APPENDIX D - Department of Defence...Geologists Log Drillers Log From (m) To (m) Thickness (m)...

PSI - BLAMEY BARRACKS KAPOOKA (0315)

APPENDIX D Other searches

14 June 2017 Report No. 1669283_001_R_Rev0 48


APPENDIX E Registered bore search


NSW Office of WaterWork Summary

GW414660

Licence: 40BL192510 Licence Status: CONVERTED

Authorised Purpose(s):

STOCK,DOMESTIC

Intended Purpose(s): STOCK, DOMESTIC

Work Type: Bore

Work Status: Supply Obtained

Construct.Method: Rotary - Percussion (Down Hole Hammer)

Owner Type: Private

Commenced Date: Final Depth: 66.00 mCompletion Date: 15/03/2010 Drilled Depth: 66.00 m

Contractor Name: Alpine Drilling Pty Ltd

Driller: Robert Mark Mclean

Assistant Driller: Paul Gooden

Property: N/A LOT 25 RIVERVIEW DRIVE MOORONG VIA WAGGA WAGGA 2650

Standing Water Level:

3.000

GWMA: Salinity:GW Zone: Yield: 1.000

Site Details

Site Chosen By:

County Parish CadastreForm A: WYNYA WYNYA.38 25//1148845

Licensed:

Region: 40 - Murrumbidgee CMA Map: 8327-1N

River Basin: 410 - MURRUMBIDGEE RIVER Grid Zone: Scale:Area/District:

Elevation: 0.00 m (A.H.D.) Northing: 6114314.0 Latitude: 35°06'48.9"SElevation

Source:Unknown Easting: 528753.0 Longitude: 147°18'55.9"E

GS Map: - MGA Zone: 0 Coordinate Source:

GIS - Geographic Information System

ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From

(m)To(m)

Outside Diameter(mm)

Inside Diameter(mm)

Interval Details

1 Hole Hole 0.00 54.00 165 Rotary - Percussion (Down Hole Hammer)


1 1 Casing Pvc Class 9 0.00 54.00 137 125 Seated on Bottom, Welded, S: 64.00-66.00m

1 1 Opening Slots - Vertical

48.00 54.00 137 1 Casing - Hand Sawn Slot, PVC Class 9, Screwed and Glued, SL: 45.0mm

Page 1 of 2

1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw414660.wsr.htm

Water Bearing ZonesFrom(m)

To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

48.00 66.00 18.00 Unknown 3.00 1.00 01:00:00 2200.00

Geologists LogDrillers LogFrom(m)

To(m)

Thickness(m)

Drillers Description Geological Material Comments

0.00 6.00 6.00 CLAY - RED Clay6.00 20.00 14.00 SILTSTONE - WHITE Siltstone

20.00 54.00 34.00 SILTSTONE - ORANGE Siltstone54.00 66.00 12.00 SILTSTONE - GREEN Siltstone

Remarks

15/03/2010: Form A Remarks: ENTERED BY PATRICIA EWERS ON 6TH APRIL 2011

*** End of GW414660 ***

Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice

should be sought in interpreting and using this data.

Page 2 of 2



GW414472

Licence: 40BL192478 Licence Status: ACTIVE


MONITORING BORE

Intended Purpose(s): MONITORING BORE

Work Type: Bore


Construct.Method:Owner Type: Private


Contractor Name:Driller: David, Michael Mcmahon

Assistant Driller:

Property: VARIOUS SITES AROUND WAGGA WAGGA TOWNSHIP WAGGA WAGGA 2650

Standing Water Level: 3.600

GWMA: Salinity:GW Zone: Yield:

Site Details

Site Chosen By:


Licensed:

Region: 40 - Murrumbidgee CMA Map:River Basin: - Unknown Grid Zone: Scale:

Area/District:




GPS - Global Positioning System


(m)To(m)


Inside Diameter(mm)

Interval Details

1 1 Casing Pvc Class 18 0.00 2.00 501 1 Opening Slots 2.00 5.00 1 PVC Class 18


To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

Page 1 of 2



To(m)

Thickness(m)


0.00 5.00 5.00 Clay, loam Clay5.00 5.00 0.00 Rock Rock

Remarks

25/06/2010: Form A Remarks: Marie Campbell 20/10/10

*** End of GW414472 ***



Page 2 of 2



GW414471



MONITORING BORE


Work Type: Bore





Assistant Driller:




Site Details

Site Chosen By:


Licensed:


Area/District:






(m)To(m)


Inside Diameter(mm)

Interval Details



To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

Page 1 of 2



To(m)

Thickness(m)


0.00 3.00 3.00 Clay Clay3.00 7.00 4.00 Loam Loam7.00 9.00 2.00 Sand Sand9.00 9.20 0.20 Gravel Gravel

Remarks


*** End of GW414471 ***



Page 2 of 2



GW414469



MONITORING BORE


Work Type: Bore





Assistant Driller:




Site Details

Site Chosen By:


Licensed:


Area/District:






(m)To(m)


Inside Diameter(mm)

Interval Details



To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

Page 1 of 2



To(m)

Thickness(m)


0.00 6.00 6.00 Clay Clay

Remarks


*** End of GW414469 ***



Page 2 of 2



GW405097



STOCK,DOMESTIC


Work Type: Bore


Construct.Method: Rotary - Percussion (Down Hole Hammer)

Owner Type: Private


Contractor Name: Dalton Water Drilling Services PTY LTD

Driller: John Michael Dalton

Assistant Driller: A. Dalton

Property: N/A 12 HENSCHKE AVENUE SAN ISIDORE 2650


15.000

GWMA: Salinity:GW Zone: Yield: 2.500

Site Details

Site Chosen By:

County Parish CadastreForm A: MITCH MITCH.33 5//730048

Licensed:

Region: 40 - Murrumbidgee CMA Map: 8327-1S







(m)To(m)


Inside Diameter(mm)

Interval Details


1 1 Casing Pvc Class 9 0.00 33.00 150 138 Driven into Hole, Glued, S: 93.00-115.00m


To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

87.00 87.20 0.20 Unknown 15.00 1.50 00:30:00

Page 1 of 2


93.00 93.20 0.20 Unknown 15.00 1.00 00:30:00


To(m)

Thickness(m)


0.00 1.00 1.00 TOPSOIL Topsoil1.00 5.00 4.00 CLAY Clay5.00 15.00 10.00 SHALE - WEATHERED Shale

15.00 17.00 2.00 SHALE - HARD Shale17.00 31.00 14.00 CLAY Clay31.00 115.00 84.00 SHALE - BLUE Shale

Remarks

24/04/2008: Form A Remarks: ENTERED BY PATRICIA EWERS ON 25TH NOVEMBER 2009

INFORMATION NOT PROVIDED ON FORM A:

NO INFORMATION ON DRAWDOWN LEVEL NO INFORMATION ON SALINITY AND WATER TASTE NO INFORMATION ON PUMPING TESTS ON BORE COMPLETION NO DETAILS ON SLOTS OR SCREENS FOR WATER ENTRY NO DETAILS ON GRAVEL PACK

*** End of GW405097 ***



Page 2 of 2



GW403806



STOCK,DOMESTIC


Work Type: Bore

Work Status: New Bore

Construct.Method: Auger - Solid Flight

Owner Type: Private


Contractor Name:Driller: Leo Murray Moloney

Assistant Driller:

Property: N/A 146 ROACH ROAD WAGGA WAGGA 2650


7.000


Site Details

Site Chosen By:


Licensed:






Unknown


(m)To(m)


Inside Diameter(mm)

Interval Details

1 Hole Hole 0.00 10.90 900 Auger - Solid Flight1 Annulus Waterworn/Rounded 4.00 4.50 Graded, Q:3.000m3,

PL:Poured/Shovelled1 Annulus Waterworn/Rounded 6.60 10.90 Graded, Q:2.000m3,

PL:Poured/Shovelled1 1 Casing Pvc Class 9 0.00 10.90 165 155 Seated on Bottom, Glued1 1 Opening Slots - Horizontal 7.80 10.90 165 1 Casing - Machine Slotted, PVC

Class 9, Glued, SL: 100.0mm, A: 5.00mm

Page 1 of 2



To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

7.20 10.90 3.70 Unknown 7.00


To(m)

Thickness(m)


0.00 4.50 4.50 BLAY CLAY STIFF Invalid Code4.50 6.30 1.80 GREY/BLACK CLAY Invalid Code6.30 6.60 0.30 FINE DAMP SAND Invalid Code6.60 7.20 0.60 FINE SILTY SAND AND MICA Invalid Code7.20 10.90 3.70 VERY CLEAN COARSE SAND AND

RIVER GRAVELInvalid Code

Remarks

09/02/2007: Form A Remarks: ENTERED BY PATRICIA EWERS 9TH OCTOBER 2007

INFORMATION NOT INCLUDED ON FORM:

NO INFORMATION ON YIELD AND DRAWDOWN LEVEL NO INFORMATION ON SALINITY AND WATER TASTE

*** End of GW403806 ***



Page 2 of 2



GW403781



MONITORING BORE


Work Type: Bore


Construct.Method: Rotary Mud

Owner Type: Private


Contractor Name: AQUA DRILLING & GROUTING PTY LTD

Driller: Lee Anthony Strutton

Assistant Driller: Jamie McKenna

Property: WAGGA WAGGA QUARRY ROACH ROAD WAGGA WAGGA 2650



Site Details

Site Chosen By:

County Parish CadastreForm A: WYNYA WYNYA.38 B//381991

Licensed:








(m)To(m)


Inside Diameter(mm)

Interval Details

1 Hole Hole 0.00 27.50 200 Rotary Mud1 Annulus Waterworn/Rounded 6.00 16.60 Graded1 Annulus Bentonite/Grout 8.00 9.001 1 Casing Pvc Class 18 0.00 9.60 114 100 Screwed1 1 Opening Slots - Horizontal 9.60 15.60 114 1 Casing - Machine Slotted, PVC

Class 18, Screwed1 1 Casing Pvc Class 18 15.60 16.60 114 100 Screwed, S: 15.60-16.60m

Water Bearing Zones

Page 1 of 2


From(m)

To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

9.00 27.50 18.50 Unknown 9.00


To(m)

Thickness(m)


0.00 1.50 1.50 SILT Silt1.50 11.00 9.50 CLAY Clay

11.00 13.00 2.00 SAND AND GRAVEL Sand13.00 25.00 12.00 GRAVEL AND SAND Gravel

Remarks

20/09/2007: Form A Remarks: ENTERED BY PATRICIA EWERS 4TH OCTOBER 2007

BORE WG 0707 (1 OF 7 MONITORING BORES)

STRATA DETAILS TAKEN FROM GRAPHIC LOG PROVIDED BY CONSULTANT

INFORMATION NOT PROVIDED ON FORM:

NO INFORMATION ON YIELD AND DRAWDOWN LEVEL NO INFORMATION ON SALINITY AND WATER TASTE NO INFORMATION ON PUMPING TESTS ON BORE COMPLETION

*** End of GW403781 ***



Page 2 of 2



GW403780



MONITORING BORE


Work Type: Bore



Owner Type: Private








Site Details

Site Chosen By:


Licensed:








(m)To(m)


Inside Diameter(mm)

Interval Details

1 Hole Hole 0.00 30.00 200 Rotary Mud1 Annulus Bentonite/Grout 5.00 6.001 Annulus Waterworn/Rounded 6.00 16.50 Graded1 1 Casing Pvc Class 18 0.00 9.50 114 100 Screwed1 1 Opening Slots - Horizontal 9.50 15.50 114 1 Casing - Machine Slotted, PVC


Water Bearing Zones

Page 1 of 2


From(m)

To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

9.00 30.00 21.00 Unknown 9.00


To(m)

Thickness(m)


0.00 2.00 2.00 SILT Silt2.00 8.00 6.00 SAND AND GRAVEL Sand8.00 9.00 1.00 GRAVEL AND SAND Gravel9.00 12.00 3.00 SILT Silt

12.00 22.00 10.00 SAND AND GRAVEL Sand22.00 29.60 7.60 SAND Sand29.60 30.00 0.40 BASEMENT Invalid Code

Remarks

20/09/2007: Form A Remarks: ENTERED BY PATRICIA EWERS 3RD OCTOBER 2007


STRATAT DETAIL TAKEN FROM GRAPHIC LOG PROVIDED BY CONSULTANT

INFORMATION NOT PROVIDED ON FORM:-


*** End of GW403780 ***



Page 2 of 2



GW403776



MONITORING BORE


Work Type: Bore



Owner Type: Private








Site Details

Site Chosen By:


Licensed:








(m)To(m)


Inside Diameter(mm)

Interval Details

1 Hole Hole 0.00 24.00 200 Rotary Mud1 Annulus Waterworn/Rounded 12.00 20.00 Graded1 1 Casing Pvc Class 18 0.00 9.00 114 100 Screwed, S: 15.00-16.00m1 1 Opening Slots - Horizontal 9.00 15.00 114 1 Casing - Machine Slotted, PVC

Class 18, Screwed


To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Duration(hr)

Salinity(mg/L)

Page 1 of 2


Hole Depth(m)

9.00 24.00 15.00 Unknown 9.00


To(m)

Thickness(m)


0.00 8.00 8.00 SILT Silt8.00 9.00 1.00 SANDY SILT Invalid Code9.00 10.00 1.00 SAND Sand

10.00 24.00 14.00 GRAVEL AND SAND Gravel

Remarks

20/09/2007: Form A Remarks: ENTERED BY PATRICIA EWERS 3RD OCTOBER 2007


STRATA INFORMATION TAKEN FROM GRAPHIC LOG PROVIDED BY CONSULTANT



*** End of GW403776 ***



Page 2 of 2



GW403775



MONITORING BORE


Work Type: Bore



Owner Type: Private








Site Details

Site Chosen By:


Licensed:








(m)To(m)


Inside Diameter(mm)

Interval Details

1 Hole Hole 0.00 30.00 200 Rotary Mud1 Annulus Waterworn/Rounded 12.00 20.00 Graded1 1 Casing Pvc Class 18 0.00 13.00 114 100 Screwed1 1 Opening Slots - Horizontal 13.00 19.00 114 1 Casing - Machine Slotted, PVC


Water Bearing ZonesWBZ Type

Page 1 of 2


From(m)

To(m)

Thickness(m)

S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

9.00 30.00 21.00 Unknown 9.00


To(m)

Thickness(m)


0.00 2.00 2.00 SILT Silt2.00 8.00 6.00 SANDY SILT Invalid Code8.00 11.00 3.00 SAND Sand

11.00 13.00 2.00 GRAVEL AND SAND Gravel13.00 16.00 3.00 SAND Sand16.00 30.00 14.00 GRAVEL AND SAND Gravel

Remarks

03/10/2007: Form A Remarks: ENTERED BY PATRICIA EWERS ON 3RD OCTOBER 2007

DETAILS FOR BORE WG0701 (1 OF 7 MONITORING BORES)

STRATA DETAIL OBTAINED FROM GRAPHIC LOG PROVIDED BY CONSULTANT


NO INFORMATION ON YIELD AND DRAWDOWN LEVEL NO INFORMATION ON SALINITY OR WATER TASTE NO INFORMATION ON PUMPING TESTS ON BORE COMPLETION NO INFORMATION ON WHO CHOSE BORE LOCATION

*** End of GW403775 ***



Page 2 of 2



GW403648



STOCK

Intended Purpose(s):

Work Type: Bore


Construct.Method: Auger - Hollow Flight

Owner Type: Private


Contractor Name: Leo Murray MOLONEY

Driller: Leo Murray Moloney

Assistant Driller:

Property: TS & CR 34463 STURT HIGHWAY YARRAGUNDRY VIA WAGGA WAGGA 2650


6.000

GWMA: - Salinity:GW Zone: - Yield:

Site Details

Site Chosen By:

County Parish CadastreForm A: MITCH MITCH.33 LOT 207

DP754567Licensed: MITCHELL URANQUINTY Whole Lot

207//754567


Area/District:



GS Map: - MGA Zone: 0 Coordinate Source: GIS - Geographic Information System


(m)To(m)


Inside Diameter(mm)

Interval Details

1 Hole Hole 0.00 13.30 900 Auger - Hollow Flight1 Annulus Waterworn/Rounded 6.00 13.30 Graded, Q:4.000m3,

PL:Poured/Shovelled1 1 Casing Pvc Class 9 0.00 13.30 164 150 Seated on Bottom, Glued1 1 Opening Slots - Horizontal 10.90 12.80 164 1 Casing - Hand Sawn Slot, PVC

Class 9, Glued, SL: 100.0mm, A: 5.00mm

Page 1 of 2



To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

10.90 22.80 11.90 Unknown 6.00


To(m)

Thickness(m)


0.00 0.30 0.30 TOPSOIL Topsoil0.30 6.00 5.70 BROWN CLAY Clay6.00 10.30 4.30 GREY BROWN CLAY Invalid Code

10.30 10.90 0.60 STIFF BROWN CLAY Invalid Code10.90 12.80 1.90 CLEAN GREY GRAVEL Invalid Code12.80 13.30 0.50 SILTY GRAVEL Invalid Code

Remarks

*** End of GW403648 ***



Page 2 of 2



GW403437



STOCK,DOMESTIC

Intended Purpose(s): TEST BORE

Work Type: Bore

Work Status:Construct.Method:

Owner Type:


Contractor Name: STRATHMERTON DRILLING PTY LTD

Driller: Gordon George Chatterton

Assistant Driller:

Property: PARAFIELD CLOUGHS ROAD YARRAGUNDRY VIA WAGGA WAGGA 2650


29.000

GWMA: - Salinity:GW Zone: - Yield: 0.400

Site Details

Site Chosen By:

County Parish CadastreForm A: MITCH MITCH.39 59 754573

Licensed: MITCHELL YARRAGUNDRY Whole Lot 59//754573


Area/District:



GS Map: - MGA Zone: 0 Coordinate Source: Map Interpretation


(m)To(m)


Inside Diameter(mm)

Interval Details

1 Hole Hole 0.00 58.00 200 Rotary Mud1 Annulus Waterworn/Rounded 45.00 48.001 1 Casing P.V.C. 0.00 53.00 130 Screwed1 1 Opening Slots 53.00 54.00 130 1 Stainless Steel1 1 Opening Slots 57.00 58.00 130 1 Stainless Steel


To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Duration(hr)

Salinity(mg/L)

Page 1 of 2


Hole Depth(m)

53.00 58.00 5.00 Unknown 29.00 04:00:00


To(m)

Thickness(m)


0.00 2.00 2.00 Sand, dry Sand2.00 53.00 51.00 Clay, pink granite Clay

53.00 58.00 5.00 Granite, decomposed Granite

Remarks

*** End of GW403437 ***



Page 2 of 2



GW403324



STOCK,DOMESTIC


Work Type: Bore


Owner Type:


Contractor Name: BRIAN DAYMAN

Driller: Brian Keith Dayman

Assistant Driller:

Property: N/A 75 CLOUGHS ROAD YARRAGUNDRY VIA WAGGA WAGGA 2650


6.300


Site Details

Site Chosen By:

County Parish CadastreForm A: MITCH MITCH.33 LT1 DP33709

Licensed: MITCHELL URANQUINTY Whole Lot 1//33709


River Basin: - Unknown Grid Zone: Scale:Area/District:


Source:(Unknown) Easting: 522558.0 Longitude: 147°14'51.3"E



(m)To(m)


Inside Diameter(mm)

Interval Details

1 Hole Hole 0.00 39.00 280 Rotary Mud1 1 Casing Pvc Class 12 0.00 16.00 165 135 Suspended in Clamps, Glued1 1 Opening Slots 16.00 19.00 165 1 PVC Class 121 1 Casing Pvc Class 12 19.00 19.50 165 135 Glued


To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

16.00 19.00 3.00 Unknown 6.30 12.00 1.50 15.00 04:00:00

Page 1 of 2



To(m)

Thickness(m)


0.00 2.00 2.00 Clay, grey Clay2.00 14.00 12.00 Clay, brown Clay

14.00 16.00 2.00 Clay, grey Clay16.00 19.00 3.00 Gravel, river Gravel19.00 20.00 1.00 Granite, white Granite20.00 34.00 14.00 Granite Granite34.00 35.00 1.00 Rock, hard Rock35.00 38.00 3.00 Granite, white Granite38.00 39.00 1.00 Rock, solid, hard Rock

Remarks

27/04/2005: Form A Remarks: Good supply shallow bore.

*** End of GW403324 ***



Page 2 of 2



GW402526



STOCK,DOMESTIC


Work Type: Bore

Work Status:Construct.Method: Auger - Solid Flight

Owner Type:



Assistant Driller:

Property: N A 191 ROACH ROAD WAGGA WAGGA 2650


6.000


Site Details

Site Chosen By:

County Parish CadastreForm A: WYNYA WYNYA.038 LT289 DP757249

Licensed: WYNYARD SOUTH WAGGA WAGGA

Whole Lot 92//1061888






Map Interpretation


(m)To(m)


Inside Diameter(mm)

Interval Details

1 Hole Hole 0.00 12.72 900 Auger - Solid Flight1 Annulus Waterworn/Rounded 5.10 12.70 Graded, Q:4.000m31 1 Casing Pvc Class 9 0.00 12.70 125 115 Seated on Bottom, Glued1 1 Opening Slots - Horizontal 7.80 12.60 130 1 Casing - Machine Slotted, PVC

Class 9, SL: 50.0mm, A: 5.00mm


Page 1 of 2


From(m)

To(m)

Thickness(m)

S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

6.30 11.80 5.50 Unknown 6.00 7.03 7.65 04:00:00


To(m)

Thickness(m)


0.00 0.30 0.30 Topsoil Topsoil0.30 3.00 2.70 Clay, black Clay3.00 6.00 3.00 Clay, yellow grey Clay6.00 6.30 0.30 Gravel, and clay Gravel6.30 9.00 2.70 Gravel, clean Gravel9.00 10.60 1.60 Sand, fine grey Sand

10.60 11.80 1.20 Gravel, clean Gravel11.80 12.70 0.90 Gravel, silty Gravel

Remarks

*** End of GW402526 ***



Page 2 of 2



GW402141



STOCK,DOMESTIC


Work Type: Bore

Work Status:Construct.Method: Auger

Owner Type:



Assistant Driller:

Property: N/A 191 ROACH ROAD WAGGA WAGGA 2650


7.800


Site Details

Site Chosen By:

County Parish CadastreForm A: WYNYA WYNYA.038 LT289 DP757249


Whole Lot 91//1061888






Map Interpretation


(m)To(m)


Inside Diameter(mm)

Interval Details

1 Hole Hole 0.00 12.10 900 Auger1 Annulus Waterworn/Rounded 6.00 12.10 Graded, Q:4.000m31 1 Casing Pvc Class 9 0.00 11.80 160 150 Seated on Bottom, Glued1 1 Opening Slots - Horizontal 9.70 11.50 160 1 Mechanically Slotted, PVC

Class 9, SL: 100.0mm, A: 4.00mm


Page 1 of 2


From(m)

To(m)

Thickness(m)

S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

9.60 11.80 2.20 Unknown 7.80 8.70 7.00 02:00:00


To(m)

Thickness(m)


0.00 0.30 0.30 Topsoil Topsoil0.30 9.00 8.70 Clay, yellow brown Clay9.00 9.60 0.60 Sandy clay, light grey Invalid Code9.60 11.80 2.20 Sand, clean grey tending to river

gravelSand

11.80 12.10 0.30 Clay, silty grey Clay

Remarks

*** End of GW402141 ***



Page 2 of 2



GW402132



IRRIGATION,FARMING

Intended Purpose(s): IRRIGATION

Work Type: Bore

Work Status:Construct.Method: Rotary

Owner Type:


Contractor Name: watson drilling

Driller: David Wilton Watson

Assistant Driller:

Property: POMINGALARANA WAGGA WAGGA 2650


9.000

GWMA: 013 - MID MURRUMBIDGEE (U/S NARRANDERA)

Salinity:

GW Zone: - Yield: 54.000

Site Details

Site Chosen By:

County Parish CadastreForm A: MITCH MITCH.033 LTPT1 DP754567








(m)To(m)


Inside Diameter(mm)

Interval Details

1 Hole Hole 0.00 43.00 300 Rotary Mud1 Hole Hole 43.00 63.50 225 Rotary Mud1 1 Casing Pvc Class 12 0.00 43.00 300 Heat Shrunk1 1 Opening Screen - Wire

Wound43.00 44.00 225 1 Stainless Steel, Welded, A: 1.75mm

1 1 Opening Screen - Wire Wound

44.00 47.00 225 1 Stainless Steel, Welded, A: 2.00mm

1 1 Casing Pvc Class 12 47.00 53.00 225 Heat Shrunk1 1 Opening Screen - Wire

Wound53.00 54.00 225 1 Stainless Steel, Welded, A: 2.25mm

Page 1 of 2









To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

43.00 47.00 4.00 Unknown 9.00 17.0053.00 63.50 10.50 Unknown 9.00 17.00


To(m)

Thickness(m)


0.00 0.30 0.30 Topsoil, sandy Topsoil0.30 6.00 5.70 Sandy clay Invalid Code6.00 7.00 1.00 Sandy clay, with ill sorted stones Invalid Code7.00 20.00 13.00 Gravel, river with large stones Gravel

20.00 21.00 1.00 Clay, with rocks Clay21.00 23.00 2.00 Clay, brown Clay23.00 25.00 2.00 Clay, dark brown Clay25.00 29.00 4.00 Sand, clay bound, brown Sand29.00 32.00 3.00 Sand, clay bound, grey brown Sand32.00 33.00 1.00 Sand, medium Sand33.00 34.00 1.00 Sand, clay bound, soft Sand34.00 38.00 4.00 Clay, silty grey Clay38.00 41.00 3.00 Sand, silty Sand41.00 42.00 1.00 Sand, grey Sand42.00 43.00 1.00 Sand, grey, dirty Sand43.00 44.00 1.00 Sand, grey, dirty Sand44.00 45.00 1.00 Sand, grey Sand45.00 46.00 1.00 Sand, with clay layer Sand46.00 47.00 1.00 Sand Sand47.00 50.00 3.00 Clay, grey Clay50.00 52.00 2.00 Clay, grey and brown Clay52.00 53.00 1.00 Sand, clean, medium Sand53.00 63.00 10.00 Sand, clean Sand63.00 63.50 0.50 Sand, coarser Sand63.50 65.00 1.50 Clay, light grey Clay65.00 68.00 3.00 Rock, decomposed, red grey Rock

Remarks

*** End of GW402132 ***



Page 2 of 2



GW401710



IRRIGATION

Intended Purpose(s):

Work Type: Bore


Owner Type:

Commenced Date: Final Depth: 14.00 mCompletion Date: 31/03/1997 Drilled Depth:

Contractor Name: DAN MOLONEY WELL DRILLING

Driller:Assistant Driller:

Property: PARAFIELD OLIVES CLOUGHS ROAD YARRAGUNDRY 2650 NSW


5.000


Site Details

Site Chosen By:

County Parish CadastreForm A: MITCH MITCH.033 23

Licensed: MITCHELL YARRAGUNDRY Whole Lot 17//1124011


Area/District:





(m)To(m)


Inside Diameter(mm)

Interval Details

1 Hole Hole 0.00 14.00 152 (Unknown)1 1 Casing Pvc Class 9 0.00 14.00 1521 1 Opening Slots 11.00 14.00 152 1 PVC Class 9


To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

11.00 14.00 3.00 Unknown 5.00 11.00 2.30

Page 1 of 2



To(m)

Thickness(m)


Remarks

*** End of GW401710 ***



Page 2 of 2



GW400462



MONITORING BORE

Intended Purpose(s): MONITORING BORE, TEST BORE

Work Type: Bore


Owner Type:


Contractor Name: DWR - GROUNDWATER DRILLING


Property: N/A 2650 Standing Water Level:


Site Details

Site Chosen By:

County Parish CadastreForm A: WYNYA WYNYA.038 SALINITY BORE

FIELDLicensed: WYNYARD SOUTH WAGGA

WAGGAWhole Lot //








(m)To(m)


Inside Diameter(mm)

Interval Details

1 Hole Hole 0.00 17.00 50 Unknown1 1 Casing P.V.C. -0.72 17.00 501 1 Opening Slots 15.00 17.00 50 1 PVC


To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

Page 1 of 2



To(m)

Thickness(m)


0.00 2.00 2.00 Topsoil & light brown silty loam Unknown2.00 8.50 6.50 Clay Unknown8.50 10.00 1.50 Clay Unknown

10.00 14.00 4.00 Clay Unknown14.00 15.00 1.00 Clay Unknown15.00 17.00 2.00 Clay Unknown

Remarks

*** End of GW400462 ***



Page 2 of 2



GW400458



MONITORING BORE

Intended Purpose(s): MONITORING BORE, TEST BORE

Work Type: Bore


Owner Type:


Contractor Name: DWR - GROUNDWATER DRILLING


Property: N/A 2650 Standing Water Level:


Site Details

Site Chosen By:

County Parish CadastreForm A: WYNYA WYNYA.038 SALINITY BORE

FIELDLicensed: WYNYARD SOUTH WAGGA

WAGGAWhole Lot //








(m)To(m)


Inside Diameter(mm)

Interval Details

1 Hole Hole 0.00 11.00 50 Unknown1 1 Casing P.V.C. -0.68 11.00 501 1 Opening Slots 9.00 11.00 50 1 PVC


To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

Page 1 of 2



To(m)

Thickness(m)


0.00 0.20 0.20 Garden Fill Unknown0.20 1.00 0.80 Clay Unknown1.00 2.00 1.00 Silty Clay Unknown2.00 3.00 1.00 Silty Clay Unknown3.00 5.00 2.00 Silt Unknown5.00 10.00 5.00 Silt Unknown

10.00 11.00 1.00 As for 5-10 but saturated Unknown

Remarks

*** End of GW400458 ***



Page 2 of 2



GW051051

Licence: 40BL110501 Licence Status: CANCELLED


TEST BORE

Intended Purpose(s): RECREATION (GROUNDWATER)

Work Type: Bore

Work Status: Test Hole

Construct.Method: Rotary

Owner Type: Private


Contractor Name:Driller:

Assistant Driller:

Property: N/A Standing Water Level (m):

GWMA: - Salinity Description: FairGW Zone: - Yield (L/s):

Site Details

Site Chosen By:

County Parish CadastreForm A: WYNYA WYNYA.038 300


Whole Lot //


River Basin: 410 - MURRUMBIDGEE RIVER

Grid Zone: Scale:

Area/District:




GD.,ACC.MAP


(m)To(m)


Inside Diameter(mm)

Interval Details

1 1 Casing Withdrawn 0.00 0.00 102


To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

10.00 14.00 4.00 Unconsolidated 6.4014.00 16.00 2.00 Unconsolidated

Page 1 of 2



To(m)

Thickness(m)


0.00 0.50 0.50 Clay Soil Clay0.50 1.00 0.50 Clay Dark Brownish Clay1.00 2.00 1.00 Clay Light Greyish Clay2.00 5.50 3.50 Clay Clay5.50 7.50 2.00 Clay Light Brownish Grey Streaks Clay7.50 9.00 1.50 Clay Light Greyish Brown Streaks Clay9.00 10.00 1.00 Clay Grey Silty Fine Sand Clay

10.00 14.00 4.00 Sand Medium-coarse Sand14.00 16.00 2.00 Sand Fine Medium-coarse Free Water

BearingSand

16.00 19.00 3.00 Clay Grey Clay19.00 23.00 4.00 Clay Dark Greyish Silty Clay23.00 24.00 1.00 Slate Decomposed Slate10.00 14.00 4.00 Gravel Large Water Bearing Gravel

Remarks

*** End of GW051051 ***



Page 2 of 2



GW044828



STOCK,DOMESTIC


Work Type: Bore

Work Status:Construct.Method: Rotary

Owner Type: Private



Assistant Driller:


GWMA: - Salinity Description: GoodGW Zone: - Yield (L/s):

Site Details

Site Chosen By:


Licensed: MITCHELL URANQUINTY Whole Lot //



Grid Zone: Scale:

Area/District:




GD.,ACC.MAP


(m)To(m)


Inside Diameter(mm)

Interval Details

1 1 Casing Threaded Steel -0.20 36.90 152 Seated on Bottom1 1 Opening Slots 30.80 36.90 152 1


To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

20.10 36.90 16.80 Unconsolidated 19.50 0.51

Page 1 of 2



To(m)

Thickness(m)


0.00 0.30 0.30 Topsoil Topsoil0.30 29.87 29.57 Clay Sand Water Supply Clay

29.87 36.88 7.01 Gravel Water Supply Gravel

Remarks

*** End of GW044828 ***



Page 2 of 2



GW030269

Licence: Licence Status:



Work Type: Bore

Work Status: Manual Observations,Monthly


Owner Type: NSW Office of Water



Assistant Driller:

Property: Standing Water Level (m):

GWMA: Salinity Description: 0-500 ppmGW Zone: Yield (L/s):

Site Details

Site Chosen By:

County Parish CadastreForm A: MITCHELL URANQUINTRY 1//1090274

Licensed:



Grid Zone: Scale:

Area/District:


Source:(unknown) Easting: 523286.000 Longitude: 147°15'19.9"E

GS Map: - MGA Zone: 55 Coordinate Source: GPS - Global


(m)To(m)


Inside Diameter(mm)

Interval Details

1 1 Casing Threaded Steel -1.20 23.80 2031 Casing Casing

Protector-1.10 0.00

1 1 Opening Slots 12.90 18.60 203 1


To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

11.50 24.30 12.80 Unconsolidated 7.60 1.36

Page 1 of 2


Drillers LogFrom(m)

To(m)

Thickness(m)


0.00 0.61 0.61 Topsoil Topsoil0.61 11.58 10.97 Clay Clay

11.58 24.38 12.80 Gravel Large Stones Coarse Water Supply

Gravel

Remarks

14/04/1976: B/N 30268 ADJ HAS GEOL LOG. 09/05/1979: POMINGALARNA. 03/12/2001: GPS COORDS TAKEN 15/10/01 - OLD COORDS 522998/6114527. 19/01/2009: Nat Carling, 19-Jan-2009: Updated RL's, casing protector details (based on RL's) & cadastre (was entered as '3'), as provided in State Water Survey database.

*** End of GW030269 ***



Page 2 of 2



GW030268




Work Type: Bore

Work Status: Manual Observations,Monthly

Construct.Method: Cable Tool




Assistant Driller:


GWMA: Salinity Description: 0-500 ppmGW Zone: Yield (L/s):

Site Details

Site Chosen By:

County Parish CadastreForm A: MITCHELL URANQUINTRY 1//1090274

Licensed:



Grid Zone: Scale:

Area/District:





(m)To(m)


Inside Diameter(mm)

Interval Details

1 Backfill Backfill 97.00 97.90 1271 Casing Casing

Protector-0.79 0.00

1 1 Casing Threaded Steel -0.70 97.00 1271 1 Casing Withdrawn 0.00 2.90 1331 1 Casing Withdrawn 0.00 96.60 2031 1 Opening Slots 79.20 82.20 127 1 A: 3.17mm1 1 Opening Slots 88.30 91.30 127 2 A: 3.17mm

Water Bearing Zones

Page 1 of 3


From(m)

To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

11.50 24.90 13.40 Unconsolidated 7.7025.20 39.80 14.60 Unconsolidated 8.2045.70 60.30 14.60 Unconsolidated 13.70 1.0661.50 63.60 2.10 Unconsolidated77.70 94.10 16.40 Unconsolidated 7.90 0.91

Drillers LogFrom(m)

To(m)

Thickness(m)


0.00 0.61 0.61 Topsoil Topsoil0.61 3.05 2.44 Loam Sandy Loam3.05 4.57 1.52 Silt Sandy Silt4.57 6.40 1.83 Clay Grey Clay6.40 11.58 5.18 Silt Grey Sandy Silt

11.58 14.02 2.44 Gravel Grey Stoney Sand Coarse Water Supply

Gravel

14.02 17.07 3.05 Gravel Sand Water Supply Gravel17.07 24.38 7.31 Gravel Stoney Water Supply Gravel24.38 24.99 0.61 Gravel Yellow Silty Sand Fine Water

SupplyGravel

24.99 25.30 0.31 Clay Grey Clay25.30 30.78 5.48 Gravel Yellow Stoney Sand Coarse

Water SupplyGravel

30.78 33.22 2.44 Gravel Yellow Silty Sand Coarse Water Supply

Gravel

33.22 35.66 2.44 Sand Yellow Silty Fine-coarse Water Supply

Sand

35.66 37.49 1.83 Gravel Fine Water Supply Gravel37.49 38.71 1.22 Sand Purple Silty Fine Water Supply Sand38.71 39.93 1.22 Sand Purple Coarse Water Supply Sand39.93 40.23 0.30 Clay Grey Clay40.23 45.11 4.88 Silt Silt45.11 45.72 0.61 Clay Black Clay45.72 48.77 3.05 Sand Yellow Fine Water Supply Sand48.77 50.60 1.83 Gravel Coarse Water Supply Gravel50.60 54.25 3.65 Sand Yellow Very Coarse Water

SupplySand

54.25 60.35 6.10 Sand Cream Sand Coarse Water Supply

Sand

60.35 61.57 1.22 Clay Grey Silty Clay61.57 62.79 1.22 Sand Yellow Coarse Water Supply Sand62.79 63.70 0.91 Sand Grey Coarse Water Supply Sand63.70 65.53 1.83 Clay Grey Sandy Clay65.53 71.32 5.79 Clay Light Grey Sandy Clay71.32 74.68 3.36 Clay Grey Clay74.68 77.72 3.04 Silt Sandy Silt77.72 81.99 4.27 Sand White Coarse Water Supply Sand81.99 85.65 3.66 Sand White Silty Coarse Water

SupplySand

85.65 86.87 1.22 Silt White Sandy Water Supply Silt86.87 91.14 4.27 Gravel Coarse Water Supply Gravel91.14 94.18 3.04 Sand Silty Fine-coarse Water Supply Sand94.18 97.84 3.66 Granite Decomposed Granite17.07 24.38 7.31 Sand Silty Sand30.78 33.22 2.44 Clay Bands Clay35.66 37.49 1.83 Clay Bands Clay45.72 48.77 3.05 Gravel Medium Gravel48.77 50.60 1.83 Sand Yellow Sand86.87 91.14 4.27 Sand White Silty Water Supply Sand

Remarks

09/12/1978: POMINGALARNA. 03/12/2001: GPS COORDS TAKEN 15/10/01 - OLD COORDS 522998/6114527. 19/01/2009: Nat Carling, 19-Jan-2009: Updated RL's, casing protector details (based on RL's) & cadastre (was entered as '3'), as provided in State Water Survey database. 07/05/2012: Karla Abbs, 7-May-2012: Entered geology log24/10/2014: M.Debono, deleted measurement taken on 03/02/2004 as 7.96m recorded, incorrect based on measurements obtained in Jan and March 2004..

Page 2 of 3


*** End of GW030268 ***



Page 3 of 3



GW030065




Work Type: Bore - Nested (2)

Work Status: Manual Observations,6-12 Months





Assistant Driller:


GWMA: Salinity Description:GW Zone: Yield (L/s):

Site Details

Site Chosen By:

County Parish CadastreForm A: MITCHELL URANQUINTRY 13

Licensed:



Grid Zone: Scale:

Area/District:





(m)To(m)


Inside Diameter(mm)

Interval Details

1 Casing Casing Protector

-0.95 1.40 203

1 1 Casing P.V.C. -0.30 21.00 631 1 Opening Slots 16.70 18.20 63 1 Slotted On Site1 1 Opening Slots 19.80 21.30 63 1 Slotted On Site1 Casing Casing

Protector-0.95 1.40 203

1 2 Casing P.V.C. -0.30 57.60 631 2 Casing Withdrawn 0.00 60.00 2031 2 Opening Slots 42.60 45.60 63 3 Slotted On Site1 2 Opening Slots 54.80 57.80 63 4 Slotted On Site

Page 1 of 2



To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

12.80 21.30 8.50 Unconsolidated 6.4040.20 60.30 20.10 Unconsolidated 8.20

Drillers LogFrom(m)

To(m)

Thickness(m)


0.00 0.60 0.60 Topsoil Topsoil0.60 6.70 6.10 Clay Sandy Clay6.70 8.53 1.83 Stones Large Sand Gravel Coarse Gravel8.53 11.58 3.05 Sand Gravel Coarse Stones Sand

11.58 12.80 1.22 Clay Silty Gravel Clay12.80 14.02 1.22 Sand Gravel Coarse Water Supply

StonesSand

14.02 15.24 1.22 Sand Grey Gravel Coarse Water Supply Stones

Sand

15.24 21.33 6.09 Sand Grey Gravel Coarse Water Supply Boulders

Sand

21.33 28.65 7.32 Sand Silty Clay Stones Sand28.65 32.61 3.96 Clay Silty Clay32.61 33.52 0.91 Clay Silty Sandy Clay33.52 34.74 1.22 Clay Silty Clay34.74 35.35 0.61 Clay Clay35.35 38.40 3.05 Clay Silty Sandy Clay38.40 40.84 2.44 Sand Silty Water Supply Stones Sand40.84 54.86 14.02 Sand Grey Coarse Water Supply Sand54.86 55.47 0.61 Gravel Grey Fine Water Supply Gravel55.47 58.52 3.05 Gravel Fine-medium Water Supply Gravel58.52 60.35 1.83 Sand Gravel Coarse Water Supply Sand60.35 61.56 1.21 Clay Sandy Clay61.56 62.78 1.22 Clay Clay62.78 64.61 1.83 Clay Grey Sticky Clay64.61 67.66 3.05 Clay Sticky Clay67.66 68.88 1.22 Clay Grey Clay68.88 75.59 6.71 Granite Decomposed Granite

Remarks

14/04/1976: 2 PVCS INSERTED IN ONE HOLE. 09/05/1979: POMINGALARNA. 03/12/2001: GPS COORDS TAKEN 15/10/01 - OLD COORDS 523999/6115269. 20/04/2009: Nat Carling, 20-Apr-2009: Updated RL's & casing protector details (based on RL's), as provided in State Water Survey database. 15/03/2012: Karla Abbs, 15-Mar-2012: Entered geology log

*** End of GW030065 ***



Page 2 of 2



GW030055




Work Type: Bore - Nested (3)

Work Status: Manual Observations,6-12 Months





Assistant Driller:


GWMA: Salinity Description:GW Zone: Yield (L/s):

Site Details

Site Chosen By:

County Parish CadastreForm A: MITCHELL URANQUINTRY 13

Licensed:



Grid Zone: Scale:

Area/District:





(m)To(m)


Inside Diameter(mm)

Interval Details


-1.11 1.40 203

1 1 Casing P.V.C. -0.30 14.90 631 1 Opening Slots 9.10 15.10 63 1 Slotted On Site1 Casing Casing

Protector-1.11 1.40 203

1 2 Casing P.V.C. -0.30 45.40 631 2 Opening Slots 39.60 45.60 63 2 Slotted On Site1 Casing Casing

Protector-1.11 1.40 203

1 3 Casing P.V.C. -0.30 61.80 63

Page 1 of 3


1 3 Casing Withdrawn 0.00 69.10 2031 3 Opening Slots 56.00 62.00 63 3 Slotted On Site


To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

10.90 20.60 9.70 Unconsolidated 7.1032.30 48.10 15.80 Unconsolidated 6.8048.70 51.10 2.40 Unconsolidated 7.1056.00 63.30 7.30 Unconsolidated 7.60

Drillers LogFrom(m)

To(m)

Thickness(m)


0.00 2.13 2.13 Topsoil Topsoil2.13 3.04 0.91 Loam Sandy Loam3.04 4.87 1.83 Clay Grey Sandy Clay4.87 7.92 3.05 Clay Sandy Clay7.92 9.14 1.22 Sand Silty Sand9.14 10.97 1.83 Sand Silty Gravel Sand

10.97 12.19 1.22 Sand Gravel Coarse Water Supply Stones

Sand

12.19 15.24 3.05 Gravel Stones Coarse Water Supply Gravel15.24 16.45 1.21 Sand Gravel Coarse Water Supply

StonesSand

16.45 17.67 1.22 Gravel Large Water Supply Stones Large

Gravel

17.67 19.50 1.83 Sand Gravel Coarse Water Supply Stones

Sand

19.50 20.72 1.22 Gravel Coarse Water Supply Stones Large Clayey

Gravel

20.72 21.33 0.61 Clay Grey Clay21.33 23.16 1.83 Clay Silty Sandy Clay23.16 24.38 1.22 Clay Gravel Clay24.38 32.30 7.92 Clay Sandy Gravel Clay32.30 39.92 7.62 Sand Grey Coarse Water Supply Sand39.92 40.84 0.92 Basalt Large Boulder Water Supply

SandBasalt

40.84 41.45 0.61 Sand Grey Stones Coarse Water Supply

Sand

41.45 45.72 4.27 Gravel Grey Stones Coarse Water Supply

Gravel

45.72 47.54 1.82 Sand Gravel Coarse Water Supply Stones Large

Sand

47.54 48.15 0.61 Sand Gravel Water Supply Stones Sand48.15 48.76 0.61 Clay Grey Clay48.76 51.20 2.44 Gravel Grey Sand Coarse Water

Supply StonesGravel

51.20 56.08 4.88 Clay Dark Grey Silty Sandy Clay56.08 59.74 3.66 Gravel Grey Fine Water Supply Gravel59.74 62.17 2.43 Sand Gravel Coarse Water Supply

StonesSand

62.17 63.39 1.22 Sand Grey Stones Water Supply Sand63.39 64.00 0.61 Clay Grey Sticky Clay64.00 66.44 2.44 Clay Grey Clay66.44 67.66 1.22 Clay Clay67.66 68.88 1.22 Clay Grey Clay68.88 70.10 1.22 Clay Silty Clay70.10 70.71 0.61 Clay Clay70.71 71.62 0.91 Clay Hard Clay71.62 75.59 3.97 Clay Reddish Clay75.59 80.16 4.57 Clay Red Clay

Remarks

14/04/1976: 3 PVCS INSERTED IN ONE HOLE. 09/05/1979: POMINGALARNA. 03/12/2001: GPS COORDS TAKEN 15/10/01 - OLD COORDS 524250/6115007. 20/04/2009: Nat Carling, 20-Apr-2009: Updated RL's & casing protector details (based on RL's), as provided in State Water Survey database.

Page 2 of 3


15/03/2012: Karla Abbs, 15-mar-2012: Entered geology log

*** End of GW030055 ***



Page 3 of 3



GW029570



STOCK,DOMESTIC

Intended Purpose(s): IRRIGATION

Work Type: Bore


Owner Type: Federal Govt



Assistant Driller:

Property: WERRINGTON Standing Water Level (m):

GWMA: - Salinity Description:GW Zone: - Yield (L/s):

Site Details

Site Chosen By:


Licensed: HARDEN CURRAWONG Whole Lot //



Grid Zone: Scale:

Area/District:




GD.,ACC.MAP


(m)To(m)


Inside Diameter(mm)

Interval Details

1 1 Casing 0.00 26.20 152 Driven into Hole


To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

Geologists Log

Page 1 of 2

19/04/2017http://allwaterdata.water.nsw.gov.au/wgen/users/484649657/gw029570.gwgwpf_org....

Drillers LogFrom(m)

To(m)

Thickness(m)


0.00 0.61 0.61 Silt Silt0.61 4.27 3.66 Clay Sand Clay4.27 5.18 0.91 Clay Gravel Clay5.18 12.19 7.01 Clay Soft Clay

12.19 19.51 7.32 Clay Sandy Clay19.51 23.77 4.26 Clay Soft Clay23.77 27.43 3.66 Sandstone Sandstone27.43 36.58 9.15 Clay Soft Clay36.58 48.77 12.19 Clay Sandstone Clay48.77 54.25 5.48 Clay Shale Sandstone Clay54.25 54.86 0.61 Clay Shale Clay54.86 56.08 1.22 Shale Grey Shale56.08 60.96 4.88 Sandstone Yellow Sandstone60.96 69.49 8.53 Clay Sandstone Clay69.49 71.93 2.44 Clay Sandstone Shale Clay71.93 76.20 4.27 Quartz Cream Clay Quartz

Remarks

*** End of GW029570 ***



Page 2 of 2

19/04/2017http://allwaterdata.water.nsw.gov.au/wgen/users/484649657/gw029570.gwgwpf_org....


GW029569

Licence: 40BL020709 Licence Status: ABANDONED


NOT KNOWN

Intended Purpose(s): NOT KNOWN

Work Type: Bore





Assistant Driller:



Site Details

Site Chosen By:





Grid Zone: Scale:

Area/District:




GD.,ACC.MAP


(m)To(m)


Inside Diameter(mm)

Interval Details


0.00 0.00

1 1 Casing Threaded Steel 0.00 51.80 152 Driven into Hole


To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

Page 1 of 2



To(m)

Thickness(m)


0.00 6.10 6.10 Topsoil Gravel Topsoil6.10 9.14 3.04 Clay Red Gravel Clay9.14 12.19 3.05 Clay Gravel Clay

12.19 15.85 3.66 Clay Red Gravel Clay15.85 17.07 1.22 Gravel Coarse Gravel17.07 19.20 2.13 Clay Clay19.20 21.34 2.14 Granite Decomposed Granite21.34 23.16 1.82 Gravel Gravel23.16 35.05 11.89 Clay Red Clay35.05 47.24 12.19 Clay Gravel Clay47.24 84.12 36.88 Shale Black Shale84.12 91.44 7.32 Shale Black Clay Shale

Remarks

12/06/1981: ARMY TRAINING IN BORING

*** End of GW029569 ***



Page 2 of 2



GW029568



RECREATION (GROUNDWATER)

Intended Purpose(s): NOT KNOWN

Work Type: Bore open thru rock





Assistant Driller:



Site Details

Site Chosen By:





Grid Zone: Scale:

Area/District:




GD.,ACC.MAP


(m)To(m)


Inside Diameter(mm)

Interval Details

1 1 Casing Threaded Steel 0.00 36.60 152 Driven into Hole


To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

73.20 86.60 13.40 Fractured 67.10 0.30

Page 1 of 2



To(m)

Thickness(m)


0.00 6.10 6.10 Clay Gravel Clay6.10 22.86 16.76 Clay Sand Clay

22.86 25.91 3.05 Clay Clay25.91 42.67 16.76 Clay Red Clay42.67 51.82 9.15 Clay Yellow Clay51.82 54.86 3.04 Clay Gravel Clay54.86 73.76 18.90 Clay Yellow Clay73.76 86.26 12.50 Shale Black Water Supply Shale86.26 86.56 0.30 Shale Black Water Supply Shale

Remarks

12/06/1981: ARMY TRAINING IN BORING

*** End of GW029568 ***



Page 2 of 2



GW020231

Licence: 40BL013278 Licence Status: ABANDONED


DOMESTIC

Intended Purpose(s): DOMESTIC

Work Type: Well


Owner Type: Private



Assistant Driller:



Site Details

Site Chosen By:



Whole Lot //



Grid Zone: Scale:

Area/District:




GD.,ACC.MAP


(m)To(m)


Inside Diameter(mm)

Interval Details

1 1 Casing Concrete Cylnder

0.00 0.00 914


To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

5.70 5.70 0.00 Unconsolidated 1.20 0.76

Page 1 of 2



To(m)

Thickness(m)


0.00 4.57 4.57 Clay Clay4.57 7.31 2.74 Gravel River Water Supply Gravel

Remarks

*** End of GW020231 ***



Page 2 of 2



GW020218



STOCK,DOMESTIC

Intended Purpose(s): GENERAL USE

Work Type: Well





Assistant Driller:

Property: RIVER PARK 86 ROACH ROAD WAGGA WAGGA 2650

Standing Water Level (m):


Site Details

Site Chosen By:



Whole Lot 7//1025035



Grid Zone: Scale:

Area/District:




GD.,ACC.MAP


(m)To(m)


Inside Diameter(mm)

Interval Details


-1.00 -1.00 914


To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

6.70 12.80 6.10 Unconsolidated 6.70

Page 1 of 2



To(m)

Thickness(m)


0.00 4.27 4.27 Loam Alluvial Loam4.27 6.71 2.44 Sand Dry Sand6.71 9.75 3.04 Sand Small Stones Water Supply Sand9.75 12.80 3.05 Gravel River Water Supply Gravel

Remarks

*** End of GW020218 ***



Page 2 of 2



GW019674



Intended Purpose(s): STOCK

Work Type: Bore

Work Status:Construct.Method: Cable Tool

Owner Type: Private

Commenced Date: Final Depth: 29.90 mCompletion Date: 01/01/1946 Drilled Depth:


Assistant Driller:


GWMA: Salinity Description: V.SaltyGW Zone: Yield (L/s):

Site Details

Site Chosen By:


Licensed:



Grid Zone: Scale:

Area/District:




GD.,ACC.MAP


(m)To(m)


Inside Diameter(mm)

Interval Details

1 1 Casing Threaded Steel 0.00 29.90 152 Seated on Bottom


To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

Geologists Log

Page 1 of 2


Drillers LogFrom(m)

To(m)

Thickness(m)


Remarks

*** End of GW019674 ***



Page 2 of 2



GW018067



STOCK,DOMESTIC


Work Type: Well


Owner Type: Private



Assistant Driller:



Site Details

Site Chosen By:





Grid Zone: Scale:

Area/District:




PR.,ACC.MAP


(m)To(m)


Inside Diameter(mm)

Interval Details


-0.80 -0.80 914


To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

11.60 16.50 4.90 Unconsolidated 6.10 1.90

Page 1 of 2



To(m)

Thickness(m)


0.00 0.91 0.91 Loam Loam0.91 11.58 10.67 Clay Clay

11.58 16.46 4.88 Sand Clay Water Supply Sand

Remarks

*** End of GW018067 ***



Page 2 of 2



GW018066



STOCK


Work Type: Well


Owner Type: Private



Assistant Driller:



Site Details

Site Chosen By:





Grid Zone: Scale:

Area/District:




GD.,ACC.MAP


(m)To(m)


Inside Diameter(mm)

Interval Details

1 1 Casing Concrete -0.60 -0.60 508


To(m)

Thickness(m)

WBZ Type S.W.L.(m)

D.D.L.(m)

Yield(L/s)

Hole Depth(m)

Duration(hr)

Salinity(mg/L)

16.50 19.90 3.40 Unconsolidated 14.60 1.26

Page 1 of 2



To(m)

Thickness(m)


0.00 16.46 16.46 Loam Clay Loam16.46 19.81 3.35 Sand Gravel Water Supply Sand

Remarks

*** End of GW018066 ***



Page 2 of 2



APPENDIX F Borehole logs


M

Silty CLAYmedium to high plasticity, brown

CLAYmedium to high plasticity, orange

CLAYmedium plasticity, pale grey with some orange

CLAYlow plasticity, pale grey

END OF BOREHOLE @ 4.00 mTARGET DEPTHGROUNDWATER NOT ENCOUNTEREDBACKFILLED

0.40

1.30

2.60

HA

PT

AD

T

0315_BH001_0.0DS 0.00-0.10 mR = 0A

0315_BH001_1.0DS 1.00-1.10 mR = 0A

0315_BH001_2.0DS 2.00-2.10 mR = 0A

0315_BH001_3.0DS 3.00-3.10 mR = 0A

0315_BH001_4.0DS 3.90-4.00 mR = 0A

D

SHEET: 1 OF 1

Field Material DescriptionSamplingDrilling

PE

NE

TR

AT

ION

RE

SIS

TA

NC

E

SOIL/ROCK MATERIAL DESCRIPTION

US

CS

SY

MB

OL

RE

CO

VE

RE

D

WA

TE

R

RLDEPTH

DE

PT

H(m

etre

s)

ME

TH

OD

GR

AP

HIC

LOG

SAMPLE ORFIELD TEST

GAP gINT FN. F01aRL3

CLIENT:

PROJECT:

LOCATION:

JOB NO:

DATE: 15/3/17

DATE: 26/4/17

This report of borehole must be read in conjunction with accompanying notes and abbreviations. It has been prepared forenvironmental purposes only, without attempt to consider geotechnical properties or the geotechnical significance of the materials

encountered. As such it should not be relied upon for geotechnical purposes.

REPORT OF BOREHOLE: BH001

Department of Defence

Defence AFFF Category 2 Site PSI - Kapooka

Kapooka

1669283

COORDS: 526049.0 m E 6110145.0 m N MGA94 56

SURFACE RL: DATUM: AHD

INCLINATION: -90°

HOLE DEPTH: 4.00 m

DRILL RIG: Geoprobe 66200DT

CONTRACTOR: Golder Associates

LOGGED: OB

CHECKED: JND

GA

P 8

_13.

0 LI

B.G

LB L

og G

AP

NO

N-C

OR

ED

FU

LL P

AG

E K

AP

OO

KA

.GP

J <

<D

raw

ingF

ile>

> 2

7/04

/201

7 15

:04

8.3

0.00

2 D

atge

l Too

ls

MO

IST

UR

EC

ON

DIT

ION

CO

NS

IST

EN

CY

DE

NS

ITY

STRUCTURE ANDADDITIONAL

OBSERVATIONS

0.0

0.5

1.0

1.5

2.0

2.5

3.0

3.5

4.0

4.5

5.0

M

H

Silty CLAYmedium to high plasticity, orange brown

CLAYhigh plasticity, orange

CLAYmedium plasticity, pale grey with some orange



0.40

2.60

3.00

HA

PT

AD

T

0315_BH002_0.0DS 0.00-0.10 mR = 0A

0315_BH002_1.0DS 1.00-1.10 mR = 0A

0315_BH002_2.0DS 2.00-2.10 mR = 0A

0315_BH002_3.0DS 3.00-3.10 mR = 0A

0315_BH002_4.0DS 3.90-4.00 mR = 0A

M

D

SHEET: 1 OF 1


PE

NE

TR

AT

ION

RE

SIS

TA

NC

E


US

CS

SY

MB

OL

RE

CO

VE

RE

D

WA

TE

R

RLDEPTH

DE

PT

H(m

etre

s)

ME

TH

OD

GR

AP

HIC

LOG

SAMPLE ORFIELD TEST


CLIENT:

PROJECT:

LOCATION:

JOB NO:

DATE: 15/3/17

DATE: 26/4/17






Kapooka

1669283

COORDS: 526078.0 m E 6110144.0 m N MGA94 56


INCLINATION: -90°

HOLE DEPTH: 4.00 m



LOGGED: OB

CHECKED: JND

GA

P 8

_13.

0 LI

B.G

LB L

og G

AP

NO

N-C

OR

ED

FU

LL P

AG

E K

AP

OO

KA

.GP

J <

<D

raw

ingF

ile>

> 2

7/04

/201

7 15

:04

8.3

0.00

2 D

atge

l Too

ls

MO

IST

UR

EC

ON

DIT

ION

CO

NS

IST

EN

CY

DE

NS

ITY


OBSERVATIONS

0.0

0.5

1.0

1.5

2.0

2.5

3.0

3.5

4.0

4.5

5.0

L

H

H

FILL: Silty CLAYlow plasticity, brown, with some grey shale gravel

CLAYlow to medium plasticity, orange with some grey

CLAYmedium plasticity, grey with some orange

Clayey CLAYmedium to high plasticity, pale grey


0.80

1.60

2.40

HA

PT

AD

T

0315_BH003_0.0DS 0.00-0.10 mR = 0A

0315_BH003_1.0DS 1.00-1.10 mR = 0A

0315_BH003_2.0DS 2.00-2.10 mR = 0A

0315_BH003_3.0DS 3.00-3.10 mR = 0A

0315_BH003_4.0DS 3.90-4.00 mR = 0A

M

D

SHEET: 1 OF 1


PE

NE

TR

AT

ION

RE

SIS

TA

NC

E


US

CS

SY

MB

OL

RE

CO

VE

RE

D

WA

TE

R

RLDEPTH

DE

PT

H(m

etre

s)

ME

TH

OD

GR

AP

HIC

LOG

SAMPLE ORFIELD TEST


CLIENT:

PROJECT:

LOCATION:

JOB NO:

DATE: 14/3/17

DATE: 26/4/17






Kapooka

1669283

COORDS: 526049.0 m E 6110117.0 m N MGA94 56


INCLINATION: -90°

HOLE DEPTH: 4.00 m



LOGGED: OB

CHECKED: JND

GA

P 8

_13.

0 LI

B.G

LB L

og G

AP

NO

N-C

OR

ED

FU

LL P

AG

E K

AP

OO

KA

.GP

J <

<D

raw

ingF

ile>

> 2

7/04

/201

7 15

:04

8.3

0.00

2 D

atge

l Too

ls

MO

IST

UR

EC

ON

DIT

ION

CO

NS

IST

EN

CY

DE

NS

ITY


OBSERVATIONS

0.0

0.5

1.0

1.5

2.0

2.5

3.0

3.5

4.0

4.5

5.0

L

H

Silty CLAYmedium plasticity, grey

CLAYlow to medium plasticity, brown orange



0.20

1.80

HA

PT

HA

0315_BH004_0.0DS 0.00-0.10 mR = 0APID = 0 ppm

0315_BH004_1.0DS 1.00-1.10 mR = 0A

0315_BH004_2.0DS 2.00-2.10 mR = 0A

0315_BH004_3.0DS 3.00-3.10 mR = 0A

0315_BH004_4.0DS 3.90-4.00 mR = 0A

D

SHEET: 1 OF 1


PE

NE

TR

AT

ION

RE

SIS

TA

NC

E


US

CS

SY

MB

OL

RE

CO

VE

RE

D

WA

TE

R

RLDEPTH

DE

PT

H(m

etre

s)

ME

TH

OD

GR

AP

HIC

LOG

SAMPLE ORFIELD TEST


CLIENT:

PROJECT:

LOCATION:

JOB NO:

DATE: 14/3/17

DATE: 26/4/17






Kapooka

1669283

COORDS: 526064.0 m E 6110113.0 m N MGA94 56


INCLINATION: -90°

HOLE DEPTH: 4.00 m



LOGGED: OB

CHECKED: JND

GA

P 8

_13.

0 LI

B.G

LB L

og G

AP

NO

N-C

OR

ED

FU

LL P

AG

E K

AP

OO

KA

.GP

J <

<D

raw

ingF

ile>

> 2

7/04

/201

7 15

:04

8.3

0.00

2 D

atge

l Too

ls

MO

IST

UR

EC

ON

DIT

ION

CO

NS

IST

EN

CY

DE

NS

ITY


OBSERVATIONS

0.0

0.5

1.0

1.5

2.0

2.5

3.0

3.5

4.0

4.5

5.0

M

H

M

Silty CLAYlow to medium plasticity, brown

CLAYmedium plasticity, brown orange

CLAYmedium plasticity, grey with some yellow

CLAYlow to medium plasticity, brown yellow

CLAYbrown yellow with some orange


0.20

0.60

1.20

2.40

HA

PT

0315_BH005_0.0DS 0.00-0.10 mR = 0A

0315_BH005_1.0DS 1.00-1.10 mR = 0A

0315_BH005_2.0DS 2.00-2.10 mR = 0A

0315_BH005_3.0DS 3.00-3.10 mR = 0A

0315_BH005_4.0DS 3.90-4.00 mR = 0A

D

SHEET: 1 OF 1


PE

NE

TR

AT

ION

RE

SIS

TA

NC

E


US

CS

SY

MB

OL

RE

CO

VE

RE

D

WA

TE

R

RLDEPTH

DE

PT

H(m

etre

s)

ME

TH

OD

GR

AP

HIC

LOG

SAMPLE ORFIELD TEST


CLIENT:

PROJECT:

LOCATION:

JOB NO:

DATE: 14/3/17

DATE: 26/4/17






Kapooka

1669283

COORDS: 526108.0 m E 6110076.0 m N MGA94 56


INCLINATION: -90°

HOLE DEPTH: 4.00 m



LOGGED: OB

CHECKED: JND

GA

P 8

_13.

0 LI

B.G

LB L

og G

AP

NO

N-C

OR

ED

FU

LL P

AG

E K

AP

OO

KA

.GP

J <

<D

raw

ingF

ile>

> 2

7/04

/201

7 15

:04

8.3

0.00

2 D

atge

l Too

ls

MO

IST

UR

EC

ON

DIT

ION

CO

NS

IST

EN

CY

DE

NS

ITY


OBSERVATIONS

0.0

0.5

1.0

1.5

2.0

2.5

3.0

3.5

4.0

4.5

5.0

M-H

H

FILL: Sandy CLAYlow plasticity, brown, fine to medium grained sand

CLAYmedium to high plasticity, red brown, with some ironstone gravel

CLAYmedium plasticity, grey with some red orange

CLAYmedium plasticity, grey orange with some white

CLAYmedium plasticity, red


0.40

1.30

2.20

3.00

HA

PT

AD

T

0315_BH006_0.0DS 0.00-0.10 mR = 0A

0315_BH006_1.0DS 1.00-1.10 mR = 0A

0315_BH006_2.0DS 2.00-2.10 mR = 0A

0315_BH006_3.0DS 3.00-3.10 mR = 0A

0315_BH006_3.0DS 3.90-4.00 mR = 0A

M

SHEET: 1 OF 1


PE

NE

TR

AT

ION

RE

SIS

TA

NC

E


US

CS

SY

MB

OL

RE

CO

VE

RE

D

WA

TE

R

RLDEPTH

DE

PT

H(m

etre

s)

ME

TH

OD

GR

AP

HIC

LOG

SAMPLE ORFIELD TEST


CLIENT:

PROJECT:

LOCATION:

JOB NO:

DATE: 14/3/17

DATE: 26/4/17






Kapooka

1669283

COORDS: 526193.0 m E 6110265.0 m N MGA94 56


INCLINATION: -90°

HOLE DEPTH: 4.00 m



LOGGED: OB

CHECKED: JND

GA

P 8

_13.

0 LI

B.G

LB L

og G

AP

NO

N-C

OR

ED

FU

LL P

AG

E K

AP

OO

KA

.GP

J <

<D

raw

ingF

ile>

> 2

7/04

/201

7 15

:04

8.3

0.00

2 D

atge

l Too

ls

MO

IST

UR

EC

ON

DIT

ION

CO

NS

IST

EN

CY

DE

NS

ITY


OBSERVATIONS

0.0

0.5

1.0

1.5

2.0

2.5

3.0

3.5

4.0

4.5

5.0

H

CLAYhigh plasticity, brown orange

CLAYmedium plasticity, orange

CLAYpale grey with some orange

CLAYlow to medium plasticity, white with some orange


1.00

2.60

3.20

HA

PT

AD

T

0315_BH007_0.0DS 0.00-0.10 mR = 0A

0315_BH007_1.0DS 1.00-1.10 mR = 0A

0315_BH007_2.0DS 2.00-2.10 mR = 0A

0315_BH007_3.0DS 3.00-3.10 mR = 0A

0315_BH007_4.0DS 3.90-4.00 mR = 0A

D

SHEET: 1 OF 1


PE

NE

TR

AT

ION

RE

SIS

TA

NC

E


US

CS

SY

MB

OL

RE

CO

VE

RE

D

WA

TE

R

RLDEPTH

DE

PT

H(m

etre

s)

ME

TH

OD

GR

AP

HIC

LOG

SAMPLE ORFIELD TEST


CLIENT:

PROJECT:

LOCATION:

JOB NO:

DATE: 15/3/17

DATE: 26/4/17






Kapooka

1669283

COORDS: 526432.0 m E 6110951.0 m N MGA94 56


INCLINATION: -90°

HOLE DEPTH: 4.00 m



LOGGED: OB

CHECKED: JND

GA

P 8

_13.

0 LI

B.G

LB L

og G

AP

NO

N-C

OR

ED

FU

LL P

AG

E K

AP

OO

KA

.GP

J <

<D

raw

ingF

ile>

> 2

7/04

/201

7 15

:04

8.3

0.00

2 D

atge

l Too

ls

MO

IST

UR

EC

ON

DIT

ION

CO

NS

IST

EN

CY

DE

NS

ITY


OBSERVATIONS

0.0

0.5

1.0

1.5

2.0

2.5

3.0

3.5

4.0

4.5

5.0

M

Silty Gravelly CLAYbrown grey

CLAYlow plasticity, orange

CLAYlow to medium plasticity, brown with some orange

CLAYmedium plasticity, grey with some orange

CLAYmedium plasticity, orange with some pale grey



0.40

1.20

2.30

3.20

3.90

HA

PT

0315_BH008_0.0DS 0.00-0.10 mR = 0A

0315_BH008_1.0DS 1.00-1.10 mR = 0A

0315_BH008_2.0DS 2.00-2.10 mR = 0A

0315_BH008_3.0DS 3.00-3.10 mR = 0A

0315_BH008_4.0DS 3.90-4.00 mR = 0A

D

SHEET: 1 OF 1


PE

NE

TR

AT

ION

RE

SIS

TA

NC

E


US

CS

SY

MB

OL

RE

CO

VE

RE

D

WA

TE

R

RLDEPTH

DE

PT

H(m

etre

s)

ME

TH

OD

GR

AP

HIC

LOG

SAMPLE ORFIELD TEST


CLIENT:

PROJECT:

LOCATION:

JOB NO:

DATE: 15/3/17

DATE: 26/4/17






Kapooka

1669283

COORDS: MGA94 56


INCLINATION: -90°

HOLE DEPTH: 4.00 m



LOGGED: OB

CHECKED: JND

GA

P 8

_13.

0 LI

B.G

LB L

og G

AP

NO

N-C

OR

ED

FU

LL P

AG

E K

AP

OO

KA

.GP

J <

<D

raw

ingF

ile>

> 2

7/04

/201

7 15

:04

8.3

0.00

2 D

atge

l Too

ls

MO

IST

UR

EC

ON

DIT

ION

CO

NS

IST

EN

CY

DE

NS

ITY


OBSERVATIONS

0.0

0.5

1.0

1.5

2.0

2.5

3.0

3.5

4.0

4.5

5.0

H

Silty CLAYlow plasticity, brown, with some angluar to subangular gravel


CLAYmedium plasticity, yellow/orange

CLAYhigh plasticity, pale grey with some orange and black


0.80

2.20

3.60

HA

PT

0315_BH009_0.0DS 0.00-0.10 mR = 0A

0315_BH009_1.0DS 1.00-1.10 mR = 0A

0315_BH009_2.0DS 2.00-2.10 mR = 0A

0315_BH009_3.0DS 3.00-3.10 mR = 0A

0315_BH009_4.0DS 3.90-4.00 mR = 0A

D

SHEET: 1 OF 1


PE

NE

TR

AT

ION

RE

SIS

TA

NC

E


US

CS

SY

MB

OL

RE

CO

VE

RE

D

WA

TE

R

RLDEPTH

DE

PT

H(m

etre

s)

ME

TH

OD

GR

AP

HIC

LOG

SAMPLE ORFIELD TEST


CLIENT:

PROJECT:

LOCATION:

JOB NO:

DATE: 15/3/17

DATE: 26/4/17






Kapooka

1669283

COORDS: 526651.0 m E 6110714.0 m N MGA94 56


INCLINATION: -90°

HOLE DEPTH: 4.00 m



LOGGED: OB

CHECKED: JND

GA

P 8

_13.

0 LI

B.G

LB L

og G

AP

NO

N-C

OR

ED

FU

LL P

AG

E K

AP

OO

KA

.GP

J <

<D

raw

ingF

ile>

> 2

7/04

/201

7 15

:04

8.3

0.00

2 D

atge

l Too

ls

MO

IST

UR

EC

ON

DIT

ION

CO

NS

IST

EN

CY

DE

NS

ITY


OBSERVATIONS

0.0

0.5

1.0

1.5

2.0

2.5

3.0

3.5

4.0

4.5

5.0

M

Silty CLAYlow plasticity, grey brown, with some angular gravel

CLAYlow to medium plasticity, brown

CLAYhigh plasticity, pale brown with some yellow

CLAYhigh plasticity, yellow with some white


0.60

1.60

2.80

HA

PT

0315_BH010_0.0DS 0.00-0.10 mR = 0A

0315_BH010_1.0DS 1.00-1.10 mR = 0A

0315_BH010_2.0DS 2.00-2.10 mR = 0A

0315_BH010_3.0DS 3.00-3.10 mR = 0A

0315_BH010_4.0DS 3.90-4.00 mR = 0A

D

M

D

SHEET: 1 OF 1


PE

NE

TR

AT

ION

RE

SIS

TA

NC

E


US

CS

SY

MB

OL

RE

CO

VE

RE

D

WA

TE

R

RLDEPTH

DE

PT

H(m

etre

s)

ME

TH

OD

GR

AP

HIC

LOG

SAMPLE ORFIELD TEST


CLIENT:

PROJECT:

LOCATION:

JOB NO:

DATE: 15/3/17

DATE: 26/4/17






Kapooka

1669283

COORDS: 526643.0 m E 6110697.0 m N MGA94 56


INCLINATION: -90°

HOLE DEPTH: 4.00 m



LOGGED: OB

CHECKED: JND

GA

P 8

_13.

0 LI

B.G

LB L

og G

AP

NO

N-C

OR

ED

FU

LL P

AG

E K

AP

OO

KA

.GP

J <

<D

raw

ingF

ile>

> 2

7/04

/201

7 15

:04

8.3

0.00

2 D

atge

l Too

ls

MO

IST

UR

EC

ON

DIT

ION

CO

NS

IST

EN

CY

DE

NS

ITY


OBSERVATIONS

0.0

0.5

1.0

1.5

2.0

2.5

3.0

3.5

4.0

4.5

5.0

H

Sandy CLAYlow plasticity, brown, medium to coarse grained, well gradedsand, with some angular gravel

CLAYmedium plasticity, brown, trace subangular gravel

CLAYmedium plasticity, brown with some red

CLAYmedium plasticity, brown


0.80

1.40

3.20

HA

PT

AD

T

0315_BH011_0.0DS 0.00-0.10 mR = 0A

0315_BH011_1.0DS 1.00-1.10 mR = 0A

0315_BH011_2.0DS 2.00-2.10 mR = 0A

0315_BH011_3.0DS 3.00-3.10 mR = 0A

0315_BH011_4.0DS 3.90-4.00 mR = 0A

D

SHEET: 1 OF 1


PE

NE

TR

AT

ION

RE

SIS

TA

NC

E


US

CS

SY

MB

OL

RE

CO

VE

RE

D

WA

TE

R

RLDEPTH

DE

PT

H(m

etre

s)

ME

TH

OD

GR

AP

HIC

LOG

SAMPLE ORFIELD TEST


CLIENT:

PROJECT:

LOCATION:

JOB NO:

DATE: 14/3/17

DATE: 26/4/17






Kapooka

1669283

COORDS: 526051.0 m E 6110389.0 m N MGA94 56


INCLINATION: -90°

HOLE DEPTH: 4.00 m



LOGGED: OB

CHECKED: JND

GA

P 8

_13.

0 LI

B.G

LB L

og G

AP

NO

N-C

OR

ED

FU

LL P

AG

E K

AP

OO

KA

.GP

J <

<D

raw

ingF

ile>

> 2

7/04

/201

7 15

:04

8.3

0.00

2 D

atge

l Too

ls

MO

IST

UR

EC

ON

DIT

ION

CO

NS

IST

EN

CY

DE

NS

ITY


OBSERVATIONS

0.0

0.5

1.0

1.5

2.0

2.5

3.0

3.5

4.0

4.5

5.0

H

Sandy CLAYlow to medium plasticity, brown red, fine to medium grained sand

Sandy CLAYmedium plasticity, brown red, medium grained sand

CLAYmedium plasticity, grey brown with some red

CLAYmedium plasticity, grey with some brown

CLAYlow plasticity, brown


0.90

1.30

2.20

3.40

HA

PT

AD

T

0315_BH012_0.0DS 0.00-0.10 mR = 0A

0315_BH012_1.0DS 1.00-1.10 mR = 0A

0315_BH012_2.0DS 2.00-2.10 mR = 0A

0315_BH012_3.0DS 3.00-3.10 mR = 0A

0315_BH012_4.0DS 3.90-4.00 mR = 0A

D

SHEET: 1 OF 1


PE

NE

TR

AT

ION

RE

SIS

TA

NC

E


US

CS

SY

MB

OL

RE

CO

VE

RE

D

WA

TE

R

RLDEPTH

DE

PT

H(m

etre

s)

ME

TH

OD

GR

AP

HIC

LOG

SAMPLE ORFIELD TEST


CLIENT:

PROJECT:

LOCATION:

JOB NO:

DATE: 14/3/17

DATE: 26/4/17






Kapooka

1669283

COORDS: 526029.0 m E 6110390.0 m N MGA94 56


INCLINATION: -90°

HOLE DEPTH: 4.00 m



LOGGED: OB

CHECKED: JND

GA

P 8

_13.

0 LI

B.G

LB L

og G

AP

NO

N-C

OR

ED

FU

LL P

AG

E K

AP

OO

KA

.GP

J <

<D

raw

ingF

ile>

> 2

7/04

/201

7 15

:04

8.3

0.00

2 D

atge

l Too

ls

MO

IST

UR

EC

ON

DIT

ION

CO

NS

IST

EN

CY

DE

NS

ITY


OBSERVATIONS

0.0

0.5

1.0

1.5

2.0

2.5

3.0

3.5

4.0

4.5

5.0

M

H

H

Sandy CLAYlow to medium plasticity, pale brown, subangular, poorley gradedsand


CLAYmedium plasticity, yellow brown



0.50

1.00

2.20

HA

PT

AD

T

0315_BH013_0.0DS 0.00-0.10 mR = 0A

0315_BH013_1.0DS 1.00-1.10 mR = 0A

0315_BH013_2.0DS 2.00-2.10 mR = 0A

0315_BH013_3.0DS 3.00-3.10 mR = 0A

0315_BH013_4.0DS 3.90-4.00 mR = 0A

D

SHEET: 1 OF 1


PE

NE

TR

AT

ION

RE

SIS

TA

NC

E


US

CS

SY

MB

OL

RE

CO

VE

RE

D

WA

TE

R

RLDEPTH

DE

PT

H(m

etre

s)

ME

TH

OD

GR

AP

HIC

LOG

SAMPLE ORFIELD TEST


CLIENT:

PROJECT:

LOCATION:

JOB NO:

DATE: 14/6/17

DATE: 26/4/17






Kapooka

1669283

COORDS: 526061.0 m E 6110402.0 m N MGA94 56


INCLINATION: -90°

HOLE DEPTH: 4.00 m



LOGGED: OB

CHECKED: JND

GA

P 8

_13.

0 LI

B.G

LB L

og G

AP

NO

N-C

OR

ED

FU

LL P

AG

E K

AP

OO

KA

.GP

J <

<D

raw

ingF

ile>

> 2

7/04

/201

7 15

:04

8.3

0.00

2 D

atge

l Too

ls

MO

IST

UR

EC

ON

DIT

ION

CO

NS

IST

EN

CY

DE

NS

ITY


OBSERVATIONS

0.0

0.5

1.0

1.5

2.0

2.5

3.0

3.5

4.0

4.5

5.0

H

CLAYlow plasticity, pale grey, with some angular gravel


CLAYmedium plasticity, orange with some brown

CLAYmedium plasticity, yellow with some grey

CLAYmedium plasticity, yellow with some grey


1.00

2.00

2.40

3.90

HA

PT

0315_BH014_0.0DS 0.00-0.10 mR = 0A

0315_BH014_1.0DS 1.00-1.10 mR = 0A

0315_BH014_2.00DS 2.00-2.10 mR = 0A

0315_BH014_3.0DS 3.00-3.10 mR = 0A

0315_BH014_4.0DS 3.90-4.00 mR = 0A

D

SHEET: 1 OF 1


PE

NE

TR

AT

ION

RE

SIS

TA

NC

E


US

CS

SY

MB

OL

RE

CO

VE

RE

D

WA

TE

R

RLDEPTH

DE

PT

H(m

etre

s)

ME

TH

OD

GR

AP

HIC

LOG

SAMPLE ORFIELD TEST


CLIENT:

PROJECT:

LOCATION:

JOB NO:

DATE: 15/3/17

DATE: 26/4/17






Kapooka

1669283

COORDS: 526506.0 m E 6109566.0 m N MGA94 56


INCLINATION: -90°

HOLE DEPTH: 4.00 m



LOGGED: OB

CHECKED: JND

GA

P 8

_13.

0 LI

B.G

LB L

og G

AP

NO

N-C

OR

ED

FU

LL P

AG

E K

AP

OO

KA

.GP

J <

<D

raw

ingF

ile>

> 2

7/04

/201

7 15

:04

8.3

0.00

2 D

atge

l Too

ls

MO

IST

UR

EC

ON

DIT

ION

CO

NS

IST

EN

CY

DE

NS

ITY


OBSERVATIONS

0.0

0.5

1.0

1.5

2.0

2.5

3.0

3.5

4.0

4.5

5.0

CLAYmedium plasticity, grey, with some gravel


CLAYmedium plasticity, grey with some orange and yellow

CLAYmedium to high plasticity, brown with some yellow


0.60

1.40

2.10

HA

PT

AD

T

0315_BH015_0.0DS 0.00-0.10 mR = 0A

0315_BH015_1.0DS 1.00-1.10 mR = 0A

0315_BH015_2.0DS 2.00-2.10 mR = 0A

0315_BH015_3.0DS 3.00-3.10 mR = 0A

0315_BH015_4.0DS 3.90-4.00 mR = 0A

D

SHEET: 1 OF 1


PE

NE

TR

AT

ION

RE

SIS

TA

NC

E


US

CS

SY

MB

OL

RE

CO

VE

RE

D

WA

TE

R

RLDEPTH

DE

PT

H(m

etre

s)

ME

TH

OD

GR

AP

HIC

LOG

SAMPLE ORFIELD TEST


CLIENT:

PROJECT:

LOCATION:

JOB NO:

DATE: 15/3/17

DATE: 26/4/17






Kapooka

1669283

COORDS: 526525.0 m E 6109562.0 m N MGA94 56


INCLINATION: -90°

HOLE DEPTH: 4.00 m



LOGGED: OB

CHECKED: JND

GA

P 8

_13.

0 LI

B.G

LB L

og G

AP

NO

N-C

OR

ED

FU

LL P

AG

E K

AP

OO

KA

.GP

J <

<D

raw

ingF

ile>

> 2

7/04

/201

7 15

:04

8.3

0.00

2 D

atge

l Too

ls

MO

IST

UR

EC

ON

DIT

ION

CO

NS

IST

EN

CY

DE

NS

ITY


OBSERVATIONS

0.0

0.5

1.0

1.5

2.0

2.5

3.0

3.5

4.0

4.5

5.0


APPENDIX G Data Validation


Golder Associates Pty Ltd.Prepared by: SM 1/05/2013

Checked by:

Number of Primary Samples: Number of Triplicate Samples:Number of Duplicate Samples: Number of Other QAQC Samples:

TypeMBRBRBRB

Sample ID

Anonymous

Analyte Group Primary ID Duplicate IDAll 0315_BH013_0.0_170314 0315_QC100_170314

All 0315_BH005_2.0_170314 0315_QC101_170314

Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates

(PFSAs)0315_BH002_1.0_170315 0315_QC102_170315


(PFSAs)0315_BH007_2.0_170315 0315_QC103_170315

All 0315_BH010_1.0_170315 0315_QC104_170315


(PFSAs)0315_BH009_0.0_170315 0315_QC105_170315


(PFSAs)0315_BH014_0.0_170315 0315_QC106_170315

All 0315_BH015_0.0_170315 0315_QC107_170315Perfluoroalkane sulfonic acids &

Perfluoroalkane sulfonates (PFSAs)

0315_SD005_170315 0315_QC108_170315

All 0315_SW005_170315 0315_QC109_170315All 0315_MW006_170316 0315_QC110_170316

Analyte Group Primary ID Triplicate ID

All 0315_BH007_2.0_170315 0315_QC203_170315


(PFSAs)0315_BH009_0.0_170315 0315_QC205_170315

All 0315_BH015_0.0_170315 0315_QC207_170315Perfluoroalkane sulfonic acids &

Perfluoroalkane sulfonates (PFSAs)

0315_SW005_170315 0315_QC209_170315


(PFSAs)0315_MW006_170316 0315_QC210_170316

Analyte Group Analyte(s)

Note: Data validation assesses each analyte in terms of all the data validation variables and only the exceedances and outliers are reported in this form.

*When concentrations are less than the LOR for both primary and duplicate/triplicate results, no RPDs are calculated

Performed By: Olga Bukhteeva Checked By: Tegen AnningDate: 4/04/2017 Date: 4/04/2017

(n:2) Fluorotelomer Sulfonic Acids (ALS)MS recovery of 10:2 Fluorotelomer sulfonic acid (10:2 FTS) was less than lower data quality objective (50-130%) in sample 0315_BH001_0.0_170315 (9.36%).

Perfluoroalkyl Sulfonamides (ALS)MS recoveries of N-Ethyl perfluorooctane sulfonamide (EtFOSA) (22.0%) and N-Ethyl perfluorooctane sulfonamidoethanol (EtFOSE) (15.3%) were less than lower data quality objective (30-130%) in sample 0315_BH001_0.0_170315.

Perfluoroalkyl Carboxylic Acids (ALS) MS recovery of Perfluoropentanoic acid (PFPeA) was less than lower data quality objective (50-130%) in sample 0315_BH001_0.0_170315 (36.2%).

Perfluoroalkyl Carboxylic Acids (ALS)MS recovery of Perfluorotetradecanoic acid (PFTeDA) was less than lower data quality objective (30-130%) in sample 0315_BH001_0.0_170315 (18.2%).

RPD for Perfluorooctane sulfonic acid (PFOS) (36%) exceeded LOR-based control limits. All other FD RPDs were within the accepted LOR based control limits or less than LOR.

All FD RPDs were within the accepted LOR based control limits or less than LOR.

RPDs for Perfluorooctane sulfonic acid (PFOS) (40%) and Perfluorohexane sulfonic acid (PFHxS) (89%) exceeded LOR-based control limits. All other FD RPDs were within the accepted LOR based control limits or less than LOR.


Laboratory Duplicates (LD) AnalysesComments

LD RPDs for Perfluorodecanesulfonic acid (PFDS) (200%), Perfluorododecanoic acid (PFDoA) (200%) and Perfluorotridecanoic acid (PFTrDA) (200%) exceeded LOR-based control limits (30%). See comments.

All other laboratory duplicate RPDs are within the laboratory based data quality objectives (Eurofins & ALS).Field Duplicates (FD) Analyses

Analyte Group

Matrix Spike (MS) AnalysesAnalyte Group Comments

Laboratory Control Spike (LCS) AnalysesAnalyte Group Comments

All results were below the LOR.

QAQC Sample Information (Method Blank - MB, Rinsate Blank - RB, Field Blank - FB, Trip Blank - TB)

0315_QC301_170315 All results were below the LOR.0315_QC300_170314 All results were below the LOR.

CommentsMethod Blank

0315_QC302_170316

All All laboratory control spike recoveries were within the laboratory based data quality objectives (Eurofins & ALS).

Sample ID

Comments

Project Name: PSI Cat 2 Blamey Barracks Kapooka (0315) Project Number: 1669283Primary Laboratory: ALS Workorder Number: ES1706394Secondary Laboratory: Eurofins MGT Workorder Number: 538644

14/03/2017 - 16/03/2017 Sample Medium: Soil / Water

Yes All: PFAS suite (standard and trace level)

YesAre there non-NATA accredited methods used? No

COC completed properly?

Yes All samples analysed within the appropriate holding times (Eurofins & ALS).

YesAll requested analysis completed?

This batch has been validated and is considered suitable for environmental interpretive use.

Eurofins & ALS: All surrogate recoveries were within the laboratory based data quality objectives.

As ALS stated: Poor Matrix Spike (MS) recoveries on various analytes is due to matrix interferences and effects. This was confirmed by re-extraction and re-analysis.

No Trip Spike was prepared in this batch.

Laboratory reports signed by authorised personnel? Yes All.

Perfluoroalkyl Sulfonic Acids, Perfluoroalkyl Carboxylic Acids,Perfluoroalkyl Sulfonamides and (n:2) Fluorotelomer

Sulfonic Acids (ALS)

MS recoveries of Perfluorohexane sulfonic acid (PFHxS), Perfluorooctane sulfonic acid (PFOS), Perfluorodecane sulfonic acid (PFDS), Perfluorohexanoic acid (PFHxA), Perfluorooctane sulfonamide (FOSA), 6:2 Fluorotelomer sulfonic acid (6:2 FTS) and 8:2 Fluorotelomer sulfonic acid (8:2 FTS) were not determined in samples 0315_BH001_0.0_170315, 0315_BH005_0.0_170314, 0315_BH009_0.0_170315 and 0315_BH013_0.0_170314. See comments.

Trip Spike Information

Analyte Spike Concentrations Recovery Concentration % Recovery

RPD outliers were reported in the interlaboratory duplicate analyses for Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs). These results are likely due to different sample dilution and preparation methods used between the laboratories or sample heterogeneity. As acceptable RPDs were reported in all other laboratory QA/QC tests performed by ALS/Eurofins and were within acceptable limits the results are not expected to affect the quality of the primary data. As a conservative measure, the highest value will be used for interpretation.

All other MS recoveries were within the laboratory based data quality objectives (Eurofins & ALS).

All results were below the LOR (Eurofins & ALS).

Field Triplicates (FT) AnalysesComments

Surrogate Compound Monitoring Analyses

DATA VALIDATION SUMMARY SHEET

11 3Documentation and Sample Handling Information

Sample Information89 6

Chromatograms supplied as appropriate? N/A

Y/N Comments

Samples received intact and chilled? Yes ALS: 5.7'c - Ice present. Intact. Eurofins: Attempt to chill evident.Samples analysed within appropriate holding times?

Signed by field staff and laboratory personnel.

Sample volumes sufficient for QC analysis?

Date Sampled:

RPDs in various field duplicate analysis exceeded LOR-based control limits. High RPDs are likely a result of sample heterogeneity. These results are not considered to affect the characterisation of the samples as both the primary and duplicate results are within the same order of magnitude.

Various MS recoveries (ALS) were not determined due to background levels being greater than or equal to 4x the spike level.

As stated by Eurofins: "Isotope dilution is used for calibration of each native compound for which an exact labelled analogue is available (Isotope Dilution Quantitation). The isotopically labelled analogues allow identification and recovery correction of the concentration of the associated native PFAS compounds. Where the native PFAS compound does not have labelled analogue then the quantification is made using the Extracted Internal Standard Analyte with the closest retention time to the analyte and no recovery correction has been made (Internal Standard Quantitation)."

The LD RPD reported passes Eurofins | mgt's QC - Acceptance Criteria as defined in the Internal Quality Control Review.


RPDs for Perfluorohexane sulfonic acid (PFHxS) (71%) and Perfluoropentanoic acid (PFPeA) (162%) exceeded LOR-based control limits. All other FT RPDs were within the accepted LOR based control limits or less than LOR.

RPDs for Perfluorooctanoic Acid (PFOA) (92%), Perfluorohexane sulfonic acid (PFHxS) (43%), Perfluorohexanoic acid (PFHxA) (136%), Perfluoroheptanoic acid (PFHpA) (120%) and Perfluoropentanoic acid (PFPeA) (117%) exceeded LOR-based control limits. All other FT RPDs were within the accepted LOR based control limits or less than LOR.

Per- and Polyfluorinated Alkyl Substances (PFASs) - Trace Level (Eurofins)

RPD for Perfluorooctanesulfonic acid (PFOS) (43%) exceeded LOR-based control limits. All other FT RPDs were within the accepted LOR based control limits or less than LOR.

All FT RPDs were within the accepted LOR based control limits or less than LOR.

As stated by Eurofins: "Quantification of linear and branched isomers has been conducted as a single total response using the relative response factor for the corresponding linear/branched standard."




RPDs for Perfluorooctane sulfonic acid (PFOS) (50%) and Perfluoroheptane sulfonic acid (PFHpS) (41%) exceeded LOR-based control limits. All other FD RPDs were within the accepted LOR based control limits or less than LOR.


Comments

Overall Comments

All FT RPDs were within the accepted LOR based control limits or less than LOR.

CommentsAll FD RPDs were within the accepted LOR based control limits or less than LOR.

Golder Associates Pty Ltd 2 of 12

Prepared by: COChecked by: LA

Duplicate Analysis RPDs Sample ID 0315 MW006 170316 0315 QC110 170316 0315 QC210 170316Project No. : 1669283 Sample Type Primary Field Duplicate Field TriplicateBatch/es: ES1706394 / 538644 Date Sampled 16/03/2017 16/03/2017 16/03/2017

Analyte Units LOR Primary vs Duplicate Primary vs Inter DuplicatePer- and polyfluoroalkyl substances (PFAS)N-Methyl PFO sulfonamidoethanol (MeFOSE) µg/L 0.001 <0.001 <0.001 <0.05 ND NDPerfluorodecane sulfonic acid (PFDS) µg/L 0.0005 <0.0005 <0.0005 <0.01 ND NDN-methyl-PFO sulfonamidoacetic acid (MeFOSAA) µg/L 0.0005 <0.0005 <0.0005 <0.05 ND NDPerfluorooctanoic Acid (PFOA) µg/L 0.0005 0.0185 0.023 0.05 21.69% 91.97%Perfluorooctane sulfonic acid (PFOS) µg/L 0.0003 0.0881 0.0888 0.11 0.79% 22.11%Perfluorohexane sulfonic acid (PFHxS) µg/L 0.0005 0.0519 0.0478 0.08 8.22% 42.61%Sum of PFHxS and PFOS (calculated) µg/L 0.0003 0.14 0.137 - 2.17% -PFAS (Sum of total - Lab Reported) µg/L 0.0003 0.204 0.202 - 0.99% -Sum of PFAS (WA DER 10, calculated) µg/L 0.0003 0.192 0.192 - 0.00% -Perfluorobutanoic acid (PFBA) µg/L 0.002 <0.002 <0.002 <0.05 ND NDPerfluorohexanoic acid (PFHxA) µg/L 0.0005 0.0057 0.0051 0.03 11.11% 136.13%Perfluoroheptanoic acid (PFHpA) µg/L 0.0005 0.005 0.0061 0.02 19.82% 120.00%Perfluorodecanoic acid (PFDA) µg/L 0.0005 0.0013 0.0013 <0.01 0.00% NDPerfluoropentanoic acid (PFPeA) µg/L 0.0005 0.0052 0.0048 0.02 8.00% 117.46%Perfluorononanoic acid (PFNA) µg/L 0.0005 0.0025 0.002 <0.01 22.22% NDPerfluorotetradecanoic acid (PFTeDA) µg/L 0.0005 <0.0005 <0.0005 <0.01 ND NDPerfluorotridecanoic acid (PFTrDA) µg/L 0.0005 <0.0005 <0.0005 <0.01 ND NDPerfluorododecanoic acid (PFDoDA) µg/L 0.0005 <0.0005 <0.0005 <0.01 ND NDPerfluoroundecanoic acid (PFUnDA) µg/L 0.0005 <0.0005 <0.0005 <0.01 ND NDPerfluoroheptane sulfonic acid (PFHpS) µg/L 0.0005 0.0028 0.0023 <0.01 19.61% NDPerfluoropentane sulfonic acid (PFPeS) µg/L 0.0005 0.0057 0.0047 <0.01 19.23% NDPerfluorobutane sulfonic acid (PFBS) µg/L 0.0005 0.0122 0.0113 0.01 7.66% 19.82%4:2 Fluorotelomer sulfonic acid (4:2 FTSA) µg/L 0.001 <0.001 <0.001 <0.01 ND ND6:2 Fluorotelomer sulfonic acid (6:2 FTSA) µg/L 0.001 0.005 0.005 <0.05 0.00% ND8:2 Fluorotelomer sulfonic acid (8:2 FTSA) µg/L 0.001 <0.001 <0.001 <0.01 ND ND10:2 Fluorotelomer sulfonic acid (10:2 FTSA) µg/L 0.001 <0.001 <0.001 <0.01 ND NDN-Ethyl PFO sulfonamide (EtFOSA) µg/L 0.001 <0.001 <0.001 - ND -N-Ethyl PFO sulfonamidoethanol (EtFOSE) µg/L 0.001 <0.001 <0.001 <0.05 ND NDN-Methyl PFO sulfonamide (MeFOSA) µg/L 0.001 <0.001 <0.001 <0.05 ND NDPerfluorooctane sulfonamide (FOSA) µg/L 0.0005 <0.0005 <0.0005 <0.05 ND NDN-ethyl-PFO sulfonamidoacetic acid (EtFOSAA) µg/L 0.0005 <0.0005 <0.0005 <0.05 ND NDLegendND = Not Detected (RPDs not calculated if both primary and duplicate results are below LOR) - = Not analysed/calculated

Acceptable RPDs: RPD <= 30%RPD > 30%, Analyis result < 10 times LORRPD <= 50%, Analysis result > 10 times LOR and < 20 times LOR

Project: PSI Cat 2 Blamey Barracks Kapooka (0315)

RPDs



Duplicate Analysis RPDs Sample ID 0315 BH013 0.0 170314 0315 QC100 170314Project No. : 1669283 Sample Type Primary Field DuplicateBatch/es: ES1706394 / 538644 Date Sampled 14/03/2017 14/03/2017

RPDsAnalyte Units LOR Primary vs Duplicate

Per- and polyfluoroalkyl substances (PFAS)N-Methyl PFO sulfonamidoethanol (MeFOSE) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorodecane sulfonic acid (PFDS) mg/kg 0.0002 <0.0002 <0.0002 NDN-methyl-PFO sulfonamidoacetic acid (MeFOSAA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorooctanoic Acid (PFOA) mg/kg 0.0002 0.0014 0.0013 7.41%Perfluorooctane sulfonic acid (PFOS) mg/kg 0.0002 0.0064 0.0062 3.17%Perfluorohexane sulfonic acid (PFHxS) mg/kg 0.0002 0.0013 0.0014 7.41%Sum of PFHxS and PFOS (calculated) mg/kg 0.0002 0.0077 0.0076 1.31%PFAS (Sum of total - Lab Reported) mg/kg 0.0002 0.0246 0.0303 20.77%Perfluorobutanoic acid (PFBA) mg/kg 0.001 <0.001 <0.001 NDPerfluorohexanoic acid (PFHxA) mg/kg 0.0002 0.0018 0.0017 5.71%Perfluoroheptanoic acid (PFHpA) mg/kg 0.0002 0.002 0.0019 5.13%Perfluorodecanoic acid (PFDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoropentanoic acid (PFPeA) mg/kg 0.0002 0.003 0.0026 14.29%Perfluorononanoic acid (PFNA) mg/kg 0.0002 0.0009 0.0009 0.00%Perfluorotetradecanoic acid (PFTeDA) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorotridecanoic acid (PFTrDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorododecanoic acid (PFDoDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroundecanoic acid (PFUnDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroheptane sulfonic acid (PFHpS) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoropentane sulfonic acid (PFPeS) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorobutane sulfonic acid (PFBS) mg/kg 0.0002 <0.0002 <0.0002 ND4:2 Fluorotelomer sulfonic acid (4:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND6:2 Fluorotelomer sulfonic acid (6:2 FTSA) mg/kg 0.0005 0.006 0.0098 48.10%8:2 Fluorotelomer sulfonic acid (8:2 FTSA) mg/kg 0.0005 0.0018 0.0036 66.67%10:2 Fluorotelomer sulfonic acid (10:2 FTSA) mg/kg 0.0005 <0.0005 0.0009 NDN-Ethyl PFO sulfonamide (EtFOSA) mg/kg 0.0005 <0.0005 <0.0005 NDN-Ethyl PFO sulfonamidoethanol (EtFOSE) mg/kg 0.0005 <0.0005 <0.0005 NDN-Methyl PFO sulfonamide (MeFOSA) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorooctane sulfonamide (FOSA) mg/kg 0.0002 <0.0002 <0.0002 NDN-ethyl-PFO sulfonamidoacetic acid (EtFOSAA) mg/kg 0.0002 <0.0002 <0.0002 NDMoisture % 1 3.4 2.8 19.35%LegendND = Not Detected (RPDs not calculated if both primary and duplicate results are below LOR) - = Not analysed/calculated







Per- and polyfluoroalkyl substances (PFAS)N-Methyl PFO sulfonamidoethanol (MeFOSE) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorodecane sulfonic acid (PFDS) mg/kg 0.0002 <0.0002 <0.0002 NDN-methyl-PFO sulfonamidoacetic acid (MeFOSAA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorooctanoic Acid (PFOA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorooctane sulfonic acid (PFOS) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorohexane sulfonic acid (PFHxS) mg/kg 0.0002 0.0004 0.0004 0.00%Sum of PFHxS and PFOS (calculated) mg/kg 0.0002 0.0004 0.0004 0.00%PFAS (Sum of total - Lab Reported) mg/kg 0.0002 0.0007 0.0004 54.55%Perfluorobutanoic acid (PFBA) mg/kg 0.001 <0.001 <0.001 NDPerfluorohexanoic acid (PFHxA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroheptanoic acid (PFHpA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorodecanoic acid (PFDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoropentanoic acid (PFPeA) mg/kg 0.0002 0.0003 <0.0002 NDPerfluorononanoic acid (PFNA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorotetradecanoic acid (PFTeDA) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorotridecanoic acid (PFTrDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorododecanoic acid (PFDoDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroundecanoic acid (PFUnDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroheptane sulfonic acid (PFHpS) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoropentane sulfonic acid (PFPeS) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorobutane sulfonic acid (PFBS) mg/kg 0.0002 <0.0002 <0.0002 ND4:2 Fluorotelomer sulfonic acid (4:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND6:2 Fluorotelomer sulfonic acid (6:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND8:2 Fluorotelomer sulfonic acid (8:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND10:2 Fluorotelomer sulfonic acid (10:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 NDN-Ethyl PFO sulfonamide (EtFOSA) mg/kg 0.0005 <0.0005 <0.0005 NDN-Ethyl PFO sulfonamidoethanol (EtFOSE) mg/kg 0.0005 <0.0005 <0.0005 NDN-Methyl PFO sulfonamide (MeFOSA) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorooctane sulfonamide (FOSA) mg/kg 0.0002 <0.0002 <0.0002 NDN-ethyl-PFO sulfonamidoacetic acid (EtFOSAA) mg/kg 0.0002 <0.0002 <0.0002 NDMoisture % 1 11.6 10.1 13.82%LegendND = Not Detected (RPDs not calculated if both primary and duplicate results are below LOR) - = Not analysed/calculated







Per- and polyfluoroalkyl substances (PFAS)N-Methyl PFO sulfonamidoethanol (MeFOSE) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorodecane sulfonic acid (PFDS) mg/kg 0.0002 <0.0002 <0.0002 NDN-methyl-PFO sulfonamidoacetic acid (MeFOSAA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorooctanoic Acid (PFOA) mg/kg 0.0002 0.0003 0.0005 50.00%Perfluorooctane sulfonic acid (PFOS) mg/kg 0.0002 0.178 0.119 39.73%Perfluorohexane sulfonic acid (PFHxS) mg/kg 0.0002 0.0034 0.0089 89.43%Perfluorobutanoic acid (PFBA) mg/kg 0.001 <0.001 <0.001 NDPerfluorohexanoic acid (PFHxA) mg/kg 0.0002 0.0009 0.0008 11.76%Perfluoroheptanoic acid (PFHpA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorodecanoic acid (PFDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoropentanoic acid (PFPeA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorononanoic acid (PFNA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorotetradecanoic acid (PFTeDA) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorotridecanoic acid (PFTrDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorododecanoic acid (PFDoDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroundecanoic acid (PFUnDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroheptane sulfonic acid (PFHpS) mg/kg 0.0002 <0.0002 0.0014 NDPerfluoropentane sulfonic acid (PFPeS) mg/kg 0.0002 <0.0002 0.0003 NDPerfluorobutane sulfonic acid (PFBS) mg/kg 0.0002 <0.0002 0.0002 ND4:2 Fluorotelomer sulfonic acid (4:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND6:2 Fluorotelomer sulfonic acid (6:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND8:2 Fluorotelomer sulfonic acid (8:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND10:2 Fluorotelomer sulfonic acid (10:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 NDN-Ethyl PFO sulfonamide (EtFOSA) mg/kg 0.0005 <0.0005 <0.0005 NDN-Ethyl PFO sulfonamidoethanol (EtFOSE) mg/kg 0.0005 <0.0005 <0.0005 NDN-Methyl PFO sulfonamide (MeFOSA) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorooctane sulfonamide (FOSA) mg/kg 0.0002 <0.0002 <0.0002 NDN-ethyl-PFO sulfonamidoacetic acid (EtFOSAA) mg/kg 0.0002 <0.0002 <0.0002 NDMoisture % 1 15.7 12.5 22.70%LegendND = Not Detected (RPDs not calculated if both primary and duplicate results are below LOR) - = Not analysed/calculated





Duplicate Analysis RPDs Sample ID 0315 BH007 2.0 170315 0315 QC103 170315 0315 QC203 170315Project No. : 1669283 Sample Type Primary Field Duplicate Field TriplicateBatch/es: ES1706394 / 538644 Date Sampled 15/03/2017 15/03/2017 15/03/2017

Analyte Units LOR Primary vs Duplicate Primary vs Inter DuplicatePer- and polyfluoroalkyl substances (PFAS)N-Methyl PFO sulfonamidoethanol (MeFOSE) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDPerfluorodecane sulfonic acid (PFDS) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDN-methyl-PFO sulfonamidoacetic acid (MeFOSAA) mg/kg 0.0002 <0.0002 <0.0002 <0.01 ND NDPerfluorooctanoic Acid (PFOA) mg/kg 0.0002 0.0015 0.0005 <0.005 100.00% NDPerfluorooctane sulfonic acid (PFOS) mg/kg 0.0002 0.0054 0.0013 <0.005 122.39% NDPerfluorohexane sulfonic acid (PFHxS) mg/kg 0.0002 0.0007 0.0004 <0.005 54.55% NDPerfluorobutanoic acid (PFBA) mg/kg 0.001 <0.001 <0.001 <0.005 ND NDPerfluorohexanoic acid (PFHxA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluoroheptanoic acid (PFHpA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluorodecanoic acid (PFDA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluoropentanoic acid (PFPeA) mg/kg 0.0002 0.0003 <0.0002 <0.005 ND NDPerfluorononanoic acid (PFNA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluorotetradecanoic acid (PFTeDA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDPerfluorotridecanoic acid (PFTrDA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluorododecanoic acid (PFDoDA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluoroundecanoic acid (PFUnDA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluoroheptane sulfonic acid (PFHpS) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluoropentane sulfonic acid (PFPeS) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluorobutane sulfonic acid (PFBS) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND ND4:2 Fluorotelomer sulfonic acid (4:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND ND6:2 Fluorotelomer sulfonic acid (6:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 <0.01 ND ND8:2 Fluorotelomer sulfonic acid (8:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND ND10:2 Fluorotelomer sulfonic acid (10:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDN-Ethyl PFO sulfonamide (EtFOSA) mg/kg 0.0005 <0.0005 <0.0005 - ND -N-Ethyl PFO sulfonamidoethanol (EtFOSE) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDN-Methyl PFO sulfonamide (MeFOSA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDPerfluorooctane sulfonamide (FOSA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDN-ethyl-PFO sulfonamidoacetic acid (EtFOSAA) mg/kg 0.0002 0.0011 0.0006 <0.01 58.82% NDMoisture % 1 11 13 10 16.67% 9.52%LegendND = Not Detected (RPDs not calculated if both primary and duplicate results are below LOR) - = Not analysed/calculated



RPDs





Per- and polyfluoroalkyl substances (PFAS)N-Methyl PFO sulfonamidoethanol (MeFOSE) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorodecane sulfonic acid (PFDS) mg/kg 0.0002 <0.0002 <0.0002 NDN-methyl-PFO sulfonamidoacetic acid (MeFOSAA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorooctanoic Acid (PFOA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorooctane sulfonic acid (PFOS) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorohexane sulfonic acid (PFHxS) mg/kg 0.0002 <0.0002 <0.0002 NDSum of PFHxS and PFOS (calculated) mg/kg 0.0002 <0.0002 <0.0002 NDPFAS (Sum of total - Lab Reported) mg/kg 0.0002 0.0008 <0.0002 NDPerfluorobutanoic acid (PFBA) mg/kg 0.001 <0.001 <0.001 NDPerfluorohexanoic acid (PFHxA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroheptanoic acid (PFHpA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorodecanoic acid (PFDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoropentanoic acid (PFPeA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorononanoic acid (PFNA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorotetradecanoic acid (PFTeDA) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorotridecanoic acid (PFTrDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorododecanoic acid (PFDoDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroundecanoic acid (PFUnDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroheptane sulfonic acid (PFHpS) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoropentane sulfonic acid (PFPeS) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorobutane sulfonic acid (PFBS) mg/kg 0.0002 <0.0002 <0.0002 ND4:2 Fluorotelomer sulfonic acid (4:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND6:2 Fluorotelomer sulfonic acid (6:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND8:2 Fluorotelomer sulfonic acid (8:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND10:2 Fluorotelomer sulfonic acid (10:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 NDN-Ethyl PFO sulfonamide (EtFOSA) mg/kg 0.0005 <0.0005 <0.0005 NDN-Ethyl PFO sulfonamidoethanol (EtFOSE) mg/kg 0.0005 0.0008 <0.0005 NDN-Methyl PFO sulfonamide (MeFOSA) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorooctane sulfonamide (FOSA) mg/kg 0.0002 <0.0002 <0.0002 NDN-ethyl-PFO sulfonamidoacetic acid (EtFOSAA) mg/kg 0.0002 <0.0002 <0.0002 NDMoisture % 1 14.4 9 46.15%LegendND = Not Detected (RPDs not calculated if both primary and duplicate results are below LOR) - = Not analysed/calculated






Analyte Units LOR Primary vs Duplicate Primary vs Inter DuplicatePer- and polyfluoroalkyl substances (PFAS)N-Methyl PFO sulfonamidoethanol (MeFOSE) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDPerfluorodecane sulfonic acid (PFDS) mg/kg 0.0002 <0.0002 0.0014 <0.005 ND NDN-methyl-PFO sulfonamidoacetic acid (MeFOSAA) mg/kg 0.0002 <0.0002 <0.0002 <0.01 ND NDPerfluorooctanoic Acid (PFOA) mg/kg 0.0002 0.0006 0.0007 <0.005 15.38% NDPerfluorooctane sulfonic acid (PFOS) mg/kg 0.0002 0.324 0.467 0.5 36.16% 42.72%Perfluorohexane sulfonic acid (PFHxS) mg/kg 0.0002 0.0038 0.0047 <0.005 21.18% NDPerfluorobutanoic acid (PFBA) mg/kg 0.001 <0.001 <0.001 <0.005 ND NDPerfluorohexanoic acid (PFHxA) mg/kg 0.0002 0.0009 0.0012 <0.005 28.57% NDPerfluoroheptanoic acid (PFHpA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluorodecanoic acid (PFDA) mg/kg 0.0002 <0.0002 0.0002 <0.005 ND NDPerfluoropentanoic acid (PFPeA) mg/kg 0.0002 <0.0002 0.0008 <0.005 ND NDPerfluorononanoic acid (PFNA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluorotetradecanoic acid (PFTeDA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDPerfluorotridecanoic acid (PFTrDA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluorododecanoic acid (PFDoDA) mg/kg 0.0002 <0.0002 0.0003 <0.005 ND NDPerfluoroundecanoic acid (PFUnDA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluoroheptane sulfonic acid (PFHpS) mg/kg 0.0002 0.002 0.0008 <0.005 85.71% NDPerfluoropentane sulfonic acid (PFPeS) mg/kg 0.0002 <0.0002 0.0003 <0.005 ND NDPerfluorobutane sulfonic acid (PFBS) mg/kg 0.0002 <0.0002 0.0002 <0.005 ND ND4:2 Fluorotelomer sulfonic acid (4:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND ND6:2 Fluorotelomer sulfonic acid (6:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 <0.01 ND ND8:2 Fluorotelomer sulfonic acid (8:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND ND10:2 Fluorotelomer sulfonic acid (10:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDN-Ethyl PFO sulfonamide (EtFOSA) mg/kg 0.0005 <0.0005 <0.0005 - ND -N-Ethyl PFO sulfonamidoethanol (EtFOSE) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDN-Methyl PFO sulfonamide (MeFOSA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDPerfluorooctane sulfonamide (FOSA) mg/kg 0.0002 0.001 0.0014 <0.005 33.33% NDN-ethyl-PFO sulfonamidoacetic acid (EtFOSAA) mg/kg 0.0002 <0.0002 <0.0002 <0.01 ND NDMoisture % 1 3 1.7 2.1 55.32% 35.29%LegendND = Not Detected (RPDs not calculated if both primary and duplicate results are below LOR) - = Not analysed/calculated



RPDs





Per- and polyfluoroalkyl substances (PFAS)N-Methyl PFO sulfonamidoethanol (MeFOSE) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorodecane sulfonic acid (PFDS) mg/kg 0.0002 <0.0002 <0.0002 NDN-methyl-PFO sulfonamidoacetic acid (MeFOSAA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorooctanoic Acid (PFOA) mg/kg 0.0002 0.0048 0.0037 25.88%Perfluorooctane sulfonic acid (PFOS) mg/kg 0.0002 0.116 0.0695 50.13%Perfluorohexane sulfonic acid (PFHxS) mg/kg 0.0002 0.0483 0.0414 15.38%Perfluorobutanoic acid (PFBA) mg/kg 0.001 <0.001 <0.001 NDPerfluorohexanoic acid (PFHxA) mg/kg 0.0002 0.0029 0.0019 41.67%Perfluoroheptanoic acid (PFHpA) mg/kg 0.0002 0.0006 0.0004 40.00%Perfluorodecanoic acid (PFDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoropentanoic acid (PFPeA) mg/kg 0.0002 <0.0002 0.0012 NDPerfluorononanoic acid (PFNA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorotetradecanoic acid (PFTeDA) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorotridecanoic acid (PFTrDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorododecanoic acid (PFDoDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroundecanoic acid (PFUnDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroheptane sulfonic acid (PFHpS) mg/kg 0.0002 0.0102 0.0067 41.42%Perfluoropentane sulfonic acid (PFPeS) mg/kg 0.0002 0.001 0.0008 22.22%Perfluorobutane sulfonic acid (PFBS) mg/kg 0.0002 0.0012 0.0007 52.63%4:2 Fluorotelomer sulfonic acid (4:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND6:2 Fluorotelomer sulfonic acid (6:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND8:2 Fluorotelomer sulfonic acid (8:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND10:2 Fluorotelomer sulfonic acid (10:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 NDN-Ethyl PFO sulfonamide (EtFOSA) mg/kg 0.0005 <0.0005 <0.0005 NDN-Ethyl PFO sulfonamidoethanol (EtFOSE) mg/kg 0.0005 <0.0005 <0.0005 NDN-Methyl PFO sulfonamide (MeFOSA) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorooctane sulfonamide (FOSA) mg/kg 0.0002 <0.0002 <0.0002 NDN-ethyl-PFO sulfonamidoacetic acid (EtFOSAA) mg/kg 0.0002 <0.0002 <0.0002 NDMoisture % 1 2 1.2 50.00%LegendND = Not Detected (RPDs not calculated if both primary and duplicate results are below LOR) - = Not analysed/calculated






Analyte Units LOR Primary vs Duplicate Primary vs Inter DuplicatePer- and polyfluoroalkyl substances (PFAS)N-Methyl PFO sulfonamidoethanol (MeFOSE) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDPerfluorodecane sulfonic acid (PFDS) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDN-methyl-PFO sulfonamidoacetic acid (MeFOSAA) mg/kg 0.0002 <0.0002 <0.0002 <0.01 ND NDPerfluorooctanoic Acid (PFOA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluorooctane sulfonic acid (PFOS) mg/kg 0.0002 0.0012 0.0006 <0.005 66.67% NDPerfluorohexane sulfonic acid (PFHxS) mg/kg 0.0002 <0.0002 0.0002 <0.005 ND NDSum of PFHxS and PFOS (calculated) mg/kg 0.0002 0.0012 0.0008 - 40.00% -PFAS (Sum of total - Lab Reported) mg/kg 0.0002 0.0012 0.0008 - 40.00% -Perfluorobutanoic acid (PFBA) mg/kg 0.001 <0.001 <0.001 <0.005 ND NDPerfluorohexanoic acid (PFHxA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluoroheptanoic acid (PFHpA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluorodecanoic acid (PFDA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluoropentanoic acid (PFPeA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluorononanoic acid (PFNA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluorotetradecanoic acid (PFTeDA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDPerfluorotridecanoic acid (PFTrDA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluorododecanoic acid (PFDoDA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluoroundecanoic acid (PFUnDA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluoroheptane sulfonic acid (PFHpS) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluoropentane sulfonic acid (PFPeS) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluorobutane sulfonic acid (PFBS) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND ND4:2 Fluorotelomer sulfonic acid (4:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND ND6:2 Fluorotelomer sulfonic acid (6:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 <0.01 ND ND8:2 Fluorotelomer sulfonic acid (8:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND ND10:2 Fluorotelomer sulfonic acid (10:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDN-Ethyl PFO sulfonamide (EtFOSA) mg/kg 0.0005 <0.0005 <0.0005 - ND -N-Ethyl PFO sulfonamidoethanol (EtFOSE) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDN-Methyl PFO sulfonamide (MeFOSA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDPerfluorooctane sulfonamide (FOSA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDN-ethyl-PFO sulfonamidoacetic acid (EtFOSAA) mg/kg 0.0002 <0.0002 <0.0002 <0.01 ND NDMoisture % 1 2.9 2 2.3 36.73% 23.08%LegendND = Not Detected (RPDs not calculated if both primary and duplicate results are below LOR) - = Not analysed/calculated



RPDs



Duplicate Analysis RPDs Sample ID 0315 SD005 170315 0315 QC108 170315Project No. : 1669283 Sample Type Primary Field DuplicateBatch/es: ES1706394 / 538644 Date Sampled 15/03/2017 15/03/2017


Per- and polyfluoroalkyl substances (PFAS)N-Methyl PFO sulfonamidoethanol (MeFOSE) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorodecane sulfonic acid (PFDS) mg/kg 0.0002 <0.0002 <0.0002 NDN-methyl-PFO sulfonamidoacetic acid (MeFOSAA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorooctanoic Acid (PFOA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorooctane sulfonic acid (PFOS) mg/kg 0.0002 0.0053 0.0025 71.79%Perfluorohexane sulfonic acid (PFHxS) mg/kg 0.0002 0.0005 0.0006 18.18%Perfluorobutanoic acid (PFBA) mg/kg 0.001 <0.001 <0.001 NDPerfluorohexanoic acid (PFHxA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroheptanoic acid (PFHpA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorodecanoic acid (PFDA) mg/kg 0.0002 <0.0002 0.0002 NDPerfluoropentanoic acid (PFPeA) mg/kg 0.0002 <0.0002 0.0072 NDPerfluorononanoic acid (PFNA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorotetradecanoic acid (PFTeDA) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorotridecanoic acid (PFTrDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorododecanoic acid (PFDoDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroundecanoic acid (PFUnDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroheptane sulfonic acid (PFHpS) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoropentane sulfonic acid (PFPeS) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorobutane sulfonic acid (PFBS) mg/kg 0.0002 <0.0002 <0.0002 ND4:2 Fluorotelomer sulfonic acid (4:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND6:2 Fluorotelomer sulfonic acid (6:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND8:2 Fluorotelomer sulfonic acid (8:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND10:2 Fluorotelomer sulfonic acid (10:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 NDN-Ethyl PFO sulfonamide (EtFOSA) mg/kg 0.0005 <0.0005 <0.0005 NDN-Ethyl PFO sulfonamidoethanol (EtFOSE) mg/kg 0.0005 <0.0005 <0.0005 NDN-Methyl PFO sulfonamide (MeFOSA) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorooctane sulfonamide (FOSA) mg/kg 0.0002 <0.0002 <0.0002 NDN-ethyl-PFO sulfonamidoacetic acid (EtFOSAA) mg/kg 0.0002 <0.0002 <0.0002 NDMoisture % 1 66.1 78 16.52%LegendND = Not Detected (RPDs not calculated if both primary and duplicate results are below LOR) - = Not analysed/calculated





Duplicate Analysis RPDs Sample ID 0315 SW005 170315 0315 QC109 170315 0315 QC209 170315Project No. : 1669283 Sample Type Primary Field Duplicate Field TriplicateBatch/es: ES1706394 / 538644 Date Sampled 15/03/2017 15/03/2017 15/03/2017

Analyte Units LOR Primary vs Duplicate Primary vs Inter DuplicatePer- and polyfluoroalkyl substances (PFAS)N-Methyl PFO sulfonamidoethanol (MeFOSE) µg/L 0.001 <0.001 <0.001 <0.05 ND NDPerfluorodecane sulfonic acid (PFDS) µg/L 0.0005 <0.0005 <0.0005 <0.01 ND NDN-methyl-PFO sulfonamidoacetic acid (MeFOSAA) µg/L 0.0005 <0.0005 <0.0005 <0.05 ND NDPerfluorooctanoic Acid (PFOA) µg/L 0.0005 0.006 0.0071 <0.01 16.79% NDPerfluorooctane sulfonic acid (PFOS) µg/L 0.0003 0.0551 0.0429 0.07 24.90% 23.82%Perfluorohexane sulfonic acid (PFHxS) µg/L 0.0005 0.0428 0.0388 0.09 9.80% 71.08%Sum of PFHxS and PFOS (calculated) µg/L 0.0003 0.0979 0.0817 - 18.04% -PFAS (Sum of total - Lab Reported) µg/L 0.0003 0.145 0.13 - 10.91% -Sum of PFAS (WA DER 10, calculated) µg/L 0.0003 0.136 0.122 - 10.85% -Perfluorobutanoic acid (PFBA) µg/L 0.002 <0.002 <0.002 <0.05 ND NDPerfluorohexanoic acid (PFHxA) µg/L 0.0005 0.0036 0.0039 < 0.05 8.00% NDPerfluoroheptanoic acid (PFHpA) µg/L 0.0005 0.0023 0.0024 < 0.01 4.26% NDPerfluorodecanoic acid (PFDA) µg/L 0.0005 <0.0005 <0.0005 <0.01 ND NDPerfluoropentanoic acid (PFPeA) µg/L 0.0005 0.0042 0.0047 0.04 11.24% 161.99%Perfluorononanoic acid (PFNA) µg/L 0.0005 0.0013 0.0015 <0.01 14.29% NDPerfluorotetradecanoic acid (PFTeDA) µg/L 0.0005 <0.0005 <0.0005 <0.01 ND NDPerfluorotridecanoic acid (PFTrDA) µg/L 0.0005 <0.0005 <0.0005 <0.01 ND NDPerfluorododecanoic acid (PFDoDA) µg/L 0.0005 <0.0005 <0.0005 <0.01 ND NDPerfluoroundecanoic acid (PFUnDA) µg/L 0.0005 <0.0005 <0.0005 <0.01 ND NDPerfluoroheptane sulfonic acid (PFHpS) µg/L 0.0005 0.0023 0.0017 <0.01 30.00% NDPerfluoropentane sulfonic acid (PFPeS) µg/L 0.0005 0.0051 0.0049 <0.01 4.00% NDPerfluorobutane sulfonic acid (PFBS) µg/L 0.0005 0.022 0.0217 <0.01 1.37% ND4:2 Fluorotelomer sulfonic acid (4:2 FTSA) µg/L 0.001 <0.001 <0.001 <0.01 ND ND6:2 Fluorotelomer sulfonic acid (6:2 FTSA) µg/L 0.001 <0.001 <0.001 <0.05 ND ND8:2 Fluorotelomer sulfonic acid (8:2 FTSA) µg/L 0.001 <0.001 <0.001 <0.01 ND ND10:2 Fluorotelomer sulfonic acid (10:2 FTSA) µg/L 0.001 <0.001 <0.001 <0.01 ND NDN-Ethyl PFO sulfonamide (EtFOSA) µg/L 0.001 <0.001 <0.001 - ND -N-Ethyl PFO sulfonamidoethanol (EtFOSE) µg/L 0.001 <0.001 <0.001 <0.05 ND NDN-Methyl PFO sulfonamide (MeFOSA) µg/L 0.001 <0.001 <0.001 <0.05 ND NDPerfluorooctane sulfonamide (FOSA) µg/L 0.0005 <0.0005 <0.0005 <0.05 ND NDN-ethyl-PFO sulfonamidoacetic acid (EtFOSAA) µg/L 0.0005 <0.0005 <0.0005 <0.05 ND NDLegendND = Not Detected (RPDs not calculated if both primary and duplicate results are below LOR) - = Not analysed/calculated



RPDs


APPENDIX H Laboratory Certificates


True

Environmental

QA/QC Compliance Assessment to assist with Quality ReviewWork Order : ES1706394 Page : 1 of 18

:Amendment 2

:: LaboratoryClient Environmental Division SydneyGOLDER ASSOCIATES

:Contact MS OLGA BUKHTEEVA Telephone : +61-2-8784 8555

:Project 1652034 Date Samples Received : 17-Mar-2017

Site : Kapooka Issue Date : 10-Apr-2017

OLGA BUKHTEEVA:Sampler No. of samples received : 110

:Order number PO01472 No. of samples analysed : 103

This report is automatically generated by the ALS LIMS through interpretation of the ALS Quality Control Report and several Quality Assurance parameters measured by ALS. This automated

reporting highlights any non-conformances, facilitates faster and more accurate data validation and is designed to assist internal expert and external Auditor review. Many components of this

report contribute to the overall DQO assessment and reporting for guideline compliance.

Brief method summaries and references are also provided to assist in traceability.

Summary of Outliers

Outliers : Quality Control Samples

This report highlights outliers flagged in the Quality Control (QC) Report.

l NO Method Blank value outliers occur.

l NO Duplicate outliers occur.

l NO Laboratory Control outliers occur.

l Matrix Spike outliers exist - please see following pages for full details.

l For all regular sample matrices, NO surrogate recovery outliers occur.

Outliers : Analysis Holding Time Compliance

l NO Analysis Holding Time Outliers exist.

Outliers : Frequency of Quality Control Samples

l Quality Control Sample Frequency Outliers exist - please see following pages for full details.

R I G H T S O L U T I O N S | R I G H T P A R T N E R

2 of 18:Page

Work Order :

:Client

ES1706394 Amendment 2

GOLDER ASSOCIATES

1652034:Project

Outliers : Quality Control Samples

Duplicates, Method Blanks, Laboratory Control Samples and Matrix Spikes

Matrix: SOIL

Compound Group Name CommentLimitsDataAnalyteClient Sample IDLaboratory Sample ID CAS Number

Matrix Spike (MS) Recoveries

ES1706394--001 355-46-4Perfluorohexane

sulfonic acid

(PFHxS)

0315_BH001_0.0_170315 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231A: Perfluoroalkyl Sulfonic Acids

ES1706394--001 1763-23-1Perfluorooctane

sulfonic acid (PFOS)




----Not

Determined







----Not

Determined







----Not

Determined







----Not

Determined


ES1706394--001 335-77-3Perfluorodecane

sulfonic acid (PFDS)




----Not

Determined


ES1706394--001 2706-90-3Perfluoropentanoic

acid (PFPeA)

0315_BH001_0.0_170315 Recovery less than lower data quality

objective

50-130%36.2 %EP231B: Perfluoroalkyl Carboxylic Acids

ES1706394--001 307-24-4Perfluorohexanoic acid

(PFHxA)




----Not

Determined

EP231B: Perfluoroalkyl Carboxylic Acids

ES1706394--001 376-06-7Perfluorotetradecanoic

acid (PFTeDA)


objective

30-130%18.2 %EP231B: Perfluoroalkyl Carboxylic Acids


sulfonamide (FOSA)




----Not

Determined

EP231C: Perfluoroalkyl Sulfonamides

ES1706394--001 4151-50-2N-Ethyl perfluorooctane

sulfonamide

(EtFOSA)


objective

30-130%22.0 %EP231C: Perfluoroalkyl Sulfonamides

ES1706394--001 1691-99-2N-Ethyl perfluorooctane

sulfonamidoethanol

(EtFOSE)


objective

30-130%15.3 %EP231C: Perfluoroalkyl Sulfonamides

ES1706394--061 27619-97-26:2 Fluorotelomer

sulfonic acid (6:2

FTS)




----Not

Determined

EP231D: (n:2) Fluorotelomer Sulfonic Acids


sulfonic acid (8:2

FTS)




----Not

Determined


3 of 18:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project

Matrix: SOIL

Compound Group Name CommentLimitsDataAnalyteClient Sample IDLaboratory Sample ID CAS Number

Matrix Spike (MS) Recoveries - Continued


sulfonic acid (10:2

FTS)


objective

50-130%9.36 %EP231D: (n:2) Fluorotelomer Sulfonic Acids

Outliers : Frequency of Quality Control Samples

Matrix: SOIL

Quality Control SpecificationQuality Control Sample Type

Method ExpectedQC Regular Actual

Rate (%)Quality Control Sample Type Count

Laboratory Duplicates (DUP)

NEPM 2013 B3 & ALS QC StandardMoisture Content 9.80 10.0010 102

Matrix: WATER


Method ExpectedQC Regular Actual

Rate (%)Quality Control Sample Type Count

Matrix Spikes (MS)

NEPM 2013 B3 & ALS QC StandardPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS 0.00 5.000 9

Analysis Holding Time Compliance

Holding times for VOC in soils vary according to analytes of interest. Vinyl Chloride and Styrene holding time is 7 days; others 14 days. A recorded breach does not guarantee a breach for all VOC analytes and

should be verified in case the reported breach is a false positive or Vinyl Chloride and Styrene are not key analytes of interest/concern.

Holding time for leachate methods (e.g. TCLP) vary according to the analytes reported. Assessment compares the leach date with the shortest analyte holding time for the equivalent soil method. These are: organics

14 days, mercury 28 days & other metals 180 days. A recorded breach does not guarantee a breach for all non-volatile parameters.

If samples are identified below as having been analysed or extracted outside of recommended holding times, this should be taken into consideration when interpreting results.

This report summarizes extraction / preparation and analysis times and compares each with ALS recommended holding times (referencing USEPA SW 846, APHA, AS and NEPM) based on the sample container

provided. Dates reported represent first date of extraction or analysis and preclude subsequent dilutions and reruns. A listing of breaches (if any) is provided herein.

Matrix: SOIL Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EA055: Moisture Content

HDPE Soil Jar (EA055-103)

0315_BH003_0.0_170314, 0315_BH003_1.0_170314,

0315_BH003_2.0_170314, 0315_BH003_3.0_170314,

0315_BH003_4.0_170314, 0315_BH004_0.0_170314,

0315_BH004_1.0_170314, 0315_BH004_2.0_170314,

0315_BH004_3.0_170314, 0315_BH004_4.0_170314,

0315_BH005_0.0_170314, 0315_BH005_1.0_170314,

0315_BH005_2.0_170314, 0315_BH005_3.0_170314,

0315_BH005_4.0_170314, 0315_BH006_0.0_170314,

0315_BH006_1.0_170314, 0315_BH006_2.0_170314,

0315_BH006_3.0_170314

28-Mar-2017---- 20-Mar-2017----14-Mar-2017 ---- ü


4 of 18:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project




EA055: Moisture Content - Continued

0315_BH006_4.0_170314, 0315_BH011_0.0_170314,

0315_BH011_1.0_170314, 0315_BH011_2.0_170314,

0315_BH011_3.0_170314, 0315_BH011_4.0_170314,

0315_BH012_0.0_170314, 0315_BH012_1.0_170314,

0315_BH012_2.0_170314, 0315_BH012_3.0_170314,

0315_BH012_4.0_170314, 0315_BH013_0.0_170314,

0315_BH013_1.0_170314, 0315_BH013_2.0_170314,

0315_BH013_3.0_170314, 0315_BH013_4.0_170314,

0315_SD001_170314, 0315_SD002_170314,

0315_QC100_170314, 0315_QC101_170314

28-Mar-2017---- 21-Mar-2017----14-Mar-2017 ---- ü


0315_BH001_0.0_170315, 0315_BH001_1.0_170315,

0315_BH001_2.0_170315, 0315_BH001_3.0_170315,

0315_BH001_4.0_170315, 0315_BH002_0.0_170315,

0315_BH002_1.0_170315, 0315_BH002_2.0_170315,

0315_BH002_3.0_170315, 0315_BH002_4.0_170315

29-Mar-2017---- 20-Mar-2017----15-Mar-2017 ---- ü


0315_BH007_0.0_170315, 0315_BH007_1.0_170315,

0315_BH007_2.0_170315, 0315_BH007_3.0_170315,

0315_BH007_4.0_170315, 0315_BH008_0.0_170315,

0315_BH008_1.0_170315, 0315_BH008_2.0_170315,

0315_BH008_3.0_170315, 0315_BH008_4.0_170315,

0315_BH009_0.0_170315, 0315_BH009_1.0_170315,

0315_BH009_2.0_170315, 0315_BH009_3.0_170315,

0315_BH009_4.0_170315, 0315_BH010_0.0_170315,

0315_BH010_1.0_170315, 0315_BH010_2.0_170315,

0315_BH010_3.0_170315, 0315_BH010_4.0_170315,

0315_BH014_0.0_170315, 0315_BH014_1.0_170315,

0315_BH014_2.0_170315, 0315_BH014_3.0_170315,

0315_BH014_4.0_170315, 0315_BH015_0.0_170315,

0315_BH015_1.0_170315, 0315_BH015_2.0_170315,

0315_BH015_3.0_170315, 0315_BH015_4.0_170315,

0315_SD005_170315, 0315_SD007_170315,

0315_QC102_170315, 0315_QC103_170315,

0315_QC104_170315, 0315_QC105_170315,

0315_QC106_170315, 0315_QC107_170315,

0315_QC108_170315

29-Mar-2017---- 21-Mar-2017----15-Mar-2017 ---- ü


0315_SD003_170316, 0315_SD004_170316,

0315_SD006_170316

30-Mar-2017---- 21-Mar-2017----16-Mar-2017 ---- ü

5 of 18:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project





HDPE Soil Jar (EP231X)

0315_BH003_0.0_170314, 0315_BH003_1.0_170314,

0315_BH003_2.0_170314, 0315_BH003_3.0_170314,

0315_BH003_4.0_170314, 0315_BH004_0.0_170314,

0315_BH004_1.0_170314, 0315_BH004_2.0_170314,

0315_BH004_3.0_170314, 0315_BH004_4.0_170314,

0315_BH005_0.0_170314, 0315_BH005_1.0_170314,

0315_BH005_2.0_170314, 0315_BH005_3.0_170314,

0315_BH005_4.0_170314, 0315_BH006_0.0_170314,

0315_BH006_1.0_170314, 0315_BH006_2.0_170314,

0315_BH006_3.0_170314, 0315_BH006_4.0_170314

30-Apr-201710-Sep-2017 21-Mar-201721-Mar-201714-Mar-2017 ü ü


0315_BH011_0.0_170314, 0315_BH011_1.0_170314,

0315_BH011_2.0_170314, 0315_BH011_3.0_170314,

0315_BH011_4.0_170314, 0315_BH012_0.0_170314,

0315_BH012_1.0_170314, 0315_BH012_2.0_170314,

0315_BH012_3.0_170314, 0315_BH012_4.0_170314,

0315_BH013_0.0_170314, 0315_BH013_1.0_170314,

0315_BH013_2.0_170314, 0315_BH013_3.0_170314,

0315_BH013_4.0_170314, 0315_SD001_170314,

0315_SD002_170314, 0315_QC100_170314,

0315_QC101_170314

01-May-201710-Sep-2017 22-Mar-201722-Mar-201714-Mar-2017 ü ü


0315_BH001_0.0_170315, 0315_BH001_1.0_170315,

0315_BH001_2.0_170315, 0315_BH001_3.0_170315,

0315_BH001_4.0_170315, 0315_BH002_0.0_170315,

0315_BH002_1.0_170315, 0315_BH002_2.0_170315,

0315_BH002_3.0_170315, 0315_BH002_4.0_170315,

0315_BH007_0.0_170315, 0315_BH007_1.0_170315,

0315_BH007_2.0_170315, 0315_BH007_3.0_170315,

0315_BH007_4.0_170315, 0315_BH008_0.0_170315,

0315_BH008_1.0_170315, 0315_BH008_2.0_170315,

0315_BH008_3.0_170315, 0315_BH008_4.0_170315



6 of 18:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project




EP231A: Perfluoroalkyl Sulfonic Acids - Continued

0315_BH009_0.0_170315, 0315_BH009_1.0_170315,

0315_BH009_2.0_170315, 0315_BH009_3.0_170315,

0315_BH009_4.0_170315, 0315_BH010_0.0_170315,

0315_BH010_1.0_170315, 0315_BH010_2.0_170315,

0315_BH010_3.0_170315, 0315_BH010_4.0_170315,

0315_BH014_0.0_170315, 0315_BH014_1.0_170315,

0315_BH014_2.0_170315, 0315_BH014_3.0_170315,

0315_BH014_4.0_170315, 0315_BH015_0.0_170315,

0315_BH015_1.0_170315, 0315_BH015_2.0_170315,

0315_BH015_3.0_170315, 0315_BH015_4.0_170315,

0315_SD005_170315, 0315_SD007_170315,

0315_QC102_170315, 0315_QC103_170315,

0315_QC104_170315, 0315_QC105_170315,

0315_QC106_170315, 0315_QC107_170315,

0315_QC108_170315



0315_SD003_170316, 0315_SD004_170316,

0315_SD006_170316


7 of 18:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project






0315_BH003_0.0_170314, 0315_BH003_1.0_170314,

0315_BH003_2.0_170314, 0315_BH003_3.0_170314,

0315_BH003_4.0_170314, 0315_BH004_0.0_170314,

0315_BH004_1.0_170314, 0315_BH004_2.0_170314,

0315_BH004_3.0_170314, 0315_BH004_4.0_170314,

0315_BH005_0.0_170314, 0315_BH005_1.0_170314,

0315_BH005_2.0_170314, 0315_BH005_3.0_170314,

0315_BH005_4.0_170314, 0315_BH006_0.0_170314,

0315_BH006_1.0_170314, 0315_BH006_2.0_170314,

0315_BH006_3.0_170314, 0315_BH006_4.0_170314



0315_BH011_0.0_170314, 0315_BH011_1.0_170314,

0315_BH011_2.0_170314, 0315_BH011_3.0_170314,

0315_BH011_4.0_170314, 0315_BH012_0.0_170314,

0315_BH012_1.0_170314, 0315_BH012_2.0_170314,

0315_BH012_3.0_170314, 0315_BH012_4.0_170314,

0315_BH013_0.0_170314, 0315_BH013_1.0_170314,

0315_BH013_2.0_170314, 0315_BH013_3.0_170314,

0315_BH013_4.0_170314, 0315_SD001_170314,

0315_SD002_170314, 0315_QC100_170314,

0315_QC101_170314



0315_BH001_0.0_170315, 0315_BH001_1.0_170315,

0315_BH001_2.0_170315, 0315_BH001_3.0_170315,

0315_BH001_4.0_170315, 0315_BH002_0.0_170315,

0315_BH002_1.0_170315, 0315_BH002_2.0_170315,

0315_BH002_3.0_170315, 0315_BH002_4.0_170315,

0315_BH007_0.0_170315, 0315_BH007_1.0_170315,

0315_BH007_2.0_170315, 0315_BH007_3.0_170315,

0315_BH007_4.0_170315, 0315_BH008_0.0_170315,

0315_BH008_1.0_170315, 0315_BH008_2.0_170315,

0315_BH008_3.0_170315, 0315_BH008_4.0_170315



8 of 18:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project




EP231B: Perfluoroalkyl Carboxylic Acids - Continued

0315_BH009_0.0_170315, 0315_BH009_1.0_170315,

0315_BH009_2.0_170315, 0315_BH009_3.0_170315,

0315_BH009_4.0_170315, 0315_BH010_0.0_170315,

0315_BH010_1.0_170315, 0315_BH010_2.0_170315,

0315_BH010_3.0_170315, 0315_BH010_4.0_170315,

0315_BH014_0.0_170315, 0315_BH014_1.0_170315,

0315_BH014_2.0_170315, 0315_BH014_3.0_170315,

0315_BH014_4.0_170315, 0315_BH015_0.0_170315,

0315_BH015_1.0_170315, 0315_BH015_2.0_170315,

0315_BH015_3.0_170315, 0315_BH015_4.0_170315,

0315_SD005_170315, 0315_SD007_170315,

0315_QC102_170315, 0315_QC103_170315,

0315_QC104_170315, 0315_QC105_170315,

0315_QC106_170315, 0315_QC107_170315,

0315_QC108_170315



0315_SD003_170316, 0315_SD004_170316,

0315_SD006_170316


9 of 18:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project






0315_BH003_0.0_170314, 0315_BH003_1.0_170314,

0315_BH003_2.0_170314, 0315_BH003_3.0_170314,

0315_BH003_4.0_170314, 0315_BH004_0.0_170314,

0315_BH004_1.0_170314, 0315_BH004_2.0_170314,

0315_BH004_3.0_170314, 0315_BH004_4.0_170314,

0315_BH005_0.0_170314, 0315_BH005_1.0_170314,

0315_BH005_2.0_170314, 0315_BH005_3.0_170314,

0315_BH005_4.0_170314, 0315_BH006_0.0_170314,

0315_BH006_1.0_170314, 0315_BH006_2.0_170314,

0315_BH006_3.0_170314, 0315_BH006_4.0_170314



0315_BH011_0.0_170314, 0315_BH011_1.0_170314,

0315_BH011_2.0_170314, 0315_BH011_3.0_170314,

0315_BH011_4.0_170314, 0315_BH012_0.0_170314,

0315_BH012_1.0_170314, 0315_BH012_2.0_170314,

0315_BH012_3.0_170314, 0315_BH012_4.0_170314,

0315_BH013_0.0_170314, 0315_BH013_1.0_170314,

0315_BH013_2.0_170314, 0315_BH013_3.0_170314,

0315_BH013_4.0_170314, 0315_SD001_170314,

0315_SD002_170314, 0315_QC100_170314,

0315_QC101_170314



0315_BH001_0.0_170315, 0315_BH001_1.0_170315,

0315_BH001_2.0_170315, 0315_BH001_3.0_170315,

0315_BH001_4.0_170315, 0315_BH002_0.0_170315,

0315_BH002_1.0_170315, 0315_BH002_2.0_170315,

0315_BH002_3.0_170315, 0315_BH002_4.0_170315,

0315_BH007_0.0_170315, 0315_BH007_1.0_170315,

0315_BH007_2.0_170315, 0315_BH007_3.0_170315,

0315_BH007_4.0_170315, 0315_BH008_0.0_170315,

0315_BH008_1.0_170315, 0315_BH008_2.0_170315,

0315_BH008_3.0_170315, 0315_BH008_4.0_170315



10 of 18:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project




EP231C: Perfluoroalkyl Sulfonamides - Continued

0315_BH009_0.0_170315, 0315_BH009_1.0_170315,

0315_BH009_2.0_170315, 0315_BH009_3.0_170315,

0315_BH009_4.0_170315, 0315_BH010_0.0_170315,

0315_BH010_1.0_170315, 0315_BH010_2.0_170315,

0315_BH010_3.0_170315, 0315_BH010_4.0_170315,

0315_BH014_0.0_170315, 0315_BH014_1.0_170315,

0315_BH014_2.0_170315, 0315_BH014_3.0_170315,

0315_BH014_4.0_170315, 0315_BH015_0.0_170315,

0315_BH015_1.0_170315, 0315_BH015_2.0_170315,

0315_BH015_3.0_170315, 0315_BH015_4.0_170315,

0315_SD005_170315, 0315_SD007_170315,

0315_QC102_170315, 0315_QC103_170315,

0315_QC104_170315, 0315_QC105_170315,

0315_QC106_170315, 0315_QC107_170315,

0315_QC108_170315



0315_SD003_170316, 0315_SD004_170316,

0315_SD006_170316


11 of 18:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project






0315_BH003_0.0_170314, 0315_BH003_1.0_170314,

0315_BH003_2.0_170314, 0315_BH003_3.0_170314,

0315_BH003_4.0_170314, 0315_BH004_0.0_170314,

0315_BH004_1.0_170314, 0315_BH004_2.0_170314,

0315_BH004_3.0_170314, 0315_BH004_4.0_170314,

0315_BH005_0.0_170314, 0315_BH005_1.0_170314,

0315_BH005_2.0_170314, 0315_BH005_3.0_170314,

0315_BH005_4.0_170314, 0315_BH006_0.0_170314,

0315_BH006_1.0_170314, 0315_BH006_2.0_170314,

0315_BH006_3.0_170314, 0315_BH006_4.0_170314



0315_BH011_0.0_170314, 0315_BH011_1.0_170314,

0315_BH011_2.0_170314, 0315_BH011_3.0_170314,

0315_BH011_4.0_170314, 0315_BH012_0.0_170314,

0315_BH012_1.0_170314, 0315_BH012_2.0_170314,

0315_BH012_3.0_170314, 0315_BH012_4.0_170314,

0315_BH013_0.0_170314, 0315_BH013_1.0_170314,

0315_BH013_2.0_170314, 0315_BH013_3.0_170314,

0315_BH013_4.0_170314, 0315_SD001_170314,

0315_SD002_170314, 0315_QC100_170314,

0315_QC101_170314



0315_BH001_0.0_170315, 0315_BH001_1.0_170315,

0315_BH001_2.0_170315, 0315_BH001_3.0_170315,

0315_BH001_4.0_170315, 0315_BH002_0.0_170315,

0315_BH002_1.0_170315, 0315_BH002_2.0_170315,

0315_BH002_3.0_170315, 0315_BH002_4.0_170315,

0315_BH007_0.0_170315, 0315_BH007_1.0_170315,

0315_BH007_2.0_170315, 0315_BH007_3.0_170315,

0315_BH007_4.0_170315, 0315_BH008_0.0_170315,

0315_BH008_1.0_170315, 0315_BH008_2.0_170315,

0315_BH008_3.0_170315, 0315_BH008_4.0_170315



12 of 18:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project




EP231D: (n:2) Fluorotelomer Sulfonic Acids - Continued

0315_BH009_0.0_170315, 0315_BH009_1.0_170315,

0315_BH009_2.0_170315, 0315_BH009_3.0_170315,

0315_BH009_4.0_170315, 0315_BH010_0.0_170315,

0315_BH010_1.0_170315, 0315_BH010_2.0_170315,

0315_BH010_3.0_170315, 0315_BH010_4.0_170315,

0315_BH014_0.0_170315, 0315_BH014_1.0_170315,

0315_BH014_2.0_170315, 0315_BH014_3.0_170315,

0315_BH014_4.0_170315, 0315_BH015_0.0_170315,

0315_BH015_1.0_170315, 0315_BH015_2.0_170315,

0315_BH015_3.0_170315, 0315_BH015_4.0_170315,

0315_SD005_170315, 0315_SD007_170315,

0315_QC102_170315, 0315_QC103_170315,

0315_QC104_170315, 0315_QC105_170315,

0315_QC106_170315, 0315_QC107_170315,

0315_QC108_170315



0315_SD003_170316, 0315_SD004_170316,

0315_SD006_170316


13 of 18:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project




EP231P: PFAS Sums


0315_BH003_0.0_170314, 0315_BH003_1.0_170314,

0315_BH003_2.0_170314, 0315_BH003_3.0_170314,

0315_BH003_4.0_170314, 0315_BH004_0.0_170314,

0315_BH004_1.0_170314, 0315_BH004_2.0_170314,

0315_BH004_3.0_170314, 0315_BH004_4.0_170314,

0315_BH005_0.0_170314, 0315_BH005_1.0_170314,

0315_BH005_2.0_170314, 0315_BH005_3.0_170314,

0315_BH005_4.0_170314, 0315_BH006_0.0_170314,

0315_BH006_1.0_170314, 0315_BH006_2.0_170314,

0315_BH006_3.0_170314, 0315_BH006_4.0_170314



0315_BH011_0.0_170314, 0315_BH011_1.0_170314,

0315_BH011_2.0_170314, 0315_BH011_3.0_170314,

0315_BH011_4.0_170314, 0315_BH012_0.0_170314,

0315_BH012_1.0_170314, 0315_BH012_2.0_170314,

0315_BH012_3.0_170314, 0315_BH012_4.0_170314,

0315_BH013_0.0_170314, 0315_BH013_1.0_170314,

0315_BH013_2.0_170314, 0315_BH013_3.0_170314,

0315_BH013_4.0_170314, 0315_SD001_170314,

0315_SD002_170314, 0315_QC100_170314,

0315_QC101_170314



0315_BH001_0.0_170315, 0315_BH001_1.0_170315,

0315_BH001_2.0_170315, 0315_BH001_3.0_170315,

0315_BH001_4.0_170315, 0315_BH002_0.0_170315,

0315_BH002_1.0_170315, 0315_BH002_2.0_170315,

0315_BH002_3.0_170315, 0315_BH002_4.0_170315,

0315_BH007_0.0_170315, 0315_BH007_1.0_170315,

0315_BH007_2.0_170315, 0315_BH007_3.0_170315,

0315_BH007_4.0_170315, 0315_BH008_0.0_170315,

0315_BH008_1.0_170315, 0315_BH008_2.0_170315,

0315_BH008_3.0_170315, 0315_BH008_4.0_170315



14 of 18:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project




EP231P: PFAS Sums - Continued

0315_BH009_0.0_170315, 0315_BH009_1.0_170315,

0315_BH009_2.0_170315, 0315_BH009_3.0_170315,

0315_BH009_4.0_170315, 0315_BH010_0.0_170315,

0315_BH010_1.0_170315, 0315_BH010_2.0_170315,

0315_BH010_3.0_170315, 0315_BH010_4.0_170315,

0315_BH014_0.0_170315, 0315_BH014_1.0_170315,

0315_BH014_2.0_170315, 0315_BH014_3.0_170315,

0315_BH014_4.0_170315, 0315_BH015_0.0_170315,

0315_BH015_1.0_170315, 0315_BH015_2.0_170315,

0315_BH015_3.0_170315, 0315_BH015_4.0_170315,

0315_SD005_170315, 0315_SD007_170315,

0315_QC102_170315, 0315_QC103_170315,

0315_QC104_170315, 0315_QC105_170315,

0315_QC106_170315, 0315_QC107_170315,

0315_QC108_170315



0315_SD003_170316, 0315_SD004_170316,

0315_SD006_170316


Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.




HDPE (no PTFE) (EP231X)

0315_QC300_170314 10-Sep-2017---- 20-Mar-2017----14-Mar-2017 ---- üHDPE (no PTFE) (EP231X)

0315_QC301_170315 11-Sep-2017---- 20-Mar-2017----15-Mar-2017 ---- üHDPE (no PTFE) (EP231X-ST)

0315_SW005_170315, 0315_SW007_170315,

0315_QC109_170315

11-Sep-201711-Sep-2017 20-Mar-201720-Mar-201715-Mar-2017 ü ü



0315_MW004_170316, 0315_MW005_170316,

0315_MW006_170316, 0315_QC110_170316


HDPE (no PTFE) (EP231X-ST)

0315_MW007_170316, 0315_MW008_170316 12-Sep-201712-Sep-2017 22-Mar-201722-Mar-201716-Mar-2017 ü ü

15 of 18:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project








0315_SW005_170315, 0315_SW007_170315,

0315_QC109_170315




0315_MW004_170316, 0315_MW005_170316,

0315_MW006_170316, 0315_QC110_170316



0315_MW007_170316, 0315_MW008_170316 12-Sep-201712-Sep-2017 22-Mar-201722-Mar-201716-Mar-2017 ü üEP231C: Perfluoroalkyl Sulfonamides




0315_SW005_170315, 0315_SW007_170315,

0315_QC109_170315




0315_MW004_170316, 0315_MW005_170316,

0315_MW006_170316, 0315_QC110_170316



0315_MW007_170316, 0315_MW008_170316 12-Sep-201712-Sep-2017 22-Mar-201722-Mar-201716-Mar-2017 ü üEP231D: (n:2) Fluorotelomer Sulfonic Acids




0315_SW005_170315, 0315_SW007_170315,

0315_QC109_170315




0315_MW004_170316, 0315_MW005_170316,

0315_MW006_170316, 0315_QC110_170316




16 of 18:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project




EP231P: PFAS Sums




0315_SW005_170315, 0315_SW007_170315,

0315_QC109_170315




0315_MW004_170316, 0315_MW005_170316,

0315_MW006_170316, 0315_QC110_170316




17 of 18:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project

Quality Control Parameter Frequency ComplianceThe following report summarises the frequency of laboratory QC samples analysed within the analytical lot(s) in which the submitted sample(s) was(were) processed. Actual rate should be greater than or equal to

the expected rate. A listing of breaches is provided in the Summary of Outliers.

Matrix: SOIL Evaluation: û = Quality Control frequency not within specification ; ü = Quality Control frequency within specification.


ExpectedQC Regular Actual

Rate (%)Quality Control Sample Type CountEvaluationAnalytical Methods Method


NEPM 2013 B3 & ALS QC Standard 9.80 10.0010 102 ûMoisture Content EA055-103

NEPM 2013 B3 & ALS QC Standard 10.99 10.0010 91 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X

Laboratory Control Samples (LCS)


Method Blanks (MB)


Matrix Spikes (MS)


Matrix: WATER Evaluation: û = Quality Control frequency not within specification ; ü = Quality Control frequency within specification.


ExpectedQC Regular Actual

Rate (%)Quality Control Sample Type CountEvaluationAnalytical Methods Method



NEPM 2013 B3 & ALS QC Standard 11.11 10.001 9 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X-ST

Laboratory Control Samples (LCS)



Method Blanks (MB)



Matrix Spikes (MS)


NEPM 2013 B3 & ALS QC Standard 0.00 5.000 9 ûPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X-ST

18 of 18:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project

Brief Method SummariesThe analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the US EPA, APHA, AS and NEPM. In house

developed procedures are employed in the absence of documented standards or by client request. The following report provides brief descriptions of the analytical procedures employed for results reported in the

Certificate of Analysis. Sources from which ALS methods have been developed are provided within the Method Descriptions.

Analytical Methods Method DescriptionsMatrixMethod

In house: A gravimetric procedure based on weight loss over a 12 hour drying period at 103-105 degrees C.

This method is compliant with NEPM (2013) Schedule B(3) Section 7.1 and Table 1 (14 day holding time).

Moisture Content EA055-103 SOIL

In-House. A portion of soil is extracted with MTBE. The extract is taken to dryness, made up in mobile phase.

Analysis is by LC/MSMS, ESI Negative Mode using MRM. PFOS is quantified using a certified, traceable standard

consisting of linear and branched PFOS isomers.

Per- and Polyfluoroalkyl Substances

(PFAS) by LCMSMS

EP231X SOIL

In house: Direct injection analysis of fresh waters after dilution (1:1) with methanol. Analysis by

LC-Electrospray-MS-MS, Negative Mode using MRM. PFOS is quantified using a certified, traceable standard

consisting of linear and branched PFOS isomers.


(PFAS) by LCMSMS

EP231X WATER

In-house: Analysis of fresh and saline waters by solid phase extraction and LC-Electrospray-MS-MS, Negative

Mode using MRM. This method is targetted to pristine environmental and drinking waters reportin at sub-parts

per trillion. PFOS is quantified using a certified, traceable standard consisting of linear and branched PFOS

isomers.


(PFAS) by LCMSMS

EP231X-ST WATER

Preparation Methods Method DescriptionsMatrixMethod

In houseSample Extraction for PFAS EP231-PR SOIL

In house: Referenced to USEPA SW 846 - 5030A. 5g of solid is shaken with surrogate and 10mL methanol prior

to analysis by Purge and Trap - GC/MS.

Methanolic Extraction of Soils for Purge

and Trap

* ORG16 SOIL

In houseSPE preparation for LL and saline PFCs EP231-SPE WATER

A 5 mL aliquot or 5 mL of a diluted sample is added to a 40 mL VOC vial for sparging.Volatiles Water Preparation ORG16-W WATER

False

2 2.00True

Environmental

QUALITY CONTROL REPORTWork Order : ES1706394 Page : 1 of 31

:Amendment 2


:Contact MS OLGA BUKHTEEVA :Contact Customer Services ES

:Address LEVEL 1, 124 PACIFIC HIGHWAY

ST LEONARDS NSW, AUSTRALIA 2065

Address : 277-289 Woodpark Road Smithfield NSW Australia 2164

::Telephone +61 02 9478 3900 +61-2-8784 8555:Telephone

:Project 1652034 Date Samples Received : 17-Mar-2017

:Order number PO01472 Date Analysis Commenced : 20-Mar-2017

:C-O-C number ---- Issue Date : 10-Apr-2017

Sampler : OLGA BUKHTEEVA

Site : Kapooka

Quote number : BN/404/16

No. of samples received 110:

No. of samples analysed 103:

This report supersedes any previous report(s) with this reference. Results apply to the sample(s) as submitted. This document shall not be reproduced, except in full.

This Quality Control Report contains the following information:

l Laboratory Duplicate (DUP) Report; Relative Percentage Difference (RPD) and Acceptance Limits

l Method Blank (MB) and Laboratory Control Spike (LCS) Report ; Recovery and Acceptance Limits

l Matrix Spike (MS) Report; Recovery and Acceptance Limits

SignatoriesThis document has been electronically signed by the authorized signatories below. Electronic signing is carried out in compliance with procedures specified in 21 CFR Part 11.

Signatories Accreditation CategoryPosition

Alex Rossi Organic Chemist Sydney Organics, Smithfield, NSW

Edwandy Fadjar Organic Coordinator Sydney Inorganics, Smithfield, NSW


2 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project

General Comments

The analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the USEPA, APHA, AS and NEPM. In house

developed procedures are employed in the absence of documented standards or by client request.

Where moisture determination has been performed, results are reported on a dry weight basis.

Where a reported less than (<) result is higher than the LOR, this may be due to primary sample extract/digestate dilution and/or insufficient sample for analysis. Where the LOR of a reported result differs from standard LOR, this may be due to high moisture content, insufficient sample (reduced weight employed) or matrix interference.

Anonymous = Refers to samples which are not specifically part of this work order but formed part of the QC process lot

CAS Number = CAS registry number from database maintained by Chemical Abstracts Services. The Chemical Abstracts Service is a division of the American Chemical Society.

LOR = Limit of reporting

RPD = Relative Percentage Difference

# = Indicates failed QC

Key :

Laboratory Duplicate (DUP) Report

The quality control term Laboratory Duplicate refers to a randomly selected intralaboratory split. Laboratory duplicates provide information regarding method precision and sample heterogeneity. The permitted ranges

for the Relative Percent Deviation (RPD) of Laboratory Duplicates are specified in ALS Method QWI -EN/38 and are dependent on the magnitude of results in comparison to the level of reporting: Result < 10 times LOR:

No Limit; Result between 10 and 20 times LOR: 0% - 50%; Result > 20 times LOR: 0% - 20%.

Sub-Matrix: SOIL Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EA055: Moisture Content (QC Lot: 799429)

EA055-103: Moisture Content (dried @ 103°C) ---- 1 % 7.9 7.7 3.38 No LimitAnonymous ES1706332-058

EA055-103: Moisture Content (dried @ 103°C) ---- 1 % 20.1 21.2 4.95 0% - 20%0315_BH002_3.0_170315 ES1706394-009





EA055-103: Moisture Content (dried @ 103°C) ---- 1 % 8.4 8.1 3.14 No Limit0315_BH007_1.0_170315 ES1706394-032







EA055-103: Moisture Content (dried @ 103°C) ---- 1 % 2.8 2.9 0.00 No Limit0315_QC100_170314 ES1706394-091

EP231A: Perfluoroalkyl Sulfonic Acids (QC Lot: 798130)

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0002 mg/kg 0.0009 0.0009 0.00 No Limit0315_BH001_0.0_170315 ES1706394-001

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0002 mg/kg 0.0015 0.0015 0.00 No Limit

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0002 mg/kg 0.0518 0.0534 3.17 0% - 20%

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0002 mg/kg 0.0013 0.0014 7.26 No Limit

EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0002 mg/kg 1.15 1.11 3.79 0% - 20%

EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0002 mg/kg 0.0172 0.0156 9.49 0% - 20%

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0002 mg/kg 0.0020 0.0016 17.9 No Limit0315_BH003_0.0_170314 ES1706394-011

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0002 mg/kg 0.0024 0.0021 11.4 0% - 50%


3 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project



EP231A: Perfluoroalkyl Sulfonic Acids (QC Lot: 798130) - continued

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0002 mg/kg 0.0054 0.0052 3.59 0% - 20%0315_BH003_0.0_170314 ES1706394-011


EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0002 mg/kg 0.0273 0.0279 2.10 0% - 20%


EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_BH005_0.0_170314 ES1706394-021

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0002 mg/kg 0.0003 0.0004 0.00 No Limit

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit


EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit









EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0002 mg/kg <0.0002 0.0002 0.00 No Limit


EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0002 mg/kg 0.0020 0.0018 10.2 No Limit





EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit


EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0002 mg/kg 0.0008 0.0008 0.00 No Limit













4 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project




EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0002 mg/kg 0.0012 0.0014 13.5 No Limit0315_BH015_0.0_170315 ES1706394-071



EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_SD006_170316 ES1706394-089




EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0002 mg/kg 0.0015 0.0016 0.00 No Limit


EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_QC108_170315 ES1706394-099






EP231B: Perfluoroalkyl Carboxylic Acids (QC Lot: 798130)

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_BH001_0.0_170315 ES1706394-001

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0002 mg/kg 0.0085 0.0091 6.33 0% - 20%

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0002 mg/kg 0.0013 0.0015 16.0 No Limit

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg 0.0050 0.0052 4.40 0% - 20%

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.0002 mg/kg 0.0004 0.0005 0.00 No Limit

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.0002 mg/kg 0.0009 0.0009 0.00 No Limit

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit

EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit

EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.001 mg/kg 0.014 0.013 0.00 0% - 50%

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0002 mg/kg 0.0049 0.0046 6.10 0% - 20%0315_BH003_0.0_170314 ES1706394-011


EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0002 mg/kg 0.0024 0.0021 14.3 0% - 50%

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg 0.0078 0.0075 4.38 0% - 20%

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.0002 mg/kg 0.0034 0.0032 6.40 0% - 50%

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.0002 mg/kg 0.0044 0.0041 5.55 0% - 20%

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0002 mg/kg 0.0024 0.0027 9.41 0% - 50%

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0002 mg/kg 0.0043 0.0046 5.03 0% - 20%

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0002 mg/kg 0.0016 0.0015 0.00 No Limit


EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.001 mg/kg <0.001 <0.001 0.00 No Limit



5 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project



EP231B: Perfluoroalkyl Carboxylic Acids (QC Lot: 798131) - continued

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_BH005_0.0_170314 ES1706394-021

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg <0.0002 0.0002 0.00 No Limit

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.0002 mg/kg <0.0002 0.0002 0.00 No Limit

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit






EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0002 mg/kg 0.0006 <0.0002 105 No Limit0315_BH007_0.0_170315 ES1706394-031

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0002 mg/kg 0.0002 <0.0002 0.00 No Limit


EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg 0.0002 0.0002 0.00 No Limit

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit









EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0002 mg/kg 0.0009 0.0010 15.0 No Limit











EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit






6 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project




EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_BH011_0.0_170314 ES1706394-051





EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0002 mg/kg 0.0030 0.0034 10.8 0% - 50%0315_BH013_0.0_170314 ES1706394-061


EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0002 mg/kg 0.0020 0.0022 7.72 0% - 50%


EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.0002 mg/kg 0.0009 0.0006 40.0 No Limit










EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit









EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_SD006_170316 ES1706394-089











EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0002 mg/kg 0.0072 0.0077 6.10 0% - 20%0315_QC108_170315 ES1706394-099

7 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project




EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_QC108_170315 ES1706394-099




EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.0002 mg/kg 0.0002 <0.0002 0.00 No Limit






EP231C: Perfluoroalkyl Sulfonamides (QC Lot: 798130)

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0002 mg/kg 0.0112 0.0114 2.46 0% - 20%0315_BH001_0.0_170315 ES1706394-001

EP231X: N-Methyl perfluorooctane

sulfonamidoacetic acid (MeFOSAA)

2355-31-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit

EP231X: N-Ethyl perfluorooctane

sulfonamidoacetic acid (EtFOSAA)

2991-50-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit

EP231X: N-Methyl perfluorooctane sulfonamide

(MeFOSA)

31506-32-8 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit

EP231X: N-Ethyl perfluorooctane sulfonamide

(EtFOSA)

4151-50-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


sulfonamidoethanol (MeFOSE)

2448-09-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


sulfonamidoethanol (EtFOSE)

1691-99-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0002 mg/kg 0.0477 0.0470 1.51 0% - 20%0315_BH003_0.0_170314 ES1706394-011



2355-31-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit



2991-50-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit


(MeFOSA)

31506-32-8 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


(EtFOSA)

4151-50-2 0.0005 mg/kg 0.0007 0.0007 0.00 No Limit



2448-09-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit



1691-99-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_BH005_0.0_170314 ES1706394-021



2355-31-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit

8 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project



EP231C: Perfluoroalkyl Sulfonamides (QC Lot: 798131) - continued



2991-50-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_BH005_0.0_170314 ES1706394-021


(MeFOSA)

31506-32-8 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


(EtFOSA)

4151-50-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit



2448-09-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit



1691-99-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit




2355-31-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit



2991-50-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit


(MeFOSA)

31506-32-8 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


(EtFOSA)

4151-50-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit



2448-09-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit



1691-99-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0002 mg/kg 0.0010 0.0012 10.8 No Limit0315_BH009_0.0_170315 ES1706394-041



2355-31-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit



2991-50-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit


(MeFOSA)

31506-32-8 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


(EtFOSA)

4151-50-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit



2448-09-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit



1691-99-2 0.0005 mg/kg <0.0005 0.0005 0.00 No Limit




2355-31-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit

9 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project








(MeFOSA)

31506-32-8 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


(EtFOSA)

4151-50-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit



2448-09-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit



1691-99-2 0.0005 mg/kg 0.0009 <0.0005 61.5 No Limit





2355-31-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit



2991-50-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit


(MeFOSA)

31506-32-8 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


(EtFOSA)

4151-50-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit



2448-09-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit



1691-99-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit




2355-31-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit



2991-50-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit


(MeFOSA)

31506-32-8 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


(EtFOSA)

4151-50-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit



2448-09-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit



1691-99-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_SD006_170316 ES1706394-089



2355-31-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit

10 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project






2991-50-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_SD006_170316 ES1706394-089


(MeFOSA)

31506-32-8 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


(EtFOSA)

4151-50-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit



2448-09-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit



1691-99-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_QC108_170315 ES1706394-099



2355-31-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit



2991-50-6 0.0002 mg/kg <0.0002 0.0002 0.00 No Limit


(MeFOSA)

31506-32-8 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


(EtFOSA)

4151-50-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit



2448-09-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit



1691-99-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QC Lot: 798130)

EP231X: 4:2 Fluorotelomer sulfonic acid (4:2

FTS)



FTS)

27619-97-2 0.0005 mg/kg 0.0032 0.0032 0.00 No Limit


FTS)

39108-34-4 0.0005 mg/kg 0.0064 0.0053 19.0 0% - 50%


FTS)

120226-60-0 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


FTS)



FTS)

27619-97-2 0.0005 mg/kg 0.0036 0.0031 16.4 No Limit


FTS)

39108-34-4 0.0005 mg/kg 0.0057 0.0050 13.1 0% - 50%


FTS)

120226-60-0 0.0005 mg/kg 0.0006 <0.0005 0.00 No Limit


11 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project



EP231D: (n:2) Fluorotelomer Sulfonic Acids (QC Lot: 798131) - continued


FTS)



FTS)

27619-97-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


FTS)

39108-34-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


FTS)

120226-60-0 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


FTS)



FTS)

27619-97-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


FTS)

39108-34-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


FTS)

120226-60-0 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit



FTS)



FTS)

27619-97-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


FTS)

39108-34-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


FTS)

120226-60-0 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


FTS)



FTS)

27619-97-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


FTS)

39108-34-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


FTS)

120226-60-0 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit



FTS)



FTS)

27619-97-2 0.0005 mg/kg 0.0060 0.0051 15.0 0% - 50%


FTS)

39108-34-4 0.0005 mg/kg 0.0018 0.0022 20.2 No Limit

12 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project



EP231D: (n:2) Fluorotelomer Sulfonic Acids (QC Lot: 798133) - continued


FTS)



FTS)



FTS)

27619-97-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


FTS)

39108-34-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


FTS)

120226-60-0 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit



FTS)

757124-72-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit0315_SD006_170316 ES1706394-089


FTS)

27619-97-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


FTS)

39108-34-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


FTS)

120226-60-0 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


FTS)

757124-72-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit0315_QC108_170315 ES1706394-099


FTS)

27619-97-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


FTS)

39108-34-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit


FTS)

120226-60-0 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit

Sub-Matrix: WATER Laboratory Duplicate (DUP) Report



EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.01 µg/L 0.20 0.20 0.00 0% - 20%Anonymous EB1705137-001

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.02 µg/L 0.04 0.04 0.00 No Limit

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.02 µg/L 0.03 0.04 0.00 No Limit

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.02 µg/L 0.23 0.21 7.64 0% - 50%

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.01 µg/L 0.03 0.04 0.00 No LimitAnonymous ES1706387-002

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.02 µg/L 0.06 0.06 0.00 No Limit

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

13 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project




EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.02 µg/L <0.02 <0.02 0.00 No LimitAnonymous ES1706387-002


EP231X-ST: Perfluorooctane sulfonic acid

(PFOS)

1763-23-1 0.0003 µg/L <0.0003 <0.0003 0.00 No Limit0315_MW007_170316 ES1706394-079

EP231X-ST: Perfluorobutane sulfonic acid

(PFBS)

375-73-5 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit

EP231X-ST: Perfluoropentane sulfonic acid

(PFPeS)

2706-91-4 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit

EP231X-ST: Perfluorohexane sulfonic acid

(PFHxS)

355-46-4 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit

EP231X-ST: Perfluoroheptane sulfonic acid

(PFHpS)

375-92-8 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit

EP231X-ST: Perfluorodecane sulfonic acid

(PFDS)

335-77-3 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit


EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.01 µg/L 0.03 0.03 0.00 No LimitAnonymous EB1705137-001

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.02 µg/L 0.05 0.04 0.00 No Limit

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.02 µg/L 0.07 0.06 0.00 No Limit

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.02 µg/L 0.02 0.02 0.00 No Limit

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.1 µg/L <0.1 <0.1 0.00 No Limit

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.01 µg/L <0.01 <0.01 0.00 No LimitAnonymous ES1706387-002

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.02 µg/L 0.08 0.08 0.00 No Limit

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.02 µg/L 0.12 0.12 0.00 No Limit

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.1 µg/L <0.1 <0.1 0.00 No Limit


EP231X-ST: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit0315_MW007_170316 ES1706394-079

EP231X-ST: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit

14 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project




EP231X-ST: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit0315_MW007_170316 ES1706394-079

EP231X-ST: Perfluorooctanoic acid (PFOA) 335-67-1 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit

EP231X-ST: Perfluorononanoic acid (PFNA) 375-95-1 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit

EP231X-ST: Perfluorodecanoic acid (PFDA) 335-76-2 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit

EP231X-ST: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit

EP231X-ST: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit

EP231X-ST: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit

EP231X-ST: Perfluorotetradecanoic acid

(PFTeDA)

376-06-7 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit

EP231X-ST: Perfluorobutanoic acid (PFBA) 375-22-4 0.002 µg/L <0.002 <0.002 0.00 No Limit


EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.02 µg/L <0.02 <0.02 0.00 No LimitAnonymous EB1705137-001



2355-31-9 0.02 µg/L <0.02 <0.02 0.00 No Limit



2991-50-6 0.02 µg/L <0.02 <0.02 0.00 No Limit


(MeFOSA)

31506-32-8 0.05 µg/L <0.05 <0.05 0.00 No Limit


(EtFOSA)

4151-50-2 0.05 µg/L <0.05 <0.05 0.00 No Limit



2448-09-7 0.05 µg/L <0.05 <0.05 0.00 No Limit



1691-99-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.02 µg/L <0.02 <0.02 0.00 No LimitAnonymous ES1706387-002



2355-31-9 0.02 µg/L <0.02 <0.02 0.00 No Limit



2991-50-6 0.02 µg/L <0.02 <0.02 0.00 No Limit


(MeFOSA)

31506-32-8 0.05 µg/L <0.05 <0.05 0.00 No Limit


(EtFOSA)

4151-50-2 0.05 µg/L <0.05 <0.05 0.00 No Limit



2448-09-7 0.05 µg/L <0.05 <0.05 0.00 No Limit



1691-99-2 0.05 µg/L <0.05 <0.05 0.00 No Limit


EP231X-ST: Perfluorooctane sulfonamide

(FOSA)

754-91-6 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit0315_MW007_170316 ES1706394-079

15 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project




EP231X-ST: N-Methyl perfluorooctane


2355-31-9 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit0315_MW007_170316 ES1706394-079

EP231X-ST: N-Ethyl perfluorooctane


2991-50-6 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit


sulfonamide (MeFOSA)

31506-32-8 0.001 µg/L <0.001 <0.001 0.00 No Limit

EP231X-ST: N-Ethyl perfluorooctane sulfonamide

(EtFOSA)

4151-50-2 0.001 µg/L <0.001 <0.001 0.00 No Limit



2448-09-7 0.001 µg/L <0.001 <0.001 0.00 No Limit

EP231X-ST: N-Ethyl perfluorooctane


1691-99-2 0.001 µg/L <0.001 <0.001 0.00 No Limit



FTS)

757124-72-4 0.05 µg/L <0.05 <0.05 0.00 No LimitAnonymous EB1705137-001


FTS)

27619-97-2 0.05 µg/L <0.05 <0.05 0.00 No Limit


FTS)

39108-34-4 0.05 µg/L <0.05 <0.05 0.00 No Limit


FTS)

120226-60-0 0.05 µg/L <0.05 <0.05 0.00 No Limit


FTS)

757124-72-4 0.05 µg/L <0.05 <0.05 0.00 No LimitAnonymous ES1706387-002


FTS)

27619-97-2 0.05 µg/L <0.05 <0.05 0.00 No Limit


FTS)

39108-34-4 0.05 µg/L <0.05 <0.05 0.00 No Limit


FTS)

120226-60-0 0.05 µg/L <0.05 <0.05 0.00 No Limit


EP231X-ST: 4:2 Fluorotelomer sulfonic acid (4:2

FTS)

757124-72-4 0.001 µg/L <0.001 <0.001 0.00 No Limit0315_MW007_170316 ES1706394-079


FTS)

27619-97-2 0.001 µg/L <0.001 <0.001 0.00 No Limit


FTS)

39108-34-4 0.001 µg/L <0.001 <0.001 0.00 No Limit

EP231X-ST: 10:2 Fluorotelomer sulfonic acid

(10:2 FTS)

120226-60-0 0.001 µg/L <0.001 <0.001 0.00 No Limit

EP231P: PFAS Sums (QC Lot: 798141)

EP231X: Sum of PFAS ---- 0.01 µg/L 0.67 0.64 4.58 0% - 20%Anonymous EB1705137-001

EP231X: Sum of PFAS ---- 0.01 µg/L 0.29 0.30 3.39 0% - 20%Anonymous ES1706387-002

16 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project



EP231P: PFAS Sums (QC Lot: 803834)

EP231X-ST: Sum of PFAS ---- 0.0003 µg/L <0.0003 <0.0003 0.00 No Limit0315_MW007_170316 ES1706394-079

17 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project

Method Blank (MB) and Laboratory Control Spike (LCS) Report

The quality control term Method / Laboratory Blank refers to an analyte free matrix to which all reagents are added in the same volumes or proportions as used in standard sample preparation. The purpose of this QC

parameter is to monitor potential laboratory contamination. The quality control term Laboratory Control Spike (LCS) refers to a certified reference material, or a known interference free matrix spiked with target

analytes. The purpose of this QC parameter is to monitor method precision and accuracy independent of sample matrix. Dynamic Recovery Limits are based on statistical evaluation of processed LCS.

Sub-Matrix: SOIL Method Blank (MB)

Report

Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 798130)

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0002 mg/kg <0.0002 58.80.00125 mg/kg 12157

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0002 mg/kg <0.0002 58.80.00125 mg/kg 12555

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0002 mg/kg <0.0002 54.70.00125 mg/kg 12652

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0002 mg/kg <0.0002 83.80.00125 mg/kg 12354

EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0002 mg/kg <0.0002 79.20.00125 mg/kg 12755

EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0002 mg/kg <0.0002 69.00.00125 mg/kg 12554





























18 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project


Report




EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 798130)

EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.001 mg/kg <0.001 52.30.00625 mg/kg 12852

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0002 mg/kg <0.0002 72.50.00125 mg/kg 12954

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0002 mg/kg <0.0002 66.60.00125 mg/kg 12758

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0002 mg/kg <0.0002 76.20.00125 mg/kg 12857

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg <0.0002 1070.00125 mg/kg 13460

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.0002 mg/kg <0.0002 1160.00125 mg/kg 13063

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.0002 mg/kg <0.0002 1120.00125 mg/kg 13055

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0002 mg/kg <0.0002 86.50.00125 mg/kg 13062

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0002 mg/kg <0.0002 1010.00125 mg/kg 13453

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0002 mg/kg <0.0002 85.40.00125 mg/kg 12949

EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 mg/kg <0.0005 94.90.00312 mg/kg 12959






EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg <0.0002 97.30.00125 mg/kg 13460


EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.0002 mg/kg <0.0002 1000.00125 mg/kg 13055


EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0002 mg/kg <0.0002 55.20.00125 mg/kg 13453


EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 mg/kg <0.0005 78.00.00312 mg/kg 12959





EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0002 mg/kg <0.0002 1020.00125 mg/kg 12857



EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.0002 mg/kg <0.0002 95.30.00125 mg/kg 13055

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0002 mg/kg <0.0002 1070.00125 mg/kg 13062



EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 mg/kg <0.0005 1170.00312 mg/kg 12959


EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.001 mg/kg <0.001 1230.00625 mg/kg 12852


19 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project


Report




EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 798133) - continued














EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0002 mg/kg <0.0002 1040.00125 mg/kg 12857

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg <0.0002 1090.00125 mg/kg 13460



EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0002 mg/kg <0.0002 1060.00125 mg/kg 13062

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0002 mg/kg <0.0002 1240.00125 mg/kg 13453

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0002 mg/kg <0.0002 1220.00125 mg/kg 12949


EP231C: Perfluoroalkyl Sulfonamides (QCLot: 798130)

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0002 mg/kg <0.0002 89.50.00125 mg/kg 13252

EP231X: N-Methyl perfluorooctane sulfonamide (MeFOSA) 31506-32-8 0.0005 mg/kg <0.0005 92.60.00312 mg/kg 12665

EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 4151-50-2 0.0005 mg/kg <0.0005 73.50.00312 mg/kg 12664

EP231X: N-Methyl perfluorooctane sulfonamidoethanol

(MeFOSE)

2448-09-7 0.0005 mg/kg <0.0005 76.10.00312 mg/kg 12463

EP231X: N-Ethyl perfluorooctane sulfonamidoethanol

(EtFOSE)

1691-99-2 0.0005 mg/kg <0.0005 69.70.00312 mg/kg 12558

EP231X: N-Methyl perfluorooctane sulfonamidoacetic acid

(MeFOSAA)

2355-31-9 0.0002 mg/kg <0.0002 1060.00125 mg/kg 13061

EP231X: N-Ethyl perfluorooctane sulfonamidoacetic acid

(EtFOSAA)

2991-50-6 0.0002 mg/kg <0.0002 72.30.00125 mg/kg 13055






(MeFOSE)

2448-09-7 0.0005 mg/kg <0.0005 68.10.00312 mg/kg 12463

20 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project


Report




EP231C: Perfluoroalkyl Sulfonamides (QCLot: 798131) - continued


(EtFOSE)

1691-99-2 0.0005 mg/kg <0.0005 66.20.00312 mg/kg 12558


(MeFOSAA)

2355-31-9 0.0002 mg/kg <0.0002 1240.00125 mg/kg 13061


(EtFOSAA)

2991-50-6 0.0002 mg/kg <0.0002 75.30.00125 mg/kg 13055



EP231X: N-Methyl perfluorooctane sulfonamide (MeFOSA) 31506-32-8 0.0005 mg/kg <0.0005 1000.00312 mg/kg 12665



(MeFOSE)

2448-09-7 0.0005 mg/kg <0.0005 1230.00312 mg/kg 12463


(EtFOSE)

1691-99-2 0.0005 mg/kg <0.0005 66.00.00312 mg/kg 12558


(MeFOSAA)

2355-31-9 0.0002 mg/kg <0.0002 1290.00125 mg/kg 13061


(EtFOSAA)

2991-50-6 0.0002 mg/kg <0.0002 1230.00125 mg/kg 13055






(MeFOSE)

2448-09-7 0.0005 mg/kg <0.0005 1210.00312 mg/kg 12463


(EtFOSE)

1691-99-2 0.0005 mg/kg <0.0005 70.00.00312 mg/kg 12558


(MeFOSAA)

2355-31-9 0.0002 mg/kg <0.0002 1050.00125 mg/kg 13061


(EtFOSAA)

2991-50-6 0.0002 mg/kg <0.0002 1010.00125 mg/kg 13055



EP231X: N-Methyl perfluorooctane sulfonamide (MeFOSA) 31506-32-8 0.0005 mg/kg <0.0005 1080.00312 mg/kg 12665

EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 4151-50-2 0.0005 mg/kg <0.0005 1000.00312 mg/kg 12664


(MeFOSE)

2448-09-7 0.0005 mg/kg <0.0005 1160.00312 mg/kg 12463


(EtFOSE)

1691-99-2 0.0005 mg/kg <0.0005 86.30.00312 mg/kg 12558

21 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project


Report






(MeFOSAA)

2355-31-9 0.0002 mg/kg <0.0002 1230.00125 mg/kg 13061


(EtFOSAA)

2991-50-6 0.0002 mg/kg <0.0002 88.20.00125 mg/kg 13055

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 798130)

EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 757124-72-4 0.0005 mg/kg <0.0005 56.70.00125 mg/kg 13054


EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 39108-34-4 0.0005 mg/kg <0.0005 1100.00125 mg/kg 13062






















Sub-Matrix: WATER Method Blank (MB)

Report





EP231X-ST: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0005 µg/L <0.0005 80.40.01 µg/L 13050

EP231X-ST: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0005 µg/L <0.0005 85.20.01 µg/L 13050

EP231X-ST: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0005 µg/L <0.0005 85.20.01 µg/L 13050

EP231X-ST: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0005 µg/L <0.0005 83.40.01 µg/L 13050

EP231X-ST: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0003 µg/L <0.0003 96.00.01 µg/L 13050

22 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project


Report




EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 798127) - continued

EP231X-ST: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0005 µg/L <0.0005 1070.01 µg/L 13050


EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.02 µg/L <0.02 84.80.5 µg/L 13070

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.02 µg/L <0.02 1070.5 µg/L 13070

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.02 µg/L <0.02 1120.5 µg/L 13070

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.02 µg/L <0.02 89.40.5 µg/L 13070

EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.01 µg/L <0.01 1030.5 µg/L 13070

EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.02 µg/L <0.02 93.00.5 µg/L 13070


EP231X-ST: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0005 µg/L <0.0005 1120.01 µg/L 13050

EP231X-ST: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0005 µg/L <0.0005 92.20.01 µg/L 13050

EP231X-ST: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0005 µg/L <0.0005 86.00.01 µg/L 13050

EP231X-ST: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0005 µg/L <0.0005 1000.01 µg/L 13050

EP231X-ST: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0003 µg/L <0.0003 1040.01 µg/L 13050

EP231X-ST: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0005 µg/L <0.0005 92.40.01 µg/L 13050


EP231X-ST: Perfluorobutanoic acid (PFBA) 375-22-4 0.002 µg/L <0.002 77.60.05 µg/L 13050

EP231X-ST: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0005 µg/L <0.0005 80.80.01 µg/L 13050

EP231X-ST: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0005 µg/L <0.0005 83.60.01 µg/L 13050

EP231X-ST: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0005 µg/L <0.0005 81.00.01 µg/L 13050

EP231X-ST: Perfluorooctanoic acid (PFOA) 335-67-1 0.0005 µg/L <0.0005 85.80.01 µg/L 13050

EP231X-ST: Perfluorononanoic acid (PFNA) 375-95-1 0.0005 µg/L <0.0005 87.80.01 µg/L 13050

EP231X-ST: Perfluorodecanoic acid (PFDA) 335-76-2 0.0005 µg/L <0.0005 89.20.01 µg/L 13050

EP231X-ST: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0005 µg/L <0.0005 92.00.01 µg/L 13050

EP231X-ST: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0005 µg/L <0.0005 83.40.01 µg/L 13050

EP231X-ST: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0005 µg/L <0.0005 97.20.01 µg/L 13050

EP231X-ST: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 µg/L <0.0005 77.00.025 µg/L 13050


EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.1 µg/L <0.1 92.02.5 µg/L 13070

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.02 µg/L <0.02 91.60.5 µg/L 13070

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.02 µg/L <0.02 1040.5 µg/L 13070

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.02 µg/L <0.02 1140.5 µg/L 13070

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.01 µg/L <0.01 89.20.5 µg/L 13070

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.02 µg/L <0.02 96.80.5 µg/L 13070

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.02 µg/L <0.02 87.80.5 µg/L 13070

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.02 µg/L <0.02 82.00.5 µg/L 13070

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.02 µg/L <0.02 1160.5 µg/L 13070

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.02 µg/L <0.02 94.60.5 µg/L 13070

23 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project


Report





EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.05 µg/L <0.05 1111.25 µg/L 12470


EP231X-ST: Perfluorobutanoic acid (PFBA) 375-22-4 0.002 µg/L <0.002 84.20.05 µg/L 13050

EP231X-ST: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0005 µg/L <0.0005 66.60.01 µg/L 13050

EP231X-ST: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0005 µg/L <0.0005 81.40.01 µg/L 13050

EP231X-ST: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0005 µg/L <0.0005 83.40.01 µg/L 13050

EP231X-ST: Perfluorooctanoic acid (PFOA) 335-67-1 0.0005 µg/L <0.0005 87.80.01 µg/L 13050

EP231X-ST: Perfluorononanoic acid (PFNA) 375-95-1 0.0005 µg/L <0.0005 84.20.01 µg/L 13050

EP231X-ST: Perfluorodecanoic acid (PFDA) 335-76-2 0.0005 µg/L <0.0005 97.00.01 µg/L 13050

EP231X-ST: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0005 µg/L <0.0005 76.00.01 µg/L 13050

EP231X-ST: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0005 µg/L <0.0005 88.80.01 µg/L 13050

EP231X-ST: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0005 µg/L <0.0005 89.60.01 µg/L 13050

EP231X-ST: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 µg/L <0.0005 1100.025 µg/L 13050


EP231X-ST: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0005 µg/L <0.0005 77.80.01 µg/L 13050

EP231X-ST: N-Methyl perfluorooctane sulfonamide

(MeFOSA)

31506-32-8 0.001 µg/L <0.001 89.00.025 µg/L 13050

EP231X-ST: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 4151-50-2 0.001 µg/L <0.001 84.20.025 µg/L 13050

EP231X-ST: N-Methyl perfluorooctane sulfonamidoethanol

(MeFOSE)

2448-09-7 0.001 µg/L <0.001 96.20.025 µg/L 13050

EP231X-ST: N-Ethyl perfluorooctane sulfonamidoethanol

(EtFOSE)

1691-99-2 0.001 µg/L <0.001 86.60.025 µg/L 13050

EP231X-ST: N-Methyl perfluorooctane sulfonamidoacetic

acid (MeFOSAA)

2355-31-9 0.0005 µg/L <0.0005 80.40.01 µg/L 13050

EP231X-ST: N-Ethyl perfluorooctane sulfonamidoacetic

acid (EtFOSAA)

2991-50-6 0.0005 µg/L <0.0005 83.00.01 µg/L 13050


EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.02 µg/L <0.02 1190.5 µg/L 13070

EP231X: N-Methyl perfluorooctane sulfonamide (MeFOSA) 31506-32-8 0.05 µg/L <0.05 93.31.25 µg/L 13070

EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 4151-50-2 0.05 µg/L <0.05 95.41.25 µg/L 12970


(MeFOSE)

2448-09-7 0.05 µg/L <0.05 87.91.25 µg/L 12970


(EtFOSE)

1691-99-2 0.05 µg/L <0.05 1041.25 µg/L 12670


(MeFOSAA)

2355-31-9 0.02 µg/L <0.02 1190.5 µg/L 13070


(EtFOSAA)

2991-50-6 0.02 µg/L <0.02 1040.5 µg/L 13070


24 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project


Report





EP231X-ST: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0005 µg/L <0.0005 99.60.01 µg/L 13050

EP231X-ST: N-Methyl perfluorooctane sulfonamide

(MeFOSA)

31506-32-8 0.001 µg/L <0.001 80.40.025 µg/L 13050

EP231X-ST: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 4151-50-2 0.001 µg/L <0.001 88.20.025 µg/L 13050

EP231X-ST: N-Methyl perfluorooctane sulfonamidoethanol

(MeFOSE)

2448-09-7 0.001 µg/L <0.001 96.30.025 µg/L 13050

EP231X-ST: N-Ethyl perfluorooctane sulfonamidoethanol

(EtFOSE)

1691-99-2 0.001 µg/L <0.001 96.90.025 µg/L 13050

EP231X-ST: N-Methyl perfluorooctane sulfonamidoacetic

acid (MeFOSAA)

2355-31-9 0.0005 µg/L <0.0005 78.20.01 µg/L 13050

EP231X-ST: N-Ethyl perfluorooctane sulfonamidoacetic

acid (EtFOSAA)

2991-50-6 0.0005 µg/L <0.0005 85.40.01 µg/L 13050


EP231X-ST: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 757124-72-4 0.001 µg/L <0.001 82.40.01 µg/L 13050



EP231X-ST: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 120226-60-0 0.001 µg/L <0.001 1100.01 µg/L 13050


EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 757124-72-4 0.05 µg/L <0.05 95.80.5 µg/L 13070

EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 27619-97-2 0.05 µg/L <0.05 1190.5 µg/L 13070








EP231P: PFAS Sums (QCLot: 798127)

EP231X-ST: Sum of PFAS ---- 0.0003 µg/L <0.0003 -------- --------

EP231P: PFAS Sums (QCLot: 803834)

EP231X-ST: Sum of PFAS ---- 0.0003 µg/L <0.0003 -------- --------

Matrix Spike (MS) ReportThe quality control term Matrix Spike (MS) refers to an intralaboratory split sample spiked with a representative set of target analytes. The purpose of this QC parameter is to monitor potential matrix effects on

analyte recoveries. Static Recovery Limits as per laboratory Data Quality Objectives (DQOs). Ideal recovery ranges stated may be waived in the event of sample matrix interference.

Sub-Matrix: SOIL Matrix Spike (MS) Report

SpikeRecovery(%) Recovery Limits (%)Spike

25 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project



HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number


0315_BH001_0.0_170315 ES1706394-001 375-73-5EP231X: Perfluorobutane sulfonic acid (PFBS) 51.20.00125 mg/kg 13050

2706-91-4EP231X: Perfluoropentane sulfonic acid (PFPeS) 75.30.00125 mg/kg 13050

355-46-4EP231X: Perfluorohexane sulfonic acid (PFHxS) # Not

Determined

0.00125 mg/kg 13050

375-92-8EP231X: Perfluoroheptane sulfonic acid (PFHpS) 1040.00125 mg/kg 13050

1763-23-1EP231X: Perfluorooctane sulfonic acid (PFOS) # Not

Determined

0.00125 mg/kg 13050

335-77-3EP231X: Perfluorodecane sulfonic acid (PFDS) # Not

Determined

0.00125 mg/kg 13050




355-46-4EP231X: Perfluorohexane sulfonic acid (PFHxS) 89.40.00125 mg/kg 13050

375-92-8EP231X: Perfluoroheptane sulfonic acid (PFHpS) 68.20.00125 mg/kg 13050


Determined

0.00125 mg/kg 13050

335-77-3EP231X: Perfluorodecane sulfonic acid (PFDS) 1100.00125 mg/kg 13050







Determined

0.00125 mg/kg 13050

335-77-3EP231X: Perfluorodecane sulfonic acid (PFDS) 1070.00125 mg/kg 13050


0315_BH013_0.0_170314 ES1706394-061 375-73-5EP231X: Perfluorobutane sulfonic acid (PFBS) 1110.00125 mg/kg 13050

2706-91-4EP231X: Perfluoropentane sulfonic acid (PFPeS) 1070.00125 mg/kg 13050




Determined

0.00125 mg/kg 13050

335-77-3EP231X: Perfluorodecane sulfonic acid (PFDS) 56.00.00125 mg/kg 13050


0315_SD006_170316 ES1706394-089 375-73-5EP231X: Perfluorobutane sulfonic acid (PFBS) 1080.00125 mg/kg 13050

2706-91-4EP231X: Perfluoropentane sulfonic acid (PFPeS) 1020.00125 mg/kg 13050



26 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project




EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 798138) - continued

0315_SD006_170316 ES1706394-089 1763-23-1EP231X: Perfluorooctane sulfonic acid (PFOS) 99.60.00125 mg/kg 13050

335-77-3EP231X: Perfluorodecane sulfonic acid (PFDS) 77.20.00125 mg/kg 13050


0315_BH001_0.0_170315 ES1706394-001 375-22-4EP231X: Perfluorobutanoic acid (PFBA) 1250.00625 mg/kg 13030

2706-90-3EP231X: Perfluoropentanoic acid (PFPeA) # 36.20.00125 mg/kg 13050

307-24-4EP231X: Perfluorohexanoic acid (PFHxA) # Not

Determined

0.00125 mg/kg 13050

375-85-9EP231X: Perfluoroheptanoic acid (PFHpA) 90.40.00125 mg/kg 13050

335-67-1EP231X: Perfluorooctanoic acid (PFOA) 99.60.00125 mg/kg 13050

375-95-1EP231X: Perfluorononanoic acid (PFNA) 90.00.00125 mg/kg 13050

335-76-2EP231X: Perfluorodecanoic acid (PFDA) 96.40.00125 mg/kg 13050

2058-94-8EP231X: Perfluoroundecanoic acid (PFUnDA) 58.80.00125 mg/kg 13050

307-55-1EP231X: Perfluorododecanoic acid (PFDoDA) 1200.00125 mg/kg 13050

72629-94-8EP231X: Perfluorotridecanoic acid (PFTrDA) 58.40.00125 mg/kg 13030

376-06-7EP231X: Perfluorotetradecanoic acid (PFTeDA) # 18.20.00312 mg/kg 13030



2706-90-3EP231X: Perfluoropentanoic acid (PFPeA) 95.90.00125 mg/kg 13050

307-24-4EP231X: Perfluorohexanoic acid (PFHxA) 74.60.00125 mg/kg 13050







72629-94-8EP231X: Perfluorotridecanoic acid (PFTrDA) 1160.00125 mg/kg 13030

376-06-7EP231X: Perfluorotetradecanoic acid (PFTeDA) 74.80.00312 mg/kg 13030


0315_BH009_0.0_170315 ES1706394-041 375-22-4EP231X: Perfluorobutanoic acid (PFBA) 86.60.00625 mg/kg 13030

2706-90-3EP231X: Perfluoropentanoic acid (PFPeA) 1200.00125 mg/kg 13050


375-85-9EP231X: Perfluoroheptanoic acid (PFHpA) 1030.00125 mg/kg 13050


375-95-1EP231X: Perfluorononanoic acid (PFNA) 1110.00125 mg/kg 13050





27 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project





0315_BH009_0.0_170315 ES1706394-041 376-06-7EP231X: Perfluorotetradecanoic acid (PFTeDA) 1190.00312 mg/kg 13030




307-24-4EP231X: Perfluorohexanoic acid (PFHxA) 1240.00125 mg/kg 13050






307-55-1EP231X: Perfluorododecanoic acid (PFDoDA) 83.20.00125 mg/kg 13050


376-06-7EP231X: Perfluorotetradecanoic acid (PFTeDA) 38.30.00312 mg/kg 13030


0315_SD006_170316 ES1706394-089 375-22-4EP231X: Perfluorobutanoic acid (PFBA) 80.20.00625 mg/kg 13030



375-85-9EP231X: Perfluoroheptanoic acid (PFHpA) 1170.00125 mg/kg 13050

335-67-1EP231X: Perfluorooctanoic acid (PFOA) 1140.00125 mg/kg 13050

375-95-1EP231X: Perfluorononanoic acid (PFNA) 1120.00125 mg/kg 13050

335-76-2EP231X: Perfluorodecanoic acid (PFDA) 1170.00125 mg/kg 13050


307-55-1EP231X: Perfluorododecanoic acid (PFDoDA) 88.00.00125 mg/kg 13050

72629-94-8EP231X: Perfluorotridecanoic acid (PFTrDA) 1040.00125 mg/kg 13030

376-06-7EP231X: Perfluorotetradecanoic acid (PFTeDA) 1030.00312 mg/kg 13030


0315_BH001_0.0_170315 ES1706394-001 754-91-6EP231X: Perfluorooctane sulfonamide (FOSA) # Not

Determined

0.00125 mg/kg 13050

31506-32-8EP231X: N-Methyl perfluorooctane sulfonamide

(MeFOSA)

1040.00312 mg/kg 13030

4151-50-2EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) # 22.00.00312 mg/kg 13030

2448-09-7EP231X: N-Methyl perfluorooctane sulfonamidoethanol

(MeFOSE)

1140.00312 mg/kg 13030

1691-99-2EP231X: N-Ethyl perfluorooctane sulfonamidoethanol

(EtFOSE)

# 15.30.00312 mg/kg 13030

2355-31-9EP231X: N-Methyl perfluorooctane sulfonamidoacetic

acid (MeFOSAA)

48.40.00125 mg/kg 13030

2991-50-6EP231X: N-Ethyl perfluorooctane sulfonamidoacetic

acid (EtFOSAA)

31.60.00125 mg/kg 13030

28 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project





0315_BH005_0.0_170314 ES1706394-021 754-91-6EP231X: Perfluorooctane sulfonamide (FOSA) 99.70.00125 mg/kg 13050


(MeFOSA)

75.00.00312 mg/kg 13030

4151-50-2EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 86.20.00312 mg/kg 13030


(MeFOSE)

72.00.00312 mg/kg 13030


(EtFOSE)

1230.00312 mg/kg 13030


acid (MeFOSAA)

68.00.00125 mg/kg 13030


acid (EtFOSAA)

63.00.00125 mg/kg 13030


0315_BH009_0.0_170315 ES1706394-041 754-91-6EP231X: Perfluorooctane sulfonamide (FOSA) 1300.00125 mg/kg 13050


(MeFOSA)

49.10.00312 mg/kg 13030

4151-50-2EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 1060.00312 mg/kg 13030


(MeFOSE)

51.10.00312 mg/kg 13030


(EtFOSE)

31.60.00312 mg/kg 13030


acid (MeFOSAA)

52.80.00125 mg/kg 13030


acid (EtFOSAA)

55.50.00125 mg/kg 13030


0315_BH013_0.0_170314 ES1706394-061 754-91-6EP231X: Perfluorooctane sulfonamide (FOSA) 82.00.00125 mg/kg 13050


(MeFOSA)

81.10.00312 mg/kg 13030

4151-50-2EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 67.50.00312 mg/kg 13030


(MeFOSE)

46.00.00312 mg/kg 13030


(EtFOSE)

63.00.00312 mg/kg 13030


acid (MeFOSAA)

60.00.00125 mg/kg 13030


acid (EtFOSAA)

86.80.00125 mg/kg 13030


29 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project





0315_SD006_170316 ES1706394-089 754-91-6EP231X: Perfluorooctane sulfonamide (FOSA) 93.60.00125 mg/kg 13050


(MeFOSA)

1120.00312 mg/kg 13030

4151-50-2EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 1070.00312 mg/kg 13030


(MeFOSE)

99.50.00312 mg/kg 13030


(EtFOSE)

78.00.00312 mg/kg 13030


acid (MeFOSAA)

94.40.00125 mg/kg 13030


acid (EtFOSAA)

95.60.00125 mg/kg 13030


0315_BH001_0.0_170315 ES1706394-001 757124-72-4EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 93.10.00125 mg/kg 13050

27619-97-2EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 82.40.00125 mg/kg 13050

39108-34-4EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) # Not

Determined

0.00125 mg/kg 13050

120226-60-0EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) # 9.360.00125 mg/kg 13050



27619-97-2EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 1030.00125 mg/kg 13050




0315_BH009_0.0_170315 ES1706394-041 757124-72-4EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 1180.00125 mg/kg 13050






27619-97-2EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) # Not

Determined

0.00125 mg/kg 13050




0315_SD006_170316 ES1706394-089 757124-72-4EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 1090.00125 mg/kg 13050



30 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project




EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 798138) - continued

0315_SD006_170316 ES1706394-089 120226-60-0EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 67.20.00125 mg/kg 13050

Sub-Matrix: WATER Matrix Spike (MS) Report




Anonymous EB1705137-001 375-73-5EP231X: Perfluorobutane sulfonic acid (PFBS) 1110.5 µg/L 13050

2706-91-4EP231X: Perfluoropentane sulfonic acid (PFPeS) 97.80.5 µg/L 13050

355-46-4EP231X: Perfluorohexane sulfonic acid (PFHxS) 1120.5 µg/L 13050

375-92-8EP231X: Perfluoroheptane sulfonic acid (PFHpS) 1070.5 µg/L 13050

1763-23-1EP231X: Perfluorooctane sulfonic acid (PFOS) 1120.5 µg/L 13050

335-77-3EP231X: Perfluorodecane sulfonic acid (PFDS) 1070.5 µg/L 13050


Anonymous EB1705137-001 375-22-4EP231X: Perfluorobutanoic acid (PFBA) 72.02.5 µg/L 13050

2706-90-3EP231X: Perfluoropentanoic acid (PFPeA) 1250.5 µg/L 13050

307-24-4EP231X: Perfluorohexanoic acid (PFHxA) 95.80.5 µg/L 13050

375-85-9EP231X: Perfluoroheptanoic acid (PFHpA) 1030.5 µg/L 13050

335-67-1EP231X: Perfluorooctanoic acid (PFOA) 85.60.5 µg/L 13050

375-95-1EP231X: Perfluorononanoic acid (PFNA) 84.20.5 µg/L 13050

335-76-2EP231X: Perfluorodecanoic acid (PFDA) 81.40.5 µg/L 13050

2058-94-8EP231X: Perfluoroundecanoic acid (PFUnDA) 95.80.5 µg/L 13050

307-55-1EP231X: Perfluorododecanoic acid (PFDoDA) 93.00.5 µg/L 13050

72629-94-8EP231X: Perfluorotridecanoic acid (PFTrDA) 88.00.5 µg/L 13050

376-06-7EP231X: Perfluorotetradecanoic acid (PFTeDA) 90.61.25 µg/L 13050


Anonymous EB1705137-001 754-91-6EP231X: Perfluorooctane sulfonamide (FOSA) 1010.5 µg/L 13050


(MeFOSA)

1191.25 µg/L 13050

4151-50-2EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 89.91.25 µg/L 13050


(MeFOSE)

1091.25 µg/L 13050


(EtFOSE)

91.41.25 µg/L 13050


acid (MeFOSAA)

83.60.5 µg/L 13050


acid (EtFOSAA)

99.60.5 µg/L 13050


Anonymous EB1705137-001 757124-72-4EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 93.40.5 µg/L 13050

31 of 31:Page

Work Order :

:Client


GOLDER ASSOCIATES

1652034:Project

Sub-Matrix: WATER Matrix Spike (MS) Report



EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 798141) - continued

Anonymous EB1705137-001 27619-97-2EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 95.80.5 µg/L 13050

39108-34-4EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 95.40.5 µg/L 13050

120226-60-0EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 84.00.5 µg/L 13050

0 0.00 True

Environmental

CERTIFICATE OF ANALYSISWork Order : Page : 1 of 49ES1706394

:Amendment 2:: LaboratoryClient GOLDER ASSOCIATES Environmental Division Sydney

: :ContactContact MS OLGA BUKHTEEVA Customer Services ES

:: AddressAddress LEVEL 1, 124 PACIFIC HIGHWAY

ST LEONARDS NSW, AUSTRALIA 2065

277-289 Woodpark Road Smithfield NSW Australia 2164

:Telephone +61 02 9478 3900 :Telephone +61-2-8784 8555

:Project 1652034 Date Samples Received : 17-Mar-2017 12:00

:Order number PO01472 Date Analysis Commenced : 20-Mar-2017

:C-O-C number ---- Issue Date : 10-Apr-2017 17:37


Site : Kapooka

Quote number : BN/404/16

110:No. of samples received

103:No. of samples analysed

This report supersedes any previous report(s) with this reference. Results apply to the sample(s) as submitted. This document shall not be reproduced, except in full.

This Certificate of Analysis contains the following information:

l General Comments

l Analytical Results

l Surrogate Control Limits

Additional information pertinent to this report will be found in the following separate attachments: Quality Control Report, QA/QC Compliance Assessment to assist with

Quality Review and Sample Receipt Notification.

SignatoriesThis document has been electronically signed by the authorized signatories below. Electronic signing is carried out in compliance with procedures specified in 21 CFR Part 11.

Signatories Accreditation CategoryPosition

Alex Rossi Organic Chemist Sydney Organics, Smithfield, NSW

Edwandy Fadjar Organic Coordinator Sydney Inorganics, Smithfield, NSW


2 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

General Comments

The analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the USEPA, APHA, AS and NEPM. In house

developed procedures are employed in the absence of documented standards or by client request.

Where moisture determination has been performed, results are reported on a dry weight basis.

Where a reported less than (<) result is higher than the LOR, this may be due to primary sample extract/digestate dilution and/or insufficient sample for analysis.

Where the LOR of a reported result differs from standard LOR, this may be due to high moisture content, insufficient sample (reduced weight employed) or matrix interference.

When no sampling time is provided, the sampling time will default 00:00 on the date of sampling. If no sampling date is provided, the sampling date will be assumed by the laboratory and displayed in brackets without a

time component.

Where a result is required to meet compliance limits the associated uncertainty must be considered. Refer to the ALS Contact for details.

CAS Number = CAS registry number from database maintained by Chemical Abstracts Services. The Chemical Abstracts Service is a division of the American Chemical Society.

LOR = Limit of reporting

^ = This result is computed from individual analyte detections at or above the level of reporting

ø = ALS is not NATA accredited for these tests.

~ = Indicates an estimated value.

Key :

EP231X: Poor Matrix Spike (MS) recoveries on various analytes is due to matrix interferences and effects. This was confirmed by re-extraction and re-analysis.l

Amendment (10/04/2017): This report has been amended with the removal of analysis for samples 105-110. All analysis results are as per the previous report.l

3 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH001_4.0_170

315

0315_BH001_3.0_170

315

0315_BH001_2.0_170

315

0315_BH001_1.0_170

315

0315_BH001_0.0_170

315

Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

[15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017]Client sampling date / time

ES1706394-005ES1706394-004ES1706394-003ES1706394-002ES1706394-001UnitLORCAS NumberCompound

Result Result Result Result Result


10.2 16.2 11.4 4.9 4.6%1----Moisture Content (dried @ 103°C)


0.0009Perfluorobutane sulfonic acid

(PFBS)

0.0448 0.0342 0.0029 0.0009mg/kg0.0002375-73-5

0.0015Perfluoropentane sulfonic acid

(PFPeS)

0.0665 0.0582 0.0020 0.0005mg/kg0.00022706-91-4

0.0518Perfluorohexane sulfonic acid

(PFHxS)

0.741 0.342 0.0134 0.0068mg/kg0.0002355-46-4

0.0013Perfluoroheptane sulfonic acid

(PFHpS)

0.0577 0.0317 0.0009 0.0004mg/kg0.0002375-92-8

1.15Perfluorooctane sulfonic acid

(PFOS)

2.60 0.0859 0.0378 0.0128mg/kg0.00021763-23-1

0.0172Perfluorodecane sulfonic acid

(PFDS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3


0.014Perfluorobutanoic acid (PFBA) 0.027 0.007 <0.001 <0.001mg/kg0.001375-22-4

<0.0002Perfluoropentanoic acid (PFPeA) 0.0281 0.0206 <0.0002 <0.0002mg/kg0.00022706-90-3

0.0085Perfluorohexanoic acid (PFHxA) 0.143 0.0713 0.0035 0.0008mg/kg0.0002307-24-4

0.0013Perfluoroheptanoic acid (PFHpA) 0.0329 0.0093 0.0005 <0.0002mg/kg0.0002375-85-9

0.0050Perfluorooctanoic acid (PFOA) 0.0560 0.0129 0.0014 0.0004mg/kg0.0002335-67-1

0.0004Perfluorononanoic acid (PFNA) 0.0019 <0.0002 <0.0002 <0.0002mg/kg0.0002375-95-1

0.0009Perfluorodecanoic acid (PFDA) 0.0003 <0.0002 <0.0002 <0.0002mg/kg0.0002335-76-2

<0.0002Perfluoroundecanoic acid

(PFUnDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8

<0.0002Perfluorododecanoic acid

(PFDoDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1

<0.0002Perfluorotridecanoic acid

(PFTrDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8

<0.0005Perfluorotetradecanoic acid

(PFTeDA)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7


0.0112Perfluorooctane sulfonamide

(FOSA)

0.0018 0.0005 0.0004 0.0002mg/kg0.0002754-91-6

<0.0005N-Methyl perfluorooctane


<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8

4 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH001_4.0_170

315

0315_BH001_3.0_170

315

0315_BH001_2.0_170

315

0315_BH001_1.0_170

315

0315_BH001_0.0_170

315


(Matrix: SOIL)





<0.0005N-Ethyl perfluorooctane

sulfonamide (EtFOSA)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2


sulfonamidoacetic acid

(MeFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9



(EtFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6


<0.00054:2 Fluorotelomer sulfonic acid

(4:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4

0.00326:2 Fluorotelomer sulfonic acid

(6:2 FTS)

0.0364 0.0038 <0.0005 <0.0005mg/kg0.000527619-97-2


(8:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4


(10:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0

EP231P: PFAS Sums

1.27 3.84 0.677 0.0628 0.0228mg/kg0.0002----Sum of PFAS

1.20Sum of PFHxS and PFOS 3.34 0.428 0.0512 0.0196mg/kg0.0002355-46-4/1763-23-

1

1.24 3.71 0.587 0.0595 0.0217mg/kg0.0002----Sum of PFAS (WA DER List)

EP231S: PFAS Surrogate

99.7 99.4 93.4 103 102%0.0002----13C4-PFOS

5 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH002_4.0_170

315

0315_BH002_3.0_170

315

0315_BH002_2.0_170

315

0315_BH002_1.0_170

315

0315_BH002_0.0_170

315


(Matrix: SOIL)








(PFBS)

<0.0002 0.0002 <0.0002 0.0018mg/kg0.0002375-73-5


(PFPeS)

<0.0002 0.0003 <0.0002 0.0016mg/kg0.00022706-91-4


(PFHxS)

0.0066 0.0089 0.0039 0.0241mg/kg0.0002355-46-4


(PFHpS)

<0.0002 0.0014 0.0004 0.0014mg/kg0.0002375-92-8


(PFOS)

0.222 0.119 0.0303 0.0458mg/kg0.00021763-23-1


(PFDS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3


<0.001Perfluorobutanoic acid (PFBA) 0.001 <0.001 <0.001 <0.001mg/kg0.001375-22-4

<0.0002Perfluoropentanoic acid (PFPeA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-90-3


0.0008Perfluoroheptanoic acid (PFHpA) <0.0002 <0.0002 <0.0002 0.0003mg/kg0.0002375-85-9


0.0011Perfluorononanoic acid (PFNA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-95-1

0.0008Perfluorodecanoic acid (PFDA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-76-2

0.0002Perfluoroundecanoic acid

(PFUnDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8


(PFDoDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1


(PFTrDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8


(PFTeDA)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7



(FOSA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8

6 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH002_4.0_170

315

0315_BH002_3.0_170

315

0315_BH002_2.0_170

315

0315_BH002_1.0_170

315

0315_BH002_0.0_170

315


(Matrix: SOIL)







<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2



(MeFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9



(EtFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6



(4:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4


(6:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2


(8:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4


(10:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0

EP231P: PFAS Sums

0.204 0.232 0.131 0.0351 0.0785mg/kg0.0002----Sum of PFAS


1



98.3 99.4 101 101 100%0.0002----13C4-PFOS

7 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH003_4.0_170

314

0315_BH003_3.0_170

314

0315_BH003_2.0_170

314

0315_BH003_1.0_170

314

0315_BH003_0.0_170

314


(Matrix: SOIL)








(PFBS)

0.0411 0.0245 0.0022 0.0011mg/kg0.0002375-73-5


(PFPeS)

0.0516 0.0403 0.0022 0.0016mg/kg0.00022706-91-4


(PFHxS)

0.0484 0.456 0.0243 0.0181mg/kg0.0002355-46-4


(PFHpS)

0.0686 0.0320 0.0015 0.0010mg/kg0.0002375-92-8


(PFOS)

3.70 0.404 0.0386 0.0239mg/kg0.00021763-23-1


(PFDS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3


<0.001Perfluorobutanoic acid (PFBA) 0.008 0.003 <0.001 <0.001mg/kg0.001375-22-4

0.0049Perfluoropentanoic acid (PFPeA) 0.0261 0.0075 <0.0002 <0.0002mg/kg0.00022706-90-3


0.0024Perfluoroheptanoic acid (PFHpA) 0.0116 0.0090 0.0004 0.0004mg/kg0.0002375-85-9


0.0034Perfluorononanoic acid (PFNA) 0.0010 0.0002 <0.0002 <0.0002mg/kg0.0002375-95-1



(PFUnDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8

0.0043Perfluorododecanoic acid

(PFDoDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1

0.0016Perfluorotridecanoic acid

(PFTrDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8


(PFTeDA)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7



(FOSA)

0.0002 0.0010 <0.0002 <0.0002mg/kg0.0002754-91-6



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8

8 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH003_4.0_170

314

0315_BH003_3.0_170

314

0315_BH003_2.0_170

314

0315_BH003_1.0_170

314

0315_BH003_0.0_170

314


(Matrix: SOIL)





0.0007N-Ethyl perfluorooctane


<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2



(MeFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9



(EtFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6



(4:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4


(6:2 FTS)

0.0138 0.0010 <0.0005 <0.0005mg/kg0.000527619-97-2


(8:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4


(10:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0

EP231P: PFAS Sums

0.648 4.08 1.05 0.0745 0.0496mg/kg0.0002----Sum of PFAS


1



99.9 101 99.0 103 99.3%0.0002----13C4-PFOS

9 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH004_4.0_170

314

0315_BH004_3.0_170

314

0315_BH004_2.0_170

314

0315_BH004_1.0_170

314

0315_BH004_0.0_170

314


(Matrix: SOIL)








(PFBS)

0.0006 0.0152 0.0048 0.0007mg/kg0.0002375-73-5


(PFPeS)

0.0006 0.0181 0.0039 0.0007mg/kg0.00022706-91-4


(PFHxS)

0.0130 0.209 0.0356 0.0081mg/kg0.0002355-46-4


(PFHpS)

0.0016 0.231 0.0019 0.0005mg/kg0.0002375-92-8


(PFOS)

0.394 0.789 0.0374 0.0129mg/kg0.00021763-23-1


(PFDS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3


<0.001Perfluorobutanoic acid (PFBA) <0.001 0.004 <0.001 <0.001mg/kg0.001375-22-4

0.0025Perfluoropentanoic acid (PFPeA) 0.0023 0.0148 0.0019 <0.0002mg/kg0.00022706-90-3


0.0016Perfluoroheptanoic acid (PFHpA) 0.0013 0.0099 0.0010 <0.0002mg/kg0.0002375-85-9


0.0035Perfluorononanoic acid (PFNA) 0.0009 0.0013 <0.0002 <0.0002mg/kg0.0002375-95-1



(PFUnDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8

0.0010Perfluorododecanoic acid

(PFDoDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1


(PFTrDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8


(PFTeDA)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7



(FOSA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8

10 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH004_4.0_170

314

0315_BH004_3.0_170

314

0315_BH004_2.0_170

314

0315_BH004_1.0_170

314

0315_BH004_0.0_170

314


(Matrix: SOIL)







<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2



(MeFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9



(EtFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6



(4:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4


(6:2 FTS)

0.0083 0.0399 0.0016 <0.0005mg/kg0.000527619-97-2


(8:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4


(10:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0

EP231P: PFAS Sums

0.176 0.428 1.39 0.0965 0.0245mg/kg0.0002----Sum of PFAS


1



85.6 85.7 99.4 91.3 116%0.0002----13C4-PFOS

11 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH005_4.0_170

314

0315_BH005_3.0_170

314

0315_BH005_2.0_170

314

0315_BH005_1.0_170

314

0315_BH005_0.0_170

314


(Matrix: SOIL)







<0.0002Perfluorobutane sulfonic acid

(PFBS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-73-5

<0.0002Perfluoropentane sulfonic acid

(PFPeS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-91-4


(PFHxS)

0.0005 0.0004 <0.0002 0.0002mg/kg0.0002355-46-4

<0.0002Perfluoroheptane sulfonic acid

(PFHpS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-92-8


(PFOS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00021763-23-1

<0.0002Perfluorodecane sulfonic acid

(PFDS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3


<0.001Perfluorobutanoic acid (PFBA) <0.001 <0.001 <0.001 <0.001mg/kg0.001375-22-4

<0.0002Perfluoropentanoic acid (PFPeA) 0.0011 0.0003 0.0007 <0.0002mg/kg0.00022706-90-3

<0.0002Perfluorohexanoic acid (PFHxA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-24-4

<0.0002Perfluoroheptanoic acid (PFHpA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-85-9

<0.0002Perfluorooctanoic acid (PFOA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-67-1

<0.0002Perfluorononanoic acid (PFNA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-95-1

<0.0002Perfluorodecanoic acid (PFDA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-76-2


(PFUnDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8


(PFDoDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1


(PFTrDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8


(PFTeDA)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7


<0.0002Perfluorooctane sulfonamide

(FOSA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8

12 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH005_4.0_170

314

0315_BH005_3.0_170

314

0315_BH005_2.0_170

314

0315_BH005_1.0_170

314

0315_BH005_0.0_170

314


(Matrix: SOIL)







<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2



(MeFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9



(EtFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6



(4:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4


(6:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2


(8:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4


(10:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0

EP231P: PFAS Sums

0.0127 0.0016 0.0007 0.0007 0.0002mg/kg0.0002----Sum of PFAS

0.0127Sum of PFHxS and PFOS 0.0005 0.0004 <0.0002 0.0002mg/kg0.0002355-46-4/1763-23-

1



82.9 128 108 94.1 100%0.0002----13C4-PFOS

13 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH006_4.0_170

314

0315_BH006_3.0_170

314

0315_BH006_2.0_170

314

0315_BH006_1.0_170

314

0315_BH006_0.0_170

314


(Matrix: SOIL)








(PFBS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-73-5


(PFPeS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-91-4


(PFHxS)

0.0002 0.0008 <0.0002 0.0005mg/kg0.0002355-46-4


(PFHpS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-92-8


(PFOS)

0.0102 <0.0002 <0.0002 <0.0002mg/kg0.00021763-23-1


(PFDS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3



0.0002Perfluoropentanoic acid (PFPeA) <0.0002 0.0002 0.0004 0.0002mg/kg0.00022706-90-3



0.0002Perfluorooctanoic acid (PFOA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-67-1




(PFUnDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8


(PFDoDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1


(PFTrDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8


(PFTeDA)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7



(FOSA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8

14 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH006_4.0_170

314

0315_BH006_3.0_170

314

0315_BH006_2.0_170

314

0315_BH006_1.0_170

314

0315_BH006_0.0_170

314


(Matrix: SOIL)







<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2



(MeFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9



(EtFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6



(4:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4


(6:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2


(8:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4


(10:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0

EP231P: PFAS Sums

0.0163 0.0104 0.0010 0.0004 0.0007mg/kg0.0002----Sum of PFAS


1



95.8 84.8 87.1 88.8 111%0.0002----13C4-PFOS

15 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH007_4.0_170

315

0315_BH007_3.0_170

315

0315_BH007_2.0_170

315

0315_BH007_1.0_170

315

0315_BH007_0.0_170

315


(Matrix: SOIL)








(PFBS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-73-5


(PFPeS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-91-4


(PFHxS)

0.0028 0.0007 <0.0002 0.0003mg/kg0.0002355-46-4


(PFHpS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-92-8


(PFOS)

0.0062 0.0054 <0.0002 <0.0002mg/kg0.00021763-23-1


(PFDS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3



0.0006Perfluoropentanoic acid (PFPeA) <0.0002 0.0003 <0.0002 0.0006mg/kg0.00022706-90-3

0.0002Perfluorohexanoic acid (PFHxA) 0.0006 <0.0002 <0.0002 <0.0002mg/kg0.0002307-24-4


0.0002Perfluorooctanoic acid (PFOA) 0.0005 0.0015 <0.0002 <0.0002mg/kg0.0002335-67-1




(PFUnDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8


(PFDoDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1


(PFTrDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8


(PFTeDA)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7



(FOSA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8

16 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH007_4.0_170

315

0315_BH007_3.0_170

315

0315_BH007_2.0_170

315

0315_BH007_1.0_170

315

0315_BH007_0.0_170

315


(Matrix: SOIL)







<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2



(MeFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9



(EtFOSAA)

<0.0002 0.0011 <0.0002 <0.0002mg/kg0.00022991-50-6



(4:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4


(6:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2


(8:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4


(10:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0

EP231P: PFAS Sums

0.0179 0.0101 0.0090 <0.0002 0.0009mg/kg0.0002----Sum of PFAS


1

0.0179 0.0101 0.0079 <0.0002 0.0009mg/kg0.0002----Sum of PFAS (WA DER List)


88.4 128 96.4 80.7 76.4%0.0002----13C4-PFOS

17 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH008_4.0_170

315

0315_BH008_3.0_170

315

0315_BH008_2.0_170

315

0315_BH008_1.0_170

315

0315_BH008_0.0_170

315


(Matrix: SOIL)








(PFBS)

0.0008 0.0012 0.0110 0.0028mg/kg0.0002375-73-5


(PFPeS)

0.0014 0.0023 0.0095 0.0038mg/kg0.00022706-91-4


(PFHxS)

0.0330 0.0768 0.0074 0.0266mg/kg0.0002355-46-4


(PFHpS)

0.0055 0.0026 <0.0002 0.0019mg/kg0.0002375-92-8


(PFOS)

0.782 1.33 0.0003 0.0023mg/kg0.00021763-23-1


(PFDS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3



0.0011Perfluoropentanoic acid (PFPeA) 0.0006 0.0009 0.0028 0.0012mg/kg0.00022706-90-3


<0.0002Perfluoroheptanoic acid (PFHpA) 0.0005 0.0013 0.0011 0.0011mg/kg0.0002375-85-9

<0.0002Perfluorooctanoic acid (PFOA) 0.0038 0.0025 <0.0002 0.0016mg/kg0.0002335-67-1




(PFUnDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8


(PFDoDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1


(PFTrDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8


(PFTeDA)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7



(FOSA)

0.0010 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8

18 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH008_4.0_170

315

0315_BH008_3.0_170

315

0315_BH008_2.0_170

315

0315_BH008_1.0_170

315

0315_BH008_0.0_170

315


(Matrix: SOIL)







<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2



(MeFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9



(EtFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6



(4:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4


(6:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2


(8:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4


(10:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0

EP231P: PFAS Sums

0.0261 0.833 1.42 0.0513 0.0507mg/kg0.0002----Sum of PFAS


1



102 88.9 79.3 95.1 77.3%0.0002----13C4-PFOS

19 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH009_4.0_170

315

0315_BH009_3.0_170

315

0315_BH009_2.0_170

315

0315_BH009_1.0_170

315

0315_BH009_0.0_170

315


(Matrix: SOIL)








(PFBS)

0.0006 0.0284 0.0024 <0.0002mg/kg0.0002375-73-5


(PFPeS)

0.0007 0.0210 0.0016 <0.0002mg/kg0.00022706-91-4


(PFHxS)

0.0138 0.109 0.0142 0.0007mg/kg0.0002355-46-4


(PFHpS)

0.0157 0.0025 0.0002 <0.0002mg/kg0.0002375-92-8


(PFOS)

0.556 0.0148 <0.0002 <0.0002mg/kg0.00021763-23-1


(PFDS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3



<0.0002Perfluoropentanoic acid (PFPeA) <0.0002 0.0063 <0.0002 <0.0002mg/kg0.00022706-90-3


<0.0002Perfluoroheptanoic acid (PFHpA) <0.0002 0.0051 0.0004 <0.0002mg/kg0.0002375-85-9

0.0006Perfluorooctanoic acid (PFOA) 0.0014 0.0019 0.0002 <0.0002mg/kg0.0002335-67-1




(PFUnDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8


(PFDoDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1


(PFTrDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8


(PFTeDA)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7



(FOSA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8

20 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH009_4.0_170

315

0315_BH009_3.0_170

315

0315_BH009_2.0_170

315

0315_BH009_1.0_170

315

0315_BH009_0.0_170

315


(Matrix: SOIL)







<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7



0.0016 <0.0005 <0.0005 0.0010mg/kg0.00051691-99-2



(MeFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9



(EtFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6



(4:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4


(6:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2


(8:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4


(10:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0

EP231P: PFAS Sums

0.332 0.593 0.237 0.0230 0.0019mg/kg0.0002----Sum of PFAS


1



76.9 93.3 108 98.3 93.9%0.0002----13C4-PFOS

21 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH010_4.0_170

315

0315_BH010_3.0_170

315

0315_BH010_2.0_170

315

0315_BH010_1.0_170

315

0315_BH010_0.0_170

315


(Matrix: SOIL)








(PFBS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-73-5


(PFPeS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-91-4


(PFHxS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002355-46-4


(PFHpS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-92-8


(PFOS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00021763-23-1


(PFDS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3




<0.0002Perfluorohexanoic acid (PFHxA) <0.0002 0.0003 <0.0002 <0.0002mg/kg0.0002307-24-4






(PFUnDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8


(PFDoDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1


(PFTrDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8


(PFTeDA)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7



(FOSA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8

22 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH010_4.0_170

315

0315_BH010_3.0_170

315

0315_BH010_2.0_170

315

0315_BH010_1.0_170

315

0315_BH010_0.0_170

315


(Matrix: SOIL)







<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7



0.0008 0.0005 0.0005 0.0006mg/kg0.00051691-99-2



(MeFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9



(EtFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6



(4:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4


(6:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2


(8:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4


(10:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0

EP231P: PFAS Sums

0.0145 0.0008 0.0008 0.0005 0.0006mg/kg0.0002----Sum of PFAS

0.0109Sum of PFHxS and PFOS <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002355-46-4/1763-23-

1

0.0109 <0.0002 0.0003 <0.0002 <0.0002mg/kg0.0002----Sum of PFAS (WA DER List)


99.4 114 89.4 102 92.4%0.0002----13C4-PFOS

23 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH011_4.0_170

314

0315_BH011_3.0_170

314

0315_BH011_2.0_170

314

0315_BH011_1.0_170

314

0315_BH011_0.0_170

314


(Matrix: SOIL)








(PFBS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-73-5


(PFPeS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-91-4

<0.0002Perfluorohexane sulfonic acid

(PFHxS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002355-46-4


(PFHpS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-92-8


(PFOS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00021763-23-1


(PFDS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3










(PFUnDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8


(PFDoDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1


(PFTrDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8


(PFTeDA)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7



(FOSA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8

24 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH011_4.0_170

314

0315_BH011_3.0_170

314

0315_BH011_2.0_170

314

0315_BH011_1.0_170

314

0315_BH011_0.0_170

314


(Matrix: SOIL)







<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7



0.0007 0.0007 0.0012 0.0008mg/kg0.00051691-99-2



(MeFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9



(EtFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6



(4:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4


(6:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2


(8:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4


(10:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0

EP231P: PFAS Sums

0.0020 0.0007 0.0007 0.0012 0.0008mg/kg0.0002----Sum of PFAS


1

0.0011 <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002----Sum of PFAS (WA DER List)


112 108 125 105 116%0.0002----13C4-PFOS

25 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH012_4.0_170

314

0315_BH012_3.0_170

314

0315_BH012_2.0_170

314

0315_BH012_1.0_170

314

0315_BH012_0.0_170

314


(Matrix: SOIL)








(PFBS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-73-5


(PFPeS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-91-4


(PFHxS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002355-46-4


(PFHpS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-92-8


(PFOS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00021763-23-1


(PFDS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3




0.0006Perfluorohexanoic acid (PFHxA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-24-4






(PFUnDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8


(PFDoDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1


(PFTrDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8


(PFTeDA)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7



(FOSA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8

26 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH012_4.0_170

314

0315_BH012_3.0_170

314

0315_BH012_2.0_170

314

0315_BH012_1.0_170

314

0315_BH012_0.0_170

314


(Matrix: SOIL)







<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7



0.0006 0.0007 0.0008 0.0008mg/kg0.00051691-99-2



(MeFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9



(EtFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6



(4:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4


(6:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2


(8:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4


(10:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0

EP231P: PFAS Sums

0.0031 0.0006 0.0007 0.0008 0.0008mg/kg0.0002----Sum of PFAS


1



102 95.6 106 104 82.8%0.0002----13C4-PFOS

27 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH013_4.0_170

314

0315_BH013_3.0_170

314

0315_BH013_2.0_170

314

0315_BH013_1.0_170

314

0315_BH013_0.0_170

314


(Matrix: SOIL)








(PFBS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-73-5


(PFPeS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-91-4


(PFHxS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002355-46-4


(PFHpS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-92-8


(PFOS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00021763-23-1


(PFDS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3



0.0030Perfluoropentanoic acid (PFPeA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-90-3

0.0018Perfluorohexanoic acid (PFHxA) 0.0008 <0.0002 <0.0002 <0.0002mg/kg0.0002307-24-4

0.0020Perfluoroheptanoic acid (PFHpA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-85-9


0.0009Perfluorononanoic acid (PFNA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-95-1



(PFUnDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8


(PFDoDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1


(PFTrDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8


(PFTeDA)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7



(FOSA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8

28 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH013_4.0_170

314

0315_BH013_3.0_170

314

0315_BH013_2.0_170

314

0315_BH013_1.0_170

314

0315_BH013_0.0_170

314


(Matrix: SOIL)







<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2



(MeFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9



(EtFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6



(4:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4


(6:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2


(8:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4


(10:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0

EP231P: PFAS Sums

0.0246 0.0008 <0.0002 <0.0002 <0.0002mg/kg0.0002----Sum of PFAS


1

0.0237 0.0008 <0.0002 <0.0002 <0.0002mg/kg0.0002----Sum of PFAS (WA DER List)


95.6 119 114 118 116%0.0002----13C4-PFOS

29 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH014_4.0_170

315

0315_BH014_3.0_170

315

0315_BH014_2.0_170

315

0315_BH014_1.0_170

315

0315_BH014_0.0_170

315


(Matrix: SOIL)








(PFBS)

0.0147 0.0012 <0.0002 <0.0002mg/kg0.0002375-73-5


(PFPeS)

0.0066 0.0007 0.0002 <0.0002mg/kg0.00022706-91-4


(PFHxS)

0.0085 0.0010 0.0002 <0.0002mg/kg0.0002355-46-4


(PFHpS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-92-8


(PFOS)

0.0017 0.0006 <0.0002 <0.0002mg/kg0.00021763-23-1


(PFDS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3




0.0029Perfluorohexanoic acid (PFHxA) 0.0083 0.0012 0.0004 <0.0002mg/kg0.0002307-24-4

0.0006Perfluoroheptanoic acid (PFHpA) 0.0005 <0.0002 <0.0002 <0.0002mg/kg0.0002375-85-9





(PFUnDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8


(PFDoDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1


(PFTrDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8


(PFTeDA)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7



(FOSA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8

30 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH014_4.0_170

315

0315_BH014_3.0_170

315

0315_BH014_2.0_170

315

0315_BH014_1.0_170

315

0315_BH014_0.0_170

315


(Matrix: SOIL)







<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2



(MeFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9



(EtFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6



(4:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4


(6:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2


(8:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4


(10:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0

EP231P: PFAS Sums

0.185 0.0403 0.0047 0.0008 <0.0002mg/kg0.0002----Sum of PFAS

0.164Sum of PFHxS and PFOS 0.0102 0.0016 0.0002 <0.0002mg/kg0.0002355-46-4/1763-23-

1

0.174 0.0337 0.0040 0.0006 <0.0002mg/kg0.0002----Sum of PFAS (WA DER List)


115 115 117 104 121%0.0002----13C4-PFOS

31 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH015_4.0_170

315

0315_BH015_3.0_170

315

0315_BH015_2.0_170

315

0315_BH015_1.0_170

315

0315_BH015_0.0_170

315


(Matrix: SOIL)








(PFBS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-73-5


(PFPeS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-91-4


(PFHxS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002355-46-4


(PFHpS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-92-8


(PFOS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00021763-23-1


(PFDS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3










(PFUnDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8


(PFDoDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1


(PFTrDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8


(PFTeDA)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7



(FOSA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8

32 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_BH015_4.0_170

315

0315_BH015_3.0_170

315

0315_BH015_2.0_170

315

0315_BH015_1.0_170

315

0315_BH015_0.0_170

315


(Matrix: SOIL)







<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2



(MeFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9



(EtFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6



(4:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4


(6:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2


(8:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4


(10:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0

EP231P: PFAS Sums

0.0012 <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002----Sum of PFAS


1



106 104 79.7 105 100%0.0002----13C4-PFOS

33 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_SD005_1703150315_SD004_1703160315_SD003_1703160315_SD002_1703140315_SD001_170314Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)








(PFBS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-73-5


(PFPeS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-91-4


(PFHxS)

0.0041 0.0007 0.0018 0.0005mg/kg0.0002355-46-4


(PFHpS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-92-8


(PFOS)

0.0539 0.0040 0.0126 0.0053mg/kg0.00021763-23-1


(PFDS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3




<0.0002Perfluorohexanoic acid (PFHxA) 0.0010 <0.0002 <0.0002 <0.0002mg/kg0.0002307-24-4

<0.0002Perfluoroheptanoic acid (PFHpA) 0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-85-9

<0.0002Perfluorooctanoic acid (PFOA) 0.0005 <0.0002 <0.0002 <0.0002mg/kg0.0002335-67-1




(PFUnDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8


(PFDoDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1


(PFTrDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8


(PFTeDA)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7



(FOSA)

0.0010 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8

34 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_SD005_1703150315_SD004_1703160315_SD003_1703160315_SD002_1703140315_SD001_170314Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)







<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2



(MeFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9



(EtFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6



(4:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4


(6:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2


(8:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4


(10:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0

EP231P: PFAS Sums

0.0108 0.0607 0.0047 0.0144 0.0058mg/kg0.0002----Sum of PFAS


1



99.3 91.2 85.6 123 109%0.0002----13C4-PFOS

35 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_QC102_1703150315_QC101_1703140315_QC100_1703140315_SD007_1703150315_SD006_170316Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)








(PFBS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-73-5


(PFPeS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-91-4


(PFHxS)

<0.0002 0.0014 0.0004 0.0034mg/kg0.0002355-46-4


(PFHpS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-92-8


(PFOS)

0.0009 0.0062 <0.0002 0.178mg/kg0.00021763-23-1


(PFDS)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3



<0.0002Perfluoropentanoic acid (PFPeA) <0.0002 0.0026 <0.0002 <0.0002mg/kg0.00022706-90-3

<0.0002Perfluorohexanoic acid (PFHxA) <0.0002 0.0017 <0.0002 0.0009mg/kg0.0002307-24-4

<0.0002Perfluoroheptanoic acid (PFHpA) <0.0002 0.0019 <0.0002 <0.0002mg/kg0.0002375-85-9

<0.0002Perfluorooctanoic acid (PFOA) <0.0002 0.0013 <0.0002 0.0003mg/kg0.0002335-67-1

<0.0002Perfluorononanoic acid (PFNA) <0.0002 0.0009 <0.0002 <0.0002mg/kg0.0002375-95-1



(PFUnDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8


(PFDoDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1


(PFTrDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8


(PFTeDA)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7



(FOSA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8

36 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_QC102_1703150315_QC101_1703140315_QC100_1703140315_SD007_1703150315_SD006_170316Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)







<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2



(MeFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9



(EtFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6



(4:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4


(6:2 FTS)

<0.0005 0.0098 <0.0005 <0.0005mg/kg0.000527619-97-2


(8:2 FTS)

<0.0005 0.0036 <0.0005 <0.0005mg/kg0.000539108-34-4


(10:2 FTS)

<0.0005 0.0009 <0.0005 <0.0005mg/kg0.0005120226-60-0

EP231P: PFAS Sums

0.0015 0.0009 0.0303 0.0004 0.183mg/kg0.0002----Sum of PFAS


1



96.3 97.5 96.7 100 98.0%0.0002----13C4-PFOS

37 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_QC107_1703150315_QC106_1703150315_QC105_1703150315_QC104_1703150315_QC103_170315Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)








(PFBS)

<0.0002 0.0002 0.0007 <0.0002mg/kg0.0002375-73-5


(PFPeS)

<0.0002 0.0003 0.0008 <0.0002mg/kg0.00022706-91-4


(PFHxS)

<0.0002 0.0047 0.0414 0.0002mg/kg0.0002355-46-4


(PFHpS)

<0.0002 0.0008 0.0067 <0.0002mg/kg0.0002375-92-8


(PFOS)

<0.0002 0.467 0.0695 0.0006mg/kg0.00021763-23-1


(PFDS)

<0.0002 0.0014 <0.0002 <0.0002mg/kg0.0002335-77-3



<0.0002Perfluoropentanoic acid (PFPeA) <0.0002 0.0008 0.0012 <0.0002mg/kg0.00022706-90-3

<0.0002Perfluorohexanoic acid (PFHxA) <0.0002 0.0012 0.0019 <0.0002mg/kg0.0002307-24-4

<0.0002Perfluoroheptanoic acid (PFHpA) <0.0002 <0.0002 0.0004 <0.0002mg/kg0.0002375-85-9

0.0005Perfluorooctanoic acid (PFOA) <0.0002 0.0007 0.0037 <0.0002mg/kg0.0002335-67-1


<0.0002Perfluorodecanoic acid (PFDA) <0.0002 0.0002 <0.0002 <0.0002mg/kg0.0002335-76-2


(PFUnDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8


(PFDoDA)

<0.0002 0.0003 <0.0002 <0.0002mg/kg0.0002307-55-1


(PFTrDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8


(PFTeDA)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7



(FOSA)

<0.0002 0.0014 <0.0002 <0.0002mg/kg0.0002754-91-6



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8

38 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_QC107_1703150315_QC106_1703150315_QC105_1703150315_QC104_1703150315_QC103_170315Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)







<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7



<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2



(MeFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9



(EtFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6



(4:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4


(6:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2


(8:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4


(10:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0

EP231P: PFAS Sums

0.0028 <0.0002 0.479 0.126 0.0008mg/kg0.0002----Sum of PFAS

0.0017Sum of PFHxS and PFOS <0.0002 0.472 0.111 0.0008mg/kg0.0002355-46-4/1763-23-

1

0.0022 <0.0002 0.475 0.119 0.0008mg/kg0.0002----Sum of PFAS (WA DER List)


99.5 93.5 95.7 96.9 95.5%0.0002----13C4-PFOS

39 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

----------------0315_QC108_170315Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

----------------[15-Mar-2017]Client sampling date / time

--------------------------------ES1706394-099UnitLORCAS NumberCompound

Result ---- ---- ---- ----


78.0 ---- ---- ---- ----%1----Moisture Content (dried @ 103°C)



(PFBS)

---- ---- ---- ----mg/kg0.0002375-73-5


(PFPeS)

---- ---- ---- ----mg/kg0.00022706-91-4


(PFHxS)

---- ---- ---- ----mg/kg0.0002355-46-4


(PFHpS)

---- ---- ---- ----mg/kg0.0002375-92-8


(PFOS)

---- ---- ---- ----mg/kg0.00021763-23-1


(PFDS)

---- ---- ---- ----mg/kg0.0002335-77-3


<0.001Perfluorobutanoic acid (PFBA) ---- ---- ---- ----mg/kg0.001375-22-4

0.0072Perfluoropentanoic acid (PFPeA) ---- ---- ---- ----mg/kg0.00022706-90-3

<0.0002Perfluorohexanoic acid (PFHxA) ---- ---- ---- ----mg/kg0.0002307-24-4

<0.0002Perfluoroheptanoic acid (PFHpA) ---- ---- ---- ----mg/kg0.0002375-85-9

<0.0002Perfluorooctanoic acid (PFOA) ---- ---- ---- ----mg/kg0.0002335-67-1

<0.0002Perfluorononanoic acid (PFNA) ---- ---- ---- ----mg/kg0.0002375-95-1

0.0002Perfluorodecanoic acid (PFDA) ---- ---- ---- ----mg/kg0.0002335-76-2


(PFUnDA)

---- ---- ---- ----mg/kg0.00022058-94-8


(PFDoDA)

---- ---- ---- ----mg/kg0.0002307-55-1


(PFTrDA)

---- ---- ---- ----mg/kg0.000272629-94-8


(PFTeDA)

---- ---- ---- ----mg/kg0.0005376-06-7



(FOSA)

---- ---- ---- ----mg/kg0.0002754-91-6



---- ---- ---- ----mg/kg0.000531506-32-8

40 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

----------------0315_QC108_170315Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

----------------[15-Mar-2017]Client sampling date / time

--------------------------------ES1706394-099UnitLORCAS NumberCompound

Result ---- ---- ---- ----




---- ---- ---- ----mg/kg0.00054151-50-2



---- ---- ---- ----mg/kg0.00052448-09-7



---- ---- ---- ----mg/kg0.00051691-99-2



(MeFOSAA)

---- ---- ---- ----mg/kg0.00022355-31-9



(EtFOSAA)

---- ---- ---- ----mg/kg0.00022991-50-6



(4:2 FTS)

---- ---- ---- ----mg/kg0.0005757124-72-4


(6:2 FTS)

---- ---- ---- ----mg/kg0.000527619-97-2


(8:2 FTS)

---- ---- ---- ----mg/kg0.000539108-34-4


(10:2 FTS)

---- ---- ---- ----mg/kg0.0005120226-60-0

EP231P: PFAS Sums

0.0105 ---- ---- ---- ----mg/kg0.0002----Sum of PFAS

0.0031Sum of PFHxS and PFOS ---- ---- ---- ----mg/kg0.0002355-46-4/1763-23-

1

0.0103 ---- ---- ---- ----mg/kg0.0002----Sum of PFAS (WA DER List)


96.8 ---- ---- ---- ----%0.0002----13C4-PFOS

41 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_MW008_1703160315_MW007_1703160315_MW006_1703160315_MW005_1703160315_MW004_170316Client sample IDSub-Matrix: WATER

(Matrix: WATER)

16-Mar-2017 00:0016-Mar-2017 00:0016-Mar-2017 00:0016-Mar-2017 00:0016-Mar-2017 00:00Client sampling date / time





(PFBS)

0.0072 0.0122 <0.0005 0.0145µg/L0.0005375-73-5


(PFPeS)

0.0058 0.0057 <0.0005 0.0088µg/L0.00052706-91-4


(PFHxS)

0.0418 0.0519 <0.0005 0.0855µg/L0.0005355-46-4


(PFHpS)

0.0036 0.0028 <0.0005 0.0034µg/L0.0005375-92-8


(PFOS)

0.0144 0.0881 <0.0003 0.0252µg/L0.00031763-23-1


(PFDS)

<0.0005 <0.0005 <0.0005 <0.0005µg/L0.0005335-77-3


<0.002Perfluorobutanoic acid (PFBA) <0.002 <0.002 <0.002 0.023µg/L0.002375-22-4

0.0037Perfluoropentanoic acid (PFPeA) 0.0006 0.0052 <0.0005 <0.0005µg/L0.00052706-90-3

0.0150Perfluorohexanoic acid (PFHxA) 0.0010 0.0057 <0.0005 <0.0005µg/L0.0005307-24-4

0.0057Perfluoroheptanoic acid (PFHpA) 0.0008 0.0050 <0.0005 <0.0005µg/L0.0005375-85-9

0.0174Perfluorooctanoic acid (PFOA) 0.0076 0.0185 <0.0005 <0.0005µg/L0.0005335-67-1

<0.0005Perfluorononanoic acid (PFNA) <0.0005 0.0025 <0.0005 <0.0005µg/L0.0005375-95-1

<0.0005Perfluorodecanoic acid (PFDA) <0.0005 0.0013 <0.0005 <0.0005µg/L0.0005335-76-2


(PFUnDA)

<0.0005 <0.0005 <0.0005 <0.0005µg/L0.00052058-94-8


(PFDoDA)

<0.0005 <0.0005 <0.0005 <0.0005µg/L0.0005307-55-1


(PFTrDA)

<0.0005 <0.0005 <0.0005 <0.0005µg/L0.000572629-94-8


(PFTeDA)

<0.0005 <0.0005 <0.0005 <0.0005µg/L0.0005376-06-7



(FOSA)

<0.0005 <0.0005 <0.0005 <0.0005µg/L0.0005754-91-6



<0.001 <0.001 <0.001 <0.001µg/L0.00131506-32-8



<0.001 <0.001 <0.001 <0.001µg/L0.0014151-50-2

42 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_MW008_1703160315_MW007_1703160315_MW006_1703160315_MW005_1703160315_MW004_170316Client sample IDSub-Matrix: WATER

(Matrix: WATER)







<0.001 <0.001 <0.001 <0.001µg/L0.0012448-09-7



<0.001 <0.001 <0.001 <0.001µg/L0.0011691-99-2



(MeFOSAA)

<0.0005 <0.0005 <0.0005 <0.0005µg/L0.00052355-31-9



(EtFOSAA)

<0.0005 <0.0005 <0.0005 <0.0005µg/L0.00052991-50-6



(4:2 FTS)

<0.001 <0.001 <0.001 <0.001µg/L0.001757124-72-4


(6:2 FTS)

0.013 0.005 <0.001 <0.001µg/L0.00127619-97-2


(8:2 FTS)

<0.001 <0.001 <0.001 <0.001µg/L0.00139108-34-4


(10:2 FTS)

<0.001 <0.001 <0.001 <0.001µg/L0.001120226-60-0

EP231P: PFAS Sums

0.307 0.0958 0.204 <0.0003 0.160µg/L0.0003----Sum of PFAS

0.210Sum of PFHxS and PFOS 0.0562 0.140 <0.0003 0.111µg/L0.0003355-46-4/1763-23-

1

0.282 0.0864 0.192 <0.0003 0.148µg/L0.0003----Sum of PFAS (WA DER List)


104 103 104 105 107%0.0005----13C4-PFOS

43 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

0315_QC300_1703140315_QC110_1703160315_QC109_1703150315_SW007_1703150315_SW005_170315Client sample IDSub-Matrix: WATER

(Matrix: WATER)






(PFBS)

0.0185 0.0217 0.0113 ----µg/L0.0005375-73-5

----Perfluorobutane sulfonic acid

(PFBS)

---- ---- ---- <0.02µg/L0.02375-73-5


(PFPeS)

0.0051 0.0049 0.0047 ----µg/L0.00052706-91-4

----Perfluoropentane sulfonic acid

(PFPeS)

---- ---- ---- <0.02µg/L0.022706-91-4


(PFHxS)

0.0692 0.0388 0.0478 ----µg/L0.0005355-46-4

----Perfluorohexane sulfonic acid

(PFHxS)

---- ---- ---- <0.02µg/L0.02355-46-4


(PFHpS)

0.0046 0.0017 0.0023 ----µg/L0.0005375-92-8

----Perfluoroheptane sulfonic acid

(PFHpS)

---- ---- ---- <0.02µg/L0.02375-92-8


(PFOS)

0.0956 0.0429 0.0888 ----µg/L0.00031763-23-1


(PFDS)

<0.0005 <0.0005 <0.0005 ----µg/L0.0005335-77-3

----Perfluorooctane sulfonic acid

(PFOS)

---- ---- ---- <0.01µg/L0.011763-23-1

----Perfluorodecane sulfonic acid

(PFDS)

---- ---- ---- <0.02µg/L0.02335-77-3


<0.002Perfluorobutanoic acid (PFBA) <0.002 <0.002 <0.002 ----µg/L0.002375-22-4

----Perfluorobutanoic acid (PFBA) ---- ---- ---- <0.1µg/L0.1375-22-4

0.0042Perfluoropentanoic acid (PFPeA) 0.0036 0.0047 0.0048 ----µg/L0.00052706-90-3

----Perfluoropentanoic acid (PFPeA) ---- ---- ---- <0.02µg/L0.022706-90-3

0.0036Perfluorohexanoic acid (PFHxA) 0.0048 0.0039 0.0051 ----µg/L0.0005307-24-4

----Perfluorohexanoic acid (PFHxA) ---- ---- ---- <0.02µg/L0.02307-24-4

0.0023Perfluoroheptanoic acid (PFHpA) 0.0023 0.0024 0.0061 ----µg/L0.0005375-85-9

----Perfluoroheptanoic acid (PFHpA) ---- ---- ---- <0.02µg/L0.02375-85-9

0.0060Perfluorooctanoic acid (PFOA) 0.0120 0.0071 0.0230 ----µg/L0.0005335-67-1

----Perfluorooctanoic acid (PFOA) ---- ---- ---- <0.01µg/L0.01335-67-1

0.0013Perfluorononanoic acid (PFNA) 0.0022 0.0015 0.0020 ----µg/L0.0005375-95-1

44 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results


(Matrix: WATER)




EP231B: Perfluoroalkyl Carboxylic Acids - Continued

----Perfluorononanoic acid (PFNA) ---- ---- ---- <0.02µg/L0.02375-95-1

<0.0005Perfluorodecanoic acid (PFDA) 0.0006 <0.0005 0.0013 ----µg/L0.0005335-76-2

----Perfluorodecanoic acid (PFDA) ---- ---- ---- <0.02µg/L0.02335-76-2


(PFUnDA)

<0.0005 <0.0005 <0.0005 ----µg/L0.00052058-94-8

----Perfluoroundecanoic acid

(PFUnDA)

---- ---- ---- <0.02µg/L0.022058-94-8


(PFDoDA)

<0.0005 <0.0005 <0.0005 ----µg/L0.0005307-55-1

----Perfluorododecanoic acid

(PFDoDA)

---- ---- ---- <0.02µg/L0.02307-55-1


(PFTrDA)

<0.0005 <0.0005 <0.0005 ----µg/L0.000572629-94-8

----Perfluorotridecanoic acid

(PFTrDA)

---- ---- ---- <0.02µg/L0.0272629-94-8


(PFTeDA)

<0.0005 <0.0005 <0.0005 ----µg/L0.0005376-06-7

----Perfluorotetradecanoic acid

(PFTeDA)

---- ---- ---- <0.05µg/L0.05376-06-7



(FOSA)

<0.0005 <0.0005 <0.0005 ----µg/L0.0005754-91-6

----Perfluorooctane sulfonamide

(FOSA)

---- ---- ---- <0.02µg/L0.02754-91-6



<0.001 <0.001 <0.001 ----µg/L0.00131506-32-8

----N-Methyl perfluorooctane


---- ---- ---- <0.05µg/L0.0531506-32-8



<0.001 <0.001 <0.001 ----µg/L0.0014151-50-2

----N-Ethyl perfluorooctane


---- ---- ---- <0.05µg/L0.054151-50-2



<0.001 <0.001 <0.001 ----µg/L0.0012448-09-7



---- ---- ---- <0.05µg/L0.052448-09-7

45 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results


(Matrix: WATER)







<0.001 <0.001 <0.001 ----µg/L0.0011691-99-2



---- ---- ---- <0.05µg/L0.051691-99-2



(MeFOSAA)

<0.0005 <0.0005 <0.0005 ----µg/L0.00052355-31-9



(MeFOSAA)

---- ---- ---- <0.02µg/L0.022355-31-9



(EtFOSAA)

<0.0005 <0.0005 <0.0005 ----µg/L0.00052991-50-6



(EtFOSAA)

---- ---- ---- <0.02µg/L0.022991-50-6



(4:2 FTS)

<0.001 <0.001 <0.001 ----µg/L0.001757124-72-4

----4:2 Fluorotelomer sulfonic acid

(4:2 FTS)

---- ---- ---- <0.05µg/L0.05757124-72-4


(6:2 FTS)

<0.001 <0.001 0.005 ----µg/L0.00127619-97-2


(6:2 FTS)

---- ---- ---- <0.05µg/L0.0527619-97-2


(8:2 FTS)

<0.001 <0.001 <0.001 ----µg/L0.00139108-34-4


(8:2 FTS)

---- ---- ---- <0.05µg/L0.0539108-34-4


(10:2 FTS)

<0.001 <0.001 <0.001 ----µg/L0.001120226-60-0


(10:2 FTS)

---- ---- ---- <0.05µg/L0.05120226-60-0

EP231P: PFAS Sums

0.145 0.218 0.130 0.202 ----µg/L0.0003----Sum of PFAS

---- ---- ---- ---- <0.01µg/L0.01----Sum of PFAS

46 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results


(Matrix: WATER)




EP231P: PFAS Sums - Continued

0.0979Sum of PFHxS and PFOS 0.165 0.0817 0.137 ----µg/L0.0003355-46-4/1763-23-

1

----Sum of PFHxS and PFOS ---- ---- ---- <0.01µg/L0.01355-46-4/1763-23-

1

0.136 0.206 0.122 0.192 ----µg/L0.0003----Sum of PFAS (WA DER List)

---- ---- ---- ---- <0.01µg/L0.01----Sum of PFAS (WA DER List)


105 99.8 104 106 ----%0.0005----13C4-PFOS

---- ---- ---- ---- 110%0.02----13C4-PFOS

47 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

------------0315_QC302_1703160315_QC301_170315Client sample IDSub-Matrix: WATER

(Matrix: WATER)

------------16-Mar-2017 00:0015-Mar-2017 00:00Client sampling date / time

------------------------ES1706394-104ES1706394-103UnitLORCAS NumberCompound

Result Result ---- ---- ----



(PFBS)

<0.02 ---- ---- ----µg/L0.02375-73-5


(PFPeS)

<0.02 ---- ---- ----µg/L0.022706-91-4


(PFHxS)

<0.02 ---- ---- ----µg/L0.02355-46-4


(PFHpS)

<0.02 ---- ---- ----µg/L0.02375-92-8

<0.01Perfluorooctane sulfonic acid

(PFOS)

<0.01 ---- ---- ----µg/L0.011763-23-1


(PFDS)

<0.02 ---- ---- ----µg/L0.02335-77-3


<0.1Perfluorobutanoic acid (PFBA) <0.1 ---- ---- ----µg/L0.1375-22-4

<0.02Perfluoropentanoic acid (PFPeA) <0.02 ---- ---- ----µg/L0.022706-90-3

<0.02Perfluorohexanoic acid (PFHxA) <0.02 ---- ---- ----µg/L0.02307-24-4

<0.02Perfluoroheptanoic acid (PFHpA) <0.02 ---- ---- ----µg/L0.02375-85-9

<0.01Perfluorooctanoic acid (PFOA) <0.01 ---- ---- ----µg/L0.01335-67-1

<0.02Perfluorononanoic acid (PFNA) <0.02 ---- ---- ----µg/L0.02375-95-1

<0.02Perfluorodecanoic acid (PFDA) <0.02 ---- ---- ----µg/L0.02335-76-2


(PFUnDA)

<0.02 ---- ---- ----µg/L0.022058-94-8


(PFDoDA)

<0.02 ---- ---- ----µg/L0.02307-55-1


(PFTrDA)

<0.02 ---- ---- ----µg/L0.0272629-94-8


(PFTeDA)

<0.05 ---- ---- ----µg/L0.05376-06-7



(FOSA)

<0.02 ---- ---- ----µg/L0.02754-91-6



<0.05 ---- ---- ----µg/L0.0531506-32-8



<0.05 ---- ---- ----µg/L0.054151-50-2

48 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Analytical Results

------------0315_QC302_1703160315_QC301_170315Client sample IDSub-Matrix: WATER

(Matrix: WATER)

------------16-Mar-2017 00:0015-Mar-2017 00:00Client sampling date / time

------------------------ES1706394-104ES1706394-103UnitLORCAS NumberCompound

Result Result ---- ---- ----




<0.05 ---- ---- ----µg/L0.052448-09-7



<0.05 ---- ---- ----µg/L0.051691-99-2



(MeFOSAA)

<0.02 ---- ---- ----µg/L0.022355-31-9



(EtFOSAA)

<0.02 ---- ---- ----µg/L0.022991-50-6



(4:2 FTS)

<0.05 ---- ---- ----µg/L0.05757124-72-4


(6:2 FTS)

<0.05 ---- ---- ----µg/L0.0527619-97-2


(8:2 FTS)

<0.05 ---- ---- ----µg/L0.0539108-34-4


(10:2 FTS)

<0.05 ---- ---- ----µg/L0.05120226-60-0

EP231P: PFAS Sums

<0.01 <0.01 ---- ---- ----µg/L0.01----Sum of PFAS

<0.01Sum of PFHxS and PFOS <0.01 ---- ---- ----µg/L0.01355-46-4/1763-23-

1

<0.01 <0.01 ---- ---- ----µg/L0.01----Sum of PFAS (WA DER List)


111 106 ---- ---- ----%0.02----13C4-PFOS

49 of 49:Page

Work Order :

:Client


1652034:Project

GOLDER ASSOCIATES

Surrogate Control Limits

Recovery Limits (%)Sub-Matrix: SOIL

Compound CAS Number Low High


13C4-PFOS ---- 70 130

Recovery Limits (%)Sub-Matrix: WATER

Compound CAS Number Low High


13C4-PFOS ---- 70 120

Environmental

SAMPLE RECEIPT NOTIFICATION (SRN)Work Order : ES1706394


: :ContactContact MS OLGA BUKHTEEVA Customer Services ES

:: AddressAddress LEVEL 1, 124 PACIFIC HIGHWAY

ST LEONARDS NSW, AUSTRALIA

2065

277-289 Woodpark Road Smithfield

NSW Australia 2164

:: E-mailE-mail [email protected] [email protected]

:: TelephoneTelephone +61 02 9478 3900 +61-2-8784 8555

:: FacsimileFacsimile +61 02 9478 3901 +61-2-8784 8500

::Project 1652034 Page 1 of 6

:Order number PO01472 :Quote number EB2016GOLASS0004 (BN/404/16)

:C-O-C number ---- :QC Level NEPM 2013 B3 & ALS QC Standard

Site : Kapooka


DatesDate Samples Received : Issue Date : 20-Mar-201717-Mar-2017 12:00

Scheduled Reporting Date: 24-Mar-2017:Client Requested Due

Date

24-Mar-2017

Delivery DetailsMode of Delivery : :Undefined Intact.Security Seal

No. of coolers/boxes : :6 Temperature 5.7'c - Ice present

: : 110 / 108Receipt Detail No. of samples received / analysed

General Comments

This report contains the following information:l

- Sample Container(s)/Preservation Non-Compliances

- Summary of Sample(s) and Requested Analysis

- Proactive Holding Time Report

- Requested Deliverables

l This is an updated SRA which indicates added analysis for this work order.

l Samples QC201, QC203, QC205, QC207, QC209, QC210 will be sent to Eurofins as per coc requestl Please refer to the Proactive Holding Time Report table below which summarises breaches of

recommended holding times that have occurred prior to samples/instructions being received at

the laboratory. The absence of this summary table indicates that all samples have been received

within the recommended holding times for the analysis requested.l Please direct any queries you have regarding this work order to the above ALS laboratory contact.

l Analytical work for this work order will be conducted at ALS Sydney.

l Sample Disposal - Aqueous (14 days), Solid (60 days) from date of completion of work order.


:Client GOLDER ASSOCIATES

Work Order : ES1706394 Amendment 02 of 6:Page

20-Mar-2017:Issue Date

Sample Container(s)/Preservation Non-Compliances

All comparisons are made against pretreatment/preservation AS, APHA, USEPA standards.

l No sample container / preservation non-compliance exists.

Any sample identifications that cannot be displayed entirely in the analysis summary table will be listed below.

ES1706394-001 : [ 15-Mar-2017 ] : 0315_BH001_0.0_170315

ES1706394-002 : [ 15-Mar-2017 ] : 0315_BH001_1.0_170315

ES1706394-003 : [ 15-Mar-2017 ] : 0315_BH001_2.0_170315

ES1706394-004 : [ 15-Mar-2017 ] : 0315_BH001_3.0_170315

ES1706394-005 : [ 15-Mar-2017 ] : 0315_BH001_4.0_170315

ES1706394-006 : [ 15-Mar-2017 ] : 0315_BH002_0.0_170315

ES1706394-007 : [ 15-Mar-2017 ] : 0315_BH002_1.0_170315

ES1706394-008 : [ 15-Mar-2017 ] : 0315_BH002_2.0_170315

ES1706394-009 : [ 15-Mar-2017 ] : 0315_BH002_3.0_170315

ES1706394-010 : [ 15-Mar-2017 ] : 0315_BH002_4.0_170315

ES1706394-011 : [ 14-Mar-2017 ] : 0315_BH003_0.0_170314

ES1706394-012 : [ 14-Mar-2017 ] : 0315_BH003_1.0_170314

ES1706394-013 : [ 14-Mar-2017 ] : 0315_BH003_2.0_170314

ES1706394-014 : [ 14-Mar-2017 ] : 0315_BH003_3.0_170314

ES1706394-015 : [ 14-Mar-2017 ] : 0315_BH003_4.0_170314

ES1706394-016 : [ 14-Mar-2017 ] : 0315_BH004_0.0_170314

ES1706394-017 : [ 14-Mar-2017 ] : 0315_BH004_1.0_170314

ES1706394-018 : [ 14-Mar-2017 ] : 0315_BH004_2.0_170314

ES1706394-019 : [ 14-Mar-2017 ] : 0315_BH004_3.0_170314

ES1706394-020 : [ 14-Mar-2017 ] : 0315_BH004_4.0_170314

ES1706394-021 : [ 14-Mar-2017 ] : 0315_BH005_0.0_170314

ES1706394-022 : [ 14-Mar-2017 ] : 0315_BH005_1.0_170314

ES1706394-023 : [ 14-Mar-2017 ] : 0315_BH005_2.0_170314

ES1706394-024 : [ 14-Mar-2017 ] : 0315_BH005_3.0_170314

ES1706394-025 : [ 14-Mar-2017 ] : 0315_BH005_4.0_170314

ES1706394-026 : [ 14-Mar-2017 ] : 0315_BH006_0.0_170314

ES1706394-027 : [ 14-Mar-2017 ] : 0315_BH006_1.0_170314

ES1706394-028 : [ 14-Mar-2017 ] : 0315_BH006_2.0_170314

ES1706394-029 : [ 14-Mar-2017 ] : 0315_BH006_3.0_170314

ES1706394-030 : [ 14-Mar-2017 ] : 0315_BH006_4.0_170314

ES1706394-031 : [ 15-Mar-2017 ] : 0315_BH007_0.0_170315

ES1706394-032 : [ 15-Mar-2017 ] : 0315_BH007_1.0_170315

ES1706394-033 : [ 15-Mar-2017 ] : 0315_BH007_2.0_170315

ES1706394-034 : [ 15-Mar-2017 ] : 0315_BH007_3.0_170315

ES1706394-035 : [ 15-Mar-2017 ] : 0315_BH007_4.0_170315

ES1706394-036 : [ 15-Mar-2017 ] : 0315_BH008_0.0_170315

ES1706394-037 : [ 15-Mar-2017 ] : 0315_BH008_1.0_170315

ES1706394-038 : [ 15-Mar-2017 ] : 0315_BH008_2.0_170315

ES1706394-039 : [ 15-Mar-2017 ] : 0315_BH008_3.0_170315

ES1706394-040 : [ 15-Mar-2017 ] : 0315_BH008_4.0_170315

ES1706394-041 : [ 15-Mar-2017 ] : 0315_BH009_0.0_170315

ES1706394-042 : [ 15-Mar-2017 ] : 0315_BH009_1.0_170315

ES1706394-043 : [ 15-Mar-2017 ] : 0315_BH009_2.0_170315

ES1706394-044 : [ 15-Mar-2017 ] : 0315_BH009_3.0_170315

ES1706394-045 : [ 15-Mar-2017 ] : 0315_BH009_4.0_170315

ES1706394-046 : [ 15-Mar-2017 ] : 0315_BH010_0.0_170315

ES1706394-047 : [ 15-Mar-2017 ] : 0315_BH010_1.0_170315

ES1706394-048 : [ 15-Mar-2017 ] : 0315_BH010_2.0_170315

ES1706394-049 : [ 15-Mar-2017 ] : 0315_BH010_3.0_170315

ES1706394-050 : [ 15-Mar-2017 ] : 0315_BH010_4.0_170315

ES1706394-051 : [ 14-Mar-2017 ] : 0315_BH011_0.0_170314

ES1706394-052 : [ 14-Mar-2017 ] : 0315_BH011_1.0_170314

ES1706394-053 : [ 14-Mar-2017 ] : 0315_BH011_2.0_170314

ES1706394-054 : [ 14-Mar-2017 ] : 0315_BH011_3.0_170314

ES1706394-055 : [ 14-Mar-2017 ] : 0315_BH011_4.0_170314




ES1706394-056 : [ 14-Mar-2017 ] : 0315_BH012_0.0_170314

ES1706394-057 : [ 14-Mar-2017 ] : 0315_BH012_1.0_170314

ES1706394-058 : [ 14-Mar-2017 ] : 0315_BH012_2.0_170314

ES1706394-059 : [ 14-Mar-2017 ] : 0315_BH012_3.0_170314

ES1706394-060 : [ 14-Mar-2017 ] : 0315_BH012_4.0_170314

ES1706394-061 : [ 14-Mar-2017 ] : 0315_BH013_0.0_170314

ES1706394-062 : [ 14-Mar-2017 ] : 0315_BH013_1.0_170314

ES1706394-063 : [ 14-Mar-2017 ] : 0315_BH013_2.0_170314

ES1706394-064 : [ 14-Mar-2017 ] : 0315_BH013_3.0_170314

ES1706394-065 : [ 14-Mar-2017 ] : 0315_BH013_4.0_170314

ES1706394-066 : [ 15-Mar-2017 ] : 0315_BH014_0.0_170315

ES1706394-067 : [ 15-Mar-2017 ] : 0315_BH014_1.0_170315

ES1706394-068 : [ 15-Mar-2017 ] : 0315_BH014_2.0_170315

ES1706394-069 : [ 15-Mar-2017 ] : 0315_BH014_3.0_170315

ES1706394-070 : [ 15-Mar-2017 ] : 0315_BH014_4.0_170315

ES1706394-071 : [ 15-Mar-2017 ] : 0315_BH015_0.0_170315

ES1706394-072 : [ 15-Mar-2017 ] : 0315_BH015_1.0_170315

ES1706394-073 : [ 15-Mar-2017 ] : 0315_BH015_2.0_170315

ES1706394-074 : [ 15-Mar-2017 ] : 0315_BH015_3.0_170315

ES1706394-075 : [ 15-Mar-2017 ] : 0315_BH015_4.0_170315

Summary of Sample(s) and Requested Analysis

Some items described below may be part of a laboratory

process necessary for the execution of client requested

tasks. Packages may contain additional analyses, such

as the determination of moisture content and preparation

tasks, that are included in the package.

If no sampling time is provided, the sampling time will

default 00:00 on the date of sampling. If no sampling date

is provided, the sampling date will be assumed by the

laboratory and displayed in brackets without a time

component

SO

IL -

EA

05

5-1

03

Mo

istu

re C

on

ten

t

SO

IL -

EP

23

1X

(so

lids)

PF

AS

- F

ull

Su

ite (

28

an

aly

tes)

SO

IL -

S-1

8 (

NO

MO

IST

)

TR

H(C

6-C

9)/

BT

EX

N w

ith N

o M

ois

ture

fo

r T

Bs

ES1706394-001 [ 15-Mar-2017 ] 0315_BH001_0.0_170315 ü ü

ES1706394-002 [ 15-Mar-2017 ] 0315_BH001_1.0_170315 ü ü

ES1706394-003 [ 15-Mar-2017 ] 0315_BH001_2.0_170315 ü ü

ES1706394-004 [ 15-Mar-2017 ] 0315_BH001_3.0_170315 ü ü

ES1706394-005 [ 15-Mar-2017 ] 0315_BH001_4.0_170315 ü ü

ES1706394-006 [ 15-Mar-2017 ] 0315_BH002_0.0_170315 ü ü

ES1706394-007 [ 15-Mar-2017 ] 0315_BH002_1.0_170315 ü ü

ES1706394-008 [ 15-Mar-2017 ] 0315_BH002_2.0_170315 ü ü

ES1706394-009 [ 15-Mar-2017 ] 0315_BH002_3.0_170315 ü ü

ES1706394-010 [ 15-Mar-2017 ] 0315_BH002_4.0_170315 ü ü

ES1706394-011 [ 14-Mar-2017 ] 0315_BH003_0.0_170314 ü ü

ES1706394-012 [ 14-Mar-2017 ] 0315_BH003_1.0_170314 ü ü

ES1706394-013 [ 14-Mar-2017 ] 0315_BH003_2.0_170314 ü ü

ES1706394-014 [ 14-Mar-2017 ] 0315_BH003_3.0_170314 ü ü

ES1706394-015 [ 14-Mar-2017 ] 0315_BH003_4.0_170314 ü ü

ES1706394-016 [ 14-Mar-2017 ] 0315_BH004_0.0_170314 ü ü

ES1706394-017 [ 14-Mar-2017 ] 0315_BH004_1.0_170314 ü ü

ES1706394-018 [ 14-Mar-2017 ] 0315_BH004_2.0_170314 ü ü

ES1706394-019 [ 14-Mar-2017 ] 0315_BH004_3.0_170314 ü ü

ES1706394-020 [ 14-Mar-2017 ] 0315_BH004_4.0_170314 ü ü

ES1706394-021 [ 14-Mar-2017 ] 0315_BH005_0.0_170314 ü ü

ES1706394-022 [ 14-Mar-2017 ] 0315_BH005_1.0_170314 ü ü

Matrix: SOIL

Client sample IDLaboratory sample

ID

Client sampling

date / time




SO

IL -

EA

055-1

03

Mois

ture

Conte

nt

SO

IL -

EP

231X

(so

lids)

PF

AS

- F

ull

Suite

(28 a

naly

tes)

SO

IL -

S-1

8 (

NO

MO

IST

)

TR

H(C

6-C

9)/

BT

EX

N w

ith N

o M

ois

ture

for

TB

s

ES1706394-023 [ 14-Mar-2017 ] 0315_BH005_2.0_170314 ü ü

ES1706394-024 [ 14-Mar-2017 ] 0315_BH005_3.0_170314 ü ü

ES1706394-025 [ 14-Mar-2017 ] 0315_BH005_4.0_170314 ü ü

ES1706394-026 [ 14-Mar-2017 ] 0315_BH006_0.0_170314 ü ü

ES1706394-027 [ 14-Mar-2017 ] 0315_BH006_1.0_170314 ü ü

ES1706394-028 [ 14-Mar-2017 ] 0315_BH006_2.0_170314 ü ü

ES1706394-029 [ 14-Mar-2017 ] 0315_BH006_3.0_170314 ü ü

ES1706394-030 [ 14-Mar-2017 ] 0315_BH006_4.0_170314 ü ü

ES1706394-031 [ 15-Mar-2017 ] 0315_BH007_0.0_170315 ü ü

ES1706394-032 [ 15-Mar-2017 ] 0315_BH007_1.0_170315 ü ü

ES1706394-033 [ 15-Mar-2017 ] 0315_BH007_2.0_170315 ü ü

ES1706394-034 [ 15-Mar-2017 ] 0315_BH007_3.0_170315 ü ü

ES1706394-035 [ 15-Mar-2017 ] 0315_BH007_4.0_170315 ü ü

ES1706394-036 [ 15-Mar-2017 ] 0315_BH008_0.0_170315 ü ü

ES1706394-037 [ 15-Mar-2017 ] 0315_BH008_1.0_170315 ü ü

ES1706394-038 [ 15-Mar-2017 ] 0315_BH008_2.0_170315 ü ü

ES1706394-039 [ 15-Mar-2017 ] 0315_BH008_3.0_170315 ü ü

ES1706394-040 [ 15-Mar-2017 ] 0315_BH008_4.0_170315 ü ü

ES1706394-041 [ 15-Mar-2017 ] 0315_BH009_0.0_170315 ü ü

ES1706394-042 [ 15-Mar-2017 ] 0315_BH009_1.0_170315 ü ü

ES1706394-043 [ 15-Mar-2017 ] 0315_BH009_2.0_170315 ü ü

ES1706394-044 [ 15-Mar-2017 ] 0315_BH009_3.0_170315 ü ü

ES1706394-045 [ 15-Mar-2017 ] 0315_BH009_4.0_170315 ü ü

ES1706394-046 [ 15-Mar-2017 ] 0315_BH010_0.0_170315 ü ü

ES1706394-047 [ 15-Mar-2017 ] 0315_BH010_1.0_170315 ü ü

ES1706394-048 [ 15-Mar-2017 ] 0315_BH010_2.0_170315 ü ü

ES1706394-049 [ 15-Mar-2017 ] 0315_BH010_3.0_170315 ü ü

ES1706394-050 [ 15-Mar-2017 ] 0315_BH010_4.0_170315 ü ü

ES1706394-051 [ 14-Mar-2017 ] 0315_BH011_0.0_170314 ü ü

ES1706394-052 [ 14-Mar-2017 ] 0315_BH011_1.0_170314 ü ü

ES1706394-053 [ 14-Mar-2017 ] 0315_BH011_2.0_170314 ü ü

ES1706394-054 [ 14-Mar-2017 ] 0315_BH011_3.0_170314 ü ü

ES1706394-055 [ 14-Mar-2017 ] 0315_BH011_4.0_170314 ü ü

ES1706394-056 [ 14-Mar-2017 ] 0315_BH012_0.0_170314 ü ü

ES1706394-057 [ 14-Mar-2017 ] 0315_BH012_1.0_170314 ü ü

ES1706394-058 [ 14-Mar-2017 ] 0315_BH012_2.0_170314 ü ü

ES1706394-059 [ 14-Mar-2017 ] 0315_BH012_3.0_170314 ü ü

ES1706394-060 [ 14-Mar-2017 ] 0315_BH012_4.0_170314 ü ü

ES1706394-061 [ 14-Mar-2017 ] 0315_BH013_0.0_170314 ü ü

ES1706394-062 [ 14-Mar-2017 ] 0315_BH013_1.0_170314 ü ü

ES1706394-063 [ 14-Mar-2017 ] 0315_BH013_2.0_170314 ü ü




SO

IL -

EA

055-1

03

Mois

ture

Conte

nt

SO

IL -

EP

231X

(so

lids)

PF

AS

- F

ull

Suite

(28 a

naly

tes)

SO

IL -

S-1

8 (

NO

MO

IST

)

TR

H(C

6-C

9)/

BT

EX

N w

ith N

o M

ois

ture

for

TB

s

ES1706394-064 [ 14-Mar-2017 ] 0315_BH013_3.0_170314 ü ü

ES1706394-065 [ 14-Mar-2017 ] 0315_BH013_4.0_170314 ü ü

ES1706394-066 [ 15-Mar-2017 ] 0315_BH014_0.0_170315 ü ü

ES1706394-067 [ 15-Mar-2017 ] 0315_BH014_1.0_170315 ü ü

ES1706394-068 [ 15-Mar-2017 ] 0315_BH014_2.0_170315 ü ü

ES1706394-069 [ 15-Mar-2017 ] 0315_BH014_3.0_170315 ü ü

ES1706394-070 [ 15-Mar-2017 ] 0315_BH014_4.0_170315 ü ü

ES1706394-071 [ 15-Mar-2017 ] 0315_BH015_0.0_170315 ü ü

ES1706394-072 [ 15-Mar-2017 ] 0315_BH015_1.0_170315 ü ü

ES1706394-073 [ 15-Mar-2017 ] 0315_BH015_2.0_170315 ü ü

ES1706394-074 [ 15-Mar-2017 ] 0315_BH015_3.0_170315 ü ü

ES1706394-075 [ 15-Mar-2017 ] 0315_BH015_4.0_170315 ü ü

ES1706394-084 [ 14-Mar-2017 ] 0315_SD001_170314 ü ü

ES1706394-085 [ 14-Mar-2017 ] 0315_SD002_170314 ü ü

ES1706394-086 [ 16-Mar-2017 ] 0315_SD003_170316 ü ü

ES1706394-087 [ 16-Mar-2017 ] 0315_SD004_170316 ü ü

ES1706394-088 [ 15-Mar-2017 ] 0315_SD005_170315 ü ü

ES1706394-089 [ 16-Mar-2017 ] 0315_SD006_170316 ü ü

ES1706394-090 [ 15-Mar-2017 ] 0315_SD007_170315 ü ü

ES1706394-091 [ 14-Mar-2017 ] 0315_QC100_170314 ü ü

ES1706394-092 [ 14-Mar-2017 ] 0315_QC101_170314 ü ü

ES1706394-093 [ 15-Mar-2017 ] 0315_QC102_170315 ü ü

ES1706394-094 [ 15-Mar-2017 ] 0315_QC103_170315 ü ü

ES1706394-095 [ 15-Mar-2017 ] 0315_QC104_170315 ü ü

ES1706394-096 [ 15-Mar-2017 ] 0315_QC105_170315 ü ü

ES1706394-097 [ 15-Mar-2017 ] 0315_QC106_170315 ü ü

ES1706394-098 [ 15-Mar-2017 ] 0315_QC107_170315 ü ü

ES1706394-099 [ 15-Mar-2017 ] 0315_QC108_170315 ü ü

ES1706394-106 14-Mar-2017 00:00 0315_QC502_170314 ü

ES1706394-108 15-Mar-2017 00:00 0315_QC504_170315 ü

ES1706394-110 16-Mar-2017 00:00 0315_QC506_170316 ü




(On H

old

) W

AT

ER

No a

naly

sis

request

ed

WA

TE

R -

EP

231X

PF

AS

- F

ull

Suite

(28 a

naly

tes)

WA

TE

R -

EP

231X

-ST

PF

AS

- F

ull

Suite

Drinki

ng W

ate

r (2

8 a

naly

tes)

WA

TE

R -

W-1

8

TR

H(C

6 -

C9)/

BT

EX

N

ES1706394-076 16-Mar-2017 00:00 0315_MW004_170316 ü

ES1706394-077 16-Mar-2017 00:00 0315_MW005_170316 ü

ES1706394-078 16-Mar-2017 00:00 0315_MW006_170316 ü

ES1706394-079 16-Mar-2017 00:00 0315_MW007_170316 ü

ES1706394-080 16-Mar-2017 00:00 0315_MW008_170316 ü

ES1706394-081 16-Mar-2017 00:00 0315_MW009_170316 ü

ES1706394-082 15-Mar-2017 00:00 0315_SW005_170315 ü

ES1706394-083 15-Mar-2017 00:00 0315_SW007_170315 ü

ES1706394-100 15-Mar-2017 00:00 0315_QC109_170315 ü

ES1706394-101 16-Mar-2017 00:00 0315_QC110_170316 ü

ES1706394-102 14-Mar-2017 00:00 0315_QC300_170314 ü

ES1706394-103 15-Mar-2017 00:00 0315_QC301_170315 ü

ES1706394-104 16-Mar-2017 00:00 0315_QC302_170316 ü

ES1706394-105 14-Mar-2017 00:00 0315_QC501_170314 ü

ES1706394-107 15-Mar-2017 00:00 0315_QC503_170315 ü

ES1706394-109 16-Mar-2017 00:00 0315_QC505_170316 ü

Matrix: WATER

Client sample IDLaboratory sample

ID

Client sampling

date / time

Proactive Holding Time Report

Sample(s) have been received within the recommended holding times for the requested analysis.

Requested Deliverables

ACCOUNTS PAYABLE

- A4 - AU Tax Invoice (INV) Email [email protected]

u

OLGA BUKHTEEVA

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - XTab (XTAB) Email [email protected]

Certificate of Analysis

Golder Associates

124 Pacific Hwy

St. Leonards

NSW 1585

Attention: Andrew Holloway

Report 538644-W

Project name KAPOOKA

Project ID 1652034

Received Date Mar 20, 2017

Client Sample ID 0315_QC209_170315

0315_QC210_170316

Sample Matrix Water Water

Eurofins | mgt Sample No. S17-Ma21088 S17-Ma21089

Date Sampled Mar 15, 2017 Mar 16, 2017

Test/Reference LOR Unit

Per- and Polyfluorinated Alkyl Substances (PFASs) - Trace Level

Perfluorobutanesulfonic acid (PFBS) 0.01 ug/L < 0.01 0.01

Perfluorobutanoic acid (PFBA) 0.05 ug/L < 0.05 < 0.05

Perfluorohexanesulfonic acid (PFHxS) 0.01 ug/L N090.09 N090.08

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N090.07 N090.11

Perfluorodecanesulfonic acid (PFDS) 0.01 ug/L < 0.01 < 0.01

Perfluoropentanoic acid (PFPeA) 0.01 ug/L 0.04 0.02

Perfluorohexanoic acid (PFHxA) 0.01 ug/L < 0.01 0.03

Perfluoroheptanoic acid (PFHpA) 0.01 ug/L < 0.01 N090.02

Perfluorooctanoic acid (PFOA) 0.01 ug/L < 0.01 N090.05

Perfluorononanoic acid (PFNA) 0.01 ug/L < 0.01 < 0.01

Perfluorodecanoic acid (PFDA) 0.01 ug/L < 0.01 < 0.01

Perfluoroundecanoic acid (PFUnA) 0.01 ug/L < 0.01 < 0.01

Perfluorododecanoic acid (PFDoA) 0.01 ug/L < 0.01 < 0.01

Perfluorotridecanoic acid (PFTrDA) 0.01 ug/L < 0.01 < 0.01

Perfluorotetradecanoic acid (PFTeDA) 0.01 ug/L < 0.01 < 0.01

Perfluorooctane sulfonamide (FOSA) 0.05 ug/L < 0.05 < 0.05

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA) 0.05 ug/L < 0.05 < 0.05

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA) 0.05 ug/L < 0.05 < 0.05

1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2 FTS) 0.01 ug/L < 0.01 < 0.01

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) 0.05 ug/L < 0.05 < 0.05

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) 0.01 ug/L < 0.01 < 0.01

13C5-PFHxA (surr.) 1 % 86 109

13C8-PFOS (surr.) 1 % 70 84

Date Reported: Mar 31, 2017

Eurofins | mgt Unit F3, Building F, 16 Mars Road, Lane Cove West, NSW, Australia, 2066

ABN : 50 005 085 521 Telephone: +61 2 9900 8400

Page 1 of 9

Report Number: 538644-W

NATA AccreditedAccreditation Number 1261Site Number 18217

Accredited for compliance with ISO/IEC 17025 – TestingThe results of the tests, calibrations and/ormeasurements included in this document are traceableto Australian/national standards.

Sample HistoryWhere samples are submitted/analysed over several days, the last date of extraction and analysis is reported.A recent review of our LIMS has resulted in the correction or clarification of some method identifications. Due to this, some of the method reference information on reports has changed. However,no substantive change has been made to our laboratory methods, and as such there is no change in the validity of current or previous results (regarding both quality and NATA accreditation).

If the date and time of sampling are not provided, the Laboratory will not be responsible for compromised results should testing be performed outside the recommended holding time.

Description Testing Site Extracted Holding Time

Per- and Polyfluorinated Alkyl Substances (PFASs) - Trace Level Brisbane Mar 23, 2017 14 Days

- Method: LTM-ORG-2100 Per- and Polyfluorinated Alkyl Substances by LC-MS/MS



ABN : 50 005 085 521 Telephone: +61 2 9900 8400

Page 2 of 9


.Company Name: Golder Associates Pty Ltd (Syd) Order No.: Received: Mar 20, 2017 11:06 AMAddress: 124 Pacific Hwy Report #: 538644 Due: Mar 27, 2017

St. Leonards Phone: 02 9478 3900 Priority: 5 DayNSW 1585 Fax: 02 9478 3901 Contact Name: Andrew Holloway

Project Name: KAPOOKAProject ID: 1652034

Eurofins | mgt Analytical Services Manager : Nibha Vaidya

Sample Detail

Moisture S

et

Per- and P

olyfluorinated Alkyl S

ubstances(P

FA

Ss) - T

race Level

Per- and P


ubstances(P

FA

Ss)

Melbourne Laboratory - NATA Site # 1254 & 14271

Sydney Laboratory - NATA Site # 18217

Brisbane Laboratory - NATA Site # 20794 X X X

Perth Laboratory - NATA Site # 18217

External Laboratory

No Sample ID Sample Date SamplingTime

Matrix LAB ID

1 0315_QC201_170314

Mar 14, 2017 Soil S17-Ma21084 X X

2 0315_QC203_170315

Mar 15, 2017 Soil S17-Ma21085 X X

3 0315_QC205_170315

Mar 15, 2017 Soil S17-Ma21086 X X

4 0315_QC207_170315

Mar 15, 2017 Soil S17-Ma21087 X X

5 0315_QC209_170315

Mar 15, 2017 Water S17-Ma21088 X

6 0315_QC210_ Mar 16, 2017 Water S17-Ma21089 X

ABN– 50 005 085 521e.mail : [email protected] : www.eurofins.com.au

MelbourneMelbourneMelbourneMelbourne2-5 Kingston Town CloseOakleigh VIC 3166Phone : +61 3 8564 5000NATA # 1261Site # 1254 & 14271

SydneySydneySydneySydneyUnit F3, Building F16 Mars RoadLane Cove West NSW 2066Phone : +61 2 9900 8400NATA # 1261 Site # 18217

BrisbaneBrisbaneBrisbaneBrisbane1/21 Smallwood PlaceMurarrie QLD 4172Phone : +61 7 3902 4600NATA # 1261 Site # 20794

PerthPerthPerthPerth2/91 Leach HighwayKewdale WA 6105Phone : +61 8 9251 9600NATA # 1261Site # 18217

Date Reported:Mar 31, 2017


ABN : 50 005 085 521 Telephone: +61 2 9900 8400

Page 3 of 9


Company Name: Golder Associates Pty Ltd (Syd) Order No.: Received: Mar 20, 2017 11:06 AMAddress: 124 Pacific Hwy Report #: 538644 Due: Mar 27, 2017




Sample Detail

Moisture S

et

Per- and P


ubstances(P

FA

Ss) - T

race Level

Per- and P


ubstances(P

FA

Ss)





170316

Test Counts 4 2 4






Page 4 of 9


Internal Quality Control Review and Glossary

General

Holding Times

Units

Terms

QC - Acceptance Criteria

QC Data General Comments

1. Laboratory QC results for Method Blanks, Duplicates, Matrix Spikes, and Laboratory Control Samples are included in this QC report where applicable. Additional QC data may be available on

request.

2. All soil results are reported on a dry basis, unless otherwise stated.

3. Actual LORs are matrix dependant. Quoted LORs may be raised where sample extracts are diluted due to interferences.

4. Results are uncorrected for matrix spikes or surrogate recoveries.

5. SVOC analysis on waters are performed on homogenised, unfiltered samples, unless noted otherwise.

6. Samples were analysed on an 'as received' basis. 7. This report replaces any interim results previously issued.

Please refer to 'Sample Preservation and Container Guide' for holding times (QS3001).

For samples received on the last day of holding time, notification of testing requirements should have been received at least 6 hours prior to sample receipt deadlines as stated on the Sample

Receipt Advice.

If the Laboratory did not receive the information in the required timeframe, and regardless of any other integrity issues, suitably qualified results may still be reported.

Holding times apply from the date of sampling, therefore compliance to these may be outside the laboratory's control.

**NOTE: pH duplicates are reported as a range NOT as RPD

mg/kg: milligrams per Kilogram mg/l: milligrams per litre

ug/l: micrograms per litre ppm: Parts per million

ppb: Parts per billion %: Percentage

org/100ml: Organisms per 100 millilitres NTU: Nephelometric Turbidity Units

MPN/100mL: Most Probable Number of organisms per 100 millilitres

Dry Where a moisture has been determined on a solid sample the result is expressed on a dry basis.

LOR Limit of Reporting.

SPIKE Addition of the analyte to the sample and reported as percentage recovery.

RPD Relative Percent Difference between two Duplicate pieces of analysis.

LCS Laboratory Control Sample - reported as percent recovery

CRM Certified Reference Material - reported as percent recovery

Method Blank In the case of solid samples these are performed on laboratory certified clean sands.

In the case of water samples these are performed on de-ionised water.

Surr - Surrogate The addition of a like compound to the analyte target and reported as percentage recovery.

Duplicate A second piece of analysis from the same sample and reported in the same units as the result to show comparison.

Batch Duplicate A second piece of analysis from a sample outside of the clients batch of samples but run within the laboratory batch of analysis.

Batch SPIKE Spike recovery reported on a sample from outside of the clients batch of samples but run within the laboratory batch of analysis.

USEPA United States Environmental Protection Agency

APHA American Public Health Association

TCLP Toxicity Characteristic Leaching Procedure

COC Chain of Custody

SRA Sample Receipt Advice

CP Client Parent - QC was performed on samples pertaining to this report

NCP Non-Client Parent - QC performed on samples not pertaining to this report, QC is representative of the sequence or batch that client samples were analysed within

TEQ Toxic Equivalency Quotient

RPD Duplicates: Global RPD Duplicates Acceptance Criteria is 30% however the following acceptance guidelines are equally applicable:

Results <10 times the LOR : No Limit

Results between 10-20 times the LOR : RPD must lie between 0-50%

Results >20 times the LOR : RPD must lie between 0-30%

Surrogate Recoveries: Recoveries must lie between 50-150%-Phenols & PFASs 20-130%

1. Where a result is reported as a less than (<), higher than the nominated LOR, this is due to either matrix interference, extract dilution required due to interferences or contaminant levels within

the sample, high moisture content or insufficient sample provided.

2. Duplicate data shown within this report that states the word "BATCH" is a Batch Duplicate from outside of your sample batch, but within the laboratory sample batch at a 1:10 ratio. The Parent

and Duplicate data shown is not data from your samples.

3. Organochlorine Pesticide analysis - where reporting LCS data, Toxaphene & Chlordane are not added to the LCS.

4. Organochlorine Pesticide analysis - where reporting Spike data, Toxaphene is not added to the Spike.

5. Total Recoverable Hydrocarbons - where reporting Spike & LCS data, a single spike of commercial Hydrocarbon products in the range of C12-C30 is added and it's Total Recovery is reported

in the C10-C14 cell of the Report.

6. pH and Free Chlorine analysed in the laboratory - Analysis on this test must begin within 30 minutes of sampling.Therefore laboratory analysis is unlikely to be completed within holding time.

Analysis will begin as soon as possible after sample receipt.

7. Recovery Data (Spikes & Surrogates) - where chromatographic interference does not allow the determination of Recovery the term "INT" appears against that analyte.

8. Polychlorinated Biphenyls are spiked only using Aroclor 1260 in Matrix Spikes and LCS.

9. For Matrix Spikes and LCS results a dash " -" in the report means that the specific analyte was not added to the QC sample.

10. Duplicate RPDs are calculated from raw analytical data thus it is possible to have two sets of data.



ABN : 50 005 085 521 Telephone: +61 2 9900 8400

Page 5 of 9


Quality Control Results

Test Units Result 1 AcceptanceLimits

PassLimits

QualifyingCode

Method Blank


Perfluorobutanesulfonic acid (PFBS) ug/L < 0.01 0.01 Pass

Perfluorobutanoic acid (PFBA) ug/L < 0.05 0.05 Pass

Perfluorohexanesulfonic acid (PFHxS) ug/L < 0.01 0.01 Pass

Perfluorooctanesulfonic acid (PFOS) ug/L < 0.01 0.01 Pass

Perfluorodecanesulfonic acid (PFDS) ug/L < 0.01 0.01 Pass

Perfluoropentanoic acid (PFPeA) ug/L < 0.01 0.01 Pass

Perfluorohexanoic acid (PFHxA) ug/L < 0.01 0.01 Pass

Perfluoroheptanoic acid (PFHpA) ug/L < 0.01 0.01 Pass

Perfluorooctanoic acid (PFOA) ug/L < 0.01 0.01 Pass

Perfluorononanoic acid (PFNA) ug/L < 0.01 0.01 Pass

Perfluorodecanoic acid (PFDA) ug/L < 0.01 0.01 Pass

Perfluoroundecanoic acid (PFUnA) ug/L < 0.01 0.01 Pass

Perfluorododecanoic acid (PFDoA) ug/L < 0.01 0.01 Pass

Perfluorotridecanoic acid (PFTrDA) ug/L < 0.01 0.01 Pass

Perfluorotetradecanoic acid (PFTeDA) ug/L < 0.01 0.01 Pass

Perfluorooctane sulfonamide (FOSA) ug/L < 0.05 0.05 Pass

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA) ug/L < 0.05 0.05 Pass

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA) ug/L < 0.05 0.05 Pass

1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2 FTS) ug/L < 0.01 0.01 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) ug/L < 0.05 0.05 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) ug/L < 0.01 0.01 Pass

LCS - % Recovery


Perfluorobutanesulfonic acid (PFBS) % 96 50-150 Pass

Perfluorobutanoic acid (PFBA) % 98 50-150 Pass

Perfluorohexanesulfonic acid (PFHxS) % 104 50-150 Pass

Perfluorooctanesulfonic acid (PFOS) % 105 50-150 Pass

Perfluorodecanesulfonic acid (PFDS) % 133 50-150 Pass

Perfluoropentanoic acid (PFPeA) % 111 50-150 Pass

Perfluorohexanoic acid (PFHxA) % 120 50-150 Pass

Perfluoroheptanoic acid (PFHpA) % 113 50-150 Pass

Perfluorooctanoic acid (PFOA) % 111 50-150 Pass

Perfluorononanoic acid (PFNA) % 113 50-150 Pass

Perfluorodecanoic acid (PFDA) % 99 50-150 Pass

Perfluoroundecanoic acid (PFUnA) % 99 50-150 Pass

Perfluorododecanoic acid (PFDoA) % 101 50-150 Pass

Perfluorotridecanoic acid (PFTrDA) % 92 50-150 Pass

Perfluorotetradecanoic acid (PFTeDA) % 102 50-150 Pass

Perfluorooctane sulfonamide (FOSA) % 102 50-150 Pass

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA) % 111 50-150 Pass

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA) % 95 50-150 Pass

1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2 FTS) % 91 50-150 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) % 90 50-150 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) % 128 50-150 Pass



ABN : 50 005 085 521 Telephone: +61 2 9900 8400

Page 6 of 9


Test Lab Sample ID QASource Units Result 1 Acceptance

LimitsPass

LimitsQualifying

Code

Spike - % Recovery

Per- and Polyfluorinated Alkyl Substances (PFASs) - Trace Level Result 1

Perfluorobutanesulfonic acid(PFBS) M17-Ma16230 NCP % 93 50-150 Pass

Perfluorobutanoic acid (PFBA) M17-Ma16230 NCP % 102 50-150 Pass

Perfluorohexanesulfonic acid(PFHxS) M17-Ma16230 NCP % 102 50-150 Pass

Perfluorooctanesulfonic acid(PFOS) M17-Ma16230 NCP % 102 50-150 Pass

Perfluorodecanesulfonic acid(PFDS) M17-Ma16230 NCP % 96 50-150 Pass

Perfluoropentanoic acid (PFPeA) M17-Ma16230 NCP % 110 50-150 Pass

Perfluorohexanoic acid (PFHxA) M17-Ma16230 NCP % 120 50-150 Pass

Perfluoroheptanoic acid (PFHpA) M17-Ma16230 NCP % 106 50-150 Pass

Perfluorooctanoic acid (PFOA) M17-Ma16230 NCP % 107 50-150 Pass

Perfluorononanoic acid (PFNA) M17-Ma16230 NCP % 101 50-150 Pass

Perfluorodecanoic acid (PFDA) M17-Ma16230 NCP % 93 50-150 Pass

Perfluoroundecanoic acid (PFUnA) M17-Ma16230 NCP % 92 50-150 Pass

Perfluorododecanoic acid (PFDoA) M17-Ma16230 NCP % 82 50-150 Pass

Perfluorotridecanoic acid (PFTrDA) M17-Ma16230 NCP % 72 50-150 Pass

Perfluorotetradecanoic acid(PFTeDA) M17-Ma16230 NCP % 102 50-150 Pass

Perfluorooctane sulfonamide(FOSA) M17-Ma16230 NCP % 96 50-150 Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-Ma16230 NCP % 99 50-150 Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-Ma16230 NCP % 96 50-150 Pass

1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-Ma16230 NCP % 86 50-150 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-Ma16230 NCP % 81 50-150 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-Ma16230 NCP % 115 50-150 Pass


LimitsPass

LimitsQualifying

Code

Duplicate

Per- and Polyfluorinated Alkyl Substances (PFASs) - Trace Level Result 1 Result 2 RPD

Perfluorobutanesulfonic acid(PFBS) M17-Ma16230 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorobutanoic acid (PFBA) M17-Ma16230 NCP ug/L < 0.05 < 0.05 <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) M17-Ma16230 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) M17-Ma16230 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanesulfonic acid(PFDS) M17-Ma16230 NCP ug/L 0.02 < 0.01 200 30% Fail Q15

Perfluoropentanoic acid (PFPeA) M17-Ma16230 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanoic acid (PFHxA) M17-Ma16230 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanoic acid (PFHpA) M17-Ma16230 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanoic acid (PFOA) M17-Ma16230 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorononanoic acid (PFNA) M17-Ma16230 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanoic acid (PFDA) M17-Ma16230 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroundecanoic acid (PFUnA) M17-Ma16230 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorododecanoic acid (PFDoA) M17-Ma16230 NCP ug/L 0.02 < 0.01 200 30% Fail Q15

Perfluorotridecanoic acid (PFTrDA) M17-Ma16230 NCP ug/L 0.02 < 0.01 200 30% Fail Q15



ABN : 50 005 085 521 Telephone: +61 2 9900 8400

Page 7 of 9



LimitsPass

LimitsQualifying

Code

Duplicate

Per- and Polyfluorinated Alkyl Substances (PFASs) - Trace Level Result 1 Result 2 RPD

Perfluorotetradecanoic acid(PFTeDA) M17-Ma16230 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctane sulfonamide(FOSA) M17-Ma16230 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-Ma16230 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-Ma16230 NCP ug/L < 0.05 < 0.05 <1 30% Pass

1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-Ma16230 NCP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-Ma16230 NCP ug/L < 0.05 < 0.05 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-Ma16230 NCP ug/L < 0.01 < 0.01 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 2 9900 8400

Page 8 of 9


Comments

Sample IntegrityCustody Seals Intact (if used) N/A

Attempt to Chill was evident Yes

Sample correctly preserved Yes

Appropriate sample containers have been used Yes

Sample containers for volatile analysis received with minimal headspace Yes

Samples received within HoldingTime Yes

Some samples have been subcontracted No

Qualifier Codes/Comments

Code DescriptionN09 Quantification of linear and branched isomers has been conducted as a single total response using the relative response factor for the corresponding linear/branched standard.

N11

Isotope dilution is used for calibration of each native compound for which an exact labelled analogue is available (Isotope Dilution Quantitation). The isotopically labelledanalogues allow identification and recovery correction of the concentration of the associated native PFAS compounds. Where the native PFAS compound does not have labelledanalogue then the quantification is made using the Extracted Internal Standard Analyte with the closest retention time to the analyte and no recovery correction has been made(Internal Standard Quantitation).

Q15 The RPD reported passes Eurofins | mgt's QC - Acceptance Criteria as defined in the Internal Quality Control Review and Glossary page of this report.

Authorised By

Nibha Vaidya Analytical Services Manager

Jonathon Angell Senior Analyst-Organic (QLD)

Glenn Jackson

National Operations Manager

- Indicates Not Requested

* Indicates NATA accreditation does not cover the performance of this service

Measurement uncertainty of test data is available on request or please click here.Eurofins | mgt shall not be liable for loss, cost, damages or expenses incurred by the client, or any other person or company, resulting from the use of any information or interpretation given in this report. In no case shall Eurofins | mgt be liable for consequential damages including, but notlimited to, lost profits, damages for failure to meet deadlines and lost production arising from this report. This document shall not be reproduced except in full and relates only to the items tested. Unless indicated otherwise, the tests were performed on the samples as received.



ABN : 50 005 085 521 Telephone: +61 2 9900 8400

Page 9 of 9


http://www.eurofins.com.au/media/311687/reporting-measurement-uncertainty-of-chemical-and-microbiology-test-results.pdf

Certificate of Analysis

Golder Associates

124 Pacific Hwy

St. Leonards

NSW 1585

Attention: Andrew Holloway

Report 538644-S

Project name KAPOOKA

Project ID 1652034

Received Date Mar 20, 2017


0315_QC203_170315

0315_QC205_170315

0315_QC207_170315

Sample Matrix Soil Soil Soil Soil

Eurofins | mgt Sample No. S17-Ma21084 S17-Ma21085 S17-Ma21086 S17-Ma21087

Date Sampled Mar 14, 2017 Mar 15, 2017 Mar 15, 2017 Mar 15, 2017


Perfluoroalkyl carboxylic acids (PFCAs)

Perfluorobutanoic acid (PFBA) 5 ug/kg < 5 < 5 < 5 < 5

13C4-PFBA (surr.) 1 % 92 78 103 100

Perfluoropentanoic acid (PFPeA) 5 ug/kg < 5 < 5 < 5 < 5

13C5-PFPeA (surr.) 1 % 77 66 89 92

Perfluorohexanoic acid (PFHxA) 5 ug/kg < 5 < 5 < 5 < 5

13C5-PFHxA (surr.) 1 % 95 73 108 104

Perfluoroheptanoic acid (PFHpA) 5 ug/kg < 5 < 5 < 5 < 5

13C4-PFHpA (surr.) 1 % 92 68 108 99

Perfluorooctanoic acid (PFOA) 5 ug/kg < 5 < 5 < 5 < 5

13C8-PFOA (surr.) 1 % 87 71 99 91

Perfluorononanoic acid (PFNA) 5 ug/kg < 5 < 5 < 5 < 5

13C5-PFNA (surr.) 1 % 90 75 105 93

Perfluorodecanoic acid (PFDA) 5 ug/kg < 5 < 5 < 5 < 5

13C6-PFDA (surr.) 1 % 95 80 105 99

Perfluoroundecanoic acid (PFUnA) 5 ug/kg < 5 < 5 < 5 < 5

13C2-PFUnDA (surr.) 1 % 90 88 107 98

Perfluorododecanoic acid (PFDoA) 5 ug/kg < 5 < 5 < 5 < 5

13C2-PFDoDA (surr.) 1 % 97 90 111 97

Perfluorotridecanoic acid (PFTrDA) 5 ug/kg < 5 < 5 < 5 < 5

Perfluorotetradecanoic acid (PFTeDA) 5 ug/kg < 5 < 5 < 5 < 5

13C2-PFTeDA (surr.) 1 % 87 87 100 90

Perfluoroalkane sulfonamides (PFASAs)

Perfluorooctane sulfonamide (FOSA) 5 ug/kg < 5 < 5 < 5 < 5

13C8-FOSA (surr.) 1 % 78 83 91 79

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA) 5 ug/kg < 5 < 5 < 5 < 5

D3-N-MeFOSA (surr.) 1 % 73 84 93 78

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA) 5 ug/kg < 5 < 5 < 5 < 5

D5-N-EtFOSA (surr.) 1 % 66 89 93 81

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol(N-MeFOSE) 5 ug/kg < 5 < 5 < 5 < 5

D7-N-MeFOSE (surr.) 1 % 82 78 86 89

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE) 5 ug/kg < 5 < 5 < 5 < 5

D9-N-EtFOSE (surr.) 1 % 71 81 89 75

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA) 10 ug/kg < 10 < 10 < 10 < 10



ABN : 50 005 085 521 Telephone: +61 2 9900 8400

Page 1 of 11

Report Number: 538644-S

NATA AccreditedAccreditation Number 1261Site Number 18217

Accredited for compliance with ISO/IEC 17025 – TestingThe results of the tests, calibrations and/ormeasurements included in this document are traceableto Australian/national standards.


0315_QC203_170315

0315_QC205_170315

0315_QC207_170315

Sample Matrix Soil Soil Soil Soil

Eurofins | mgt Sample No. S17-Ma21084 S17-Ma21085 S17-Ma21086 S17-Ma21087

Date Sampled Mar 14, 2017 Mar 15, 2017 Mar 15, 2017 Mar 15, 2017



D5-N-EtFOSAA (surr.) 1 % 104 71 115 104

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA) 10 ug/kg < 10 < 10 < 10 < 10

D3-N-MeFOSAA (surr.) 1 % 108 67 116 114

Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs)

Perfluorobutanesulfonic acid (PFBS) 5 ug/kg < 5 < 5 < 5 < 5

13C3-PFBS (surr.) 1 % 97 91 109 102

Perfluoropentanesulfonic acid (PFPeS) 5 ug/kg < 5 < 5 < 5 < 5

Perfluorohexanesulfonic acid (PFHxS) 5 ug/kg < 5 < 5 < 5 < 5

18O2-PFHxS (surr.) 1 % 91 91 102 95

Perfluoroheptanesulfonic acid (PFHpS) 5 ug/kg < 5 < 5 < 5 < 5

Perfluorooctanesulfonic acid (PFOS)N11 5 ug/kg < 5 < 5 N09500 < 5

13C8-PFOS (surr.) 1 % 89 94 87 91

Perfluorodecanesulfonic acid (PFDS) 5 ug/kg < 5 < 5 < 5 < 5

n:2 Fluorotelomer sulfonic acids

1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2 FTS) 5 ug/kg < 5 < 5 < 5 < 5

13C2-4:2 FTS (surr.) 1 % 56 20 79 80

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) 10 ug/kg < 10 < 10 < 10 < 10

13C2-6:2 FTS (surr.) 1 % 54 23 66 62

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) 5 ug/kg < 5 < 5 < 5 < 5

13C2-8:2 FTS (surr.) 1 % 60 31 68 68

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2FTS) 5 ug/kg < 5 < 5 < 5 < 5

% Moisture 1 % 11 10.0 2.1 2.3



ABN : 50 005 085 521 Telephone: +61 2 9900 8400

Page 2 of 11


Sample HistoryWhere samples are submitted/analysed over several days, the last date of extraction and analysis is reported.A recent review of our LIMS has resulted in the correction or clarification of some method identifications. Due to this, some of the method reference information on reports has changed. However,no substantive change has been made to our laboratory methods, and as such there is no change in the validity of current or previous results (regarding both quality and NATA accreditation).

If the date and time of sampling are not provided, the Laboratory will not be responsible for compromised results should testing be performed outside the recommended holding time.

Description Testing Site Extracted Holding Time

Per- and Polyfluorinated Alkyl Substances (PFASs)

Perfluoroalkyl carboxylic acids (PFCAs) Brisbane Mar 21, 2017 180 Day


Perfluoroalkane sulfonamides (PFASAs) Brisbane Mar 21, 2017 180 Day


Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs) Brisbane Mar 21, 2017 180 Day


n:2 Fluorotelomer sulfonic acids Brisbane Mar 21, 2017 180 Day


% Moisture Brisbane Mar 20, 2017 14 Day

- Method: LTM-GEN-7080 Moisture



ABN : 50 005 085 521 Telephone: +61 2 9900 8400

Page 3 of 11






Sample Detail

Moisture S

et

Per- and P


ubstances(P

FA

Ss) - T

race Level

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0315_QC201_170314

Mar 14, 2017 Soil S17-Ma21084 X X

2 0315_QC203_170315

Mar 15, 2017 Soil S17-Ma21085 X X

3 0315_QC205_170315

Mar 15, 2017 Soil S17-Ma21086 X X

4 0315_QC207_170315

Mar 15, 2017 Soil S17-Ma21087 X X

5 0315_QC209_170315

Mar 15, 2017 Water S17-Ma21088 X

6 0315_QC210_ Mar 16, 2017 Water S17-Ma21089 X






Date Reported:Mar 31, 2017


ABN : 50 005 085 521 Telephone: +61 2 9900 8400

Page 4 of 11






Sample Detail

Moisture S

et

Per- and P


ubstances(P

FA

Ss) - T

race Level

Per- and P


ubstances(P

FA

Ss)





170316

Test Counts 4 2 4






Page 5 of 11


Internal Quality Control Review and Glossary

General

Holding Times

Units

Terms

QC - Acceptance Criteria

QC Data General Comments

1. Laboratory QC results for Method Blanks, Duplicates, Matrix Spikes, and Laboratory Control Samples are included in this QC report where applicable. Additional QC data may be available on

request.

2. All soil results are reported on a dry basis, unless otherwise stated.

3. Actual LORs are matrix dependant. Quoted LORs may be raised where sample extracts are diluted due to interferences.

4. Results are uncorrected for matrix spikes or surrogate recoveries.

5. SVOC analysis on waters are performed on homogenised, unfiltered samples, unless noted otherwise.

6. Samples were analysed on an 'as received' basis. 7. This report replaces any interim results previously issued.

Please refer to 'Sample Preservation and Container Guide' for holding times (QS3001).

For samples received on the last day of holding time, notification of testing requirements should have been received at least 6 hours prior to sample receipt deadlines as stated on the Sample

Receipt Advice.

If the Laboratory did not receive the information in the required timeframe, and regardless of any other integrity issues, suitably qualified results may still be reported.

Holding times apply from the date of sampling, therefore compliance to these may be outside the laboratory's control.

**NOTE: pH duplicates are reported as a range NOT as RPD

mg/kg: milligrams per Kilogram mg/l: milligrams per litre

ug/l: micrograms per litre ppm: Parts per million

ppb: Parts per billion %: Percentage

org/100ml: Organisms per 100 millilitres NTU: Nephelometric Turbidity Units

MPN/100mL: Most Probable Number of organisms per 100 millilitres

Dry Where a moisture has been determined on a solid sample the result is expressed on a dry basis.

LOR Limit of Reporting.

SPIKE Addition of the analyte to the sample and reported as percentage recovery.

RPD Relative Percent Difference between two Duplicate pieces of analysis.

LCS Laboratory Control Sample - reported as percent recovery

CRM Certified Reference Material - reported as percent recovery

Method Blank In the case of solid samples these are performed on laboratory certified clean sands.

In the case of water samples these are performed on de-ionised water.

Surr - Surrogate The addition of a like compound to the analyte target and reported as percentage recovery.

Duplicate A second piece of analysis from the same sample and reported in the same units as the result to show comparison.

Batch Duplicate A second piece of analysis from a sample outside of the clients batch of samples but run within the laboratory batch of analysis.

Batch SPIKE Spike recovery reported on a sample from outside of the clients batch of samples but run within the laboratory batch of analysis.

USEPA United States Environmental Protection Agency

APHA American Public Health Association

TCLP Toxicity Characteristic Leaching Procedure

COC Chain of Custody

SRA Sample Receipt Advice

CP Client Parent - QC was performed on samples pertaining to this report

NCP Non-Client Parent - QC performed on samples not pertaining to this report, QC is representative of the sequence or batch that client samples were analysed within

TEQ Toxic Equivalency Quotient

RPD Duplicates: Global RPD Duplicates Acceptance Criteria is 30% however the following acceptance guidelines are equally applicable:

Results <10 times the LOR : No Limit

Results between 10-20 times the LOR : RPD must lie between 0-50%

Results >20 times the LOR : RPD must lie between 0-30%

Surrogate Recoveries: Recoveries must lie between 50-150%-Phenols & PFASs 20-130%

1. Where a result is reported as a less than (<), higher than the nominated LOR, this is due to either matrix interference, extract dilution required due to interferences or contaminant levels within

the sample, high moisture content or insufficient sample provided.

2. Duplicate data shown within this report that states the word "BATCH" is a Batch Duplicate from outside of your sample batch, but within the laboratory sample batch at a 1:10 ratio. The Parent

and Duplicate data shown is not data from your samples.

3. Organochlorine Pesticide analysis - where reporting LCS data, Toxaphene & Chlordane are not added to the LCS.

4. Organochlorine Pesticide analysis - where reporting Spike data, Toxaphene is not added to the Spike.

5. Total Recoverable Hydrocarbons - where reporting Spike & LCS data, a single spike of commercial Hydrocarbon products in the range of C12-C30 is added and it's Total Recovery is reported

in the C10-C14 cell of the Report.

6. pH and Free Chlorine analysed in the laboratory - Analysis on this test must begin within 30 minutes of sampling.Therefore laboratory analysis is unlikely to be completed within holding time.

Analysis will begin as soon as possible after sample receipt.

7. Recovery Data (Spikes & Surrogates) - where chromatographic interference does not allow the determination of Recovery the term "INT" appears against that analyte.

8. Polychlorinated Biphenyls are spiked only using Aroclor 1260 in Matrix Spikes and LCS.

9. For Matrix Spikes and LCS results a dash " -" in the report means that the specific analyte was not added to the QC sample.

10. Duplicate RPDs are calculated from raw analytical data thus it is possible to have two sets of data.



ABN : 50 005 085 521 Telephone: +61 2 9900 8400

Page 6 of 11


Quality Control Results


PassLimits

QualifyingCode

Method Blank


Perfluorobutanoic acid (PFBA) ug/kg < 5 5 Pass

Perfluoropentanoic acid (PFPeA) ug/kg < 5 5 Pass

Perfluorohexanoic acid (PFHxA) ug/kg < 5 5 Pass

Perfluoroheptanoic acid (PFHpA) ug/kg < 5 5 Pass

Perfluorooctanoic acid (PFOA) ug/kg < 5 5 Pass

Perfluorononanoic acid (PFNA) ug/kg < 5 5 Pass

Perfluorodecanoic acid (PFDA) ug/kg < 5 5 Pass

Perfluoroundecanoic acid (PFUnA) ug/kg < 5 5 Pass

Perfluorododecanoic acid (PFDoA) ug/kg < 5 5 Pass

Perfluorotridecanoic acid (PFTrDA) ug/kg < 5 5 Pass

Perfluorotetradecanoic acid (PFTeDA) ug/kg < 5 5 Pass

Method Blank


Perfluorooctane sulfonamide (FOSA) ug/kg < 5 5 Pass

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA) ug/kg < 5 5 Pass

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA) ug/kg < 5 5 Pass

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol (N-MeFOSE) ug/kg < 5 5 Pass

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE) ug/kg < 5 5 Pass

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA) ug/kg < 10 10 Pass

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA) ug/kg < 10 10 Pass

Method Blank


Perfluorobutanesulfonic acid (PFBS) ug/kg < 5 5 Pass

Perfluoropentanesulfonic acid (PFPeS) ug/kg < 5 5 Pass

Perfluorohexanesulfonic acid (PFHxS) ug/kg < 5 5 Pass

Perfluoroheptanesulfonic acid (PFHpS) ug/kg < 5 5 Pass

Perfluorooctanesulfonic acid (PFOS) ug/kg < 5 5 Pass

Perfluorodecanesulfonic acid (PFDS) ug/kg < 5 5 Pass

Method Blank


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2 FTS) ug/kg < 5 5 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) ug/kg < 10 10 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) ug/kg < 5 5 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2 FTS) ug/kg < 5 5 Pass

LCS - % Recovery


Perfluorobutanoic acid (PFBA) % 94 50-150 Pass

Perfluoropentanoic acid (PFPeA) % 109 50-150 Pass

Perfluorohexanoic acid (PFHxA) % 98 50-150 Pass

Perfluoroheptanoic acid (PFHpA) % 99 50-150 Pass

Perfluorooctanoic acid (PFOA) % 96 50-150 Pass

Perfluorononanoic acid (PFNA) % 101 50-150 Pass

Perfluorodecanoic acid (PFDA) % 101 50-150 Pass

Perfluoroundecanoic acid (PFUnA) % 96 50-150 Pass

Perfluorododecanoic acid (PFDoA) % 105 50-150 Pass

Perfluorotridecanoic acid (PFTrDA) % 108 50-150 Pass

Perfluorotetradecanoic acid (PFTeDA) % 106 50-150 Pass

LCS - % Recovery




ABN : 50 005 085 521 Telephone: +61 2 9900 8400

Page 7 of 11



PassLimits

QualifyingCode

Perfluorooctane sulfonamide (FOSA) % 98 50-150 Pass

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA) % 111 50-150 Pass

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA) % 129 50-150 Pass

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol (N-MeFOSE) % 85 50-150 Pass

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE) % 104 50-150 Pass

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA) % 102 50-150 Pass

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA) % 99 50-150 Pass

LCS - % Recovery


Perfluorobutanesulfonic acid (PFBS) % 97 50-150 Pass

Perfluoropentanesulfonic acid (PFPeS) % 95 50-150 Pass

Perfluorohexanesulfonic acid (PFHxS) % 95 50-150 Pass

Perfluoroheptanesulfonic acid (PFHpS) % 98 50-150 Pass

Perfluorooctanesulfonic acid (PFOS) % 94 50-150 Pass

Perfluorodecanesulfonic acid (PFDS) % 107 50-150 Pass

LCS - % Recovery


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2 FTS) % 107 50-150 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) % 142 50-150 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) % 137 50-150 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2 FTS) % 101 50-150 Pass


LimitsPass

LimitsQualifying

Code

Spike - % Recovery

Perfluoroalkyl carboxylic acids (PFCAs) Result 1

Perfluorobutanoic acid (PFBA) M17-Ma19364 NCP % 93 50-150 Pass

Perfluoropentanoic acid (PFPeA) M17-Ma19364 NCP % 106 50-150 Pass

Perfluorohexanoic acid (PFHxA) M17-Ma19364 NCP % 97 50-150 Pass

Perfluoroheptanoic acid (PFHpA) M17-Ma19364 NCP % 96 50-150 Pass

Perfluorooctanoic acid (PFOA) M17-Ma19364 NCP % 98 50-150 Pass

Perfluorononanoic acid (PFNA) M17-Ma19364 NCP % 99 50-150 Pass

Perfluorodecanoic acid (PFDA) M17-Ma19364 NCP % 97 50-150 Pass

Perfluoroundecanoic acid (PFUnA) M17-Ma19364 NCP % 94 50-150 Pass

Perfluorododecanoic acid (PFDoA) M17-Ma19364 NCP % 100 50-150 Pass

Perfluorotridecanoic acid (PFTrDA) M17-Ma19364 NCP % 66 50-150 Pass

Perfluorotetradecanoic acid(PFTeDA) M17-Ma19364 NCP % 102 50-150 Pass

Spike - % Recovery

Perfluoroalkane sulfonamides (PFASAs) Result 1

Perfluorooctane sulfonamide(FOSA) M17-Ma19364 NCP % 99 50-150 Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) M17-Ma19364 NCP % 114 50-150 Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) M17-Ma19364 NCP % 129 50-150 Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) M17-Ma19364 NCP % 101 50-150 Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) M17-Ma19364 NCP % 80 50-150 Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-Ma19364 NCP % 123 50-150 Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-Ma19364 NCP % 130 50-150 Pass

Spike - % Recovery

Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs) Result 1



ABN : 50 005 085 521 Telephone: +61 2 9900 8400

Page 8 of 11



LimitsPass

LimitsQualifying

Code

Perfluorobutanesulfonic acid(PFBS) M17-Ma19364 NCP % 97 50-150 Pass

Perfluoropentanesulfonic acid(PFPeS) M17-Ma19364 NCP % 95 50-150 Pass

Perfluorohexanesulfonic acid(PFHxS) M17-Ma19364 NCP % 93 50-150 Pass

Perfluoroheptanesulfonic acid(PFHpS) M17-Ma19364 NCP % 97 50-150 Pass

Perfluorooctanesulfonic acid(PFOS) M17-Ma19364 NCP % 93 50-150 Pass

Perfluorodecanesulfonic acid(PFDS) M17-Ma19364 NCP % 87 50-150 Pass

Spike - % Recovery

n:2 Fluorotelomer sulfonic acids Result 1

1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-Ma19364 NCP % 106 50-150 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-Ma19364 NCP % 140 50-150 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-Ma19364 NCP % 134 50-150 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) M17-Ma19364 NCP % 135 50-150 Pass


LimitsPass

LimitsQualifying

Code

Duplicate

Perfluoroalkyl carboxylic acids (PFCAs) Result 1 Result 2 RPD

Perfluorobutanoic acid (PFBA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass

Perfluoropentanoic acid (PFPeA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass

Perfluorohexanoic acid (PFHxA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass

Perfluoroheptanoic acid (PFHpA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass

Perfluorooctanoic acid (PFOA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass

Perfluorononanoic acid (PFNA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass

Perfluorodecanoic acid (PFDA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass

Perfluoroundecanoic acid (PFUnA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass

Perfluorododecanoic acid (PFDoA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass

Duplicate

Perfluoroalkane sulfonamides (PFASAs) Result 1 Result 2 RPD

Perfluorooctane sulfonamide(FOSA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) B17-Ma20923 NCP ug/kg < 10 < 10 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) B17-Ma20923 NCP ug/kg < 10 < 10 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 2 9900 8400

Page 9 of 11


Duplicate

Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs) Result 1 Result 2 RPD

Perfluorobutanesulfonic acid(PFBS) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass

Perfluoropentanesulfonic acid(PFPeS) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass

Perfluorodecanesulfonic acid(PFDS) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass

Duplicate

n:2 Fluorotelomer sulfonic acids Result 1 Result 2 RPD

1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) B17-Ma20923 NCP ug/kg < 10 < 10 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass

Duplicate

Result 1 Result 2 RPD

% Moisture S17-Ma09089 NCP % 25 28 9.0 30% Pass



ABN : 50 005 085 521 Telephone: +61 2 9900 8400

Page 10 of 11


Comments

Sample IntegrityCustody Seals Intact (if used) N/A

Attempt to Chill was evident Yes

Sample correctly preserved Yes

Appropriate sample containers have been used Yes

Sample containers for volatile analysis received with minimal headspace Yes

Samples received within HoldingTime Yes

Some samples have been subcontracted No

Qualifier Codes/Comments

Code DescriptionN09 Quantification of linear and branched isomers has been conducted as a single total response using the relative response factor for the corresponding linear/branched standard.

N11

Isotope dilution is used for calibration of each native compound for which an exact labelled analogue is available (Isotope Dilution Quantitation). The isotopically labelledanalogues allow identification and recovery correction of the concentration of the associated native PFAS compounds. Where the native PFAS compound does not have labelledanalogue then the quantification is made using the Extracted Internal Standard Analyte with the closest retention time to the analyte and no recovery correction has been made(Internal Standard Quantitation).

Authorised By

Nibha Vaidya Analytical Services Manager

Bryan Wilson Senior Analyst-Metal (QLD)

Jonathon Angell Senior Analyst-Inorganic (QLD)

Jonathon Angell Senior Analyst-Organic (QLD)

Glenn Jackson

National Operations Manager

- Indicates Not Requested

* Indicates NATA accreditation does not cover the performance of this service

Measurement uncertainty of test data is available on request or please click here.Eurofins | mgt shall not be liable for loss, cost, damages or expenses incurred by the client, or any other person or company, resulting from the use of any information or interpretation given in this report. In no case shall Eurofins | mgt be liable for consequential damages including, but notlimited to, lost profits, damages for failure to meet deadlines and lost production arising from this report. This document shall not be reproduced except in full and relates only to the items tested. Unless indicated otherwise, the tests were performed on the samples as received.



ABN : 50 005 085 521 Telephone: +61 2 9900 8400

Page 11 of 11


http://www.eurofins.com.au/media/311687/reporting-measurement-uncertainty-of-chemical-and-microbiology-test-results.pdf





Sample Detail

Moisture S

et

Per- and P


ubstances(P

FA

Ss) - T

race Level

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0315_QC201_170314

Mar 14, 2017 Soil S17-Ma21084 X X

2 0315_QC203_170315

Mar 15, 2017 Soil S17-Ma21085 X X

3 0315_QC205_170315

Mar 15, 2017 Soil S17-Ma21086 X X

4 0315_QC207_170315

Mar 15, 2017 Soil S17-Ma21087 X X

5 0315_QC209_170315

Mar 15, 2017 Water S17-Ma21088 X

6 0315_QC210_ Mar 16, 2017 Water S17-Ma21089 X










Sample Detail

Moisture S

et

Per- and P


ubstances(P

FA

Ss) - T

race Level

Per- and P


ubstances(P

FA

Ss)





170316

Test Counts 4 2 4






ABN – 50 005 085 521 e.mail : [email protected] web : www.eurofins.com.au

MelbourneMelbourneMelbourneMelbourne3-5 Kingston Town CloseOakleigh Vic 3166Phone : +61 3 8564 5000NATA # 1261Site # 1254 & 14271



PerthPerthPerthPerth2/91 Leach HighwayKewdale WA 6105Phone : +61 8 9251 9600NATA # 1261 Site # 18217

Environmental LaboratoryAir AnalysisWater AnalysisSoil Contamination Analysis

NATA AccreditationStack Emission Sampling & AnalysisTrade Waste Sampling & AnalysisGroundwater Sampling & Analysis

38 Years of Environmental Analysis & Experience38 Years of Environmental Analysis & Experience38 Years of Environmental Analysis & Experience38 Years of Environmental Analysis & Experience

Sample Receipt AdviceSample Receipt AdviceSample Receipt AdviceSample Receipt Advice

Company name: Golder Associates Pty Ltd (Syd)Golder Associates Pty Ltd (Syd)Golder Associates Pty Ltd (Syd)Golder Associates Pty Ltd (Syd)

Contact name: Andrew HollowayProject name: KAPOOKAProject ID: 1652034COC number: Not providedTurn around time: 5 DayDate/Time received: Mar 20, 2017 11:06 AMEurofins | mgt reference: 538644538644538644538644

Sample informationSample informationSample informationSample information

☑ A detailed list of analytes logged into our LIMS, is included in the attached summary table.

☑ Sample Temperature of a random sample selected from the batch as recorded by Eurofins | mgtSample Receipt : 24.5 degrees Celsius.

☑ All samples have been received as described on the above COC.

☑ COC has been completed correctly.

☑ Attempt to chill was evident.

☑ Appropriately preserved sample containers have been used.

☑ All samples were received in good condition.

☑ Samples have been provided with adequate time to commence analysis in accordance with therelevant holding times.

☑ Appropriate sample containers have been used.

☑ Sample containers for volatile analysis received with zero headspace.

☒ Some samples have been subcontracted.

N/A Custody Seals intact (if used).

Contact notesContact notesContact notesContact notes

If you have any questions with respect to these samples please contact:

Nibha Vaidya on Phone : +61 (2) 9900 8400 or by e.mail: [email protected]

Results will be delivered electronically via e.mail to Andrew Holloway - [email protected].

Note: A copy of these results will also be delivered to the general Golder Associates Pty Ltd (Syd) email address.


APPENDIX I Calibration Certificates



APPENDIX J Report Limitations


IMPORTANT INFORMATION RELATING TO THIS REPORT

The document (“Report”) to which this page is attached and which this page forms a part of, has been issued by Golder Associates Pty Ltd (“Golder”) subject to the important limitations and other qualifications set out below.

This Report constitutes or is part of services (“Services”) provided by Golder to its client (“Client”) under and subject to a contract between Golder and its Client (“Contract”). The contents of this page are not intended to and do not alter Golder’s obligations (including any limits on those obligations) to its Client under the Contract.

This Report is provided for use solely by Golder’s Client and persons acting on the Client’s behalf, such as its professional advisers. Golder is responsible only to its Client for this Report. Golder has no responsibility to any other person who relies or makes decisions based upon this Report or who makes any other use of this Report. Golder accepts no responsibility for any loss or damage suffered by any person other than its Client as a result of any reliance upon any part of this Report, decisions made based upon this Report or any other use of it.

This Report has been prepared in the context of the circumstances and purposes referred to in, or derived from, the Contract and Golder accepts no responsibility for use of the Report, in whole or in part, in any other context or circumstance or for any other purpose.

The scope of Golder’s Services and the period of time they relate to are determined by the Contract and are subject to restrictions and limitations set out in the Contract. If a service or other work is not expressly referred to in this Report, do not assume that it has been provided or performed. If a matter is not addressed in this Report, do not assume that any determination has been made by Golder in regards to it.

At any location relevant to the Services conditions may exist which were not detected by Golder, in particular due to the specific scope of the investigation Golder has been engaged to undertake. Conditions can only be verified at the exact location of any tests undertaken. Variations in conditions may occur between tested locations and there may be conditions which have not been revealed by the investigation and which have not therefore been taken into account in this Report.

Golder accepts no responsibility for and makes no representation as to the accuracy or completeness of the information provided to it by or on behalf of the Client or sourced from any third party. Golder has assumed that such information is correct unless otherwise stated and no responsibility is accepted by Golder for incomplete or inaccurate data supplied by its Client or any other person for whom Golder is not responsible. Golder has not taken account of matters that may have existed when the Report was prepared but which were only later disclosed to Golder.

Having regard to the matters referred to in the previous paragraphs on this page in particular, carrying out the Services has allowed Golder to form no more than an opinion as to the actual conditions at any relevant location. That opinion is necessarily constrained by the extent of the information collected by Golder or otherwise made available to Golder. Further, the passage of time may affect the accuracy, applicability or usefulness of the opinions, assessments or other information in this Report. This Report is based upon the information and other circumstances that existed and were known to Golder when the Services were performed and this Report was prepared. Golder has not considered the effect of any possible future developments including physical changes to any relevant location or changes to any laws or regulations relevant to such location.

Where permitted by the Contract, Golder may have retained subconsultants affiliated with Golder to provide some or all of the Services. However, it is Golder which remains solely responsible for the Services and there is no legal recourse against any of Golder’s affiliated companies or the employees, officers or directors of any of them.

By date, or revision, the Report supersedes any prior report or other document issued by Golder dealing with any matter that is addressed in the Report.

Any uncertainty as to the extent to which this Report can be used or relied upon in any respect should be referred to Golder for clarification.

GAP Form No. LEG04RL2July 2015 1/1

Golder Associates Pty Ltd 124 Pacific Highway St. Leonards, New South Wales 2065 Australia T: +61 2 9478 3900

APPENDIX D - Department of Defence...Geologists Log Drillers Log From (m) To (m) Thickness (m)...

Documents

Transcript of APPENDIX D - Department of Defence...Geologists Log Drillers Log From (m) To (m) Thickness (m)...