featherweight Union Vespel ® Ferrule, 0.8mm i.d. 28992 Vespel ® Ferrule, 0.5mm i.d. 28993 Vespel ® Ferrule, 0.4mm i.d. 28994 *Order ferrules separately. Fused Silica Outlet Splitters • Accommodates capillaries from 0.22 to 0.32mm i.d. and provides a 1:1 ratio • Includes a glass-lined SS bulkhead union, a 0.4mm i.d. two-hole Vespel ® graphite ferrule and two lengths of deactivated fused silica tubing Use this inert outlet splitter with two detectors or one detector and a sample collection device. OUTLET SPLITTER DESCRIPTION PART NO. PRICE Outlet Splitter 14898 VALCO ® REDUCING FERRULES DESCRIPTION AND VALCO ® NO. PART NO. PRICE Valco ® Reducing Ferrules 1/32" to 0.4mm (Valco ® FS.4), 10/pk 907010 1/32" to 0.5mm (Valco ® FS.5), 10/pk 907110 1/16" to 0.8mm (Valco ® FS1.8), 10/pk 903410 * Includes 2 stainless steel ferrules. Table 1 CONNECT FROM: TO 0.25MM I.D. FUSED SILICA TO 0.32MM I.D. FUSED SILICA TO 0.53MM I.D. FUSED SILICA TO 1/16” SS TUBING 0.25mm i.d. Fused Silica 9068 9068 + 907110 45849 + 907010 + 903410 45849 + 907010 0.32mm i.d. Fused Silica 9069 + 907010 9069 45849 + 907110 + 903410 45849 + 907110 0.53mm i.d. Fused Silica 45849 + 907010 + 903410 45849 + 907110 + 903410 9031 45835 + 903410 1/16" SS Tubing 45849 + 907010 45849 + 907110 45835 + 903410 45835 Valco ® Zero-Dead Volume Union Use these stainless steel unions to make connections with fused silica capillaries. Unions feature specially designed Vespel ® /graphite ferrules and are bored through. Table 1 shows the parts needed for different connections. VALCO ® ZERO-DEAD VOLUME UNIONS DESCRIPTION AND VALCO ® NO. PART NO. PRICE Zero Dead-Volume Unions 1/32", 0.4mm (Valco ® ZU.5TFS.4) 9068 1/32", 0.5mm (Valco ® ZU.5TFS.5) 9069 1/16", 0.8mm (Valco ® ZU1TFS.8) 9031 1/16" - 1/32", 1/32" Bore (Valco ® ZRU1.5T) 45849* 1/16", 1/16" Bore (Valco ® ZU1T) 45835* Capillary Connectors

Transcript of Capillary Accessories · 2009-10-08 · Capillary Accessories ACCESSORIES Universal Guard Column...

Page 1: Capillary Accessories · 2009-10-08 · Capillary Accessories ACCESSORIES Universal Guard Column Kits • Universal kits connect to any capillary column • Guard columns are deactivated

Contact your Alltech office or distributor for current or local prices.© Copyright 2004 Alltech Associates, Inc.

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Capillary AccessoriesA C C E S S O R I E S

CONNECTORSDESCRIPTION QTY. PART NO. PRICE

Straight ConnectorsFused SilicaUniversal Straight Connector 5 20400Universal Straight Connector 25 20401Angled Universal Connector 5 20694Angled Universal Connector 25 20695Borosilicate Universal Straight Connector 5 20490Universal Straight Connector 25 20492Y-ConnectorsFused SilicaUniversal Y-Connector 1 20405Angled Universal Y-Connector 1 20500Borosilicate Universal Y-Connector 1 20480Universal Y-Connector 5 20482AccessoriesPolyimide Sealing Resin 5g 5825

Universal Capillary Connectors• One size fits tubing from 0.25mm i.d. to 0.53mm i.d.• Available in straight or Y configurations

Capillary connectors form a gas-tight seal when heated to typical GC temperatures. The angled connectors conform to the curvature of a fused silica capillary column. To create a permanent seal, add a small amount of polyimide resin to the outside of the capillary tube before inserting. Order under "Accessories" below.

Universal Straight Connector

Featherweight Capillary Union• Lightweight• High temperature Vespel®

construction• Accommodates all tubing sizes

FEATHERWEIGHT CAPILLARY UNIONDESCRIPTION PART NO. PRICE

Featherweight Union with 2 Nuts* 28990Vespel® Ferrules for Use with Featherweight UnionVespel® Ferrule, 0.8mm i.d. 28992Vespel® Ferrule, 0.5mm i.d. 28993Vespel® Ferrule, 0.4mm i.d. 28994*Order ferrules separately.

Fused Silica Outlet Splitters• Accommodates capillaries

from 0.22 to 0.32mm i.d. and provides a 1:1 ratio

• Includes a glass-lined SS bulkhead union, a 0.4mm i.d. two-hole Vespel® graphite ferrule and two lengths of deactivated fused silica tubing

Use this inert outlet splitter with two detectors or one detector and a sample collection device.

OUTLET SPLITTERDESCRIPTION PART NO. PRICE

Outlet Splitter 14898

VALCO® REDUCING FERRULESDESCRIPTION AND VALCO® NO. PART NO. PRICE

Valco® Reducing Ferrules1/32" to 0.4mm (Valco® FS.4), 10/pk 9070101/32" to 0.5mm (Valco® FS.5), 10/pk 9071101/16" to 0.8mm (Valco® FS1.8), 10/pk 903410* Includes 2 stainless steel ferrules.

Table 1CONNECT FROM: TO 0.25MM I.D. FUSED SILICA TO 0.32MM I.D. FUSED SILICA TO 0.53MM I.D. FUSED SILICA TO 1/16” SS TUBING

0.25mm i.d. Fused Silica 9068 9068 + 907110 45849 + 907010 + 903410 45849 + 9070100.32mm i.d. Fused Silica 9069 + 907010 9069 45849 + 907110 + 903410 45849 + 9071100.53mm i.d. Fused Silica 45849 + 907010 + 903410 45849 + 907110 + 903410 9031 45835 + 9034101/16" SS Tubing 45849 + 907010 45849 + 907110 45835 + 903410 45835

Valco® Zero-Dead Volume UnionUse these stainless steel unions to make connections with fused silica

capillaries. Unions feature specially designed Vespel®/graphite ferrules and are bored through. Table 1 shows the parts needed for different connections.

VALCO® ZERO-DEAD VOLUME UNIONSDESCRIPTION AND VALCO® NO. PART NO. PRICE

Zero Dead-Volume Unions1/32", 0.4mm (Valco® ZU.5TFS.4) 90681/32", 0.5mm (Valco® ZU.5TFS.5) 90691/16", 0.8mm (Valco® ZU1TFS.8) 90311/16" - 1/32", 1/32" Bore (Valco® ZRU1.5T) 45849*1/16", 1/16" Bore (Valco® ZU1T) 45835*

Capillary Connectors

Page 2: Capillary Accessories · 2009-10-08 · Capillary Accessories ACCESSORIES Universal Guard Column Kits • Universal kits connect to any capillary column • Guard columns are deactivated

Contact your Alltech office or distributor for current or local prices.© Copyright 2004 Alltech Associates, Inc. Contact your Alltech office or distributor for current or local prices.© Copyright 2004 Alltech Associates, Inc.

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Capillary AccessoriesA C C E S S O R I E S

Universal Guard Column Kits• Universal kits connect to any capillary column• Guard columns are

deactivated

Universal guard column kits contain three - 5m deactivated capillaries, three-universal fused silica connectors, ceramic cutter, and instructions. Order sealing resin separately under “Accessories” to reinforce connections. Replacement kit parts are available below.

UNIVERSAL GUARD COLUMN KITSDESCRIPTION PART NO. PRICE

Universal Guard Column Kits0.53mm Universal Guard Column Kit 139920.32mm Universal Guard Column Kit 139980.25mm Universal Guard Column Kit 14005Replacement PartsUniversal Connectors, 5/pk 20400Angled Universal Connector, 5/pk 206945m x 0.53mm i.d. Capillaries, 5/pk 139905m x 0.32mm i.d. Capillaries, 5/pk 139995m x 0.25mm i.d. Capillaries, 5/pk 14007AccessoriesPolyimide Sealing Resin, 5g 582520X Magnifier 3163

Deactivated Guard Columns• Three different deactivation polarities• Chemically inert

These guard columns protect your analytical column by collecting non-volatile, pyrolyzable, or particulate contamination.

DEACTIVATED GUARD COLUMNSDESCRIPTION PART NO. PRICE

Non-Polar0.25mm x 5m 190630.32mm x 5m 190640.53mm x 5m 19065Intermediate Polar0.25mm x 5m 190540.32mm x 5m 190550.53mm x 5m 19056Polar0.25mm x 5m 190570.32mm x 5m 190580.53mm x 5m 19059

Fused Silica Capillary Tubing• Deactivated and undeactivated tubing available• Available mounted on a cage

Alltech provides the finest quality fused silica capillary tubing either untreated or deactivated by our proprietary high temperature process. Use tubing to prepare your own capillaries or guard columns.

FUSED SILICA CAPILLARY TUBINGI.D. QTY. LENGTH PART NO. PRICE

Deactivated Tubing with Cage0.18mm — 10m 6020260.18mm — 20m 6020280.18mm — 40m 6020290.25mm — 15m 6029150.25mm — 30m 6029300.25mm — 60m 6029600.32mm — 15m 6039150.32mm — 30m 6039300.32mm — 60m 6039600.45mm — 15m 6020300.45mm — 30m 6020320.45mm — 60m 6020340.53mm — 15m 6059150.53mm — 30m 6059300.53mm — 60m 605960Deactivated Tubing, Without Cage0.05mm per meter 6020380.10mm — per meter 6020370.18mm — per meter 6020100.25mm — per meter 6026400.25mm x 1m 5/pk — 58270.25mm x 2m 5/pk — 58290.32mm — per meter 6036400.32mm x 1m 5/pk — 58310.32mm x 2m 5/pk — 58330.45mm — per meter 6020120.53mm — per meter 6056400.53mm x 1m 5/pk — 58320.53mm x 2m 5/pk — 5834Undeactivated Tubing, Without Cage0.05mm — per meter 6020350.10mm — per meter 6020360.18mm — per meter 196030.25mm — per meter 6026000.32mm — per meter 6036000.45mm — per meter 196020.53mm — per meter 605600

Capillary Guards & Tubing

Page 3: Capillary Accessories · 2009-10-08 · Capillary Accessories ACCESSORIES Universal Guard Column Kits • Universal kits connect to any capillary column • Guard columns are deactivated

Contact your Alltech offi ce or distributor for current or local prices.© Copyright 2004 Alltech Associates, Inc. Contact your Alltech offi ce or distributor for current or local prices.© Copyright 2004 Alltech Associates, Inc.

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Capillary AccessoriesA C C E S S O R I E S

Capillary Cages

These cages are made of a heavy gauge stainless steel and are electropolished to prevent abrasion. All are 7 inches in diameter.

CAPILLARY CAGESDESCRIPTION PART NO. PRICE

7" x 3/4" Cage 752007" x 1-1/4" Cage 752017" x 1-3/4" Cage 75202High Temperature String, 10ft 6344

Capillary Column Washer

This easy to use column washer is designed for solvent fl ushing of bonded or cross-linked fused silica capillaries. It is made of heavy duty glass and will hold up to 20mL of solvent. Maximum pressure is 125psig. Order appropriate sized ferrules separately below.

CAPILLARY COLUMN WASHERDESCRIPTION QTY. PART NO. PRICE

Capillary Column Washer ea 5819Ferrules1/8" to 0.4mm VG1 10 200/0.4-VG11/8" to 0.5mm VG1 10 200/0.5-VG11/8" to 0.8mm VG1 10 200/0.8-VG1

For a listing of suitable solvents for various stationary phases, request Data Sheet 5819.

Capillary Endcaps

Increase column life by preventing contaminants from entering column during storage.

CAPILLARY ENDCAPSDESCRIPTION QTY. PART NO. PRICE

Fused Silica 2 20699Fused Silica 20 20701Silicone 10 4018

SPLIT-VENT TRAP KITDESCRIPTION PART NO. PRICE

Split-Vent Trap Kit 5870Replacement Charcoal Cartridge, 10/pk 58721/8" Stainless Steel Union 14165

Split-Vent Trap Kit• Charcoal fi lter cartridges are

economical and easy to replace• Adsorbs toxic vapors• Connects directly to Agilent GC’s

Alltech’s split-vent trap kit effectively adsorbs toxic or noxious vapors that might otherwise be released into the workplace. The trap has a 1/8" fi tting to connect directly to Agilent GC’s and can be adapted for use with most other GC’s.

The split-vent trap features a corrosion-resistant base and a disposable NIOSH-type charcoal fi lter cartridge that is easy to replace. Order replacement cartridges below.

What’s included: split-vent trap, three charcoal cartridges, cartridge scorer, and tip breaker.

Capillary Accessories

Approximate Column Volume RequiredLENGTH 0.25MM I.D. 0.32MM I.D. 0.53MM I.D.

10m 0.5mL 0.8mL 2.2mL15m 0.7mL 1.2mL 3.3mL25m 1.2mL 2.0mL 5.5mL30m 1.5mL 2.4mL 6.6mL50m 2.5mL 4.0mL 11.0mL60m 2.9mL 4.8mL 13.2mL

How much solvent is needed to wash your column? Refer to the table below.

Page 4: Capillary Accessories · 2009-10-08 · Capillary Accessories ACCESSORIES Universal Guard Column Kits • Universal kits connect to any capillary column • Guard columns are deactivated

Contact your Alltech office or distributor for current or local prices.© Copyright 2004 Alltech Associates, Inc. Contact your Alltech office or distributor for current or local prices.© Copyright 2004 Alltech Associates, Inc.

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Packed AccessoriesA C C E S S O R I E S

Air/Vacuum Pump• Oil-less operation• Portable and reliable

This compact rotary vane air/vacuum pump will deliver 1 liter per minute of oil free air at 15psig. It features graphite vanes and sealed-for-life ball bearings. The maximum vacuum is 20" (508mm) Hg continuous. Pump measures 6-7/16" H x 5-5/8" W x 12" L (163.51mm H x 142.88mm W x 304.8mm L) and weighs 10lbs (4.54kg).

What’s included: muffler, filter, 1/4" MPT ports, 10ft power cord with US standard plug.

AIR/VACUUM PUMPDESCRIPTION PART NO. PRICE

Air/Vacuum Pump, 115V 1531 AccessoriesPressure Relief Valve 1534Vacuum Gauge 1536Pressure Gauge 1537Nalgene Vacuum Tubing, 1/4" i.d. x 5/8" o.d., 5ft 1599

Attachable Funnel

This anodized aluminum funnel attaches easily to 1/8" and 1/4" o.d. glass and metal tubing—ideal for column packing. Funnel can be disassembled for cleaning. Order adapters separately to attach funnel to columns with fittings already connected. Replacement o-rings are also available below.

GC Column Vibrator

This vibrator is ideal for use when filling GC columns, including glass columns. This two-speed unit comes supplied with a 7-foot cord and US standard plug.

GC COLUMN VIBRATORDESCRIPTION PART NO. PRICE

110V 4012

Premium Glass Wool

Untreated - A soft fine denier Pyrex™ wool, primarily used for non-chromatographic applications.

Silane Treated - Fine wool treated with di-methyldichlorosilane (DMDCS) to yield an inert material that won't decompose sensitive compounds. This material is ideal for most chromatographic applications.

Phosphoric Acid (H3PO4), Treated - For analysis of acidic compounds such as free acids, phenols and glycols.

Quartz Wool - Made from high-purity quartz, extremely low in metallic oxide impurities.

PTFE Wool - Commonly used as a plug for packed columns when analyzing for low levels of sulfur.

Pesticide Grade Glass Wool - A superbly inert glass wool ideal for use with electron capture, nitrogen-phosphorous, flame photometric, alkali-bead flame and all electrolytic detectors.

Glass Wool Inserter/ Remover

Wool Inserter

Glass Wool Tools

PREMIUM GLASS WOOLDESCRIPTION QTY. PART NO. PRICE

Glass WoolUntreated Glass Wool 50g 4035Silane Treated Glass Wool 50g 4037Silane Treated Glass Wool 250g 4038H3PO4 Treated Glass Wool 25g 4039Quartz Wool 10g 4033Silane Treated Quartz Wool 10g 4233PTFE Wool 10g 4736Pesticide Grade Glass Wool 10g 4034Glass Wool ToolsGlass Wool Inserter/Remover 2 6292Wool Inserter ea 6285

Delrin® Plugs• Use these plugs to seal the ends of

columns

Simply slip plug into your ferrule and nut, and attach to your fittings. Ferrules will not lock in place. Plugs are reusable.

DELRIN® PLUGSSIZE QTY. PART NO. PRICE

1/16" 25 28981/8" 25 29001/4" 25 2902

Packing Accessories

ATTACHABLE FUNNELDESCRIPTION PART NO. PRICE

Attachable Funnel 4008Adaptersfor 1/8" Column 4050for 3/16" Column 4052for 1/4" Column 4054for 3/8" Column 4056Replacement O-rings, 12/pk 4010

Page 5: Capillary Accessories · 2009-10-08 · Capillary Accessories ACCESSORIES Universal Guard Column Kits • Universal kits connect to any capillary column • Guard columns are deactivated

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Pressed Frits

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Pressed Frits

These frits are precision-fabricated from Type 316 stainless steel and are ideal for sealing the ends of GC columns.

Pressed frits are easy to install. Drill the column ends to the proper diameter and depth using the drill bits sold below. Rest the frit on top of the tubing and gently tap it into place.

Glass Column Repair Kits

This repair kit includes a 1ft (30.5cm) piece of shrinkable TFE-FEP tubing that encapsulates the broken section creating a tight and reliable seal.

Easy to apply, just slip over one end of the broken tubes, butt the tubes, and heat to 330°C with a heat gun.

Packed AccessoriesA C C E S S O R I E S

GC End Caps

These end caps are non-shredding, flexible, and easily applied and removed. They provide a positive barrier to moisture and air. The 5/16" size fits over 1/4" columns that have ferrules swaged on the ends. The 3/16" size fits 1/8" columns with ferrules in place.

GC END CAPSTUBE O.D. QTY. PART NO. PRICE

1/16" 100 40201/8" 100 40213/16" 100 40221/4" 100 40235/16" 100 40253/8" 100 40241/2" 100 4026

GLASS COLUMN REPAIR KITSTUBING SIZE PART NO. PRICE

Glass Column Repair KitsUp to 0.036" (0.91mm) 5800Up to 0.060" (1.52mm) 5801Up to 0.130" (3.30mm) 58020.125" (3.18mm) to 0.250" (6.35mm) 5803Heat Gun110V 2518220V 2518-220V

Column Tags

Use these aluminum tags to create a permanent heat resistant record of pertinent column information. Writing surface of tag is 1" x 2" (25.4 x 50.8mm). Order a Vibrograver at right to permanently inscribe the tags.

COLUMN TAGSDESCRIPTION QTY. PART NO. PRICE

Embossed GC Tags 100 8011Embossed GC Tags 25 8012Embossed LC Tags 25 8005Plain Tags 100 8009

STAINLESS STEEL PRESSED FRITS

PORE DIAMETER QTY.

FOR USE WITH 1/8" O.D. TUBING

FOR USE WITH 1/4" O.D. TUBING PRICE

0.5µm 25 702625 —2.0µm 25 703425 7035255.0µm 25 702825 70292510.0µm 25 703025 70312520.0µm 25 703225 703325

Drill Bits

These drill bits are specifically designed to prepare tubing for frit installation. They include a bushing that acts as a stop to control the depth of the hole.

DRILL BITSDIAMETER QTY. PART NO. PRICE

for 1/8" Frits ea 7032for 1/4" Frits ea 7033

VIBROGRAVERDESCRIPTION PART NO. PRICE

Vibrograver110V 8006220V 8018Replacement PointDiamond 15044Carbide 15045

Vibrograver

Use for engraving or column packing. A carbide point is included. Remove the point to use for column packing. Order replacements below.

Packing Accessories

Page 6: Capillary Accessories · 2009-10-08 · Capillary Accessories ACCESSORIES Universal Guard Column Kits • Universal kits connect to any capillary column • Guard columns are deactivated

Contact your Alltech offi ce or distributor for current or local prices.© Copyright 2004 Alltech Associates, Inc. Contact your Alltech offi ce or distributor for current or local prices.© Copyright 2004 Alltech Associates, Inc.

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wall mount cylinder holderwith safety strap

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Matheson Switchover Systems• Automatically change cylinders• Compact design minimizes wall

space consumption

Automatically switch from one cylinder to another without interruption providing a continuous supply of gas. Systems also minimize the risk of ambient contamination within your gas delivery network. Available in brass or stainless steel and with or without regulators. Order connecting fl ex hose separately under “Accessories” below.

Gas FlowA C C E S S O R I E S

9-way Cylinder Wrench

Cylinder Status Tags

Cylinder status tags help to organize and positively identify cylinders.

CYLINDER STATUS TAGSDESCRIPTION PART NO. PRICE

Cylinder Status Tags, 25/pk 8004

Cylinder Tools

Conveniently open valves, tighten gauges, connections, regulators, etc.

CYLINDER TOOLSDESCRIPTION PART NO. PRICE

ToolsCylinder Valve & Cap Wrench 371359-Way Cylinder Wrench 412933

Cylinder Holders

Prevent toppling of cylinders with these cast aluminum cylinder holders. Holders feature a nylon web strap with a sturdy buckle and are available with an optional safety chain. Cylinder holders handle cylinders from 4 to 15 inches in diameter. Choose from benchtop or wall mount styles.

CYLINDER HOLDERSDESCRIPTION PART NO. PRICE

Bench Top Model with Cylinder Strap 37132Bench Top Model with Cylinder Strap and Safety Chain

37214

Wall Mount Model with Cylinder Strap 37133Wall Mount Model with Cylinder Strap and Safety Chain

37215

Flash Arrestors• Prevent dangerous fl ashbacks• Meets OSHA requirements

Flash arrestors shut off gas fl ow in the event of a fl ashback and extinguish the fl ame within the housing before it reaches your gas source. Flash arrestors are available in brass for general laboratory applications and stainless steel for high purity applications.

Specifi cationsPART NO. 37126 PART NO. 37128

Materials of Construction Body: Brass 316 SS Seat: Butyl Rubber Viton A O-rings: Butyl Rubber PTFE-coated Viton Internal Parts: Brass & Steel SS Connections: 1/4" FPTMax Service Pressure: Acetylene and Natural Gas - 15 psig

Oxygen - 150 psigPropane and Hydrogen - 50 psig

Dimensions: 2" o.d. x 3-1/2"L (without fi ttings)Weight: 2 lbs

MATHESON SWITCHOVER SYSTEMSDESCRIPTION PART NO. PRICE

Matheson Switchover SystemsModel 5234 Brass 37139Model 5244 SS 37143Model 5230 Brass w/Regulator 37138Model 5240 SS w/Regulator 37141Accessories (Flex Hoses)3ft. SS with 1/4" NPT Female Connections 371183ft. SS with Brass CGA Connections* 371223ft. SS with SS CGA Connections* 37124* Specify CGA number.

For additional information on Matheson Switchover Systems, request Data Sheet 37138.

Cylinder Valve & Cap Wrench

FLASH ARRESTORSDESCRIPTION PART NO. PRICE

Brass 37126316 SS 37128

Cylinder Accessories

Page 7: Capillary Accessories · 2009-10-08 · Capillary Accessories ACCESSORIES Universal Guard Column Kits • Universal kits connect to any capillary column • Guard columns are deactivated

Contact your Alltech office or distributor for current or local prices.© Copyright 2004 Alltech Associates, Inc. Contact your Alltech office or distributor for current or local prices.© Copyright 2004 Alltech Associates, Inc.

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Gas FlowA C C E S S O R I E S

FLOW DIVERTERDESCRIPTION PART NO. PRICE

Flow Diverter 4200

Flow Diverter

Easily divert the gas stream from your detector to your soapfilm flowmeter. One Flow Diverter is required for each gas. It is supplied with 1/8" fittings.

FLOW CONTROLLERDESCRIPTION PART NO. PRICE

Adjustable Flow Controller 8149

Adjustable Flow Controller• Control flow rates from 0.5 mL/min

up to 1.6 L/min

This adjustable flow controller features a user variable span adjustment permitting it to be used for a variety of flow ranges. Use the ten-turn knob to easily adjust flow rates from zero to maximum. Pipe adapters for 1/8" o.d. tubing are included.

Specifications:Flow rate: Adjustable from 1.6mL/min to 0.5L/minBody: AluminumDiaphragm: Stainless SteelMax Pressure: 250psigMax Temp: 120°CPorts: 1/8" MPT

Eco-Mizer• Conserve expensive gases during

standby periods• Decrease laboratory operating expenses• Directly connects to 1/8" o.d. tubing

The Eco-Mizer is a compact standby valve designed to conserve gases overnight and during other non-use periods. The adjustable fine metering valve sets the standby flow rate and a concentric, independent valve allows selection of either standby flow rate or straight-through flow.

Aalborg Flow ControllersTiltable LCD readout for easy viewing

• Indicate and control set flow rates of gases

• Compact design won’t take up valuable bench space

• NIST traceable certification

These flow controllers feature a built-in electromagnetic valve that allows the flow to be set to any desired rate within the flow range. The valve is normally closed to ensure that gas flow is shut off in the event of a power outage. Setpoints can be controlled locally or remotely via the 4-20mA output.

The LCD readout can be tilted over 90° and is easily removable for remote reading. Flow controllers are available in aluminum and brass for use with non-corrosive gases or 316 stainless steel for corrosive applications. Order power supply separately under “Accessories”.

Specifications:Accuracy: +/-1.5% full scaleRepeatability: +/-0.5% full scaleMax Pressure: 500psigAmbient Temperature: 5 to 50°COutput: 0-5 VDC, 4-20mAConnections: 1/4" compressionDisplay: 3-1/2 digit LCDPower: Order power supply separately

ECO-MIZERDESCRIPTION PART NO. PRICE

Eco-Mizer 7070

ACCESSORIESDESCRIPTION PART NO. PRICE

Flow Controller Power Supplies110V/12VDC 74487220V/12VDC European 74488Shield Cable, 8ft., Unterminated Ends 74492Battery Pack (Includes Case)110V 74418220V 74419

Flow Controllers

FLOW CONTROLLERS*

FLOW RATEALUMINUM BODY

PART NO. PRICESS BODYPART NO. PRICE

0-50mL/min 74428 744350-100mL/min 74429 744360-200mL/min 74430 744370-500mL/min 74431 744380-1L/min 74432 74439

$775.00775.00775.00775.00775.00

*Please specify metered gas, and flow range

Page 8: Capillary Accessories · 2009-10-08 · Capillary Accessories ACCESSORIES Universal Guard Column Kits • Universal kits connect to any capillary column • Guard columns are deactivated

Contact your Alltech offi ce or distributor for current or local prices.© Copyright 2004 Alltech Associates, Inc. Contact your Alltech offi ce or distributor for current or local prices.© Copyright 2004 Alltech Associates, Inc.

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Need Help Timing Your Flowmeter?

Gas FlowA C C E S S O R I E S

Digital Soapfi lm FlowmeterPatented U-tube design for lighter than air gases

• NIST traceable calibration• 2-3% of reading accuracy• LCD display• Autoranging

Alltech digital soapfi lm fl owmeters provide for easy gas measurement and allow you to visually confi rm gas fl ow. Flowmeters feature microprocessor control and display fl ow rates, default conditions and set test results on the LCD. Automatic shut off extends battery life and manual reset corrects fault conditions. Part No. 4068 also measures split ratios. Optional carrying case, tubing and tubing clamps are available under “Accessories” below.

What’s included: 9V battery and operation manual

Soapfi lm FlowmeterEconomical fl ow measurement

This soapfi lm fl owmeter is easy to use. Simply time the movement of a soap bubble be tween two calibration marks. Alltech’s soapfi lm fl owmeters have a unique bubble burster at the top to eliminate the overfl ow of the soap solution. A rubber bulb is included with each soapfi lm fl owmeter. The 100µL and 500µL fl owmeters are complete with stand and tubing. Order soapfi lm solution and tubing under “Accessories” below.

Visibly Detect Small Leaks in Any SystemLeak Check Solution

Lightweight StopwatchThis stopwatch counts up to 24 hours with 0.01sec readout and has split interval function, alarm clock with a choice of 12 or 24 hour format, a calendar displaying date and day of the week, hourly chime option and button cell battery.

Large Display StopwatchThis stopwatch features a large, 1/2" LCD display. It counts with a resolution of 0.01sec and has split interval, clock and calendar functions. It includes a rugged ABS plastic clip, neck cord, leatherette case, stand clip and a 1.5V battery.

DIGITAL SOAPFILM FLOWMETERSDESCRIPTION PART NO. PRICE

Alltech Digital Flowmeter0.10-50mL/min 40740.5-700mL/min 40685.0mL- 5.00L/min 4077AccessoriesCarrying Case 4087Small Tubing Clamp 4091Large Tubing Clamp 4093Gum Rubber Tubing, 3/32" i.d. x 24" 4099Replacement PartsSmall Bulb 4095Large Bulb 4097Recalibration Service0.10-50mL/min 407400.5-500mL/min 4068015.0mL- 5.00L/min 40770

SOAPFILM FLOWMETERSDESCRIPTION PART NO. PRICE

Flowmeters100µL 14184500µL 141851cc 404110cc 404225cc 4043100cc 40451000cc 4047AccessoriesSoapfi lm Solution, 8oz 20405/16" o.d. Tygon™ Tubing, 10ft 4333

STOPWATCHESDESCRIPTION PART NO. PRICE

Lightweight Stopwatch 4069Large Display Stopwatch 4071

LEAK CHECKDESCRIPTION PART NO. PRICE

Leak Check, 8oz. 2025

Flowmeters

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Aalborg Single Tube Variable Area FlowmetersBuilt-in needle valve controls flow

• Magnifier lens enhances reading resolution

• Ideal for panel mounting

Aalborg single tube flowmeters are equipped with easy to change flowtubes and a control valve. Each flowtube is precision fabricated from heavy wall, shock resistant borosilicate glass. Flowtubes are available in 65mm or 150mm sizes. The floats are retained by TFE plugs. Order a bench stand and fittings separately under “Accessories” below.

SINGLE TUBE FLOWMETERSFLOWTUBE RANGE DIV. PART NO. PRICE

65mm Flowtubes, Direct Reading ScaleHelium 0-120cc/min 5mL 7900Hydrogen 0-100cc/min 5mL 7902Nitrogen 0-120cc/min 5mL 7904Air 0-1.15L/min .05L 7906General Purpose 0-2L/min (air) 1mm 7908150mm Flowtubes, Direct Reading ScaleHelium 0-100cc/min 5mL 7910Hydrogen 0-100cc/min 5mL 7912Nitrogen 0-100cc/min 5mL 7914Air 0-1.25L/min .05L 7916General Purpose 0-2L/min (air) 1mm 7918AccessoriesBench Mount for Above Flowmeters 79201/8" to 1/8" MPT Brass Connector 600381/4" to 1/8" MPT Brass Connector 60042

SpecificationsAccuracy: +/-5% full scaleRepeatability: +/-0.25%Max Pressure: 200psigMax Temperature: 121°CConnections: 1/8" FPT inlet and outlet

Aalborg Three Tube Variable Area FlowmeterMeasure hydrogen, air and carrier gases with one meter

• Direct reading for hydrogen and air• Carrier gas tube can be correlated for

any gas• Can be panel-mounted or free standing

This three tube flowmeter is ideal for monitoring carrier gas, hydrogen and air flows used with flame ionization detectors. A direct reading of hydrogen and air flow rates can be directly read on the flow tube. The carrier gas tube features a 0 to 76mm scale, graduated in 1mm increments. The tubes and flow control valves are easily disassembled for cleaning.

PORTABLE FLOW CHECKDESCRIPTION PART NO. PRICE

Portable Flow Check 7080

Portable Flow CheckDirect analog reading of gas flows

• Easy-to-read 4-inch scale• NIST traceable calibration

The Portable Flow Check allows you to directly measure air, nitrogen, helium and hydrogen flow rates.

Each flowmeter is factory calibrated prior to shipment. A one-point NBS/NIST traceable calibration certificate is included with each flowmeter.

SpecificationsFlow rate: He and N2: 0-100mL/min H2: 0-200mL/min Air: 0-500mL/minMax Pressure: 15psigAccuracy: +/-5% full scaleDisplay: Analog scaleDimensions: 6-3/4"H x 2-1/2"W x 5-1/4"L

SpecificationsAccuracy: +/-5% full scaleRepeatability: +/-0.25%Max Pressure: 200psigMax Temperature: 121°CConnections: 1/8" FPT inlet and outlet

THREE TUBE FLOWMETERDESCRIPTION PART NO. PRICE

Three Tube Flowmeter 4040

Flowmeters

Need a leak detector?

See page 397 for our complete selection.

Page 10: Capillary Accessories · 2009-10-08 · Capillary Accessories ACCESSORIES Universal Guard Column Kits • Universal kits connect to any capillary column • Guard columns are deactivated

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Gas Flow A C C E S S O R I E S

FlowmetersAlltech Digital Flow Check™ Mass FlowmetersNIST traceable calibration for seven gases

• Measure Air, Helium, Hydrogen, Nitrogen, Oxygen, 5% Argon/Methane and Carbon Dioxide

• Water vapor will not affect readings—suitable for purge and trap applications• +/-2% of reading accuracy insures your fl ow rates are on target• DFC-HR™ high resolution model is ideal for low-fl ow applications

Alltech’s model DFC™ and DFC-HR™ Digital Flow Check™ fl owmeters feature unsurpassed versatility. Both models come standard with NIST traceable calibration for seven gases making them suitable for GC applications such as monitoring detector gases, packed column fl ow rates and determining split ratios. Flowmeters can be used in SFC, SFE, and industrial hygiene applications as well as in the general lab. Install fl owmeters in-line for continuous fl ow monitoring to traps, sorbent tubes, incubators, fermentors or reaction vessels without interrupting gas fl ow. Use fl owmeters with either a positive or negative (vacuum) fl ow source.

The DFC™ and DFC-HR™ mass fl owmeters incorporate a rugged solid-state sensor with microprocessor control that measures true mass fl ow eliminating the ambient temperature and pressure change errors associated with other types of fl owmeters. Water vapor errors have also been eliminated. Flow measurements will be precise and accurate to within +/-2% of your reading. Gas fl ow travels straight through the meter reducing backpressure, internal volume and sensor purge time allowing for readings to stabilize quickly. Easily change between mass fl ow, linear velocity and split ratio modes.

Both Digital Flow Check™ meters are shipped with an NIST traceable multi-point certifi cate of calibration that includes percent error data. Meters are calibrated for seven gases using NIST traceable standards. Periodic recalibration is recommended to maintain accuracy and compliance with ISO, GLP, GMP and other quality standards.

Model DFC™ Standard Mass Flowmeter has a measurement range of 0.1 to 300 SCCM for CO2 and 0.1 to 500 SCCM for the remaining gases. It is lightweight, portable and easy to use. Display resolution of 0.1 SCCM makes it ideal for most applications.

Model DFC-HR™ High Resolution Mass Flowmeter features a display resolution of 0.01 SCCM when measuring below 10 SCCM providing a higher degree of precision required for low-fl ow applications such as setting capillary GC fl ow or leak testing. Measurement range is 0.01 to 300 SCCM for CO2 and 0.1 to 500 SCCM for the remaining gases. Use the autozero function to quickly zero the meter for current ambient conditions.

What’s included: Both models include 1 ft of 1/32" (0.8mm) i.d. silicone tubing, 1 ft of 1/8" (3.8mm) i.d. silicone tubing, 2 barbed inlet/outlet fi ttings for each tubing size, a general purpose adapter to connect to Agilent FID, splint vent traps, packed GC columns and gas lines, split vent adapter for connection to Agilent GC split vents, and 9V battery. Model DFC-HR™ also includes a capillary column adapter. Replacement accessories on facing page.

Suggested Flowmeter ApplicationsLow Flow Applications (DFC-HR™)• Capillary GC Flows• Split Ratios• Leak Testing• Applications Requiring Precise Flow

Measurement Below 10cc/minGC Applications (DFC™ and DFC-HR™)• Detector Gases• Packed Column Flow• Split Ratios• Linear Velocity

Lab Applications (DFC™ and DFC-HR™)• Set Instrument Operating Parameters• Industrial Hygiene Applications• Monitor Flow to Traps, Sorbent Tubes,

Incubators, Fermentors & Reaction Vessels• SFC and SFE Applications• In-Line Applications• Monitor Vacuum & Purging Processes• Gas Blending• Gas Sampling

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Gas FlowA C C E S S O R I E S

Flowmeter SpecificationsFlow range: Model DFC: 0.1 to 500 SCCM autoranging (except CO2); 0.1 to 300 SCCM autoranging for CO2

Model DFC-HR: 0.01 to 500 SCCM autoranging (except CO2); 0.01 to 300 SCCM autoranging for CO2

Accuracy: Model DFC: +/-2% of reading or 0.1 SCCM Model DFC-HR: +/-2% of reading or 0.01 SCCM (for range of 0.01 to 9.99 SCCM),0.1 SCCM (for range of 10 to 500 SCCM)Calibrated Gases: He, H2, N2, O2, CO2, Air, Ar/CH4 (5%)Sensor type: Solid-state mass flow, silicon on ceramicDisplay: 16-character alphanumeric LCD, autorangingDisplay modes: Mass flow, split ratio, linear velocity (standard flow range)Power: 9V alkaline battery (included), auto-off function, low battery warningDimensions: 190.5 x 57.4 x 101.6mm (7.5” x 2.26” x 4.0”)

Keep your flowmeter in check! DIGITAL FLOW CHECK™ FLOWMETERSMODEL PART NO. PRICE

DFC™ 4700DFC-HR™ 5700

Accessories:

A1/16" (1.6mm) Barbed Inlet/Outlet Fitting for DFC-HR™ Flowmeter (Part No. 5707)

B1/8" (3.8mm) Barbed Inlet/Outlet Fitting for DFC-HR™ Flowmeter (Part No. 5706)

C Split Vent Adapter (Part No. 4705)D General Purpose Adapter (Part No. 4704)E Capillary Column Adapter (Part No. 5705)F 1/32" (0.8mm) i.d. Connecting Tubing (Part No. 4703)G 1/8" (3.8mm) i.d. Connecting Tubing (Part No. 4785)

REPLACEMENT ACCESSORIESDESCRIPTION PART NO. PRICE

1/16" (1.6mm) Barbed Inlet/Outlet Fitting for DFC-HR™, 2/pk

5707

1/8" (3.8mm) Barbed Inlet/Outlet Fitting for DFC-HR™, 2/pk

5706

Split Vent Adapter 4705General Purpose Adapter 4704Capillary Column Adapter for DFC-HR™ 57051/32" (0.8mm) i.d. Connecting Tubing, 10' 47031/8" (3.8mm) i.d. Connecting Tubing, 1m 4785

Accessories included with DFC™ & DFC-HR™

Insure your connections are leak free

See page 397 for Alltech's Helium Leak Detector

When it’s time to recalibrate your Digital Flow Check™, contact Alltech Customer Service!

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Agilent ADM Digital FlowmetersMeasure any non-corrosive, non-flammable gas

• Continuous, hands-free flow measurement

• Quickly measure split ratios

• NIST traceable calibration

These Agilent ADM flowmeters are ideal for basic GC analysis. They accurately measure volumetric gas flow making them compatible with any non-corrosive, non-flammable gas. Flowmeters are easy to use — flow measurements are displayed at the touch of a button. All meters include five-point calibration traceable to NIST standards.

SpecificationsAccuracy: +/-3%Display: 16-character alphanumeric

SpecificationsAccuracy +/-1.5% full scaleRepeatability +/-0.5%Max Pressure 500psigMax Temperature 50°CDisplay 3-1/2 digit LCDOutput 0-5 VDC or 4-20mAConnections 1/4" compression fittings

Gas FlowA C C E S S O R I E S

AGILENT ADM DIGITAL FLOWMETERS MODEL DESCRIPTION FLOW RATE RS-232 OUTPUT POWER PART NO. PRICE

ADM 1000 Basic 0.5-1000 mL/min No 9V battery 9965ADM 3000 Standard 1.0-750 mL/min Yes 9V battery or AC 6365 ADM 2000 Deluxe 0.5-1000 mL/min Yes 9V battery or AC 7065

Aalborg Mass FlowmetersHandle pressures up to 500psig

• Tiltable LCD readout for easy viewing

• Flow rates displayed in engineering units

• NIST traceable certification

These compact mass flowmeters are designed to directly read flow rates of gases. Meters feature a display module that is tiltable over 90 degrees and can be easily removed for remote reading. Flowmeters are available in aluminum or stainless steel and can be used on the benchtop or wall-mounted. Order power supply separately under “Accessories”.

AALBORG FLOWMETERS*

FLOW RATEALUMINUM BODY

PART NO. PRICESS BODYPART NO. PRICE

0-50 mL/min 74400 74401 0-100 mL/min 74402 74403 0-200 mL/min 74404 74405 0-500 mL/min 74406 74407 0-1 L/min 74422 74425 Accessories (Power Supplies)110V/12VDC 7447220V/12VDC European 7449*specify type of gas and pressure range when ordering

Flowmeters

ADM-1000 - This basic flowmeter has all of the features required for basic GC analysis—continuous real time volumetric flow measurements, automatic split ratio measurements and operates on a 9V battery.

ADM-3000 - This standard flowmeter includes all of the features of the ADM-1000, as well as RS-232 output for data logging. Flowmeter operates on AC power or a 9V battery

ADM-2000 - This deluxe flowmeter includes all of the features of the ADM-3000 plus it measures mass flow rates independent of atmospheric temperature and pressure.

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LEAK-CHECK™

POWER DESCRIPTION QTY. PART NO. PRICE

Leak-Check™, 8oz ea 202512 2026

Leak-Check™ Testing Solution

Leak-Check™ is non-toxic, non-fl ammable, chloride-free and dries cleanly leaving no residue behind. Temperature range is 30 to 200°F. Bottle includes a 15" snorkel tube allowing for easy access to hard-to-reach spaces.

Specifi cationsPORTABLE BENCHTOP

Detector: Thermal conductivity cell with thermistorsRange: Low: x1 High: x100Sensitivity: 1.0 x 10-5 mL/sec for heliumDisplay: LED bar graph Graduated analog scaleZero Function: Automatic ManualAudible Signal: None YesBattery Life: 3.5 hours 4 hoursDimensions: 3-1/4"W x 1-13/16"H x

5-1/4"L(8.255cmW x 2.064cmH

x 13.335cmL)

8-1/4"W x 3-5/8"H x 10-3/4"L

(20.955cmW x 9.206cmH x 27.305cmL)

Weight: 2 lbs (.9072 kg) 9 lbs (4.082 kg)

Gas Leak Detection

Leak-Tec® High Temp Testing SolutionTemperature range is 210 to 415°F

This testing solution wets and spreads evenly and quickly responding to small leaks. Leak-Tec® is non-corrosive and residue free. Convenient aerosol can allows spray to be directed in tight spaces.

Alltech Helium Leak DetectorDesigned specifi cally to detect helium gas leaks

• Portable—operates up to 6.5 hours fully charged • Visual and audible detection

indicators• Change polarity setting to

detect other gases

The Alltech helium leak detector is perfect for detecting gas leaks in GC, GC/MS, and purge/trap systems. Leaks are detected via a thermal conductivity cell and indicated visually on the LCD display and by an audible alarm. The long fl exible probe makes it convenient to detect small and hard to reach gas leaks. Use the detector for gases other than helium by simply changing the polarity setting. Detector features a simple one-step zero adjustment and is fully portable operating on rechargeable Ni-Cd batteries.

What’s included: probe, rechargeable batteries and charger

Gow-Mac® Gas Leak DetectorsControl meter sensitivity — ideal for detecting small leaks

• Zero in ambient air • Detect helium leaks as small as

1.0 x 10-5mL/sec

These gas leak detectors easily and quickly pinpoint gas leaks emitting from pressurized systems. The detectors conveniently zero in ambient air and feature a streamlined probe that is designed to reach diffi cult and confi ned spaces.

The portable model is light weight and features an LED bar graph visual readout and automatic zeroing. The benchtop model has an audible signal in addition to the analog graduated scale.

What’s included: probe with 3ft cable, rechargeable batteries and power adapter.

Helium Leak DetectorDetector: Thermal conductivity cell with thermistorsSensitivity: 0.01 mL/min for HeliumAmbient Temp: 10 to 35°CDisplay: LCD indicator lightsZero Function: YesAudible Signal: YesBattery Life: 6.5 hours continuous fully chargedDimensions: 2.9"W x 1.6"H x 6.3"L

(7.366cmW x 4.064cmH x 16.002cmL)Weight: 1 lb (.454 kg)

Note: The Alltech helium leak detector is not explosion-proof and should not be used to detect combustible or corrosive gas leaks

HELIUM LEAK DETECTOR POWER DESCRIPTION PART NO. PRICE

120 VAC charger w/rechargeable Ni-Cd batteries 60229220 VAC charger w/rechargeable Ni-Cd batteries 60231

GAS LEAK DETECTORSDESCRIPTION PART NO. PRICE

Portable115VAC/60Hz or rechargeable Ni-Cd batteries 21-050230VAC/50Hz or rechargeable Ni-Cd batteries 21-052Benchtop115VAC/60Hz or rechargeable battery pack 21-250230VAC/50Hz or rechargeable battery pack 21-252AccessoriesCarrying case for portable gas leak detectors 59-050

LEAK-TEC®

DESCRIPTION QTY. PART NO. PRICE

Leak-Tec®, 10oz ea 20276 2028

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PurifiersA C C E S S O R I E S

How Contaminants Affect Your Gas Stream

Follow the path that your carrier gas or detector fuel gases take to get to the GC. They start at either a gas tank or a gas generator, and travel through long lengths of tubing, pressure gauges, various fittings, and valves. Each is a potential culprit for introducing contaminants into your gas stream, which ultimately degrades chromatography results and shortens column life.

Typical contaminants, such as moisture, oxygen, and hydrocarbons wreak havoc with GC columns and detectors. Capillary and packed columns can degrade when exposed to moisture or oxygen, particularly at high temperatures. Detector performance may also be compromised. Since the detector can actually “see” the contaminants, spikes, baseline noise, and drift result.

Why Use Gas Purifiers?

A clean gas stream helps guarantee the quality of your GC analysis and the reliability of your results. It also helps prolong column life and minimize detector noise. Gas purifiers act as an insurance policy, protecting your instrumentation and analytical columns from these contaminants. They will not however, convert low purity gas into ultra high purity gas. Alltech carries a variety of gas purifiers in three different styles. See Table 1 for details.

Table 2 - Gas Purifier RecommendationsSYSTEM DETECTOR GAS STREAM RECOMMENDED PURIFIER

Packed Column GCAll Carrier Gas Hydrocarbon, Moisture,

Oxygen, and Indicating Oxygen

Capillary Column GCAll Carrier Gas Hydrocarbon, Moisture,

Oxygen, and Indicating Oxygen

ECD Make-Up Moisture and OxygenFID Make-Up HydrocarbonFID Air for FID HydrocarbonFID Hydrogen for FID HydrocarbonELCD ELCD Reaction Gas Hydrocarbon

Baseplate Style Cartridge Style In-Line Style

*Refills for most materials are available. See specific gas purifiers for refill kit part numbers.

Choosing the Right Gas Purifier for Your Application

There are a variety of gas purifiers available. Some remove a specific contaminant while others remove multiple contaminants from your gas stream. There are several factors you need to consider when selecting purifiers for your application. These include contaminants potentially present in your gas stream, gas purity levels required, flow and pressure limitations, space availability, and desired convenience when replacing spent traps.

Moisture, hydrocarbon, and oxygen traps are the most commonly used purifiers for GC applications. Moisture traps are typically packed with molecular sieves. After extensive heating, these crystalline structures lose their water of hydration opening a cavity that is readily filled with any compound that can fit. Water fits perfectly. However, it will also remove HCl, CO2, SO2, Cl2, or any gas with an effective diameter smaller than water.

Hydrocarbon traps are packed with an activated charcoal that adsorbs any organic compound larger than methane. Size and molecular weight of the organic contaminants will greatly effect the capacity of the trap, and to a smaller degree, trap efficiency. Activated charcoal has a higher capacity for larger (>C4) hydrocarbons than for smaller hydrocarbons.

Oxygen traps are packed with a metal catalyst. Oxygen is the most detrimental contaminant to analytical columns. It produces irreversible oxidation damage particularly to polar stationary phases. Refer to Table 2 for a recommendation of what purifiers to use for various GC applications.

Gas Purifiers and Traps

Table 1 - Gas Purifier StylesSTYLE BASEPLATE CARTRIDGE IN-LINE

Placement: Stands on Benchtop

Stands on Benchtop

Freely supported on gas lines

Repeat Use: Refill* Replace Cartridge Refill*Benefit: Convenient

access, no mounting required

Convenient access, stops gas flow when changing

cartridges

Occupies wall space not bench space

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PurifiersA C C E S S O R I E S

Physical Characteristics

You will also need to consider what physical characteristics your purifier should possess to meet your application requirements. Do you require 1/8" or 1/4" fittings, or are you performing bulk gas purification that requires 1/2" fittings? What are the pressure requirements of your application? This will determine if you need a purifier with a polycarbonate, glass, or metal body. Where will you be installing the purifier and is your installation space limited? This will determine the dimension and style of purifier you should choose.

Purifier Styles

Alltech offers three purifier styles – in-line, baseplate, and cartridge. The in-line style is the traditional style that is most commonly used. It can be directly installed into your gas lines with no support depending on its dimension or can be easily mounted on the wall with mounting clips. In-line purifiers must be removed from the gas line to be refilled or regenerated. We recommend installing them with quick-connect connectors and keeping an extra purifier on hand.

The baseplate and cartridge purifiers sit on the countertop making them easy to access when it is time to replace spent traps. Both styles can be installed in series with shut off valves allowing you to easily isolate them from your gas lines when it is time to replace them. Baseplate units allow you to easily refill the purifier with new adsorbent material. Cartridge purifiers allow you to quickly remove the spent purifier from your gas line and replace it with a new one.

Purifier Capacity

Purifier capacity indicates the amount of contaminant a trap is capable of removing before it reaches its point of saturation. It is dependent on both the adsorbent’s capabilities and purifier’s volume. You need to consider the amount of impurities in your gas stream and the volume of gas you need to purify. If you are purifying a large volume of gas or a less pure gas, you should select a high capacity trap with a large volume adsorbent bed that will trap and retain more contaminants.

Purifier Efficiency

Purifier efficiency is the most important purifier characteristic. It indicates how effective the adsorbent is at removing the desired contaminant from your gas stream. If your application requires high purity levels or the lowest detection limits, select a purifier that is packed with a highly efficient adsorbent material that removes contaminants to ppb levels.

4138

Gas Purifier Installation Order

The order in which you install purifiers into your gas lines is very important. Figure 1 demonstrates the correct order for installing purifiers into your carrier gas line. The moisture trap should be placed first in line. Both hydrocarbon and oxygen traps will adsorb water. Installing a moisture trap before these traps prevents them from becoming prematurely saturated with moisture. It also allows them to more effectively remove their specified contaminants from the gas stream. The hydrocarbon trap should be placed after the moisture trap. A high capacity oxygen trap and an indicating oxygen trap should be placed closest to the GC. We recommend installing the series of purifiers as close to the GC as possible.

Gas purifiers should be installed in a vertical position to prevent channeling. Channeling is a phenomenon that occurs when a purifier is installed in a horizontal position. The adsorbent bed settles and the gas stream passes over the top of the bed rather than through the bed. The gas stream does not sufficiently interact with the adsorbent bed to effectively remove impurities.

Gas purification systems simplify purifier installation in to your gas lines. Systems are available as multi-adsorbent single purifiers or compact panels that contain multiple purifiers.

Purifier Replacement/Regeneration

You need to replace your gas purifiers before they are fully saturated. You can either change them at a predetermined time interval or use an indicating trap that changes color as it becomes saturated. There are potential problems with scheduled replacements. Undetected leaks or accidental exposure to air during cylinder changes can prematurely saturate gas purifiers. Early breakthrough means your column and detectors are exposed to a constant stream of damaging contaminants. An indicating trap located downstream from a high capacity trap is the best way to determine when it’s time to replace a spent trap. Some purifiers contain both the high capacity and indicating adsorbent in the same purifier body while others rely on a separate trap that serves solely as an indicator. Either way, purifier replacement should coincide with the first signs of color change in the indicating adsorbent.

Figure 1 — How to Set Up Carrier Gas Purifiers

1. High Capacity or Indicating Moisture Trap 2. High Capacity or Indicating Hydrocarbon Trap

3. Oxygen Trap (high capacity) 4. Indicating Oxygen Trap

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Purifi ers

Cartridge & Baseplate Style Moisture Traps

A) Baseplate Style Moisture Traps - Convenient access for refi lling/changing- sits on the benchtop - requires no

mounting

B) Cartridge Style Moisture Traps- Simply replace the cartridge when spent- Gas fl ow stops while cartridge is changed- Order baseplate unit separately below

In-Line Style Moisture Traps

In-Line Traps are freely supported on gas lines and require no bench space. Various types of in-line traps are available to handle most applications.

Alltech Moisture TrapsRemove moisture from your gas system

• Eliminate stationary phase degradation• Increase column life• Improve the quality of your chromatography

Remove moisture from gas cylinders, regulators and gas lines with an Alltech moisture trap. In addition to H2O, most traps (except the ALL-Pure™ and Sodium Sulfate) also remove HCl, SO2, NO2, H2S, CO2, oil, and small aliphatics. Both indicating and non-indicating traps are available. Many traps can be regenerated and are refi llable—order refi ll kits separately.

Alltech offers a wide variety of moisture traps to meet all of your gas purifying needs. Choose from three different styles.

C) Economy Moisture Trap- Suitable for air lines- Disposable- Available with SS or Brass endfi ttings

D) Standard Moisture Trap- Suitable for air lines- Refi llable- SS screen at outlet prevents particulates from

entering the gas stream- Available in 2 capacities

E) Traditional Hydro-Purge® Moisture Trap- Molecular sieve 4A indicating material- SS screens at each end prevent particulates from

entering the gas stream

F) Hydro-Purge II® Moisture Trap- 40µm SS frits in endfi ttings prevent

particulates from entering gas stream- Larger capacities than the Traditional Hydro-Purge®

CARTRIDGE AND BASEPLATE MOISTURE TRAPS

PHOTO CARTRIDGE DESCRIPTIONCAPACITY(ML) EFFICIENCY

PRESSURELIMIT FITTING

DIMENSIONS(L X O.D.) INDICATOR PART NO. PRICE

REFILL KITPART NO. PRICE

Cartridge & Baseplate Style Traps

A Baseplate Moisture Trap12

<1ppm 100psig

1/8"12.5" x 1.5"

Yes

8122 81321/4" 8126 8132

331/8"

13.5" x 2"8127 8132

1/4" 8130 8132B Cartridge Moisture Trap 14 <1ppm 100psig N/A 13.2" x 1.5" Yes 81005 8132

Baseplate Unit (for cartridge style traps) 81025

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400 401

4823 4825

46544827

4824

4655

A C C E S S O R I E S

Purifiers

L) Sodium Sulfate Moisture Trap- Specifically designed to remove only H2O- Contains Drierite® indicating material

G) Glass Moisture Trap- Best for carrier gas lines - Glass housing eliminates diffusion- 40µm SS frits in endfittings prevent particulates from

entering gas stream

H) ALL-Pure™ Moisture Trap- Removes moisture down to <1 ppb- Specific for H2O and CO2 only- SS body endures 1000psig pressure limit

I) SS Hydro-Purge®

- Handles pressures up to 400psig- Endfittings contain porous frits for particulate control

K) BIG Moisture Trap - High capacity—removes up to 130mL of moisture- One piece body handles pressures up to 250psig- 40µm SS frits in endfittings prevent particulates from

entering gas stream

J) High Pressure Gas Drier- Handles pressures up to 1800psig

IN-LINE MOISTURE TRAPS

PHOTO CARTRIDGE DESCRIPTIONCAPACITY(ML) EFFICIENCY

PRESSURELIMIT FITTING

DIMENSIONS(L X O.D.) INDICATOR

PART NO. PRICE

REFILLPART NO. PRICE

In-Line Style Traps

C Economy Moisture Trap† 31 <1ppm 100psig

1/8" Brass

9.75" x 2" Yes

8151 N/A† N/A†

1/4" Brass 81531/8" SS 81551/4" SS 8157

D Standard Moisture Trap12

<1ppm 100psig

1/8"13" x 1.25"

Yes

8121 81321/4" 8125

311/8"

14.5" x 2"8123

1/4" 8128

E Traditional Hydro-Purge® 13 <1ppm 100psig1/8"

9.9" x 1.5" Yes14505 14637

1/4" 14503 14637

F Hydro-Purge II®

22 <25ppb125psig

1/8"8.6" x 1.5"

Yes

14626 146421/4" 14625 14642

36 <20ppb1/8"

12.8" x 1.5"14628 14642

1/4" 14627 14642

G Glass Moisture Trap 16 <10ppb 125psig1/8"

12.25" x 1.5" Yes7214 7218

1/4" 7216 7218

H ALL-Pure™ Moisture Trap† 35 <1ppb 1000psig1/8"

22.5" x 1.5" No7034 N/A† N/A†

1/4" 7036

I SS Hydro-Purge®† 9 <1ppm 400psig1/8"

13.8" x 0.75" No14517 N/A† N/A†

1/4" 14515J High Pressure Gas Drier† 27 <1ppm 1800psig 1/4" 11.5" x 1.5" No 8113 N/A† N/A†

K BIG Moisture Trap 130 <5ppb 250psig1/8"

17.5" x 2.4" No7207 7202

1/4" 72091/2" 7211

L Sodium Sulfate Moisture Trap 59** <1ppm 100psig 1/4" 9.0" x 1.5" Yes 81533 81534*Length is measured from endfitting to endfitting †these traps are disposable **Capacity based on 50% efficiency

Page 18: Capillary Accessories · 2009-10-08 · Capillary Accessories ACCESSORIES Universal Guard Column Kits • Universal kits connect to any capillary column • Guard columns are deactivated

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4829

46534833

48364661

A C C E S S O R I E S

Purifi ers

Alltech Oxygen TrapsProtect columns from oxygen contamination

Prevent oxidation of column stationary phases with Alltech oxygen traps. Use an oxygen trap to help maintain column performance and prolong column life. Traps are available in cartridge and in-line styles. Choose an indicating trap to easily identify when trap is spent or to use in conjunction with larger capacity traps. Some traps can be regenerated—see table on following page.

CARTRIDGE OXYGEN TRAPSPHOTO DESCRIPTION CAPACITY(ML) EFFICIENCY PRESSURE LIMIT DIMENSIONS (L X O.D.) INDICATOR PART NO. PRICE

Cartridge Style TrapsA AT™-Indicating Oxy 104 <1ppb 100 psig 13.2" x 1.5" Yes 81015B AT™-Omni 48 <1ppb 100 psig 13.2" x 1.5" Yes 81012

Baseplate Unit 81025

C) Oxy-Trap™

- Features OXY-MAX™ adsorbent- Compact coil design

In-Line Style Oxygen Traps

Traps are freely supported on gas lines taking up no bench space. Several types are available to suit most applications.

D) Large Oxy-Trap™

- Same as original Oxy-Trap™ except larger capacity

E) Indicating Oxy-Trap™

- Features OXY-MAX™ adsorbent- Glass housing eliminates diffusion

F) Indicating Oxy-Purge™

- Glass housing eliminates diffusion- Endfi ttings contain 40µm SS frits for particulate

control

Alltech’s OXY-MAX™ is the most effi cient oxygen adsorbent available. Traps containing OXY-MAX™ remove 02 to less than 1ppb.

B) AT™-Omni Cartridge- features the OXY-MAX™ adsorbent- Also removes moisture and hydrocarbons- Easy to replace - simply change

cartridge- Gas fl ow stops while cartridge is charged- Order baseplate separately below

Cartridge Style Oxygen Traps

A) AT™-Indicating Oxy Cartridge - features the OXY-MAX™ adsorbent- Easy to replace - simply change cartridge- Gas fl ow stops while cartridge is charged- Order baseplate separately below

Glass housing eliminates diffusionGlass housing eliminates diffusion

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402 403

4830

4831

48324835

4837

4839

IN-LINE OXYGEN TRAPS

PHOTO DESCRIPTIONCAPACITY(ML) EFFICIENCY

PRESSURELIMIT FITTING

DIMENSIONS(L X O.D.) INDICATOR PART NO. PRICE

REGENERATIONSERVICE

PART NO. PRICE

In-Line Style TrapsC Oxy-Trap™ 133 <1ppb 100psig 1/8" 3.5" dia coil No 4001 4001R

1/4" 4002 4002RD Large Oxy-Trap™ 206 <1ppb 100psig 3/8" 3-7/8" dia coil No 4003 4003RE Indicating Oxy-Trap™ 20 <1ppb 100psig 1/4"* 16" x .375" Yes 4004 4014F Indicating Oxy-Purge™ 50 <3ppb 100psig 1/8" 9.5" x 1.5" Yes 14563 N/A† N/A

1/4" 14562G Oxy-Purge®N 156 <30ppb 250psig 1/8" 11" x 1.5" No 14636 N/A† N/A

1/4" 14635H ALL-Pure™ Oxygen Trap 1030 <5ppb 1000psig 1/8" 22.5" x 1.5" No 7040 N/A† N/A

1/4" 7042I Oxi-Clear® Trap 48 <5ppb 125psig 1/8" 5.5" x 2" No 8866 N/A† N/A

1/4" 8864J BIG Oxygen Trap 3000 <50ppb 250psig 1/8" 17.5" x 2.4" No 7213 7204

1/4" 72151/2" 7217

K High Pressure Oxy-Trap™ 456 <1ppb 1800psig 1/4" 11.5" x 1.5" No 8115 8147L Low Pressure Oxisorb® 48 <50ppb 90psig 1/4" 9.0" x 1.0" No 60678 N/A† N/A

*Reducing ferrules are supplied for installation into 1/8" lines. † These traps are disposable.

A C C E S S O R I E S

Purifi ers

G) Oxy-Purge® N- Also removes moisture- Rugged aluminum housing- 40µm SS frits in endfi ttings prevent particulates

from entering gas stream

H) ALL-Pure™ Oxygen Trap- Also removes moisture- Capacity of 1030mL of oxygen

I) Oxi-Clear® Oxygen Trap- Removes oxygen, moisture, and hydrocarbons

J) BIG Oxygen Trap- Our highest capacity trap—3000mL

K) High Pressure Oxy-Trap™

- Features OXY-MAX™ adsorbent- Handles pressures up to 1800psig

L) Low Pressure Oxisorb®

- Also removes moisture

Page 20: Capillary Accessories · 2009-10-08 · Capillary Accessories ACCESSORIES Universal Guard Column Kits • Universal kits connect to any capillary column • Guard columns are deactivated

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404 405

4841

4829

4821

6463

CARTRIDGE AND BASEPLATE HYDROCARBON, CO2, AND SULFUR TRAPS

PHOTO DESCRIPTION SIZE EFFICIENCYPRESSURE

LIMIT FITTINGDIMENSIONS (L X O.D.) INDICATOR PART NO. PRICE

REFILL KIT PART NO. PRICE

Baseplate Style

A Activated Charcoal Trap120cc

<100ppb 100psig1/4" 12.5" x 1.5"

No8133 8124

400cc 1/4" 13.5" x 2.0" 8134

B Hi-EFF®Organic 400cc <100ppb 100psig 1/4" 13.5" x 2.0" Yes (forH2O only)

81300 81352

Cartridge Style (Order baseplate separately below)

C AT™-IndicatingHydrocarbon Trap — <3ppb 100psig — 13.2" x 1.5" Yes

81017 N/A† N/A

D Organic Trap 150cc <100ppb 100psig — 13.2" x 1.5" No 81010 8124

E AT™-Omni Cartridge — <100ppb 100psig — 13.2" x 1.5" Yes (forO2 only)

81012 N/A† N/A

Baseplate 81025 N/A N/A

PurifiersA C C E S S O R I E S

4840

Alltech Hydrocarbon, CO2, and Sulfur Traps

D) Organic Cartridge Trap - Economical

E) AT™-Omni Cartridge Trap- Removes hydrocarbons, moisture

and oxygen- Indicating for oxygen

Eliminate detector noise and increase baseline stability

• Choose baseplate, cartridge, or in-line styles• Indicating hydrocarbon trap available

Alltech hydrocarbon traps adsorb trace amounts of hydrocarbons and organics from your gas stream. Most traps are packed with activated charcoal and adsorb organic compounds larger than methane. Traps are available in a baseplate style that sits on the benchtop, a cartridge style that allows for easy replacement of the trap (requires baseplate unit to be ordered separately), and an in-line style that is freely supported on gas lines. Traps for CO2, and sulfur are also available.

Baseplate Style Traps

A) Activated Charcoal Baseplate Trap- Two sizes available

† These traps are disposable.

Part No. 81025

Don’t forget the baseplate for cartridge style traps C, D, & E!

B) Hi-EFF® Organic Trap- Removes hydrocarbons and moisture- Indicating for moisture

C) AT™-Indicating Hydrocarbon Trap- The only indicating trap available for

hydrocarbons- Changes from bright yellow to dark green

when spent- Reduce costs by changing trap only when

needed- Adsorbs organics larger than C2 down to

<3ppb

Cartridge Style Traps

Page 21: Capillary Accessories · 2009-10-08 · Capillary Accessories ACCESSORIES Universal Guard Column Kits • Universal kits connect to any capillary column • Guard columns are deactivated

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404 405

4847

6365

4845

4849

4846

48484843

65794843

Purifi ersA C C E S S O R I E S

K) ALL-Pure™ Hydrocarbon Trap- Removes hydrocarbons to <3ppb- 1000psig pressure limit

N) Sulfur Purifi er- Also removes moisture, oxygen, C2 and above hydrocarbons, halocarbons, and fl uoro lubricants

M) High Pressure CO2 Adsorber- 1800psig pressure limit- 27mL capacity- Also removes NO2

L) High Pressure Charcoal Trap- 1800psig pressure limit

J) BIG Hydrocarbon Trap- Large 750cc size- Helium purged prior to shipment

H) Hydrocarbon Trap- Economical- 250psig pressure rating

G) Activated Charcoal Trap- Two sizes available

I) Hi-EFF® Organic Trap- Removes hydrocarbons and moisture- Indicating for moisture

F) AT™-Indicating Hydrocarbon Trap- Same features as cartridge format now available in

the in-line style

IN-LINE HYDROCARBON, CO2, AND SULFUR TRAPS

PHOTO DESCRIPTION SIZE EFFICIENCYPRESSURE

LIMIT FITTINGDIMENSIONS

(L** X O.D.) INDICATORPART NO. PRICE

REFILL KIT PART NO. PRICE

In-Line Style

F AT™-Indicating Hydrocarbon Trap — <3ppb 100psig1/8"

16" x .375" Yes 7210 N/A† N/A†

1/4" 7212

G Activated Charcoal Trap120cc

<100ppb 100psig 1/4"13" x 1.25"

No8129 8124

400cc 14.5" x 2.0" 8131

H Hydrocarbon Trap 200cc <20ppb 250psig1/8"

11.5" x 1.5" No14634 7200

1/4" 14633

I Hi-EFF® Organic 400cc <100ppb 100psig 1/4" 14.5" x 2" Yes (for H2O only)

81350 81352

J BIG Hydrocarbon Trap 750cc <15ppb 250psig1/8"

17.5" x 2.4" No7201 7200

1/4" 72031/2" 7205

K ALL-Pure™ Hydrocarbon Trap — <3ppb 1000psig1/8"

22.5" x 1.5" No7035 N/A† N/A†

1/4" 7038L High Pressure Charcoal Trap 200cc <100ppb 1800psig 1/4" 11.5" x 1.5" No 8117 N/A† N/A†

M High Pressure CO2 Adsorber 200cc — 1800psig 1/4" 11.5" x 1.5" No 8119 N/A† N/A†

N Sulfur Purifi er 150cc <1ppb 300psig 1/8" 21" x 1.5" No 7006 N/A† N/A†

*Effi ciency applies to compounds >C4 **Length is measured from endfi tting to endfi tting †These traps are disposable

In-Line Style Traps

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Convenient cartridge baseplate automatically stops gas flow when changing cartridges

Knurled locking ring

4851

A C C E S S O R I E S

Purifiers

ALL-PURE™ GAS PURIFIERS

DESCRIPTION1/8" FITTING

PART NO. PRICE1/4" FITTING

PART NO. PRICE

ALL-Pure™ Gas Specific PurifiersHelium Purifier 7008 7010Hydrogen Purifier 7026 7028Nitrogen Purifier 7007 7009Air Purifier 7029 7031ALL-Pure™ PurifiersMoisture Trap 7034 7036Hydrocarbon Trap 7035 7038Oxygen Trap 7040 7042

Purifier Selectivity and Purity Specifications

PURIFIER CO CO2 O2 H2OSULFUR

COMPOUNDSNON-METHANE HYDROCARBONS

Helium Purifier <1 <1 <1 <1 <1 <3Hydrogen Purifier <1 <1 <1 <1 <1 <3Nitrogen Purifier <1 <1 <1 <1 <1 <3Air Purifier <1 <3Moisture Trap <1 <1Hydrocarbon Trap <3Oxygen Trap <1 <1

* Outlet levels listed indicate ppb concentration based on 50ppm nominal inlet concentration level.

ALL-Pure™ SpecificationsDimensions: 400cc, 21"L x 1.5"o.d. (50.8cm x 3.8cm)Max Flow: 500mL/minMax. Pressure: 1000psigMax. Temp: 80°CMounting: Purifier must be mounted in vertical position

GAS PURIFICATION CARTRIDGE SYSTEMS*

DESCRIPTION PART NO. PRICEREFILL KITPART NO. PRICE

Cartridge System Base Unit** 81025 —Moisture Trap Cartridge 81005 8132Organic Trap Cartridge 81010 8124AT™-Omni Cartridge 81012 —AT™-Indicating Oxy Cartridge 81015 —*Alltech Gas Purification Cartridges are compatible with Chrompack baseplates. Baseplate must be purchased separately.

**Reducing ferrules are supplied for installation into 1/8" gas lines. Includes 1/4" fittings.

Alltech Gas Purification Cartridge Systems

• Replace spent purifiers without shutting down your system

Alltech gas purification cartridges allow replacement of spent cartridges in seconds without shutting down your GC system. Simply pull the spent cartridge off the baseplate and push a new one into place. A knurled locking ring keeps the cartridge locked in place. Four different purification cartridges are available. Multiple cartridges and baseplates can be plumbed together to customize a gas purification system for your application. Order each cartridge separately below.

Moisture Trap Cartridge - Filled with indicating Drierite® and molecular sieve pellets to maximize moisture removal and to indicate when the cartridge requires refilling or replacement. A refill kit is available below.

Organic Trap Cartridge - Removes non-methane hydrocarbons from your gas stream. A refill kit is available below.

AT™-Omni Cartridge - A multi-purpose cartridge filled with OXY-MAX™ and Hi-EFF® Charcoal to effectively remove oxygen, moisture and hydrocarbons. AT™-Omni cartridges are disposable.

AT™-Indicating Oxy Cartridge - Filled with OXY-MAX™ and indicating oxygen adsorbent to efficiently remove oxygen and small amounts of moisture. The indicating material shows a color change when the cartridge is saturated. AT™-Indicating Oxy cartridges are disposable.

ALL-Pure™ Gas Purifiers• One purifier removes multiple contaminants• Reduce impurities to low ppb levels

ALL-Pure™ Gas Purifiers feature a unique proprietary broad spectrum adsorbent material that removes multiple contaminants with a single purifier. Replace three separate purifiers for oxygen, moisture, and hydrocarbons with a single ALL-Pure™ purifier. Purifiers are gas specific or choose purifiers specific for moisture, hydrocarbons or oxygen.

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406 407

Type A Type B6250 6251

4853

AT™-MULTI-PURGE IIDESCRIPTION PART NO. PRICE

AT™-Multi-Purge II®

with 1/8" Fittings 14565with 1/4" Fittings 14564Replacement PartsRefill Kit for Hydro-Purge II® 146371/8" Hydrocarbon Trap 146341/4" Hydrocarbon Trap 14633 1/8" Oxy-Purge® N 146361/4" Oxy-Purge® N 14635

A C C E S S O R I E S

Purifiers

AT™-Multi-Purge II®• Three traps conveniently mounted in one panel• Removes water, oxygen, and hydrocarbons• Easy wall mounting

The AT™-Multi Purge II® is a high capacity, three stage gas purifying module that removes all common contaminates – moisture, hydrocarbons, and oxygen – from GC gas streams. It combines three high capacity traps (Hydro-Purge II®, Hydrocarbon, and Oxy-Purge® N) to permit longer, maintenance-free operation.

The first stage of gas purification removes moisture from the gas stream with the Alltech Hydro-Purge II®. It contains indicating molecular sieve that changes from blue to tan when saturated. Stage two removes hydrocarbon contamination from the gas stream with the Alltech Hydrocarbon trap. The final stage of purification removes oxygen from the gas stream with the Oxy-Purge® N oxygen trap.

An indicating Oxy-Trap™ can be added to the AT™-Multi-Purge II® for maximum column protection. It will monitor the performance of the oxygen trap and undergo a color change from tan to dark brown when spent indicating when the high capacity Oxy-Purge® N requires replacement. Order separately under “Accessories” below.

Each AT™-Multi-Purge II® is supplied with all internal plumbing and installation and operating instructions.

Gas Control/Purification Panels

• Complete gas control and purification station

• Operating pressures up to 100psig

• Allows safer remote placement of cylinders

Alltech’s gas panels provide convenient control and purification of laboratory gases. The panels are supplied with valves, gauges, regulators, purifiers, and fittings that make installing and maintaining gas purifiers easier. Their wall mount design conserves bench top space and allows you to easily view the status of your gas system. Panels can be used as individual stations or grouped together to form a gas control center for the entire lab. Each panel is ready to connect to 1/4" o.d. gas lines. Vespel® reducing ferrules allow connection to 1/8" lines.

Two types of panels are available. Type “A” includes an Alltech Gas Purifier that removes moisture, oil, small aliphatics, HCl, SO2, NO2, H2S, and CO2, and it measures 29" x 4-5/8" x 3" . Type “B” includes an Alltech Gas Purifier and an Alltech Indicating Oxy-Trap™ that also removes oxygen in addition to the other contaminants, and measures 29" x 5-5/8" x 3". Both traps contain indicating adsorbents that allow you to visually determine when they require replacement.

REPLACEMENT PARTSDESCRIPTION PART NO. PRICE

In-Line Gas Purifier, 1/4" 8125Indicating Oxy-Trap™ 4004Regeneration Service for 4004 4014Refill Kit for 8125 8132

GAS CONTROL/PURIFICATION PANELS

GASTYPE A

PART NO. PRICETYPE B

PART NO. PRICE

Hydrogen 8150 8162Air 8152 —Oxygen 8154 —Helium 8156 8164Nitrogen 8158 8166Argon 8160 8168

ACCESSORIESDESCRIPTION PART NO. PRICE

1/4" Indicating Oxygen Trap* 4004* 1/8" reducing ferrules are supplied.

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408 409

6516

A C C E S S O R I E S

Purifiers

SGT Super-Clean® FiltersImprove baselines, minimize interferences, and reduce MS maintenance

• Remove impurities to deliver 99.9999% pure gas• Exchange filters in seconds, without introducing air into the system• Diffusion-proof with glass and metal construction• Pressure resistant up to 150psig (11 bar)

These SGT Super-Clean® filters can be used on all of your GC gas lines to deliver 99.9999% pure gas. Filters are available for oxygen, moisture and hydrocarbons. The Combi filter removes both moisture and hydrocarbons. The Triple filter removes moisture, oxygen, and hydrocarbons and is available purged with Argon for standard applications or purged with Helium for MS applications.

Filters feature a quick change baseplate/cartridge design. Cartridges can be exchanged within seconds, during analysis, and without tools. 1-,2-,3-, or 4-position baseplates are available and will accept any of the GC filter cartridges. Baseplates must be ordered separately (except for systems). Filter cartridge bundles include the most popular filters in one package. Various filter systems are available and include the appropriate baseplate.

SpecificationsMaximum Flow: 7.0L/minEfficiency: <0.1ppm@2L/minMaximum Pressure: 150psigConnectors: 1/8" Brass

Capacities

TYPE OF FILTER H20 02

HYDROCARBON(AS N-BUTANE) INDICATOR

Moisture: 7.2g — — YesOxygen: — 1000mL — YesHydrocarbon: — — 12.0g NoCombi: 3.6g — 6.0g Moisture OnlyTriple (Argon): 1.8g 500mL 4.0g Moisture & OxygenTriple (Helium): 2.0g 600mL 4.0g Moisture & Oxygen

FILTER BUNDLES AND SYSTEMSDESCRIPTION PART NO. PRICE

Filter Cartridge Bundles1-Triple (Argon packed) + 2-Combi F0730Oxy + Moisture + 2-Hydrocarbon F0740Filter System (Cartridges+Baseplate)1-Triple (Argon packed) + 1-position Baseplate B10101-Triple (Helium packed) + 1-position Baseplate B10112-Combi + 2-position Baseplate B10202-Moisture + 2-position Baseplate B10221-Triple (Argon packed) + 2-Combi +3-position Baseplate

B1030

1-Oxygen + 1-Moisture + 2-Hydrocarbon + 4-position Baseplate

B1040

Triple Filter F0301 shown on baseplate (order separately).

FILTERS AND BASEPLATESDESCRIPTION PART NO. PRICE

Filter CartridgesTriple Filter (Argon packed) F0301Triple Filter (Helium packed) F0302Combi Filter F0201Moisture Filter F0101Oxygen Filter F0102Hydrocarbon Filter F0103Baseplates1-Position Baseplate B00102-Position Baseplate B00203-Position Baseplate B00304-Position Baseplate B0040

Contact Alltech Tech Support:

Email: [email protected] Online: www.alltechWEB.com

Not sure which filter you need?

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408 409

4858

4859

4854

A C C E S S O R I E S

Purifiers

Universal Mounting Panel• Mount up to 5 purifiers for easy monitoring and

replacement• Pre-drilled for easy mounting• Fits most manufacturers’ purifiers

This lightweight aluminum mounting panel will hold up to five purifiers. Pre-drilled holes are spaced at 3⁄4" centers in five vertical rows to allow for maximum versatility. Mounting clips to accommodate purifiers from 7/8" to 2-1/2" o.d. are sold separately below. Panel measures 17"W x 24"H.

UNIVERSAL MOUNTING PANELDESCRIPTION QTY. PART NO. PRICE

Universal Mounting Panel ea 7220Universal Mounting ClipsFits 7/8" to 1" o.d. Traps 2/pk 7221 Fits 1-1/8" to 1-3/8" o.d. Traps 2/pk 7223Fits 1-3/8" to 1-5/8" o.d. Traps 2/pk 7225Fits 1-5/8" to 1-7/8" o.d. Traps 2/pk 7227Fits 2" to 2-1/2" o.d. Traps 2/pk 7229

IN-LINE PARTICULATE FILTERSDESCRIPTION PART NO. PRICE

1/4" In-line Brass Filter 80521/8" In-line Brass Filter 8054

In-Line Particulate Filter• Economically remove particulates from gas streams

This brass in-line particulate filter is a convenient, inexpensive way to remove particulates from critical gas streams. Each unit includes one 10 micron filter cartridge. The maximum pressure rating is 500psig.

Leaking?Ensure leak-free installation of your gas purifiers. See page 397 for gas leak detectors.

AT™-Purifier Shield for In-Line Traps• Protect AT™ purifiers from damage

This shield is compatible with the Alltech In-Line acrylic purifiers. The AT™-Purifier Shield slips over your existing Alltech purifier, protecting the cartridge while still allowing visual monitoring of the contents of the trap.

Make quick purifier connections!See page 421 for Quick-Connect Fittings.

Purifier Accessories

AT™ CARTRIDGE SHIELDDESCRIPTION PART NO. PRICE

Shield for 120cc Purifier 81210

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410

5244

5246

5247

5248

5245

Pressure RegulatorsA C C E S S O R I E S

A) Dual Stage Economy Regulators

These regulators are suitable for pressure control of general purpose laboratory gases with applications requiring constant pressure control and delivery regardless of supply pressure variations. Typical applications include purging, pressure testing, blanketing, and chamber pressurization.

E) Panel Mount Regulators These regulators can also be used in-line.

Order gauges and mounting nut separately.

D) Single Stage Liquid Cylinder Regulators

These regulators are suitable for primary pressure control of gases supplied from cryogenic liquid cylinders. Typical applications include regulation of liquid nitrogen, oxygen, and carbon dioxide.

C) Single Stage Regulators These regulators are suitable for secondary

pressure control of noncorrosive, high purity gases or as point of use pressure control in high purity gas distribution systems. Typical applications include point of use laboratory systems, gas supply purging, and bulk gas distribution systems.

B) Dual Stage HighPurity Regulators

These regulators are suitable for secondary pressure control of noncorrosive or high purity gases for applications requiring constant pressure control and delivery regardless of supply pressure variations. Typical applications include gas supply purging, gas system charging, fuel gas supply control, and calibrations gas control.

DUAL STAGE HIGH PURITYDESCRIPTION CGA NO. PART NO. PRICE

H2, Ar/Methane 350 8109He, N2, Ar, Ne 580 8111

DUAL STAGE ECONOMYDESCRIPTION CGA NO. PART NO. PRICE

H2, Ar/Methane 350 8101O2 540 8102He, N2, Ar, Ne 580 8103Air 590 8104Air, Breathing Quality 346 8105

SINGLE STAGEDESCRIPTION CGA NO. PART NO. PRICE

0-40psig (delivery pressure) — 818900-120psig (delivery pressure) — 818910-200psig (delivery pressure) — 81892

PANEL MOUNTDESCRIPTION CGA NO. PART NO. PRICE

Panel Mount Regulator — 81896Panel Mounting Nut — 81895Pressure Gauges for Panel Mount Regulators0-30psig — 868000-60psig — 868020-100psig — 868040-200psig — 86808

Alltech Regulators

Specifi cations for Alltech RegulatorsA) DUAL STAGE ECONOMY B) DUAL STAGE HIGH PURITY C) SINGLE STAGE D) SINGLE STAGE LIQUID CYLINDER E) PANEL MOUNT

Body: Forged Brass Chrome-plated forged brass Chrome-plated forged brass Chrome-plated forged brass BrassBonnet: Brass-plated die cast zinc Chrome-plated die cast zinc Chrome-plated die cast zinc Chrome-plated die cast zinc Acetal ResinDiaphragm: PTFE -lined neoprene 316L Stainless Steel 316L Stainless Steel 316L Stainless Steel NitrileSeat & Internal Seal: PTFE PTFE PTFE PTFE Acetal ResinMas. Inlet Pressure: 3000psig (210 bar) 3000psig (210 bar) 3000psig (210 bar) 3000psig (210 bar) 400psigDelivery Press. Range: 0-120psig 0-120psig 0-40, 0-120, or 0-200psig 0-40 or 0-120psig —Delivery Press. Gauge: 0-20psig 0-200psig 0-60, 0-200, or 0-400psig 0-60 or 0-200psig Order SeparatelyCylinder Press. Gauge: 0-4000 psig 0-4000psig 0-4000psig 0-4000psig 0-4000psigTemperature Range: -40 to 60°C -40 to 60°C -40 to 60°C -40 to 60°C -34 to 65°CGauges: 2-1/2" diameter brass 2-1/2" diameter brass 2-1/2" diameter brass 2-1/2" diameter brass Order SeparatelyPorts: 1/4" FPT 1/4" FPT 1/4" FPT 1/4" FPT 1/8" FPT

SINGLE STAGE LIQUID CYLINDERDESCRIPTION CGA NO. PART NO. PRICE

CO2, 0-40psig 320 81899N2, 0-40psig 580 81893O2, 0-40psig 540 81897CO2, 0-120psig 320 81900N2, 0-120psig 580 81894O2, 0-120psig 540 81898

Need Cylinder Accesories?Alltech carries cylinder accessories. See page 390 for more information.

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6644 6642 6738 6645 6643

Gas SamplingA C C E S S O R I E S

Fittings

Alltech offers a large variety of gas sampling bag fi ttings. Consider the following when selecting a fi tting:1. How will you collect the sample? What type of connection is available to connect to the bag?2. How will you need to access the sample once it is collected in the bag?3. Is your sample compatible with the fi tting material?

Gas Sampling Bag Selection GuideFEP Gas Sampling Bags, 5mil

FITTINGS AVAILABLETENSILE STRENGTH*

(BY ASTM D-882) PERMEABILITYTEMPERATURE RANGE (°C) SAMPLE COMPATIBILITY ADVANTAGE

2,500-3000psig (Note: This is NOT a burst pressure rating for the bag.)

Gas CO2

HydrogenNitrogenOxygenAcetic AcidVaporAcetoneBenzeneCCl4EthanolHexaneWater

Permeability**167022003207500.41Permeability***0.950.640.310.690.560.45

-240 to 260 Inert and solvent resistant to virtually all chemicals except molten alkali metals, gaseous fl uorine, complex halogenated compounds at elevated pressure and temperature

Low permeability to liquids, gases, moisture and organic vapors; suitable for cryogenic use

Barbed on/off Septum Port Dual 1/4" SS Fitting2N1 Combination

Nickel-plated Barbed On-Off Valve

PTFE Septum Port Dual On-Off/Septum 1/4" SS Swagelok® 2N1 CombinationOn-Off/Septum

Need a syringe? See pages 55-71 for our complete selection of syringes.

Tedlar® PVF, 2mil

FITTINGS AVAILABLETENSILE STRENGTH*

(BY ASTM D-882) PERMEABILITYTEMPERATURE RANGE (°C) SAMPLE COMPATIBILITY ADVANTAGE

Barbed on/off Septum Port Dual 1/4" SS Fitting2N1 Combination

17,000-18,000psig (Note: This is NOT a burst pressure rating for the bag.)

Gas CO2

HydrogenNitrogenOxygenVaporAcetic AcidAcetoneBenzeneCCl4Ethyl AcetateEthanolHexaneWater

Permeability**11.11500.253.2Permeability***4510,00090501.0003555180

-234 to 300 Recommended for analysis of non-corrosive gases, TCLP gases, CO, H2S, radon, and mercaptans; “Grab” sampling; preparation of calibration gas standards; gas blending; stack sampling; emission testing

Lowest permeability of all types of bags; economical alternative to PTFE; easily cleaned and reused

Cali-5-Bond™ 5.5mil (polyethylene, polyamide, aluminum foil, polyvinyl, chloride polyester)

FITTINGS AVAILABLETENSILE STRENGTH*

(BY ASTM D-882) PERMEABILITYTEMPERATURE RANGE (°C) SAMPLE COMPATIBILITY ADVANTAGE

2N1 Combination Barbed on/off Septum Port

— — Max. 54 Designed specifi cally for collecting air samples; suitable for the storage and transportation of gas samples

Opaque bag protects sample from UV degradation; bags may be purged with nitrogen or pure air and reused

*Tensile strength is the maximum force required to rupture a one inch wide specimen. ** cc/(100in2)(24hrs)(atm/mil) *** gms/(100in2)(24hrs/mil)

© Copyright 2004 Alltech Associates, Inc.© Copyright 2004 Alltech Associates, Inc.

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6646

Gas SamplingA C C E S S O R I E S

Alltech Tedlar® Gas Sampling Bags• High tensile strength resists puncture• Low permeability minimizes sample loss

Alltech Tedlar® bags are manufactured from sturdy 2mil PVF film that is inert to a wide range of gases. Low permeability ensures the integrity of your sample and makes Tedlar® bags the ideal choice for off site analysis.

ALLTECH TEDLAR® GAS SAMPLING BAGS

NOMINAL SIZE VOLUMEBARBED ON-OFF VALVE PART NO. PRICE

SEPTUM PORTPART NO. PRICE

DUAL ON-OFF/SEPTUM PORT PART NO. PRICE

1/4" SS SWAGELOK® PART NO. PRICE

6" x 6" 0.6L 41021 41023 41025 410276" x 10" 1.2L 41029 41031 41033 410356" x 12" 1.5L 41037 41039 41041 410439" x 9" 2L 41045 41047 41049 41051

12" x 12" 5L 41053 41055 41057 4105912" x 19" 10L 41063 41065 41067 4106918" x 18" 16L 41071 41073 41075 4107724" X 24" 40L 41079 41081 41083 4108524" x 30" 56L 41087 41089 41091 4109324" x 36" 73L 41095 41097 41099 4103230" x 30" 80L 41034 41036 41038 41042

Alltech FEP Gas Sampling Bags• 5mil thickness for durability• Manufactured and packaged under GLP conditions

Alltech FEP bags have a 5mil film thickness making them suitable for harsh sampling conditions. Bags are chemically resistant to the most severe corrosives. Choose from 4 different port types.

ALLTECH FEP GAS SAMPLING BAGS

NOMINAL SIZE VOLUMEBARBED ON-OFF VALVE PART NO. PRICE

SEPTUM PORT PART NO. PRICE

DUAL ON-OFF/SEPTUM PORT PART NO. PRICE

1/4" SS SWAGELOK® PART NO. PRICE

6" x 6" 0.6L 41044 41046 41048 410526" x 10" 1.2L 41054 41056 41058 410646" x 12" 1.5L 41066 41068 41072 410749" x 9" 2L 41076 41078 41082 41084

12" x 12" 5L 41086 41088 41092 4109412" x 19" 10L 41106 41108 41109 4112518" x 18" 16L 41127 41129 41131 4113324" x 24" 40L 41135 41137 41139 4114924" x 30" 56L 41151 41153 41155 4115724" x 36" 73L 41126 41128 41132 4113430" x 30" 80L 41136 41138 41152 41154

REPLACEMENT PARTS FOR TEDLAR® AND FEP BAGSDESCRIPTION PART NO. PRICE

Replacement Septa for Septa Port, 10/pk 411581/4" PTFE No Hole Ferrules for 1/4" SS Fitting, 10/pk RF-400/0-T

Replacement Parts

Gas Sampling Bags

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412 413

6648 1651

Gas SamplingA C C E S S O R I E S

Cali-5-Bond™ 5-Layer Gas Sampling Bags• Non-permeable• Opaque to UV and visible light• Inert, fl exible, tough and reusable

5-LAYER GAS SAMPLING BAGSNOMINAL SIZE VOLUME PORT DESCRIPTION PART NO. PRICE

Snout-Shaped Gas Sampling Bags8 x 15" 2L Barbed Valve 1" Septa 41508 x 27" 5L Barbed Valve 1" Septa 415216 x 16" 10L Barbed Valve 1" Septa 418616 x 29" 22L Barbed Valve 1" Septa 415423.5 x 28" 44L Barbed Valve 1" Septa 4156Pillow-Shaped Gas Sampling Bags8 x 8" 1L Barbed Valve 1" Septa 41888 x 11" 2L Barbed Valve 1" Septa 419016 x 19" 15L Barbed Valve 1" Septa 419223.5 x 31" 60L Barbed Valve 1" Septa 419431 x 31.5" 90L Barbed Valve 1" Septa 419631 x 55" 170L Barbed Valve 1" Septa 4198

COMBO VALVE GAS SAMPLING BAGS

SIZE VOLUME PORT DESCRIPTION PART NO. PRICE

Tedlar® Gas Sampling Bags7 x 7" 1L 2N1 41001 9 x 9" 2L 2N1 410039 x 12" 3L 2N1 4100512 x 12" 5L 2N1 4100712 x 19" 10L 2N1 4101112 x 21" 12L 2N1 4101318 x 24" 25L 2N1 41017FEP Gas Sampling Bags6 x 6" 0.6L 2N1 410026 x 10" 1.2L 2N1 410046 x 12" 1.5L 2N1 410069 x 9" 2L 2N1 4100812 x 12" 5L 2N1 4101212 x 19" 10L 2N1 4101618 x 18" 16L 2N1 41018

TEDLAR® COMBO VALVE MULTI-PACKS

SIZE VOLUMEPORT

DESCRIPTION QTY PART NO. PRICE

7 x 7" 1L 2N1 10 480019 x 9" 2L 2N1 10 4800312 x 12" 5L 2N1 10 4800712 x 19" 10L 2N1 10 4801118 x 24" 25L 2N1 5 48017

Combo valve gas sampling bags give the convenience and ease of a barbed on/off valve and a septum port combined into one fi tting. The valve fi tting features a 3/16" stem, which is suitable for use with most 1/4" tubing, and a sampling port. Bags are available in Tedlar® and FEP as well as convenient multi-packs.

Combo Valve Gas Sampling Bags• On/off valve and septum in one fi tting• Save with convenient multi-packs

Cali-5-bond™ gas sampling bags are constructed from inert 5.5mil thick material made from fi ve layers of fi lm. The layers are comprised of an inner layer of high-density polyethylene, followed by polyamide, an aluminum foil barrier, a polyvinylidene chloride layer and an outer layer of polyester. These bags are specifi cally designed for air sampling and are suitable for the storage and transportation of gas samples.

Cali-5-Bond™ bags are available in both pillow and snout shapes. The snout provides additional entry into the bag for fl ushing and sample collection.

Bags are equipped with a barbed on-off valve and silicone septum for easy sampling and can be purged with nitrogen or pure air gas and reused.

Gas Sampling Bags

Contact Alltech Customer Service:

Online Ordering 24 hours a day: www.alltechWEB.comEmail: [email protected]

Have a Question about Your Order?

• On/off valve and septum in one fi tting• On/off valve and septum in one fi tting

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4668

4663

4664

4665

4667

6310

(Can not included)

Gas SamplingA C C E S S O R I E S

Gas Sampling Bulb with Septum Ports• PTFE stop cocks for increased compatibility

GAS SAMPLING BULBSDESCRIPTION PART NO. PRICE

125mL, PTFE Stopcock 7012250mL, PTFE Stopcock 7013500mL, PTFE Stopcock 70111000mL, PTFE Stopcock 7066Replacement Septa, 12/pk 7000

CAN PIERCING UNITDESCRIPTION PART NO. PRICE

Can Piercer 8013Replacement Septa, 12/pk 8015Replacement Gaskets, 12/pk 8016

Can Piercing Unit

Can piercer allows small samples to be taken without signifi cantly disturbing the equilibrium conditions in the container. The piercer can be affi xed to the side of a round container with supplied steel straps.

VACUUM SAMPLERDESCRIPTION PART NO. PRICE

280mL (1 needle), ea 8020280mL (2 needles) 12/pk 8022Replacement Septa, 12/pk 8015

Vacuum Sampler• No external pump required• Reusable

These evacuated 280mL vacuum samplers are fi tted with a unique septum port and needle guide through which the container is fi lled and samples removed. A 4" long needle is supplied with each vacuum sampler (2 needles with the package of 12 samplers).

Gas Sampling Bulb with Injection Port & Valve Stopcocks

• Stored sample contacts only glass and PTFE• Suitable for vacuum or pressure• Semi-needle valve control

Gas Sampling Bulb with Twist-Lock Stopcocks

• Unique twist-lock stopcocks• PTFE outlet tube connectors

GAS AND VAPOR SAMPLERDESCRIPTION PART NO. PRICE

Gas and Vapor Sampler Kit 4182Replacement Bags, 10/pk 4184

Gas and Vapor Sampler• Sample bags are removable and resealable

Collect samples in resealable 200cc multilayer bags. Simply evacuate the can is ter using the supplied aspirator bulb. The bags can be re moved for stor age or ship ment, free ing the canister for fur ther sam pling. Ten bags are in clud ed with each kit.

GAS SAMPLING BULBSDESCRIPTION PART NO. PRICE

125mL 6940250mL 6942500mL 694413-425 Open-Hole Caps, 100/pk 73090TFE/Silicone Liners, 100/pk 98123

GAS SAMPLING BULBSDESCRIPTION PART NO. PRICE

125mL, PTFE Stopcock 6950250mL, PTFE Stopcock 6952500mL, PTFE Stopcock 6954Replacement Septa, 10/pk 6900

Gas Sampling Accessories

• PTFE stop cocks for increased compatibility• PTFE stop cocks for increased compatibility

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414 415

FerrulesA C C E S S O R I E S

PTFE FerrulesPTFE ferrules are completely inert and an economical

choice. They have an upper temperature limit of 250°C. PTFE ferrules conform well to the shape of the column upon compression and can be reused if handled carefully.

Graphite FerrulesThese 99.95% pure graphite ferrules can be used at

temperatures up to 450°C without producing bleed or decomposition products. The one-piece design requires no back ferrules. Graphite ferrules are very soft and conform well to the column on compression. These ferrules can be reused as long as care is taken not to overtighten them.

Vespel® FerrulesVespel® ferrules do not cold flow, are easily reusable,

and withstand temperature up to 350°C. At high temperatures, Vespel® may adhere to glass or metal.

Ferrule PropertiesMATERIAL TEMP. LIMIT REUSABILITY RESEALING PROPERTIES SUITABILITY FOR GLASS TEMP. PROG.PTFE 250°C Good Excellent Excellent NoGraphite 450°C Good Excellent Excellent YesVespel® 350°C+ Excellent Good Good YesVG1 400°C Excellent Good Excellent YesVG2 400°C Excellent Good Excellent Yes

Vespel®/Graphite FerrulesComposites of Vespel® and graphite combine the

advantages of the two materials. They are less likely to adhere to the column than Vespel® but are more durable than graphite. Ferrules are easy to reuse and stable at temperatures to 400°C.

Two types of composites are available. The VG1 composite is 85% Vespel®/15% graphite and suitable for all-purpose applications. The VG2 type is 60% Vespel®/40% graphite and exhibits added lubricity.

PTFE AND GRAPHITE FERRULESDESCRIPTION FITTING SIZE TUBING SIZE QTY PTFE PART NO. PRICE GRAPHITE PART NO. PRICE

Straight Ferrules

Used when the tubing o.d. matches the nominal size of the fitting being used.

1" 1" 2 — — 143617/8" 7/8" 2 — — 143603/4" 3/4" 2 — — 143585/8" 5/8" 2 — — 143571/2" 1/2" 10 — — SF-800-G3/8" 3/8" 10 SF-600-T SF-600-G1/4" 1/4" 10 SF-400-T SF-400-G3/16" 3/16" 10 SF-300-T SF-300-G1/8" 1/8" 10 SF-200-T SF-200-G1/16" 1/16" 10 SF-100-T SF-100-G

Reducing Ferrules1/4" 1/16" 10 RF-400/100-T RF-400/100-G1/4" 0.8mm 10 — — RF-400/0.8-G1/4" 1/8" 10 RF-400/200-T RF-400/200-G1/4" 3/16" 10 RF-400/300-T 143271/4" 4mm 10 — — 14384

Used when the tubing o.d. is smaller than the nominal size of the fittings.

1/4" 6mm 10 RF-400/6MM-T RF-400/6MM-G1/8" 1/16" 10 RF-200/100-T RF-200/100-G1/8" 1.2mm 10 — — 143261/8" 1.0mm 10 — — 143111/8" 0.8mm 10 — — RF-200/0.8-G1/8" 0.5mm 10 — — RF-200/0.5-G1/8" 0.4mm 10 — — RF-200/0.4-G1/8" 1.2mm 10 — — 143051/16" 1.0mm 10 — — RF-100/1.0-G1/16" 0.8mm 10 — — RF-100/0.8-G1/16" 0.5mm 10 — — RF-100/0.5-G1/16" 0.4mm 10 — — RF-100/0.4-G1/16" 0.3mm 10 — — 14308

GC Ferrule Selection

What ferrule type do you need?FERRULE TYPE USE FOR:0.4mm Hole: Capillaries with i.d. of 0.10-0.25mm0.5mm Hole: Capillaries with i.d. of 0.28-0.35mm0.8mm Hole: Capillaries with i.d. of 0.45-0.53mmNO-HOLE: As plugs, or drill for special needs2-HOLE: Connecting 2 pieces of capillary tubing

or columns to the same fitting end

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416 417

PTFE AND GRAPHITE FERRULES (CONT’D)DESCRIPTION FITTING SIZE TUBING SIZE QTY PTFE PART NO. PRICE GRAPHITE PART NO. PRICE

HP/Agilent Short Ferrules1/16" 1.2mm 10 — — 143701/16" 1.0mm 10 — — 143251/16" 0.8mm 10 — — 143241/16" 0.5mm 10 — — 143231/16" 0.4mm 10 — — 143221/16" 0.3mm 10 — — 14321

Two-Hole Ferrules1/8" 0.8mm 10 — — 143341/8" 0.5mm 10 — — 143071/16" 0.5mm 10 — — 14330

No-Hole Ferrules3/8" 10 — 143321/4" 10 RF-400/0-T 143281/8" 10 RF-200/0-T 143141/16" 10 RF-100/0-T 14310

Graphite Ferrules for HP/Agilent Nuts0.5mm 10 — — 15479011.0mm Hole 10 — — 1548001

FerrulesA C C E S S O R I E S

VESPEL® AND VESPEL®/GRAPHITE FERRULES

DESCRIPTIONFITTING SIZE TUBING SIZE QTY

VESPEL®

PART NO. PRICEVG1

PART NO. PRICEVG2

PART NO. PRICE

Straight Ferrules1/4" 1/4" 10 SF-400-V SF-400-VG1 SF-400-VG21/4" 1/4" 10 15449* 15449* 15451*1/8" 1/8" 10 SF-200-V SF-200-VG1 SF-200-VG21/8" 1/8" 10 — — 15450* 15452*1/16" 1/16" 10 SF-100-V SF-100-VG1 SF-100-VG2

Reducing Ferrules1/4" 6mm 10 RF-400/6MM-V 400/6MM-VG1 400/6MM-VG21/4" 3/16" 10 RF-400/300-V 400/300-VG1 400/300-VG21/4" 1/8" 10 RF-400/200-V 400/200-VG1 400/200-VG21/4" 1/16" 10 RF-400/100-V 400/100-VG1 400/100-VG21/4" 0.8mm 10 — — 400/0.8-VG1 400/0.8-VG21/8" 1/16" 10 RF-200/100-V 200/100-VG1 200/100-VG21/8" 0.8mm 10 — — 200/0.8-VG1 200/0.8-VG21/8" 0.5mm 10 — — 200/0.5-VG1 200/0.5-VG21/8" 0.4mm 10 — — 200/0.4-VG1 200/0.4-VG21/16" 1.0mm 10 RF-100/1.0-V 100/1.0-VG1 100/1.0-VG21/16" 0.9mm 10 RF-100/0.9-V 100/0.9-VG1 100/0.9-VG21/16" 0.8mm 10 RF-100/0.8-V 100/0.8-VG1 100/0.8-VG21/16" 0.5mm 10 RF-100/0.5-V 100/0.5-VG1 100/0.5-VG21/16" 0.4mm 10 RF-100/0.4-V 100/0.4-VG1 100/0.4-VG21/16" 0.3mm 10 — — 100/0.3-VG1 — —

No-Hole Ferrules1/4" — 10 RF-400/0-V 400/0-VG1 400/0-VG21/8" — 10 RF-200/0-V 200/0-VG1 200/0-VG21/16" — 10 RF-100/0-V 100/0-VG1 100/0-VG2

Two-Hole Ferrules1/16" 0.5mm 10 — — 15486 15488 1/16" 0.4mm 10 — — 15481 15487

* Equivalent to Parker one-piece metal ferrule.

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416 417

Tubing

FittingsA C C E S S O R I E S

Female Pipe Thread Connectors

Fittings Selection GuideTo determine the size of a nut or female pipe thread, compare it to the silhouettes below. To determine the size

of a ferrule, measure its inside diameter. Please note that tubing fi tting sizes are based on the outside diameter of the tube, while pipe thread fi tting sizes are based on the inside dimension of the pipe. Pipe and tubing fi ttings are not interchangeable.

Tubing Nut Sizes

* Silhouettes shown at actual size

1/16" 1/8" 3/16" 1/4" 3/8" 1/2"0127

Parker FittingsParker fi ttings are available in two forms: the CPI one-piece ferrule and the A-Lok two piece ferrule. Most parts

are available in brass or stainless steel and should be matched to the tubing, particularly in thermal applications.

Tubing

5767

1/8" (6-2-GBG) 1/4" FPT 3/8" FPT 1/2" FPT1/8" FPT

PARKER FITTINGS

DESCRIPTION DIMENSIONS QTY

A-LOKBRASS

PART NO. PRICE

CPIBRASS

PART NO. PRICE QTY

A-LOK SS

PART NO. PRICE

CPI SS

PART NO. PRICE

Nuts1/16" 10/pk 11600 14057 10/pk 11700 1415751/8" 10/pk 11601 14058 10/pk 11701 141583/16" 10/pk 11602 60000 10/pk 11702 610001/4" 10/pk 11603 14059 10/pk 11703 141593/8" 10/pk 11604 60002 10/pk 11704 6100251/2" 10/pk 11605 600045 5/pk 11705 610045

Ferrules1/16" 10/pk 11606 14060 10/pk 11706 1416051/8" 10/pk 11607 14061 10/pk 11707 141613/16" 10/pk 11608 60006 10/pk 11708 610061/4" 10/pk 11609 14062 10/pk 11709 141623/8" 10/pk 11610 60008 10/pk 11710 6100851/2" 5/pk 11611 600105 5/pk 11711 610105

Tees1/16" ea 11612 14075 ea 11712 141751/8" ea 11613 14053 ea 11713 141763/16" ea 11614 60012 ea 11714 610121/4" ea 11615 14077 ea 11715 141773/8" ea 11616 60014 ea 11716 610141/2" ea 11617 60016 ea 11717 61016

CPI A-LOK

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418 419

FittingsA C C E S S O R I E S

PARKER FITTINGS (CONT'D)

DESCRIPTION DIMENSIONS QTY

A-LOK BRASS

PART NO. PRICE

CPI BRASS

PART NO. PRICE QTY

A-LOK SS

PART NO. PRICE

CPI SS

PART NO. PRICE

Unions1/16" ea 11618 14063 ea 11718 141631/8" ea 11619 14065 ea 11719 141653/16" ea 11620 60018 ea 11720 610181/4" ea 11621 14068 ea 11721 141683/8" ea 11622 60020 ea 11722 610201/2" ea 11623 60022 ea 11723 61022

Reducing Unions1/8" to 1/16" ea 11624 14064 ea 11724 141643/16" to 1/8" ea 11625 60024 ea 11725 610241/4" to 1/16" ea 11626 60026 ea 11726 141661/4" to 1/8" ea 11627 60028 ea 11727 610281/4" to 3/16" ea 11628 14067 ea 11728 141673/8" to 1/16" ea — — — — ea 11729 141743/8" to 1/4" ea 11630 60030 ea 11730 61030

Capillary Union1/16" ea — — — — ea — 28812

Female Pipe Thread Connectors (Tube to FPT)1/8" to 1/8" FPT ea 11800 60048 ea 11750 610481/8" to 1/4" FPT ea 11801 14071 ea 11751 610841/4" to 1/8" FPT ea 11802 60050 ea 11752 610501/4" to 1/4" FPT ea 11803 14072 ea 11753 610863/16" to 1/8" FPT ea 11804 60052 ea 11754 610523/8" to 1/8" 6-2-GBZ ea 11805 60054 ea 11755 610543/8" to 1/4" FPT ea 11806 60056 ea 11756 61056

Male Pipe Thread Connectors (Tube to MPT)1/16" to 1/16" MPT ea 11632 60034 ea 11732 610341/16" to 1/8" MPT ea 11633 60036 ea 11733 610361/8" to 1/8" MPT ea 11634 60038 ea 11734 610381/8" to 1/4" MPT ea 11635 60039 ea 11735 610393/16" to 1/8" MPT ea 11636 60040 ea 11736 610401/4" to 1/8" MPT ea 11637 60042 ea 11737 610423/8" to 1/8" MPT ea 11638 60044 ea 11738 610441/4" to 1/4" MPT ea 11639 14069 ea 11739 610823/8" to 1/4" MPT ea 11640 60046 ea 11740 61046

Tube End Connectors (Reducers)1/16" to 1/8" tube ea 11807 60058 ea 11757 610581/16" to 1/4" tube ea — — — — ea 11758 610591/8" to 1/4" tube ea 11809 60060 ea 11759 610601/8" to 3/16" tube ea 11810 60062 ea 11770 610623/16" to 1/4" tube ea 11811 4052 ea 11771 610641/4" to 1/8" tube ea 11812 14073 ea 11772 141691/4" to 3/8" tube ea 11813 60066 ea 11773 610663/8" to 1/4" tube ea 11814 60068 ea 11774 61068

Caps1/16" ea 11815 14047 ea 11835 141511/8" ea 11816 14051 ea 11836 141523/16" ea 11817 60070 ea 11837 610701/4" ea 11818 14052 ea 11838 141533/8" ea 11819 60072 ea 11839 610721/2" ea 11820 60074 ea 11840 61074

Plugs1/16" ea 11821 14054 ea 11841 141541/8" ea 11822 14055 ea 11842 141553/16" ea 11823 60076 ea 11843 610761/4" ea 11824 14066 ea 11844 141563/8" ea 11825 60078 ea 11845 610781/2" ea 11826 60080 ea 11846 61080

Page 35: Capillary Accessories · 2009-10-08 · Capillary Accessories ACCESSORIES Universal Guard Column Kits • Universal kits connect to any capillary column • Guard columns are deactivated

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418 419

SWAGELOK® FITTINGS

DESCRIPTION DIMENSIONS QTY BRASS PART NO. PRICE QTYSTAINLESS STEEL

PART NO. PRICE

Nuts1/16" 10 55002 10 551991/8" 10 55003 10 551933/16" 10 55004 10 551941/4" 10 55005 10 55195

Male Nut1/16" ea 55084 ea 55184

Front Ferrules1/16" 10 55006 10 551961/8" 10 55007 10 551973/16" 10 55008 10 551981/4" 10 55013 10 55093

Back Ferrules1/16" 10 55014 10 550941/8" 10 55015 10 550953/16" 10 55016 10 550961/4" 10 55017 10 55097

Union (Low Dead Volume)1/16" ea 55001 ea 55101

Unions1/16" ea 55009 ea 551091/8" ea 55010 ea 551103/16" ea 55011 ea 551141/4" ea 55012 ea 55112

Bulkhead Unions1/16" ea 51017 ea 551171/8" ea 55018 ea 551183/16" ea 55019 ea 551191/4" ea 55020 ea 55120

Reducing Unions1/8" to 1/16" ea 55021 ea 551213/16" to 1/16" ea 55022 ea 551223/16" to 1/8" ea 55023 ea 551231/4" to 1/16" ea 55024 ea 551241/4" to 1/8" ea 55025 ea 551251/4" to 3/16" ea 55026 ea 55126

FittingsA C C E S S O R I E S

SWAGELOK® Tube FittingsSWAGELOK® Tube Fittings provide a leak-proof,

torque-free seal at all tubing connections and eliminate costly, hazardous leaks in instrumentation and process tubing.

All the action in the fitting moves along the tube axially instead of with a rotary motion. Since no torque is transmitted from the fitting to the tubing, there is no initial strain which might weaken the tubing.

CAUTION: Do not mix or interchange parts of tube fittings made by other manufacturers with SWAGELOK® tube fitting parts.

Page 36: Capillary Accessories · 2009-10-08 · Capillary Accessories ACCESSORIES Universal Guard Column Kits • Universal kits connect to any capillary column • Guard columns are deactivated

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420 421

SWAGELOK® FITTINGS (CONT’D)

DESCRIPTION DIMENSIONS QTY BRASS PART NO. PRICE QTYSTAINLESS STEEL

PART NO. PRICE

Female Pipe Thread Connectors (Tube to FPT ) 1/8" to 1/8" FPT ea 55046 ea 551461/8" to 1/4" FPT ea 55047 ea 551473/16" to 1/8" FPT ea 55048 ea 551481/4" to 1/8" FPT ea 55049 ea 551491/4" to 1/4" FPT ea 55050 ea 551501/4" to 3/8" FPT ea 55051 ea 551511/4" to 1/2" FPT ea 55052 ea 55152

Male Pipe Thread Connectors (Tube to MPT) 1/16" to 1/16" MPT ea 55033 ea 551331/16" to 1/8" MPT ea 55034 ea 551341/8" to 1/16" MPT ea 55035 ea 551351/8" to 1/8" MPT ea 55036 ea 551361/8" to 1/4" MPT ea 55037 ea 551371/8" to 3/8" MPT ea 55038 ea 551383/16" to 1/8" MPT ea 55039 ea 551393/16" to 1/4" MPT ea 55040 ea 551401/4" to 1/16" MPT ea 55041 ea 551411/4" to 1/8" MPT ea 55042 ea 551421/4" to 1/4" MPT ea 55043 ea 551431/4" to 3/8" MPT ea 55044 ea 551441/4" to 1/2" MPT ea 55045 ea 55145

Tees1/16" ea 55027 ea 551271/8" ea 55028 ea 551283/16" ea 55029 ea 551291/4" ea 55030 ea 55130

Crosses1/8" ea 55031 ea 55131

1/4" ea 55032 ea 55132

Caps1/16" ea 55085 ea 551851/8" ea 55086 ea 551863/16" ea 55087 ea 551871/4" ea 55088 ea 55188

Plugs1/16" ea 55089 ea 551891/8" ea 55090 ea 551903/16" ea 55091 ea 551911/4" ea 55092 ea 55192

FittingsA C C E S S O R I E S

Need Tubing?See pages 422-424 for a complete selection of stainless steel, metal, and polymeric tubing.

Contact Alltech Tech Support:

Email: [email protected] Online: www.alltechWEB.com

Need Technical Assistance?

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420 421

5078

6693

5077

4855

FittingsA C C E S S O R I E S

PFA Fittings

PFA fittings offer superior chemical resistance. The one-piece ferrule and nut assembly allows for easy tubing connections. Maximum temperature rating is 250°C. Order a grooving tool (to groove tubing) separately below to achieve maximum pressure rating of 125psig.

PFA FITTINGSDESCRIPTION SIZE QTY PART NO. PRICE

Ferrule Nut1/16" 5 457001/8" 5 457011/4" 5 45702

Union 1/16" 2 45715

1/8" 2 457161/4" 2 45717

Reducing Union1/8"-1/16 2 457201/4"-1/8" 2 45721

Tee1/16" ea 457251/8" ea 45726

1/4" ea 45727Grooving Tool

1/8" ea 457461/4" ea 45747

SS Quick-Connects

SS QUICK-CONNECTSDESCRIPTION PART NO. PRICE

1/8" 70921/4" 7093

Brass Quick-Connects

Use Quick-Connects where gas lines are frequently broken and reassembled for convenient handling and to avoid air contamination in the gas line. Both ends of the fitting are completely shut off when the ends are separated and flow is automatically started when recoupled. Fittings are constructed of brass with Buna-N® seals. Maximum coupled pressure is 3000psig.

BRASS QUICK-CONNECTSDESCRIPTION PART NO. PRICE

1/8" 70881/4" 7089

PTFE Tape

Use PTFE tape for a dry thread lubricant and sealant when making pipe thread (NPT) connections. Temperature limit is 200˚C.

PTFE TAPEDESCRIPTION QTY PART NO. PRICE

1/2" x 260"L ea 32261/2" x 260"L 12 Rolls 3227

WRENCH-FREE GC FITTINGSDESCRIPTION PART NO. PRICE

1/4" Wrench-Free Fitting Kit (2 Fittings, 4 Ferrules) 32004Repl. Ferrules, 5/pk 320021/8" Wrench-FreeFitting Kit (2 Fittings, 4 Ferrules) 32006Repl. Ferrules, 5/pk 32008

Wrench-Free GC Fittings• Special reusable ferrules• Star knob grip seals

finger tight

These fittings provide leak-free connections without the use of wrenches.

The easy-grip star knob is designed for use with bulky, heat resistant gloves. A special graphite ferrule with a stainless steel sleeve is provided with the 1/4" kit; a specially designed Vespel®/Graphite ferrule is provided with the 1/8" kit (Both sizes can be used at temperatures up to 400°C.).

These quick connects are 100% helium leak tested for optimum performance. They feature leak-tight Viton® o-ring seals with a temperature range of -29 to 204°C. Simple push-pull action connects and disconnects lines without leakage. Fittings are rated for 3000psig when coupled.

Specialty Fittings

Page 38: Capillary Accessories · 2009-10-08 · Capillary Accessories ACCESSORIES Universal Guard Column Kits • Universal kits connect to any capillary column • Guard columns are deactivated

Contact your Alltech office or distributor for current or local prices.© Copyright 2004 Alltech Associates, Inc. Contact your Alltech office or distributor for current or local prices.© Copyright 2004 Alltech Associates, Inc.

422 423

5105

TubingA C C E S S O R I E S

AT™ Steel - Activity Tested Steel TubingDelivers the Strength of Stainless Steel and the Inertness of Deactivated Fused Silica

• Flexible, and strong • Maximum temperature limit of 340°C to 350°C

A combination of chemical vapor deposition techniques and silicone chemistries transform durable stainless steel tubing into a chromatographically inert material. AT™ Steel activity tested steel tubing is suitable for sample loops, transfer lines, capillary and packed GC columns.

AT™-Steel may be cut with standard tubing cutters or high speed wheel cutters and can be rinsed with common solvents to remove particulates and contamination that have built up during use. To ensure a truly inert pathway, use AT™-Steel treated fittings. Sold separately below.

AT™ STEEL TUBINGI.D. 6FT LENGTH PART NO. PRICE 25FT LENGTH PART NO. PRICE 50FT LENGTH PART NO. PRICE 100FT LENGTH PART NO. PRICE 1/32" o.d. Tubing0.021" 11085 11086 11087 110881/16" o.d. Tubing0.010" 11060 11061 11062 110630.020" 11064 11065 11066 110670.030" 11068 11069 11070 110710.040" 11072 11073 11074 — —1/8" o.d. Tubing0.085" 11076 11077 11078 — —1/4" o.d. Tubing0.210" 11092 11093 — — — —

Choosing a Tubing MaterialA number of options are available for packed column tubing. The most inert material is glass, which should be used for active compounds. Glass-lined tubing and AT-steel™ provide the inert surface of glass combined with the mechanical strength of a metal column. Metal tubing provides an economical and rugged column for suitable application. Passivated nickel tubing can frequently be used with active compounds such as phenols and amines. Stainless steel tubing is recommended for hydrocarbon, fixed gas, and solvent analyses where column inertness is less of a concern. PTFE tubing is extremely inert, but due to temperature limitations and poor column efficiency, PTFE is generally only recommended for the analysis of corrosive gases which are too reactive for glass.

Hi-EFF® Grade Stainless Steel Tubing• Acetone washed to remove residual contaminants

HI-EFF® Stainless Steel tubing meets the exact specification required to fabricate GC columns. Tubing is specially tempered for easy bending. Type 304 is the most commonly used for GC. Type 316 offers more corrosion resistance.

HI-EFF® TUBINGO.D. I.D. PER FT* PART NO. PRICE PER METER PART NO. PRICE 50FT COIL PART NO. PRICE

Type 316 SS1/8” (3.18mm) 0.085" (2.16mm) 30105 30107 301091/4" (6.35mm) 0.210" (5.33mm) 30307 30308 30309Type 304 SS1/8" (3.18mm) 0.085" (2.16mm) 30102 30104 301061/4" (6.35mm) 0.210" (5.33mm) 30302 30304 30306*Minimum tubing order is 3 ft

Stainless Steel Tubing

AT™-STEEL UNIONSDESCRIPTION PART NO. PRICE

1/8" - 1/16 Reducing Union 110801/16" Union 110811/8" Union 11082

AT™-STEEL TEESDESCRIPTION PART NO. PRICE

1/16" Tee 110831/8" Tee 11084

Fittings are Parker A-Lok fittings with two-piece ferrules that have been chemically modified for improved inertness.

Page 39: Capillary Accessories · 2009-10-08 · Capillary Accessories ACCESSORIES Universal Guard Column Kits • Universal kits connect to any capillary column • Guard columns are deactivated

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422 423

5098

50975103

5101 5102

TubingA C C E S S O R I E S

Standard Grade Stainless Steel Tubing• Economical• Same as HI-EFF® without washing

STANDARD STAINLESS STEEL TUBING

O.D. I.D.PER FT* PART NO. PRICE

PER METERPART NO. PRICE

50FT COILPART NO. PRICE

200FT COILPART NO. PRICE

Type 316 SS1/32" (0.79mm) 0.007" (0.18mm) 8195 81953 81951 — —

1/16" (1.59mm)

0.004" (0.10mm) 30211 30213 30212 — —0.007" (0.18mm) 30141 301430 30142 — —0.010" (0.25mm) 30051 300530 3005 300520.020" (0.51mm) 3002100 300230 3002 3002200.030" (0.76mm) 300010 300030 3000 3000200.040" (1.02mm) 30031 30033 3003 — —0.050" (1.27mm) 30041 30043 3004 — —

Type 304 SS1/8" (3.18mm) 0.085" (2.16mm) 30101 30103 3010 301083/16" (4.76mm) 0.147" (3.73mm) 30201 30203 3020 — —1/4" (6.35mm) 0.210" (5.33mm) 30301 30303 3030 — —3/8" (9.53mm) 0.305" (7.75mm) 30321 30323 3032† — —*Minimum tubing order is 3ft †40 ft coil

Straight Stainless Steel Tubing• Type 304 SS• 6ft or 10ft lengths

Glass-Lined Stainless Steel Tubing (GLT)

• Flow lines for corrosives• GC/MS interfaces• Capillary column connections

PTFE-Coated Stainless Steel Tubing• Sturdy SS tube with 0.001" thick PTFE

coating• Must be preconditioned at 250°C for

three hours

PTFE-Lined Stainless Steel Tubing• Ideal for use with reactive chemicals

and for trace quantities of water• Order PTFE ferrules to grip SS and PTFE

portions of tubing below

Stainless Steel Tubing

PTFE-COATED STAINLESS STEEL TUBINGO.D. I.D. LENGTH PART NO. PRICE

1/8" (3.18mm) 0.085"(2.16mm) per ft* 314211/8" (3.18mm) 0.085"(2.16mm) 50 ft 31421/4" (6.35mm) 0.210"(5.33mm) per ft* 314411/4" (6.35mm) 0.210"(5.33mm) 50 ft 3144*Minimum tubing order is 3 ft

PTFE-LINED STAINLESS STEEL TUBINGO.D. I.D. LENGTH QTY PART NO. PRICE

1/8" (3.18mm) 0.070" (1.78mm) 6 ft 1 31521/8" (3.18mm) 0.070" (1.78mm) 10 ft 1 31541/4" (6.35mm) 0.180" (4.57mm) 6 ft 1 31561/4" (6.35mm) 0.180" (4.57mm) 50 ft 1 3158

GLASS-LINED STAINLESS STEEL TUBINGO.D. I.D. LENGTH PART NO. PRICE

1/16" (1.59mm) 0.3mm 180cm 31371/16" (1.59mm) 0.5mm 180cm 31641/16" (1.59mm) 0.7mm 180cm 31391/8" (3.18mm) 0.75mm 180cm 31661/8" (3.18mm) 1.0mm 180cm 31681/8" (3.18mm) 1.5mm 180cm 31701/8" (3.18mm) 1.8mm 180cm 31411/4" (6.35mm) 4.0mm 180cm 3149

STRAIGHT STAINLESS STEEL TUBINGO.D. I.D. LENGTH* QTY PART NO. PRICE

1/8" (3.18mm) 0.085" (2.16mm) 6 ft 10 30106ST1/8" (3.18mm) 0.085" (2.16mm) 10 ft 10 301010ST1/4" (6.35mm) 0.210" (5.33mm) 6 ft 10 30306ST1/4" (6.35mm) 0.210" (5.33mm) 10 ft 10 303010ST*10ft lengths must ship via motor freight

Alltech Can Provide an Acetone Washing ServiceRemove residual contaminants from any tubing surface between 1/8" and 3/8" o.d. and up to 50' coils. Order Part Number C-3001.

PTFE FERRULESO.D. QTY PART NO. PRICE

1/8" 10 65521/4" 10 6554

Page 40: Capillary Accessories · 2009-10-08 · Capillary Accessories ACCESSORIES Universal Guard Column Kits • Universal kits connect to any capillary column • Guard columns are deactivated

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424 425

5104a

PFA FEP PTFE POLYPROPYLENE

5106

5100

TubingA C C E S S O R I E S

Nickel Tubing• Pure Nickel 200, more inert than

stainless steel• Acid washed and rinsed for additional

inertness

COPPER TUBINGO.D. I.D. LENGTH PART NO. PRICE

1/8" (3.18mm) 0.065" (1.65mm) 50ft 30403/16" (4.76mm) 0.128" (3.25mm) 50ft 305091/4" (6.35mm) 0.190" (4.83mm) 50ft 306093/8" (9.53mm) 0.315" (8.00mm) 50ft 30709

Copper Tubing• Economical choice for GC gas lines

Aluminum Tubing• Economical choice for GC gas lines

ALUMINUM TUBINGO.D. I.D. LENGTH PART NO. PRICE

1/8" (3.18mm) 0.065" (1.65mm) 50ft 30903/16" (4.76mm) 0.128" (3.25mm) 50ft 31001/4" (6.35mm) 0.190" (4.83mm) 50ft 31103/8" (9.53mm) 0.315" (8.00mm) 50ft 3120

For PEEK and other HPLC tubing, refer to pages 230-235. For fused silica tubing, see page 386.

Need Fittings?See pages 417-421 for a complete selection of GC fi ttings.

PFA (PERFLUOROALKOXY) TUBINGO.D. I.D. LENGTH PART NO. PRICE

1/16" (1.59mm) 0.030" (0.76mm) 25 ft 457341/8" (3.18mm) 0.062" (1.57mm) 25 ft 457351/4" (6.35mm) 0.156" (3.96mm) 25 ft 45736

FEP (FLUORINATED ETHYLENE POLYPROPYLENE) TUBINGO.D. I.D. LENGTH PART NO. PRICE

1/16" (1.59mm) 0.030" (0.76mm) 25 ft 457391/8" (3.18mm) 0.062" (1.57mm) 25 ft 457401/4" (6.35mm) 0.156" (3.96mm) 25 ft 45741

TFE (TETRAFLUOROETHYLENE) TUBINGO.D. I.D. LENGTH PART NO. PRICE

1/16" (1.59mm) 0.038" (0.96mm) per ft† 313211/16" (1.59mm) 0.038" (0.96mm) per meter† 313231/16" (1.59mm) 0.038" (0.96mm) 50 ft 31321/8" (3.18mm) 0.098" (2.49mm) per ft* 313411/8" (3.18mm) 0.098" (2.49mm) per meter† 313431/8" (3.18mm) 0.098" (2.49mm) 50 ft 31341/4" (6.35mm) 0.125" (3.17mm) per ft* 313611/4" (6.35mm) 0.125" (3.17mm) per meter† 313631/4" (6.35mm) 0.125" (3.17mm) 50 ft 3136*6ft minimum †2m minimum

POLYPROPYLENE/POLYETHYLENE TUBINGO.D. I.D. TYPE LENGTH PART NO. PRICE

1/8" (3.18mm) 0.080" (2.03mm) PP 50 ft 32031/8" (3.18mm) 0.080" (2.03mm) PP 100 ft 32011/4" (6.35mm) 0.125" (3.17mm) PE 50 ft 32071/4" (6.35mm) 0.125" (3.17mm) PE 100 ft 3205

NICKEL TUBINGO.D. I.D. PART NO. PRICE

Per Foot*1/16" (1.59mm) 0.010" (0.25mm) 308311/16" (1.59mm) 0.020" (0.51mm) 313111/16" (1.59mm) 0.040" (1.02mm) 308511/8" (3.18mm) 0.083" (2.11mm) 308011/4" (6.35mm) 0.210" (5.33mm) 30811Per Meter1/16" (1.59mm) 0.010" (0.25mm) 308331/16" (1.59mm) 0.020" (0.51mm) 313131/16" (1.59mm) 0.040" (1.02mm) 308531/8" (3.18mm) 0.083" (2.11mm) 308031/4" (6.35mm) 0.210" (5.33mm) 3081350 Foot Coil1/16" (1.59mm) 0.010" (0.25mm) 30831/16" (1.59mm) 0.020" (0.51mm) 31311/16" (1.59mm) 0.040" (1.02mm) 30851/8" (3.18mm) 0.083" (2.11mm) 30801/4" (6.35mm) 0.210" (5.33mm) 3081200 Foot Coil1/16" (1.59mm) 0.010" (0.25mm) 308321/16" (1.59mm) 0.020" (0.51mm) 31312*Minimum tubing order is 3ft

Metal Tubing Polymeric Tubing

PFA (Perfl uoroalkoxy) Tubing

FEP (Fluorinated Ethylene Polypropylene) Tubing

PTFE (Tetrafl uoroethylene) Tubing

Polypropylene/Polyethylene Tubing

• MaximumInertness

Page 41: Capillary Accessories · 2009-10-08 · Capillary Accessories ACCESSORIES Universal Guard Column Kits • Universal kits connect to any capillary column • Guard columns are deactivated

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424 425

5376

5114

0033

5110

5111

3306

5112

3314

5377

5113

Glass Knife Cutter• Cuts capillary fused silica

and glass tubing of all sizes.• Includes a double edged

tungsten carbide blade.

TubingA C C E S S O R I E S

Plastic Tubing Shear• Cuts all types of plastic tubing• Stainless steel blade makes clean, square cuts• Compact - only 3" Long

Rotary Tubing Cutter• Cuts 1/32" to 1/8" o.d. tubing• Leaves tubing i.d. open• Cuts metal and glass-lined tubing• No deburring or ream ing necessary

Cutting Kit For 1/16" Tubing• Knife fi le and rig for scoring

the tubing to a preset depth • Scoring provides a clean and

even break • Stops are provided for 0.010", 0.020" and

0.030" i.d. tubing

Plier-Type Tubing Cutter• Cuts 1/16" o.d. tubing• Ideal for cutting tubing in tight places

Clean-Cut™ Tubing Cutter• Cuts PTFE, Tefzel®, Polyolefi n, PEEK• Make clean, square cuts without

deforming i.d.s

Imperial Tubing Cutter• Cuts 1/8" to 1-1/8" o.d. tubing• Makes clean, right-angle cuts with no

burring• Includes spare cutting wheel

Heavy-Duty Tubing Cutter• Cuts stainless steel, copper,

nickel, and aluminum tubing • Cuts 1/8" to 1-1/8" o.d.

tubing

Imp Tubing Cutter• Cuts SS, copper, nickel, & aluminum tubing• Ideal for tight spaces• Requires only 1-3/4" swing radius

Glass Tubing Cutter• Makes glass cutting a snap• More accurate than a fi le

Tubing Cutters

PLASTIC TUBING SHEARDESCRIPTION QTY PART NO. PRICE

Plastic Tubing Shear ea 3206Replacement Blade ea 3214

CLEAN-CUT™ TUBING CUTTERDESCRIPTION QTY PART NO. PRICE

Clean-Cut™ Tubing Cutter ea 35902Replacement Blade ea 35903

PLIER-TYPE TUBING CUTTERDESCRIPTION QTY PART NO. PRICE

Plier-Type Tubing Cutter ea 3169

CUTTING KIT FOR 1/16" TUBINGDESCRIPTION QTY PART NO. PRICE

Cutting Kit ea 7180Replacement Knife File ea 7181

GLASS TUBING CUTTERDESCRIPTION QTY PART NO. PRICE

Glass Tubing Cutter ea 3150Replacement Cutting Wheels 3 3150CW

ROTARY TUBING CUTTERDESCRIPTION QTY PART NO. PRICE

Rotary Tubing Cutter ea 3165Replacement Cutting Wheels 3 3167

IMP TUBING CUTTERDESCRIPTION QTY PART NO. PRICE

Imp Tubing Cutter ea 3208Replacement Cutting Wheels 5 320210

IMPERIAL TUBING CUTTERDESCRIPTION QTY PART NO. PRICE

Imperial Tubing Cutter ea 3210Replacement Cutting Wheels 2 3212Heavy-Duty Cutting Wheels 3 13984

HEAVY-DUTY TUBING CUTTERDESCRIPTION QTY PART NO. PRICE

Heavy-Duty Tubing Cutter ea 13995Replacement Cutting Wheels 3 13981

GLASS KNIFE CUTTERDESCRIPTION QTY PART NO. PRICE

Glass Knife Cutter ea 5600Replacement Blade ea 5601

Page 42: Capillary Accessories · 2009-10-08 · Capillary Accessories ACCESSORIES Universal Guard Column Kits • Universal kits connect to any capillary column • Guard columns are deactivated

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426 427

6281

5116

5115

5118

5117

4502

6258 6259

4394

TubingA C C E S S O R I E S

SGT Shortix™ Capillary Column Cutter

• Makes perfect fused silica cuts• Rotating diamond blade precisely

scores capillary columns• Edges are clean & straight, column

walls are undamaged• Cuts 100-500µm i.d. capillaries

Fused Silica Cutter• Cleanly cut fused silica tubing• Small enough to keep handy in

your pocket

Capillary Scribers• Make clean scratches and breaks of fused silica

capillary tubing• Tungsten carbide tipped marks steel, stainless steel,

and ceramics• Diamond-tipped marks any surface - even glass

Electric Tubing CutterAssure zero dead volume connections

• Clamp vise securely holds tubing in place

• Cut 1/16", 1/8" and 1/4" o.d. tubings with i.d.’s as small as 0.008"

• Requires no lubricant or cutting fluid

This electric tubing cutter assures square and burr-free cuts for maximum chromatographic performance. Use the included dressing tool for 1/16" o.d. tubing to finish the inside and outside diameters of tubing ends. Dressing tool for 1/8" and 1/4" o.d. tubing and replacement cutting wheels can be ordered separately below. Tubing cutter is voltage selectable for 110-120/220-240 VAC, 50/60 Hz.

Tubing Reamers• Smooth and debur metal tubing ends• 1/16" reamer set includes inner & outer reamers• Inner reamers handles most tubing i.d.s

Inner Reamer

Outer ReamerHeavy-Duty Tube Benders

• Bend heavy-walled tubing with ease

Compact Tube Bender• Bends 1/8", 3/16", 1/4", 3-, 4-,

5-, and 6mm tubing• Easily bends copper,

aluminum, and thin walled steel tubing

ELECTRIC TUBING CUTTERDESCRIPTION QTY PART NO. PRICE

Electric Tubing Cutter ea 10-0200Replacement Part and AccessoriesDressing tool for 1/8" and 1/4" o.d. Tubing ea 13984Replacement cutting wheels 3 10-0124Repl. dressing tool for 1/16" o.d. tubing ea 10-0116

FUSED SILICA CUTTERDESCRIPTION QTY PART NO. PRICE

Fused Silica Cutter 5 3194

TUBING REAMERSDESCRIPTION QTY PART NO. PRICE

1/16" Reamer Set ea 139741/8" Outer Reamer ea 321991/4" Outer Remer ea 32219Inner Reamer for 1/8"-3/8" o.d. ea 32159

CAPILLARY SCRIBERSDESCRIPTION QTY PART NO. PRICE

Tungsten Carbide Scriber ea 3155Diamond-tipped Scriber ea 3159

Diamond-Tipped Scriber Tungsten Carbide Scriber

CAPILLARY COLUMN CUTTERDESCRIPTION QTY PART NO. PRICE

Shortix™ Column Cutter ea 5190Replacement Blade ea 5192

COMPACT TUBE BENDERDESCRIPTION QTY PART NO. PRICE

Compact Tube Bender ea 3232

HEAVY-DUTY TUBE BENDERDESCRIPTION QTY PART NO. PRICE

For 1/8" Tubing ea 3220For 1/4" Tubing ea 3224

Tubing Cutters & Accessories

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426 427

*Also compatible with Varian Model CP-1177 Split/Splitless Injector Port

Injection LinersA C C E S S O R I E S

Deactivated Injection LinersDEACTIVATED INJECTION LINERS

DESCRIPTION AND LENGTH X O.D. DIAGRAMEACH

PART NO. PRICE5/PK

PART NO. PRICE25/PK

PART NO. PRICE

Injection Liners for Agilent/Hewlett-Packard Instruments*Cup Splitter 78.5 x 6.3mm

4825 4827 4829

Split/Splitless with Deactivated Quartz Wool, 78.5 x 6.3mm o.d., 4mm i.d.

4906 4924 4928

Splitless, 78.5 x 6.3mm o.d., 4mm i.d.

4929 4934 4936

Quartz Splitless, 78.5 x 6.0mm, 2mm i.d.

4962 4963 4964

Recessed Gooseneck with Deactivated Quartz Wool, 78.5 x 6.3mm, 4mm i.d.

4959 4960 4961

Recessed Gooseneck, 78.5 x 6.3mm, 2mm i.d.

4958 4938 4957

Direct, 78.5 x 6.3mm, 1.5mm i.d.

4967 4968 4969

Injection Liners for Varian InstrumentsSplitter with Deactivated Quartz Wool, 1075/1077, 72 x 6.3mm, 4mm i.d.

4970 4971 4972

Frit Splitter, 1075/1077, 72 x 6.3mm, 4mm i.d.

4973 4974 4975

Baffl e Splitter, 1075/1077, 72 x 6.3mm, 4mm i.d.

4977 4978 4979

Splitless 1075/1077, 74 x 6.3mm, 2mm i.d.

4980 4981 4982

0.8mm SPI 1093/1094, 54 x 4.6mm

4983 4984 4985

0.5mm SPI 1093/1094, 54 x 4.6mm

4986 4987 4988

SPI with Buffer 1093/1094, 54 x 4.6mm

4989 4990 4991

Injection Liners for Perkin-Elmer InstrumentsSplit/Splitless 8500, 8600, 100 x 5.0mm, 3mm i.d.

4790 4792 4794

Splitless 8500, 8600, 100 x 5.0mm, 2mm i.d.

4992 4993 4994

PTV Liner 8500, 8600, 88 x 2.0mm, 1mm i.d.

4995 4996 4997

Split/Splitless Autosystem, 92 x 5.8mm, 4mm i.d.

4796 4798 4800

Split/Splitless Autosystem, 92 x 5.8mm, 2mm i.d.

4810 4812 4814

Injection Liners for Shimadzu InstrumentsSplit 17A with Deactivated Quartz Wool, 95.5 x 5.0mm, 3mm i.d.

4748 4750 4752

Splitless 17A, 95.5 x 5.0mm, 3mm i.d.

4754 4756 4758

Gooseneck/Splitless, 95.5 x 5.0mm, 3mm i.d.

4760 4762 4764

Split 9A, 15A, 16A, 127.5 x 5.0mm, 3mm i.d.

4766 4768 4770

Splitless 9A, 15A, 16A, 127.5 x 5.0mm, 3mm i.d.

4772 4774 4776

Injection Liners for Finnigan InstrumentsSplitless 5100 Series, 85 x 6.3mm, 2mm i.d.

4856 4857 4858

Splitless 4100 Series, 112 x 4.5mm, 2mm i.d.

4859 4860 4862

25/PK

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428 429

DEACTIVATED SGE FOCUSLINERS

DESCRIPTION AND LENGTH X O.D. DIAGRAM5/PK

PART NO. PRICE25/PK

PART NO. PRICE

for Agilent/Hewlett Packard Instruments*FocusLiner, 78.5 x 6.3 x 4mm i.d. 85474 85480

Tapered FocusLiner, 78.5 x 6.3 x 4mm i.d. 85481 85574

FAST FocusLiner, 78.5 x 6.3 x 2.3mm i.d. 85605 85606

Tapered FAST FocusLiner, 78.5 x 6.3 x 2.3mm i.d.

85607 — —

for Varian Injector Models 1075/1077FocusLiner, 72 x 6.3 x 4mm i.d. 85477 — —

Tapered FocusLiner, 74 x 6.3 x 4mm i.d. 85484 — —

FocusLiner w/Top Restriction, 72 x 6.3 x 4mm i.d.

85633 — —

FAST FocusLiner, 72 x 6.3 x 2.3mm i.d. 85634 — —

for Varian Injector Models 1078/1079FocusLiner, 54 x 5 x 3.4mm i.d. 85437 — —

Tapered FocusLiner, 54 x 5 x 3.4mm i.d. 85635 — —

for Shimadzu 17AFocusLiner, 95 x 5 x 3.4mm i.d. 85476 — —

Tapered FocusLiner, 95 x 5 x 3.4mm i.d. 85483 — —

for Shimadzu 14/15A/16FocusLiner, 99 x 5 x 3.4mm i.d. 85608 — —

Tapered FocusLiner, 99 x 5 x 3.4mm i.d. 85630 — —

for Perkin Elmer AutosystemFocusLiner, 92 x 6.2 x 4mm i.d. 85478 — —

Tapered FocusLiner, 92 x 6.2 x 4mm i.d. 85482 — —

for ThermoQuest Model 8000/TRACEFocusLiner, 105 x 8 x 5mm i.d. 85631 — —

Tapered FocusLiner, 105 x 8 x 5mm i.d. 85632 — —

* Also compatible with Varian model CP-1177 Split/Splitless injection port.

Injection LinersA C C E S S O R I E S

DEACTIVATED INJECTION LINERS (CONT’D)

DESCRIPTION AND LENGTH X O.D. DIAGRAMEACH

PART NO. PRICE5/PK

PART NO. PRICE25/PK

PART NO. PRICE

Injection Liners for Carlo Erba-Fisons InstrumentsSplit/Splitless 6000 Series with Deactivated Quartz Wool, 79.5 x 5.0mm, 3mm i.d.

4742 4744 4746

Splitless 6000 Series, 79.5 x 5.0mm, 4mm i.d.

4853 4854 4855

Splitless 6000 Series, 79.5 x 5.0mm, 2mm i.d.

4998 4851 4852

Split 8000 Series, 105 x 8.0mm, 3mm i.d. 4784 4786 4788

Deactivated SGE FocusLiners

25/PK

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428 429

6651

6650

Injector AccessoriesA C C E S S O R I E S

GC O-rings• Thermally Stable• No Bleed• Suitable for GC/MS

Graphite O-rings may replace the Viton® or silicone O-rings normally used to seal the Agilent 5890 Split and Splitless injection liners. Splitless liners have an internal diameter of 6.5mm and split liners have an internal diameter of 6.35mm.

SpecificationsPROPERTY GRAPHITE SILICONE PTFE VITON®

Max. Temp. 450°C 230°C 230°C 200°CChem. Rest. Good Good Superb SuperbDurability Superb Moderate Superb GoodBleed None Medium Low LowColor Black Red White Black

O-RINGSSIZE QTY. PART NO. PRICE

Graphite GC O-rings (450°C Limit)1/4" (6.5mm i.d.) 10 71601/4" (6.35mm i.d.) 10 7176Silicone O-rings (230°C Limit)1/8" 100 70203/16" 100 70211/4" 100 7022PTFE O-rings (230°C Limit)1/8" 100 70233/16" 100 70241/4" 100 7025Viton® O-rings (200°C Limit)1/8" 100 70173/16" 100 70181/4" 100 7019Graphite Washer (450°C Limit)1/4" i.d. x 7/16" o.d., 1/32" Thick 10 7165

Injector Supplies for HP/Agilent 5890/6890 GCs

Inlet Seals for HP/Agilent 5890/6890 GCs are available either stainless steel (similar to HP/Agilent part no. 18740-20880) or gold plated (similar to HP/Agilent part no. 18740-20885). Washers are included with the inlet seals.

The Reducing Nut for HP/Agilent 5890/6890 GCs is made from stainless steel and is similar to HP/Agilent part no. 18740-20800.

INJECTOR SUPPLIES FOR HP/AGILENT 5890/6890 GCSDESCRIPTION QTY PART NO. PRICE

Inlet Seal, stainless steel (0.8mm hole)1 1514610 15146125 151462

Inlet Seal, gold plated (0.8mm hole)1 1514710 15147125 151472

Reducing Nut Replacement for HP 5890/6890

1 15145

Washers, stainless steel (0.375"o.d.) 10 15148MSD Source Nut, brass 1 15104

Accessories for HP/Agilent & Varian Capillary Systems

HP/Agilent nuts are available in both standard and “deep well” versions, with either standard wrench flats or knurled for easy wrench-free fingertight connections. The deep well nuts have 2.4mm deep ferrule wells to accommodate standard capillary ferrules, and the standard type has a 1.65mm deep ferrule well for HP-type capillary ferrules.

ACCESSORIES FOR HP/AGILENT AND VARIANDESCRIPTION QTY PART NO. PRICE

Capillary NutsCapillary Nuts for Varian 2 154740Capillary Nuts for HP/Agilent 2 154780Wrench-Free Capillary Nuts for HP/Agilent 2 154785Deep Well Capillary Nuts for HP/Agilent 2 154781Wrench-Free Deep Well for HP/Agilent 2 154782Graphite Ferrules for HP/AgilentGraphite Ferrules, 0.5mm Hole* 10 1547901Graphite Ferrules, 1.0mm Hole** 10 1548001Wrench5/16" x 1/4" Open-End Wrench ea 1998

* for 0.25 and 0.32mm i.d. Capillary Column. ** for 0.45 and 0.53mm i.d. Capillary Column.

Don't Forget Septa!See pages 431-433 for a complete selection of septa.

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58283967

KitsA C C E S S O R I E S

Alltech Maintenance Kit for HP/Agilent GC’s

• Easily maintain the injector and FID• For use with HP/Agilent 5890 and 6890 GC’s

Your results rely on the performance of your GC. The Maintenance Kit for HP/Agilent GC’s contains all the supplies you need to perform routine maintenance and trouble-shooting on your injector and FID.

Kit Includes:For Column Installation

• 2 - HP style capillary nuts • 10 - 0.5mm HP style graphite ferrules • 10 - 1.0mm HP style graphite ferrules

For Injector Maintenance & Troubleshooting• 5 - split/splitless liner with deactivated quartz wool,

4mm i.d.• 5 - splitless liner, 4mm i.d. • 100 - 1/4" Viton o-rings • 10 -1/4" graphite ferrules • 25 - 9.5mm ThermoRed septa • 2 - 0.8mm stainless steel inlet seals

For Detector Maintenance & Troubleshooting• 40 - 1' lengths redi cut wire (10 each 0.003", 0.005",

0.010", & 0.020" o.d.)• 4 - stainless steel tube brushes

ALLTECH’S MAINTENANCE KIT FOR HP/AGILENT GC’SDESCRIPTION PART NO. PRICE

Alltech Answer Maintenance Kit 20814

For other Alltech Kits, including the EPA Method 552.1 for Haloacetic Acids in Water Kit, and the USP Method 467 Kits, request data sheet 20830.

Alltech GC Start-Up Kit

• Convenient• Suitable for use with any capillary GC

Kit contains the necessary tools to set up and operate your GC. Alltech’s GC Start Up Kit includes all the supplies you need to install columns, set gas fl ows, set linear velocity, and perform routine maintenance on your GC.

Kit includes:For General Maintenance

• 4 - open-end wrenches (2 each, 7/16" x 1/2" & 9/16" x 5/8")

• 1 - 2-way reversible screwdriver• 25 - 9.5mm and 11mm ThermoRed septa• 1 - septa puller • 4 - stainless steel tube brushes • 40 - 1' lengths redi-cut wire

(10 of each diameter - 0.003", 0.005", 0.010" & 0.020" o.d.)

• 8oz. - leak-check soapfi lm solutionFor Column Installation

• 2 - open-end wrenches (1/4" x 5/16")• 1 - scriber for cutting fused silica tubing• 1 pair - PTFE coated forceps• 1 - Pick (for removing ferrules from fi ttings)• 1 - laminated ruler • 10' length - high temperature string • 1 - 20X magnifi er (for checking ends of tubing)• 2' length - pipecleaner (for cleaning liners)• 10 - 1/16" to 0.4mm, 0.5mm, and 0.8mm graphite

ferrulesFor Setting Gas Flows

• 1 - 100cc soapfi lm fl ow meter• 10' length - 5/16" Tygon™ tubing• 1 - stopwatch

For Setting Linear Velocity• 1- Hamilton 1701 and 701 Gastight Syringe with

Removable needle and 3 replacement needles • 1 - 14L Scotty II 99.99% methane standard• 1 - Scotty II syringe adapter

ALLTECH’S GC START UP KITDESCRIPTION PART NO. PRICE

Alltech Answer GC Start Up Kit 20810

Contact Alltech Customer Service:

Online Ordering 24 hours a day: www.alltechWEB.comEmail: [email protected]

Have a Question about Your Order?

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430 431

4610

SeptaA C C E S S O R I E S

Septa Selection GuidePRODUCT MAX. TEMP. COLOR DUROMETER* LOW BLEED

Thermo Red 300°C Red 50-55 ExcellentXLB 350°C Green 50-55 ExcellentHT-X High Performance 350°C Blue 50-60 Excellent

General Purpose White 250°C White 40-45 Very Good

Standard Blue 300°C Blue 55-60 Very GoodGeneral Purpose Blue 250°C Blue 40-45 Good

Cylindrical Half Hole 250°C Blue 50-55 Very Good

Cylindrical 3-layer 200°C Red 50-55 Excellent

Three Layer 300°C Red/White 50-55 Good

Four Layer 225°C Red/White 50-55 Good

MicrosepPTFE-lined 250°C Off

White 25-35 Good

Microsep Low bleed PTFE-lined 250°C

Yellow/Off

White25-35 Very Good

* Durometer - Harness of the silicone material. The lower the number, the softer the material.

SpecificationsACTUAL SIZE DRAWING MEASUREMENT CHROMATOGRAPH

1/4"(6mm) Shimadzu*, SRI*

3/8" (9.5mm)

Antek, Finnigan 9100, 9600, Gow-Mac, Agilent 5700, 5880 & 5900, IBM, Packard 427-433, Pye-Unicam (early models), Varian (except capillary inj.), Tracor 550, 560.

7/16" (11mm)

Carle, Agilent 5890,6850,6890. P-E Sigma, 900, 990, 3920, 8300, 8400, 8500 Autosys, Varian (capillary injector), SPI, Varian 1078/1079

1/2" (12.5mm)

Fisons/Carlo Erba, Finnigan 9500, HP/Agilent 5750 and earlier models, Packard 409-421, Tracor 220, 222, 540.

21/32" (17mm)

Fisons/Carlo Erba 8000 Series, CE TRACE GC

* Use cylindrical plug septa, see page 432.

With so many septa to choose from, choosing a septum for your application can be a confusing task. There are a number of criteria you need to consider when selecting a septum.

1. Make and Model of Gas Chromatograph – This will determine what size of septum you need. Alltech carries a full range of septum sizes to fit most gas chromatographs.

2. Performance – A high performance, low bleed septum is desirable so that septa bleed does not interfere with the chromatography of your sample. Keep in mind that all septa bleed to some extent. The amount of bleed visible to the detector is affected by several factors which include:

- The composition and pretreatment of the septum material.

- The sensitivity setting of the detector amplifier.

- The type of detector. - The injection port setting. - Isothermal or temperature programming. - The type of injection (direct, splitless,

split, etc.)

Choose a high performance septum such as Alltech’s ThermoRed or XLB septa to minimize septa bleed.

3. Injection Port Temperature - The temperature of the septum never reaches the injection port temperature setting. The center of the injector heated zone, where the sample is deposited, is regulated to correspond to the injector port setting. Be sure to select a septum with a maximum temperature that exceeds your injection port temperature.

4. Penetration/Resealing Qualities - Ideally, you want a septum that is soft and easily penetrated by a syringe needle and has excellent resealing properties. This will prevent you from bending syringe needles and coring of the septum to give you longer septum life. Excellent resealing properties will prevent leaks that might adversely affect your chromatography or damage your analytical column.

How to select a septum for your application

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4604

4607

4597

4608

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SeptaA C C E S S O R I E S

General Purpose Blue Septa• Maximum temperature of 250°C (300°C for short periods)• Lifetime of up to 150 injections• Suitable for most GC analysis

XLB Septa• Maximum temperature to 350°C• Extremely low bleed• Superior resealing properties• Soft, easily penetrated by syringe needle

XLB SEPTASIZE (O.D.) QTY PART NO. PRICE 1/4" (6mm) 50 154273/8" (9.5mm) 50 154287/16" (11mm) 50 154291/2" (12.5mm) 50 1543021/32" (17mm) 50 15039

General Purpose White Septa• Maximum temperature of 250°C• Lifetime of over 100 injections• Designed for use in 90% of all GC analysis

HT-X High Performance Septa• Maximum temperature of 350°C• Long injection life - over 200 injections

CYLINDRICAL SEPTASIZE (O.D.) QTY PART NO. PRICE Cylindrical Half-Hole Septa1/4" (6mm) 25 65241/4" (6mm) 4 x 25 65263 Layer 1/4" (6mm) 50 9602Cylindrical Plug Septa for Shimadzu and SRI

50 15498

Cylindrical Septa• 8mm Long x 6mm o.d.

with half-hole

The standard half-hole septa is red silicone with an upper temperature limit of 225°C. 3-layer septa features the shielding and reinforcing properties of PTFE. The plug septa are low bleed, have an upper temperature limit of 350°C, and are compatible with Shimadzu and SRI.

ThermoRed Septa• Maximum temperature of 300°C• Packed in glass jars under strict QC

standards to protect from contaminants

THERMORED SEPTASIZE (O.D.) QTY PART NO. PRICE 11/32'' (9mm) 25 151293/8'' (9.5mm) 25 151317/16'' (11mm) 25 151321/2" (12.5mm) 25 1514121/32'' (17mm) 25 15133Plug Type (For Shimadzu & SRI) 25 15134

Standard Blue Septa• Maximum temperature of 300°C• Lifetime of over 50 injections

GENERAL PURPOSE BLUE SEPTASIZE (O.D.) QTY PART NO. PRICE

1/4" (6mm) 100 65121/4" (6mm) 10 x 100 651223/8" (9.5mm) 100 65143/8" (9.5mm) 10 x 100 651427/16" (11mm) 100 6518 7/16" (11mm) 10 x 100 651821/2" (12.5mm) 100 65201/2" (12.5mm) 10 x 100 6520212" x 12" Sheet ea 6528

GENERAL PURPOSE WHITE SEPTASIZE (O.D.) QTY PART NO. PRICE 3/8" (9.5mm) 50 78123/8" (9.5mm) 2 x 50 781017/16" (11mm) 50 78137/16" (11mm) 2 x 50 781111/2" (12.5mm) 50 78161/2" (12.5mm) 2 x 50 78141

STANDARD BLUE SEPTASIZE (O.D.) QTY PART NO. PRICE 3/8" (9.5mm) 100 78247/16" (11mm) 100 78261/2" (12.5mm) 100 7830

HT-X HIGH PERFORMANCE SEPTASIZE (O.D.) QTY PART NO. PRICE 1/4" (6mm) 50 154905/16" (8mm) 50 154913/8" (9.5mm) 50 154927/16" (11mm) 50 1549321/32" (17mm) 50 1549411/2" (12.5mm) 50 1549412" x 12" Sheet ea 15496Plug Type (For Shimadzu & SRI) 50 15498

Septa

Half-Hole Septa Shown Here

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433433

4595 4594

4596

4593

4591

SeptaThree- and Four-Layer Septa

• Excellent sealing characteristics• Maximum temperature of 300ºC (3-layer) and 225ºC

(4-layer)

The Three-Layer Septa consists of a layer of red silicone rubber, a layer of translucent soft silicone rubber and another layer of red silicone rubber. The Four-Layer Septa is the same but with a 10-mil (0.010") PTFE facing.

3-Layer Septa 4-Layer Septa

Hamilton Three-Layer Septa• Maximum temperature of 200ºC

These septa feature a center layer of soft silicone rubber for good resealing and two harder rubber outer layers for long life. The soft inner layer clings to the syringe needle and returns quickly to its original shape when the needle is withdrawn to prevent “blow back”.

Microsep® PTFE-Lined Septa• Maximum temperature of 250ºC• Off-white silicone rubber with an ivory PTFE backing

Microsep® Low-Bleed PTFE-Lined Septa• Maximum temperature of 250ºC• Off-white silicone septa with yellow PTFE backing

G C A C C E S S O R I E S

Septa

THREE- AND FOUR-LAYER SEPTASIZE (O.D.) QTY. PART NO. PRICE Three-Layer Septa3/8" (9.5mm) 100 78367/16" (11mm) 100 78381/2" (12.5mm) 100 7840Four-Layer Septa3/8" (9.5mm) 100 78447/16" (11mm) 100 78461/2" (12.5mm) 100 7848

HAMILTON THREE-LAYER SEPTASIZE (O.D.) QTY. PART NO. PRICE

0.197" (5mm) 12 760220.250" (6.35mm) 12 760010.281" (7mm) 12 760100.312" (8mm) 12 760020.355" (9.0mm) 12 760030.375" (9.5mm) 12 760040.394" (10.0mm) 12 760050.438" (11mm) 12 760070.469" (12mm) 12 760130.500" (12.7mm) 12 760060.594" (15mm) 12 760160.750" (19.0mm) 12 76020

MICROSEP® PTFE-LINED SEPTASIZE (O.D.) QTY. PART NO. PRICE 0.250" (6mm) 12 758010.250" (6mm) 100 793910.281" (7mm) 12 758100.355" (9mm) 12 758030.375" (9.5mm) 12 758040.375" (9.5mm) 100 794110.394" (10mm) 12 758050.394" (10mm) 100 794510.438" (11mm) 12 758070.438" (11mm) 100 794710.469" (12mm) 12 758130.500" (12.5mm) 12 758060.500" (12.5mm) 100 79491

MICROSEP® LOW-BLEED PTFE-LINED SEPTASIZE (O.D.) QTY. PART NO. PRICE

3/8" (9.5mm) 50 78023/8" (9.5mm) 2 x 50 780013/8" (9.5mm) 20 x 50 780027/16" (11mm) 50 78037/16" (11mm) 2 x 50 780117/16" (11mm) 20 x 50 780121/2" (12.5mm) 50 78061/2" (12.5mm) 2 x 50 780411/2" (12.5mm) 20 x 50 78042

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434434 435435

2808 2809

The JADE™ Mechanical Inlet works like a miniature airlock. First, the syringe needle passes through a needle guide forming an annular seal. Next, the needle guide encounters the ball-and-seat valve, unseats the ball, and enters the injection port. When the needle is removed from the ball valve, a powerful return magnet pulls the ball back onto the seat, sealing the injection port.

The elegantly simple ball-and-seat is the system’s most technologically complex component. For the utmost in reliability, it uses sophisticated materials and close tolerances found in the most advanced instrumentation.

The JADE™ Inlet’s long lifetime, heat resistance, and low-maintenance design make it the obvious solution for autosampling. After the JADE™ Inlet is installed, there’s minimal need for operator attention, enabling chromatographers to focus on more important tasks instead of monitoring septum failure.

Ultimately, the JADE™ Inlet serves as a vital link in implementing online GC applications where system longevity, reliability, and low maintenance are absolute requirements.

JADE™ Mechanical Inlet Injection Kits

• Models available to accommodate 39 different inlets from 16 different manufacturers

• No need to modify your existing GC• Temperature limit up to 400°C set point (with Hi-

Temp Needle Guide)• Cost effective and reliable

JADE™ MECHANICAL INLET INJECTION KITS0.47MMPART NO.

0.63MMPART NO. PRICE

HP/Agilent5830/5840 9774 97885880/5890/6890 Split/Splitless 9764 97785880/5890/6890 Packed 9762 97765710/5790 Packed 9774 97885700 Capillary 9764 97785993 GC/MS 9764 97785890 Purged/Packed 9909 9683Cool/On-Column (0.53mm i.d.) 9755 —HP/Agilent Autosamplers*7673A&B Split/Splitless — 99257673A&B Packed — 99277673A&B Purged/Packed — 9198Carlo-Erba (Except TRACE 2000) 9750 9752Chrompack 9774 9788Dani (All Models) 9754 9756Dionex (602D) 8850 8852Finnigan (9610/9611 Series) 9751 9753Fisons (Series 8000) 9033 9178Gow-Mac (All Models) 9774 9788 HNU Systems (3000 Series) 9774 9788Konik (HRGC 3000C) 9774 9788Perkin Elmer*2000/8300/8700/8500 Sigma Series 9774 9788Shimadzu8/9/14A and 15A Packed 9738 973214A and 15A Split/Splitless 9736 973017A Split/Splitless 7268 8014SiemensTemp. Programmed Injector 9735 9737SRI (Split & Packed) 8858 8860Tracor/Tremetrics540/570 Series 9739 9747560/565 Series 8950 89849000 Series 9959 9962ThermoQuest Trace GC 7258 7260GCQ 7189 7196Varian**1040 Packed 9748 97341075/1077/1078/1079 Split/Splitless 9768 97861075/1077/1078/1079 Split/Splitlesswith Trigger

9193 9195

1085 9197 91991093/1094 SPI Injector with Trigger 9689 96991400/2400/2700 Series 9921 99233400/3700 Capillary, 1cm Septum 9768 97863400/3700 Capillary, 8mm Septum 9748 97343300 Capillary 9768 9786Universal7/16" x 20 Swagelok® Thread 9774 9788Econo Kit† — 97505

* JADE™ Inlet is incompatible with HP 6890 autosamplers and Perkin Elmer autosampler.**JADE™ Inlets are compatible with Varian Star autosamplers, but may be incompatible with other Varian models. † Includes inlet body, green cap and 0.63mm needle guide. Adapter nut not included.

G C A C C E S S O R I E S

Septa

JADE™ Inlets are also available for SPME. Request datasheet 9778.

Each JADE™ Inlet Kit Includes:- JADE™ Inlet Injector (complete with needle guide)

- Adapter for GC inlet with gasket(s)

- Extra needle guide

- Spare gasket for adapter

- Two 10µL syringes for sample injection

- “BAKE-OUT” plug for cleaning inlet before installation

- Complete instructions

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434434 435435

2208

2210

2209

2211

4907

6252

*Note: The instructions are for installation on a Agilent/Hewlett-Packard injection port. Installation may vary slightly for other instruments.

Ball seat

No-bleed high temperature gasket seals off GC port

Durable hard anodized finish

US. Patent #5,062,310

High precision balls provide perfect sealing

Ball magnet return

Installing a JADE™ Inlet*

After removal of the septum nut and septum, clean out old septum particles. A polyimide gasket (included) is placed in the septum well.

A one-time bake-out step is recommended to remove residual septum materials from the injection port. The brass bake-out plug (included) is installed on the adapter nut for this step. The bake-out plug is removed when done.

The adapter nut is threaded on to the injection port finger tight.

The JADE™ Inlet body is threaded into the adapter nut finger tight. With the appropriate wrench in place on the adapter nut, tighten the valve body 1/4 to 1/2 turn using a 1/2" wrench. The completely assembled JADE™ Inlet is now ready for worry-free operation.

1 2

3 4

Precision-made, tapered needle guide

The JADE™ Mechanical Inlet

REPLACEMENT JADE™ INLET GASKETSDESCRIPTION QTY. PART NO. PRICE

HP/AgilentCool/On-Column 2 96885830/5840/5880/5890/6890 2 9763HP/Agilent Autosamplers5880/5890 and 7673A&B Capillary 2 97595880/5890 and 7673A&B Packed 2 9761Carlo Erba 2 9666Dani 2 9684Finnigan 9610/9611 2 9686Fisons 8000 2 7911Gow Mac 2 9763Packard 2 9763Perkin Elmer 2000/8300/8500/8700 2 9763Shimadzu (all) 2 9789SiemensCapillary 2 7989TP 2 7991ThermoQuestTrace GC 2 7266GCQ 2 7236Tracor540/570 2 7992560/565 2 72649000 2 7993Varian1075/1077/1078/1079 2 97951040/3400/3700 2 97961093/1094 2 79941400/2400/2700 2 7996Universal 2 9763

SYRINGES FOR JADE™ INLETS

VOLUMENEEDLE TYPE

NEEDLE O.D.

HAMILTON PART NO. PRICE

SGE PART NO. PRICE

Manual Injection Syringes0.5µL RN 0.63mm 86240 — —1.0µL RN 0.63mm 801400 853721.0µL RN 0.47mm 80141 — —10µL Fixed 0.63mm 80343 994210µL Fixed 0.47mm 80344 85374

Autosampler Syringes HP76732.5µL Fixed 0.63mm — — 96585.0µL Fixed 0.63mm 87948 853765.0µL Fixed 0.47mm — — 850755.0µL Fixed 0.63mm — — 853765.0µL Fixed 0.47mm — — 85075

REPLACEMENT JADE™ INLET NEEDLE GUIDES

DESCRIPTION0.47MM PART NO.

0.63MM PART NO. PRICE

Standard, Up to 350°C 9790 9794Hi-Temp, 250°C - 400°C 9792 9797

G C A C C E S S O R I E S

Septa

Replacement Parts

Syringes for JADE™ Inlets

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436436 437437

4585

4583

4582

5070

4588

4584

Septa AccessoriesMerlin Microseal™ Septum

• Lasts for thousands of injections

• No instrument modification needed

• Installation as easy as changing a standard septum

• High pressure model allows operation up to 100psig

The Merlin Microseal™ Septum is a long-life replacement for the septum and septum nut on the capillary inlet system of an Agilent GC. It incorporates two sequential seals to provide a much longer period of use between seal changes. Use the Merlin Microseal™ with the HP 7673 Autosampler to allow many more samples to be run unattended while reducing the risk of lost or compromised data caused by septum leaks or fragmentation. It also allows for easier manual injections.

The Microseal™ Septum lasts longest when a syringe needle with a truncated cone shaped tip is used. It may also be used with the standard 0.63mm diameter (0.026", 23-gauge) needle recommended for use with the HP 7673 Autosampler.

MERLIN MICROSEAL™ SEPTUM*DESCRIPTION PART NO. PRICE

Microseal™ Septum KitsFor HP/Agilent GCsMicroseal™ Nut and 2 Septa 80060Microseal™ Nut and 1 Septum 80062

Microseal™ High Pressure Septum KitsStandard Kit, Nut and 2 Septa 80190Starter Kit, Nut and 1 Septum 80192For Varian 1078 & 1079 GCs with SPME InjectorVarian Kit, Nut with start switch, 1 septum and o-ring

80031

Replacement PartsFor HP/Agilent GCsMicroseal™ Septum, ea 80063Microseal™ High Pressure Septum, ea 80194Microseal™ High Pressure Nut, ea 80196

For Varian 1078 & 1079 GCs with SPME InjectorMicroseal™ High Pressure Septum, ea 80035

Inlet Pressure Gauge

Insert the needle directly into the inlet of any gas chromatograph for direct pressure measurement. The small, 0.028" o.d. needle permits repeated inlet pressure checks without damage to the septum.

Septum Needle Guide

This septum needle guide helps reduce bent syringe needles and extends septum life. With the septum needle guide you get double leak protection. A cylindrical septum acts as a double seal should your primary septum start leaking. Needle guide is self-centering to aid in on-column injection.

Septa-Out

Safely extract cylindrical septa without the danger of breaking your glass column or sampling bulb port.

Heat Resistant Gloves• Protect your hands from burns• Heavyweight cotton/Kevlar®

combination

Knit construction offers superior comfort and lessens hand fatigue. Gloves are ambidextrous and feature a glove-within-a-glove design.

G C A C C E S S O R I E S

Septa

*Regular Merlin Microseal™ has a 30psig limit. High Pressure Merlin Microseal™ has a 100psig limit.

Septum Remover

90º hooked point allows for safe septum removal. Aluminum body. 8" length.

SEPTUM REMOVERDESCRIPTION PART NO. PRICE

Septum Remover 24030

SEPTA-OUTDESCRIPTION PART NO. PRICE

Septa-Out 6412

HEAT RESISTANT GLOVESDESCRIPTION QTY. PART NO. PRICE

Heat Resistant Gloves pr 2906

INLET PRESSURE GAUGEDESCRIPTION PART NO. PRICE

0-30psig 868050-60psig 868060-100psig 868070-200psig 86808Replacement Needle Assembly 18260

SEPTUM NEEDLE GUIDEDESCRIPTION PART NO. PRICE

Needle Guide, 7/16" x 20 Thread* 6401Needle Guide, 7/16" x 24 Thread 6403Needle Guide without Nut 6400Drill Bit for Enlarging Hole 6402Replacement Cylindrical Septa, 25/pk 6524

*Fits most injection ports including: PE-3920 and Sigma Series; HP5700, 5800, and 6900 Series (5890 and 6890).

Page 53: Capillary Accessories · 2009-10-08 · Capillary Accessories ACCESSORIES Universal Guard Column Kits • Universal kits connect to any capillary column • Guard columns are deactivated

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436436 437437

5325 2156

5181

5688 5687

5772

6691

5270

5509

Organizer Box

These organizers are ideal for storing small parts such as septa, ferrules, and fittings. The 9-compartment organizer includes eight 1-3/8" x 1-5/8" slots and one 1-1/8" x 3-1/4" slot. The 18-compartment organizer includes twelve 2" x 2" slots and six 2" x 4-3/16" slots.

Capillary Magnifiers

These magnifiers are ideal for inspecting the ends of capillary columns. The lighted magnifier includes a battery.

20X Magnifier Lighted Magnifying Glass

Gas Torch

Ideal for sealing the ends of capillary columns. Basic kit contains the torch, two Micronox cylinders, one butane cylinder, three silver soldering rods, flux tube, two flame tips and complete instructions.

Adjustable Organizer

This extra-large organizer has 14 adjustable dividers and 4 shelves for convenient access to common lab supplies. PVC construction is chemically resistant and makes cleaning easy. 20"H x 24"W x 10.5"D

Organizers and ToolsGC Column and Accessory Organizers

Keep all your high-use columns readily available and protected with these 5-column or 10-column storage units. Both units feature a covered 7-bin, small-parts storage on top. Larger tools can be stored in the tool holder on the side. Columns are easy to remove and ID tags are readily visible.

5-Column Organizer14L x 13H x 10.5"W (35.5L x 33H x 26.5cmW)

10-Column Organizer25L x 12.75H x 10.5"W(63.5L x 32H x 26.5cmW)

Heat Gun

Ideal for heating polyimide sealing resin when connecting capillaries and guard columns. Gun heats to 350ºC, features a 3-position switch (off/cool/hot) and includes an adjustable stand.

G C A C C E S S O R I E S

Organizers and Tools

Drawer Organizer

This compact organizer features 30 drawers for storing all of your small parts and accessories. Clear plastic drawers are 1-1/8"L x 2"W x 4-5/8"D and can be easily labeled. Overall organizer dimensions are 8-1/4"L x 11-1/4"W x 5-1/8"D.

ORGANIZER BOXDESCRIPTION PART NO. PRICE

9-Compartment Box 626418-Compartment Box 6266

DRAWER ORGANIZERDESCRIPTION PART NO. PRICE

Drawer Organizer 6260

CAPILLARY MAGNIFIERSDESCRIPTION PART NO. PRICE

20X Magnifier 3163Lighted Magnifier 3196

GAS TORCHDESCRIPTION PART NO. PRICE

Basic Torch Kit 14600Cylinder Kit (4 Micronox and 2 Butane) 14601Micronox Cylinders, 6/pk 14602Butane Cylinders, 6/pk 14603Piercing Knob, Butane 14604Piercing Knob, Micronox 14605

HEAT GUNDESCRIPTION PART NO. PRICE

120VAC, 4.5A, 60Hz 2518220VAC, 2.0A, 50/60Hz 2518-220V

ADJUSTABLE ORGANIZERDESCRIPTION PART NO. PRICE

Adjustable Organizer 5242

GC COLUMN AND ACCESSORY ORGANIZERSDESCRIPTION PART NO. PRICE

GC Column Organizer, 5-Column 6390GC Column Organizer, 10-Column 6392

Page 54: Capillary Accessories · 2009-10-08 · Capillary Accessories ACCESSORIES Universal Guard Column Kits • Universal kits connect to any capillary column • Guard columns are deactivated

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438438 439439

5715

5321

5324

5322

5323

5179

5178

6279

6779

Flame Checker

Pivoting mirror head fogs when flame is lit.

G C A C C E S S O R I E S

Tools

ToolsCapillary Tool Kit

Kit includes diamond scriber, 2 open end wrenches, PTFE coated forceps, ruler, ferrule pick, 10' high temperature string, 20X magnifier, and pipe cleaner.

23-Piece Tool Kit in Zippered Case

Kit includes 7 screwdrivers, adjustable wrench, 2 pliers, wire stripper, knife, alignment tool, stainless rule, hex key set, scissors, 2 flexible files, burnisher, miniature soldering iron, solder aid, coil of solder, and desoldering braid.

Adjustable Wrench• Chrome-Plated

Open-End Wrench• Chrome-Plated

Autoranging Digital Multimeter

Unit has a 1/2" 3-3/4 digit LCD. Measures DCV, ACV, OHM, DC current, AC current, frequency plus diode check and continuity test. Uses 1-9V battery.

Miniature Reamers

Set includes six different sizes: 0.028"/0.018", 0.040"/0.026", 0.048"/0.032", 0.080"/0.050", 0.085"/0.053", 0.104"/0.062".

Miniature Files, Fine Cut

Set includes six different shaped, 5-1/2" long files. They are made of hard chrome steel suitable for smoothing and deburring.

9-Way Cylinder Wrench

CAPILLARY TOOL KITDESCRIPTION PART NO. PRICE

Capillary Tool Kit 16879

FLAME CHECKERDESCRIPTION PART NO. PRICE

Flame Checker 7047

23-PIECE TOOL KIT IN ZIPPERED CASEDESCRIPTION PART NO. PRICE

23-Piece Tool Kit and Case 16533

AUTORANGING DIGITAL MULTIMETERDESCRIPTION PART NO. PRICE

Autoranging Digital Multimeter 25970

ADJUSTABLE WRENCHDESCRIPTION PART NO. PRICE

4" Long – 1/2" Capacity 165496" Long – 3/4" Capacity 32118" Long – 7/8" Capacity 16522

OPEN-END WRENCHDESCRIPTION PART NO. PRICE

1/4" x 5/16" – Fits 1/16" Fitting Nuts 19987/16" x 1/2" – Fits 1/8" & 3/16" Fitting Nuts 19999/16" x 5/8" – Fits 1/4" & 3/8" Fitting Nuts 2000

MINIATURE REAMERSDESCRIPTION QTY. PART NO. PRICE

Miniature Reamers 6/pk 7330

MINIATURE FILESDESCRIPTION QTY. PART NO. PRICE

Miniature Files, Fine Cut 6/pk 7237

9-WAY CYLINDER WRENCHDESCRIPTION PART NO. PRICE

9-Way Cylinder Wrench 412933

Page 55: Capillary Accessories · 2009-10-08 · Capillary Accessories ACCESSORIES Universal Guard Column Kits • Universal kits connect to any capillary column • Guard columns are deactivated

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438438 439439

5225 5259

5228

5231

5230

5238

HOKE TOGGLE VALVESDESCRIPTION PART NO. PRICE

Straight Toggle Valves1/8" Brass 121311/4" Brass 121331/8" SS 121321/4" SS 12134Angled Toggle Valves1/8" Brass 121351/4" Brass 12136

Flow Control ValvesValve Selection Guide

Hoke Toggle Valves

These valves feature a simple, reliable, low-maintenance design that is well suited for a wide variety of applications. They are made of brass or stainless steel and include long-lasting Viton® seat and o-ring packing for positive pressure or vacuum applications. The maximum operating pressure is 200psig and the maximum operating temperature is 149°C.

Parker Toggle Valves

These forged-body valves are positive, soft-seat shut-off valves designed for quick opening and closing. Shut-off force is constant because of the spring load. The handle locks in the open or closed position. A TFE stem tip provides a leak-tight seal. The maximum working pressure is 250psig; maximum temperature is 93°C. They are made of brass or 316 stainless steel with TFE seat, Viton® packing and nylon handle. All other parts are 316 stainless steel.

PARKER TOGGLE VALVESDESCRIPTION PART NO. PRICE

1/8" Brass 23281/4" Brass 23321/8" SS 23361/4" SS 2340

ValvesG C A C C E S S O R I E S

Toggle Valves

Toggle valves are designed primarily as on-off valves for low pressure applications (less than 250 psig). The handle position provides a quick verifi cation of the on/off status.

Metering Valves

Metering valves are multi-turn valves designed to regulate gas fl ow.

Ball Valves

Ball valves are designed to throttle or shut off liquid and gas lines in high pressure applications (1500-2500psig). They are available in 2-way or 3-way confi gurations.

Plug Valves

Plug valves are designed to throttle or shut off liquid and gas lines in intermediate pressure applications (less than 500 psig). They generally have a higher temperature limit than ball or toggle valves.

For order information on Plug Valves, Ball Valves and Metering Valves, see page 440.

Part No. 2328

Part No. 12131

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440440 441441

5232 5233 5234

5262 5260 5263

5264

52355261

NUPRO AND WHITEY FINE METERING VALVESDESCRIPTION PART NO. PRICE

Straight Pattern1/8", Brass 86001/4", Brass 86021/8", SS 86041/4", SS 8606Angle Pattern1/8", Brass 86081/4", Brass 86101/8", SS 86121/4", SS 8614

HOKE FINE METERING VALVESDESCRIPTION PART NO. PRICE

Straight Pattern1/8", Brass 860011/4", Brass 860211/8", SS 860411/4", SS 86061Angle Pattern1/8", Brass 860811/4", Brass 861011/8", SS 861211/4", SS 86141

Flow Control ValvesNupro and Whitey Plug and Ball Valves

The plug valves are constructed of brass or stainless steel and TFE. The compact plug valves can be used up to 3000psig and the temperature limit is 200°C. They have a plug orifice of 0.172" for high flow capacity.

The 2-way and 3-way ball valves can be used up to 65°C and are pressure-rated to 2500psig. Both can be panel-mounted in a 19/32" hole. The 1/8" valves have a 0.093" orifice while the 1/4" valves have a 0.125" orifice.

NUPRO AND WHITEY PLUG AND BALL VALVES

DESCRIPTION

PLUG VALVE

PART NO. PRICE

2-WAY BALL VALVE PART NO. PRICE

3-WAY BALL VALVE PART NO. PRICE

1/8", Brass 14320 14318 143161/4", Brass 14319 14317 143151/8", SS 16013 16017 160221/4", SS 16015 16019 16024

Nupro and Whitey Fine Metering Valves

These valves give extremely fine control in the 0-400cc/minute gas flow range. The maximum pressure rating is 1000psig at 70°C. The maximum temperature limit for brass valves is 150°C; 200°C for stainless steel. They can be panel mounted in a 37/64" hole.

Hoke Plug and Ball Valves

The plug valves are constructed of brass or stainless steel and PTFE. They have an upper pressure limit of 3000psig and an upper temperature limit of 205°C. They have a plug orifice of 0.093".

The 2-way ball valves are made of brass or stainless steel and PTFE. They have an upper temperature limit of 179°C and an upper pressure limit of 1500psig. The 1/8" version has a 0.093" orifice while the 1/4" version has a 0.187".

The 3-way ball valves are made of brass or stainless steel and PTFE/Nylatron®. They have an upper pressure limit of 500psig and an upper temperature limit of 179°C. Both sizes have a 0.187" orifice.

Hoke Fine Metering Valves with Vernier Knob

These valves allow reproducibility of precise flows. All valves use a TFE seat seal and packing. Brass valves are rated at 3000psig; stainless steel at 5000psig. Temperatures up to 230°C can be used but at lower pressures.

AnglePart No. 8612

G C A C C E S S O R I E S

Valves

HOKE PLUG AND BALL VALVES

DESCRIPTION

PLUG VALVE

PART NO. PRICE

2-WAY BALL VALVE PART NO. PRICE

3-WAY BALL VALVE PART NO. PRICE

1/8", Brass 12126 12118 121221/4", Brass 12128 12120 121241/8", SS 12127 12119 121231/4", SS 12129 12121 12125Plug Valve Repair Kit 12130

Part No. 14320 Part No. 14318 Part No. 14316

Part No. 12126 Part No. 12119 Part No. 12123

StraightPart No. 8604 Part No. 86001

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440440 441441

5689

6239

• Replace columns without GC/MS shutdown

• Protect and maintain fl ow path integrity

• Compatible with any GC/MS system

• Installs quickly and easily

Alltech’s GC/MS switching valve eliminates long downtimes associated with column changes. Use the valve as a bypass valve to supply continuous carrier gas to the MS while changing a column in a single injector system or to switch between two columns from two injection ports to one MS.

The GC/MS switching valve is easy to install. Simply place the valve directly in the GC oven, connect the capillary columns and transfer lines to the appropriately labeled ports and the valve is ready to use.

GC/MS Switching Valve Specifi cationsTemperature Range: Ambient to 350°CMaximum Pressure: 25psigConnections: Zero Dead VolumeCompatible Column Sizes: 0.25mm or 0.32mm i.d.

GC/MS SWITCHING VALVEDESCRIPTION QTY. PART NO. PRICE

GC/MS Switching ValveFor 0.25mm i.d. ea 12325For 0.32mm i.d. ea 12327Replacement PartsNuts, 1/32" 5 123170.25mm Ferrule & Liner Set 5 123190.32mm Ferrule & Liner Set 5 12324

• Simple operation • Direct GC/MS

interface • Save 6-12 hours

The ms-NoVent™ is a fl uidic valve that can be retrofi tted to any GC mass spectrometer. It allows column changeover without the need to vent the MS resulting in a time saving of 6-12 hours. The unique design ensures a helium purge maintains a positive fl ow from the valve, to the atmosphere, when a column is not connected. Certain GC/MS models require a restrictor to be ordered separately at right.

SGE MS-NOVENT™

DESCRIPTION PART NO. PRICE

ms-NoVent™

Suitable for Varian, Shimadzu, Perkin-Elmer, ThermoQuest, and HP/Agilent (all HP models including 5890 and 6890)

113400

ms-NoVent™ RestrictorsRestrictor for HP5970 113405Restrictor for HP5971/5972 113407Restrictor for HP5973 113409Restrictor and Adapter for Varian Saturn 2000 113412Restrictor and Adapter for Shimadzu 5000/5050 113410

G C A C C E S S O R I E S

Valves

For more information on the GC/MS Switching Valve, request IS037. Also available on our website.

Alltech GC/MS Switching ValveSwitch Between Columns with the Turn of a Valve

SGE ms-NoVent™ ValvePrevents Air and Water from Entering the MS during Column Changeover

Call Alltech Tech Support:

Email: [email protected] Online: www.alltechWEB.com

Need Technical Assistance?

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2102

2103

2104

Valco® Sampling/Switching Valve SpecificationsValve Body: Type 316 Stainless Steel Max. Temp: 175°C for medium temperature valves

300°C for high temperature valves*Valve Seal: Carbon-filled PTFE (Medium Temp.) or

Carbon-filled Polyimide (High Temp.)Active Ports: 3,4,6,8 or 10 Ports (Note: a 10-port valve can be used

as a 6- or 8-port valve)Outlet Fitting: 1/16" zero-volume fittings or

1/8" zero-volume fittings (included)Mounting: Valves supplied with angle mounting brackets for

mounting on the side of the instruments or they can be flush mounted. Valves are tapped with 8-32TPI holes. Most GCs are designed to accept these valves.

Max. Pressure: 400psig

*Cannot be used below 200°C.

• Easily adapt to any type of tubing• Eliminate pressure surges during sample injections• Carefully leak tested

Valco® sampling/switching valves are ideal for all GC sample injections and flow switching applications. The low internal volume and uniform flow paths eliminate peak broadening and loss of resolution. Medium temperature valves have a limit of 175ºC and high temperature valves have a limit of 300ºC. Valves require sample loops—order separately on facing page.

Valco® valves feature zero volume fittings that allow tubing connections to the valve body without increasing the internal sample volume. Fittings also make direct, on-column injections possible. Replacement zero volume fittings are available on facing page.

What’s included: zero-volume fittings, mounting bracket, and handle.

G C A C C E S S O R I E S

Valves

Valco® Sampling/Switching ValvesZero Volume Fittings Allow for Direct Valve Connections

* By special order, valves can be fabricated from Hastalloy C®. Call for pricing information.

VALCO® SAMPLING/SWITCHING VALVES*

DIAGRAM PORTS FITTINGSMEDIUM TEMP.

VALVE PART NO. PRICEHIGH TEMP.

VALVE PART NO. PRICE

REPL. SHAFT & SEAL FOR MEDIUM TEMP. VALVE PART NO. PRICE

3-Port 1/16" Zero Volume 9099 39099 2909901/8" Zero Volume 9101 39101 291010

4-Port 1/16" Zero Volume 9103 39103 291031/8" Zero Volume 9104 39104 29104

6-Port 1/16" Zero Volume 9105 39105 291051/8" Zero Volume 9110 39110 29110

8-Port 1/16" Zero Volume 9115 39115 291151/8" Zero Volume 9116 39116 29116

10-Port 1/16" Zero Volume 9119 39119 291191/8" Zero Volume 9120 39120 291200

Page 59: Capillary Accessories · 2009-10-08 · Capillary Accessories ACCESSORIES Universal Guard Column Kits • Universal kits connect to any capillary column • Guard columns are deactivated

Contact your Alltech office or distributor for current or local prices.© Copyright 2004 Alltech Associates, Inc. Contact your Alltech office or distributor for current or local prices.© Copyright 2004 Alltech Associates, Inc.

442442 443443

1578

1577

SampleLoop

Valve Body

ColumnInlet

Fused Silica Tubing

Nut

PolyimideFerrule

RotorSlot

Valve Body

Adapter

.010" Orifice (.25mm)

RemovablePolyimideLiner

1579

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Adapters Shown in a Valve

Zero Volume Fittings

ZERO VOLUME FITTINGS

DESCRIPTION

USE WITH 1/16" VALVES

PART NO. PRICE

USE WITH 1/8" VALVES

PART NO. PRICE

Nuts, 5/pk 458015 458025Ferrules, 5/pk 458125 458155

VALCO® SS SAMPLE LOOPS*

LOOP SIZE

USE WITH 1/16" VALVES

PART NO. PRICE

USE WITH 1/8" VALVES

PART NO. PRICE

15µL 91056 9110625µL 91057 9110750µL 91058 91108100µL 91059 91109250µL 91050 91100500µL 91051 911011.0mL 91052 911022.0mL 91053 911035.0mL 91054 9110410.0mL 91055 91105

*One pair of nuts and ferrules are included.

Stainless Steel Sample Loops

Valve Actuators

The Valco® 2-position helical actuators permit the application of controlled, constant torque for the actuation of rotary devices. Minimum actuation pressure is typically less than 30psig for operation of Valco® sample injection and switching valves. Low internal leakage permits either pulsed or continuous operation with low gas consumption.

Actuators are designed for room temperature operation, but high temperature versions are also available. Valves intended for mounting in ovens or heated detector zones are used with a stand-off assembly which locates the actuator out of the heated zone and supports both valve and actuator. Order a stand-off assembly separately below.

Fused Silica Adapters

Fused silica adapters permit easy use of capillary columns with 1/16" Valco® valves.

FUSED SILICA ADAPTERSDESCRIPTION PART NO. PRICE

Fused Silica Adapter for:0.53mm i.d. Column 15380.32mm i.d. Column 15670.25mm i.d. Column 1569Replacement Liner for:0.53mm i.d. Column, 2/pk 15390.32mm i.d. Column, 2/pk 15710.25mm i.d. Column, 2/pk 1573Counter-bored Nut, 2/pk 1549Replacement Ferrule, 2/pk 1558

VALVE ACTUATORSDESCRIPTION PART NO. PRICE

Air Actuators90° Air Actuator for 3-8 Port Valves and 3,000psig HPLC Valve

9121

60° Air Actuator for 10 Port Valves and 7,000psig HPLC Valve

9122

90° Hi-Temp Air Actuator for 3-8 Port and 3,000psig HPLC Valves

91211

Air Switch for Air Actuators, 110V 9123Air Switch for Air Actuators, 220V 9124DVI-Digital Valve Interface 13916" Stand-Off Assembly 91216

G C A C C E S S O R I E S

Valves

Accessories for Valco® Sampling/Switching Valves