•-INM3•-INM3 1A SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: CHEMTECH Contract: US...

•-INM31A SAMPLE NO.

VOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: CHEMTECH Contract: US EPA REGION HI

Project No.: CHEM Site: A440-S Location:

Matrix: (soil/water) SOIL

Sample wt/vol: 5.0 (g/mL) G

Level: (low/med) LOW

% Moisture: not dec. 80

Lab Sample ID:

0770306PD4RR

Group:

039578RR

Lab File ID: E1038.D

Date Received:

Date Analyzed:

GC Column: DB624 ID: 0.53 (mm) Dilution Factor:

Soil Extract Volume: (uL) Soil Aliquot Volume:

. . . . Concentration Units:GAS No. Compound (ug/L or ug/Kg) ug/Kg

>

<1330-20-7 Xylenes(total) 50

•

3/8/95

3/17/95

1.0

Qu

,.

(uL)

Page2of2 FORM I VGA UUUU«J<* 3/90

1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ————————•——

0770307D02Lab Name: CHEMTECH Contract: US EPA REGION Hi

Project No.: CHEM Site: A440-S Location: _________ Group: ___

Matrix: (soil/water) SOIL Lab Sample ID: O39579

Sample wt/vol: 5.0 (g/mL) G Lab File ID: E1039.D

Level: (low/med) LOW Date Received: 3/9/95

% Moisture: not dec. 18 Date Analyzed: 3/17/95

GC Column: DB624________ ID: 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: _____(uL) Soil Aliquot Volume: ______ (uL)

Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg Q

75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5

DichlorodifluoromethaneChlorome thaneBromome thaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1,1-Dichloroethanel,2-Dichlorocthene(total)Chloroform1,2-Dichloroc thane2-Butanone1,1,1-Triculoroethane •Carbon TctrachlorideBromodichloromethanc1 ,2-Dichloropropane •cis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobcnzeneEthylbenzeneStyrene

1212 ,12121219121212121212121212121212121212121212121212121212121212

UUUUUBUUUU

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Page 1 of 2 0FORMIVOA 00000.3 3/90

1A. . ._ VOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: CHEMTECH Contract: US EPA REGION II






Lab Sample ID:

SAMPLE NO.

0770307D02

Group:

O39579


Date Received:

Date Analyzed:

GC Column: DB624 ED: 0.53 (mm) Dilution Factor:


Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg

1330-20-7 Xylenes(total)

.

'

.

12

3/9/95

3/17/95

1.0

Q

U

(uL)

•

Page 2 of 2

°00064

1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ————————

0770307D28Lab Name: CHEMTECH Contract: US EPA REGION H


Matrix: (soil/water) SOIL Lab Sample ID: 039580




GC Column: DB624_____ ID: 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (uL)


75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5

DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideCuloroethaneMethylene ChlorideAcetoneCarbon Bisulfide1 , 1-Dichloroethene1, 1-Dichloroe thane1 ,2-Dichloroethene( total)Chloroform1,2-Dichloroethane2-Butanone1, 1, 1-Trichloroe thaneCarbon TetrachlorideBromodiculoromethane1,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1 , 1 ,2-TrichloroethaneBenzenemns-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroetnene1, 1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene

2323232323210572323232323232323232323232323232323232323232323232323

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Page 1 of2

flft3l6i*75 MKMIVOA 000070 3/9°

LabNam

Project N

Matrix:

Sample u

Level:

% Moisti

GCColui

SoilExtr

* • "" -~" ~ 1AVOLATILE ORGANICS ANALYSIS DATA SHEET

e: CHEMTECH Contract: US EPA REGION II

o.: CHEM Site: A440-S Location:

(soil/water) SOIL

it/vol: 5.0 (g/mL) G

(low/med) LOW

ire: not dec. 57

Lab Sample ID:

SAMPLE NO.

0770307D28

Group:

O39580


Date Received:

Date Analyzed:

ran: DB624 ID: 0.53 (mm) Dilution Factor:

act. Volume: (uL) Soil Aliquot Volume:


. . __._ _ - - • • -1330-20-7 Xylencs(total)

*

•

23

*

3/9/95

3/13/95

1.0

QU

.

(uL)

Page2of2FORMIVOA. 000071 3/9°

1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET —————————^~~

0770307D28RRLab Name: CHEMTECH Contract: US EPA REGION HI _____


Matrix: (soil/water) SOIL Lab Sample ID: O39580RR


Level: Gow/med) LOW Date Received: 3/9/95

% Moisture: not dec. 57 . Date Analyzed: 3/17/95


Soil Extract Volume: ______(uL) Soil Aliquot Volume: _________ (uL)


75-71-874-87-374-83-975-01-4 '75-00-375-09-267-64-175-15-075-35475-344540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5

DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1, 1-Dichloroethanel,2-Dichloroethene(total)Chloroform1 ,2-Dichloroethane2-Butanone1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1,1.2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1, 1,2,2-TetrachloroethaneTolueneChlorobenzeneEtbylbenzeneStyrene

232323232345742323232323232323232323232323232323232323232323232323

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Page 1 of2FokMIVOA 000072 3/90

LabNam

Project Is

Matrix:

Sample u

Level:

% Moistt

GCColui

Soil Extr

. 1AVOLATILE ORGANICS ANALYSIS DATA SHEET

K CHEMTECH Contract: US EPA REGION ID

fo.: CHEM Site: A440-S Location:

(soil/water) SOIL

rt/vol: 5.0 (g/mL) G

(low/med) LOW

:ire: not dec. 57

Lab Sample ID:

SAMPLE NO.

0770307D28RR

Group:

O39580RR

Lab File ID: E1040.D: .

Date Received:

Date Analyzed:

inn: DB624 ID: 0.53 (mm) Dilution Factor:

act Volume: (uL) Soil Aliquot Volume:



*

.

.

-

23

•

3/9/95

3/17/95

1.0

Q,U

(uL)

Page 2 of 2 .FORMIVOA n 3/9°

•;AR3 161*7.8 ....

1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

0770307D29Lab Name: CHEMTECH Contract: US EPA REGION IE

Page 1 of 2

Project No.: CHEM Site: A440-S Location: '______ Group: ___

Matrix: (soil/water) SOIL Lab Sample ID: O39S81




GC Column: DB624________ ED: 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______._ (uL)


75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35475-344540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-57M3-210061-02-675-25-2108-10-1591-78-6127-18479-34-5108-88-3108-90-7100-4M100-42-5

DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1 , 1-Dichloroe thane1 ,2-Dichloroethene(total)Chloroform1,2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1, 1,2-Trichloroe thaneBenzenetrans-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1 , 1 ,2,2-TetrachlorocthaneTolueneChlorobenzcneEmylbenzeneStyrcne

313131313145723131313131313131313131313131313131313131313131313131

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AR3i6t*79 KB*'™ 000082 3/9°

1A -VOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: CHEMTECH Contract: US EPA REGION U

Project No.: CHEM Site: A440-S . Location:





Lab Sample ID:

SAMPLE NO.

0770307D29

Group:

039581


Date Received:

Date Analyzed:

GC Column: DB624" ED: 0.53 (mm) Dilution Factor:


Concentration Units;CASNo. Compound (ug/L or ug/Kg) ug/Kg


-

•

31

3/9/95

3/17/95

1,0

QU

-.,

'

(uL)

Page2of2 00008'}UUUUOOFORMIVOA 3/90











75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4KXW2-5

DichlorodifluorometbaneChloromethaneBromomethaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1, 1-Dichloroethanel,2-Dichloroethene(total)Chloroform1,2-Dichloroe thane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroetuaneBenzenetrans-1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTerrachloroethene1,1,2,2-Tetrachloroe thaneTolueneChlorobenzeneEthylbenzeneStyrene

141414141422841414141414141414141414141414141414141414141414141414

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Page 1 of2

flR3l6i»8lFOWIV0*' 000089 3"°

1AVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: CHEMTECH Contract: US EPA REGION EL






Lab Sample ID:

SAMPLE NO.

0770307D22

Group:

O39582

Lab File ID: E1042.D, . - • f • • '

Date Received:

Date Analyzed:



Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg

1330-20-7 Xylenes(total) 14

3/9/95

3/17/95

1.0

QU

(uL)

»

Page 2 of2FORMIVOA nnnnnn 3/9°000030

1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ———————

0770307D34Lab Name: CHEMTECH Contract: US EPA REGION IE__________

Project No.: CHEM Site: A440-S Location: _________ Group:


Sample wt/vol: 5.0 (g/mL) G , Lab File ID: E1031.D



GC Column: DB624 ED: 0.53 (mm) Dilution Factor: 1.0


Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q

75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-612448-179-00-57W3-210061-02-675-25-2108-10-1591-78-6127-18479-34-5108-88-3108-90-7100-41-4100-42-5

DichlorodifluoromcthaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1, 1-Dichloroethane1 ,2-Dichloroethene(total)Chloroform1 ,2-Dichloroethane2-Butanone1 , 1 , 1-TrichloroethaneCarbon TetrachlorideBromodicfaloromethane1,2-Dichloropropanecis-l,3-DichloropropencTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzencEthylbenzeneStyrcnc

161616161665461616161616161616161616161616161616161616161616161616

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Page 1 of 2AR316^83 FORMIVOA 000096 3/9°

LabNam

Project N

Matrix:

Sample u

Level:

% Moisti

GC Colm

Soil Ex tr




(soil/water) SOIL Lab Sample ID:

t/vol: 5.0 (g/mL) G

(low/med) LOW

ire: not dec. 37 ..... __._...._

SAMPLE NO.

0770307D34

Group:

039583


Date Received:

Date Analyzed:

con: DB624 ED: 0.53 (mm) Dilution Factor

act Volume: (uL).

Soil Aliquot Volume:

3/9/95

3/13/95

1.0

(uL)



•

16 U

Page 2 of 2 . --• SR3iC,.^'F°RMI™A. 000097 3/9°


0770308D05Lab Name: CHEMTECH' Contract: US EPA REGION EC

Project No.: CHEM . Site: A440-S Location: _________ Group:




% Moisture: not dec. 48 - Date Analyzed: 3/17/95




75-71-874-87-3

DichlorodiOuoromethaneChloromethane

74-83-9 Bromomethane75-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5

Vinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1 , 1-Dichloroc thanel,2-Dichloroethene(total)Chloroform1 ,2-Dichloroe thane2-Butanone1,1,1-Trichloroethane .Carbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1, 1,2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEmylbenzeneStyrene

191919191928211919191919191919191919191919191919191919191919191919

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Page 1 of 2

••;«R3I61*85 •' FORMIVOA 000103 3/9°

LabNain

Project N

Matrix:

Sample w

Level:

% Moisti

GCColiu

Soil Extr




(soil/water) SOIL


(low/med) LOW•

ire: not dec. 48

Lab Sample ID:

SAMPLE NO.

0770308D05

Group:

039584

Lab File ED: E1043.Ds'

Date Received:

. Date Analyzed:

nn: DB624 ED: 0.53 (mm) Dilution Factor:


Concentration Units:CAS No. Compound , (ug/L or ug/Kg) ug/Kg

• -- -1330-20-7 Xylenes(total)

.

•

,

— - -19

.

3/9/95

3/17/95

1.0

Q

U

.

»

(uL)

Page 2 of2At FORM I VGA nr\nin/! 3/9°AR3i6if86 000104.

1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ——————————




Sample wt/vol: 5.0 (g/mL) G . Lab File ID: E1044.D

Level: '(low/med) LOW Date Received: 3/10/95W BWMH-l - | «————————^^MM



Soil Extract Volume: _____(uL) Soil Aliquot Volume: ______ (uL)


75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-612448-179-00-57143-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-410042-5

DichlorodiQuoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disuifide1, 1-Dichloroethene1, 1-Dichloroethane1 ,2-Dichloroethene( total)Chloroform1,2-Dichloroc thane2-Butanone1,1,1-Trichloroethane 'Carbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1, 1,2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneBromofonn4-Methyl-2-Pentanone2-HexanoneTetrachloroethcne1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene

232323232338232323232323232323232323232323232323232323232323232323

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Page 1 of2FORMIVOA 000110 2/90


Lab.Name: CHEMTECH Contract: US EPA REGION ID


Matrix: (soil/water) SIOIL


Level: (low/med) IX>W


Lab Sample ID:

SAMPLE NO.

0770308D03

> Group:

O39679


Date Received:

Date Analyzed:




1330-20-7 Xyl«nes(total)

>

%

•

23

•

3/10/95

3/17/95

1.0

Q

U

••-

(uL)

Page 2 of2

AR3I6488 FORJiIVOA 000111 3/9°


0770313D06Lab Name: CHEMTECH Contract: US EPA REGION II '

Project No.: CHEM Site; A440-S Location: _________ Group:





GC Column: DB624 EO; 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: _______(uL) Soil Aliquot Volume: _______ (uL)


75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5

DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1 , 1-Dichloroethanel,2-Dichloroethene( total)Chloroform1 ,2-Dichloroe thane2-Butanone1 , 1 , 1 -TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-l,3-DicMoropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromofonn4-Metbyi-2-Pentanone2-HexanoneTetrachloroethene1, 1,2,2-TetrachloroethaneTolueneChlorobcnzencEthylbenzeneStyrene

40404040406917040404040404040404040.40404040404040404040404040404040

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Page 1 of 2

000117



Project No.: CHEM • Site: A440-S Location:





Lab Sample ID:

SAMPLE NO.

0770313D06

Group:

039815


Date Received:

Date Analyzed:




'.•


,

,

-

40

,

..-.

3/15/95

3/17/95

1.0

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Page 2 of2FORMIVOA 000118 3/9°

1A _ SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

0770313D06RRLab Name: CHEMTECH Contract: US EPA REGION ID

Project No.: CHEM Site; A440-S Location: _________ Group: ___

Matrix: (soil/water) SOIL Lab Sample ED: 039815RR

Sample wt/vol: 5.0 (g/mL) G Lab File ID: E10S3.D



GC Column: DB624________ ED; 0.53 (mm) Dilution Factor; 1.0



75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5

DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1, 1-Dichloroethanel,2-Dichloroethene(total)Chloroform1 ,2-Dichloroethane2-Butanone1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethanc1, 1,2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene

404040404020021040404040404040404040404040404040404040404040100404040

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Page 1 of2AR3i6t*9i •FOkMIVOA 000119 3/9°

LabNam

Project N

Matrix:

Sample w

Level:

% Moisa

GCColui

Soil Extr


~ , * " - - ~ j , - - - - ' -

e: CHEMTECH Contract: US EPA REGION IE


(soil/water) SOIL

t/vol: 5.0 (g/mL) G

(low/med) LOW

ire: not dec. 75

Lab Sample ID:

SAMPLE NO.

07703 13D06RR

Group:

O39815RR

Lab File ID: E1053.D. . . S

Date Received:

Date Analyzed:

am: DB624 ED: 0.53 (mm) Dilution Factor:

net Volume: (uL) Soil Aliquot Volume:



.

.. .. .

40

'

.

3/15/95

3/17/95

1.0

Q

U

(uL)

Page 2 of2 r FORMIVOA nnnion 3/9°AR3I6**92 . 0001,0


0770313D07Lab Name: CHEMTECH Contract: US EPA REGION II]

Page 1 of2 . .*•.•

CroRMtvOA 000130

Project No.: CHEM Site; A440-S Location: _________ Group: ___

Matrix: (soil/water) SOIL Lab Sample ED: O39818

Sample wt/vol: v 5.0 (g/mL) G . Lab File ID: E1056.D



GC Column: DB624________ ED; 0.53 (mm) Dilution Factor: 1.0'



75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-3 4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5 .

DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideCbloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1 , 1-Dichloroethanel,2-Dichloroethene(total)Chloroform1,2-Dichloroethane2-Butanone1,1,1-Trichloroe thaneCarbon TetrachlorideBromodichloromethane1,2-DichloroproDanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1, 1,2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene

1515151515591515151515151515151515151515151515151515151515261515

' 15 .

UUUUUBUUUUUUUUUUUuuuuuuuuuuuujfr-:-..uuu

o LabNam

Project N

Matrix:

Sample w

Level:

% Moistt

GCColui

Soil Extr

1A__ : VOLATILE ORGANICS ANALYSIS DATA SHEET

e: CHEMTECH Contract: US EPA REGION IT


(soil/water) SOIL

i/vol: 5.0 (g/mL), G

(low/med) LOW

ax: not dec. 32

Lab Sample ID:

SAMPLE NO.

0770313D07

Group:

039818

LabFileID:E1056.D

Date Received:

Date Analyzed:

on: DB624 ED: 0.53 (mm) Dilution Factor:

ict Volume: (uL) Soil Aliquot Volume:


1330-20-7 Xyh!nes(total)

.

.... ___..

15

3/15/95

3/18/95

1.0

QU

•

(uL)

Page 2 of2FORMIVOA . .. 000131 3/9°


0770313D6DLab Name: CHEMTECH Contract: US EPA REGION HI _______









75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3 .108-90-7100-41-410042-5

DichlorodifiuoromethaneChloromethaneBromomethaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1,1-Dichloroethanel,2-Dichloroethene(total)Chloroform1,2-Dichloroethane2-Butanone1, 1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1, 1,2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneCbloiobenzeneEthylbenzeneStyrcne

131313131355611313131313131313131313131313131313131313131325131313

UUUuuBBUUUUUUUUUUUUUUuuuuuuuuuuu

Page 1 of 2

000137 3/9°

. . . . . . .- - 1AVOLATILE ORGANIC

Lab Name: CHEMTECH

S ANALYSIS DATA SHEET

Contract: US EPA REGION II






Lab Sample ID:

SAMPLE NO.

0770313D6D

Group:

O39819


Date Received:

Date Analyzed:



Concentration Units:CAS No. Compound . (ug/L or ug/Kg) ug/Kg


.

" ' ' •"" ' *

13

'

3/15/95

3/18/95

1.0

Qu

.

--

-

(uL)

Page 2 of2

>:'-.'"<Wfl3161.96-WVOA 000138" 3/9°

1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ———————————

0770313D09Lab Name: CHEMTECH Contract: US EPA REGION II]



Sample wt/vol: 5.0 (g/mL) G . Lab File ID: E10S8.D



GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0



75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5

DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1,1-Dichloroethanel,2-Dichloroethene(total)Chloroform1,2-Dichloroethane2-Butanone1, 1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-l,3-DichloropropcneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene

191919191975591919191919191919191919191919191919191919191931191919

UUuuuBB

" UUUUUUUUUUUuuuuuuuuuuuuuu

Page 1 of 2FORMIVOA rtrvAi AK 3/9°

000145







% Moisture: not .dec. 47

Lab Sample ID:

SAMPLE NO.

0770313D09

Group:

O39820


Date Received:

Date Analyzed:

GC Column: DB624 ED: 0.53 (mm) Dilution Factor:i



f - -"

1330-20-7 Xylcnesl total)

'

- •

,^

19

3/15/95

3/18/95

1.0

QU

(uL)

Page 2 of2FORMIVOA 000146 3/9°

lA _ SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

0770313D13Lab Name: CHEMTECH Contract: US EPA REGION EC






GC Column: DB624________ ED; 0.53 (mm) Dilution Factor; 1.0



75-71-874-87-374-83-975-01475-00-3 .75-09-267-64-175-15-075-35475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18479-34-5108-88-3108-90-710041-4100-42-5

DichlorodiSuoromethaneChloromethaneBromomethaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1,1-Dichloroc thanel,2-Dichloroethene(total) .Chloroform1,2-Dichloroethane2-Butanone1 , 1 , 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1, 1,2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneBromofonn4-MethyI-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TerrachloroethaneTolueneChlorobenzeneEthylbenzcneStyrene

30303030308237030303030303098303030303030303030303030303030380303030

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Page 1 of2

000168 3/9°

TAVOLATILE ORGANICS ANALYSIS DATA SHEET


Project No.: CHEM Site: A440-S Location:.





•Lab Sample ID:

SAMPLE NO.

0770313D13

Group:

039823

LabFHeID:E1070.D>.'

Date Received:

Date Analyzed:





. - .

.

. *

30

3/15/95

3/18/95

1.0

QU

(uL)

Page 2 of 2 0001 £Quuuib* 3/90




Matrix: (soil/water) SOIL Lab Sample ID: .O39822





Soil Extract Volume: ________(uL) Soil Aliquot Volume: ______ (uL)


75-71-874-87-374-83-975-01-475-00-3 .75-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-612448-179-00-57143-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4KXW2-5

DichlorodifuioromethaneChloromethaneBromomethaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1 , 1-Dichloroe thanel,2-Dichloroethene(total)Chloroform1 ,2-Dichloroethane2-Butanone1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromofbrm4-Methyl-2-Pentanone2-HexanoneTerrachloroethene1, 1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStymie

141414141448141414141414141414141414141414141414141414141414141414

UUUuuBUUUUUUUuuuuuuuuuuuuuuuuuuu

Page Iof2•AR3I650I FORMIVOA 000161 3/9°

IAVOLATILE ORGANICS ANALYSIS DATA SHEET





Level: (Eow/med) LOW


Lab Sample ID:

SAMPLE NO.

0770313D14

Group:

039822

.Lab File ID: E1060.D

Date Received:

Date Analyzed:

GC Column: DB624 ED: 0.53 (mm) Dilution Factor


Concentration Units:GAS No. Compound (ug/L or ug/Kg) ug/Kg


- --

-14

•

3/15/95

3/18/95

1.0

QU

(uL)

Page2of2FORMIVOA 3/9°000162


0770313D16Lab Name: CHEMTECH ___ Contract: US EPA REGION IE ________


Matrix: (soil/water) SOIL Lab Sample ED: O39821



% Moisture: not dec. SO Date Analyzed: 3/18/95



Concentration Units:CASNo. Compound . (ug/L or ug/Kg) ug/Kg Q

75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-344540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100414100-42-5

DichlorodiQuoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1 , 1-Dichloroe thanel,2-Dichloroethene(total)Chloroform1 ,2-Dichloroethane2-Butanone1 , 1 , 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene

2020202020719320202020202020202020202020202020

, 20202020202012202020

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Page 1 of 2 ... ...AR3J6503 FORMIVOA 000153 3/9°

LabNam

Project N

Matrix:

Sample u

Level:

% Moisti

GCColui

Soil Extr


e: CHEMTECH Contract: US EPA REGION EC

o.: CHEM . Site: A440-S Location:

(soil/water) SOIL

l7vol: 5.0 (g/mL) G

(low/med) LOW• - i

ire: not dec. 50

Lab Sample ID:

SAMPLE NO.

0770313D16

Group:

O39821


Date Received:

Date Analyzed:

mil: DB624 ED: 0.53 (mm) Dilution Factor:



1330-20-7 XylenesUotal)

- '

, i

•

...

..— .

20

~•

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3/15/95

3/18/95

LO

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Page 2 of 2FORMTVOA 3/9°

•AR3-I650U-

IA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

0770313PD3Lab Name: CHEMTECH Contract: US EPA REGION U

Project No.: A446-S Site: _____ Location: _________ Group: ___





GC Column: DB624________ ED; 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: _______(uL) Soil Aliquot Volume: ______ (uL)


75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-57143-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-414100-42-5

DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1, 1-Dichloroethanel,2-Dichloroethene(total)Chloroform1,2-Dichloroethane2-Butanone1, 1, 1-TrichloroethaneCarbon TettachlorideBromodichloromethane1 ,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1 , 1 ,2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneBromoform4-MethyI-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachIoroethaneTolueneChlorobenzeneEthylbenzeneStyrene

16161616163816161616161616161616161616161616161616161616169.1161616

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Page 1 of2

;'J;"«'R3I6505 'roRMIVOA 000017

1AVOLATILE ORGANIC

Lab Name: CHEMTECH

S ANALYSIS DATA SHEET

Contract: US EPA REGION EC

Project No.: A446-S Site: Location:





Lab Sample ID:

Lab File ID:

Date Received:

Date Analyzed:




Page 2 of

1330-20-7 Xylenesdotal) 16

T

SAMPLE NO.

0770313PD3

Group:

O39824

E1071.D

3/15/95

3/18/95

1.0

Qu

~..

. •

2 ' ' - ' ' . ' . . . . .\,, Mi FORMIVOA OOOO1 8

SR3/6506

(uL)

3/90


0770313D33Lab Name: CHEMTECH Contract: US EPA REGION II


Matrix: (soil/water) SOIL Lab Sample ID: O3982S





Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (iiL)

Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q.

75-71-874-87-374-83-975-01475-00-375-09-267-64-175-15-075-3575-344540-59-067-66-3107-06-278-93-371-55-656-23-575-27478-87-510061-01-579-01-6124-48-179-00-57143-210061-02-675-25-2108-10-1591-78-6127-18479-34-5108-88-3108-90-7100-41-4100-42-5

DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfidc1 , 1-Dichloroethene1 , 1-Dichloroc thane1 ,2-Dichloroethene(total)Chloroform1 ,2-Dichloroethane2-Butanone1 , 1 , 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethanc1 , 1,2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene

151515151556

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Page 1 of2

fiR3l6507FORMIVOA 000095 3"°

LabNam

Project N

Matrix:

Sample u

Level:

% Moisti

GCColui

Soil Extr



fo.: A446-S Site: Location:

(soil/water) SOIL


(low/med) LOW

ire: not dec. 33

Lab Sample ID:

Lab File ID:. : . •- - .,,.' • •

Date Received:

Date Analyzed:

mn: DB624 ED: 0.53 (mm) Dilution Factor:




t

15

•

-

SAMPLE NO.

0770313D33

Group:

039825

E1063.D

3/15/95

3/18/95

1.0

Qu

.

(uL)

Page 2 of 2 ,3/9°

AR3I6508

1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET —————————

0770314PD5Lab Name: CHEMTECH Contract: US EPA REGION IE ____'

Project No.: A446-S Site: _____ Location: ___________ Group:


Sample wt/vol: 5.0 (g/mL) G Lab File ID:E106S.D




Pagelof2 ,. 00004?

'

Soil Extract Volume: ______(uL) Soil Aliquot Volume: _______ (uL)


75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10*1591-78-6127-18-479-34-5108-88-3108-90-710041-4100-42-5

DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1 , 1-Dichloroethanc1 ,2-Dichloroethene( total)Chloroform1 ,2-Dichloroe thane2-Butanone1,1, 1-TricbloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-l,3-DichloropropencTrichloroetheneDibromochlorometnane1 , 1,2-TrichloroethaneBenzenetrans- 1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzene • .Styrene ~ -.

43684343432601200434343364343180434343434343434343434343434343

24004343

~ 43

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1A__ VOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: CHEMTECH Contract US EPA REGION tt

Project No,: A446-S Site: Location:




% Moisture: not.dec. 77

Lab Sample ID:

SAMPLE NO.

0770314PD5•

Group:

O39963


Date Received:

Date Analyzed:





,

43

3/16/95

3/18/95

1.0

QU

-

(uL)

Page 2 of2FORMiyOA 000043 3/9°

A R 3 I 6 5 1 0


0770314PD5DLLab Name: CHEMTECH Contract: US EPA REGION EC

Project No.: A446-S Site: _____ Location: _________ Group:

Matrix: (soil/water) SOIL Lab Sample ID: O39963DL


Level: (low/med) MED Date Received: 3/16/95



Soil Extract Volume: 10000 (uL) Soil Aliquot Volume: ____100 (uL)


75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-344540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18 *79-34-5108-88-3108-90-7100-41-4100-42-5

DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1 , 1-Dichloroethanel,2-Dichloroethene(total)Chloroform1,2-Dichloroethane2-Butanone1,1,1-TricbloroethaneCarbon TetracblorideBromodichloromethane1,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1, 1,2-Trichloroe thaneBenzenetrans-l ,3-DichloropropeneBromofonn4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene

5200520052005200520052004700520052005200520052005200520052005200520052005200520052005200520052005200520052005200520015300520052005200

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flR3l65H ^^ °°00-4

. .. . - 1AVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: CHEMTECH Contract: US EPA REGION EC




Level: (low/med) MED


Lab Sample ID:

SAMPLE NO,

0770314PD5DL

Group:

O39963DL,

LabFileID:E1103.Ds

Date Received:

Date Analyzed:


Soil Extract Volume; 10000 (uL) Soil Aliquot Volume:


1330-20-7 Xylenss(total) 5200

,

•

•

,

3/16/95

3/24/95

1.0

100

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Page2of2FORMIVOA t\nr\f\AK 3/9°

•AR3I6SI2 ' 000045


0770314PD6Lab Name: CHEMTECH Contract: US EPA REGION IE _____









75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35475-344540-59-067-66-3107-06-278-93-371-55-656-23-575-2778-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5

DicnlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1 , 1-Dicbloroethane1 ,2-Dichloroethene(total)Chloroform1,2-Dichloroethane2-Butanone1 , 1 , 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzene. * _. . -trans-i,j-LMcnioropropeneBromoform4-Memyl-2-Pentanone2-HexanoneTetrachloroethene1, 1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzene

• Styrene

232323232310011023232323232323232323232323232323

. 23232323132346232323

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Page 1 of2A'R3165 i 3FORM1VOA 000033 3/9°

O


Lab Name: CHEMTECH Contract: US EPA REGION Et






Lab Sample ID:

SAMPLE NO.

0770314PD6

Group:

O39962 •


Date Received:

. Date Analyzed:





f

.

23

3/16/95

3/18/95

1.0

QU

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Page 2 of 2 , ;s .-i «««««*' FORMIVOA 000034 3/90

AR3I65U

1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ————————

0770314D35Lab Name: CHEMTECH Contract: US EPA REGION IE ____'

Project No.: A446-S . Site: _____ Location: ___________ Group:

Matrix': (soil/water) SOIL Lab Sample ID: O39964







75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34540-59-067-66-3107-06-278-93-371-55-656-23-575-27478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18479-34-5108-88-3108-90-7KXM1-4100-42-5

DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethane 'Methylene ChlorideAcetoneCarbon Disulfidc1,1-Dichloroethene1, l-Dichloroethane1 ,2-Dichloroethene(total)Chloroform1 ,2-Dichloroethane2-Butanone1,1,1 -TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobcnzcncEmylbenzeneStyrene

141414141437151414141414141414141414141414141414141414141414141414

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Pagelof2 0000 7FORMIVOA VUUUo ( 3/90AR3I65I5


Lab Name: CHEMTECH Contract: US EPA REGION IT






Lab Sample ID:

SAMPLE NO.

0770314D35

Group:

O39964

LabFiIeID':E1074.D'• ' ' s'

Date Received:

Date Analyzed:




•


~~

i

14

3/16/93

3/18/95

1.0

QU

(uL)

Page 2 of 2 nnAnc;QFORM IVOA U U U U J O 3/90

AR3I65I6


0770315D08Lab Name: CHEMTECH Contract: US EPA REGION III'

Project No.: A446-S Site: _______ Location: __________ Group:








75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18479-34-5108-88-3108-90-710CM1-4HXW2-5

DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1,1-Dichloroethanel,2-Dichloroethene( total)Chloroform1 ,2-Dichloroe thane2-Butanone1, 1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1, 1,2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene

131313131344131313131313131313131313131313131313131313131313131313

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• uuuuuuuuuuu

Page 1 of 2FORMIVOA OOOOR4 3/9°Anoirr"!-* wvv/uj*±RJ I 65 i 7

VOLATILE ORGANICS .ANALYSIS DATA SHEET

Lab Name: CHEMTECH Contract: US EPA REGION H



Sample wt/vol: 5.0 (g/mL)' G



Lab Sample ID:

OT70315D08'•

Group:

039965


Date Received:

Date Analyzed:




•


'

-

13

3/16/95

3/18/95

1.0

Qu

(uL)

Page 2 of 2 , " _ " r\r\r\r\r"FORMIVOA OUUUbO 3/90

A R 3 I 6 5 I 8

1A SAMPLE NO..VOLATILE ORGANICS ANALYSIS DATA SHEET ~

0770316D10Lab Name: CHEMTECH Contract: US EPA REGION H ______"

Project No.: A446-S Site: _____ Location: ___________ Group: ___


Sample wt/vol: 5.0 (g/mL) G ' Lab File ID:E1081.D


% Moisture: not dec. 43 Date Analyzed: 3/18/95.

GC Column: DB624_________ ED; 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: ______(uL) , Soil Aliquot Volume: ______ (uL)


75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-344540-59-067-66-3107-06-278-93-371-55-656-23-575-27478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-lOrl

591-78-6127-18479-34-5108-88-3108-90-7100-41-4100-42-5

DichlorodifluoromethaneChloromedianeBromomethaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1, 1-Dichloroethane1 ,2-Dichloroethene( total)Chloroform1,2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1, 1,2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1 , 1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene ~ _

18181818185238181818181818181818181818181818181818181818189.1181818

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Pagelof2 OOOJ11FORM IVOA v u u J. I i 3/90

AR3I65I9

€>1A

VOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: CHEMTECH Contract: US EPA REGION El






Lab Sample ID:

SAMPLE NO.

0770316D10

Group:

O40047


Date Received:

Date Analyzed:



3/17/95

3/18/95

1.0

(uL)


1330-20-7 Xyleiies(totaJ) 18

„

QU

^

-

Page2of2 00011?FORM IVOA U U U 11'- 3/90

AR316520

1A ' SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ———————

077031SD12Lab Name: CHEMTECH Contract: US EPA REGION III ________"

Page 1 of 2FORMIVOA

AR3I652I




Level: (low/med) LOW Date Received: 3/16/95 •


GC Column: DB624_________ ED: 0.53 (mm) Dilution Factor: 1.0



75-71-874-87-374-83-975-01475-00-375-09-267-64-175-15-075-35-475-34540-59-067-66-3107-06-278-93-371-55-656-23-575-27478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18479-34-5108-88-3108-90-7100-41-4100-42-5

DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1,1-Dichloroe thane1 ,2-Dichloroethenc( total)Chloroform1 ,2-Dichloroethane2-Butanone1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1 , 1 ,2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetracnloroemene1, 1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene

2424242424242902424242424248424242424242424242424242424242420242424

UUUUUJB

UUU

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. ..• - - - - - - • .-. 1AVOLATILE ORGANICS ANALYSIS DATA SHEET






% Moisture: not dec. .59

Lab Sample ID:

SAMPLE NO.

0770315D12"

Group:

039966


Date Received:

Date Analyzed:





.

.

24

*

•

3/16/95

3/22/95

1.0

QU

"

„

(uL)

Page 2 of 2 .FORMIVOA 00007P 3/9°

AR316522

1A • SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ———————-

0770316D23Lab Name: CHEMTECH Contract: US EPA REGION II '_____







Soil Extract Volume: ______(uL) Soil Aliquot Volume: _______ (uL)u

Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg • Q

75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-2778-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-lOrl

591-78-6127-18-479-34-5108-88-3108-90-7100-41-410CM2-5

DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMetbylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1, 1-Dichloroethanel,2-Dichloroethenc{ total)Chloroform1 ,2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromediane1,2-Dichloropropanccis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1 , 1 ,2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachlorocthene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene

1919

,_ 19191948551919191919191919191919191919191919191919191919191919

UUUuuB

UUu

... uuuuuuuuuuuuuuuuuuuuuuu

000095SR3I6523 3/9°

<l

IAVOLATILE ORGANICS ANALYSIS DATA SHEET







Lab Sample ID:

SAMPLE NO.

0770316D23

Group:

O40045

Lab File ID: E1079.D. . . ' *

Date Received:

Date Analyzed:




1330-20-7 Xylencs(total)

• - - - - .

19

3/17/95

3/18/95

1.0

QU

(uL)

Page2of2 000096FORMIVOA vv/vu

A"R3 165214

1A __SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET


Page 1 of2



Sample wt/vol: 5.0 (g/mL) G Lab File ED: E1086.D






75-71-874-87-374-83-975-01475-00-375-09-267-64-175-15-075-35475-344540-59-067-66-3107-06-278-93-371-55-656-23-575-27478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18479-34-5108-88-3108-90-7100-41-4100-42-5

DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichlorocrnene1,1-Dichloroethancl,2-Dichloroethene(total)Chloroform1,2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1 , 1 ,2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneBromoform4-Mernyl-2-Pentanone2-HexanoneTetrachloroethene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene

2424242424211102424242424242424242424242424242424242424242419242424

UUUUUJB

UUUUUUUUUUUUUuuuuuuuuuJuuu

FORMIVOA 000103 3/90AR3I6525





Sample wr/vol: 5.0 (g/mL) G

Level:/

(low/med) LOW


Lab Sample ID:

SAMPLE NO.

0770316D24"

Group:

O40046

LabFileID:E1086.D

Date Received:

Date Analyzed:



i Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg

•

1330-20-7 Xytenes(total) 24

3/17/95

3/22/95

1.0

QU

-., .

(uL)

30010

Page 2 of2FORM IVOA 3/90

AR3I6526



Project No.: A446-S . Site: _____ Location: _________ Group: ___








75-71-874-87-374-83-975-01475-00-375-09-267-64-175-15-075-35-475-344540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-1879-34-5108-88-3108-90-7100-41-410042-5

DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1 , 1-Dichloroe thane1 ,2-Dichloroethene(total)Chloroform1 ,2-Dichloroethane2-Butanone1, 1. 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-l,3-DicnloropropeneTrichloroetheneDibromochloromethane1, 1,2-TrichloroethaneBenzenetnms-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetracnloroethaneTolueneChlorobenzeneEthylbenzeneStyrene

141414141414451414141414141414141414141414141414141414141412141414

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Page 1 of 2 0001 1 9K FORM I VGA U U U 1 - 3/9Q

AR3I6527






Level: (low/med) 1LOW


Lab Sample ID:

SAMPLE NO.

0770316D27

Group:

O40048


Date Received:

Date Analyzed:

GC Column: DB624 ED: 0.53 (mm) Dilution Factor


—- Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg


.

.* - . - - -

14

3/17/95

3/22/95

1.0

QU

„

(uL)

0001;Page 2 of 2 ; . ' •

FORMIVOA 3/90

AR3I6528

1A SAMPLE NO.VOLATILE pRGANICS ANALYSIS DATA SHEET







GC Column: DB624____•_____ ED: 0.53 (mm) Dilution Factor: 1.0



75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-57143-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5

DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethyiene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1, 1-Dichloroethane1 ,2-Dichloroethene(total)Chloroform1 ,2-Dichloroe thane2-Butanone1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1 , 1 ,2-TrichlorocthaneBenzenetnns-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-Tetrachloroe thaneTolueneChlorobenzeneEthylbenzeneStyrene

212121212161212121212121212121212121212121212121212121212111212121

UUUuuBUUUUUUuuuuuuuuuuuuuuuuuJuuu

Pagelof2 000030FORMIVOA 3/90

'AR3I6529

• - . • ... .'"-;- IAVOLATILE ORGANICS ANALYSIS DATA SHEET





Level: (Jow/med) LOW


Lab Sample ID:

SAMPLE NO.

0770316D31

Group:

O40043


Date Received:

Date Analyzed:





i

21

,

3/17/95

3/18/95

LO

QU

(uL)

Page 2 of2FORMIVOA 000081 3/90

-AR3I6S3D







% Moisture: not dec, 37 Date Analyzed: 3/18/95


75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18479-34-5108-88-3108-90-7100-41-4100-42-5

DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMernylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroediene1, 1-Dichloroc thanel,2-Dichloroethene(total)Chloroform1 ,2-Dichloroc thane2-Butanone1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromcthanc1,1,2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromofonn4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1, 1,2,2-TetrachloroethaneTolueneChlorobcnzencEthylbenzeneStyrcne

16161616164216161616161616161616161616161616161616161616169161616

UUUuuBUUUU

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Page 1 of 2

«R3I653I



o LabNam

Project N

Matrix:

Sample u

Level:

% Moisti

GCColui

SoilExtr



To.: A446-S Site: Location:

(soil/water) SOIL


(low/med) LOW

as: not dec. 37

Lab Sample ID:

SAMPLE NO.

0770316D32

Group:

0400-44


Date Received:

Date Analyzed:

am: DB624 ID: 0.53 (mm) Dilution Factor-

act Volume: (uL) Soil Aliquot Volume:' . - - , . • - - - - - : - •• ---T- -— r --••-•

• Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg

•


,

•

3/17/95

3/18/95

1.0

Q

. U

*

(uL)

Page 2 of2nnnnoo 3/90

°88

1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET —————————

0770320D15Lab Name: CHEMTECH__ Contract: US EPA REGION II



Sample wt/vol: 5.0 (g/mL) G Lab File ED: E1088.D






75-71-874-87-374-83-975-01475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6 '124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-1879-34-5108-88-3108-90-7100-41-4100-42-5

DichlorodifluoromethaneChloromethaneBromomedianeVinyl ChlorideChloroedianeMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1 , 1-Dichloroethanel,2-Dichloroethene(total)Chloroform1 ,2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1 , 1 ,2-TricbloroetbaneBenzenetnms-l,3-DichloropropeneBromofonn4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1, 1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrcne

1919191919191001919191919191919191919191919191919191919191918191919

UUUuuB

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000177

Page 1 of2FORM I VGA 3/90

'••..-":.-.-±.J. 1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET '—————

r " - 0770320D18Lab Name: CHEMTECH Contract: US EPA REGION IE

Project No.: A446-S Site: _____ Location: , Group:

Matrix: (soil/water) SOIL Lab Sample ID: 040095 _


Leyel: (low/med) LOW Date Received: 3/21/95

% Moisture: not dec. 65__ Date Analyzed: 3/23/95


Soil Extract Volume: _____._(uL) . . Soil Aliquot Volume: _____ (uL)


75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18479-34-5108-88-3108-90-710041-410042-5

DicliilorodifluoromeuianeChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1,1-Dichloroethane1 ,2-Dichloroethene( total)Chloroform1 ,2-Dichloroethane2-Butanonc1 , 1 , 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-l,3-DichloropropeaeTricliloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzenetrans-l,3-DichloropropcneBromoform4-Mcthyl-2-Pentanone2-HexanoneTetntchloroethene1, 1,2,2-TetracnloroethaneTolueneChlorobenzeneEthylbenzeneStyrene

292929292920

1700292929292929590292929292929292929292929292929

7800292929

UUUuuIBEUUuuuuEUuuuuuuuuuuuuuuEuuu

Page I of 2 ___FDRMIVOA 000144 3/9°

AR3 1653*4


Lab Name: CHEMTECH Contract: US EPA REGION II)





% Moisture; not dec. 65

Lab Sample ID:

SAMPLE NO.

0770320D18

Group:

O40095


Date Received:

Date Analyzed:


Soil Extract Volume: 1 (uL) Soil Aliquot Volume:



'

29

3/21/95

3/23/95

1.0

I

QU

-

(uL)

Page2of2 QQn 1 4 <r

SR3I6535


0770320D18DLLab Name: CHEMTECH Contract: US EPA REGION IE

Project No.: A446-S Site: ^ ^ Location: _________ Group:

Matrix: (soil/water) _SOIL Lab Sample ID: 040095DL

Sample wt/vol: 4.0__(g/mL) G ' Lab File ID: EU02.D

Level: (low/med) MED_ Date Received: 3/21/95



Soil Extract Volume: JiOQQO (uL) Soil Aliquot Volume: ____100 (uL)


75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35475-344540-59-067-66-3107-06-278-93-371-55-656-23-575-27478-87-510061-01-579-01-61244S-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-4 •79-34-5108-88-3108-90-710041-410042-5

DichlorodifluoromethaneChloromethaneBromomethancVinyl ChlorideChlotoethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1,1-Dichloroethanel,2-Dichloroethene(totai)Chloroform1,2-Dichloroethane2-Butanone1, 1, 1-Trichloroe thaneCarbon TetrachlorideBromodichloromediane1 ,2-Dichloropropanecis-l,3-DichloropropeneTricMoroetheneDibromochloromethane. 1 , 1 ,2-TrichlorpethaneBenzenetrans-l,3-DichloropropeneBromoform4-Melhyl-2-Pentanone2-HexanoneTetrac:hloroethene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrerc

3400340034003400340034003000340034003400340034003400340034003400340034003400340034003400340034003400340034003400340010200340034003400

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Page 1 of2

1-6536 FORMIVOA °°°H6

LabNam

Project N

Matrix: (

Sample w

Level:

% Moisti

GCColui

SoilExtn


s: CHEMTECH Contract: US EPA REGION II

o.: A446-S Site: Location:

soil/water) SOIL

t/vol: 4.0 (g/mL) G

(low/med) MED

ire: not dec. 65

Lab Sample ID:

Lab File ID:

Date Received:

Date Analyzed:

nn: DB624 ED: 0.53 (mm) Dilution Factor:

ict Volume: 10000 (uL) Soil Aliquot Volume:

Concentration Units:'CAS No. Compound (ug/L or ug/Kg) ug/Kg

-i


SAMPLE NO.

0770320D18DL

Group:

O40095DL

E1102.D

3/21/95

3/24/95

1.0

100

Qu

-.

*

'

(uL)

Page2of2FORMIVOA 3/90

AR3I6537

1A . SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET '——————, : 0770320D2i



Matrix: (soil/water) SOIL Lab Sample ID: O40094 _

Sample wt/vol: j.0 (g/mL) G Lab File ID: E1089.D_

Level: . (low/med) LOW Date Received: 3/21/95_

% Moisture: not dec. 66 Date Analyzed: 3/22/95_


Soil Extract Volume: ____(uL) Soil Aliquot Volume: __ (uL)


75-71-874-87-374-83-975-01475-00-3 '75-09-267-64-175-15-075-35475-344540-59-067-66-3107-06-278-93-371-55-656-23-575-27478-87-510061-01-579-01-612448-179-00-57143-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-710041-410042-5

DichlorodifluoromedianeChloromcthaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1 , 1-Dichloroethane1 ,2-Dichloroethene(total)Chloroform1 ,2 -Dichloroediane2-Butanone1, IJ-TrichloroethaneCarbon TetrachlorideBromodichloromethaue1,2-Dichloropropane .cis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1, 1,2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetiachloroethene1; 1,2,2-TetrachloroethaneTolueneChlorobenzeneEtfaylbenzeneStyrene

2929292929266402929292929292402929292929292929292929292929

- 29110292929

UUUuuJB

UUU

, UUu

uuuuuuuuuuuuuuu

uuu

Page 1 of 2FORMIVOA J 3/90

AR3I6538

Lab Nam

Project N

Matrix:

Sample w

Level:

% Moisa

GCColui

Soil Extn




'soil/water) SOIL

t/vol: 5.0 (g/mL) G

(low/med) LOW

ire: not dec. 66

Lab Sample ID:

SAMPLE NO.

0770320D21

Group:

O40094


Date Received:

Date Analyzed:

nn: DB624 ID: 0.53 (mm) Dilution Factor:




*

3/21/95

3/22/95

1.0

QU

-

(uL)

Page 2 of 2 HOH1 QC'FORMIVOA UUIUJO 3/90

AR3I6539"



Project No.: A446-S Site: _______ Location: -_________ Group: ___

Matrix: (soil/water) _SOIL Lab Sample ID: O40096

Sample wt/vol: 5.0 (g/mL) G . Lab File ED:E1100.D

Level: (low/med) _LOW Date Received: 3/21/95

% Moisture: not dec. __29__ Date Analyzed: 3/24/95 _

GC Column: DB624________ ED: 0.53 (mm) Dilution Factor: 1.0 _

Soil Extract Volume: ______(uL) Soil Aliquot Volume: _____' (uL)

Concentration Units:CAS No. Com|X>und (ug/L or ug/Kg) ug/Kg Q

75-71-874-87-374-83-975-01475-00-375-09-2 .67-64-175-15-075-354 -75-34-4540-59-067 6-3107-06-278-93-371-55-656-23-575-27478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18479-34-5108-88-3108-90-7100-41-4100-42-5

DicMorodifiuoromethaneChloiromethaneBronaiomethaneVinyl ChlorideChloiroethaneMethylene ChlorideAcetoneCarbon Disulfide .1,1-Dichloroethene1,1-Dichloroethane1 ,2-Dichloroethene(total)Chloroform1,2-Dichloroethane2-Buianone1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzene .tnns-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HejtanoneTetrachloroethene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylltenzeneStyreiie

141414141411171414141414141414141414141414141414141414141414141414

UUUuuJB

UUUuuuuuuuuuuuuuuuuuuuuuuu

Pagelof2 0001^8' FORMIVOA vvvx.o 3/90

~AR3"l 651*0

r^h Nam

Project N

Matrix: (

Sample w

Level:

% Moisti

GCColui

SoilExtn


e: CHEMTECH Contract: US EPA REGION III

o.: A446-S ' Site: Location:

soil/water) SOIL

t/vol: 5.0 (g/mL) G

(low/med) LOW

ire: not dec. 29

Lab Sample ID:

SAMPLE NO.

0770320D36

Group:

O40096

LabFileID:E1100.D

Date Received:

Date Analyzed:





--

14

3/21/95

3/24/95

1.0

QU

.

(uL)

Page 2 of 2FORM IVOA ^ 3/9°

AR3l65t*l •

1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ————

0770320D37Lab Name: CHEMTECH Contract: US EPA REGION II


Matrix: (soil/water) _SOIL Lab Sample ID: O40097

Sample wt/vol: 5.0__(g/mL) G Lab File ID: E1092.D






75-71-874-87-374-83-975-01475-00-375-09-267-64-175-15-075-354 •75-344540-59-067-66-3107-06-278-93-371-55-656-23-575-27478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18479-34-5108-88-3108-90-710041-410042-5

DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoineCarbon Disulfide1,1-Dichloroethene1,1-Dichloroethanel,2-Dichloroethene(total)Chloroform1,2-Dichloroethane2-Butanone1 , 1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzenetrans-9. ,3-DichloropropeneBromoform4-Mediyl-2-Pentanone2-HeximoneTetrachloroethene1, 1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrcn;

1414141414132214141414141414141414141414141414.14141414141440141414

UUUuuJB

U-UUU

~ uuuuuuuuuuuuuuuuuuuuu

Page 1 of 2x FORMIVOA 000166 3/9°

A.R3I65H2

Lab Nam

Project N

Matrix:

Sample w

Level:

% Moisti

GCColui

Soil Extn




[soil/water) SOIL

t/vol: 5.0 (g/mL) G

(low/med) LOW

ire: not dec. 30

Lab Sample ID:

Lab File ID:

Date Received:

Date Analyzed:




*•


*

14

SAMPLE NO.

0770320D37

Group:

O40097

E1092.D

3/21/95

3/23/95

1.0

Qu

———— £

(uL)

001*'

Page 2 of 2

flR3l65»,3 roSMIV°A


077IJ320D37BLab Name: CHEMTECH Contract: US EPA REGION II'

Project No.: A446-S Site: _____ Location: __________ Group:


Sample wt/vol: 5.0 (g/mL) G Lab File ID; E1095.D


% Moisture: not dec. 51__ Date Analyzed: 3/23/95


Soil Extract Volume: _\.____(uL) , . Soil Aliquot Volume: ___ (uL)


75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-410042-5

DiclilorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethyiene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1,1-Dichloroethanel,2-Dichloroethene(total)Chloroform1 ,2-Dichloroethane2-Butanone1 , 1 , 1-TrichloroethaneCarixm TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-Ii ,3-DichloropropeneTrichloroetheneDibromochloromethane1, 1,2-TrichloroethaneBemienetranii-1 ,3-DichloropropeneBrornoform4-Methyl-2-Pentanone2-Hftxanone .Tetr,ichloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene

2020202020191902020202020202020202020202020202020202020202047202020

UUuuuJB

Uuuuuuuuuuuuuuuuuuuuuu

uuu

000175

Page 1 of2FORMIVOA 3/90

AR3I65U


Lab Name: CHEMTECH Contract: US EPA REGION IE






Lab Sample ID:

SAMPLE NO.

0770320D37B

Group:

O40100


Date Received:

Date Analyzed:




1330-20-7 Xylenes(tptal) 20

3/21/95

3/23/95

1.0

QU

_

(uL)

ooorPage 2 of2

FORMIVOA . 3/90

Appendix DReviewed and Corrected

Tentatively Identified Compounds

-AR3I651*'6

IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770306PW1

Lab Name: CHEMTECH_________________ Contract: US EPA REGION III

Project No. A43S Site: _____ Location: _________ Group:

Matrix: (soil/water) WATER Lab Sample ID: O39493

Sample wt/vol: 25.0 (g/mL) ML - LabFileID:L1145.D

Level: (low/med) _______ Date Received: 3/8/95

% Moisture: not dec. _________ Date Analyzed: 3/9/95

GC Column: DB624______ ED: 0.53 (mm) Dilution Factor: 1.0


Concentration Units:Number TICs found: 1___ (ug/L or ug/Kg) ug/L

CAS Number1. 110-54-3 ———2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Namei L\f A &Uw

•

.

RTf f*\-*••>*•

-

Est. Cone.———— 7—

-

Q—— J-

IRMI VOA-TIC 000041 3/90


Lab Name: CHEMTECH _______________ Contract: US EPA REGION EQ


Matrix: (soil/water) WATER Lab Sample ID: 039494

Sample wt/vol: 25.0 (g/mL) ML ,-• Lab File ID: LI 146.D


% Moisture: not dec. _______ Date Analyzed: 3/9/95

GC Column: DB624 ^ ^ ID: 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: _______(uL) Soil Aliquot Volume: _____ (uL)* > - , - ' . . - ' . . ^ - - . , . . . - - . . .

Concentration Units:Number TICs found: __ 1 ._.,_. _ _ . ' (ug/L or ug/Kg) ug/L

CAS Numljer, 1. 110-54-3 ——2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound NameHexane —————————————

1

,

RT—— 5rS3-

Est Cone.—— 6rfi—

'- _.

Q— j_

. "„. ; FORMI VOA-TIC 000049 3/9°A f^ I /* r- t *» *' • - • , ' >;, \* ** \*r \j £ \j

AR3 165^8

IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS Q770306PW4

Lab Name: CHEMTECH__________________. Contract: US EPA REGION in

Project No. A435 Site: _____ Location: __________ Group:

Matrix: (soil/water) WATER Lab Sample ED: O39495

Sample wt/vol: 25.0 (g/mL) ML -' Lab File ED: LI 147.D



GC Column: DB624 ED; 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: _______(uL) Soil Aliquot Volume: _____ (uL)


CAS Number1. 110-54-3 ———2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound NameHexaae ———————————

1

i

RT5M

EstConc.—— fc?—

*•

Qw"

flf?3l65I»9 FORMIVOA-11C °0005S

4 IE SAMPLENO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS U770306W17


Project No. A435 Site: _____ Location: _________ Group:


Sample wt/vol: 25.0 (g/mL) ML - Lab File ID: LI 142.D

Level: (low/med) "___ Date Received: 3/8/95

% Moisture: not dec. ______ Date Analyzed: 3/9/95

GC Column: DB624 __ ED: 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: _______(uL) Soil Aliquot Volume: __ __ (uL)

"Concentration Units:Number TICs found: 1 (ug/L or ug/Kg) ug/L

CAS Number1. 110-54-3 ———2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound NameHexanc —————————————

t

i

RT- «j -yt

Est. Cone.——— 5rt—

' -

Q— t—

- FORMI VOA-TIC 000019 3/90

AR3J6550

IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS Q770306W19

Lab Name: CHEMTECH_____________,______ Contract: US EPA REGION Ed

Project No. A435 Site: ______ Location: _________ Group:


Sample wt/vol: 25.0 (g/mL) ML - Lab File ID:L1143.D

Level: (low/med) ________ Date Received: 3/8/95



Soil Extract Volume: ________(uL) Soil Aliquot Volume: _____ (uL)

Concentration Units:Number TICs found: 1 . (ug/L or ug/Kg) ug/L

CAS Number1. 110*540 ———2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name[lexane —————————————

I

RTf etj*JnJt*

EstConc.. i . . ^ £J.J

-

QJ

TORMI VOA-TIC 0000 6

;- .-:•.-"-. ' IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770306W20

Lab Name: CHEMTECH________________ Contract: US EPA REGION III



Sample wt/vol: 25.0 (g/mL) ML -- Lab FileID:L1144.D

Level: (low/med) ____' ' Date Received: 3/8/95

56 Moisture: not dec. Date Analyzed: 3/9/95

GC Column: DB624 ED: 0.53 (mm) Dilution Factor __U{__

Soil Extract Volume: _;______^uL) Soil Aliquot Volume: ___ __ (uL)

Concentration Units:Number TICs found: 1____ (ug/L or ug/Kg) ug/L

CAS Number1. 110-M-3 ———2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound NameHexane ————————————

'

RT—— 5-53-

Est. Cone.—— 6r6—

• -

Q— j_

AR3I6552- FORMIVOA-TIC 000033 3/90

IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770307TB1

Lab Name: CHEMTECH__________________ Contract: US EPA REGION ffl

Project No. A435 Site: _______ Location: _________ Group:

Matrix: (soil/water) WATER . Lab Sample ED: 039496

Sample wt/vol: 25.0 (g/mL) ML „•• Lab File ID:L1148.D



GC Column: DB624 ED: 0.53 (mm) Dilution Factor 1.0


Concentration Units:Number TTCs found: 2 (ug/L or ug/Kg) ug/L

CAS Number1.2. 110-54-33.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound NameUnknownHexane

•

*

RT3.635.52

EstConc.2.213

1 ^.

QJJ

000065 3/9°

; IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770307W02

Lab Name: CHEMTECH _________ Contract: US EPA REGION in

Project No. A435 Site: . Location: _________ Group:


Sample wt/vol: _ 25.0 (g/mL) ML --• Lab File ID:L1157.D

Level: (low/med) . • Date Received: 3/9/9.5

% Moisture; not dec. _______ Date Analyzed: 3/11/95


Soil Extract Volume: ________(uL) Soil Aliquot Volume: ___ (uL)i ' , . . . . . . - - - -

, Concentration Units:Number TICs found: ___ 0___ (ug/L or ug/Kg) ug/L

CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name RT Est. Cone.

.

Q

FOR^I VOA-TIC 000073 3/90

A R3T65:§iT'"'"''.'

IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770307W22

Lab Name: CHEMTECH____________________ Contract: US EPA REGION III



Sample wt/vol: 25.0 (g/mL) ML - Lab FileID:L1163.D


% Moisture: not dec. ________ Date Analyzed: 3/12/95

GC Column: DB624______ ED: ,0.53 (mm) Dilution Factor: 1.0


Concentration Units:Number TICs found: 0 (ug/L or ug/Kg) ug/L

CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name

\

RT Est. Cone.

•-.

Q

AR3J6555F°RMIVOA~11C 000093 3/9°


Lab Name: CHEMTECH__________________ Contract: US EPA REGION III


Matrix: (.soil/water) WATER Lab Sample ID: 039586

Sample wt/vol: 25.0 (g/mL) ML ,- Lab File ID: LU58.D

Level: (low/med) _______ . , Date Received: 3/9/95

% Moisture: not dec. _^_____ Date Analyzed: 3/11/95

GC Column: DB624 ____ ID: 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: ________(uL) Soil Aliquot Volume: _____ (uL)

Concentration Units:Number TICs found: ___ 0___ (ug/L or ug/Kg) ug/L

CAS Number1.2.3.

. 4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name

v

•

RT

,

Est. Cone. Q

"A'R3|fiC:qc FORM I VOA-TIC 000080 3/90


Lab Name: CHEMTECH___________________ Contract: US EPA REGION ETC

Project No. A435 Site: ______ Location: __________ Group:






Soil Extract Volume: _________(uL) Soil Aliquot Volume: ______ (uL)


CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name

•

*

.

RT Est. Cone.

,

Q

A R 3 16557 FC*M I VOA~TIC 000086 3/90


Lab Name: CHEMTECH_____________• Contract: US EPA REGION EH



Sample wt/vol: __25.0 (g/mL) ML -' Lab File ID: LI 164. D

Level: (low/med) _______ Date Received: _3/9/95_

% Moisture: not dec. . ...... - Date Analyzed: 3/12/95



Concentration Units:Number TICs found: _0____ (ug/L or ug/Kg) ug/L

9

CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name

'

RT Est. Cone. Q

flnol6558 FORMI VOA-TIC 000100 3/9°


Lab Name: CHEMTECH___________________ Contract: US EPA REGION ffl

Project No. A43S Site: ______ Location: _________ Group:

Matrix: (soil/water) WATER Lab Sample ID: O39S90

Sample wt/vol: 25.0 (g/mL) ML -• Lab Hie ED: LI 165.D






CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name

-

'

*

RT Est, Cone. Q

»

165 FORMIVOA-TIC 000107 3/9°

_; . "-,'"": ,1E SAMPLEJSTO, VOLATILE ORGANICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUNDS 0770308W03

Lab Name: CHEMTECH _________________ Contract: US EPA REGION EQ



Sample wt/vol: 25.0 (g/mL) ML -- Lab File ID; L1174.D

Level: (low/med) _ ______ Date Received: 3/10/95

% Moisture: not dec. _______ Date Analyzed: J3/12/95

GC Column: DB624____' .ED; 0.53 (mm) Dilution Factor __1.0__

Soil Extract Volume: ____ (uL) Soil Aliquot Volume: ______ (uL)

Concentration Units:Number TICs found: 0 • (ug/L or ug/Kg) ug/L

CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name

,

t •

RT [Est Cone.1

„

«

Q

FORMI VOA-TIC «««-«-• 3/9°flR3l6560 000135


Lab Name: CHEMTECH___________________ Contract: US EPA REGION Ed


Matrix: (soil/water) WATER - LabSgmpleED: O39S93

Sample wt/vol: 25.0 (g/mL) ML -' Lab FileID:L1168.D

Level: (low/med) _________ Date Received: 3/9/95


GC Column: DB624______ ED; 0.53 (mm) Dilution Factor: 1.0



CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name

•

RT Est. Cone.

-

Q

AR3/656/ FORM I VOA-TIC 000128 3/90

" - - IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 077030829B

Lab Name: CHEMTECH . Contract: US EPA REGION Ed


Matrix: (soil/water) WATER ' Lab Sample ED: 039591

Sample wt/vol: 2S.O___(g/mL) ML - Lab File ED:L1166.D

Level: (low/imed) _______ Date Received: 3/9/95

% Moisture: not dec. ' . . : . , , , . . Date Analyzed: 3/12/95

GC Column: DB624 ____ ED: 0.53 (mm) Dilution Factor; 1.0


, Concentration Units:Number TICs found: 0 (ug/L or ug/Kg) ug/L

CAS NumberI.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name

•

'

RT Est. Cone.

• _

Q

.-- FORMIVOA-TIC OOQ114 3/9°AR3I6562

IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 077030829C

Lab Name: CHEMTECH___________________ Contract: US EPA REGION IE



Sample wt/vol: 25.0 (g/mL) ML - Lab File ID:L1167.D


% Moisture: not dec. Date Analyzed: 3/12/95

GC Column: DB624 ED; 0.53 (mm) Dilution Factor: 1.0



CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name

•

RT Est. Cone. Q

AR3I6563 w""*0 ™' 000121 3/90

IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

II

IDI770309TB1

Lab Name: CHEMTECH _______________ Contract: US EPA REGION in


Matrix: (soil/water) WATER Lab Sample ID: 039678_

Sample wt/vol: 25.0 (g/mL) ML -' Lab File ID: L117S.D

Level: (low/med) _______ Date Received: 3/10/95; ' •, ,. • . . •;•<.• r- : . - • - . ' ' ' -

% Moisture: not dec. __._____ Date Analyzed: 3/12/95• ; 2'__ ~ ' ' , - . ' - ' ' ! . ' ' ' ' - - ' "


Soil Extract Volume: _______(uL) Soil Aliquot Volume: ___ __ (uL)

Concentration Units:Number TICs found: ___ 1___ (ug/L or ug/Kg) ug/L

CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound NameUnknown

•

RT3.72

Est Cone.2.6

-•-. .

QJ

FORM I VOA-TIC 000142 3/90AR3I656U

IE ^AMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770313W06

Lab Name: CHEMTECH_________________ Contract: US EPA REGION IE

Project No. A435 Site: • Location: _________ Group:


Sample wt/vol: 25.0 (g/mL) ML - Lab FileID:L___80_D


% Moisture: not dec. _______ , Date Analyzed: 3/16/95


Soil Extract Volume: __________(uL) Soil Aliquot Volume: ______ (uL)


CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name

•

RT Est. Cone.

-

Q

AR3 I 6565 FORMI VOA-TIC 000149 3/9°

ME SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770313W07




Sample wt/vol: 25.0 (g/mL) ML -•' LabFileID:L118LD

Level: (low/med) ' ___ Date Received: _3/15V95_

% Moisture: not dec. __ __' Date Analyzed: 3/16/95


Soil Extract Volume: (uL) Soil Aliquot Volume: _____ (uL)

Concentration Units:Number TICs found: 0___ . . .' . (ug/L or ug/Kg) ug/L

CAS Numtier1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name

.

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FORM I VOA-TIC n A n i r- * ' 3/90a -. ~ ruKM j; YUA-UU A n n •> i- r»SR3J6566 OOOloB

IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770313W6D

Lab Name: CHEMTECH_____________;____ Contract: US EPA REGION ffl

Project No. A447 Site: _____ Location: ___________ Group:


Sample wt/vol: 25.0 (g/mL) ML -' Lab File ID:L1189.D

Level: (low/med) _________ Date Received: 3/15/95



Soil Extract Volume: _______(uL) Soil Aliquot Volume: _______ (uL)


CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name

i

RT EstConc.

• -

Q

AR3i6567RMIVOA-Tlc 000015 3/90

IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS CI770313W09

Lab Name: CHEMTECH_________________ Contract: US EPA REGION EP

Project No. A447 Site: ______ Location: _________ Group:


Sample wt/vol: 25.0 (g/mL) ML ,- Lab FileED:L1190.D

Level: (low/med) __\_______ Date Received: 3/15/95

% Moisture; not dec. .___ . Date Analyzed: 3/19/95

GC Column: DB624 EO: 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: __________(uL) Soil Aliquot Volume: _____ (uL)


<l

CAS Number1.2.3.

. 4.5.6.7.8.

* 9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name

i

RT Est Cone. Q

•!_ FORM I VOA-TIC 000022 3/90AR3I6568


Lab Name: CHEMTECH____________________ Contract: US EPA REGION III


Matrix: (soil/water) WATER • Lab Sample ID: O39828

Sample wt/vol: 25.0 (g/mL) ML -• LabFileID:L1191.D





Concentration Units:Number TTCs found: 0____ (ug/L or ug/Kg) ug/L

CAS NumberI.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name

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RT Est, Cone.

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AR3 16569 FORMIVOA-TIC 000029 3/90

, r , ; IE .'. SAMPLE NO..... VOLATILE ORGANICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUNDS 0770313W14


Project No. A447 Site: • Location: _____________ Group:


Sample wt/vol; 25,0 (g/mL) ML -- LabFileID:L1192.D

Level: (low/med) _______ Date Received: 3/15/95_

% Moisture: not dec. _______ Date Analyzed: 3/19/95_

GC Column: DB624______ EP; 0.53 (mm) Dilution Factor: 1.0 _


; - Concentration Units:Number TICs found: ___ 0 (ug/L ot ug/Kg) ug/L

CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name

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RT Est. Cone.

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Q

FORM I VOA-TIC 000035 3/90AR316570


Lab Name: CHEMTECH__________________ Contract: US EPA REGION EQ

Project No. A447 Site: _______ Location: _________ Group:


Sample wt/vol: 25.0 (g/mL) ML - LabFileID:L1193.D



GC Column: DB624___________ ED: 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: _________(uL) Soil Aliquot Volume: ________ (uL)


CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.


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AR31657! FORM I VOA-TIC 000042 3/9°


Lab Name: CHEMTECH_________________ Contract: US EPA REGION EQ

Project No. A447 Site: _____ Location: _______' Group:

Matrix: (soil/water) WATER Lab Sample ED: 039831

Sample wt/vol: 25.0 (g/mL) ML ',- Lab FileID:L1194.D

Level: (low/med) . . ' . . . . . . Date Received: 3/15/95

% Moisture: not dec. _______ Date Analyzed: _3/19/_95_

GC Column: DB624 ED: ,0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: ___ (uL) Soil Aliquot Volume: _ (uL)

, -Concentration Units:Number TTCs found: ___ 0___ (ug/L or ug/Kg) ug/L

CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name

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RT EstConc.

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FORM I VOA-TIC 000048 3/90

•AR3I6572

IE - SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770313PW33

Lab Name: CHEMTECH_________________ Contract: US EPA REGION ETC






GC Column: DB624______ ED; 0.53 (mm) Dilution Factor; 1.0

Soil Extract Volume: _______(uL)' Soil Aliquot Volume: _____ (uL)


CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name

t

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m

AR3I6573 FORM I VOA-TIC 000056 3/9°

rr ilE SAMPLE NO.: VOLATILE ORGANICS ANALYSIS DATA SHEET

TENfAtrVELY IDENTIFIED COMPOUNDS 0770314TB1

Lab Name: CHEMTECH ______;_______ Contract: US EPA REGION ffl

Project No. A447 Site: . Location: _________ Group:


Sample wt/vol: 25.0 (g/mL) ML „, Lab File ID:U196.D

Level: (low/med) __ _ _ _ _ _ Date Received: 3/15/95

% Moisture: not dec. . • Date Analyzed: 3/19/95


Soil Extract Volume: (uL) Soil Aliquot Volume: _____ (uL)

. : Concentration Units:Number TICs found: 0 (ug/L or ug/Kg) ug/L

CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.


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Lab Name: CHEMTECH___________________ Contract: US EPA REGION EH


Matrix: (soil/water) WATER Lab Sample ED: 039967

Sample wt/vol: 25.0 (g/mL) ML ,. LabFileEO:L1197.D



GC Column: DB624 ED; 0.53 (mm) Dilution Factor. 1.0



CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name

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RT Est Cone.

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AR3I6575 FORM I VOA-TIC 000072 3/90

^ -IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770314PW5

Lab Name: CHEMTECH_________________ Contract: US EPA REGION m


Matrix: (soil/water) WATER Lab Sample ED:. O39968


Level: (k»w/med) _______ Date Received: _3/16/95_

% Moisture: not dec. . . •__ Date Analyzed: 3/19/9!)_


Soil Extract Volume: '_____(uL) Soil Aliquot Volume: ______ (uL)

1 Concentration Units:Number TICs found: 1___. . (ug/L or ug/Kg) ug/L

CAS Number

2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name

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RT (Est. Cone."5 £1 1 IT

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^316576 FORMIVOAJnc 000081 3/90


Lab Name: CHEMTECH_________________ Contract: US EPA REGION EH


Matrix: (soil/water) WATER , Lab Sample ID: O39969


Level: (low/med) _____' Date Received: 3/16/95



Soil Extract Volume: __________(uL) Soil Aliquot Volume: _____ (uL)

Concentration Units:Number TICs found: 0 ___ (ug/L or ug/Kg) ug/L

CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name

i

RT Est. Cone.

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Q

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SR3I6577 FORM I VOA-TIC 000089 3/90

IE SAMPLE NO.VOLATELE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770315TB1




Sample wt/vol: 25.0 (g/mL) ML „- Lab FileID:L1200.D

Level: (low/med) _______ Date Received: j/16/95_

% Moisture: not dec. ________ Date Analyzed: _3/19/95_

GC Column: DB624________ ED: '0.53 (mm) Dilution Factor: __U)__

Soil Extract Volume: _______(uL) Soil Aliquot Volume: ___ __ (uL)

; Concentration Units:Number TICs found: Q .... (ug/L or ug/Kg) ug/L

41

CAS Number. 1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29. .30.

Compound Name

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FORM I VOA-TIC n n n A n r 3/90AR3(6578 """•""""• 0.00096





Sample wt/vol: 25.0 (g/mL) ML - Lab File ED; L1203.D

Level: (low/med) _______ ' Date Received: 3/16/95





CAS Number•4, ————————2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound NameWafcaewa —————————————

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j

RT—— Z&t-

ist. Cone.—— &*—

-

Q—— j ——

AR3I6579 FORMIVOA-TIC Q00103 3/9°

v llE ' SAMP1LENO.VOLATILE ORGANICS ANALYSIS DATA SHEETtfiNTATEVELY IDENTIFIED COMPOUNDS 077031SW12

Lab Name: CHEMTECH______' Contract: US EPA REGION III

Project No. A447___ Site: Location: ___________ Group:

Matrix: (soil/water) WATCR Lab Sample ED: 039972

Sample wt/vol: __25.0 (g/mL) ML -' Lab File ID: L1202.D


% Moisture: not dec. _______ Date Analyzed; 3/19/95 _GC Column: DB624 ED; 0.53 (mm) Dilution Factor __1.0


Concentration Units:Number TICs found: ___0___ (ug/L or ug/Kg) ug/L

CAS NumberI.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name RT Est Cone.

-

Q

;AR3!658G





Sample wt/vol: 25.0 (g/mL) ML -' Lab File ID: L1207.D


% Moisture: not dec. _______ Date Analyzed: 3/20/95GC Column: DB624_______ ED; 0.53 (nun) Dilution Factor 1.0

Soil Extract Volume: _______(uL) Soil Aliquot Volume: ^ ^ (uL)


CAS Number_L, ————————2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound NameyaknewH ————————————

RT——— Zr6rf-

Est. Cone.—— i-fi— .

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Q—— f ——

FORM I VOA-TIC ^ 3/90000119


Lab Name: CHEMTECH__________________ Contract: US EPA REGION EQ

Project No. A447 • Site: _____ Location: _________ Group:

Matrix: (soU/water) WATER Lab Sample ID: O400S2

Sample wt/vol: 25.0 (g/mL) ML - Lab File ED; L1208.D


% Moisture: not dec. _____' Date Analyzed: 3/20/95_

GC Column: DB624______ ED; 0.53 (mm) Dilution Factor: __L£ _

Soil Extract Volume: ' ____(uL) Soil Aliquot Volume: _____ (uL)

Concentration Units:Number TICs found: ___0___ (ug/L or ug/Kg) ug/L

CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.


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AR3I658-2 K"*"™-™ 000127

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Lab Name: CHEMTECH_________________ Contract: US EPA REGION in

Project No. A447 Site: _____ Location: ____________ Group:


Sample wt/vol: 25.0 (g/mL) ML - Lab File ED: L1209.D

Level: (low/med) ___________ Date Received: 3/17/95

% Moisture: not dec. Date Analyzed: 3/20/95

GC Column: DB624 ______ ED: 0.53 (mm) Dilution Factor; 1.0

Soil Extract Volume: _______ (uL) Soil Aliquot Volume; (uL)

Concentration Units:Number TICs found: 1 ___ (ug/L or ug/Kg) ug/L

CAS Number— fc ————— , ——2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound NameUnkaawB — : ——————————

RT—— 3 46-

Est, Cone.| ——— S—-

Q—— J ——

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AR3 { 6583 FORMI VOA-TIC 000135 3/90


Lab Name: CHEMTECH________________ Contract: US EPA REGION ffl

Project No. A447___ Site: _____ Location: _________ Group:


Sample wt/vol: __25.0__(g/mL) ML -' LabFileID:L1210.D


% Moisture:: not dec. ________ Date Analyzed: 3/20/9S

GC Column: DB624 ED; 0.53 (mm) Dilution Factor 1.0

Soil Extract Volume: __ (uL) Soil Aliquot Volume: __ _ (uL)


CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.IS.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name.

i

RT (Est Cone. Q

FORMI VOA-TIC - 3/900 0 0 1 4 -


Lab Name: CHEMTECH_________________ Contract: US EPA REGION Ed

Project No. A447 Site: ________ Location: _________ Group:


Sample wt/vol: 25.0 (g/mL) ML ,- LabFileID:L1211.D



GC Column: DB624 EO: 0.53 (mm) Dilution Factor 1.0

Soil Extract Volume: _______(uL) Soil Aliquot Volume: _____._ (uL)


CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Namei

i -

RT (Est. Cone.

•

1

Q

lk>RMIVOA-'nc °00143


Lab Name: CHEMTECH ____________ Contract: US EPA REGION ffl

Project No. A447 Site: _____ Location: ____________ Group:

Matrix: (soil/water) WATER Lab Sample ID:. O40056

Sample wt/vol: 25.0 (g/mL) ML -• Lab File ID: L1212.D


% Moisture: not dec. _______ Date Analyzed: _3/20/95_

GC Column: DB624____, ID: 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: (uL) Soil Aliquot Volume: __ (uL)

Concentration Units:Number TICs found: 0_____ (ug/L or ug/Kg) ug/L

CAS NumberI.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name

i

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RT Est. Cone.

• -

Q

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FORM * VOA-TIC 000155 3/90


Lab Name: CHEMTECH_______________ __ Contract: US EPA REGION III

Project No. A4S5 Site: ______ Location: _______• Group:


Sample wt/vol: 25.0 (g/mL) ML -• Lab File ID: L1232.D


% Moisture: not dec. • Date Analyzed: . 3/25/95




CAS Number

2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound NameUnit-own ————————————

RT—— SrW-

Est Cone.——— £9—

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Q1 j —

A R 3 / 6 5 £ 7 FORMl VOA"TIC

IE • SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770320TB1

Lab Name: CHEMTECH_____________-_____ Contract: US EPA REGION III

Project No. A45S Site: _____ Location: _______'• Group:


Sample wt/vol: 25.0 (g/mL) ML - Lab File ID: L1243.D



GC Column: DB624 __' ID: 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: ___ (uL) Soil Aliquot Volume: _____ (uL)

Concentration Units:Number TICs found; 0 (ug/L or ug/Kg) ug/L

CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.


' -

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FORMI VOA-TIC 000 71 3/90

AR3I6588



Project No. A4S5 Site: _____ Location: ___________ Group:


Sample wt/vol: 25.0 (g/mL) ML ' Lab File ID: L1233.D






:AS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.


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Lab Name: CHEMTECH_____________• Contract: US EPA REGION III

Project No. A45S Site: _____ Location: __________ Group:


Sample wt/vol: 25.0 (g/mL) ML - Lab File ID: LI235.D



GC Column: DB624 ______ ED: 0.53 (mm) Dilution Factor: 1.0

Soil Exiract Volume: ________(uL) Soil Aliquot Volume: _____ (uL)


CAS Number-4, ———————2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound NameC _T— I IJJL j-y •. _m

,

RT—— 3*69-

Est Cone.—— 24-

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Q— , ——

000 35FORM I VOA-TIC 3/90





Sample wt/vol: 25.0 (g/mL) ML ' Lab File ID: L1234.D




Soil Extract Volume: __________(uL) Soil Aliquot Volume: ______ (uL)


CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.


-

Q

FORMI VOA-TIC 3/90

7AVOLATILE CONTINUING CALIBRATION CHECK

Lab Name: CHEMTECH_______ Contract: US EPA REGION III

Project No. A446-S____ Site: _____ Location: _____ Group: _______

Instrument ID: VOA1__________ Calibration Date: 3/18/95 Time: 0956

Lab File ID: E1067.D_____;____ Init Calib. Date(s): 2/24/95 2/24/95

Heated Purge: (Y/N) Y Init Calib. Times: 0918 T256

GC Column: DB624 EO; 0.53 (mm)

COMPOUND

i

•

Toluene-d8Bromofluorobenzene1 ,2-Dichlorocthane-d4

RRF

1.0160.6941.413

RRF50

0.9860.6561.931

MINRRF

0.0100.2000.010

%D

3.05.5-36.7

MAX%D

100.0|25.0100.0

All other compounds must meet a minimum RRF of 0.010.;

Page 2 of 2 , .AR3 i 6592FORM VOA 3/9°



Project No. A446-S_____ Site: _____ , Location: ______ Group:

Lab File ID: E1067.D Init Calib. Date(s): 2/24/95 2/24/95

Heated Purge: (Y/N) Y Init Calib. Times: 0918 1256

GC Column: DB624 ED; 0.53 (mm)

COMPOUNDDichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroetnaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1.1-Dichloroethanetrans-1 ,2-Dichloroethenecis-l,2-DichloroetheneChloroform1,2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochlorometbane1 , 1 ,2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroediene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrcnem+p-Xyleneso-xylene

RRF0.5170.6170.4020.6610.2921.7190.4342.9591.9232.7282.0791.4372.9361.8230.1660.5400.5350.7020.4330.5550.3930.6410.3690.9120.3950.4960.4890.3280.5560.7041.2240.9771.4840.8770.5441.133

RRF500.3370.5680.4790.6300.4432.7260.4443.9342.3273.2232.4331.4013.4631.8730.1010.6050.4710.7680.3600.6140.3750.5370.2871.0300.4160.3940.2700.1590.4500.4371.2040.7301.4510.8080.5271.114

MINRRF

0.1000.100

0.1000.200

0.2000.100

0.1000.1000.200

0.2000.3000.1000.1000.5000.1000.100

0.2000.5000.4000.5000.1000.3000.3000.300

%D34.& >7.9-19.24.7

< 51.7< 58.6 >

-2.3< 3.QJ-21.0-18.1-17.02.5-17.9-2.7

f"39.2_H.T -12.0

12.0-9.416.9-10.64.616.222.2-12.9-5.320.6

C5L5_>19.1

C37.g1.6

CT25.32.27.93.01.7

MAX%D100.0100.025.025.0100.0100.0100.0100.025.025.0100.0100.0•25.025.0'100.025.025.025.0100.025.025.025.025.025.025.025.0100.0100.025.025.025.025.025.025.025.025.0

Instrument ID: VOA1 Calibration Date: 3/18/95 Time: 0956

All other compounds must meet a minimum RRF of 0.010. 000205

Pagei0f2 AR3I6593


Lab Name: CHEMTECH_____' Contract: US EPA REGION III

Project No. A446-S_____ Site: _____ Location: ______ Group:


Lab File ID: E1051.D______\_____"Init Calib. Date(s): 2/24/95 2/24/95

Heated Purge: (Y/N) . Y Init. Calib. Times: 0918 (256

GC Column: DB624 ED: 0.53 (mm)

COMPOUND

Toluene-d8Bromofluorobenzenel,2-Dichloroetliane-d4

RRF

1.0160.6941:413

RRF50

0.9870.6462.014

MINRRF

0.0100.2000.010

%D

2.96.9-42.5

MAX%D

100.025.0100.0

All other compounds must meet a minimum RRF of 0.010.000204Page2of2 •

FORM VH VGA flR3|659U •-.*»

7A •VOLATILE CONTINUING CALIBRATION CHECK


Project No. A446-S____ Site: ____ Location: ________ Group:

Lab File ID: E1051.D_____________ l. Calib. Date(s): 2/24/95 2/24/95

Heated Purge: (Y/N) Y Init Calib. Times: 0918 1256


COMPOUNDDichlorodifluoromethaneChloromediancBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroemene1 , 1-Dichloroethanetrans- 1 ,2-Dichloroethenecis-1 ,2-DichloroetheneChloroform1 ,2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1, 1,2-TrichloroethaneBenzenetrans-1, 3-DichloropropcncBromofbrm4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1 , 1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrencm+p-Xyleneso-xylene

RRF0.5170.6170.4020.6610.2921.7190.4342.9591.9232.7282.0791.4372.9361.8230.1660.5400.5350.7020.4330.5550.3930.6410.3690.9120.3950.4%0.4890.3280.5560.7041.2240.9771.4840.8770.5441.133

RRF500.3850.6220.4800.7470.4112.5400.4454.1992.6303.3382.5931.6843.6282.0080.1010.6270.5280.8200.3940.6360.4090.5870.3091.0340.4230.3970.3080.1740.4630.4531.1830.7491.4370.8450.5271.091

MENRRF

I

0.1000.100

0.1000.200

0.2000.100

0.1000.1000.200

0.2000.3000.1000.1000.5000.1000.100

1

0.2000.5000.4000.5000.1000.3000.3000.300

%D*75.5 >-0.8-19.4-13.0Q0.8

-2.5C31.9CSeTsJ?-22.4-24.7-17.2-23.6-10.1CJ2-W-16.11.3-16.89.0-14.6-4.18.416.3-13.4-7.120.0

1137.0-T371C?16.7

C.3SJ*?3.323.33.23.63.03.7

MAX%D100.0100.025.025.0100.0100.0100.0100.025.025.0100.0100.025.025.0100.025.025.025.0100.025.025.025.025.025.025.025.0100.0100.025.025.025.025.025.025.025.025.0


All other compounds must meet a minimum RRF of 0.010.000203

Pagelof2 AR3I6595

6A . ^ r .. N ,,VOLATILE ORGANICS INITIAL CALIBRATION DATA " ~" " "

Lab Name: CHEMTECH________ Contract: US EPA REGION III

Lab Code: CHEM_____ Case No.: A446-S SAS No.: ' SDG No.: _______

Instrument ID: VOA1_____ Calibration Date(s): 2/24/95 2/24/95Heated Purge: (Y/N) _Y_ Calibration Times: 0918 1256

GC Column DB624 _____ EOT 0.53 (mm)

Lab File ID: RRF10 = E1002.D RRF20 = E1004.DRRF50 = E1001.D RRFlOO = E1005.D RRF200 = E1003.D

COMPOUNDChloromethaneDichlorodifiuoromethaneBromomethane *Vinyl Chloride *ChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichlorocthene *1,1-Dichloroethane *trans- 1 ,2-Dichloroethenecis-l,2,-DichloroetheneChloroform *1,2-Dichloroethane *2-Butanone1,1,1-Trichloroethane *Zarbon Tetrachloride *Bromodichloromethane *1 ,2-Dichloropropanecis-1, 3-Dichloropropene *Frichloroethene *Dibromochloroinethane *1,1,2-TrichlQroethane *Benzene *trans-l,3-Dichloropropene *Bromoform *4-Methyl-2-Pentanone2-Hexanoneretrachloroetheae *1 , 1 ,2,2-Tetrachloroethane *Toluene *Chlorobenzene *Ethylbenzene *Styrene *n+p-Xylenes *o-xylene ;Foluene-dSBromofluorobenzene *1 ,2-Dichloroethane-d4

RRF100.5730.4420.4340.5510.3651.6910.5482.5361.6232.2631.6891.1652.4441.4610.1490.4760.4530.6180.3770.4800.3420.5920.3330.7910.3420.4720.4690.2830.5240.8031.1500.9021.3740.7670.4891.0490.9650.6911.195

RRF200.6560.5260.4170.7010.2731.9010.7553.0362.0412.9732.2751.5633.2452.2000.3190.6070.5980.7940.4990.6580.4490.7800.4921.0390.4870.6810.8410.5980.6540.6681.4011.1261.6520.9710.5971.2331.2080.7861.736

RRF500.7020.6310.4610.7530.3241.8160.2923.3442.0842.9512.2541.5613.1641.847.0.1140.5710.5870.7320.4460.5620.4260.6470.3540.9490.3950.4640.3660.2330.6040.7011.3091.0301.5950.9420.6041.2521.0340.7041.382

RRFlOO0.5650.4530.3420.6480.2511.6410.3342.8131.9732.7792.1511.4662.9731.9030.1520.5290.5250.7100.4340.5480.3800.6070.3510.9110.3920.4450.4550.3150.4880.7521.1320.8951.3930.8570.5041.0790.9840.6781.494

RRF2000.5900.5310.3590.6490.2461.5440.2403.0661.8932.6742.0261.4312.8561.7040.0990.5150.5110.6550.4080.5250.3690.5780.3170.8710.3610.4190.3140.2110.5130.5981.1260.9351.4080.8460.5241.0510.8890.6121.257

RRF0.6170.5170.4020.6610.2921.7190.4342.9591.9232.7282.0791.4372.9361.8230.166 <0.54010.5350.7020.4330.5550.3930.6410.3690.9120.3950.4960,489 (0.328 t0.5560.7041.2240.9771.4840.8770.5441.1331.0160.6941.413

%RSD9.614.712.611.317.68.22E&10.29.510.511.511.410.714.92.£9.4ll.l9.810.511.911.112.819.010.1

L___l21.3JiHr=_L__'12.511.110.210.18.79.39.88.911.79.015.2

000185

* Compounds .with required minimum RRF and maximum %RSD values.All other compounds must meet a minimum RRF of 0.010. A ft 3 j 6 S Q £


Lab Name: CHEMTECH________ Contract: US EPA REGION ffl

Project No. CHEM_____ Site: A440-S Location: _____ Group:

Instrument ID: VOA1 Calibration Date: 3/18/95 Tune: 0956

Lab File ED: E1067.D__________ Init. Calib. Date(s): 2/24/95 2/24/95

Heated Purge: (Y/N) ____ Init Calib. Times: 0918 1256


COMPOUND

Toluene-d8Bromofluorobenzene1 ,2-Dichloroethane-d4

RRF

1.0160.6941.413

RRF50

0.9860.6561.931

MENRRF

0.0100.2000.010

%D

••-.

•

3.05.5-36.7

MAX%D

100.025.0100.0

All other compounds must meet a minimum RRF of 0.010.

Page2of2 - Q „ . - _ . ^AR3I6597 FORMVHVOA - uuu-^u^ 3/9Q

7A 'VOLATILE CONTINUING CALIBRATION CHECK ,

Lab Name: CHEMTECH ____ Contract: US EPA REGION III


Instrument ED1: VOA1 Calibration Date: 3/18/95 Time: 0956

Lab File ID: E1067.D____. Init Calib. Date(s): 2/24/95 2/24/95

Heated Purge: (Y/N) ____ Init. Calib. Times: 0918 1256


COMPOUNDDichlorodifluoromethaneChloromcdianeBromomethaneVinyl ChloriiieChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1,1-Dichloroetnanetrans-1 ,2-Dichloroethenecis-1, 2-DichloroetfaeneChloroform «1 ,2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1, 3-DichloropropeneTrichloroethcneDibromochloromethane1, 1,2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-Hexanone

' Tetrachloroeihene1,1,2,2-TetrsichloroethaneTolueneChlorobenzeiieEfhylbenzeneStyrenem+p-Xyleneso-xylene

RRF0.5170.6170.4020.6610.2921.7190.4342.9591.9232.7282.0791.4372.9361.8230.1660.5400.5350.7020.4330.5550.3930.6410.3690.9120.3950.4960.4890.3280.5560.7041.2240.9771.4840.8770.5441.133

RRF500.3370.5680.4790.6300.4432.7260.4443.9342.3273.2232.4331.4013.4631.8730.1010.6050.4710.7680.3600.6140.3750.5370.2871.0300.4160.3940.2700.1590.4500.4371.2040.7301.4510.8080.5271.114

MENRRF

0.1000.100

<

(0.1000.200

0.2000.100

i0.1000.1000.200

0.2000.3000.1000.1000.5000.1000.100

0.2000.5000.4000.500 i0.1000.3000.3000.300

%DC_J4,8 >

7.9-19.24.7

T-51.7J5CT-58.6

-2.31-33.0-21.0-18.1-17.02.5-17.9-2.7

L 39.2 2-12.012.0-9.416.9-10.64.616.222.2-12.9-5.320.6

(_44.8 _C51.5 >

19.137.9-21.6

, 25.32.27.93.01.7

MAX%D100.0100.025.025.0100.0100.0100.0100.025.025.0100.0100.025.025.0100.025.025.025.0100.025.025.025.025.025.025.025.0

> 100.0Lioo.o25.025.025.025.025.025.025.025.0

077 3 BOlb

Pan. 1 nf t


AR3I6598 000201


Lab Name: CHEMTECH_________ Contract: US EPA REGION lEt

Project No. CHEM Site: A440-S Location: _______ Group:

Instrument ED: VOA1 Calibration Date: 3/17/95 Tune: 2132

Lab File ID: E1051.D____________ Mt Calib. Date(s): 2/24/95 2/24/95

Heated Purge: (Y/N) _.___ Init Calib. Times: 0918 1256


COMPOUND


RRF

i

1.0160.6941.413

RRF50

0.9870.6462.014

MINRRF

0.0100.2000.010

%D

-

2.96.9-42.5

MAX56D

100.025.0100.0

All other compounds must meet a minimmn RRF of 0.010.

Page2of2 fl P J C q Q n 000200"* H n O f O O y \m

.. - - - •- , • . . - : , 7A

VOLATILE CONTINUING CALIBRATION CHECK

Lab Name: CHEMTECH Contract: US EPA REGION ETC

Project No. CHEM Site: A440-S Location: _____ Group:

Instrument ID: VOAl Calibration Date: 3/17/95 Time: 2132

Lab File ID: E1051.D_______ Init. Calib. Date(s): 2/24/95 2/24/95

Heated Purge: (Y/N) ___ Init Calib. Tunes: 0918 1256


COMPOUNDDichlorodifluoromethaneChloromethane •BromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1 , 1-Dichloroethanecis-l,2-Dichloroethenetrans-1 ,2-DichloroetheneChloroform1 ,2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetracMorideBromodichloromethane1 ,2-Dichloropropanecis-1, 3-Dichlo:ropropeneTrichloroetheneDibromochloromethane1 , 1 ,2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrenem+p-Xyleneso-xylene

RRF0.5170.6170.4020.6610.2921.7190.4342.9591.9232.7282.0791.4372.9361.8230.1660.5400.5350.7020.4330.5550.3930.6410.3690.9120.3950.4960.489

. 0.3280.5560.7041.2240.9771.4840.8770.5441.133

RRF500.3850.6220.4800.7470.4112.5400.4454.1992.6303.3382.5931.6843.6282.0080.1010.6270.5280.8200.3940.6360.4090.5870.3091.0340.4230.3970.3080.1740.4630.4531.1830.7491.4370.8450.5271.091

M1NRRF

0.1000.100

0.1000.200

0.2000.100

0.1000.1000.200

0.2000.3000.1000.1000.5000.1000.100

(0.2000.5000.4000.5000.1000.3000.3000.300

%DT 25.5 J

-0.8-19.4-13.0

I -40.8(~3fl&

-2.5""-41-JLx1-36.8 -22.4-24.7-17.2-23.6-10.1

_ 39.2I>>-16.11.3-16.89.0-14.6-4.18.416.3-13.4-7.120.0

C37.0L2"47.0316.7

-~35.7 :>3.323.33.23.63.03.7

MAX%D100.0100.05.025.0100.0100.0™'100.0100.025.025.0100.0100.025.025.0100.05.025.025.0100.025.025.025.025.025.025.025.0100.0100.0""25.025.025.025.025.025.025.025.0

I

cdtcc

T»_— i -.e


AR3I6600 °001"




Instrument ED: VOA1___________ Calibration Date: 3/17/95 Tune: 0926

Lab File ED: E1035.D__________ Init Calib. Date(s): 2/24/95 2/24/95

Heated Purge: (Y/N) ___ Init Calib. Times; 0918 1256


COMPOUND


RRF

1.0160.6941.413

RRF50

0.7300.5031.637

MINRRF

0.0100.2000.010

%D

••--

28.127.5 \-15.9

MAX%D

100.0;>25.0100.0


Page2of2 AR3I660I FORMVII>OA 000198 3/90

-— — 7AVOLATILE CONTINUING CALIBRATION CHECK

Lab Name: CHEMTECH Contract: US EPA REGION III

Project No. CHEM____ Site: A440-S Location: _____ Group:

Instrument ED; VOA1________ Calibration Date: 3/17/95 Time: 0926

Lab File ID: E1035.D_____ '. Init Calib. Date(s): 2/24/95 2/24/95

Heated Purge: (Y/N) ___ Init Calib. Times: 0918 1256

GC Column: k DB624 ED: 0.53 (nan)

COMPOUNDDichlorodifluoromethaneChlorometharic

. BromomethaceVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroefflene1 , 1-Dichloroethanetrans-1 ,2-Dicliloroethenecis-l,2-DichloroetheneChloroform1 ,2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheioeDibromochloromethane1 , 1,2-TrichloiroethaneBenzenetrans-1 ,3-DicliloropropeneBromoform4-Methyl-2-Pcntanone2-HexanoneTetrachloroediene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrenem+p-Xyleneso-xylene

RRF0.5170.6170.4020.6610.2921.7190.4342.9591.9232.7282.0791.4372.936

. 1.8230.1660.5400.5350.7020.4330.5550.3930.6410.3690.9120.3950.4960.4890.3280.5560.7041.2240.9771.4840.8770.5441.133

RRF500.2950.5130.4440.6260.3272.3840.5014.0242.2583.3822.5731.5043.7372.1470.1360.6590.5000.8700.3740.6760.3760.5830.3191.1060.4690.4330.3290.2080.4210.5431.1970.7%1.5140.8460.5541.173

MENRRF

0.1000.100

0.1000.200

0.2000.100

0.1000.1000.200

0.2000.3000.1000.1000.5000.1000.100

0.2000.5000.4000.5000.1000.300

. 0.3000.300

%D£~42JD

16.9-10.45.3

-12.038'.7I>-15.4

(-36.0-17.4-24.0-23.8-4.6

T -274-2-17.818. I-22.06.5

-23.913.6-21.84.39.013.6-21.3-18.712.7

C32.7 >^ 36.6 >24.322.92.218.5-2.03.5-1.8-3.6

MAX%D100.0100.025.025.0100.0100.0100.0100.025.025.0100.0100.025.025.0100.025.025.025.0100.025.025.025.025.0

\2S.6.25.025.0100.0100.025.025.025.025.025.025.025.025.0

All other compounds must meet a minimum RRF of 0.010.000197

Pare 1 of 2


Lab Name: CHEMTECH_______ Contract: US EPA REGION HI

Project No. CHEM Site: A440-S Location: _____ Group:

.Instrument ID: VOA1 Calibration Date: 3/13/95 Tune: 0937

Lab File ID: E1019.D__________ Init Calib. Date(s): 2/24/95 2/24/95

Heated Purge: (Y/N) ___ Init. Calib. Times: 0918 ' 1256


COMPOUND


RRF

1.0160.6941.413

RRF50

0.7800.5191.706

MINRRF

0.0100.2000.010

%D

••-

22_2_25.2 '"~3X}?I "

MAX%D

100.0}25.0100.0


Page2of2 fl D Q I fi c n ~ -- 000198& n 3 ] 6603 FORM VTT VOA 3/90


Lab Name: CHEMTECH Contract: US EPA REGION in

Project No. CHEM____ Site: A440-S Location: _____ Group:


Lab File ID: E1019.D Init Calib. Date(s): 2/24/95 2/24/95

Heated Purge: (Y/N) ___ Init. Calib. Tunes: 0918 1256

GC Column: DB624 ED; 0.53 (mm) '\l&(-\<0 I

COMPOUN1DDichlorodifluoromethaneChloromedianeBromomethaneVinyl ChlorideChloroethancMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1 , 1-Dichloroedianetrans-1, 2-Dii:hloroethenecisl,2-DichloroetheneChloroform1 ,2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1. 3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-Trichloroethane

I Benzenei trans-1, 3-Dicbloropropene! Bromoform

4-Methyl-2-]Pentanone2-HexanoneTetrachloroethene1 * 1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene ,m+p-Xyleas(total)o-xylene

RRF0.5170.6170.4020.6610.2921.7190.4342.959 .1.9232.7282.0791.4372.9361.8230.1660.5400.5350,7020.4330.5550.3930.6410.3690.9120.3950.4960.4890.3280.5560.7041.2240.9771.4840.8770.5441.133

RRF500.4320.6290.4430.7150.3352.3400.6214.2752.2723.3642.5542.3083.6912.1630.1400.6400.5020.8400.3940.6450.3800.5800.3231.0770.4580.4260.3640.2300.4390.5381.2150.7591.4910.8590.5711.172

MINRRF

0.1000.100

0.1000.200

(0.2000.100

0.1000.1000.200

0.2000.3000.1000.1000.5000.1000.100

0.2000.5000.4000.5000.1000.3000.3000.300

%D16.4-1.9-10.2-8.2-14.736. 0

C-44 >-18.1-23.3-22.8r so-25.7-18.715:7-.-18.56.2-19.79.0-16.23.39.512.5-18.1-15.914.1

C3335C29.9_>21.023.60.722.3-0.52.1-5.0-3.5

MAX%D100.0100.025.025.0100.0100.0100.0100.025.025.0100.0100.025.025.0100.025.025.025.0100.025.025.025.025.025.025.025.0100.0100025.025.025.025.025.025.025.025.0

All other compounds must meet a minimum RRF of 0.010. •'.. ' ... „. >' U"-/J •

ppt.

6AVOLATILE ORGANICS INITIAL CALIBRATION DATA

Lab Name: CHEMTECH _____ Contract: US EPA REGION EQ

Lab Code: CHEM_____ Case No.; A440-S SASNo.: _____ SDGNo.:

Instrument ID: VOA1 Calibration Date(s): 2/24/95 2/24/95

Heated Purge: (Y/N) _Y_ CaUbration Times: 0918 1256

GC Column DB624 ED: 0.53 (mm)

Lab File ID: RRF10 = E1002.D RRF20 = E1004.DRRF50 = E1001.D RRFlOO = E1005.D RRF200 - E1003.D

COMPOUNDChloromethaneDichlorodifluoromethaneBromomethane *Vinyl Chloride *ChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene *1 , 1 -Dichloroethane *trans-1, 2-Dichloroethcnecis-1 ,2,-DichloroetheneChloroform *1,2-Dichloroethane *2-Butanone1,1,1-Trichloroethane *Carbon Tetrachloride *Bromodichloromethane *1 ,2-Dichloropropanecis-1, 3-Dichloropropene *rrichloroethene *Dibromochloromethane *1,1,2-Trichloroethane - *Benzene *trans-l,3-Dichloropropene *Bromoform *4-Methyl-2-Pentanone2-Hexanoneretrachloroethene *1,1,2,2-Tetrachloroethane *roluene *Chlorobenzene *Ethylbenzene *Styrene *m+p-Xylcnes *o-xyleneroluene-48Bromofluorobenzene *1 ,2-Dichloroethane-d4

RRF100.5730.4420.4340.5510.3651.6910.5482.5361.6232.2631.6891.1652.4441.4610.1490.4760.4530.6180.3770.4800.3420.5920.3330.7910.3420.4720.4690.2830.5240.8031.1500.9021.3740.7670.4891.0490.9650.6911.195

RRF200.6560.5260.4170.7010.2731.9010.7553.0362.0412.9732.2751.5633.2452.2000.3190.6070.5980.7940.4990.6580.4490.7800.4921.0390.4870.6810.8410.5980.6540.6681.4011.1261.6520.9710.5971.2331.2080.7861.736

RRF500.7020.6310.4610.7530.3241.8160.2923.3442.0842.9512.2541.5613.1641.8470.1140.5710.5870.7320.4460.5620.4260.6470.3540.9490.3950.4640.3660.2330.6040.7011.3091.0301.5950.9420.6041.2521.0340.7041.382

RRFlOO0.5650.4530.3420.6480.2511.6410.3342.8131.9732.7792.1511.4662.9731.9030.1520.5290.5250.7100.4340.5480.3800.6070.3510.9110.3920.4450.4550.3150.4880.7521.1320.8951.3930.8570.5041.0790.9840.6781.494

RRF2000.5900.5310.3590.6490.2461.5440.2403.0661.8932.6742.0261.4312.8561.7040.0990.5150.5110.6550.4080.5250.3690.5780.3170.8710.3610.4190.3140.2110.5130.5981.1260.9351.4080.8460.5241.0510.8890.6121.257

RRF0.6170.5170.4020.6610.2921.7190.434 <2.9591.9232.7282.0791.4372.9361.8230.166 <0.5400.5350.7020.4330.5550.3930.6410.3690.9120.3950.4960.489 i0.328 <0.5560.7041.2240.9771.4840.8770.5441.1331.0160.6941.413

%RSD9.614.712.611.317.68.242dL10.29.510.511.511.410.714.9-52.99.411.19.810.511.911.112.819.010.114.121.342.3£LL.12.511.110.210.18.79.39.88.911.79.015.2

* Compounds with required minimum RRF and marin tm %RSD values. 0 0 O 1.„,,_,.,~:-:»t>n~,nn,« ^^^ j ^^^


Lab Name: CHEMTECH _______ Contract: US EPA REGION III

Project No. A455-S Site: _____ Location: ______ Gromp:


Lab File ID: L1238.D Init. Calib. Date(s): 1/31/95 1/31/95

Heated Purge: (Y/N) ____ Init Calib. Times: 1022 . 1314


COMPOUND2-Hexanone1, 1,2,2-Tetrachloroethane1 ,3-Dichlorobenzene1 ,4-Dichlorobenzene1 ,2-Dichlorobenzene1 ,2-Dibromo-3-chloropropane

X

.

1 .4-Bromofluorobenzene

RRF0.1310.3370.8840.8790.7500.062

0.521

RRF50.1130.3500.8290.8470.7360.066

0.548

MINRRF

0.5000.6000.5000.400

%D13.7-3.96.23.61.9-6.5

'--• -

-5.2

MAX%D

30.030.030.030.0

M other compoiinds must meet a minimum RRF of 0.010. - '-:'-;

Page2of2 ' - , • • • • fi D Q 1 C C n C 000110urwvr vn vn* ft ft J J 0 u U D 7/Qn


Lab Name: CHEMTECH_________ Contract: US EPA REGION III

Project No. A455-S____ Site: _____ Location: _______ Group:

Instrument ED: VOA1 Calibration Date: 3/25/95 Time: 0940

Lab File ED: L1238.D__________ Init. Calib. Date(s): 1/31/95 1/31/95

Heated Purge: (Y/N) ___ Init. Calib. Times: 1022 1314


COMPOUNDDichlorodifluoromcthaneChloromethaneVinyl ChlorideBromomethaneChloroethane1 , 1-DichloroetheneMethylene ChlorideAcetoneCarbon Disulfidetrahs- 1 ,2-Dichloroemene1 , 1-Dichloroe thanecis-l,2-DichloroetheneBromochloromethaneChloroform2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBenzene1 ,2-DichloroethaneTrichloroethene1 ,2-Dichloropropanc1 ,2-DibromoethaneBromodichloromethanecis-1, 3-DichloropropeneToluenetrans-1 ,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzene *Ethylbenzenem&p-xyleneso-xyleneStyreneBromoform4-Methyl-2-pentanone

RRF0.3300.2640.2690.1240.1280.4790.5160.0760.9530.4730.6200.5370.4700.7040.1420.7560.6191.1980.2850.4600.5000.3820.6690.5571.3110.3930.2580.5370.4520.9451.5901.1421.1650.8620.2640.185

RRF50.1830.2180.2330.0950.1080.4250.259(G.Q49}0.8160.4170.5480.4690.3950.6010.1260.6860.6271.1040.2770.4460.4450.3320.6180.5271.2480.3770.2470.5220.4570.8771.5021.0871.0940.8170.3120.163

MENRRF

0.1000.100

0.100

0.200

0.1000.200

0.1000.1000.5000.1000.300

0.1000.2000.2000.4000.1000.1000.2000.1000.5000.1000.3000.3000.3000.100

%DC44.5>

17.413.423.415.611.3f W*35.5 14.411.811.612.716.014.611.3-9.3-1.37.82.83.011.013.17.65.44.84.14.32.8-1.17.25.54.86.15.2

-18.211.9

MAX%D

30.030.0

30.0

30.0

30.030.0

30.030.030.030.030.0

30.030.030.030.030.030.030.030.030.030.030.030.030.030.0

*J&+*~r'"-3

\/6l-H.o2.OjfOjZPST-A0f-f.o310l*A0Ho*3.<*<* &Off.o3**ralS&**** **-***•

%

•All other compounds must meet a minimiim RRF of 0.010.

Pagelof2 fiDQICCm 000109FORM vn VOA A R J I b b u 7 3/90

. ' -, ., . ...., ...-:_-. .... • .: . ~ '..it. 'VOLATILE CONTINUING CALIBRATION CHECK

Lab Name: CHEMTECH ______ Contract: US EPA REGION III

Project No. A455-S____ Site: _____ Location: _____ Group:

Instrument ID: VOA1 Calibration Date: 3/24/95 . Time: 1742

Lab File ID: L1222.D___________ Init. Calib. Date(s): 1/31/95 1/31/95


GC Column: DB624 ID: 0.53 (mm)

COMPOUND2-Hexanone1, 1,2,2-Tetirachloroe thane1 ,3-Dichlorobenzene1 ,4-Dichlorobenzene1 ,2-Dichlorobenzene1 ,2-Dibromo-3-chloropropane

4-Bromofluoirobenzene

RRF0.1310.3370.8840.8790.7500.062

.

0.521

RRF50.0840.2820.8670.8470.7320.060

0.441

MINRRF

0.5000.6000.5000.400

%D .(35V)16.31.93.62.43.2

"

15.4

MAX%D

30.030.030.030..0

--


/90


Lab Name: CHEMTECH ______ Contract: US EPA REGION III

Project No. A4S5-S____ Site: ______ Location: ______ Group:


Lab File ID: L1222.D Init. Calib. Date(s): 1/31/95 1/31/95


GC Column: DB624 ID: 0.53 (mm)


Pagelof2 ' flp~ , rrnn 0001^7FORM vn VGA H n o i o o u y

COMPOUNDDichlorodifluoromethaneChloromethaneVinyl ChlorideBromomethaneChloroe thane1,1-DichIoroemeneMethylene ChlorideAcetoneCarbon Disulfidetrans-1 ,2-Dichloroethene1,1-Dichloroethanecis-1 ,2-DichloroetheneBromochloromethaneChloroform2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBenzene1 ,2-DichloroethaneTrichloroemene1 ,2-Dichloropropane1 ,2-DibromoethaneBromodichloromethanecis-1 ,3-DichloropropeneToluenetrans-l,3-Dichloropropene1 , 1 ,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneEthylbenzenem&p-xyleneso-xyleneStyreneBromoform4-Methyl-2-pentanone

RRF0.3300.2640.2690.1240.1280.4790.5160.0760.9530.4730.6200.5370.4700.7040.1420.7560.6191.1980.2850.4600.5000.3820.6690.5571.3110.3930.2580.5370.4520.9451.5901.1421.1650.8620.2640.185

RRF50.2950.2310.2540.1270.1480.4590.4845.0400.9130.4500.5960.4730.364.0.6270.0950.6950.6471.0510.2480.4720.3920.2940.5640.4601.2150.3260.2150.5890.4090.8661.4481.1001.0610.8060.2760.118

MINRRF

0.1000.100

0.100

0.200

0.1000.200

0.1000.1000.5000.1000.300

0.1000.2000.2000.4000.1000.1000.2000.1000.5000.1000.3000.3000.3000.100

%D10.612.55.6-2.4-15.64.26.2

C47.4J4.24.9

• 3.911.922.610.9C33.D8.1-4.5'12.313.0-2.621.623.015.717.47.317.016.7-9.79.58.48.93.78.96.5-4.5f36.2)

MAX%D

30.030.0

30.0

30.0

30.030.0

30.030.030.030.030.0

30.030.030.030.030.030.030.030.030.030.030.030.030.030.0

fLt~V*&~J

VIMK»Io??o*tyr*i0WOH°*"*ofT-osio"-*-1e,?7o3*o »"*O-fl-03*- ° "3~J

•

i

^VOLATILE ORGANICS INITIAL CALIBRATION DATA

Lab Name: CHEMTECH________ Contract: US EPA REGION III

Project No.: A455-S_____ Site: _____ Location: _____ Group:

Instrument ID: VOA1_____ Calibration Date(s): 1/31/95 1/31/95

Heated Purge: (Y/N) _ Calibration Tunes: 1Q22 1314

GC Column DB-624 ED: 0.53 (mm)Lab File DD: . , RRF1 =L1011.D . RRF2 = L1007.DRRF5 = L1008.D RRF10 = L1010.D RRF25 = L1009.D

COMPOUND2-Hexanone1,1,2,2-Tetrachloroethane *1,3-Dichlorobenzene *1,4-Dichlorobenzene *1,2-Dichlorobenzene *1 ,2-Dibromo-3-chloropropane

4-Bromofluorobenzene

RRF10.1710.3851.1421.1020.9660.062

0.595

RRF20.1250.3381.0051.0180.8500.072

0.711

RRF50.1230.3290.9170.9110.7820.067

0.512

RRF100.1270.3430.7930.8010.6740.064

0.428

RRF250.1070.2930.5640.5650.4760.047

0.360

RRF0.1310.3370.8840.8790.7500.062

—~

0.521

%RSD18.39.824.923.824.815.2

26.5

* Compounds with required minimum RRF and maximum 9&RSD values.All other compounds must meet a minimum RRF of 0.010.

Page2of2

, A R 3 I 6 6 I O ' FORMVIVC)A



Project No.: A455-S_____ Site: _______ Location: _____ Group:

Instrument ID: VOA1_____ Calibration Date(s): 1/31/95 1/31/95

Heated Purge: (Y/N) _ Calibration Tunes: 1022 1314

GC Column DB-624 _____ ED: 0.53 (mm)

Lab File ID: RRF1 , = L1011.D RRF2 = L1007.DRRF5 = L1008.D RRF10 - L1010.D RRF25 = L1009.D

COMPOUNDChloromethaneVinyl Chloride *Bromomethane *Chloroe thane1 , 1-Dichloroethene *VIeth'ylene ChlorideAcetoneCarbon Disulfidetrans- 1 ,2-Dichloroethene1 , 1-Dichloroethane *:is-l,2-DichloroetheneBromochloromethane *Chloroform *2-Butanone1,1,1-Trichloroethane *Carbon Tetrachloride *Benzene *1,2-Dichloroethane *rrichloroethene *1 ,2-Dichloropropane1,2-Dibromoethanc *Bromodichloromethane *cis-l,3-Dichloropropene *Toluene *trans-l,3-Dichloropropene *1,1,2-Trichloroethane *Fetrachloroediene *Dibromochloromethane *Chlorobenzene *Ediylbenzene *m&p-xylenes *o-xylene *Styrene *Bromoform *4-Methyl-2-pentanone

RRF10.2900.2800.1410.1890.5340.7070.1361.0550.5280.7070.6240.6020.9170.2050.8680.6741.4320.3380.5350.5930.5170.7860.6671.2720.4850.3440.7010.5771.2752.0821.4071.5021.0870.3020.264

RRF20.2920.2%0.162

L 0.1870.5100.7700.0751.0410.5050.6780.5620.4940.7570.1360.7790.6291.2230.2830.4600.5160.3620.6670.5381.5890.3810.2480.5280.4370.9231.5801.1821.2010.8490.2950.177

RRF50.2760.2860.1330.1290.5030.4690.0660.9940.4760.6270.5450.4600.6820.1300.7700.6361.1870.2850.4700.4880.3630.6810.5521.3760.3840.2450.5260.4380.9051.5421.1521.1570.8480.2800.170

RRF100.2380.2490.1030.0750.4530.3660.0530.8920.4610.5940.5080.4230.6200.1270.7400.6261.1670.2760.4490.4850.3590.6520.5531.2710.3830.2450.5090.4330.8751.4861.0671.0670.8210.2570.170

RRF250.2220.2340.0800.0610.3950.2670.0490.7840.3930.4950.4480.3730.5450.1120.6210.5320.9800.2420.3860.4200.3100.5590.4761.0500.3330.2070.4240.3770.7501.2610.9030.8990.7040.1860.145

RRF0.2640.2690.1240.128 i0.4790.5160.0760.9530.4730.6200.5370.4700.7040.1420.7560.6191.1980.2850.4600.5000.3820.6690.5571.3110.3930.2580.5370.4520.9451.5901.1421.1650.8620.2640.185

%RSD12.29.826.0"46.911.5"32.0,r46.4 ,12.010.913.312.218.420.225.511.88.513.412.111.512.520.512.112.414.914.219.918.816.420.719.016.119.016.217.724.8

41 Compounds with required minimum RRF and maximum XRSD values.All other compounds must meet a minimum RRF of 0.010. .

Page 1 of 2 , ^ .....FORM VI VOA nnn «-_• 3/90

6AVOLATILE ORGANICS INmAL CALIBRATION DATA

Lab Name: CHEMTECH________ Contract: US EPA REGION in


Instrument ID: VOA1 ___ Calibration Date(s): 1/30/95 1/30/95

Heated. Purge: (Y/N) _ CalibrationTim.es: 1628 2013

GC Column DB-624 ED: 0.53 (mm) --

Lab File ID: RRF1 =L1002.D RRF2 = L1004.DRRF5 == L1001.D RRF10 = L1005.D RRF25 = L1003.D

COMPOUNDDichlorodifluoromethane

. - •

• - - -----

RRF10.253

(

;

RRF20,458

RRF50.334

RRF100.294

.

RRF250.310

RRF"0.330

-

""•

•

%RSD23.4

\

* Compounds with required minimum RRF and maximum 56RSD values.All other compounds muiit meet a minimum RRF of 0.010.

Pagelof2 000 1FORM VI VOA l/ •

AR3I66I2


Lab Name: CHEMTECH_________ Contract: US EPA REGION Ed

Project No. A447-S____ Site: ____ • Location: _____ Group:


Lab File ED: L1205.D_____________ Init Calib. Date(s): 1/31/95 1/31/95s



COMPOUND2-Hexanone1 , 1 ,2,2-Tetrachloroethane1 ,3-Dichlorobenzene1 ,4-Dichlorobenzene1 ,2-Dichlorobenzene1 ,2-Dibromo-3-chloropropane


RRF0.1310.3370.8840.8790.7500.062

0.521

RRF50.1090.3400.9370.9370.8110.062

0.582

MINRRF

f

0.5000.6000.5000.400

%D16.8-0.9-6.0-6.6-8.10.0

-

-11.6

MAX%D

30.030.030.030.0


Pag'2of2 4R3I66I3 FORM vn VGA 000195 3rao


Lab Name: CHEMTECH_______ Contract: US EPA REGION EQ

Project No. A447-S____ . Site: ___ Location: ' Group:


Lab File ED: L120S.D Init Calib. Date(s): 1/31/95 1/31/95


GC Column: DB624 ED; 0.53 (mm)'

•fe»

COMPOUNDDichlorodifluoromethaneChloromethani;Vinyl ChlorideBromomethanciChloroethane1,1-DichloroeiheneMethylene ChlorideAcetoneCarbon Disul£idetrans-1 ,2-Dichloroethene1 , 1-Dichloroethanecis-l,2-DichloroetheneBromochloromethaneChloroform2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBenzene1 ,2-DichloroeihaneTrichloroe there1 ,2-Dichloropropane1 ,2-DibromoeithaneBromodichloromethanecis-l,3-DichloropropeneToluenetnns-l,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroctheneDibromochloromethaneChlorobenzeneEthylbenzenem&p-xyleneso-xyleneStyreneBromoform4-Methyl-2-pentanone

RRF0.3300.2640.2690.1240.1280.4790.5160.0760.9530.4730.6200.5370.4700.7040.142

, 0.7560.6191.1980.2850.4600.5000.3820.6690.5571.3110.3930.2580.5370.4520.9451.590

- 1.1421.1650.8620.2640.185

RRF50.2530.2570.2640.1280.1660.5230.374(0.048 \1.0350.4990.6670.5520.4520.6770.1170.8140.7271.2030.2840.5570.4590.3620.6720.5431.4310.3980.2550.6490.5130.9851.5891.1571.161 ,0.8550.3260.149

MENRRF

0.1000.100

0.100

0.200

0.1000.200

0.1000.1000.5000.1000.300

0.1000.2000.2000.4000.1000.1000.200

' 0.1000.5000.1000.3000.3000.3000.100

%D23.32.71.9-3.2-29.7-9.227.5

C36.8)-8.6-5.5-7.6-2.83.83.817.6 --7.7-17.4-0.40.4-21.18.25.2-0.42.5-9.2-1.31.2

-20.9-13.5-4.20.1-1.30.40.8-23.519.5

MAX%D

30.030.0

30.0

30.0

30.030.0

30.030.030.030.030.0

30.030.0

130.030.030.030.030.030.030.030.030.030.030.030.0

.•C't~~S&-A

V&LKoZOtlollbwZld 7703/4 K32.0??03/£v^307703/c' V/-i*7077^31$ W/DQllfZiyv/JlLc*ShAtAJL «l«*

V


Page 1 of2FORM VH VOA wvi.^-* 3/9Q



Project No. A447-S____ Site: ____ Location: _____ Group:


Lab File ID: L1187.D__________ Init Calib. Date(s): 1/31/95 1/31/95



COMPOUND2-Hexanone1, 1,2,2-Tetrachloroethane1 ,3-Dichloro benzene1 ,4-Dichlorobenzene1,2-Dichlorobenzene1 ,2-Dibromo-3-chloropropane


RRF0.1310.3370.8840.8790.7500.062

0.521

RRF50.1070.3330.9921.0150.8400.064

0.455

MINRRF

0.5000.6000.5000.400

'

%D18.31.2-12.2-15.5-12.0-3.2

"--•

12.7

MAXS6D

30.030.030.030.0

AU other compounds must meet a minimum RRF of 0.010.

Page2of2 . -»* 000193- « n J l o 6 l 5 FORM vn VOA 3/90

'• --" ---- r. . . , . . . . • 7A

VOLATILE CONTINUING CALIBRATION CHECK

Lab Name: CHEMTECH Contract: US EPA REGION EQ

Project No. A447-S Site: ____ Location: _____ Group:

Instrument ED: VOA1____^_____ Calibration Date: 3/19/95 Time: 1229

Lab File EO: L1187.D__________ Init. Calib. Date(s): 1/31/95 1/31/95

Heated Purge: (Y/N) ____ Init. Calib. Times: 1022 1314


COMPOUNDDichlorodifiuoromethaneChloromethaneVinyl ChlorideBromomethaneChloroethanj1,1-DichloroetheneMethylene ChlorideAcetoneCarbon Bisulfidetrans-1 ,2-Dichloroethene1,1-Dichloroethanecis-1 ,2-DichloroetheneBromochloromethaneChloroform2-Butanone1, 1,1-TrichloroethaneCarbon TetrachlorideBenzene1 ,2-DichloroethaneTrichloroethene1 ,2-Dichloropropane1,2-Dibromoe thaneBromodichloromethanecis*l ,3-DichloropropeneToluenetrans-1 ,3-Dichloropropene1,1 ,2-TrichloroedianeTetrachloroetheneDibromochloromethaneChlorobenzeneEthylbenzenem&p-xyleneso-xyleneStyreneBromoform4-Methyl-2-]jentanone

RRF0.3300.2640.2690.1240.1280.4790.5160.0760.9530.4730.6200.5370.4700.7040.1420.7560.6191.1980.2850.4600.5000.3820.6690.5571.3110.3930.2580.5370.4520.9451.5901.1421.1650.8620.2640.185

RRF50.2260.2540.2580.1250.1660.5080.310.049")1.0670.4860.6030.5650.4370.7300.1160.8580.7521.2350.2910.5540.4760.3610.7150.5631.4430.3980.2600.6760.5111.0181.6981.2211.2440.9210.3320.148

MINRRF

0.1000.100

0.100

0.200

0.1000.200

0.1000.1000.5000.1000.300

0.1000.2000.2000.4000.1000.1000.2000.1000.5000.1000.3000.3000.3000.100

%D01.50

4.1-0.8-29.7-6.1

C39.9 )( 35.5 J-12.0-2.72.7-5.27.0-3.718.3 --13.5-21.5-3.1-2.1 .-20.44.85.5-6.9-1.1-10.1-1.3-0.8-25.9-13.1-7.7-6.8-6.9-6.7-6.8-25.820.0

MAXXD

30.030.0

30.0

t

30.0

30.030.0

30.030.030.030.0

L30.0

30.030.030.030.030.030.030.030.030.030.030.030.030.030.0

V&i-Kot°77o3/sw££3?*£>3)3 v/ey.C ft 3 3 '-A W/aO77O3I3 V/'tf077$ 3/3 v/ 13&$ T'.O'/J pyvvO 7Q3i 3pW S'

/o?yo3)yf>w£>6"7-?62H->t>\?/G&7*&3!iib/3g<3<z?_>3f5T"J3/7?n3tz»s 2Of f 0? 5 / -OJJ03 5 0%


Pa*,of* ,„„_ 000192A R 3 I 6 6 I 6 FORM w VOA 3/9°


Lab Name: CHEMTECH________ Contract: US EPA REGION EQ

Project No.: A447-S_____ Site: ______ Location: _____ Group:Instrument ED: VOA1 Calibration Date(s): 1/31/95 1/31/95

Heated Purge: (Y/N) _ Calibration Tunes: 1022 1314GC Column DB-624 ED: 0.53 (mm)

Lab File ED: RRF1 =L1011.D RRF2 = L1007.DRRF5 « L1008.D RRF10 « L1010.D RRF25 = L1009.D .

COMPOUND2-Hexanone1,1,2,2-Tetrachlorocthane *1,3-Dichlorobenzene *1,4-Dichlorobenzene *1,2-Dichlorobenzene *1 ,2-Dibromo-3-chloropropane

*

*


RRF10.1710.3851.1421.1020.9660.062

O.S95

RRF20.1250.3381.0051.0180.8500.072

•

0.711

RRF50.1230.3290.9170.9110.7820.067

0.512

RRF100.1270.3430.7930.8010.6740.064

0.428

RRF250.1070.2930.5640.5650.4760.047

0.360

RRF0.1310.3370.8840.8790.7500.062

~ -

0.521

%RSD18.39.824.923.824.815.2

26.5* Compounds with required minimum RRF and maximum %RSD values.All other compounds must meet a minimum RRF of 0.010.

Page2of2 nnm CO


Lab Name: CHEMTECH Contract: US EPA REGION Ed


Instrument ID: VQA1 _____ Calibration Date(s): 1/31/95 1/31/95

Heated Purge: (Y/N) _ Calibration Times: 1022 1314

GC Column DB-624 ED: 0.53 (mm) ; --

Lab File ID: RRF1 =L1011.D RRF2 = L1007.DRRF5 = L1008.D RRF10 = L1010.D RRF25 - L1009.D

COMPOUNDChloromethanejVinyl Chloride *JBromomethane *jChloroethane|l,l-Dichlorctethene *JMethylene Chloride[AcetoneCarbon Disulfidetrans-l,2-Dichloroethene1,1-Dichloroethane *cis-l,2-DichtoroetheneBromochloromethane *Chloroform *2-Butanone1,1,1-Trichloroethane *Carbon Tetrachloride *[Benzene *|l,2-Dichloroethane *jrrichloroethcne *1 ,2-Dichl oropropane1,2-Dibromoethane *[Bromodichloromethane *bis-l,3-Dichloropropene *[Toluene *[trans-1, 3-Dichloropropene *1 , 1 ,2-Trichloroethane *retrachloroethene *Dibromochloromethane *Chlorobenzene *Ethylbenzene *n&p-xylenes *o-xylene *Styrene • *Bromofonn *4-Methyl-2-pentanone

RRF10.2900.2800.1410.1890.5340.7070.1361.0550.5280.7070.6240.6020.9170.2050.8680.6741.4320.3380.5350.5930.5170.7860.6671.2720.4850.3440.7010.5771.2752.0821.4071.5021.0870.3020.264

RRF20.2920.2960.1620.1870.5100.7700.0751.0410.5050.6780.5620.4940.7570.1360.7790.6291.2230.2830.4600.5160.3620.6670.5381.5890.3810.2480.5280.4370.9231.5801.1821.2010.8490.2950.177

RRF50.2760.2860.1330.1290.5030.4690.0660.9940.4760.6270.5450.4600.6820.1300.7700.6361.187 .0.2850.4700.4880.3630.6810.5521.3760.3840.2450.5260.4380.9051.5421.1521.1570.8480.2800.170

RRF100.2380.2490.1030.0750.4530.3660.0530.8920.4610.5940.5080.4230.6200.1270.7400.6261.1670.2760.4490.4850.3590.6520.5531.2710.3830.2450.5090.4330;8751.4861.0671.0670.8210.2570.170

RRF250.2220.2340.0800.0610.3950.2670.0490.7840.3930.4950.4480.3730.5450.1120.6210.5320.9800,2420.3860.4200.3100.5590.4761.0500.3330.2070.4240.3770.7501.2610.9030.8990.7040.1860.145

RRF0.2640.2690.1240.1280.4790.5160.0760.9530.4730.6200.5370.4700.7040.1420.7560.6191.1980.2850.4600.5000.3820.6690.5571.3110.3930.2580.5370.4520.9451.5901.1421.1650.8620.2640.185

%RSD12.29.826.06.911.5T21T;'46.412.010.913.312.218.420.225.511.88.513.412.111.512.520.512.112.4Li4,-914,219.918.816.420.719.016,119.016.217.724.8

* Compounds; with required minimum RRF and maximum %RSD values.All other compounds must meet a minimum RRF of 0.010.

Page 1 o f 2 , . . ' . .. FORM VI VOA 3/90

Aft3l66l8 ' 000162


Lab Name: CHEMTECH _____ Contract: US EPA REGION III


Instrument ED: VOA1________ Calibration Date(s): 1/30/95 1/30/95Heated Purge: (Y/N) _ Calibration Times: 1628 2013

GC Column DB-624 ED: 0.53 (mm)

Lab File ID: RRF1 =L1002.D RRF2 « L1004.DRRF5 - L1001.D RRF10 = L1005.D RRF25 - L1003.D

COMPOUNDDichlorodifluoromediane

RRF10.253

RRF20.458

•

•

RRF50.334

RRF100.294

RRF250.310

RRF0.330

"•*•-

%RSD23.4

* Compounds with required minimum RRF and maiimum 56RSD values.All other compounds must meet a minimum RRF of 0.010.

Page 1 of2FORM VI VOA 3/90

AR3I66I9 000161



Project No. A435-S Site; Location:_____ Group:

Instrument ED: VOA1 __ Calibration Date: 3/16/95 Tune: 0822

Lab File ID: L1178.D Init Calib. Date(s): 1/31/95 1/31/95

Heated Purge: (Y/N) ___ Init Calib. Tunes; 1025 1314


COMPOUND2-Hexanone1 , 1 ,2,2-Tetrachloroethanel,3-Dichlorol>enzene1 ,4-Dichlorobenzene1 ,2-Dichlorobenzene1 ,2-DibromO"3-chloropropane

.

.1


RRF0.1310.3370.8840.8790.7500.062

0.521

RRF500.1210.3510.9060.9130.7890.079

0.548

MINRRF

0.5000.6000.5000.400

%D7.6-4.2-2.5-3.9-5.2-27.4

-5.1

MAX%D

30.030.030.030.0


Page2of2 Afni£C9n 000200Hn.iiKi.vn. FORMvnvOA uv 3/90


Lab Name: CHEMTECH_________ Contract: US EPA REGION Etl

Project No. A43S-S____ Site: _____ Location: _____ Group:


Lab File ED: L1178.D_____________ Init Calib. Date(s): 1/31/95 1/31/95



COMPOUNDDichlorodifluoromethaneChloromethaneVinyl ChlorideBromomethaneChloroethane1 , 1-DichloroetheneMethylene ChlorideAcetoneCarbon Disulfidetrails- 1 ,2-Dichloroethene1 , 1-Dichloroe thanecis-1 ,2-DichloroetheneBromochloromethaneChloroform2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBenzene1 ,2-DichloroethaneTrichloroethene1 ,2-Dichloropropane1 ,2-DibromoethaneBromodichloromethanecis-l,3-DichloropropeneToluenetrans-1 ,3-Dichloropropene1 , 1,2-TrichloroethaneTetrachloroethcneDibromochloromethane

. ChlorobenzeneEthylbenzenem&p-xyleneso-xylcneStyreneBromoform4-Metbyl-2-pentanone

RRF0.3300.2640.2690.1240.1280.4790.5160.0760.9530.4730.6200.5370.4700.7040.1420.7560.6191.1980.2850.4600.5000.3820.6690.5571.3110.3930.2580.5370.4520.9451.5901.1421.1650.8620.264

• 0.185

RRF500.2620.2470.2630.1250.1490.5060.5180.0511.0030.4870.5800.5510.4310.7110.1220.8710.7631.2300.2950.5430.4820.3560.7150.5861.4700.4270.2620.6070.5220.9721.6841.2361.2620.9050.3300.164

MENRRF

0.1000.100

0.100

0.200

0.1000.200

0.1000.1000.5000.1000.300

0.1000.2000.2000.4000.1000.1000.2000.1000.5000.1000.3000.3000.3000.100

%D20.46.42.2-0.8-16.4-5.6-0.4

O2.9J-5.2-3.06.5-2.68.3-1.014.1--15.2-23.3-2.7-3.5-18.03.66.8-6.9-5.2-12.1-8.7-1.6-13.0-15.5-2.9-5.9-8.2 .-8.3-5.0-25.011.4

MAX%D

30:030.0

30.0

30.0

30.030.0

30.030.030.030.030.0

30.030.030.030.030.030.030.030.030.030.030.030.030.030.0

AjjeCiaW'Scales

VSTD050VBLK04)770313W06)770313W07STORAGE BLALCS

-

4

1All other compounds must meet a minimum RRF of 0.010.

P*elof2 1R3I662; FOKMVDVOA 000199 3/90

7AVOLATILE CONTINUING CALIBRATION.CHECK


Project No. A43S-S____ Site: _____ Location: _____ Group:


Lab File ED: L1160.D __________ Init Calib. Date(s): 1/31/95 1/31/95

Heated Purge: (Y/N) ___ Init Calib. Times: • 1025 1314


COMPOUND2-Hexanone1,1,2,2-Teaachloroethane1 ,3-Dichlorobenzenc1 ,4-Dichlorobenzcnc1 ,2-Dichlorobenzcnel,2-Dibromo-3-chloropropane

•


RRF0.1310.3370.8840.8790.7500.062

,

I

0.521

RRF500.0910.2970.9670.9540.8230.055

0.469

MENRRF

0.5000.6000.5000.400

%DC30.5)11.9-9.4-8.5-9.711.3

-•-..

10.0

MAX96D

30.030.030.030.0

*

All other compounds must meet a minimum RRF of 0.010. •

' 000198$ R3 i 66 22 FORM VH VOA 3/90


Lab Name: CHEMTECH_____• Contract: US EPA REGION Efl



Lab File ED: L1160.D__________ Init Calib. Date(s): 1/31/95 1/31/95



COMPOUNDDichlorodifiuoromedianeChloromethaneVinyl ChlorideBromomethaneChloroethane1,1-DichIoroetheneMethylene ChlorideAcetoneCarbon Disulfidetrans-1 ,2-Dichloroethene1 , 1-Dichloroethanecis-1 ,2-DichloroetheneBromochloromethaneChloroform2-Butanone1, 1, 1-TrichloroethaneCarbon TetrachlorideBenzene1,2-DichloroethaneTrichloroethene1 ,2-Dichloropropane1 ,2-DibromoethaneBromodichloromethanecis-1 ,3-DichloropropeneToluenetrans-1, 3-Dichloropropcne1 , 1 ,2-TrichloroethaneTetrachloroethene

. Dibromochloromethane

. ChlorobenzeneEthylbenzenem&p-xyleneso-xyleneStyreneBromoform4-Methyl-2-pentanone

RRF1 0.3300.2640.2690.1240.1280.4790.5160.0760.9530.4730.6200.5370.4700.7040.1420.7560.6191.1980.2850.4600.5000.3820.6690.5571.3110.3930.2580.5370.4520.9451.5901.1421.1650.8620.2640.185

RRF500.2400.2580.2730.1430.1700.5180.326C0.042)1.0330.5060.6510.5540.4210.6850.1000.8590.7451.1950.2710.5360.4590.3360.6570.5541.3570.3810.2390.6560.4790.9741.6421.2291.1890.8880.3030.130

MINRRF

0.1000.100

0.100

0.200

0.1000.200

0.1000.1000.5000.1000.300

0.1000.2000.2000.4000.1000.1000.2000.1000.5000.1000.3000.3000.3000.100

%D27.32.3-1.5

-15.3C-32.83

-8.1G6.O(44.7)-8.4-7.0-5.0-3.210.42.729.6--13.6-20.40.34.9

-16.58.212.01.80.5-3.53.17.4-22.2-6.0-3.1-3.3-7.6-2.1-3.0-14.829.7

MAX%D

30.030.0

30.0

30.0

30.030.0,30.030.030.0.30.030.0

30.030.030.030.030.030.030.030.030.030.030.030.030.030.0

Assoti*rt*'Sa le;

VSTD050VBLK03)770307W293770307W22)770307W340770308TB1)77030829B377030829C0770308W05 '3770308WGr||3770309TB. V

4All other compounds must meet t minimum, RRF of 0.010. n • • • •

Pa*Iof2 AR3I6623 FORMIVOA 000197 3/90


Lab Name: CHEMTECH Contract: US EPA REGION Efl

Project No, A43S-S Site: _____ Location: _______ Group:


Lab File ED: L1150.D___________ Init. Calib. Date(s): 1/31/95 1/31/95

Heated Purge: (Y/N) Init Calib. Times: 1025 1314


COMPOUND2-Hexanone1, 1,2,2-Tetrachloroethane1 ,3-Dichlorobenzene1,4-Dichlorobenzene1 ,2-Dichlorobenzene1 ,2-Dibromo-3-chloropropaiie

'

.


RRF0.1310.3370.8840.8790.7500.062

I

0.521

RRF50.1180.3711.0251.0020.8950.069

0.488

MENRRF

0.5000.6000.5000.400

%D9.9

-10.1-16.0-14.0-19.3-11.3

~--.

6.3

MAX%D

30.030.030.030.0

All other compounds must meet a rninimum RRF of 0.010.

Page2of2 A fi^i fi £ 9 i, 000136v:rHHO I D0_:l4 BAim vn VOA lion


Lab Name: CHEMTECH________ Contract: US EPA REGION Efl

Project No. A435-S____ Site: ____ Location: _____ Group:


Lab File ID: L11SO.D__________ Init. Calib. Date(s): 1/31/95 1/31/95


GC Column: DB624 CO: 0.53 (mm)

COMPOUNDDichlorodifluoromethaneChloromethaneVinyl ChlorideBromomethaneChloroethane1,1-DichloroetheneMethylene ChlorideAcetoneCarbon Disulfidetrans-l,2-Dichloroethene1 , 1-Dichloroethanecis-l,2-DichloroetheneBromochloromethaneChloroform2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBenzene1 ,2-DichloroedianeTrichloroethene1 ,2-Dichloropropane1,2-DibromoethaneBromodichloromethanecis-l,3-DichloropropeneToluenetrans-1 ,3-Dichloropropene1,1,2-TrichloroethaneTetnchloroetheneDibromochloromethane

. ChlorobenzeneEthylbenzenem&p-xyleneso-xyleneStyreneBromoform4-Methyl-2-pentanone

RRF0.3300.2640.2690.1240.1280.4790.5160.0760.9530.4730.6200.5370.4700.7040.1420.7560.6191.1980.2850.4600.5000.3820.6690.5571.3110.3930.2580.5370.4520.9451.5901.1421.1650.862

> 0.2640.185

RRF50.3480.2910.3080.1610.1810.5830.3640.0551.1550.5480.7420.6250.4780.7760.1280.9350.8131.2730.3270.5650.4930.3950.7570.6071.4280.4240.2790.6920.5571.0521.7461.3201.2740.9790.3630.164

MINRRF

0.1000.100

0.100

0.200

0.1000.200

0.1000.1000.5000.1000.300

0.1000.2000.2000.4000.1000.1000.2000.1000.5000.1000.3000.3000.3000.100

%D-5.5-10.2-14.5-29.8G41.4}-21.729.527.6-21.2-15.9-19.7-16.4-1.7-10.29.9--23.731.33-6.3-14.7-22.81.4-3.4-13.2-9.0-8.9-7.9-8.1-28.9-23.2-11.3-9.8-15.6-9.4-13.607.5}11.4

.MAX%D

30.030.0

30.0

30.0

30.030.0

30.030.030.030.030.0

30.030.030.030.030.030.030.030.030.030.030.030.030.030.0

Associate*S«*flt*

VSTD050VBLK02)770307W023770307W28

-

•

iAll other compounds must meet a minim im, RRF of 0.010.

AR3I6625 K*MvnvoA 000195


Lab Name: CHEMTECH _____ Contract: US EPA REGION ffl



Lab File ED: L1137.D__________ Init Calib. Date(s): 1/31/95 1/31/95

Heated Purge: (Y/N) ___ InitCalib.Tim.es: 1025 1314

GC Column: DB624___ ED: 0.53 (mm)

O

COMPOUND2-Hexanone1, 1,2,2-Tetraichloroethane1 ,3-Dichlorobenzene1 ,4-Dichlorobenzene1 ,2-Dichlorobenzene1 ,2-Dibromo-3-chloropropane

.


RRF0.1310.3370.8840.8790.7500.062

0.521

RRF50.0700.2410.7950.7910.6750.050

0.568

MENRRF

0.5000.6000.5000.400

*

%DO6.6}28.510.110.010.019.4

•-

-9.0

MAX56D

30.030.030.030.0

-

All other compounds must meet a minimum RRF of 0.010. ••••-• ,.;:.... j.

AR3I6626 FORM w VOA 000194 3/90


Lab Name: CHEMTECH___________ Contract: US EPA REGION EQ

Project No. A435-S____ Site: _____ Location: ________ Group:


LabFileID:L1137.D Init Calib. Date(s): 1/31/95 1/31/95



COMPOUNDDichlorodifluoromethaneChloromethaneVinyl ChlorideBromometbaneChloroethane1,1-DichloroetheneMethylene ChlorideAcetoneCarbon Disulfidetrans-1, 2-Dichloroediene1 , 1-Dichloroethanecis-1 ,2-DichloroctheneBromochloromethaneChloroform2-Butanone.1 , 1 , 1-TrichloroethaneCarbon TetrachlorideBenzene1 ,2-DichloroethaneTrichloroethene1 ,2-Dichloropropane1,2-DibromoethaheBromodichloromethanecis-1 ,3-DichloropropeneToluenetrans-1 ,3-Dichloropropene1, 1,2-TrichloroethaneTetrachloroetheneDibromochloromethane

. ChlorobenzeneEthylbenzenem&p-xyleneso-xyleneStyreneBrouioform4-Methyl-2-pentanone

RRF0.3300.2640.2690.1240.1280.4790.5160.0760.9530.4730.6200.5370.4700.7040.1420.7560.6191.1980.2850.4600.5000.382

. 0.6690.5571.3110.3930.2580.5370.4520.9451.5901.1421.1650.8620.2640.185

RRF50.2380.2190.2230.1210.1340.4210.660r 6.035 J0.8550.4080.5510.4540.3400.5880.0790.6860.6070.9640.2290.4380.3650.2700.5280.4241.1300.3040.1930.5310.3880.7691.2750.9700.9240.6930.2670.100

MINRRF

0.1000.100

0.100

0.200

0.1000.200

0.1000.1000.5000.1000.300

0.1000.2000.2000.4000.1000.1000.2000.1000.5000.1000.3000.3000.3000.100

%D27.917.017.12.44.112.1-27.9O3.9J10.313.711.115.527.716.544.439.31.919.519.64.827.029.321.123.913.822.625.21.114.218.619.815.120.719.6-1.1

G5.91

MAX%D

30.030.0

30.0

30.0

30.030.0

30.030.030.030.030.0

30.030.030.030.030.030.030.030.030.030.030.030.030.030.0

Associw**5a»v»lt?

VSTDOSOVBLK01)770306W17)770306W193770306W203770306PW1)770306PW2)770306PW4)770307TB1

4

IAll other compounds must meet t minimum RRF of 0.010.

SR3I6627 mRMvnvo» 000193


Lab Name: CHEMTECH _______ Contract: US EPA REGION HIProject No.: A43S-S Site:, _____ Location: _____ Group:

Instrument ED: VOA1 CalibrationDate(s): 1/31/95 1/31/95Heated Purge: (Y/N) _ Calibration Times: 1022 1314

GC Column DB-624 ED: 0.53 (mm)Lab File ED: RRF1 =L1011.D RRF2 - L1007.DRRF5 - L1008.D RRFIO - L1010.D RRF25 - L1009.D

COMPOUND2-Hexanone1,1,2,2-Tetrachloroethane *1,3-Dichlorobenzene *1,4-Dichlorobenzene *1,2-DichloroIjenzene *1 ,2-Dibromo-3-chloropropane

,

"

4-Bromofluorobenzeoe

RRF10.1710.3851.1421.1020.9660.062

0.595

RRF20.1250.3381.0051.0180.8500.072

l

1

0.711

RRF50.1230.3290.9170.9110.7820.067

0.512

RRFIO0.1270.3430.7930.8010.6740.064

.

0.428

RRF250.1070.2930.5640.5650.4760.047

0.360

RRF0.1310.3370.8840.8790.7500.062

0.521

%RSD18,39,,824,923.824,815.2

26.5

* Compounds with required minimum RRF and maximum XRSD values.All other compounds must meet a minimum RRF of 0.010.

Page2of2 ' JFORM VI VOA 000164 3/9°R31552g


Lab Name: CHEMTECH _____ Contract: US EPA REGION EQ

Project No.: A435-S_______ Site: _____ Location: _____ Group:

Instrument ED: VOA1_____ Calibration Date(s): 1/31/95 1/31/95


GC Column DB-624 ED: 0.53 (mm)

Lab File ED: RRF1 =L1011.D RRF2 - L1007.DRRF5 - L1008.D RRFIO - L1010.D RRF25 = L1009.D

COMPOUNDChloromethaneVinyl Chloride *Bromomethane *Chloroethane1,1-Dichloroethene *Methylene Chloride[AcetoneCarbon Disulfidetrans-1 ,2-Dichloroethene1,1-Dichloroethane *:is-l,2-DichloroetheneBromochloromethane *Chloroform ' *2-Butanone1,1,1-Trichloroediane *Carbon Tetrachloride *Benzene *1,2-Dichloroethane *rrichloroethene *1 ,2-Dichloropropane1,2-Dibromoethane *[Bromodichloromethane *cis-1, 3-Dichloropropene *Toluene *trans-l,3-DichIoropropene *1 , 1 ,2-Trichloroethane *retrachloroethene *Dibromochloromedume *Chlorobenzene *Emylbenzene *n&p-xylenes • *o-xylene *Btyrene *Bromofonn *|4-Methyl-2-pentanone

RRF10.2900.2800.1410.1890.5340.7070.1361.0550.5280.7070.6240.6020.9170.2050.8680.6741.4320.3380.5350.5930.5170.7860.6671.2720.4850.3440.7010.5771.2752.0821.4071.5021.0870.3020.264

RRF20,2920.2960.1620.1870.5100.7700.0751.0410.5050.6780.5620.4940.7570.1360.7790.6291.2230.2830.4600.5160.3620.6670.5381.5890.3810.2480.5280.4370.923• 1.5801.1821.2010.8490.2950.177

RRF50.2760.2860.1330.1290.5030.4690.0660.9940.4760.6270.5450.4600.6820.1300.7700.6361.1870.2850.4700.4880.3630.6810.5521.3760.3840.2450.5260.4380.9051.5421.1521.1570.8480.2800.170

RRFIO0.2380.2490.1030.0750.4530.3660.0530.8920.4610.5940.5080.4230.6200.1270.7400.6261.1670.2760.4490.4850.3590.6520.5531.2710.3830.2450.5090.4330.8751.4861.0671.0670.8210.2570.170

RRF250.2220.2340.0800.0610.3950.2670.0490.7840.3930.4950.4480.3730.5450.1120.6210.5320.9800.2420.3860.4200.3100.5590.4761.0500.3330.2070.4240.3770.7501.2610.9030.8990.7040.1860.145

RRF0.2640.2690.1240.1280.4790.5160.0760.9530.4730.6200.5370.4700.7040.1420.7560.6191.1980.2850.4600.5000.3820.6690.5571.3110.3930.2580.5370.4520.9451.5901.1421.1650.8620.2640.185

%RSD12.29.826.0:46.£>11.5?-P6.4:12.010.913.312.218.420.225.511.88.513.412.111.512.520.512.112.414.914.219.918.816.420.719.016.119.016.217.724.8

* Compounds with required minimum RRF and marimnm XRSD values.All other compounds must meet a minimum RRF of 0.010.

Page 1 of 2 . ' . " ; . 'FORM VI VOA 3/90

AR3I6629 : °°0]G3

6AVOLATILE ORGANICS. INITIAL CALIBRATION DATA

Lab Name: CHEMTECH Contract: US EPA REGION Ed

Project No.: A435-S_____ Site: . Location: _____ Group:

Instrument LD: VOA1 Calibration Date(s): 1/30/95 1/30/95


GC Column DB-624_______ ED: 0.53 (mm)

Lab File ED: . . , . RRF1 =L1002.D , RRF2 = L1004.DRRF5 = LlOOl.D RRFIO = L1005.D RRF25 = L1003.D

COMPOUNDDichlorodifluoromethane

•

•

•* ' "*

--

RRF10.253

RRF2a.458

RRF50.334

RRFIO0.294

RRF250.310

RRF0.330

%RSD?3.4

* Compounds with required minimum RRF and maTimum 56RSD values.All other compounds must meet a minimum RRF of 0.010.

Page 1 of 2 7 ""•FORM VI VOA 3/9°

flR3l6630

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DEFINITION OF CODES USED IN TABLE I(Loir Concentration)

I = %RSD exceeded 30% in the volatile initial calibration.Positive results are qualified HJ". When the %RSD exceeded50*, guantitation limits are qualified "UJ11.

C — %D exceeded 30% in the volatile continuing calibrationPositive results are qualified "J". When the %D exceeded50%, quantitation limits are qualified "UJ".

F = RF less than 0.05 in the calibration. All quantitationlimits are qualified "R" and positive results are qualified"L".

+ = The "B" qualifier, denoting blank contamination, supersedesthe qualifier issued in this table.

R = The "R" qualifier, denoting unusable results, supersedes thequalifier issued in this table.

AR31663

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