ASTM Wear Testing

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    .Wear 225229 1999 11591170

    Development and use of ASTM standards for wear testing 1

    Peter J. Blau a,), Kenneth G. Budinski b

    aOak Ridge National Laboratory, P.O. Box 2008, Oak Ridge, TN 37831-6063, USA

    bEastman Kodak, Rochester, NY 14652-4347 USA

    Abstract

    Standard wear test methods have been developed under the auspices of various ASTM technical committees. Committee G-2 on Wear

    and Erosion was established in 1964 and has been a leader in developing such standards. Some ASTM wear testing standards are aimed

    at specific components, like the jaws of rock crushers, but others are designed to determine a materials resistance to a specific wear type,

    like solid-particle erosion or two-body abrasive wear. Having identified a need for a new wear testing standard, ASTM G-2 typicallyfollows a process of first assigning responsibility to a relevant subcommittee. The subcommittee chair may then decide to establish a task

    group to develop the given method, conduct one or more inter-laboratory testing programs, write a draft standard, conduct ballots, and

    revise or rewrite the draft standard to achieve consensus. Since the repeatability and reproducibility varies between test methods

    understanding the role of instrumental and measurement factors of each wear testing standard is critical before it can become approved. In

    addition, each standard is critically reviewed on a continuing 5-year basis, and revised or updated as needed. This paper describes the

    development of standard wear testing methods and provides five examples of how ASTM G-2 wear testing standards were used to help

    solve important industrial problems involving sliding wear, abrasive wear, galling, and erosive wear. q 1999 Published by Elsevier

    Science S.A. All rights reserved.

    Keywords: Wear; ASTM G-2; Erosion; Galling

    1. Introduction

    There are many types of wear test methods both be-

    cause there are many types of wear and because there are

    many different situations in which wear has become a

    problem. Wear test methods fall into any of several cate-

    gories. Some wear test methods are aimed at a specificw xtype of material, such as wear test methods for plastics 1 .

    Some are aimed at evaluating a materials response to a

    specific type of wear, such as solidparticle erosion, slid-

    ing wear, or two-body abrasive wear. Other wear tests are

    designed to simulate a particular field application in orderto screen materials, surface treatments, or lubricants for

    )

    Corresponding author. Tel.: q1-423-574-5377; fax: q1-423-574-

    6918; E-mail: [email protected]

    The research of the first author was sponsored in part by the U.S.

    Department of Energy, Office of Transportation Technologies, High

    Temperature Materials Laboratory User Program, under contract DE-

    AC05-96OR 22464 with Lockheed Martin Energy Research.

    that type of service. Finally, some wear tests are intended

    for fundamental research into the basic nature of wear.

    Standard wear test methods have been used for all of these

    reasons, but like any type of wear test, standard test

    methods have both strengths and limitations.

    The principal advantages of using ASTM standard wear .test methods are: 1 the test methods have been rigorously

    .evaluated and the procedures carefully documented; 2 the

    repeatability and reproducibility of results tends to be

    better documented and understood than for specialized or .one-of-a-kind types of wear testing machines; 3 in many

    cases, a great deal of previous data exists and it is conve-nient to compare new results with the existing data; and .4 documentation and reporting requirements have been

    established so that all the major variables and results of the

    work can be presented in a complete and organized man-

    ner. On the other hand, there are occasions when no

    ASTM test method satisfactorily meets the current need

    for wear data. Perhaps it does not simulate an intended

    application sufficiently well, or perhaps the specified test-

    ing parameters lie outside the interests of the current

    investigation.

    0043-1648r99r$ - see front matter q 1999 Published by Elsevier Science S.A. All rights reserved.

    .P II: S 0 0 4 3 -1 6 4 8 9 9 0 0 0 4 5 -9

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    Table 1

    ASTM wear tests developed by several committees

    Designation Test description

    D-4172 Wear preventive characteristics of lubricating fluids

    D-4170 Fretting wear protection by lubricating greases

    G-32 Vibratory cavitation erosion test

    G-56 Abrasiveness of ink-impregnated fabric printer ribbons

    G-65 Dry sandrrubber wheel abrasion test

    G-73 Liquid impingement erosion test

    G-75 Slurry abrasivityG-76 Erosion by solid particle impingement using gas jets

    G-77 Ranking resistance of materials to wear using block-on-ring wear test

    G-81 Jaw crusher gouging abrasion test

    G-83 Crossed-cylinder wear test

    G-98 Galling test

    G-99 Pin-on-disk test

    G-105 Wet sandrrubber wheel abrasion test

    G-119 Synergism between wear and corrosion

    G-132 Pin abrasion test methods

    G-133 Reciprocating sliding wear test

    G-134 Cavitating liquid jet erosion test

    G-137 Ranking resistance of plastic materials for sliding wear using a block-on-

    ring configuration

    ASTM is an organization with about 36,000 members

    and 132 standards committees. Several of these commit-

    tees have produced wear testing standards. A list of the

    ASTM wear testing standards is provided in Table 1. The

    number of standards changes periodically since each stan-

    dard must be re-balloted for approval every 5 years, and

    new standards are added from time to time. The two

    committees which have produced more wear tests than the

    others are committee D-2 on Lubrication and Committee

    G-2 on Wear and Erosion.

    The current paper focuses on the Committee G-2s

    work in developing new wear testing standards, and illus-

    trates how specific standards can be used to solve practical

    wear problems. Committee G-2 was formed in 1964, based

    on a growing interest in erosive wear, particularly in utility

    power plants. Since that time, the committees scope has

    widened to comprise other forms of wear as well. The

    breath of the committees interests is reflected in the

    continuing series of technical publications. Some of the

    standard wear test methods of today have resulted from

    Fig. 1. Coefficient of variation within laboratories and between laboratories for five ASTM wear test methods. Data obtained from the respective standards

    documents.

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    needs identified in technical symposia and workshops or-

    ganized by G-2 members.

    2. How ASTM standard wear testing methods are de-

    veloped

    Any new ASTM testing standard arises out of a need

    for the systematic collection of materials property mea-surements in a certain area of science or engineering. In

    the case of wear data, the usual process begins at the

    subcommittee level. The current standards-writing sub-

    committees in Committee G-2 on Wear and Erosion are

    G02.091Erosion by Solids and Liquids, G02.20Com-

    puterization in Wear, G02.30Abrasive Wear, G02.40

    Non-Abrasive Wear, G02.50Friction, and G02.91

    Terminology. Other subcommittees perform supporting

    functions like editorial review and long-range planning

    When a proposal for a new standard is introduced and

    there is a consensus agreement within the subcommittee

    that a widespread need exists, then the subcommittee

    chairman may establish a task group in that area. The new

    task group draws its members from experts and interestedparties, whether they are ASTM members or not. If several

    task group members possess wear machines which can

    provide certain agreed-upon conditions, then an interlabo-

    ratory test program can be conducted. Several rounds of

    interlaboratory tests may be needed to define the appropri-

    Table 2 .Typical variabilities of ASTM wear test methods Data from interlaboratory studies

    Standard Wear type Material Conditions Within-Lab Between-a a . .COV % Lab COV %

    G-32 cavitation erosion Ni 200 20 Hz freq., 50 mm amplitude, 8.9 20distilled water at 25 " 28C, .max. loss rate in mmrh

    G-65 abrasion by sand 4340 steel 130 N force, 1000 revolutions 5.9 5.23 .between a wear loss in mm

    specimen and a

    rubber wheel

    4340 steel 130 N force, 2000 revolutions 2.4 3.53 .wear loss in mm

    WC 20% 130 N force, 6000 revolutions 6.4 19.33. .Co wear loss in mm

    G-76 erosion by 1020 steel 50 mm alumina particles, 30 17.1 29.3

    particles in a gas mrs vel., 908 incidence,3stream 2 grmin feed wear in mm rg

    .erodant

    1020 steel 50 mm alumina particles, 70 3.4 17.0mrs vel., 908 incidence,32 grmin feed wear in mm rg

    .erodant

    304 50 mm alumina particles, 70 4.9 21.0

    stainless mrs vel., 908 incidence,3steel 2 grmin feed wear in mm rg

    .erodant

    G-77 block sliding on a 01 tool 134 N force, 72 rpm, 5400 37.6 18.8ring steel block r revolutions, no lubricant wear

    3.4620 steel of the block in mm

    ring

    01 tool 134 N force, 197 rpm, 5400 14.9 40.2steel blockr revolutions, no lubricant wear

    3.4620 steel of the block in mm

    ring01 tool 803 N force, 72 rpm, 5400 25.9 25.9

    steel blockr revolutions, no lubricant wear3.4620 steel of the block in mm

    ring

    G-133 reciprocating self-mated 25 N force, 5.0 Hz, 10 mm 34.7 sliding Si N stroke wear of the flat3 4

    3.specimen in mm

    self-mated 200 N force, 10.0 Hz, 10 mm 23.7 48.6Si N stroke, mineral oil wear of the3 4

    3 .flat specimen in mm

    aCoefficient of variation, as defined in ASTM E-691.

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    Fig. 2. Gravure pattern for toller application of coatings.

    ate test conditions and establish which variables must be

    controlled to reduce any variability in the results.

    After successful interlaboratory testing is completed, adraft standard is written and submitted for editorial review.

    Then a subcommittee ballot is conducted. All negative

    ballots must be resolved either by revision of the draft,

    withdrawal of the negative, or being voted non-persua-

    sive after discussion. Having passed subcommittee, the

    main committee votes on the draft standard. All these

    procedures are instituted to assure that published ASTM

    wear test methods provide meaningful data for the users of

    the standards. Due to the rigors of the process, the time

    required to produce a new standard can range from 2 to 10

    years. In addition, each standard for which a committee is

    responsible must be reapproved every 5 years to assure its

    Fig. 4. Wear data for the doctor blade and gravure pattern. Top-unim-

    planted; bottom-implanted.

    continuing validity and to incorporate new knowledge and

    measurement techniques.

    3. Interlaboratory testing to validate a proposed stan-

    dard wear test method

    The leader of the task group works to develop the set of

    operating instructions for the test, obtains materials, and

    assembles specimens for distribution to the participants

    The procedures developed for the interlaboratory test se-

    ries may eventually form the basis for the standard when

    the draft version is prepared. Interlaboratory tests are

    normally conducted in a manner which is prescribed by

    Fig. 3. Schematic of the pin-on-disk testing machine.

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    w xASTM E-691 2 . This is done to ensure that the tests

    produce statistically valid information for establishing the

    precision of the test method. In addition, ASTM Commit-

    tee G-2 has its own standard for reporting interlaboratoryw xdata specific to wear testing 3 . Two aspects of an inter-

    .laboratory test are particularly important: 1 establishing

    the repeatability of results within each participating labora- .tory and 2 establishing the reproducibility of the results

    from one laboratory to another. These are quite differentissues. Sometimes data can be extremely consistent within

    a given laboratory but vary widely from one laboratory to

    another. Therefore, it is common to have to conduct

    several of rounds of interlaboratory tests until the reasons

    for any variabilities have been sorted out, and the group

    has identified all the aspects which must be controlled to

    assure consistent results. The data from interlaboratory

    programs may often be summarized in an appendix to the

    standard, and becomes part of the research report which is

    archived at ASTM headquarters to provide backgroundinformation for each published standard.

    Fig. 5. Scoring of a gear tooth.

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    Fig. 1 shows the variability in data for five types of

    ASTM standard wear tests, as determined from interlabora-

    tory studies and published in their respective standards

    documents. Table 2 provides information on the conditions

    and materials. Additional details, such as the numbers of

    participants and interpretation of the data, may be found in

    the referenced standards which appear in the ASTM An- .nual Book of Standards Volume 03.02 1996 . The

    .within-laboratory coefficients of variation COVs rangefrom 2.4% to above 37% and the between laboratory

    COVs range between 3.5% and up to nearly 50%. Of the

    data presented here, the dry sandrubber wheel abrasive

    wear test exhibited the lowest COVs and the reciprocating

    wear test G-133 the highest. In majority of cases, the

    within-laboratory COVs are lower than the between labo-

    ratory COVs, but this is not always true. The information

    contained within standards therefore provides important

    information for determining whether the differences be-

    tween wear values for candidate materials are truly signifi-

    cant or whether they fall within expected variations for

    that particular type of test. For sliding wear tests, it has

    been the authors experience that variations in friction and

    wear tend to be greater for unlubricated than for lubricated

    testing conditions.

    There are three major sources of wear data scatter: the

    testing machine, the operators technique, and the materi-

    als themselves. No source of error or variability can neces-

    sarily be ruled out a priori. The term testing machine

    includes not only the calibration and construction of the

    machine, but also its proximity to sources of vibration and

    environmental cross-contamination. The operators tech-

    nique includes such issues as judgment when making

    measurements, proper specimen handling and cleaning,

    attention to procedural details, and operator fatigue. Thescatter in data can also result from microstructural hetero-

    geneities or lot-to-lot variations within the materials them-

    selves.

    The potential for material heterogeneities contributing

    to scatter raises the issue of whether it is feasible to

    produce standard reference materials to calibrate wear

    testing machines. Standard G-65 for dry sandrubber wheel

    abrasion testing describes standard reference materials and

    how they are to be prepared for each of the optional testing

    procedures, and Standard Practice G-76 for liquid impinge-

    ment erosion also suggests materials for use as reference.

    For example, ASTM G-65 specifies for its Procedure Areference material a D-2 tool steel which has been heat

    treated to a certain Rockwell C hardness and which will

    produce a mass loss of 36 " 5 mm3. Despite the desirabil-

    ity of having materials with which to calibrate wear ma-

    chines, it is not an easy task to ensure that such materials

    can be produced in a consistent manner, and to in some

    manner certify that any specimen selected from within a

    characterized lot of reference material will fall within a

    given range in terms of wear rate or wear volume. While it

    is certainly possible for a testing laboratory to purchase

    and maintain a large stock of carefully characterized refer-

    ence materials and lubricants for future wear use, an

    alternative is to maintain and calibrate wear testing and

    measuring instruments using the best practices available.

    In addition, reference alloy specimens can corrode or

    develop surface films if not well protected, and lubricants

    can have a finite shelf life. The issue of reference material

    storage practices is important, but beyond the scope of this

    paper.

    4. Applications of ASTM wear testing standards

    The following five case studies show how ASTM stan-

    dard wear tests can be used to help evaluate and select

    materials for service in wear-critical applications.

    4.1. Case study 1: ion implantation to increase the life of

    graure cylinders

    Gravure cylinders are rollers that are covered with .surface dimples called cells. These features Fig. 2 come

    in different sizes and depths. They are used to apply

    coatings to web surfaces. The gravure roller dips into a

    tray of the material to be coated. Then a doctor blade

    contacts the gravure cylinder and removes all of the mate-

    rial except what is retained in the cells. The gravure

    cylinder then contacts the web and deposits the coating on

    the web at a consistent thickness. These cylinders are used

    to apply a wide variety of coatings to flexible plastic webs. .The steel spring doctor blade 47 HRC can produce

    unacceptable wear of the cells on the chromium-plated

    gravure roller. Since the implantation of chromium and

    Fig. 6. Schematic of the ASTM G-98 galling test arrangement.

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    Table 3

    Threshold galling stresses of candidate materials

    Upper specimen, Lower specimen, Threshold galling stress . . .Rockwell hardness Rockwell hardness ksi

    U U . .Steel 2 61 HRC Steel 2 61 HRC ) 40.0U U . .Steel 2 57 HRC Steel 2 57 HRC 10.0U U . .Steel 1 59 HRC Steel 2 59 HRC ) 40.0

    . .D2 60 HRC D2 60 HRC ) 40.0 . .D2 55 HRC D2 55 HRC 10.0

    . .D2 50 HRC D2 55 HRC 2.5 . .D2 50 HRC D2 60 HRC 5.0

    USpecimens taken from gears used in service.

    other metals with various atomic species has been knownw xto significantly improve wear life 4 , a study was con-

    ducted to determine if ion implantation of the would

    improve roller life without causing significant reduction in

    doctor blade life. The prime criterion for an acceptable .tribosystem materials pairing was increased uptime, com-

    pared with the present.w x .The ASTM G-99 pin-on-disk wear test 5 , Fig. 3 was

    selected to compare ion-implanted with non-implanted .chromium flat panels 3 panels containing the same

    gravure cell patterns. Plasma-assisted N implantation was

    used at a dosage level recommended by the supplier. A .flat-ended pin was made from Type 1080 steel 47 HRC ,

    the same material as the doctor blade. Wear tests were

    conducted using test parameters to simulate the production

    system. Damage to the gravure cells and the pin was

    measured by stylus profiling and converted to wear vol-

    ume. As shown in Fig. 4, results of these tests indicated

    that implantation increased the wear of the doctor blade

    material. In fact, the doctor blade would have to be

    replaced almost three times as often with an implantedgravure cylinder, and this would have a negative impact on

    process time. Thus, a decision was made to seek an

    alternative solution. Use of this relatively simple ASTM

    test provided a fast answer on the feasibility of a candidate

    process and it avoided costly testing on production cylin-

    ders.

    4.2. Case study 2: scoring of spur gears

    Spur gears, 150 mm in diameter, were used in a preci-

    sion timing mechanism. They were made of air-hardening,

    high-carbon, high-chromium tool steel. One gear set had

    been running for 10 years without problems. One set, then

    another failed by pitch line scoring. Metallurgical studies

    indicated that severe adhesive wear occurred on the loaded

    .side of a significant number of teeth see Fig. 5 . Thisscoring caused timing errors and subsequent shutdown of a

    manufacturing operation, and the gears had to be replaced

    at significant cost. A study was conducted to determine thew xcause of these failures and propose a solution 6 .

    The gears were failing by severe adhesive wear, and

    further investigation disclosed that the gear material com-

    position had been changed by the gear supplier to a grade

    of high-carbon, high-chromium steel to allow the applica- .tion of high-temperature, physical-vapor-deposited PVD

    coatings without loss of hardness. The hardness of the new

    gear material was 56 HRC, compared to a range of 5658

    HRC for the gear steels which did not fail. We wondered ifa drop in Rockwell hardness of only two points would

    make the new steel more prone to galling.

    Gear scoring is due to adhesion under high load com-

    bined with relative motion between the mating gear teeth.

    The pin-on-flat galling test provides a reasonable simula-

    tion of this tribosystem. Therefore, we selected the ASTM

    Fig. 7. Schematic of the reciprocating wear testing machine.

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    . .Fig. 8. Arbitrary scale used to rank the degree of wear debris formation on the ball specimen top and flat specimen bottom .

    w xG-98 test method for use in our galling evaluation 7 . The .test involves rotation of a flat-ended pin 3608 under a

    predetermined normal force on a flat counterface see Fig.

    .6 . The test metric is called the threshold galling stress.Its value is determined by conducting a series of tests

    with increasing the normal force until severe adhesive

    wear occurs. The threshold galling stress is the apparent

    contact stress at the highest load before galling starts.

    Table 3 compares the threshold galling stresses of seven

    material combinations. Results suggest that a minimum

    hardness of HRC 59 was needed with these steels to obtain

    maximum galling resistance.

    In summary, the ASTM G-98 galling test was used to

    uncover the reasons for an expensive gear failure. Follow-

    ing the initial work, G-98 was also used to screen and

    select additional steels for the improved scoring resistance

    needed for their use in timing gears.

    4.3. Case study 3: material couples for plastic-to-plasticsliding

    A potential contamination problem occurred in the de-

    velopment of an optical disk drive system. The drive

    system design specified the use of injection-molded plas-

    tics for a cam and follower mechanism that was used to

    move an actuator. Early polystyrene prototypes proved to

    be an unsuitable couple because both parts wore and

    produced debris which could contaminate the disk drive.

    The optical disk drive is very sensitive to particulate

    contaminants; hence, none are allowed, so freedom from

    w . . . .Fig. 9. Wear of candidate plastic riders reciprocating on a PTFE-filled acetal counterface. a acetal 12 N, b acetal 4, c acetalq PTFE, d Nylon . . x6r6q 10% aramidq 10% PTFE, e Nylon 6r6q 30% glass q silicone, f Nylon 6r6q silicone.

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    Fig. 10. Schematic of contact slitting knives.

    debris generation was just as important to this application

    as low wear. A study was therefore initiated to rank the

    wear resistance and lack of debris formation of various

    plasticplastic couples.

    Both cam and follower materials were open to all

    candidates. However, the requirements were that they be

    comparable in cost to other engineering plastics and that

    they be injection-moldable. In addition, the tribosystem

    had to survive 100,000 actuations with wear less than 0.2

    mm on the cam profile. Actuations were intermittent 3008

    forward and reverse rotations of the cam against the

    follower under a 4 N normal force.

    The test method selected was a modified version of the

    w x .ASTM G-132 8 pin abrasion test method. Fig. 7 Proce-dural modifications were necessary to mimic the load and

    sliding distance of this particular tribosystem. It was also

    necessary to develop a rating system to quantify the type

    of debris produced from the wear tests. Fig. 8 shows the

    rating scheme which was used to quantify debris build-up

    on both the ball and flat specimens. Previous reciprocating

    motion tests with a wide variety of metal counterfaces .indicated that poly-tetrafluoroethylene PTFE -filled acetal

    usually exhibits very low wear. Therefore, we used this .material as the standard counterface flat specimen with a

    variety of plastic sliders. The test length was 100,000

    cycles and the stroke length matched that to be experi-enced in service.

    Test results indicated that nylon with a proprietary

    lubricant had acceptable wear, and its debris rating was 0 .see Fig. 9 . This cost-effective screening procedure re-

    quired only about 4 h of technician attention time and

    produced a candidate material couple for production test-

    ing. The recommended couple showed no wear or debris in

    prototype testing, and as a result, the component design

    was changed to use this couple. The high cost and long

    lead time of full-size prototype tests were prohibitive in

    this case. Thus, laboratory screening tests are essential

    when dealing with unusual tribosystems such as plastic-

    on-plastic.

    4.4. Case study 4: materials for rotary slitter knies

    Plastic webs, cloth, paper, sheet metal and many related

    materials are manufactured in wide roll format and then

    are slit to salable width, usually by rotary slitter knives.

    Some products, such as photographic film and paper

    require very precise slitting with no debris generation

    Many slitters use contacting knives, like those shown inw xFig. 10 9 . The knives usually have a very small area of

    contact with the material being slit, and knife wear iscaused by a combination of metal-to-metal wear and abra-

    Fig. 11. Schematic of the cross-cylinders test.

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    Fig. 12. Summary of wear data for a variety of candidate material combinations tested with the crossed cylinders apparatus.

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    sive wear from the paper product. Thus, a study of a

    variety of candidate materials was conducted to find com-

    binations with improved wear life over the present couple

    in slitting paper.w xThe ASTM G-78 crossed-cylinder test 10 was selected

    for this work. A rotating cylinder is rubbed against the

    same size stationary cylinder, as shown in Fig. 11. Wear of

    the rotating member is assessed by measuring the volume

    of the groove formed on its outside diameter. Wear volumeof the wear spot or divot on the stationary cylinder is

    also measured, and together, the total system wear is

    determined.

    Test results on wide variety of candidate couples are

    shown in Fig. 12. These results clearly indicated that it is

    necessary to use cemented carbide for at least one member

    of the couple in order to get low system wear. This study

    indicated that replacing the current steelsteel couple with

    a tool steel-cemented carbide couple will produce a signifi-

    cant reduction in wear.

    Additional abrasion tests were conducted to rank these

    couples for paper abrasion resistance. These screening tests

    were essential because of the significant cost of testing

    different knives in slitting product. In addition to the set-up

    cost, if a knife couple worked poorly, it could produce

    unsalable product. Laboratory tests are again proved more

    cost-effective in this case.

    4.5. Case study 5: erosiity of dicalcium phosphate

    A certain manufacturing facility was trying to assess the

    feasibility of replacing a containerized bulk handling sys-

    tem for dry-sand-like dicalcium phosphate powder with a

    fluidized pipe transfer system. The plan showed significant

    savings in reduced labor and improved quality powder.cleanliness . But before making this large capital invest-

    ment decision, it was necessary to know whether the

    piping system would be fraught with blowouts due to

    erosion at bends. If the powder material was abrasive, it

    would be necessary to use much more expensive wear-re- .sistant piping e.g., hardened steel, basalt-lined pipe, etc.

    and this might make the whole project uneconomical Fig..13 .

    A laboratory test program was initiated to determine if

    particulate dicalcium phosphate with a particle size range

    Fig. 13.

    Table 4

    Erosion rates of two steels after impingement by 2000 grams of various

    erodants

    Candidate alloy Particle type Erosion ratey8 3 .=10 mm rg

    316 stainless steel dicalcium phosphate 6.4

    316 stainless steel silica 582.6

    D2 tool steel silica 750.1

    316 stainless steel aluminum oxide 968.2

    D2 tool steel aluminum oxide 1018.5

    of 1300 mm is abrasive to stainless steel or to hardened

    steel. There are several ways of assessing the erosivity ofw xdry powers 11 , but since the proposed transport system

    conveys the product in the fluidized state with flowing air,

    it was decided that the system could be modeled in the

    laboratory using the ASTM G-76 impingement erosion testw x12 . This test is essentially a sand-blasting nozzle aimed at

    a target material of choice. The standard test uses alu-

    minum oxide particles, but we substituted dicalcium phos-

    phate. The erosion rates of several test materials are shown

    in Table 4. Dicalcium phosphate by itself was capable of

    producing scratching abrasion on 300-series stainless steel,

    but used as a directed particle stream, it did not produce

    erosive wear. The impinging material apparently formed a

    protective coating on the target surface that in turn reduced

    the erosion rate to an insignificant level. Based on these

    results, it was recommended to install the pneumatic con-

    veyance system with soft stainless steel piping. In service

    the system, worked as predicted by the ASTM laboratory

    test method, and significant savings were realized.

    5. Summary

    ASTM committee G-2 friction and wear test methods

    address many of the most common occurrences of friction

    and wear in machinery. During test development, every

    effort is made to ensure that the tests are reliable and

    repeatable, and more importantly, to ensure that they add

    value to wear studies. The five case histories described

    here illustrate how ASTM wear tests or their variants can

    be used to solve design problems, production problems, or

    simply screen candidate materials for general applications.

    Sometimes application of these laboratory-scale tests canprevent the shutdown of a manufacturing operation that

    costs thousands of dollars per hour when it is not running.

    Solving existing or perceived wear problems at the design

    stage results in significant cost avoidance and, more impor-

    tantly, it can prevent loss of customers due to failures in

    service. Service failures not only raise costs, but result in

    loss of company reputation and business revenues. ASTM

    wear tests do not address the needs of every tribosystem,

    but where there is a match with an industrial tribosystem,

    they should be considered for application because they can

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    ( )P.J. Blau, K.G. Budinski r Wear 225229 1999 115911701170

    provide significant savings if used and interpreted prop-

    erly.

    Acknowledgements

    The research of the first author was sponsored in part

    by the U.S. Department of Energy, Office of Transporta-

    tion Technologies, High Temperature Materials LaboratoryUser Program, under contract DE-AC05-96OR 22464 with

    Lockheed Martin Energy Research.

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