Quantitative Determination of Porosity by Active Thermography
Active Thermography Maierhofer
Transcript of Active Thermography Maierhofer
InnoTesting 2015 Active Thermography
Application of active thermography in production
processesChristiane Maierhofer, Mathias Ziegler, Rainer Krankenhagen,
Philipp Myrach, Florian JonietzBundesanstalt für Materialforschung und –prüfung
FB 8.7
Energy Infrastructure Environment Material
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Content
• Principle of active thermography• Actual research for applications in production
processes: theory and experiment� Planar excitation: Comparison of flash and lockin
thermography
� Light weight constructions
� Join connections
� Local excitation: crack characterisation
� Large structures: Windmill and building structures
• Outlook: Standardisation
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Principle of active thermography
Flash thermography of an airplane side rudder
• Reflection configuration using 4 flashes from the front side
• InSb IR camera, 640x512 pixel• 100 Hz frame rate• Subtraction of zero image• Measurement duration: 10 s
ca. 300x350 mm2
C. Maierhofer et al, Composites Part B57, 2014, 35-46
Reflection configuration
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Heating sources
• Flash lamp• Halogen lamp• Infrared radiator• LED-Array• Laser• Hot air• Ultrasonic sonotrode• Induction
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Theory
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Non-stationary heat conduction process in anisotropic solids is described by the proportionality of heat flux and temperature gradient using the heat equation (diffusion equation):
T: temperature: position vector
t: time
Heat equation
Solution of parabolic DE:• Spatial boundary conditions
(temperature or heat flux) have to be set
• Temporal starting conditions, i.e. temperature distribution at t = 0, have to be set
• Strong attenuation
Comparison to solution of hyperbolic DE (wave equation):• Spatial boundary conditions have to be
set• Two temporal starting conditions:
temperature distribution at t = 0 and first derivative to time
• Little attenuation
λ: therm. conductivityρ: densityc: spec. heat capacity
[ ] )(),()(),(
)()( rqtrTrt
trTrcr p +∇⋅∇=
∂∂ λρ
rq: introduced heat
per volume: nabla operator∇
InnoTesting 2015 Active Thermography
Theory of flash excitation
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Solution for Dirac pulse (flash excitation)
t
qtTe
t
qtzT tz
πεπεα == − ),0(,),( 42
1D, for semi infinite isotropic bodies
effusivity
diffusivity
cρλε =
max. traceable penetration depth Lmax depends on heat density , thermal sensitivity of IR camera (NETD) and spec. heat capacity (n=2 bis 3)NETDTnc
qL
∆⋅= 1
max ρ
Penetration depth L depends on time t and on diffusivity αtL απ=
Depth resolution ∆L depends on time resolution and thus on frame rate of the IR camerat
tLL ∆=∆
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cρλα =
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Testing of steel and copper
Comparison of penetration depths at similar ρρρρ and c(thermograms after subtraction of zero image)
copper
t = 0.11 ms t = 0.2 ms t = 0.47 ms
t = 0.5 ms t = 1.1 ms t = 3.2 ms
steel
Similar penetration depth of about 8 mm
FBH with 12 mm Ø and remaining wall thickness of 2, 4, 6 und 8 mm
Depth resolution in steel is 10x better as in cupper
TNS Project Flash Thermography >> Draft standard on flash thermography in DIN AA 062-08-27 AA Visual and thermographic testing
NETDTncq
L∆⋅
= 1max ρ
Cu steel
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3D Reconstruction: Inverse Solution
thermogram reconstruction
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back sidegeometry
z
front sidetemperature field
T(x, y, t)
inverse problemF-1(T) = z
?
direct problemF with F(z) = T
Regina Richter, DissertationTU Braunschweig, Dez. 2013
DFG-Project for reconstruction ofdamage, together with ZIBVh 8590, 2014-2017
pipe with corrosion
Wall thickness: 3.6 mm
Pre knowledge: Material parameters are known
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Objective: Determination of diameter of spot welds in reflection configuration without additional coating
M. Ziegler, IGF project Diatherm 17686 N / 1Project partner: BAM 9.3 Prof. Rethmeier
Visualisation of heat diffusion by projection of a laser line along the sample edge:P = 50 W v = 10 m/s t = 50 ms
Laser
Adhesive joint
Optimum
Diameter of spot welds
Adhesive joint
D = 2.33 mm
Optimum
D = 5.23 mm
Spatter limit
D = 6.12 mm
Full automation pf spot welding in automotive industrywww.kuka-systems.com
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Frame rate: 40 Hz
Intensity devolution at mid point
Division
Result: Good correction of inhomogeneous emissivity, radial symmetry can be recognized
� Data analysis is possible (e.g. full width at half maximum)
Diameter of spot welds
Thermogram at time of max. intensity , strong emissivity variations � no reasonable data analysis
Thermogram at the end of the sequence shows only emissivity differences (due to scratches, discoloration, pollution etc.)
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Validation at CFRP test specimen
Comparison of flash thermography and CT, specimen R 1
3rd layer1st layer
T R
x = 1.2 mmx = 0.48 mm
Set-up:120x120x2 mm3
5 layers 0°/90°CFRP fabric6k carbon fibre bundleEpoxy matrixDefects during production:Reinjected areaAdditional fibre bundleWooden stick
TT
CT
Cooperation with BAM 8.5 and Benteler SGLEC project Thermobot (www.thermobot.eu)
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2 cm∆x = 81 µm
∆x = 240 µm
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Comparison of flash thermography and CT, specimen R 3/4
3rd layer
x = 1.28 mm
Set-up:2 plates glued with 4 beadsDefects:Broken fibre bundleBeads:1: release agent2: without sand blasting3: o.k.4: wrong mixture
TT
CT
R
Phase image from mid
x = 2.1 mm
T3
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1
3
2
1
C. Maierhofer et al., Composites Part B, 64, 2014, 175-186
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2 cm
Validation at CFRP test specimen
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Theory of lockin excitation
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Solution for periodic heating(lockin excitation, thermal waves)
Penetration depth (or thermal diffusion length ) of thermal wave: • decreases with increasing frequency• Increases with increasing diffusivity
Phase velocity of thermal wave: • Increases with increasing frequency and
with increasing diffusivity
>> thermal waves have a high dispersion and high at tenuation>> broadening of heat impulses (multi frequency)
)4//(/0),( πω −−−− ⋅= µztiµz eeTtzT
ωα2=µ
ωαω 2=⋅= µv
1D, for semi infinite isotropic bodies
effusivity
diffusivity
cρλε =
cρλα =
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Comparison of flash/lockin thermography
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time
A
ϕ
FT(fA)
time
FT(f)A
ϕ
Flash thermography Lockin thermography
• Thermograms at raising or max. contrast• Pulse-Phase-Thermography (PPT)• Thermal signal reconstruction (TSR)
• Online FFT or 4 point method at excitation frequency
• Offline FFT at excitation frequency
f
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Comparison: 4.4 J impact damage in CFRP
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Frequency in Hz
1 Hz 0.1 Hz 0.05 Hz0.45 mm 0.63 mm 2 mm
Depth in mm
• Phase images at 1 Hz are similar• Phase images at lower frequency have less contrast for lockin
excitation• Possible reason: Material separation due to thermal expansion
is larger for flash excitation>> Comparison to laser speckle interferometry/shearography
C. Maierhofer, ECNDT 2014, Keynote, www.ndt.netCFRP samples from ZFL Haldensleben, Prof. Dr. J. Häberle, ZIM Kooperationsnetzwerk
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Comparison: Cu-Shunts am LHC, CERN
2 mm Cu sheet
3 mm Cu sheet
Flash
Lockin1 Hz20 P.
Flash
Lockin1 Hz20 P.
www.cern.ch
Cu-Shunts are supporting the connection of two cable heads
Customer: CERN, C. ScheuerleinC. Maierhofer et al, NDT&E International, 52, 2012, 103-111
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New excitation sources: LED -Array
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Stand atControl 2014
LEDcontrol Computer
IR camera
Photo-diode
Sample
M. Ziegler, MNPQ project, 2013-2014
Advantages of LED excitation source
� Can be modulated up to 1 kHz
� Narrow spectrum, no overlap with IR camera
InnoTesting 2015 Active Thermography
Current: Pores in aluminium
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Al pressure casting: rear axle carrier of the chassis of BMW i3
http://www.springerprofessional.de/, Hengst, BMW
Cooperation with Bergakademie TU Freiberg
Thermogram after flash
Phase image at 4.6 Hz
Section of a crankcase, Length150 mm, thickness 2 mm
KCT fromBAM 8.5
Lockin excitation at 8 HzLaser widening
U. Richter, C. Maierhofer, R. Mischke, M. Röllig, Int. Foundry Research, 2015, accepted
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Flash thermography Lockin thermography
Advantages:• Very short measurement time• Multi spectral
>> all penetration depth until Lmax
Disadvantages:• Strong thermal strain• less SNR especially at higher
penetration depths
Advantages:• Less thermal strain• Higher SNR at larger penetration depth• Higher frequencies (LED, LASER)• Depth selective
Disadvantages:• Much long measurement times• Each measurement is only optimized for one
penetration depth
time
A
ϕ
FT(fA)
time
FT(f)A
ϕ
f
Comparison of flash/lockin thermography
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Cracks and local excitation
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Characterisation of vertical cracks by heating with a laser spot
Joachim Schlichting, Dissertation, TU Berlin, 2012Adolf-Martens-Award 2013
Static laser spotDetermination of crack depth and crack angle is possible
Moved laser spotFast detection of shallow and
narrow cracks is possible
time
InnoTesting 2015 Active Thermography
Test parameters:• Scan speed: 12 mm/s
• Trace distance: 0.5 mm
• Scan time: 40 s• Power density: ~0.7 kW/cm² (9 W, 1.3 mm Spot Ø)
• Camera resol.: 39 µm/pixel
Calibration block 1 (aka MTU Nr. 3) Ø 50 mm:• Reference for MT (fluorescent) EN ISO 9934-2 Annex B • 90MnCrV8 steel, hardened, browned• Stress corrosion cracks and grinding cracks:
width: 0.1-5 µm, depth: 2 µm-1 mm, approved by microscopy
Reference specimen for magnetic particle testing
Sub-µm cracks are recognized! Below diffraction limit (~5 µm)
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Natural cracks
P. Myrach, M. Ziegler, C. Maierhofer, M. Kreutzbruck, AIP conference proceedings, QNDE, 1581, 2014, 1624-1630
INS Project Laser-Thermography M. Ziegler
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Testing of large scaled structures
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Objective:Testing and
inspection withoutscaffolding and
access aids
Building facades
Funded by
Rotor blades of windmills
VIP-Project IKARUS, BMBF R. Krankenhagen
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Testing of rotor blades
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Cross section of a rotor blade
leading edge
trailing edge
beam
foamFull GFRP
Adhesive defects
Which structures and which defects and inhomogeneities can be detected with active thermography?
18 to 22 °C
Project IKARUS (Funding program VIP of BMBF, FKZ 03V0135, 2011-2015):Infrared-Kameratechnology for non-touching Analysis of Rotor blades under Offshore conditions
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10 p.m.
~ 180 cm
~ 20
0 cm• Segment of a rotor blade with natural and
artificial defects and inhomogeneities• Comparison of measurements and numerical
simulations under different environmental conditions (solar radiation, air temperature, background radiation)
Testing of a rotor blade segment
103 cm 57 cm
Measurement Simulation
Worzewski et al, DGZfP Jahrestagung 2014
Testing of rotor blades
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Detection of voids during solar heating
Thermogram after 3 h sun radiationTmax = 48 °C
Plaster scratches at Magdeburger Dom
From: maps.google.deFrom: maps.google.deFrom: maps.google.deFrom: maps.google.de
• Plaster scratches from 13th century• Voids and delaminations are getting warmer due to
solar heating• Heating as well as cooling down (e. g. due to
shadowing) enable further structural investigations >> active thermography
Steel engraving of central picture: Otto I. with his two wives Adelhaid and Editha
BBR project 3D-Mapping, Cooperation with with FhG IFF and IDK, local restorers
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Alternate heating with sun and clouds
11:00 12:00 13:00 14:00 15:00 16:00
0,0
0,5
1,0
Nor
mal
isie
rt
Zeit in Stunden
Temperaturentwicklung Fassade Globalstrahlung Hukseflux
Testing of building facades
BBR project ERBE, ZukunftBau, 2013-2015
• Culture house in Cobbelsdorf, Coswig• Mural painting Industrialized agriculture of
Erich Enge 1970/71• Beam construction• Sun radiation
from 150 W/m2 to850 W/m2 on 9.9.2014
• Time: 10:45 to 15:50 o’clock
2nd phase image of the sequence
10th phase image of the sequence
steel beams
cracks
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Standardisation
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DIN 54192Active thermography
Draft standardflash thermography
Structure of draft standardlockin thermography
DIN NA 062-08-27 AA Visual and thermographic testing
CEN TC 138/WG 11 Infrared and thermographic testing
prEN 16714-1Part 1 Gener-al principles
prEN 16714-2Part 2 Equip-ment
prEN 16714-3Part 3 Terms and definitions
Active thermography
EMRP VITCEA: Validated inspection methodsfor composites in energy applications
Pre Normative EMPIR-Proposal of EURAMET Focus Group on Standardization of Thermal Imagers (from 2016): Calibration of infrared cameras, crack detection
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Thermography Team
Thank you!
Mathias ZieglerPhilipp MyrachFlorian JonietzMarco LuchtTamara WorzewskiManoucher DoroshtnasirHenrik SteinfurthMathias Röllig
Rainer KrankenhagenNick RothbartSven AugustinErik ThielMarc KreutzbruckRegina RichterJoachim SchlichtingMercedes Reischel
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