ANAL & MINERALOGICAL INVESTIGATION OF SAMP OF JEAN L & …

52H81NE8883 2 .12408 HANSON LAKE 010

Analytical and Mineralogical

Investigation of

Samples of JEAN LAKE and MHW ORE

submitted by

PHANTOM EXPLORATIONS SERVICES

Progress Report No. l

1989

Project No. LR-3471

Note:This report refers to the samples as received.

The practice of this Company in issuing reports of this nature is to require the recipient not to publish the report or any part thereof without the written consent of Lakefield Research.

LAKEFIELD RESEARCHA Division of Falconbridge Limited

Lakefield/ OntarioMarch 15, 1988

LA^1"" niiiiiinniiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiii52H01NEeee3 2.12488 HANSON LAKE 010C

Page No.

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TITLE ........................................................ i

TABLE OP CONTENTS ............................................ li

INTRODOCTION ................................................. l

SIJWARY ................................,..................... 2

1. Sample Description .................................. 2

2. Sample Analysis ..................................... 2

2.1. Direct Quantitative Analysis . ..........*..... 2

2.2. Semi-quantitative Spectrographic Analysis ..... 3

2.3. Whole Rock Analysis ........................... 4

3. Mineralogical Examination ......................*... 5

3.1. Preparation and Procedure ..................... 5

3.2. Results ....................................... 5

3.3. Jean Lake Specimens ......................*.... 6

3.3.1. Selvage Zone .......................... 6

3.3.2. Muscovite Zone ........................ 6

3.3.3. Spodumene / Quartz Zone ............... 6

3.4. MHW Specimens ................................. 6

3.4.1. Muscovite Zone ........................ 6

3.4.2. Quartz / Spodumene Zone ............... 6

PHOTOMICROGRAPHS ............................................... 7

INTRODUCTION

This report details the results of analytical and mineralogical testwork

conducted on samples of Jean Lake and MNW ore submitted by Phantom Exploration

Services Limited of Thunder Bay, Ontario.

The test program included sample preparation to extract representative

samples from 50 kilogram bulk field samples, semi-quantitative spectrographic

analysis, whole rock analysis, direct quantitative analysis for Li 20, as well

as a mineralogical examination of four polished thin sections.

The results and direction of testwork were discussed in telephone

conversations with Mr. Richard Middaugh of Phantom Exploration Services Ltd.

during the course of the project.

LAKEFIELD RESEARCH

A --Robert S. Salter

General Manager

James T. Futey

Senior Project Engineer

Petrographic Examination By: W. Dean - Mineralogist

- 2 -

SUMMARY

1. Sample Description

A shipment consisting of four plastic pails of broken rock samples

totalling 107 kilograms were recieved at Lakefield Research on February 15,

1988 (our ref LR-8829057).

Pails l and 2 were combined (approximately 50 kg) and labelled "Jean

Lake". Pails 3 and 4 were combined (approximately 50 kg) and labelled

"MNW". Two large pieces of broken rock were hand picked from each sample

for mineralogical examination. The remaining samples were individually

stage crushed to -1/4 inch in a laboratory jaw crusher. From each 50 kg

bulk, a 5 kg sample was riffled out and stage crushed to -10 mesh in a

laboratory cone crusher. From each -10 mesh sample, two sub-samples were

riffled out, these being 200 grams for analysis and 100 grams for

mineralogical examination.

The quantities of each sample remaining in storage at Lakefield Research

consist of about 45 kg of -1/4 inch plus about 4.7 kg of -10 mesh material.

2. Sample Analysis

2.1. Direct Quantitative Analysis

A portion of the 200 gram analytical sub-sample was submitted for direct

determination of Lithium as Li 20. Results were as follows:

Jean Lake Composite - 1.25 % Li^O

MNW Composite - 4.44 % Li00

Summary (continued)

2.2. Semi-quantitative Spectrographic Analysis

A portion of the 200 gram analytical sub-sample was submitted for

with the following results:

Range jean Lake MHW

10 - 100 1 Si Si

3 30 %

1 10 1 Na (Li)

0.3 31 Fe, (Li) , K Fe

0.1 11 Na, K

0.03 - 0.3 i

0.01 - 0.1 1 Mn

0.003 - 0.03 1 Ga, Al Sn, Cu, Al

0.001 - 0.01 1 Tl, Mg, Sn, Cu, Zn, Tl, Mg, Mn, Ga, Ni, CrCa, Cr

0.0003 - 0.003 1 Ni, Co Co

0.0001 - 0.001 1 Pb Pb

^.0003 1 Be, Bi, Mo, Ag Bi, Mo, Ag

I

S Li Li

I - Interference prevents positive identification.

S - Strong spectral lines, unable to estimate amount.

Unless specified above, the following were not detected at the approximatelower limits of 0.5 (Cu, Ag) ; 5 (Mg, Cr) ; 10 (Be, Bi, Ca, Co, Ni,V); 25Fe, Pb, Mo, Si, Sr, Sn, Ti, Zr, Tl, Pd, U, Th) ; 50 (Al, Sb, Bi, Cd, Ga,Zn) ; 100 (As, Au, Ba, In, Na) ; 200 (Nb, Ta, W, Rb, Pt) ; 300 (P, Te, Y,1000 (K).

3 -

SQS

ppm(Ge,Li,

Ce);

1 jSummary (continued) - 4 -

2.3. Whole Rock Analysis

A portion of the 200 gram sub-sample was submitted for whole rock

analysis with the following results:

Analysis Jean Lake MHW

% Si02 73.8 73.5

l A1 203 16.3 16.9

l Fe.O 0.43 0.48tt J

% MgO 0.10 0.18

\ CaO 0.28 0.05

l Na20 4.25 0.69

% K20 2.69 0.83

0.01 0.01 4.

l P205 0.14 0.05

l MnO 0.15 0.02

\ L .O.I. 0.52 0.26

Sub-total 98.67 92.97

l Li 20 1.25 4.44

Total 99.92 97.41

l.Sumnary (continued) - 5 -

3. Mineralogical Examination

Two large hand-picked pieces of broken rock plus a representative 100

gram sub-sample of each zone were submitted for mineralogical examination. In

summary, the specimens contained spodumene, quartz/ muscovite/ albite and

microcline in amounts which varied with the sample and with the part of the

specimen from which the section was cut.

The grain size of spodumene in the sections ranged from a maximum of 6

millimeters to less than 150 micrometers. An estimeated 65 l of the observed

spodumene measured between 0.5 and 1.5 millimeters.

3.1. Preparation and Procedure

Two polished thin sections were cut from each specimen. Sections from

the Jean Lake specimen were cut to include the finer grained contact zone as

well as the obviously spodumene-bearing area. Sections from the MNW specimen

were cut from the "massive" spodumene area and from the strongly micaceous

area.

3.2. Results

The samples were roughly similiar with respect to mineral composition.

Both contained spodumene/ muscovite and quartz as the major minerals of the

spodumene "zone" with albite, quartz and muscovite in the selvage. Accessory

minerals indentified included acicular tourmaline in the MNW specimen and

microcline in the Jean Lake specimen.

Both specimens reflected mineral zoning in the structure with spodumene

in the coarser mineral zones. Other lithium-bearing minerals were not

identified.

Some alteration of spodumene was noted with muscovite and albite as

alteration products. In general, however, the spodumene appeared to be fresh

and there were not many instances of complex association between spodumene and

other minerals. Some instances of inclusions of quartz or albite in spodumene

were noted but these may be expected to liberate readily in melting.

Summary (continued) - 6 -

3.3. Jean Lake Specimens

3.3.1. Selvage Zone

The selvage zone was finer grained than the rest of the specimen with

little or no spodumene. The major minerals of this zone were albite,

muscovite and quartz. Hydromica and microcline were accessory constituents

present in amounts less than 5 l by weight. The average grain size of the

minerals was on the order of 400 to 700 micrometers.

3.3.2. Muscovite Zone

In the muscovite zone the major mineral constituents were muscovite,

spodumene and quartz. Grain size of the spodumene ranged from 0.5 to 4

millimeters in length with approximately 65 l measuring between 0.5 and l

millimeter.

3.3.3. Spodumene f Quartz Zone

In this zone spodumene and quartz were the major minerals with muscovite

a minor mineral and albite either absent or present as an accessory. Grain

size of the spodumene ranged from 0.4 to a maximum of 2.2 millimeters. The

average grain size was between 0.5 and 1.5 millimeters.

3.4. MNW Specimens

3.4.1. Muscovite Zone

Muscovite, spodumene and quartz were the major minerals with albite

present as a minor mineral. Accessory minerals included tourmaline and

possibly beryl.

3.4.2. Quartz f Spodumene Zone

In this zone the major minerals were quartz and spodumene with albite and

microcline as minor to accessory minerals. Muscovite ranged from minor

through accessory to absent altogether. Grain size of the spodumene ranged

from a maximum of 6 to 7 millimeters to smaller than 150 micrometers. The

average size of 65 l of the spodumene in both zones was between 0.6 and 1.2

millimeters.

wac cu405o

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Photomicrographs (continued) - 8 -

Illustration l - Jean Lake

Muscovite {yellow, orange, pink) withQuartz {brown) in Muscovite plus Albite{dark brownish gray) penetratingMuscovite.Magnification 100X {Nichols crossed)

Illustration 2 - Jean Lake

Muscovite (blue) with Albite (brown and white) plus Quartz (gray). Magnification 100X (Nichols crossed)


Illustration 3 - M N W

Quartz (gray) with Spodumene (yellows and dark colours), Albite (white) plus Muscovite (blue). Magnification 100X (Nichols crossed)


Spodumene (yellows and brown) with Quartzinclusions.Magnification 100X (Nichols crossed)

J*hotomicrographs (continued) - 10 -


Quartz (light colours) cutting Spodumene(dark colours).Magnification 100X (Nichols crossed)

Illustration 6 - H N W

Spodumene (high relief) plus Quartz. Note alteration of Spodumene (dark colours). Magnification 100X (plain light)



Shows alteration of Spodumene but not all of the Spodumene shows alteration. Magnification 100X (Nichols crossed)


Quartz veinlet (blue) plus Albite (colourless) cutting Spodumene (brown). Magnification 100X (Nichols crossed)



Quartz around Spodumene (high relief) Magnification 100X (Plain light)

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•/^•^Sy^'^^ftJV'.:;^:'!-

i:;';;;^: ;^:l^fiM:S; : -. '10935 a ao 10

Ministry o) Report of Work Northern Developmentand Mines (Geophysical, Geological,

Ontario .. Geochemical and Expenclitu

DOCUMENT" 'tractions: - Pleasu type or pi int.

-- If number of mining claims traverseduxcceds space on this form, attach o list.

Nfitp: Onlv davs r.r firlil^ ra Ir 11 la t fid in t IIP

/f/*t*'6* MiningType of Survey(s)

CiairrTHolderU!

Address

Survey Company

Name and Address of Author (of Geo-Technical report)

2.12408 HANSON LAKE 900

..,.^Date of Survey (from a lo)

-..|Tot*l Miles of line Cot

Credits Requested per Each Claim in Columns at right___ Mining Claims Traversed {List i n numerical sequence)Special Provisions

For first survey:

Enter 40 days. (This includes line cutting)

For each additional survey- using the same grid:

Enter 20 days (for each)

Man Days

Complete reverse side and enter total(s) here

Airborne C'P'i'ts

Note: Sp'.'fiJl prouvons ci, 'ellis do not ijpply lo A'lhnim? Sut vfys.

Geophysical

- Electromagnetic

- Magnetometer

- Radiometric

- Other

Geological

Geochemical

Geophysical

- Electromagnetic

* Magnetometer

- Radiometric

- Other

Geological

Geochemical

Eiocuomagnetic

Mdgnetomeier

RiidiotTietric

Days per Claim

———— ——

—— ————

Days perClaim

- ~ -——

-———— -

Days per Claim

(excludes powci stripping)lypeo' V.or' Pt- 1 o' rued

tii.'.i' o ' ( ' t*p.,"--i U*rc Days C rvdiTS

Total f n ficnint ,n csTotal

Days Credits

'ns'mf t'O*'*

T ota D i, i O t; J its M..1 y tie apportioned a l the c UT i m holder's 11-.o iv C •ill'1 ' MU mi io' ol days r roti*ts per claim sclcritul

D.) i of ArfL-nt (Signa/urc)

v M z.f/fft —,^—Jei/iTi.iii.ii-Ve'Mying Repoft'offlork ' ^~~'~7

JN'iARIO QEOLCASSBSSMt

OFF

,-r r: t \ , - 11 .r s i' 1 -'! f tuivu a t it-1 soiVil and intmiaio knowledge of the farts se l forth in th^ Ropni t of Work annexed hereto, having performed the work f.: 1 - - , - .1 ..i'' 1 '- -lufing und;oi jlit.-r its compUMion and the iinnexed ti'poil is line

•j; t,il A.l.licSS Ot . C^Mitying

73(s* T u BJYDate Co rfnaturUl

g^yfc

COSGRAVE

ARMENO RESOURCES INC.

PROPERTYCOSGRAVE LAKE AREA

Thunder Bay Mining Division N.T.S. 42-E-5Dote : Nov., 1987 | Scale: i: 31680 FIG. 5

PHANTOM EXPLORATION SERVICES LTD

o o-t- oJCQ

AN

-•.•-r..-j., -iL..-*- L 2 +00 S

863303

10915-I..I..JI,————..nil.————— J*. L 3+00 S

L 4-f 00 S

863304

10915

LE G E N D

Area of new drilling and blasting

Bulk sample location

Old trenches

Grab sample location

ARMENO RESOURCES INC.

M.N.W. PROPERTYHANSON LAKE AREA DISTRICT OF THUNDER BAY

SAMPLE LOCATION MAPDATE: FEB.,1988 SCALE: 112500 N.T.S.:52-H-

PHANTOM E XPLORATION SERVICES LTD.

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ANAL & MINERALOGICAL INVESTIGATION OF SAMP OF JEAN L & …

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Transcript of ANAL & MINERALOGICAL INVESTIGATION OF SAMP OF JEAN L & …