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    INVESTIGATION OF TESTING METHODS TO DETERMINE LONG-TERM

    DURABILITY OF WISCONSIN NATURAL AGGREGATE RESOURCES

    GREGORY S. WILLIAMSONGraduate Student in Civil and Environmental Engineering, Virginia Polytechnic Institute and State University

    Blacksburg, VA, USA

    RICHARD E. WEYERS, Ph.D.Professor in Civil and Environmental Engineering, Virginia Polytechnic Institute and State University

    Blacksburg, VA, USA

    DAVID W. MOKAREM, Ph.D.

    Research Scientist, Virginia Transportation Research Council

    Charlottesville, VA, USA

    DANIEL S. LANE

    Research Scientist, Virginia Transportation Research Council

    Charlottesville, VA, USA

    ABSTRACT

    The Wisconsin Department of Transportation (WisDOT) uses approximately 11,000,000

    tons of aggregate per year for transportation projects. Therefore, being able to select durable

    aggregates for use in transportation projects is of considerable importance. If the aggregate

    deteriorates then the constructed facility will require premature repair, rehabilitation or

    replacement. Realizing the importance aggregate durability and also those deficiencies in the

    current WisDOT testing protocol may exist, it has been concluded that the durability-testing

    protocol for Wisconsin aggregates needs to be updated.

    This project has identified recent advances in the understanding and testing of aggregate

    durability. An in depth literature review was conducted and from the compiled information a

    laboratory testing program was developed.

    From the test results it was found that the WisDOT aggregate testing protocol could be

    reduced substantially by eliminating many of the testing requirements for aggregates that have

    vacuum saturated absorptions of less than 2%. The Micro-Deval abrasion test is recommended

    for inclusion in WisDOT testing protocols as a test to measure the abrasion resistance of

    aggregate while the L.A. Abrasion test is better suited as a measure of aggregate strength.

    Additional conclusions were made based on the durability testing conducted and an overall

    testing protocol was developed.

    Keywords: aggregate, durability, soundness, abrasion resistance, aggregate strength

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    INTRODUCTION

    Aggregate is the most fundamental component of construction. It is used as an unbound

    or lightly bound material in base courses and as a bound material in bituminous and Portland

    Cement Concretes (PCC). Aggregate constitutes in excess of 90% of the volume of base courses

    and bituminous concrete and 60 to 80% of the volume of Portland cement concrete. Aggregate

    is exposed to a number of physical and chemically degrading forces during processing,

    transporting, and construction as well as during the constructed facilitys life. As the main load-

    carrying component of unbound, bituminous concrete, and Portland cement concretes, if the

    aggregate fails, the facility fails to perform its design intent.

    Durability is a term used to define resistance to the chemical and physical forces of

    degradation to which a material is subjected throughout its service life. Given WisDOTs

    investment in its transportation infrastructure, it is important that the aggregate testing protocol

    be appropriate for the assessment of the long-term durability of constructed facilities. An ideal

    protocol would neither accept non-durable materials nor reject sufficiently durable materials.

    To ensure the durability of pavements and structures, WisDOT has used a number of test

    methods to assess aggregate quality and durability. The test methods include gradation,

    plasticity, resistance to abrasion (impact), soundness, and freezing and thawing resistance. Some

    of the tests have been developed as aggregate quality assurance tests and others have been

    borrowed from other materials testing programs. These tests have been in use for well over 50years and for the most part have served the highway industry well. However, these tests were

    developed when high quality natural sources of aggregate were abundant and social and political

    pressures on the use of industrial by-products and recycled/reclaimed materials were nonexistent.

    In addition, some of these tests have been kept in use in the name of tradition and simplicity

    rather than being replaced by other methods based on our ever-increasing understanding of the

    science of aggregate durability. In light of these changes and advances in technology, WisDOT

    sponsored a project to assess the adequacy of its aggregate testing protocol

    BACKGROUND

    The following discussion is presented to illustrate the underlying philosophy that was

    used to develop the WisDOT aggregate durability testing protocol.

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    WisDOT projects use aggregates as unbound pavement base courses, bituminous and

    PCC pavements and structural concretes for bridges, box culverts, and retaining walls. Each one

    of these facility components is exposed to a set of chemical and physical degrading forces during

    construction and throughout the facilitys service life. For example, structural Portland cement

    concrete aggregates are exposed to:

    Abrasive forces while the aggregate is in a moist/wet state during stock piling,

    transporting, batching, mixing, and placing of the concrete,

    Tensile, shear, and compressive stresses during loading of the reinforced concrete

    structure,

    Chemical environments of a saturated solution of calcium hydroxide, sodium and

    potassium hydroxide, and sulfates in the concrete,

    Wetting and drying cycles of the concrete, and

    Temperature changes including freezing and thawing of absorbed moisture of the

    concrete.

    With respect to temperature changes, an unconfined aggregate must be capable of

    handling the stresses that are developed due to water freezing within the aggregate pore

    structure. During the freezing of saturated aggregates bound together by Portland cement paste,

    the pressure being created by the freezing water must not be sufficient to fracture the aggregate

    nor be extruded into the surrounding cement paste at a rate which fractures the cement paste

    (1). Of these three potential aggregate freezing and thawing destructive mechanisms, two are

    related to the aggregate being bound within cement paste. An unbound aggregate test such as

    soundness or the freezing and thawing test would not assess these aggregate performance related

    aspects. This may be the reason why these tests have been poor predictors of the freezing and

    thawing durability of certain aggregate types. It is noteworthy that the expulsion distance

    mechanism may become more important in the future as more low permeable concretes are

    produced which have denser aggregate-paste transition zones.

    The above could be interpreted that it is necessary to test all concrete aggregates exposed to

    freezing and thawing under saturated conditions in a concrete freezing and thawing test. This

    will not be necessary because an aggregate with porosity below 0.3% produces expansions

    within the elastic limits of the aggregate and surrounding cement paste (1). Thus, a concrete

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    aggregate protocol may consist of a simple, precise test for water absorption and saturated

    specific gravity to identify the very good and very poor aggregates and a freezing and thawing or

    surrogate test for marginal aggregates.

    However, since the freezing and thawing of base courses takes place in the unbound state,

    the soundness test may be sufficient if the lack of precision aspects of this test can be addressed.

    Also, PCC pavement aggregates need to be assessed for the propensity of D-cracking (durability

    cracking), a somewhat different freezing and thawing property (2). D-cracking is cracking that

    occurs along the edges or at the corners of concrete slabs due to the expansion of non-durable

    coarse aggregates during freezing and thawing. The resulting deterioration is crescent shaped

    cracks or spalls in the concrete.

    Thus, the developed aggregate durability testing protocol is based on construction-service

    life performance criteria. The protocol is then based on performance tests, which will

    realistically simulate the field exposure and degradation process (3).

    EXPERIMENTAL METHODS

    Aggregate Performance Assessment Program

    Aggregate performance durability issues may be categorized as physical or chemical.

    Physical degradation mechanisms include:

    Attrition during handling and construction,

    Degradation under in-service loads, and

    Environmental degradation from freezing and thawing, wetting and drying, and/or

    thermal expansion and contraction.

    Chemical degradation mechanisms include the following but are not assessed in this study:

    Reactive oxides as CaO and MgO and sulfides as ferrous sulfide,

    Alkali-silica reaction, and

    Alkali-carbonate reaction.

    Aggregate performance properties have a direct influence on the stability of aggregate

    particles in the unbound and bound state. For example, an aggregate with a high porosity and

    low permeability defines the aggregates freezing and thawing critical size whether in the

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    unbound state or the bound state. An aggregate with a high porosity and high permeability may

    not fracture as an unbound material but will degrade the binding forces in bituminous and PCC.

    Thus, aggregate performance properties not only influence aggregate durability, but also the

    durability of their inclusion material. Therefore, the proposed aggregate testing program is

    presented for unbound, and bound aggregate such as bituminous concrete, PCC pavement, and

    structural elements and their associated durability performance parameters.

    Aggregate Physical Properties

    Aggregate physical durability properties are typically inter-related. For example, both

    freezing and thawing degradation mechanisms, aggregate fracture and degradation of binder-

    aggregate forces occur when the aggregate has a high porosity. Porosity and absorption are

    directly related, as are absorption and specific gravity. Aggregate that has a high specific gravitygenerally has a low absorption. These aggregates would generally have a high strength, high

    abrasion resistance, and a high resistance to dimensional changes. Relative to physical

    degrading forces, some aggregates may be accepted based on specific combinations of specific

    gravity and absorption. The physical performance characteristics of other aggregates may have

    to be determined by abrasion, strength, and freezing and thawing testing. Thus, the objective of

    the proposed testing program is to develop a tiered aggregate assessment protocol.

    Aggregate Chemical Properties

    While aggregate physical durability properties are generally inter-related, chemical

    degradation mechanisms are typically dependent upon the mineralogical composition of the

    aggregate. WisDOT officials have determined that chemical degradation mechanisms relating to

    aggregate mineralogy are not a significant problem in Wisconsin. Therefore, the proposed

    testing protocol does not contain any chemical durability testing.

    LABORATORY TESTING

    Current WisDOT Testing Protocol

    WisDOTs current aggregate durability testing protocol is presented below in Table 1:

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    Aggregate Test Selection

    Selection of the tests was based upon the tests precision, repeatability, efficiency, and

    predictive capabilities. Wisconsins current aggregate tests were also conducted for comparative

    purposes. The tests selected were as follows:

    Lightweight Pieces in Aggregate (ASTM C 123-98) (4)

    Vacuum Saturated Specific Gravity and Absorption (Coarse)(Modified - ASTM C 127)

    Sodium Sulfate Soundness (ASTM C 88) (4)

    Frost Resistance of Aggregates in Concrete (ASTM C 666) (4)

    Unconfined Freezing and Thawing of Aggregate (CSA A23.2-24A) (5)

    Micro-Deval Abrasion (Coarse) (AASHTO TP 58) (7)

    L.A. Abrasion (ASTM C 131-01) (4)

    Aggregate Crushing Value (British Standard 813-Part 3) (6)

    Crushed stone and gravel aggregates were all subjected to the same testing protocol. The

    use of the same testing procedures for all sources will increase efficiency and will also

    encompass the full spectrum of durability testing needs. Testing for Lightweight Pieces in

    Aggregate is an important screening test used to determine the percentage of non-durable

    aggregates for crushed stone and gravel samples, as excessive amounts of lightweight aggregate

    will result in a reduction in durability. The test for Vacuum Saturated Specific Gravity (VSSG)

    and Absorption (VSA) may be used as an indicator for aggregate soundness. VSSG and VSA

    testing was selected in place of standard SG and absorption testing because it is a better predictor

    of the long-term absorptions of aggregate in the field. Soundness tests that were investigated

    were the Sodium Sulfate Soundness (ASTM C88), Unconfined Freezing and Thawing of

    Aggregates (CSA A23.2-24A), and Frost Resistance of Aggregates in Concrete (ASTM C 666)

    tests.

    Unconfined Freezing and Thawing of Aggregate (CSA A23.2-24A) testing was carried out inplace of Soundness of Aggregates by Freezing and Thawing (AASHTO T 103) because it was

    recommended over AASHTO T 103 and the Sulfate Soundness Test by Senior and Rogers (8).

    The test has better precision and better correlation with field performance, which are among the

    reasons cited for its recommendation. Additionally, the Canadian test requires only 5 freezing

    and thawing cycles in comparison to the 25 required by AASHTO T 103.

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    Testing of the resistance of aggregates to abrasion was conducted using both the L.A.

    Abrasion test and the Micro-Deval test. The Micro-Deval test was selected because it can be

    applied to both fine and coarse aggregates, and recent reports have shown that test results

    correlate better with field performance records (9, 10, 11). Also, the L.A. Abrasion and Impact

    Test includes the effects of impact on the aggregate sample, thus both the effects of abrasion and

    impact are present in the test results. As a result, brittle aggregates may have a higher L.A.

    Abrasion loss do to the impact forces in the test. There is no clear understanding on how to

    interpret the results so that mass losses of the aggregate sample can be attributed to the abrasion

    resistance or the impact resistance of the aggregate. If the Micro-Deval test is used, another test

    must also be used to measure the aggregate strength. The British Aggregate Crushing test and

    the L.A. Abrasion test have been chosen to assess the strength of the aggregate.

    Although, not included in the testing program, aggregates which may be alkali carbonate

    or alkali silica reactive are to be tested in accordance with ASTM C 1293 (Determination of

    Length Change of Concrete Due to Alkali-Silica Reaction) (4). This recommendation is based

    on the results of the literature review (12).

    Laboratory Testing Program

    Seventy natural aggregate samples, representing the full range of aggregate available in

    Wisconsin, were collected for testing. Initially all 70 crushed stone and crushed gravel samples

    were tested for VSSG and VSA in a test procedure similar to ASTM C 127. The modification

    was to place the aggregate under a vacuum of 635 mm (25 in.) of mercury for 5 minutes prior to

    saturating the aggregates. Aggregate saturation consisted of the introduction of tap water while

    the aggregate was under vacuum and subsequent submersion in water for 24 +/- 1 hour. From

    these results 30 aggregates were selected for further analysis throughout the range of the VSA

    values. The selected aggregates were then subjected to the full suite of selected tests with one

    exception. Only nine aggregates were tested in concrete for freezing and thawing durability

    using ASTM C 666-97 (Resistance of Concrete to Rapid Freezing and Thawing) due to limited

    time and resources. ASTM procedure C 666-97 was modified to 28 days of curing in lime

    saturated water rather than the 14 days specified and the aggregate was saturated by soaking it in

    water for 24 hours prior to the mixing of the concrete. These modifications were carried out to

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    ensure complete saturation of the aggregate prior to freezing and thawing testing. This is

    intended to simulate the worst-case field condition.

    Selection of Aggregates

    With the assistance of WisDOT officials, 70 natural aggregate samples were selected for

    testing from across the state. Among the aggregates tested were unconsolidated deposits and

    bedrock from different geologic groups. A variety of glacial deposits were tested because the

    material often varies widely depending upon from which direction the depositing glacier

    originated. It was also important to test bedrock from groups with good and poor field

    performance ratings. The performance ratings of poor, intermediate, and good were based on

    either field performance or test results. The performance ratings were designated by WisDOT

    officials and should be verified due to their subjective nature. Figure 1 presents the sample sitelocations throughout the state of Wisconsin for both the pits and quarries.

    The importance of testing the range of aggregate durability performance based on field

    performance ratings cannot be over emphasized. It is often very easy to identify good and poor

    performing aggregates based on laboratory test results. It is much more difficult to identify

    aggregates that have adequate field performance histories but would be classified as intermediate

    aggregate based on laboratory testing.

    For the 30 aggregate samples that were selected for further testing it was important to

    ensure that the full range of aggregate qualities was reflected in the sample set with an emphasis

    on intermediate quality aggregates. The distribution of the aggregate samples tested was as

    follows: 7 Poor, 13 Intermediate, and 10 Good

    Once the sample distribution had been determined, the individual samples within the

    performance categories were selected based on VSA data, as there is a strong relationship

    between VSSG and VSA. Aggregates with low, moderate, and high absorption values were

    selected from each group in order to be certain that aggregate qualities can be identified without

    any dependence on absorption i.e. a poor aggregate with a low absorption can be identified as

    poor just the same as a poor aggregate with a high absorption.

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    TEST RESULTS

    Vacuum Saturated Specific Gravity and Absorption

    VSSGs and VSAs were determined for all 70 natural aggregate samples using the

    modified version of ASTM C 127. VSA was then plotted against VSSG to investigate the

    relationship (see Figure 2). The use of the VSA as a preliminary durability indicator will be

    investigated in comparisons with other test data. As shown, there is a general linear relationship

    between VSA and VSSG for carbonate rocks. The relationship was not investigated for

    igneous/metamorphic rocks because of their tendency to have low absorptions regardless of

    specific gravity. The siliceous granites and metamorphic aggregates have lower VSAs and

    VSSGs and are shown with VSAs of about 1% and VSSGs ranging between 2.55 and 2.65.

    Lightweight Particles in Aggregate

    The percentage of lightweight particles in aggregate was determined using WisDOT

    modified ASTM procedure 123-98. The ASTM procedure was modified to test only coarse

    aggregate material retained on the 3/8 in. sieve. WisDOT sets a limit of 5% and 2% chert, with a

    SSD specific gravity of less than 2.45, by mass for standard concrete and pre-stressed concrete,

    respectively. Chert is a white or buff colored siliceous material that is highly porous and non-

    durable. Freezing and thawing deterioration caused by chert tends to manifest itself in the form

    of popouts. The percentages of chert were determined by petrographic analysis from those

    aggregate samples that contained lightweight material (See Table 2).

    L.A. Abrasion

    L.A. Abrasion tests were performed using 500 revolutions in accordance with ASTM C

    131-01. Figure 3 presents the relationship between L.A. Abrasion and VSA. The failure limits

    are shown as solid lines. The dashed line represents the range for which all L.A. Abrasion values

    will lie for VSAs of less than 2%.

    As demonstrated, aggregate with VSAs of less than 2% will have a L.A. Abrasion value

    of less than 35%, which is substantially lower than the 50% loss failure criterion used by

    WisDOT. It should be noted that only one aggregate had a L.A. Abrasion value of greater than

    50%.

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    Micro-Deval

    Figure 4 presents the relationship between VSA and Micro-Deval % loss. A loss of 18%

    was used as the failure criterion as recommended by Kandhal and Parker for HMA (13).

    As demonstrated, a failure limit of 18% may be too stringent and a limit of 25-30% may

    be more appropriate for Wisconsin aggregate. Also, for aggregate with VSA less than 2% only

    one has a % loss greater than 12%. Therefore, it is reasonable to conclude that aggregate with

    VSA less than 2% will have a low Micro-Deval value.

    Aggregate Crushing Value

    Figure 5 presents the Aggregate Crushing Values of the aggregates tested with respect to

    VSA. The British Standard suggests that the allowable aggregate crushing loss should be based

    on the parent material. Average losses range from 16% for igneous material to 27% for

    argillaceous limestone.

    With no discernable relationship or recommended failure criteria it is not possible to

    draw any conclusions from this data. However, for aggregates with a VSA of less than 2%, the

    Aggregate Crushing Value is less than 22%.

    Strength and Abrasion Test Comparison

    A comparison of L.A. Abrasion and Micro-Deval test results demonstrated that there is a

    linear relationship although not a strong one (See Figure 6). Thus, it can be reasoned that the

    two tests are measuring different aggregate properties.

    Figure 7 presents the relationship between L.A. Abrasion and Aggregate Crushing Value.

    As shown, the two tests have a distinct correlation implying that the L.A. Abrasion test is more a

    test of aggregate strength than of abrasion resistance. The results indicate that it may be

    necessary to perform both the L.A. Abrasion Test and the Micro-Deval Test or possibly the

    Micro-Deval and Aggregate Crushing tests.

    The Micro-Deval, Aggregate Crushing Value, and L.A. Abrasion test results demonstrate

    that the tests are measuring different physical properties of the aggregate. The Micro-Deval Test

    measures the abrasion resistance of the aggregate while the L.A. Abrasion and Aggregate

    Crushing Value measure strength.

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    Sodium Sulfate Soundness

    Figure 8 presents the relationship between VSA and sodium sulfate soundness loss with a

    failure criterion of 12% loss, which is currently being used by WisDOT. There is no apparent

    correlation between the two data sets.

    As shown aggregates with VSA of less than 2% will have sulfate soundness losses of less

    than approximately 5%. It should also be noted that the soundness test was only able correctly

    identify 2 out of the 7 poor aggregates tested.

    Unconfined Freezing and Thawing

    Unconfined Freezing and Thawing of Aggregate tests were conducted in accordance to

    Canadian Standard A23.2-24A. The failure criterion is a 10% loss after five cycles of freezing

    and thawing, as stated in the Canadian Standards Association specification. Figure 9 presents the

    relationship between VSA and freezing and thawing loss.

    There is no apparent relationship between VSA and unconfined freezing and thawing

    loss. A full third of the aggregates tested were greater than the failure limit of 10%. Present

    WisDOT specifications for unconfined freezing and thawing limit the loss to 18% for AASHTO

    T 103, which is similar to the Candian Freeze/Thaw test. Thus, a 15% loss limit appears to be

    reasonable.

    Freezing and Thawing in Concrete

    The freezing and thawing of concrete specimens containing Wisconsin aggregate was

    conducted in accordance with ASTM C 666 (Resistance of Concrete to Rapid Freezing and

    Thawing). The failure criterion for ASTM C 666 is a reduction in the fundamental transverse

    frequency of greater than 40%. Due to time constraints only 9 of the 30 aggregates were tested.

    The aggregates selected for testing represented all three performance categories with samples

    having low, moderate, and high absorptions. Of the nine aggregate samples tested, none failed.

    The poorest performing aggregate reflected a 30% reduction in transverse frequency. It is useful

    to note, however, the deterioration that occurs throughout the test. Those aggregate samples

    containing chert resulted in more popouts in the concrete specimens, which is generally more of

    an aesthetics concern rather than a structural problem. It may be necessary to conduct freezing

    and thawing in concrete tests where lightweight aggregate particles are a concern because one

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    aggregate, sandstone containing in excess of 16% lightweight aggregate, disintegrated during

    the testing and left voids in the concrete where the aggregate once was.

    CONCLUSIONS AND RECOMMENDATIONS

    1. The absorption of an aggregate, while not directly related to the quality of the aggregate, can

    still be used as a preliminary indicator of durability. Aggregates with vacuum saturated

    absorptions of less than 2% do not need to be tested for L.A. Abrasion loss, Micro-Deval

    loss, Unconfined or Confined Freezing and Thawing tests. They will still, however, need to

    be tested for Lightweight Pieces in Aggregate.

    2. The inclusion of ASTM C 123 (Lightweight Pieces in Aggregate) in the WisDOT aggregate

    durability testing protocol is necessary in order to quantify non-durable lightweight material

    percentages. This is important particularly for gravel resources where high variability inparent material is common. The WisDOT pre-established maximum allowable chert

    percentages of 5% for normal concrete and 2% for pre-cast concrete are appropriate.

    However, rather than specifying only chert with a SSD specific gravity of less than 2.45, it

    would be best to limit all lightweight aggregate to 5%, and test those aggregates that fail in a

    confined freezing and thawing test. For concrete structures where aesthetics are a concern

    there should be no chert present in the aggregate to prevent popouts from occurring.

    3. The L.A. Abrasion test was only able to identify the very worst aggregate sample as being

    poor. This indicates that the L.A. Abrasion test does have some ability to predict

    performance. From this data it can be concluded that the L.A. Abrasion test cannot directly

    predict the overall performance of an aggregate, but it can accurately estimate a key

    parameter, aggregate strength. The L.A. Abrasion test should continue to be used to evaluate

    aggregate strength. Realizing that the Aggregate Crushing Value measures this same

    parameter, it is not recommended that the Aggregate Crushing Value test be implemented at

    this time.

    4. The Micro-Deval test (AASHTO TP 58) with the recommended maximum allowable loss

    limit of 18% rejects nearly 50% of all aggregates tested. It is clear, however, that more poor

    aggregates are accurately classified than with the L.A. Abrasion test. For Wisconsin

    aggregate it appears that a maximum allowable loss limit of 25% is more reasonable. The

    Micro-Deval test should be added to WisDOT testing protocol to evaluate the abrasion

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    resistance of aggregate, as this test more accurately models the degradation that occurs

    during handling and mixing.

    5. The Sodium Sulfate Soundness test (ASTM C 88) was able to correctly identify two out of

    seven poor aggregates without rejecting any intermediate or good aggregates. The problem

    with this test is that it is highly variable with a potential multi-laboratory difference between

    two tests of 116%.

    6. The Unconfined Freezing and Thawing test (A23.2-24A) data has no correlation with

    Sodium Sulfate Soundness results. Due to the poor precision of the sodium sulfate test, it is

    recommended that the unconfined freezing and thawing test be included in the WisDOT

    aggregate testing protocol with an upper limit of 15% loss.

    7. The Freezing and Thawing of Concrete test is recommended for aggregate that are to be used

    in the bound state. This test helps to identify non-durable aggregates that may result in

    popouts, aggregate deterioration, and cracking of concrete.

    PROPOSED TESTING PROTOCOL

    Based on the conclusions presented above proposed testing protocols have been

    developed for unbound and PCC aggregates and are presented in Figures 10 and 11, respectively.

    The testing protocols were developed with the aim of improving the aggregate durability testing

    program while also reducing the amount of testing required. The results of the proposed testing

    protocol in comparison with current WisDOT testing protocol are presented in Table 3. The

    proposed testing protocol rejected more of the poor performing aggregate samples while

    rejecting fewer good samples. Additionally, by using the proposed testing protocols the required

    L.A. Abrasion testing can be reduced by 37% and the Unconfined Freezing and Thawing testing

    can be reduced by 30% for the 30 aggregate samples tested.

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    REFERENCES

    1. Verbeck, G. and R. Landgren, Influence of Physical Characteristics of Aggregate on

    Frost Resistance of Concrete, Proceedings, ASTM, Vol. 60, pp. 1063-1079.

    2. Dubberke, W. and V. Marks, The Relationship of Aggregate Durability to TraceElement Content, Interim Report on Project HR-266, Iowa DOT, p. 12, Jan.

    1984.

    3. Frohnsdoff, G. and J. Clifton, Cement and Concrete Standards of the Future,

    Workshop on Cement and Concrete Standards Report, NIST, p. 48, Oct. 1995.

    4. ASTM, Annual Book of ASTM Standards. Vol. 04.02, ASTM, Philadelphia, PA,

    2002.

    5. CSA, Canada Materials and Methods of Concrete Construction/Methods of Test forConcrete: National Standards of Canada, CSA-A23.1-00 and CSA-A23.2-00,

    August 2001.

    6. British Standard, Testing Aggregates Part 110: Methods for determination of

    aggregate crushing value (ACV), BS 812-110 1990, 1998.

    7. AASHTO, 2000, Standard Specifications for Transportation Materials and Methods

    of Sampling and Testing. Part II Tests: 1136.

    8. Senior, S. A. and Rogers, C. A., 1991-2, Laboratory Tests for Predicting CoarseAggregate Performance in Ontario, Transportation Research Record 1301,

    Washington, D.C.

    9. Folliard, K.J. and Smith, K.D., 2003, Aggregate Tests for Portland Cement Concrete

    Pavements Review and Recommendations. National Cooperative Highway

    Research Program, Research Reports Digest No. 281, Transportation Research Board,

    Washington, D.C.

    10. Kandhal, P.S., and Parker, F., 1998, Aggregate Tests Related to Asphalt ConcretePerformance in Pavements. National Cooperative Highway Research Program,

    Report No. 405, Transportation Research Board, National Research Council,

    Washington, D.C.

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    11. Saeed, A., Hall, J. and Barker, W, 2001, Performance-related Tests of aggregates

    for Use in Unbound Pavement Layers. NCHRP Report # 453, National

    Academy Press, Washington, D.C.

    12. Williamson, G., Weyers, R. E., Mokarem, D., Lane, D., and Cady, P., Investigation

    of Testing Methods to Determine Long-Term Durability of Wisconsin Aggregate

    Resources Including Natural Materials, Industrial By-Products, and

    Recycled/Reclaimed Materials. August, 2005.

    13. Kandhal, P.S., and Parker, F., 1998, Aggregate Tests Related to Asphalt Concrete

    Performance in Pavements. National Cooperative Highway Research Program,

    Report No. 405, Transportation Research Board, National Research Council,

    Washington, D.C.

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    TABLES AND FIGURES

    Figure 1 Pit and Quarry LocationsFigure 2 Vacuum Saturated Absorption vs. Vacuum Saturated Specific Gravity

    Figure 3 Vacuum Saturated Absorption vs. L.A. Abrasion

    Figure 4 Vacuum Saturated Absorption vs. Micro-Deval

    Figure 5 Vacuum Saturated Absorption vs. Aggregate Crushing ValueFigure 6 L.A. Abrasion vs. Micro-Deval

    Figure 7 L.A. Abrasion vs. Aggregate Crushing Value

    Figure 8 Vacuum Saturated Absorption vs. Sodium Sulfate SoundnessFigure 9 Vacuum Saturated Absorption vs. Unconfined Freezing and Thawing

    Figure 10 Aggregate Durability Testing Flowchart for Unbound Aggregate

    Figure 11 Aggregate Durability Testing Flowchart for Bound Aggregate in PortlandCement Concrete

    Table 1 Current WisDOT Testing Protocol

    Table 2 Lightweight and Chert PercentagesTABLE 3 Current vs. Proposed Testing Protocol Comparison

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    Quarry

    Pit

    FIGURE 1 - Pit and Quarry locations

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    Vacuum Saturated Absorption vs. Vacuum Saturated Specific Gravity

    R2= 0.7539

    0

    1

    2

    3

    4

    5

    6

    7

    2.5 2.55 2.6 2.65 2.7 2.75 2.8 2.85 2.9 2.95 3

    Vacuum Saturated Specific Gravity

    VacuumS

    aturatedAbs

    orption

    Igneous/Metamorphic Carbonate Linear (Carbonate)

    FIGURE 2 - Vacuum Saturated Absorption vs. Vacuum Saturated Specific Gravity

    Vacuum Saturated Absorption vs. L.A. Abrasion

    R2= 0.572

    0

    1

    2

    3

    4

    5

    6

    7

    0 10 20 30 40 50

    L.A. Abrasion (% Loss)

    VacuumS

    aturatedAbsorption(%)

    60

    FIGURE 3 - Vacuum Saturated Absorption vs. L.A. Abrasion

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    Vacuum Saturated Absorpt ion vs . Micro-Deval

    R2= 0.8756

    0

    1

    2

    3

    4

    5

    6

    7

    0 5 10 15 20 25 30 35 40 45

    Micro-Deval (% Loss )

    VacuumS

    aturatedAbsorp

    tion(%)

    FIGURE 4 - Vacuum Saturated Absorption vs. Micro-Deval

    Vacuum Saturated Absorption vs. Aggregate Crushing Value (VT)

    R2= 0.547

    0

    1

    2

    3

    4

    5

    6

    7

    10 12 14 16 18 20 22 24 26 28

    Aggregate Crushing Value (% Los s)

    VacuumS

    aturatedAbsorpt

    ion(%)

    FIGURE 5 - Vacuum Saturated Absorption vs. Aggregate Crushing Value

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    L.A. Abrasion vs. Mic ro-Deval

    R2= 0.5623

    0

    10

    20

    30

    40

    50

    60

    0 5 10 15 20 25 30 35 40 45

    Micro-Deval (% Loss)

    L.A.

    Abrasion(%L

    oss

    )

    FIGURE 6 - L.A. Abrasion vs. Micro-Deval

    L.A. Abrasion vs . Aggregate Crushing Value (VT)

    R

    2

    = 0.794

    0

    10

    20

    30

    40

    50

    60

    10 12 14 16 18 20 22 24 26 28

    Aggregate Crushing Value (% Loss)

    L.A.

    Abrasion(%L

    oss)

    FIGURE 7 - L.A. Abrasion vs. Aggregate Crushing Value

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    Williamson, Weyers, Mokarem, and Lane 21

    FIGURE 8 - Vacuum Saturated Absorption vs. Sodium Sulfate Soundness

    FIGURE 9 - Vacuum Saturated Absorption vs. Unconfined Freezing and ThawingFIGURE 9 - Vacuum Saturated Absorption vs. Unconfined Freezing and Thawing

    Vacuum Saturated Absorption vs. Sodium Sulfate Soundness

    R2= 0.3249

    0

    1

    2

    3

    4

    5

    6

    7

    0% 5% 10% 15% 20% 25% 30% 35%

    Sodium Sulfate So

    VacuumS

    aturatedAbsorp

    tion(%)

    undness (% Loss)

    Vacuum Saturated Absorption vs.

    0

    1

    2

    3

    4

    5

    6

    7

    0 2 4 6

    Unconfined Freezing

    VacuumS

    aturatedAbsorption(%)

    Unconfined Freezing and Thawing

    R2= 0.1773

    8 10 12 14 16

    and Thawing (% Loss)

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    FIGURE 10 - Aggregate Durability Testing Flowchart for Unbound Aggregate

    Abs

    L.A. Micro

    % Lightweight >5%

    No

    Yes

    Yes

    REJECT

    ACCEPT

    A

    Yes

    Uncon

    S

    No

    Samples Accepted

    (Based on WisDOT

    performance ratings)

    Poor 2

    Intermediate 4

    Good - 5

    Samples Rejected

    (Based on WisDOT

    performance ratings)

    Poor 5

    Intermediate 2

    Good - 0

    Samples Accepted

    (Based on WisDOT

    performance ratings)

    Poor 0Intermediate 7

    Good - 5

    Unconfined F&T >15%

    Yes

    No

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    illiamson, Weyers, Mokarem, and Lane 23

    FIGURE 11 - Aggregate Durability Testing Flowchart for Bound Aggregate in P

    Absorption > 2

    L.A. Abrasion >Micro-Deval >2

    % Lightweight >5%

    Ye

    No

    Yes

    Yes

    REJECT

    ACCEPT

    ACCEPT

    N

    START

    No

    F&T C 666 > 40%

    reduction in Freq.

    excessive Agg. De

    Yes

    No

    Samples A

    (Based on Wi

    performa

    Poor 2

    Intermedia

    Good - 5

    ccepted

    sDOT

    nce ratings)

    te 4

    Samples Rejected

    (Based on WisDOT

    performance ratings)

    Poor 5Intermediate 2

    Good - 0

    Samples Accepted

    (Based on WisDOT

    performance ratings)

    Poor 0Intermediate 7

    Good - 5

    F&T C 666 > 40%

    reduction in Freq. or

    excessive Agg. Det.

    Yes

    No

    W

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    TABLE 1 Current WisDOT Testing Protocol

    Test Failure Criterion

    Lightweight Pieces in Aggregate (AASHTO T 113) (7) > 5% Chert

    Sodium Sulfate Soundness (AASHTO T 104) (7) > 12% Loss

    Soundness of Aggregates by Freezing and Thawing (AASHTO T 103) (7) > 18% Loss

    L.A. Abrasion (AASHTO T 96) (7) > 50% Loss

    Current WisDOT Testing Protocol

    TABLE 2 - Lightweight and Chert Percentages

    Sample # % Lightweight (3/8") % Chert Sample # % Lightweight (3/8") % Chert

    2 12.91 0.00 24 2.14 0.23

    4 0.00 0.00 55 4.62 1.62

    6 0.00 0.00 57 9.09 0.00

    8 2.25 0.21 59 9.20 0.00

    10 0.00 0.00 60 3.08 2.50

    50 16.19 0.00 31 8.38 1.78

    52 7.80 0.00 33 0.5 0.00

    11 3.41 1.58 36 0.00 0.00

    12 2.35 0.56 39 0.00 0.00

    13 0.5 0.00 40 3.86 3.86

    14 0.5 0.00 42 5.45 1.25

    16 0.5 0.00 48 4.79 0.65

    19 1.28 0.23 64 5.38 0.00

    21 0.5 0.00 68 0.95 0.85

    22 5.24 1.83 69 0.5 0.00

    TABLE 3 Current vs. Proposed Testing Protocol Comparison

    Aggregate

    Quality Rating Rejected Accepted Rejected Accepted

    Poor 3 4 5 2

    Intermediate 1 12 2 11

    Good 1 9 0 10

    Current WisDOT Testing Protocol Proposed Protocol