AN EXPERIMENTAL INVESTIGATION OF … EXPERIMENTAL INVESTIGATION OF COMPOSITE BRICKS A PROJECT REPORT...
Transcript of AN EXPERIMENTAL INVESTIGATION OF … EXPERIMENTAL INVESTIGATION OF COMPOSITE BRICKS A PROJECT REPORT...
AN EXPERIMENTAL INVESTIGATION OF
COMPOSITE BRICKS
A PROJECT REPORT
Submitted by
DEEPIKA.D 714112103013
DINESH.S 714112103015
KAMALRAJ.S 714112103027
ARUL SENTHUR NATHAN.A 714112103303
In partial fulfillment for the award of the degree
Of
BACHELOR OF ENGINEERING
in
CIVIL ENGINEERING
SRIGURU INSTITUTE OFTECHNOLOGY,
COIMBATORE.
ANNA UNIVERSITY: CHENNAI 600 025
APRIL 2016
ANNA UNIVERSITY: CHENNAI 600 025
BONAFIDE CERTIFICATE
Certified that this project report titled “AN EXPERIMENTAL
INVESTIGATION OF COMPOSITE BRICKS”is the bonafide work of
DEEPIKA.D (714112103013), DINESH.S (714112103015), KAMALRAJ.S
(714112103027) and ARUL SENTHUR NATHAN.A (714112103303) who
carriedout the project work under my supervision.
SIGNATURE
Prof. C.V.BINDU, M.E.,(Ph.D.)
Head of the Department,
Department of Civil Engineering,
SriGuru Institute of Technology,
Coimbatore.
SIGNATURE
Prof. C.V.BINDU, M.E.,(Ph.D.)
SUPERVISOR
Head of the Department,
Department of Civil Engineering,
SriGuru Institute of Technology,
Coimbatore.
Certified that the candidate were examined in the project viva –voce
Examination held on……………………….
INTERNAL EXAMINER EXTERNAL EXAMINER
i
ACKNOWLEDGEMENT
First of all, we would like to articulate our humble thanks to God for
showering his blessing upon us. We owe our sincere thanks to our parents who
helped, motivated and encouraged us in this endeavor.
Our thanks to the philanthropists of SriGuru Institute of Technology, for
providing us quality engineering education and sculpturing, our director and our
principal Dr. S.BABU DEVASENAPATHI, for providing all facilities.
We are extremely grateful to Prof. C.V.BINDU M.E., (Ph.D.,) Head of
the Department of Civil Engineering SriGuru Institute of Technology,
Coimbatore, for her remarkable guidance, advice and motivation in completing
this project.
We sincerely express our gratitude to our project guide Prof.
C.V.BINDU M.E., (Ph.D.,) Head of the Department of Civil Engineering,
SriGuru Institute of Technology, Coimbatore, for guidance throughout the
project.
We also thank all the teaching and non-teaching staff of the department
for encouraging and supporting us during the entire process of this project. We
also extend our gratitude to all our friends who all stood behind our project by
helping us in many aspects.
ii
ABSTRACT
Disposal of used Plastics is a major problem in the present era, as the
usage of plastics is growing day by day and it takes hundreds of years for plastic
material to degrade. So effective ways to recycle & reuse of plastics are being
formulated. According to their composition, plastics have been classified into
seven types each having their own recycle rate.
One such type HDPE (High Density Polyethylene) was taken into
consideration as it was easily available & had higher density than other types.
The used plastics were collected , ground into smaller components, melted &
pulverized in order to get granules of plastic of about 1mm size. The density of
the Pulverized plastic was found to be 460 kg/m³ & its specific gravity was
0.46. Sieve analyses were carried out & about 75% of the plastics were found to
be in the range of 1-1.7mm.
In this experimental investigation the laboratory test of fly ash bricks by
adding pulverized plastic powder. The waste plastic pulverized powder is to be
added in proportions of 5%, 10%, 15% and 20% in the volume of bricks.
The compressive strength and water absorption were determined at the
end of 7, 14 and 21 days. In this investigation at 20% of pulverized waste
plastic powder content effect of bricks on compressive strength and water
absorption were determined. Strength comparison of a normal fly ash bricks and
composite fly ash bricks. The paper also shows the cost comparison per each
block.
CONTENTS
CHAPTER TITLE PAGE NO
ACKNOWLEDGEMENT i
ABSTRACT ii
LIST OF TABLES
LIST OF FIGURES
1 INTRODUCTION
1.1 General 1
1.2 Introduction 1
1.3 Ash from coal combustion 3
1.3.1 Dry fly ash 3
1.3.2 Bottom ash 3
1.3.3 Pond ash 4
1.3.4 Boiler slag 4
1.3.5 FGD gypsum 4
1.4 Environmental Impacts Of Fly Ash 4
1.4.1 Hazards 4
1.5 Goal 5
1.6 Objectives 5
2 LITERATURE REVIEW
2.1 Strength and durability of fly ash cement and
gypsum bricks 6
2.2 Utilization of pulverized plastic in cement concrete
as fine aggregate 7
3 MATERIALS AND METHODOLOGY
3 General 8
3.1 Fly ash 8
3.1.1 Origin of the fly-ash 8
3.1.2 Properties of fly-ash 8
3.1.3 Testing of fly ash 8
3.1.3.1 Specific gravity test 8
3.1.3.2 Sieve analysis test 10
3.2 Quarry dust 12
3.2.1 Origin of quarry dust 12
3.2.2 Physical and chemical properties 12
3.2.3 Advantages of quarry dust 14
3.2.4 Disadvantages of quarry dust 14
3.2.5 Testing of fly ash 14
3.2.5.1 Specific gravity test 14
3.2.5.2 Sieve analysis test 16
3.3 Cement 18
3.4 Water 18
3.5 Pulverized waste plastic powder 18
3.5.1Properties 18
3.5.2 Physical properties 19
3.5.3 Applications 19
3.5.4 Grade selection 19
3.5.5 Advantages 20
3.5.6 Disadvantages 20
3.5.7 Applications 20
3.5.8 PH test 20
4 PROCESS OF MOULDING
4 General 23
4.1 Collection of material 23
4.2 Mixing 23
4.2.1 Proportioning of raw materials 23
4.2.2 Calculation of mix proportions 24
4.3 Casting of bricks 25
4.4 Drying of bricks 26
4.5 Curing of bricks 26
5 RESULTS AND DISCUSSION
5.1 General 27
5.2 Testing of bricks 27
5.2.1 Compressive strength test 27
5.2.2 Water absorption test 36
5.2.3 Efflorescence test 41
5.2.4 Structure test 42
5.2.5 Soundness test 42
5.2.6 Hardness test 43
5.2.7 Dimensional tolerance 43
COMPARISON STATEMENT 44
6 CONCLUSION 45
REFERENCES 46
IS CODE REFERENCE 47
LIST OF TABLES
TABLE TITLE PAGE NO
1 Comparison between Clay brick and Fly ash Brick 2
3.1 Specific Gravity Test For Fly Ash 10
3.2 Sieve Analysis Test For Fly Ash 11
3.3 Showing The Physical Properties Of Quarry Dust
And Natural Sand 13
3.4 Showing The Typical Chemical Properties Of
Quarry Dust And Natural Sand 13
3.5 Specific Gravity Test For Fly Ash 15
3.6 Sieve Analysis Test For Quarry Dust 17
3.7 Ph Test Result 22
4.1 Mix Proportion For 3 Bricks 25
5.0 Class Designation Of Bricks 28
5.1 Compression Test On Hand Mould Clay Brick 29
5.2 Compression Test On Clay Bricks In Machine
Mould 29
5.3 Compression Test On Fly Ash Brick In Hydraulic
Mould 29
5.4.1 Compression Test On Nominal Fly Ash Brick (7
Days Curing) 30
5.4.2 Compression Test On Nominal Fly Ash Brick (14
Days Curing) 30
5.4.3 Compression Test On Nominal Fly Ash Brick (21
Days Curing) 30
5.5.1 Compression Test On Composite Fly Ash Brick 5%
PWP Powder Added At 7 Days Curing 31
5.5.2 Compression Test On Composite Fly Ash Brick 5%
PWP Powder Added At 14 Days Curing 31
5.5.3 Compression Test On Composite Fly Ash Brick 5%
PWP Powder Added At 21 Days Curing 31
5.6.1 Compression Test On Composite Fly Ash Brick
10% PWP Powder Added At 7 Days Curing 32
5.6.2 Compression Test On Composite Fly Ash Brick
10% PWP Powder Added At 14 Days Curing 32
5.6.3 Compression Test On Composite Fly Ash Brick 10%
PWP Powder Added At 21 Days Curing 32
5.7.1 Compression Test On Composite Fly Ash Brick 15%
PWP Powder Added At 7 Days Curing 33
5.7.2 Compression Test On Composite Fly Ash Brick 15%
PWP Powder Added At 14 Days Curing 33
5.7.3 Compression Test On Composite Fly Ash
Brick 15% PWP Powder Added At 21 Days Curing 33
5.8.1 Compression Test On Composite Fly Ash Brick 20%
PWP Powder Added At 7 Days Curing 34
5.8.2 Compression Test On Composite Fly Ash Brick 20%
PWP Powder Added At 14 Days Curing 34
5.8.3 Compression Test On Composite Fly Ash Brick 20%
PWP Powder Added At 21 Days Curing 34
5.9 Compressive Strength Of Composite Bricks 35
5.10 Compressive Strength Comparison Of Conventional
Bricks Composite Bricks 36
5.11.1 Water Absorption Test On Conventional Clay Brick 37
5.11.2 Water Absorption Test On Conventional Clay Brick 38
5.11.3 Water Absorption Test On Conventional Flyash Brick 38
5.11.4 Water Absorption Test On Composite Flyash Brick (0%
PWP Powder Added) 38
5.11.5 Water Absorption Test On Composite Flyash Brick (5%
PWP Powder Added) 39
5.11.6 Water Absorption Test On Composite Flyash Brick (10%
PWP Powder Added) 39
5.11.7 Water Absorption Test On Composite Flyash Brick (15%
PWP Powder Added) 39
5.11.8 Water Absorption Test On Composite Flyash Brick (20%
PWP Powder Added) 40
5.12 Water Absorption Test On Composite Bricks 40
5.13 Water Absorption Test Comparison Of Conventional And
Composite Bricks 41
5.14 Efflorescence Test Report 42
LIST OF FIGURES
FIGURE TITLE PAGE NO
1 Fly Ash “F” Class 48
2 Quarry Dust 48
3 OPC 53 Grade Cement (Dalmia) 48
4 PWP Powder (Polypropylene 48
5 PWP Powder Was Sieved Before Mixing 48
6 Mixing Of Raw Materials 49
7 Dry Mixing Of Raw Material 49
8 Wet Mixing Of Raw Materials Bricks 49
9 Moulding Of BRICKS 49
10 Air Drying Process 49
11 Curing Process 49
12 Compression test for clay brick in hand mould (sample
code H10) 50
13 Compression test for clay brick in machine mould
(sample code M4) 50
14 Compression test for fly ash brick in hydraulic mould
(sample code F2) 50
15 Compression test for nominal fly ash brick in hand
mould (sample code P12) 51
16 Compression test on composite fly ash brick 10%
PWP powder (sample code R11) 51
17 water absorption test (before and after immersion of
water) 51
18 During efflorescence test 52
19 After 24 hrs on efflorescence test 52
20 Structure test - Nominal bricks 52
21 Structure test - 5% Composite bricks 52
22 Structure test - 10% Composite bricks 52
23 Structure test - 20% Composite bricks 52
24 During soundness test 53
25 During hardness test 53
26 Dimension test for length wise 53
27 Dimension test for width wise 54
28 Dimension test for depth wise 54
1
INTRODUCTION
1.1 GENERAL
Fly Ash bricks are made of fly ash, lime, gypsum cement and sand. These
can be extensively used in all building constructional activities similar to that of
common burnt clay bricks. The fly ash bricks are comparatively lighter in
weight and stronger than common clay bricks. Since fly ash is being
accumulated as waste material in large quantity near thermal power plants and
creating serious environmental pollution problems, its utilization as main raw
material in the manufacture of bricks will not only create ample opportunities
for its proper and useful disposal but also help in environmental pollution
control to a greater extent in the surrounding areas of power plants.
Manufacturing of commercial brick produce a lot of air pollution. The
technology adopted for making. The fly ash bricks are eco-friendly. It is no need
fire operation in production unlike the conventional bricks Among the
traditional fossil fuel sources, coal exists in quantities capable of supplying a
large portion of nation’s energy need. That’s why the power sector in India is a
major consumer of coal in India and will continue to remain so far many years
to come. Combustion of coal in thermal power plant not only produces steam to
run electricity-generating turbine but also produces a large quantity of by-
products like fly ash etc.
1.2 INTRODUCTION
About 80 thermal power plants in India are sources of fly ash, where
around millions of tones of coal are used annually. India currently generates 100
million tones of fly ash every year. This produces 30-40 million tones of fly ash
unused every year. This disposal will need thousands hectares of storage land,
which may cause further ecological imbalance. In fact, this waste material is
simply disposed off in the form aqueous slurry on the adjoining areas. This type
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of disposal not only converts useful agricultural land to waste ones but also
possesses a threat to the quality of environment.
The human development of united nation development programmed
indicates that annually 83-163 million hectares of land is eroded in India
causing productivity loss of about 4 to 6.3% of the total agricultural output
worth $2.4 billion. Therefore, using fly ash as a building material has assumed
great significance like never before. Several investigations have been carried out
throughout the world to make an attempt to use fly ash in many civil
engineering projects by virtue of its good properties as an ingredient of
concrete. The Comparison between Clay brick and Fly ash Brick is shown in
Table 1.
Table 1: Comparison between Clay brick and Fly ash Brick
Clay Brick Fly Ash Brick
Varying colour as per soil Uniform pleasing colour like cement
Uneven shape as hand made Uniform in shape and smooth in finish
Lightly bonded Dense composition
Plastering required No plastering required
Heavier in weight Lighter in weight
Compressive strength is around 35
kg/Cm²
Compressive strength is around 100
kg/Cm²
More porous Less porous
Thermal conductivity
1.25 – 1.35 W/m² ºC
Thermal conductivity
0.90-1.05 W/m² ºC
Water absorption 20-25% Water absorption 6-12%
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1.3 ASH FROM COAL COMBUSTION
The quality of coal depends upon its rank and grade. The coal ranks are
arranged in an ascending order of carbon contents is:
Peat <Lignite < sub-bituminous coal< bituminous coal < anthracite
Indian coal is mostly sub-bituminous rank followed by bituminous and
lignite (brown coal). The ash content in Indian coal ranges from 35 % to 50 %.
The coal properties including calorific values differ depending upon the colliery
location. The calorific value of the Indian coal (~ 15 MJ/kg) is less than the
normal range of 21 MJ/kg to 33 MJ/kg (gross). There are generally five
categories of coal ashes available from thermal power stations. Those are:
1.3.1 Dry fly ash – It is collected from different rows of electrostatic
precipitators in dry form. The fly ash is produced from the burning of
pulverized coal in a coal-fired boiler. It is a fine grained, powdery particulate
material in nature. It is carried through the flue gas and collected from the flue
gas by means of electrostatic precipitators, bag-houses, or mechanical collection
devices such as cyclones. Fly ash is the finest of coal ash particles. It is
transported from the combustion chamber by exhaust gases.
1.3.2 Bottom ash –It is collected at the bottom of the boiler furnace and is
characterized by better geotechnical properties. Coal bottom ash and fly ash are
different physically, mineralogically and chemically. Bottom ash is a coarse,
granular, incombustible by-product that is collected from the bottom of the
furnaces that burn coal for the generation of steam, the production of electric
power or both. Bottom ash is coarser than fly ash, and grain sizes varying from
fine sand to fine gravel.
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1.3.3 Pond ash – Bottom ashes and Fly ash are mixed together with water to
form slurry which is pumped to the ash pond area. In the ash pond the ash gets
settled and excess water is poured out. This deposited ash is called pond ash.
1.3.4 Boiler slag - Boiler slag is coarser than conventional fly ash and is formed
in cyclone boilers, which produce a molten ash that is cooled with water. Boiler
slag is generally a black granular material. It can be used in numerous
engineering applications.
1.3.5 FGD gypsum - Flue Gas Desulfurization (FGD) gypsum is also known as
scrubber gypsum. FGD gypsum is the by-product of an air pollution control
system that removes sulphur from the flue gas in calcium based scrubbing
systems. It is produced by employing forced oxidation in the scrubber and is
composed mostly of calcium sulphate.
1.4 ENVIRONMENTAL IMPACTS OF FLY ASH
The World Bank has cautioned India that by 2015, disposal of coal ash
would require 1000 sq. km. of land. Since coal currently accounts for 70% of
power generation in the country, there is a need of new and innovative methods
for reducing impacts on the environment. The problem with fly ash lies in the
fact that not only does its disposal require large quantities of land, water and
energy, its fine particles, if not managed well, can become airborne. Currently
more than 120 million tones of fly ash are being generated annually in India,
with 65000 acres of land being occupied by ash ponds.
1.4.1 HAZARDS
Due to physical characteristics and large volumes generated, fly ashes pose
problems like:
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1. It is very difficult to handle the material in dry state because it is very fine
and readily air borne even in mild wind.
2. It disturbs the ecology of that region, becomes source of soil, air and water
pollution.
3. Long inhalation of fly ash causes fibrosis of lungs, silicosis, pneumonitis
bronchitis etc.
4. Flying fine particles of ash poses problems for living near power stations,
corrode structural surfaces and affect horticulture.
5. Ultimate settlement of fly ash particles over many hectares of land in the
vicinity of power station brings about perceptible degeneration in soil
characteristics.
1.5 GOAL
The basic aim of this project is to evaluate the strength potential of fly ash
with cement & water. The aim has been achieved through covering the
following specific objectives.
1.6 OBJECTIVES
The above goal was achieved with the following specific objectives.
Investigating the engineering properties and characteristics of the fly ash
samples collected.
Investigating the strength gain of composite material aspects associated
with the fly ash specimen collected.
Establishment of better suitable combinations of fly ash – pulverizes
waste plastic powder compositions for under laboratory test.
6
LITERATURE REVIEW
2.1 STRENGTH AND DURABILITY OF FLY ASH, CEMENT
AND GYPSUM BRICKS (INTERNATIONAL JOURNAL OF COMPUTATIONAL ENGINEERING
RESEARCH (IJCER) - MAY – 2014)
Nitin S. Naik, B.M.Bahadure and C.L.Jejurkar present that strength and
durability aspect of bricks prepared using Fly Ash, Cement and
Phosphogypsum.
The results of compressive strength on cubes of fly ash, cement and
phosphogypsum when cured in potable water are shows along with results of
water absorption of the cubes. This paper shows compressive strength of fly
ash, cement and phosphogypsum cubes for different mix proportions. From the
table it is clear that the said binder gives good compressive strength though the
water absorption is slightly on higher side of the I.S. requirements. When bricks
are prepared with mix M-5 and tested for compressive strength and water
absorption, it has been found that the bricks are having good compressive
strength of 6.360MPa at the age of 14 days and 9.420 MPa at the age of 28
days, which is well above the I.S. requirement of 3.5 MPa.
The water absorption of the bricks is found to be 28.44 % after
submergence in water for 28 days which is above the I.S. requirement. The
results are shown in table 3. Table 4 shows compressive strength of cubes of all
mix proportions when exposed to sulphate solution for 28 days. If it is
compared with compressive strength of cubes, it can be observed that curing in
sulphate solution has resulted in reduction in compressive strength.
Thus the bricks prepared from fly ash, cement and phosphogypsum can
offer good resistance to sulphate attack. For higher percentage of cement in the
mix the percentage reduction in compressive strength is very high i.e. up to
16%. Due to action of fly ash with sulphate solution and due to increased
percentage of phosphogypsum resistance of the mix against sulphate attack
7
increases. From the above results and discussion following conclusions can be
drawn.
2.2UTILIZATION OF PULVERIZED PLASTIC IN CEMENT
CONCRETE AS FINE AGGREGATE
(IJRET: International Journal of Research in Engineering and Technology
ISSN: 2319-1163 / JUNE 2013)
P. Suganthy, Dinesh Chandrasekar and Sathish Kumar. P. K
The water cement ratio of concrete is found to increase with increase in
replacement of Sand by Plastic material. The Weight of the cube decreases with
an increase in replacement of Sand by Plastic material. It is seen that the
decrease in weight is linear with increase in replacement. The variation of
strength with age of Conventional and concrete with 25% replacement Sand by
Plastic material follows a similar pattern. There is not much change in strength
with the age of concrete for Concrete which contains more than 25%
replacement of sand by plastic material.
There is Gradual decrease in strength for replacement up to 25% and then
the strength decreases rapidly for 25% to 50% of Sand by Plastic material, after
50% the strength variation is somewhat gradual. The ultimate as well as the
yield strength of concrete at 7th day decreased by about 3 to 3.2 N/mm²for
25%replacement & 4 to 6.5 N/mm² for higher replacements of Plastic when
compared to conventional concrete. The ultimate as well as the yield strength of
concrete at 14th day & 28th day decreased by about 0.2 to 1 N/mm² for 25%
replacement & 9.1to14.6 N/mm² for higher replacements of Plastic when
compared to conventional concrete.
8
MATERIALS AND METHODOLOGY
3 GENERAL
The following ingredients are used for manufacturing the structural
element namely fly ash, quarry dust, cement, waste plastic powder and water.
To investigate the properties of the materials that were used for casting the
specimens, various laboratory tests were performed following the codes IS
2386:1963 and is 383:1970. The results are as follows.
3.1 FLYASH
3.1.1 ORIGIN OF THE FLY-ASH
The fly ash is the by-product that is formed in the thermal power plants.
This is used as a partial replacement of cement now-a-days in general cases.
3.1.2 Properties of Fly-ash:
Property Result
Specific Gravity 2.79
Fineness
Retained on 75μ
Sieve 9%
Specific Surface,
Blaine, m²/Kg 526
3.1.3 TESTING OF FLYASH
3.1.3.1 SPECIFIC GRAVITY TEST
Objective
Determination of specific gravity of fly ash by pycnometer
method.
Reference Standard
IS : 2720 (Part 4) – 1985 – Method of test for soil (Part 4-Grain
size analysis)
9
Equipment & Apparatus
Pycnometer
Sieve(4.75 mm)
Weighing balance
Preparation sample
After receiving the soil sample it is dried in oven at a temperature
of 105 to 1150C for a period of 16 to 24 hours.
Procedure
Dry the pycnometer and weigh it with its cap(W1)
Take about 200 g to 300 g of oven dried soil passing through
4.75mm sieve into the pycnometer and weigh again(W2)
Add water to cover the soil and screw on the cap.
Shake the pycnometer well and connect it to the vacuum pump to
remove entrapped air for about 10 to 20 minutes.
After the air has been removed, fill the pycnometer with water and
weigh it (W3). Clean the pycnometer by washing thoroughly.
Fill the cleaned pycnometer completely with water up to its top
with cap screw on. Weigh the pycnometer after drying it on the
outside thoroughly(W4).
Calculation
The Specific gravity of soil solids (Gs) is calculated using the
following equation.
10
Where,
W1=Empty weight of pycnometer
W2=Weight of pycnometer + oven dry soil
W3=Weight of pycnometer + oven dry soil + water
W4=Weight of pycnometer + water full
TABLE 3.1 SPECIFIC GRAVITY TEST FOR FLY ASH
Sample No W1
(gm)
W2
(gm)
W3
(gm)
W4
(gm)
Specific
Gravity
1 630 840 1550 1420 2.625
2 630 950 1640 1420 3.200
3 630 1050 1675 1420 2.545
Mean 2.790
Report
The result of the specific gravity test is 2.79.
3.1.3.2 SIEVE ANALYSIS TEST
Objective
Determination of particle size distribution of fly ash.
Reference standard
IS : 2720 (Part 4) – 1985 – Method of test for soil (Part 4-Grain size
analysis)
Equipment & Apparatus
Balance
Sieves
Sieve shaker
Preparation sample
After receiving the soil sample it is dried in air or in oven
(maintained at a temperature of 600C). If clods are there in soil sample
then it is broken with the help of wooden mallet.
11
Procedure
The sample is dried to constant mass in the oven at a temperature
of 1100±50C and all the sieves which are to be used in the analysis
are cleaned.
The oven dry sample is weighed and sieved successively on the
appropriate sieves starting with largest. Each sieve is shaken for a
period of not less than 2 minutes.
On completion of sieving the material retained on each sieve is
weighed.
Calculation
The percent retained (%), Cumulative retained (%) &
percent finer (%) is calculated.
Percent retained on each sieve = Weight of retained sample in each
sieve / Total weight of sample
The cumulative percent retained is calculated by adding
percent retained on each sieve as a cumulative procedure.
The percent finer is calculated by subtracting the cumulative
percent retained from 100 percent.
TABLE 3.2 SIEVE ANALYSIS TEST FOR FLY ASH
Weight of Sample taken, W = 800 grams
S.No
Sieve
Opening
in mm
Weight Of Soil/
Sand Retained
in gm
Percentage
Of Weight
Retained
Cumulative
Percentage
Retained
Percentage
Finer
1 4.750 0 0 0 100
2 2.360 0 0 0 100
3 1.180 10 1.25 1.25 98.75
4 0.600 125 15.625 16.875 83.125
5 0.300 210 26.25 43.125 56.875
6 0.150 200 25 68.125 31.875
7 0.075 135 16.875 85 15
8 pan 120 15 100 0
12
Graph 1.Semi-log graph for fly ash particle size distribution
RESULT
Effective Size = 0.045mm
Fineness modulus = 3.14
Uniformity coefficient = 7.77
3.2 QUARRY DUST
3.2.1 ORIGIN OF QUARRY DUST:
The quarry dust is the by-product which is formed in the processing of
the granite stones which broken downs into the coarse aggregates of different
sizes.
3.2.2 PHYSICAL AND CHEMICAL PROPERTIES:
The physical and chemical properties of quarry dust obtained by testing
the sample as per the Indian Standards are listed in the below table
4.750 2.360 1.180 0.600 0.300 0.150 0.075 pan
Series1 100 99.625 86.5 74.625 55.25 30.25 13.375 0.25
0
20
40
60
80
100
120P
ER
CE
NT
AG
E O
F F
INE
R
SIEVE OPENING IN mm
SIEVE ANALYSIS FOR FLYASH
13
TABLE 3.3 SHOWING THE PHYSICAL PROPERTIES OF QUARRY
DUST AND NATURAL SAND
Property Quarry Dust Natural Sand Test method
Specific gravity 2.54 -2.60 2.60 IS2386(Part
III)- 1963
Bulk density (kg/m³) 1720- 1810 1460 IS2386(Part
III)- 1963
Absorption (%) 1.20- 1.50 Nil IS2386(Part
III)- 1963
Moisture Content (%) Nil 1.50 IS2386(Part
III)- 1963
Fine particles less than
0.075 mm (%) 12-15 6
IS2386(Part
III)- 1963
Sieve analysis Zone-II Zone-II IS 383- 1970
TABLE 3.4 SHOWING THE TYPICAL CHEMICAL PROPERTIES OF
QUARRY DUST AND NATURAL SAND
Constituents Quarry Dust (%) Natural Sand (%) Test Method
SiO2 62.48 80.78
IS 4032- 1968
Al2O3 18.72 10.52
Fe2O3 6.54 1.75
CaO 4.83 3.21
MgO 2.56 0.77
Na2O Nil 1.37
K2O 3.18 1.23
TiO2 1.21 Nil
Loss of ignition 0.48 0.37
14
3.2.3 ADVANTAGES OF QUARRY DUST:
The Specific gravity depends on the nature of the rock from which it is
processed and the variation is less [3].
3.2.4 DISADVANTAGES OF QUARRY DUST:
Shrinkage is more in when compared to that of the natural river sand.
Water absorption is present so that increase the water addition to the dry mix.
3.2.5 TESTING OF FLYASH
3.2.5.1 SPECIFIC GRAVITY TEST
Objective
For determination of specific gravity of soil solids by pycnometer
method.
Reference Standard
IS : 2720 (Part 4) – 1985 – Method of test for soil (Part 4-Grain
size analysis)
Equipment & Apparatus
Pycnometer
Sieve(4.75 mm)
Weighing balance
Preparation sample
After receiving the soil sample it is dried in oven at a temperature
of 105 to 1150C for a period of 16 to 24 hours.
Procedure
Dry the pycnometer and weigh it with its cap(W1)
Take about 200 g to 300 g of oven dried soil passing through
4.75mm sieve into the pycnometer and weigh again(W2)
Add water to cover the soil and screw on the cap.
15
Shake the pycnometer well and connect it to the vacuum pump to
remove entrapped air for about 10 to 20 minutes.
After the air has been removed, fill the pycnometer with water and
weigh it (W3).
Clean the pycnometer by washing thoroughly.
Fill the cleaned pycnometer completely with water up to its top
with cap screw on.
Weigh the pycnometer after drying it on the outside
thoroughly(W4).
Calculation
The Specific gravity of soil solids (Gs) is calculated using the
following equation.
Where,
W1=Empty weight of pycnometer
W2=Weight of pycnometer + oven dry soil
W3=Weight of pycnometer + oven dry soil + water
W4=Weight of pycnometer + water full
TABLE 3.5 SPECIFIC GRAVITY TEST FOR FLY ASH
Sample No W1
(gm)
W2
(gm)
W3
(gm)
W4
(gm)
Specific
Gravity
1 630 840 1550 1420 2.625
2 630 950 1640 1420 3.200
3 630 1050 1675 1420 2.545
Mean 2.790
Report
The result of the specific gravity test is 2.79.
16
3.2.5.2 SIEVE ANALYSIS TEST
Objective
Determination of particle size distribution of quarry dust.
Reference standard
IS: 2720 (Part 4) – 1985 – Method of test for soil (Part 4-Grain size
analysis)
Equipment & Apparatus
Balance
Sieves
Sieve shaker
Preparation sample
After receiving the soil sample it is dried in air or in oven
(maintained at a temperature of 600C). If clods are there in soil sample
then it is broken with the help of wooden mallet.
Procedure
The sample is dried to constant mass in the oven at a temperature
of 1100 ± 50C and all the sieves which are to be used in the analysis
are cleaned.
The oven dry sample is weighed and sieved successively on the
appropriate sieves starting with largest. Each sieve is shaken for a
period of not less than 2 minutes.
On completion of sieving the material retained on each sieve is
weighed.
Calculation
The percent retained (%), Cumulative retained (%) &
percent finer (%) is calculated.
Percent retained on each sieve = Weight of retained sample in each
sieve / Total weight of sample
17
The cumulative percent retained is calculated by adding
percent retained on each sieve as a cumulative procedure.
The percent finer is calculated by subtracting the cumulative
percent retained from 100 percent
TABLE 3.6 SIEVE ANALYSIS TEST FOR QUARRY DUST
Weight Of Quarry Sand Taken, W = 800 grams
S.No
Sieve
Opening
in mm
Weight of
Soil/ Sand
Retained in
gm
Percentage of
Weight
Retained
Cumulative
Percentage
Retained
Percentage
Finer
1 4.750 0 0 0 100
2 2.360 3 0.375 0.375 99.625
3 1.180 105 13.125 13.5 86.5
4 0.600 95 11.875 25.375 74.625
5 0.300 155 19.375 44.75 55.25
6 0.150 200 25 69.75 30.25
7 0.075 135 16.875 86.625 13.375
8 Pan 105 13.125 99.75 0.25
Graph 2.Semi-log graph for quarry dust particle size distribution
4.750 2.360 1.180 0.600 0.300 0.150 0.075 pan
Series1 100 99.625 86.5 74.625 55.25 30.25 13.375 0.25
0
20
40
60
80
100
120
PE
RC
EN
TA
GE
OF
FIN
ER
SIEVE OPENING IN mm
SIEVE ANALYSIS FOR QUARRY DUST
18
RESULT
Effective Size = 0.065mm
Fineness modulus = 3.40
Uniformity coefficient = 5.79
3.3 CEMENT
It is a binding material in concrete which binds the other materials to
forms a compact mass. Generally Ordinary Portland Cement is used for all
engineering construction works. In this project work, 53 grade OPC cement is
used for experimental study.
3.4 WATER
Clean, portable drinking water is available in the college campus is used
for casting and curing of bricks.
3.5 PULVERIZED WASTE PLASTIC POWDER
This waste powder is Polypropylene (PP) linear hydrocarbon
polymer, expressed as CnH2n. PP, like polyethylene and polybutene (PB), is a
polyolefin or saturated polymer. Polypropylene is one of those most versatile
polymers available with applications, both as a plastic and as a fibre, in virtually
all of the plastics end-use markets.
3.5.1 Properties
The properties of Polypropylene include...
Semi-rigid
Translucent
Good chemical resistance
Tough
Good fatigue resistance
Integral hinge property
19
Good heat resistance
PP does not present stress-cracking problems and offers excellent
electrical and chemical resistance at higher temperatures. While the properties
of PP are similar to those of Polyethylene, there are specific differences. These
include a lower density, higher softening point (PP doesn't melt below 160ºC,
Polyethylene, a more common plastic, will anneal at around 100ºC) and higher
rigidity and hardness. Additives are applied to all commercially produced
polypropylene resins to protect the polymer during processing and to enhance
end-use performance.
3.5.2 Physical Properties
Tensile Strength = 0.95 - 1.30 N/mm²
Notched Impact Strength = 3.0 - 30.0 KN/m²
Thermal Coefficient of expansion = 100 - 150 x 10-6
Max Cont Use Temp = 80 °C
Density = 0.905 g/cm³
3.5.3 Applications
Polypropylene can be processed by virtually all thermoplastic-processing
methods. Most typically PP Products are manufactured by: Extrusion Blow
Moulding, Injection Moulding, and General Purpose Extrusion. Expanded
Polypropylene (EPP) may be moulded in a specialist process.
3.5.4 Grade Selection
The choice of grade for any application is based on consideration of any,
or all, of the following points:
Homopolymer: stronger, stiffer - higher HDT
Copolymer: better impact, more transparent
20
MFI: ease of flow vs. toughness.
3.5.5 Advantages
Good chemical resistance. Good fatigue resistance. Better temperature
resistance than HDPE. Lower density than HDPE.
3.5.6 Disadvantages
Oxidative degradation is accelerated by contact with certain materials,
e.g. copper. High mould shrinkage and thermal expansion. High creep. Poor
U.V. resistance.
3.5.7 Applications
Buckets, bowls, crates, toys, medical components, washing machine
drums, battery cases, bottle caps. Elastomer modified for bumpers, etc. Talc
filled for additional stiffness at elevated temperatures - jug kettles, etc. OPP
films for packaging (e.g. crisps, biscuits, etc.). Fibres for carpets, sports
clothing.
3.5.8 PH test
Objective
This test method is the procedure for determining the PH of plastic
waste powder samples by use of a PH meter.
Apparatus and Materials
A 0.1 pt. (50 ml), wide-mouth glass beaker with a watch glass for
cover.
A PH meter, suitable for laboratory or field analysis, with either
one or two electrodes.
Standard buffer solutions of known PH values - standards to be
used are PH of 4.0, 7.0, and 10.0.
Distilled water.
21
A teaspoon or small scoop.
A thermometer capable of reading 77±18°F (25±10°C) to the
nearest 0.1°C.
A ¼ in. (6.3 mm) sieve conforming to the requirements of
AASHTO Designation M-92-91 (excluding Column 7, pg. 87) and
a pan.
A glass stirring rod.
A scale, minimum capacity of 1.1 lb. (500 g). It shall be accurate to
0.1% and be readable to 0.1 g.
Procedure
The material must be separated on the ¼ in. (6.3 mm) sieve. Only
the minus ¼ in. (6.3 mm) material is to be used for testing.
Weigh and place 30±0.1 g of soil into the glass beaker.
Add 30±0.1 g of distilled water to the soil sample. Stir to obtain a
soil slurry and then cover with watch glass.
The sample must stand for a minimum of one hour, stirring every
10 to 15 minutes. This is to allow the PH of the soil slurry to
stabilize.
The electrode(s) require immersion 30 seconds or longer in the
sample before reading to allow the meter to stabilize. If the meter
has an auto read system, it will automatically signal when
stabilized.
Read and record the PH value to the nearest tenth of a whole number.
22
TABLE 3.7 : pH TEST RESULT
SAMPLE NO VALUE
1 8.26
2 8.34
3 8.30
Mean value 8.30
Result
pH value of given PWP powder sample is 8.30.
This value is adoptable for construction. Limitation of pH value at any material
is 6.0 to 10.
23
PROCESS OF MOULDING
4. GENERAL
In this experimental work, the standard size of brick mould used in this
project is 220mm X 100mm x75mm. The average amount of water is used for
mixing. Mixing is made by hand mixing. Various proportions of PWP
(pulverized waste plastic) powder are 0%,5%, 10%, 15% and 20% is added with
OPC.
4.1 COLLECTION OF MATERIAL
First all the proportions are weighed. Clean the surface without any dirt,
for mixing of all materials in proper proportions. Then the mix has done with
using trowel. Add water 10 to 15% to the mix proportion. Before mixing the
PWP powder was sieved in IS 2.36mm.
4.2 MIXING
The five different types of mixtures are prepared to the requirement of BS
6073 in laboratory trials. The water proportions in the mixes are taken as
constant to determine the effect of various combinations of fly ash and PWP
powder.
Fly ash (55%)
Quarry dust (35%)
Cement (OPC) (10%)
Pulverized Waste Plastic (PWP) Powder
4.2.1 PROPORTIONING OF RAW MATERIALS
Proportioning of raw materials in an important aspect of ensuring
quality of ash bricks. The Proportioning will depend on the quality of raw
24
materials and the class of brick required. The following mix proportion is
being adopted by various types.
4.2.2 CALCULATION OF MIX PROPORTIONS
1) NOMINAL FLYASH BRICK (5% PWP POWDER ADDED BRICK)
100% = 100kg
Fly Ash 55% = 55kg
Quarry Dust 35% = 35kg
Cement 10% = 10kg
PWP POWDER 0% = 0kg
TOTAL = 100kg
2) COMPOSITE BRICK (5% PWP POWDER ADDED BRICK)
Flyash (55x95%) = 52.25% = 52.25kg
Quarry Dust (35x95%) = 33.25% = 33.25kg
Cement (10x95%) = 9.5% = 9.5kg
PWP Powder 5.0% = 5.0kg
Total = 100.0kg
3) COMPOSITE BRICK (10% PWP POWDER ADDED BRICK)
Fly Ash (55X90%) = 49.5% = 49.50kg
Quarry Dust (35X90%) = 31.5% = 31.50kg
Cement (10X90%) = 9.0% = 9.00kg
PWP Powder 10% = 10.00kg
Total = 100.00kg
25
4) COMPOSITE BRICK (15% PWP POWDER ADDED BRICK)
Flyash (55X85%) = 46.75% = 46.75kg
Quarry Dust (35X85%) = 29.75% = 29.75kg
Cement (10X85%) = 8.5% = 8.5kg
PWP Powder 15% = 15.00kg
Total = 100.00kg
5) COMPOSITE BRICK (20% PWP POWDER ADDED BRICK)
Flyash (55X80%) = 44.0% = 49.50kg
Quarry Dust (35X80%) = 28.0% = 31.50kg
Cement (10X80%) = 8.0% = 8.00kg
PWP Powder 20.0% = 20.00kg
Total = 100.00kg
TABLE 4.1 MIX PROPORTION FOR 3 BRICKS
S.NO MATERIALS SYMBOL
NOMINAL
FLYASH
BRICK
5% PWP
POWER
ADDED
FLYASH
BRICK
10% PWP
POWER
ADDED
FLYASH
BRICK
15% PWP
POWER
ADDED
FLYASH
BRICK
20% PWP
POWER
ADDED
FLYASH
BRICK
1 FLYASH W1 5.775 5.486 5.198 4.910 4.620
2 QUARRY
DUST W2 3.675 3.492 3.302 3.124 2.940
3 CEMENT W3 1.050 0.998 0.945 0.893 0.840
4 PWP
POWDER W4 - 0.525 1.050 1.575 2.100
5 WATER L 1.750 1.850 1.850 1.850 1.850
4.3 CASTING OF BRICKS
The non-modular brick sample of size 220 X 100 X 75 mm. where
casting lab using the OPC, fly ash, PWP powder in the proper proportion. For
26
hand moulding, the mixed proportions is forced in the mould in such a way that
is fills all the corners of the mould. The proper compaction is must done. The
surplus mix was removed either by frame with and top surface was leveled.
Finally the mould is lifted up and raw bricks are left on the ground. Above
process repeated till sufficient raw bricks are ready when such bricks become
sufficiently dry for 2 minutes in direct sun light.
4.4 DRYING OF BRICKS
After the bricks are moulded they are dried. This is done on specially
prepared drying yards. Bricks are stacked in the yard 8 to 10 bricks in each row.
Bricks are dried for a period of 1 to 2 days. During drying it must be protected
from wind, rain. Sometimes bricks are dried artificially by hot gases from kiln.
But here is change of warping of bricks in case of artificial drying.
4.5 CURING OF BRICKS
Proper curing is done for 7 days to 14 days for require the strength of the
bricks.
27
RESULTS AND DISCUSSION
5.1 GENERAL
Checking the strength of bricks is vital in analyzing civil engineering
design. Engineers have to be very sure about strength and worthiness of basic
building unit i.e. Bricks.
5.2 TEST OF BRICKS
Following tests are performed to check the quality of bricks.
1. Compressive Strength Test
2. Absorption Test
3. Efflorescence Test
4. Structure Test
5. Soundness Test
7. Hardness Test
8. Dimensional tolerance
5.2.1 COMPRESSIVE STRENGTH TEST
AIM
To determine the compressive strength of bricks as per IS 3495
(Part 1) : 1992.
APPARATUS
Compression testing machine ,the compression plate of which shall have
ball seating in the form of portion of a sphere center of which coincides with the
centre of the plate.
SPECIMENS
Three numbers of whole bricks from sample collected should be taken
.the dimensions should be measured to the nearest 1mm.
28
PROCEDURE
Place the specimen with flat face s horizontal and mortar
filled face facing upwards between plates of the testing
machine.
Apply load axially at a uniform rate of 14 N/mm² per minute
till failure occurs and note maximum load at failure.
The load at failure is maximum load at which the specimen
fails to produce any further increase in the indicator reading
on the testing machine.
CALCULATION
TABLE 5.0 CLASS DESIGNATION OF BRICKS
CLASS DESIGNATION
AVERAGE WET COMPRESSIVE STRENGTH NOT
LESS THAN
N/mm² kg f/cm² ( Approx )
30 30 300
25 25 250
20 20 200
17.5 17.5 175
15 15 150
12.5 12.5 125
10 10 100
7.5 7.5 75
5 5 50
3.5 3.5 35
29
COMPRESSIVE STRENGTH TEST RESULT
TABLE 5.1 COMPRESSION TEST ON HAND MOULD CLAY BRICK
CLAY BRICKS COMPANY NAME: POWER BRICKS,COIMBATORE
S.No Sample
Description
Sample
Code
Weight
(kg)
Dimensions Compressive
Load
(KN)
Compressive
Strength
(N/mm²) Length Width Depth
1 Hand Mould H8 3.280 220 105 75 110.6 4.79
2 Hand Mould H9 3.245 225 105 75 94.7 4.01
3 Hand Mould H10 3.235 220 105 75 116.9 5.06
Mean 4.62
TABLE 5.2 COMPRESSION TEST ON CLAY BRICKS IN MACHINE
MOULD
CLAY BRICK IN MACHINE MOULD COMPANY NAME: POWER BRICKS,COIMBATORE
S.No Sample
Description
Sample
Code
Weight
(kg)
Dimensions Compressive
Load
(KN)
Compressive
Strength
(N/mm²) Length Width Depth
1 Machine Mould M4 3.225 220 105 75 170.6 7.39
2 Machine Mould M5 3.175 225 100 75 185.1 8.23
3 Machine Mould M6 3.280 220 105 75 176.9 7.66
Mean 7.76
TABLE 5.3 COMPRESSION TEST ON FLY ASH BRICK IN
HYDRAULIC MOULD
FLY ASH BRICK COMPANY NAME: INDIAN FLY ASH BRICKS,
COIMBATORE
S.No Sample
Description
Sample
Code
Weight
(kg)
Dimensions Compressive
Load
(KN)
Compressive
Strength
(N/mm²) Length Width Depth
1 Hydraulic Mould F1 2.760 220 110 75 125.6 5.19
2 Hydraulic Mould F2 2.810 220 110 75 115.7 4.78
3 Hydraulic Mould F3 2.785 220 110 75 120.4 4.98
Mean 4.98
30
TABLE 5.4.1 COMPRESSION TEST ON NOMINAL FLY ASH BRICK
(7 DAYS CURING)
NOMINAL FLY ASH BRICK (0% PWP POWDER ADDED)
S.No Sample
Description
Sample
Code
Weight
(kg)
Dimensions Compressive
Load
(KN)
Compressive
Strength
(N/mm²) Length Width Depth
1 Hand Mould P4 3.700 220 105 75 120.3 5.21
2 Hand Mould P5 3.510 225 105 75 124.6 5.27
3 Hand Mould P6 3.440 220 105 75 115.6 5.00
Mean 5.16
TABLE 5.4.2 COMPRESSION TEST ON NOMINAL FLY ASH BRICK
(14 DAYS CURING)
NOMINAL FLY ASH BRICK (0% PWP POWDER ADDED)
S.No Sample
Description
Sample
Code
Weight
(kg)
Dimensions Compressive
Load
(KN)
Compressive
Strength
(N/mm²) Length Width Depth
1 Hand Mould P7 3.265 220 105 75 166.6 7.21
2 Hand Mould P8 3.130 220 105 75 172.6 7.47
3 Hand Mould P9 3.250 220 105 75 185.4 8.03
Mean 7.57
TABLE 5.4.3 COMPRESSION TEST ON NOMINAL FLY ASH BRICK
(21 DAYS CURING)
NOMINAL FLY ASH BRICK (0% PWP POWDER ADDED)
S.No Sample
Description
Sample
Code
Weight
(kg)
Dimensions Compressive
Load
(KN)
Compressive
Strength
(N/mm²) Length Width Depth
1 Hand Mould P12 3.445 220 105 75 337.8 14.62
2 Hand Mould P13 3.255 220 105 75 325.6 14.10
3 Hand Mould P14 3.360 220 105 75 319.4 13.83
Mean 14.18
31
TABLE 5.5.1 COMPRESSION TEST ON COMPOSITE FLY ASH
BRICK 5% PWP POWDER ADDED AT 7 DAYS CURING
COMPOSITE FLY ASH BRICK
S.No Sample
Description
Sample
Code
Weight
(kg)
Dimensions Compressive
Load
(KN)
Compressive
Strength
(N/mm²) Length Width Depth
1 Hand Mould Q4 3.330 200 100 75 110.6 5.53
2 Hand Mould Q5 3.320 200 100 75 104.6 5.23
3 Hand Mould Q6 3.375 200 100 75 108.4 5.42
Mean 5.39
TABLE 5.5.2 COMPRESSION TEST ON COMPOSITE FLY ASH
BRICK 5% PWP POWDER ADDED AT 14 DAYS CURING
COMPOSITE FLY ASH BRICK
S.No Sample
Description
Sample
Code
Weight
(kg)
Dimensions Compressive
Load
(KN)
Compressive
Strength
(N/mm²) Length Width Depth
1 Hand Mould Q9 3.420 200 100 75 140.6 7.03
2 Hand Mould Q10 3.355 200 100 75 153.3 7.67
3 Hand Mould Q11 3.265 200 100 75 148.2 7.41
Mean 7.37
TABLE 5.5.3 COMPRESSION TEST ON COMPOSITE FLY ASH
BRICK 5% PWP POWDER ADDED AT 21 DAYS CURING
COMPOSITE FLY ASH BRICK
S.No Sample
Description
Sample
Code
Weight
(kg)
Dimensions Compressive
Load
(KN)
Compressive
Strength
(N/mm²) Length Width Depth
1 Hand Mould Q12 3.300 200 100 75 210.9 10.55
2 Hand Mould Q13 3.230 200 100 75 190.9 9.55
3 Hand Mould Q14 3.130 200 100 75 194.2 9.71
Mean 9.93
32
TABLE 5.6.1 COMPRESSION TEST ON COMPOSITE FLY ASH
BRICK 10% PWP POWDER ADDED AT 7 DAYS CURING
COMPOSITE FLY ASH BRICK
S.No Sample
Description
Sample
Code
Weight
(kg)
Dimensions Compressive
Load
(KN)
Compressive
Strength
(N/mm²) Length Width Depth
1 Hand Mould R1 2.645 200 100 75 104.2 5.21
2 Hand Mould R2 2.860 200 100 75 98.6 4.93
3 Hand Mould R3 2.940 200 100 75 105.4 5.27
Mean 5.14
TABLE 5.6.2 COMPRESSION TEST ON COMPOSITE FLY ASH
BRICK 10% PWP POWDER ADDED AT 14 DAYS CURING
COMPOSITE FLY ASH BRICK
S.No Sample
Description
Sample
Code
Weight
(kg)
Dimensions Compressive
Load
(KN)
Compressive
Strength
(N/mm²) Length Width Depth
1 Hand Mould R5 3.320 200 100 75 102.6 5.13
2 Hand Mould R6 3.145 200 100 75 110.2 5.51
3 Hand Mould R7 3.200 200 100 75 120.0 6.00
Mean 5.55
TABLE 5.6.3 COMPRESSION TEST ON COMPOSITE FLY ASH
BRICK 10% PWP POWDER ADDED AT 21 DAYS CURING
COMPOSITE FLY ASH BRICK
S.No Sample
Description
Sample
Code
Weight
(kg)
Dimensions Compressive
Load
(KN)
Compressive
Strength
(N/mm²) Length Width Depth
1 Hand Mould R10 3.090 200 100 75 164.7 8.24
2 Hand Mould R11 3.250 200 100 75 171.7 8.59
3 Hand Mould R12 3.140 200 100 75 168.4 8.42
Mean 8.41
33
TABLE 5.7.1 COMPRESSION TEST ON COMPOSITE FLY ASH
BRICK 15% PWP POWDER ADDED AT 7 DAYS CURING
COMPOSITE FLY ASH BRICK
S.No Sample
Description
Sample
Code
Weight
(kg)
Dimensions Compressive
Load
(KN)
Compressive
Strength
(N/mm²) Length Width Depth
1 Hand Mould S4 3.265 200 100 75 100.2 5.01
2 Hand Mould S5 3.130 200 100 75 98.0 4.90
3 Hand Mould S7 3.250 200 100 75 112.4 5.62
Mean 5.18
TABLE 5.7.2 COMPRESSION TEST ON COMPOSITE FLY ASH
BRICK 15% PWP POWDER ADDED AT 14 DAYS CURING
COMPOSITE FLY ASH BRICK
S.No Sample
Description
Sample
Code
Weight
(kg)
Dimensions Compressive
Load
(KN)
Compressive
Strength
(N/mm²) Length Width Depth
1 Hand Mould S8 3.125 200 100 75 125.6 6.28
2 Hand Mould S10 3.060 200 100 75 129.9 6.50
3 Hand Mould S11 3.015 200 100 75 108.1 5.41
Mean 6.06
TABLE 5.7.3 COMPRESSION TEST ON COMPOSITE FLY ASH
BRICK 15% PWP POWDER ADDED AT 21 DAYS CURING
COMPOSITE FLY ASH BRICK
S.No Sample
Description
Sample
Code
Weight
(kg)
Dimensions Compressive
Load
(KN)
Compressive
Strength
(N/Mm²) Length Breadth Depth
1 Hand Mould S12 3.055 200 100 75 132.7 6.64
2 Hand Mould S13 3.020 200 100 75 143.4 7.17
3 Hand Mould S14 3.105 200 100 75 152.9 7.65
Mean 7.15
34
TABLE 5.8.1 COMPRESSION TEST ON COMPOSITE FLY ASH
BRICK 20% PWP POWDER ADDED AT 7 DAYS CURING
COMPOSITE FLY ASH BRICK
S.No Sample
Description
Sample
Code
Weight
(kg)
Dimensions Compressive
Load
(KN)
Compressive
Strength
(N/mm²) Length Width Depth
1 Hand Mould T4 2.945 200 100 75 89.0 4.45
2 Hand Mould T5 2.965 200 100 75 92.4 4.62
3 Hand Mould T6 2.890 200 100 75 88.6 4.43
Mean 4.50
TABLE 5.8.2 COMPRESSION TEST ON COMPOSITE FLY ASH
BRICK 20% PWP POWDER ADDED AT 14 DAYS CURING
COMPOSITE FLY ASH BRICK
S.No Sample
Description
Sample
Code
Weight
(kg)
Dimensions Compressive
Load
(KN)
Compressive
Strength
(N/mm²) Length Width Depth
1 Hand Mould T7 2.785 200 100 75 118.2 5.91
2 Hand Mould T8 2.670 200 100 75 110.8 5.54
3 Hand Mould T9 2.720 200 100 75 101.6 5.08
Mean 5.51
TABLE 5.8.3 COMPRESSION TEST ON COMPOSITE FLY ASH
BRICK 20% PWP POWDER ADDED AT 21 DAYS CURING
COMPOSITE FLY ASH BRICK
S.No Sample
Description
Sample
Code
Weight
(kg)
Dimensions Compressive
Load
(KN)
Compressive
Strength
(N/Mm²) Length Breadth Depth
1 Hand Mould T10 2.700 200 100 75 122.7 6.14
2 Hand Mould T11 2.610 200 100 75 137.1 6.86
3 Hand Mould T12 2.605 200 100 75 128.9 6.45
Mean 6.48
35
TABLE 5.9 COMPRESSIVE STRENGTH OF COMPOSITE BRICKS
S.No Sample 7 Days 14 Days 21 Days
1
0%
5.21 7.21 14.62
2 5.27 7.47 14.10
3 5.00 8.03 13.83
4
5%
5.53 7.03 10.55
5 5.23 7.67 9.55
6 5.42 7.41 9.71
7
10%
5.21 5.13 8.24
8 4.93 5.51 8.54
9 5.27 6.00 8.42
10
15%
5.01 6.28 6.64
11 4.90 6.50 7.17
12 5.62 5.41 7.65
13
20%
4.45 5.91 6.14
14 4.62 5.54 6.86
15 4.43 5.08 6.45
GRAPH 5.1 SHOWS COMPRESSIVE STRENGTH OF COMPOSITE BRICKS
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
7 Days 5.21 5.27 5.00 5.53 5.23 5.42 5.21 4.93 5.27 5.01 4.90 5.62 4.45 4.62 4.43
14 Days 7.21 7.47 8.03 7.03 7.67 7.41 5.13 5.51 6.00 6.28 6.50 5.41 5.91 5.54 5.08
21 Days 14.62 14.10 13.83 10.55 9.55 9.71 8.24 8.54 8.42 6.64 7.17 7.65 6.14 6.86 6.45
0.00
2.00
4.00
6.00
8.00
10.00
12.00
14.00
16.00
CO
MP
RES
SIV
E ST
REN
GTH
in N
/mm
²
SAMPLE - 0% | 5% | 10% | 15% | 20%
COMPRESSIVE STRENGTH OF BRICKS
36
TABLE 5.10 COMPRESSIVE STRENGTH COMPARISON OF
CONVENTIONAL BRICKS COMPOSITE BRICKS
S.NO SAMPLE TYPE COMPRESSIVE
STRENGTH N/mm²
% INCREASE IN
COMPRESSIVE
STRENGTH
1 CLAY BRICK HAND MOULD 4.62 -
2 CLAY BRICK MACHINE MOULD 7.76 67.97
3 FLYASH BRICK IN HYDRAULIC
MOULD 4.98 7.79
4 COMPOSITE BRICK (20% PWP
POWDER) IN HAND MOULD 6.48 40.26
GRAPH 5.2 SHOWS COMPRESSIVE STRENGTH COMPARISON OF
CONVENTIONAL BRICKS AND COMPOSITE BRICKS
5.2.2 WATER ABSORPTION TEST
Aim
Determination of water absorption of bricks as per IS 3495
(Part-2) : 1992.
Apparatus
A sensitive balance capable of weighing within 0.1 percent of the
mass of the specimen and a ventilated oven.
0123456789
CLAY BRICKHAND MOULD
CLAY BRICKMACHINEMOULD
FLYASH BRICK INHYDRAULIC
MOULD
COMPOSITEBRICK (20% PWP
POWDER) INHAND MOULDC
OM
PR
ESSI
VE
STR
ENG
TH I
N N
/mm
²
SAMPLE TYPE
COMPRESSIVE STRENGTH
37
Preconditioning
• Dry the specimen in a ventilated oven at a temperature of 105 to
115°C till it attains sub-stantially constant mass.
• Cool the specimen to room temperature and obtain its weight
(M1). Specimen warm to touch shall not be used for the
purpose.
Procedure
• Immerse completely dried specimen in clean water at a temperature
of 27 ± 2°C for 24 hours.
• Remove the specimen and wipe out any traces of water with a
damp cloth and weigh the specimen.
• Complete the weighing 3 minutes after the specimen has been
removed from water (M2).
Water absorption, percent by mass, after 24-hour immersion in cold water
is given by the following formula:
Water absorption in % = (W2 – W1)/W1 x 100
WATER ABSORPTION TEST REPORT
TABLE 5.11.1 WATER ABSORPTION TEST ON CONVENTIONAL
CLAY BRICK
Clay Brick In Hand Mould Power Bricks, Coimbatore
S.No Sample
Description
Sample
Code
Initial
Weight
(W1) kg
Final
Weight
(W2) kg
Water
Absorption
%
1 Hand Mould H1 3.305 3.725 12.71
2 Hand Mould H2 3.305 3.710 12.25
3 Hand Mould H3 3.280 3.680 12.20
Mean 12.39
38
TABLE 5.11.2 WATER ABSORPTION TEST ON CONVENTIONAL
CLAY BRICK
Clay Brick In Machine Mould Power Bricks, Coimbatore
S.No Sample
Description
Sample
Code
Initial
Weight
(W1) kg
Final
Weight
(W2) kg
Water
Absorption
%
1 Machine Mould M1 3.400 3.815 12.21
2 Machine Mould M2 3.290 3.655 11.09
3 Machine Mould M3 3.320 3.705 11.60
Mean 11.63
TABLE 5.11.3 WATER ABSORPTION TEST ON CONVENTIONAL
FLYASH BRICK
Fly ash Brick In Hydraulic
Mould Indian Fly ash Bricks, Coimbatore
S.No Sample
Description
Sample
Code
Initial
Weight
(W1) kg
Final
Weight
(W2) kg
Water
Absorption
%
1 Hydraulic Mould F6 2.780 3.015 8.45
2 Hydraulic Mould F7 2.750 2.945 7.09
3 Hydraulic Mould F8 2.810 3.015 7.30
Mean 7.61
TABLE 5.11.4 WATER ABSORPTION TEST ON COMPOSITE
FLYASH BRICK (0% PWP POWDER ADDED)
Nominal Fly Ash Brick
S.No Sample
Description
Sample
Code
Initial
Weight
(W1) kg
Final
Weight
(W2) kg
Water
Absorption
%
1 Hand Mould P1 3.445 3.710 7.69
2 Hand Mould P2 3.560 3.840 7.87
3 Hand Mould P3 3.470 3.745 7.93
Mean 7.83
39
TABLE 5.11.5 WATER ABSORPTION TEST ON COMPOSITE
FLYASH BRICK (5% PWP POWDER ADDED)
Composite Fly Ash Brick
S.No Sample
Description
Sample
Code
Initial
Weight
(W1) kg
Final
Weight
(W2) kg
Water
Absorption
%
1 Hand Mould Q1 3.060 3.280 7.19
2 Hand Mould Q2 3.040 3.245 6.74
3 Hand Mould Q3 3.040 3.230 6.25
Mean 6.73
TABLE 5.11.6 WATER ABSORPTION TEST ON COMPOSITE
FLYASH BRICK (10% PWP POWDER ADDED)
Composite Fly Ash Brick
S.No Sample
Description
Sample
Code
Initial
Weight
(W1) kg
Final
Weight
(W2) kg
Water
Absorption
%
1 Hand Mould R13 3.040 3.245 6.74
2 Hand Mould R14 2.985 3.190 6.87
3 Hand Mould R15 2.940 3.130 6.46
Mean 6.69
TABLE 5.11.7 WATER ABSORPTION TEST ON COMPOSITE
FLYASH BRICK (15% PWP POWDER ADDED)
Composite Fly Ash Brick
S.No Sample
Description
Sample
Code
Initial
Weight
(W1) kg
Final
Weight
(W2) kg
Water
Absorption
%
1 Hand Mould S1 2.785 2.955 6.10
2 Hand Mould S2 2.810 2.985 6.23
3 Hand Mould S3 2.805 3.005 7.13
Mean 6.49
40
TABLE 5.11.8 WATER ABSORPTION TEST ON COMPOSITE
FLYASH BRICK (20% PWP POWDER ADDED)
Composite Fly Ash Brick
S.No Sample
Description
Sample
Code
Initial
Weight
(W1) Kg
Final
Weight
(W2) Kg
Water
Absorption
%
1 Hand Mould T1 2.765 2.955 6.87
2 Hand Mould T2 2.655 2.810 5.84
3 Hand Mould T3 2.600 2.765 6.35
Mean 6.35
TABLE 5.12 WATER ABSORPTION TEST ON COMPOSITE BRICKS
S.No Percentage Of PWP Powder
Added
Water Absorption
%
1 0% 7.83
2 5% 6.73
3 10% 6.69
4 15% 6.49
5 20% 6.35
GRAPH 5.3 SHOWS WATER ABSORPTION ON COMPOSITE BRICKS
0
2
4
6
8
10
0% 5% 10% 15% 20%
WA
TE
R A
BS
OR
PT
ION
IN
%
PERCENTAGE OF PWP POWDER ADDED
WATER ABSORPTION
41
TABLE 5.13 WATER ABSORPTION TEST COMPARISON OF
CONVENTIONAL AND COMPOSITE BRICKS
S.NO SAMPLE TYPE WATER
ABSORPTION %
% OF DECREASE IN
WATER ABSORPTION
1 CLAY BRICK HAND MOULD 12.39 -
2 CLAY BRICK MACHINE MOULD 11.63 6.13
3 FLYASH BRICK IN HYDRAULIC
MOULD 7.61 38.58
4 COMPOSITE BRICK (20% PWP
POWDER) IN HAND MOULD 6.35 48.75
GRAPH 5.4 SHOWS WATER ABSORPTION COMPARISON ON CONVENTIONAL
AND COMPOSITE BRICKS
5.2.3 EFFLORESCENCE TEST
• The soluble salts if present in bricks cause efflorescence on the
surface of brick as per IS 3495 (Part 3) : 1992.
• Brick is immersed in water for 24hr. It is then taken out and allowed
to dry in shade. The absence of grey or white deposits on its surface
indicates absence of soluble salts. Observation is made with naked
eyes and classified as below.
• Nil – Imperceptible efflorescence
• Slight – Deposit covers area < 10% of exposed area
0
2
4
6
8
10
12
14
CLAY BRICK HANDMOULD
CLAY BRICKMACHINE MOULD
FLYASH BRICK INHYDRAULIC MOULD
COMPOSITE BRICK(20% PWP POWDER)
IN HAND MOULD
WA
TER
AB
SOR
PTI
ON
IN
%
SAMPLE TYPE
WATER ABSORPTION %
42
• Moderate – deposit covers exposed area 10% to 50%
• Heavy – Deposit covers exposed area > 50%
• Serious – Deposits are heavy and powder or flake away the surface
TABLE 5.14 EFFLORESCENCE TEST REPORT
Conventional Brick (Hand Mould) Slight (less than 10%)
Conventional Brick (Machine Mould) Slight (less than 10%)
Fly Ash Brick (Hydraulic Mould) The grey deposit are less than 8%
Nominal Fly Ash Brick (0%) The grey deposit are less than 7%
Composite Fly Ash Brick (5%) The grey deposit are less than 7%
Composite Fly Ash Brick (10%) The grey deposit are less than 7%
Composite Fly Ash Brick (15%) The grey deposit are less than 6%
Composite Fly Ash Brick (20%) The grey deposit are less than 6%
5.2.4 STRUCTURE TEST
A specimen is broken and its structure is examined. It should be homogeneous,
compact, and free from defects e.g. lumps and holes, etc.
This test report all composite brick samples free from lumps and holes.
5.2.5 SOUNDNESS TEST
This test is performed by striking two specimen bricks with each other. The
bricks should not break and a clear ringing sound should be produced.
This test report all composite brick samples are produced clear ringing
sounds without any breaks.
43
5.2.6 HARDNESS TEST
This test is performed by making a scratch on brick surface with the help of
finger nail. If no impression is left on surface, the brick is considered to be
sufficiently hard.
This test report all composite brick samples are hard on surface.
5.2.7 DIMENSIONAL TOLERANCE
The dimensions of, modular bricks when tested as described above as per
procedure described in appendix A on page 155 shall be within the following
limits per 20 bricks.
For non-modular size as per IS13757 : 1993.
Length 4520 to 4680 mm (4600 ± 80 mm)
Width 2240 to 2160 mm (2200 ± 40 mm )
Height 1440 to 1360 mm ( 1400 ± 40 mm ) For 70 mm high bricks
Test report:
Length (20 bricks) = 4650 mm
Width (20 bricks) = 2165 mm
Height (20 bricks) = 160 cm for 75mm high brick
44
COMPARISON STATEMENT
Compressive strength of composite bricks are decrease in strength
increase of PWP powder added. The average compressive strength of composite
bricks are 6.48N/mm2 the class designation 5 as per IS 13757: 1993.
The compressive strength of composite 20% PWP powder added fly ash
bricks are 40% more than conventional clay brick and 30% more than
conventional clay brick. The water absorption of composite 20% PWP powder
added fly ash bricks are 48% less than conventional clay brick and 16% less
than conventional clay brick.
Fly-Ash bricks are eco-friendly as it protects environment though
conservation of top soil and utilization of waste products of coal or lignite used
in thermal power plants. It is three times stronger than the conventional burnt
clay bricks. It plays a vital role in the abatement of carbon dioxide a harmful
greenhouse gas mass emission of which is threatening to throw the earth’s
atmosphere out of balance. Being lighter in weight as compared to conventional
bricks, dead load on the structure is reduced and hence saving is overall cost of
construction.
The possibility of using innovative building materials and eco-friendly
technologies, more so covering waste material like plastic and fly ash is the
need of the hour. Fly ash affects the plastic properties of bricks by improving
workability, reducing water demand, reducing segregation and bleeding, and
lowering heat of hydration. It also increases strength, reduces permeability,
reduces corrosion of reinforcing steel, increases sulphate, resistance when
compared to the conventional bricks.
45
CONCLUSION
Based on limited experimental investigations concerning compressive strength
of Brick, the following observations are made regarding the resistance of adding
PWP powder:
Compressive strength decreases on increase in percentage of PWP
Powder as compare to fly ash.
Use of PWP Powder in brick can solve the disposal problem; reduce cost
and produce a ‘greener’ Ecofriendly bricks for construction.
Environmental effects of wastes and disposal problems of waste can be
reduced through this research.
A better measure by an innovative Construction Material is formed
through this research.
It provides innovative use of class F fly ash which contains less than
20%lime.
This study helps in converting the non-valuable PWP Powder ash into
bricks and makes it valuable.
46
REFERENCES
Mucahit S, Sedat A. The use of recycled paper processing residue in
making porous brick with reduced thermal conductivity. Ceram Int
2009;35:2625–31.
S.P. Raut a,b, Rohant Sedmake c, Reuse of recycle paper mill waste in
energy absorbing light weight bricks
Faria, K. C. P., Gurgel, R. F. and Holanda, J. N. F., Recycling of
sugarcane bagasse ash waste in the production of clay bricks. J. Environ.
Manage., 2012, 101, 7–12.
Sengupta, P., Saikia, N. and Borthakur, P., Bricks from petroleum
effluent treatment plant sludge:properties and environmental
Shakir, A. A., Naganathan, S. and Mustapha, K. N., Properties of bricks
made using fly ash, quarry dustand billet scale. Constr.Build. Mater.,
2013, 41, 131–138.
Amrilphale, S. S. and Patel, M., Utilization of red mud, fly ash for
manufacturing bricks with pyrophyllite. Silic. Ind., 1987, 52(3-4), 31–35.
Om Prakash (1990), “Utilization of Pulverized (Fertilizer Plant) Fly Ash
as Low-Cost Bricks and ConstructionMaterial” M. Tech. Thesis
Submitted to MNREC, Allahabad.
47
IS CODE REFERENCE
IS: 3495-1992 (Part 1 to 4), “Methods of Tests for Burnt Clay Bricks”,
Bureau of Indian Standards, Third Revision, New Delhi.
IS: 383-1970, “Specification for coarse and fine aggregates from natural
sources for concrete”, Bureau of Indian Standards. New Delhi.
IS: 8112-1989, “Specification for 43grade Ordinary Portland Cement”,
Bureau of Indian Standards. New Delhi.
IS: 1077-1992, “Common burnt clay building bricks – Specification”,
Bureau of Indian Standards. New Delhi.
48
PROJECT PHOTOS
1. COLLECTION OF MATERIALS
Figure 1: Fly ash “F” class Figure 2 : Quarry Dust
Figure 3 : OPC 53 Grade cement (Dalmia) Figure 4 : PWP powder (Polypropylene)
2. PROCESS OF BRICK MOULDING
Figure 5 : PWP Powder was sieved before mixing
49
Figure 6 : Mixing of raw materials Figure 7 : Dry mixing of raw material
Figure 8 : Wet mixing of raw materials Figure 9 : Moulding of bricks
Figure 10 : Air drying process Figure 11 : Curing process
50
3.TESTING OF BRICKS
3.1 COMPRESSION TEST
Figure 12 : Compression test for clay brick in hand mould (sample code H10)
Figure 13 : Compression test for clay brick in machine mould (sample code M4)
Figure 14 : Compression test for fly ash brick in hydraulic mould (sample code F2)
51
Figure 15 : Compression test for nominal fly ash brick in hand mould (sample code P12)
Figure 16 : Compression test on composite fly ash brick 10% PWP powder (sample
code R11)
3.2 WATER ABSORPTION TEST
Figure 17 : water absorption test (before and after immersion of water)
52
3.3 EFFLORESCENCE TEST
Figure 18 : During efflorescence test Figure 19 : after 24 hrs on efflorescence test
3.4 STRUCTURE TEST
Figure 20 : Nominal bricks Figure 21 : 5% Composite bricks
Figure 22 : 10% Composite bricks Figure 23 : 20% Composite bricks
53
3.5 SOUNDNESS TEST
Figure 24 : During soundness test
3.6 HARDNESS TEST
Figure 25 : During hardness test
3.7 DIMENSION AND TOLERANCE TEST
Figure 26 : Dimension test for length wise
54
Figure 27 : Dimension test for width wise
Figure 28 : Dimension test for depth wise