Analytical Test Report Wifi OG - Amazon S3 · 2017-12-13 · 11119 SE Division St. Portland, OR...

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11119 SE Division St. Portland, OR 97266 (503) 307-0096 ORELAP #4096 OLCC #1002112892C Science First. Analytical Test Report Wifi OG Gardens of Odin Laboratory ID: 1710112-05 Metrc Tag: 1A401030000DF71000000583 Date Printed: 11/7/17 Date Sampled: 10/28/17 020-1003851CB2B Batch ID: 0575 Potency Analysis Analytical Method: De Backer, Journal of Chromatography b.2009. 11.004 - SOP 19 & 20 Cannabinoids (% weight) Moisture Adjusted Notes 20.9 24.8 THCA < LOQ < LOQ delta 9-THC 1.43 1.70 CBGA < LOQ < LOQ CBDA 0.358 0.424 CBD < LOQ < LOQ CBN < LOQ < LOQ CBG < LOQ < LOQ CBC Total THC 21.8 % Total CBD 0.424 % Moisture Analysis Method/SOP: SOP 7 Moisture: 15.6 % Water Activity Analysis Method/SOP: SOP 8 Results above 0.65 fail state testing requirements and will be highlighted Red. Water Activity: 0.568 PASS Sample tested in compliance with OAR 333-007 (TNI standards). Lab accredited for CBDA, THCA, CBD, THC, and sampling. These results relate only to the sample included on this report. The report may not be reproduced except in full, without the written permission of Rose City Labs. Chris Nielsen, Lab Director 11/7/2017 Page 1 of 4

Transcript of Analytical Test Report Wifi OG - Amazon S3 · 2017-12-13 · 11119 SE Division St. Portland, OR...

Page 1: Analytical Test Report Wifi OG - Amazon S3 · 2017-12-13 · 11119 SE Division St. Portland, OR 97266 (503) 307-0096 ORELAP #4096 OLCC #1002112892C Science First. Analytical Test

11119 SE Division St.

Portland, OR 97266

(503) 307-0096ORELAP #4096

OLCC #1002112892C Science First.

Analytical Test Report

Wifi OGGardens of Odin

Laboratory ID: 1710112-05

Metrc Tag: 1A401030000DF71000000583

Date Printed: 11/7/17

Date Sampled: 10/28/17

020-1003851CB2B

Batch ID: 0575

Potency Analysis

Analytical Method: De Backer, Journal of Chromatography b.2009. 11.004 -

SOP 19 & 20

Cannabinoids (% weight) Moisture Adjusted Notes

20.9 24.8THCA

< LOQ < LOQdelta 9-THC

1.43 1.70CBGA

< LOQ < LOQCBDA

0.358 0.424CBD

< LOQ < LOQCBN

< LOQ < LOQCBG

< LOQ < LOQCBC

Total THC

21.8 %

Total CBD

0.424 %

MoistureAnalysis Method/SOP: SOP 7

Moisture: 15.6 %

Water Activity

Analysis Method/SOP: SOP 8 Results above 0.65 fail state testing requirements and will be highlighted Red.

Water Activity: 0.568 PASS

Sample tested in compliance with OAR 333-007 (TNI standards). Lab accredited for CBDA, THCA, CBD, THC, and sampling. These results relate only to the

sample included on this report. The report may not be reproduced except in full, without the written permission of Rose City Labs.

Chris Nielsen, Lab Director 11/7/2017Page 1 of 4

Page 2: Analytical Test Report Wifi OG - Amazon S3 · 2017-12-13 · 11119 SE Division St. Portland, OR 97266 (503) 307-0096 ORELAP #4096 OLCC #1002112892C Science First. Analytical Test

11119 SE Division St.

Portland, OR 97266

(503) 307-0096ORELAP #4096

OLCC #1002112892C Science First.

Analytical Test Report

Laboratory ID: 1710112-05

Gardens of Odin

Wifi OG

020-1003851CB2B

Terpene Analysis

Analysis Method/SOP: Terp

Analyte Result ug/g

alpha-Bisabolol < LOQ

Camphene 101.4

delta-3-Carene < LOQ

beta-Caryophyllene 538.3

Caryophyllene Oxide < LOQ

p-Cymene < LOQ

Eucalyptol < LOQ

Geraniol < LOQ

Guaiol < LOQ

alpha-Humulene 129.2

Isopulegol < LOQ

Limonene 2252

Linalool 540.3

beta-Myrcene 1552

Ocimene < LOQ

alpha-Pinene 374.3

beta-Pinene 622.0

gamma-Terpinene < LOQ

alpha-Terpinene < LOQ

Terpinolene 25.74

cis-Nerolidol < LOQ

Total Terpenes 6151

Sample tested in compliance with OAR 333-007 (TNI standards). Lab accredited for CBDA, THCA, CBD, THC, and sampling. These results relate only to the

sample included on this report. The report may not be reproduced except in full, without the written permission of Rose City Labs.

Chris Nielsen, Lab Director 11/7/2017Page 2 of 4

Page 3: Analytical Test Report Wifi OG - Amazon S3 · 2017-12-13 · 11119 SE Division St. Portland, OR 97266 (503) 307-0096 ORELAP #4096 OLCC #1002112892C Science First. Analytical Test

11119 SE Division St.

Portland, OR 97266

(503) 307-0096ORELAP #4096

OLCC #1002112892C Science First.

Analytical Test Report

Laboratory ID: 1710112-05

Gardens of Odin

Wifi OG

020-1003851CB2B

Quality Control

Potency

Batch: B17J155 - Potency

Blank(B17J155-BLK1)

Result LOQ Units Analyte Extracted Analyzed%Recovery Limits Notes

THCA 10/31/17 16:28 11/01/17 06:52< LOQ 0.0600 %

delta 9-THC 10/31/17 16:28 11/01/17 06:52< LOQ 0.0600 %

CBGA 10/31/17 16:28 11/01/17 06:52< LOQ 0.0600 %

CBDA 10/31/17 16:28 11/01/17 06:52< LOQ 0.0600 %

CBD 10/31/17 16:28 11/01/17 06:52< LOQ 0.0600 %

CBN 10/31/17 16:28 11/01/17 06:52< LOQ 0.0600 %

CBG 10/31/17 16:28 11/01/17 06:52< LOQ 0.0600 %

CBC 10/31/17 16:28 11/01/17 06:52< LOQ 0.0600 %

LCS(B17J155-BS1)

% Recovery LOQ Units Analyte Extracted Analyzed%Recovery Limits Notes

THCA 10/31/17 16:28 11/01/17 06:34110 0.0600 % 80-120

delta 9-THC 10/31/17 16:28 11/01/17 06:34111 0.0600 % 80-120

CBDA 10/31/17 16:28 11/01/17 06:3485.8 0.0600 % 80-120

CBD 10/31/17 16:28 11/01/17 06:34116 0.0600 % 80-120

Moisture Content

Batch: B17J146 - Grav

Blank(B17J146-BLK1)

Result LOQ Units Analyte Extracted Analyzed%Recovery Limits Notes

Percent Moisture 10/30/17 17:40 10/30/17 17:400.00800 0.00 %

Batch: B17J147 - WA

Blank(B17J147-BLK1)

Result LOQ Units Analyte Extracted Analyzed%Recovery Limits Notes

Water Activity 10/31/17 09:14 10/31/17 09:14< LOQ 0.328 AW

Sample tested in compliance with OAR 333-007 (TNI standards). Lab accredited for CBDA, THCA, CBD, THC, and sampling. These results relate only to the

sample included on this report. The report may not be reproduced except in full, without the written permission of Rose City Labs.

Chris Nielsen, Lab Director 11/7/2017Page 3 of 4

Page 4: Analytical Test Report Wifi OG - Amazon S3 · 2017-12-13 · 11119 SE Division St. Portland, OR 97266 (503) 307-0096 ORELAP #4096 OLCC #1002112892C Science First. Analytical Test

11119 SE Division St.

Portland, OR 97266

(503) 307-0096ORELAP #4096

OLCC #1002112892C Science First.

Analytical Test Report

Laboratory ID: 1710112-05

Gardens of Odin

Wifi OG

020-1003851CB2B

Notes and Definitions

B Analyte detected in method blank, but not associated samples.

B2 Analyte detected in sample and associate methold blank.

C Interference due to co-elution.

D Initial result exceeded calibration range, reported data are based on analysis of a dilution.

H Non-homogenous samle matrix affecting RPD and/or QC.

I Manual Integration was performed.

L Duplicate sample relative precent difference (RPD) exceeds QC limits.

M Anomalous results due to matrix interference

P Peaks manually split.

Q1 QC out of limits but still oK

Q2 Quality Control outside QC limits. Data considered estimate.

Q3 CCV was above the acceptance criteria. Non-detect samples are considered acceptable.

Q4 CCV was below the acceptance criteria, however the sample still exceeds the regulatory limit.

R Marginal Exceedence.

U Reported result is an estimate. The analyte was detected above the calibration range.

X Problems with initial analysis, reported data are from reinjection of prepared sample.

<LOQ - Results below the Limit of Quantitation - Compound not detected

Sample tested in compliance with OAR 333-007 (TNI standards). Lab accredited for CBDA, THCA, CBD, THC, and sampling. These results relate only to the

sample included on this report. The report may not be reproduced except in full, without the written permission of Rose City Labs.

Chris Nielsen, Lab Director 11/7/2017Page 4 of 4

Page 5: Analytical Test Report Wifi OG - Amazon S3 · 2017-12-13 · 11119 SE Division St. Portland, OR 97266 (503) 307-0096 ORELAP #4096 OLCC #1002112892C Science First. Analytical Test

12423 NE Whitaker WayPortland, OR 97230

503-254-1794

Job Number:

Report Date:

ORELAP#:

11/07/2017

OR100028

12:00Received: 10/31/17

17-002217

Purchase Order:Purchase Order:

Report#: 029736-00

Product identity:

Customer:

1710112-02+05 Odin 103017 Composite B

10/28/17Sample Date:

17-002217-0002Laboratory ID:

Client/Metrc ID: 1A401030000620E000001�76

Rose City Labs11119 SE Division St.Portland Oregon 97266United States

SubcontractGrower:

Daniel HusonRelinquished by:

13.4 °CTemp:

12.80 gWeight Received:

Sample Results

Pesticides Batch 1702223Method AOAC 2007.01 & EN 15662 (mod) Units mg/kg Analyze 11/7/17 12:00:00

LOQAnalyte Result Limits Status Notes LOQAnalyte Result Limits Status Notes

Abamectin < LOQ 0.50 0.30 pass Acephate < LOQ 0.40 0.20 pass

Acequinocyl < LOQ 2.00 1.0 pass Acetamiprid < LOQ 0.20 0.10 pass

Aldicarb < LOQ 0.40 0.20 pass Azoxystrobin < LOQ 0.20 0.10 pass

Cyfluthrin (incl. Beta-Cyfl < LOQ 1.00 1.0 pass Bifenazate < LOQ 0.20 0.10 pass

Bifenthrin < LOQ 0.20 0.10 pass Boscalid < LOQ 0.40 0.10 pass

Carbaryl < LOQ 0.20 0.10 pass Carbofuran < LOQ 0.20 0.10 pass

Chlorantraniliprole < LOQ 0.20 0.10 pass Chlorfenapyr < LOQ 1.00 1.0 pass

Chlorpyrifos < LOQ 0.20 0.10 pass Clofentezine < LOQ 0.20 0.10 pass

Cypermethrin < LOQ 1.00 1.0 pass Daminozide < LOQ 1.00 1.0 pass

Diazinon < LOQ 0.20 0.10 pass Dichlorvos < LOQ 1.00 0.50 pass

Dimethoate < LOQ 0.20 0.10 pass Ethoprophos < LOQ 0.20 0.10 pass

Etofenprox < LOQ 0.40 0.10 pass Etoxazole < LOQ 0.20 0.10 pass

Fenoxycarb < LOQ 0.20 0.10 pass Fenpyroximate < LOQ 0.40 0.10 pass

Fipronil < LOQ 0.40 0.10 pass Flonicamid < LOQ 1.00 0.40 pass

Fludioxonil < LOQ 0.40 0.10 pass Hexythiazox < LOQ 1.00 0.40 pass

Imazalil < LOQ 0.20 0.10 pass Imidacloprid < LOQ 0.40 0.20 pass

Kresoxim-methyl < LOQ 0.40 0.10 pass Malathion < LOQ 0.20 0.10 pass

Metalaxyl < LOQ 0.20 0.10 pass Methiocarb < LOQ 0.20 0.10 pass

Methomyl < LOQ 0.40 0.20 pass Parathion-Methyl < LOQ 0.20 0.20 pass

MGK-264 < LOQ 0.20 0.10 pass Myclobutanil < LOQ 0.20 0.10 pass

Naled < LOQ 0.50 0.20 pass Oxamyl < LOQ 1.00 0.40 pass

Paclobutrazole < LOQ 0.40 0.20 pass Permethrin < LOQ 0.20 0.10 pass

Phosmet < LOQ 0.20 0.10 pass Piperonyl butoxide < LOQ 2.00 1.0 pass

Page 1 of 8Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unlessotherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be kept a maximum of 15 days from the report date unless priorarrangements have been made.

Testing in accordance with: OAR 333-007-0400

Page 6: Analytical Test Report Wifi OG - Amazon S3 · 2017-12-13 · 11119 SE Division St. Portland, OR 97266 (503) 307-0096 ORELAP #4096 OLCC #1002112892C Science First. Analytical Test

12423 NE Whitaker WayPortland, OR 97230

503-254-1794

Job Number:

Report Date:

ORELAP#:

11/07/2017

OR100028

12:00Received: 10/31/17

17-002217

Purchase Order:Purchase Order:

Report#: 029736-00

Pesticides Batch 1702223Method AOAC 2007.01 & EN 15662 (mod) Units mg/kg Analyze 11/7/17 12:00:00

LOQAnalyte Result Limits Status Notes LOQAnalyte Result Limits Status Notes

Prallethrin < LOQ 0.20 0.20 pass Propiconazole < LOQ 0.40 0.20 pass

Propoxur < LOQ 0.20 0.10 pass Pyrethrins < LOQ 1.00 0.50 pass

Pyridaben < LOQ 0.20 0.10 pass Spinosad < LOQ 0.20 0.10 pass

Spiromesifen < LOQ 0.20 0.10 pass Spirotetramat < LOQ 0.20 0.10 pass

Spiroxamine < LOQ 0.40 0.10 pass Tebuconazole < LOQ 0.40 0.20 pass

Thiacloprid < LOQ 0.20 0.10 pass Thiamethoxam < LOQ 0.20 0.10 pass

Trifloxystrobin < LOQ 0.20 0.10 pass

Page 2 of 8Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unlessotherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be kept a maximum of 15 days from the report date unless priorarrangements have been made.

Testing in accordance with: OAR 333-007-0400

Page 7: Analytical Test Report Wifi OG - Amazon S3 · 2017-12-13 · 11119 SE Division St. Portland, OR 97266 (503) 307-0096 ORELAP #4096 OLCC #1002112892C Science First. Analytical Test

12423 NE Whitaker WayPortland, OR 97230

503-254-1794

Job Number:

Report Date:

ORELAP#:

11/07/2017

OR100028

12:00Received: 10/31/17

17-002217

Purchase Order:Purchase Order:

Report#: 029736-00

AbbreviationsLimits: Action Levels per OAR-333-007-0400, OAR-333-007-0210, OAR-333-007-0220Limit(s) of Quantitation (LOQ): The minimum levels, concentrations, or quantities of a target variable (e.g., target analyte) that can be

reported with a specified degree of confidence.

Units of Measure

g = Gram

mg/kg = Milligram per kilogram

% wt = µg/g divided by 10,000

Derrick TannerGeneral Manager

Approved Signatory

Page 3 of 8Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unlessotherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be kept a maximum of 15 days from the report date unless priorarrangements have been made.

Testing in accordance with: OAR 333-007-0400

Page 8: Analytical Test Report Wifi OG - Amazon S3 · 2017-12-13 · 11119 SE Division St. Portland, OR 97266 (503) 307-0096 ORELAP #4096 OLCC #1002112892C Science First. Analytical Test

12423 NE Whitaker WayPortland, OR 97230

503-254-1794

Job Number:

Report Date:

ORELAP#:

11/07/2017

OR100028

12:00Received: 10/31/17

17-002217

Purchase Order:Purchase Order:

Report#: 029736-00

Page 4 of 8Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unlessotherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be kept a maximum of 15 days from the report date unless priorarrangements have been made.

Testing in accordance with: OAR 333-007-0400

Page 9: Analytical Test Report Wifi OG - Amazon S3 · 2017-12-13 · 11119 SE Division St. Portland, OR 97266 (503) 307-0096 ORELAP #4096 OLCC #1002112892C Science First. Analytical Test

12423 NE Whitaker WayPortland, OR 97230

503-254-1794

Job Number:

Report Date:

ORELAP#:

11/07/2017

OR100028

12:00Received: 10/31/17

17-002217

Purchase Order:Purchase Order:

Report#: 029736-00

Page 5 of 8Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unlessotherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be kept a maximum of 15 days from the report date unless priorarrangements have been made.

Testing in accordance with: OAR 333-007-0400

Page 10: Analytical Test Report Wifi OG - Amazon S3 · 2017-12-13 · 11119 SE Division St. Portland, OR 97266 (503) 307-0096 ORELAP #4096 OLCC #1002112892C Science First. Analytical Test

12423 NE Whitaker WayPortland, OR 97230

503-254-1794

Job Number:

Report Date:

ORELAP#:

11/07/2017

OR100028

12:00Received: 10/31/17

17-002217

Purchase Order:Purchase Order:

Report#: 029736-00

Page 6 of 8Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unlessotherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be kept a maximum of 15 days from the report date unless priorarrangements have been made.

Testing in accordance with: OAR 333-007-0400

Page 11: Analytical Test Report Wifi OG - Amazon S3 · 2017-12-13 · 11119 SE Division St. Portland, OR 97266 (503) 307-0096 ORELAP #4096 OLCC #1002112892C Science First. Analytical Test

12423 NE Whitaker WayPortland, OR 97230

503-254-1794

Job Number:

Report Date:

ORELAP#:

11/07/2017

OR100028

12:00Received: 10/31/17

17-002217

Purchase Order:Purchase Order:

Report#: 029736-00

Page 7 of 8Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unlessotherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be kept a maximum of 15 days from the report date unless priorarrangements have been made.

Testing in accordance with: OAR 333-007-0400

Page 12: Analytical Test Report Wifi OG - Amazon S3 · 2017-12-13 · 11119 SE Division St. Portland, OR 97266 (503) 307-0096 ORELAP #4096 OLCC #1002112892C Science First. Analytical Test

12423 NE Whitaker WayPortland, OR 97230

503-254-1794

Job Number:

Report Date:

ORELAP#:

11/07/2017

OR100028

12:00Received: 10/31/17

17-002217

Purchase Order:Purchase Order:

Report#: 029736-00

Code Explanation

Q Matrix interferences affecting spike or surrogate recoveries.

Q1 Quality control result biased high. Only non-detect samples reported.

Q2 Quality control outside QC limits. Data considered estimate.

Q3 Sample concentration greater than four times the amount spiked.

Q4 Non-homogenous sample matrix, affecting RPD result and/or % recoveries.

Q5 Spike results above calibration curve.

Q6 Quality control outside QC limits. Data acceptable based on remaining QC.

R Relative percent difference (RPD) outside control limit.

R1 RPD non-calculable, as sample or duplicate results are less than five times the LOQ.

R2 Sample replicates RPD non-calculable, as only one replicate is within the analytical range.

LOQ1 Quantitation level raised due to low sample volume and/or dilution.

LOQ2 Quantitaion level raised due to matrix interference.

B Analyte detected in method blank, but not in associated samples.

B1 The sample concentration is greater than 5 times the blank concentration.

B2 The sample concentration is less than 5 times the blank concentration.

Explanation of QC Flag Comments:

Page 8 of 8Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unlessotherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be kept a maximum of 15 days from the report date unless priorarrangements have been made.

Testing in accordance with: OAR 333-007-0400