9 8 7 6 5 4 3 2 1 ppm - Royal Society of Chemistry9 8 7 6 5 4 3 2 1 ppm 7.27 5.84 5.83 5.82 5.81...
145
9 8 7 6 5 4 3 2 1 ppm 1.72 1.74 1.76 1.77 1.79 2.10 2.10 2.10 2.12 2.14 2.15 2.15 2.16 2.36 2.38 2.40 4.99 5.00 5.00 5.00 5.00 5.02 5.02 5.02 5.03 5.03 5.03 5.04 5.07 5.07 5.08 5.08 5.74 5.76 5.77 5.77 5.78 5.80 5.81 5.82 5.83 5.84 7.27 2.05 2.04 2.08 2.02 1.00 Current Data Parameters NAME 07312013-50-michaelM EXPNO 10 PROCNO 1 F2 - Acquisition Parameters Date_ 20130731 Time 22.58 INSTRUM AVII400 PROBHD 5 mm PABBO BB/ PULPROG zg30 TD 65536 SOLVENT CDCl3 NS 8 DS 2 SWH 5597.015 Hz FIDRES 0.085404 Hz AQ 5.8545494 sec RG 456 DW 89.333 usec DE 6.50 usec TE 295.6 K D1 1.00000000 sec TD0 1 ======== CHANNEL f1 ======== SFO1 400.1324008 MHz NUC1 1H P1 12.50 usec PLW1 15.04800034 W F2 - Processing parameters SI 32768 SF 400.1300059 MHz WDW EM SSB 0 LB 0.30 Hz GB 0 PC 1.00 Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is © The Royal Society of Chemistry 2015
Transcript of 9 8 7 6 5 4 3 2 1 ppm - Royal Society of Chemistry9 8 7 6 5 4 3 2 1 ppm 7.27 5.84 5.83 5.82 5.81...
9 8 7 6 5 4 3 2 1 ppm
1.72
1.74
1.76
1.77
1.79
2.10
2.10
2.10
2.12
2.14
2.15
2.15
2.16
2.36
2.38
2.40
4.99
5.00
5.00
5.00
5.00
5.02
5.02
5.02
5.03
5.03
5.03
5.04
5.07
5.07
5.08
5.08
5.74
5.76
5.77
5.77
5.78
5.80
5.81
5.82
5.83
5.84
7.27
2.0
5
2.0
4
2.0
8
2.0
2
1.0
0
Current Data Parameters
NAME 07312013-50-michaelM
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130731
Time 22.58
INSTRUM AVII400
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 5597.015 Hz
FIDRES 0.085404 Hz
AQ 5.8545494 sec
RG 456
DW 89.333 usec
DE 6.50 usec
TE 295.6 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 400.1324008 MHz
NUC1 1H
P1 12.50 usec
PLW1 15.04800034 W
F2 - Processing parameters
SI 32768
SF 400.1300059 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry.This journal is © The Royal Society of Chemistry 2015
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
23.93
33.13
33.32
76.91
77.23
77.55
115.78
137.68
179.42
Current Data Parameters
NAME 08012013-29-michaelM
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130802
Time 2.18
INSTRUM AVII400
PROBHD 5 mm PABBO BB/
PULPROG udeftnoe.and
TD 8650
SOLVENT CDCl3
NS 1024
DS 4
SWH 24038.461 Hz
FIDRES 2.779013 Hz
AQ 0.1799200 sec
RG 203
DW 20.800 usec
DE 6.50 usec
TE 296.4 K
D1 2.00000000 sec
D6 0.03000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D15 0.00302000 sec
D20 1.53362894 sec
D21 0.21294050 sec
D24 0.10000000 sec
L4 1
======== CHANNEL f1 ========
SFO1 100.6238364 MHz
NUC1 13C
P1 8.50 usec
P12 40000.00 usec
P26 500.00 usec
PLW1 55.73500061 W
SPNAM[2] Q3.1000
SPOAL2 0.500
SPOFFS2 0 Hz
SPW2 0.00043873 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 6.15259981 W
======== CHANNEL f2 ========
SFO2 400.1316005 MHz
NUC2 1H
CPDPRG[2 waltz16
PCPD2 90.00 usec
PLW2 15.04800034 W
PLW13 0.21670000 W
F2 - Processing parameters
SI 32768
SF 100.6127477 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
9 8 7 6 5 4 3 2 1 ppm
1.79
1.80
1.80
1.81
1.83
1.84
1.86
2.11
2.12
2.13
2.14
2.15
2.15
2.16
2.86
2.87
2.88
2.89
2.89
2.91
2.91
2.92
2.98
3.00
3.00
3.01
3.02
3.03
3.03
3.05
4.15
4.15
4.97
4.97
4.98
4.99
4.99
5.00
5.02
5.02
5.02
5.03
5.05
5.05
5.06
5.06
5.77
5.78
5.79
5.80
5.80
5.82
5.82
5.83
5.84
5.85
7.27
3.2
1
3.1
7
3.2
0
3.2
0
2.1
3
3.1
2
1.0
4
1.0
5
1.0
4
2.0
3
1.0
0
Current Data Parameters
NAME 08052013-14-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130805
Time 20.30
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 64
DW 71.400 usec
DE 11.40 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 500.1330008 MHz
NUC1 1H
P1 10.35 usec
PLW1 24.00000000 W
F2 - Processing parameters
SI 65536
SF 500.1300085 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
17.26
21.59
21.72
23.96
29.01
29.75
33.28
34.98
66.42
76.98
77.23
77.48
82.94
115.49
138.05
153.76
173.87
Current Data Parameters
NAME 08052013-14-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130805
Time 21.25
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG udeft
TD 21424
SOLVENT CDCl3
NS 800
DS 0
SWH 29761.904 Hz
FIDRES 1.389185 Hz
AQ 0.3599232 sec
RG 128
DW 16.800 usec
DE 7.96 usec
TE 295.0 K
D1 3.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D20 200.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 125.7716224 MHz
NUC1 13C
P1 8.90 usec
P13 2000.00 usec
P26 500.00 usec
PLW1 125.00000000 W
SPNAM[5] Crp60comp.4
SPOAL5 0.500
SPOFFS5 0 Hz
SPW5 15.12800026 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 15.12800026 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 262144
SF 125.7577662 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
9 8 7 6 5 4 3 2 1 ppm
1.50
1.50
1.52
1.56
1.85
1.87
1.88
1.89
1.90
1.91
1.92
2.04
2.06
2.07
2.09
2.11
2.12
2.13
2.13
2.14
2.15
2.16
2.16
2.17
2.18
3.75
3.76
3.78
3.79
3.81
3.82
4.19
4.19
4.94
4.94
4.94
4.96
4.96
4.98
4.98
4.99
5.01
5.01
5.02
5.02
5.74
5.76
5.76
5.77
5.78
5.79
5.80
5.80
5.81
5.82
7.27
3.1
4
3.1
6
3.2
3
3.2
7
1.1
1
3.1
7
1.0
5
2.1
2
1.0
7
1.0
2
1.0
3
2.0
4
1.0
0
Current Data Parameters
NAME 08062013-10-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130807
Time 0.47
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 128
DW 71.400 usec
DE 11.40 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 500.1330008 MHz
NUC1 1H
P1 10.35 usec
PLW1 24.00000000 W
F2 - Processing parameters
SI 65536
SF 500.1300086 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
17.14
18.65
21.57
21.79
28.94
29.84
31.85
32.35
37.50
66.32
76.98
77.23
77.48
82.75
115.15
138.35
153.38
177.70
Current Data Parameters
NAME 08062013-10-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130807
Time 1.42
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG udeft
TD 21424
SOLVENT CDCl3
NS 800
DS 0
SWH 29761.904 Hz
FIDRES 1.389185 Hz
AQ 0.3599232 sec
RG 128
DW 16.800 usec
DE 7.96 usec
TE 295.0 K
D1 3.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D20 200.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 125.7716224 MHz
NUC1 13C
P1 8.90 usec
P13 2000.00 usec
P26 500.00 usec
PLW1 125.00000000 W
SPNAM[5] Crp60comp.4
SPOAL5 0.500
SPOFFS5 0 Hz
SPW5 15.12800026 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 15.12800026 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 262144
SF 125.7577640 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
9 8 7 6 5 4 3 2 1 ppm
0.93
0.95
1.20
1.20
1.21
1.22
1.22
1.22
1.23
1.23
1.24
1.24
1.25
1.26
1.50
1.51
1.52
1.52
1.52
1.53
1.54
1.54
1.54
1.55
1.64
1.65
1.67
1.67
1.68
2.05
2.05
2.06
2.06
2.07
2.08
2.08
2.12
2.13
2.14
2.15
2.15
3.43
3.44
3.45
3.47
3.51
3.52
3.53
3.54
4.94
4.95
4.95
4.96
4.97
4.97
5.01
5.01
5.01
5.02
5.04
5.04
5.05
5.05
5.78
5.79
5.80
5.81
5.81
5.83
5.85
7.27
3.1
9
1.1
9
1.1
9
1.1
9
1.1
0
2.1
2
1.0
1
1.0
0
2.0
3
1.0
0
Current Data Parameters
NAME 08192013-18-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130820
Time 2.24
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 90.5
DW 71.400 usec
DE 11.40 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 500.1330008 MHz
NUC1 1H
P1 10.35 usec
PLW1 24.00000000 W
F2 - Processing parameters
SI 65536
SF 500.1300084 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
16.64
31.38
32.49
35.41
68.39
76.97
77.23
77.48
114.62
139.10
Current Data Parameters
NAME 08192013-18-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130820
Time 3.18
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG udeft
TD 21424
SOLVENT CDCl3
NS 800
DS 0
SWH 29761.904 Hz
FIDRES 1.389185 Hz
AQ 0.3599232 sec
RG 128
DW 16.800 usec
DE 7.96 usec
TE 295.0 K
D1 3.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D20 200.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 125.7716224 MHz
NUC1 13C
P1 8.90 usec
P13 2000.00 usec
P26 500.00 usec
PLW1 125.00000000 W
SPNAM[5] Crp60comp.4
SPOAL5 0.500
SPOFFS5 0 Hz
SPW5 15.12800026 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 15.12800026 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 262144
SF 125.7577647 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
9 8 7 6 5 4 3 2 1 ppm
0.95
0.96
1.22
1.22
1.23
1.23
1.24
1.24
1.25
1.25
1.26
1.54
1.55
1.55
1.56
1.57
1.57
1.57
1.58
1.59
1.79
1.80
1.82
1.83
2.04
2.04
2.05
2.05
2.05
2.07
2.07
2.11
2.12
2.14
3.26
3.27
3.28
3.29
3.33
3.34
3.35
3.36
4.52
4.52
4.94
4.94
4.94
4.96
4.96
4.96
4.99
5.00
5.00
5.00
5.03
5.03
5.04
5.04
5.80
5.82
5.83
5.85
7.27
7.28
7.28
7.29
7.30
7.31
7.34
7.35
7.36
3.1
8
1.1
5
1.3
0
1.0
3
2.1
1
1.0
3
1.0
3
2.0
8
2.0
5
1.0
0
5.2
3
Current Data Parameters
NAME 08192013-19-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130820
Time 0.35
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 90.5
DW 71.400 usec
DE 11.40 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 500.1330008 MHz
NUC1 1H
P1 10.35 usec
PLW1 24.00000000 W
F2 - Processing parameters
SI 65536
SF 500.1300085 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
17.21
31.42
33.04
33.17
73.17
75.99
76.98
77.23
77.48
114.46
127.64
127.73
128.53
138.99
139.27
Current Data Parameters
NAME 08192013-19-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130820
Time 1.29
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG udeft
TD 21424
SOLVENT CDCl3
NS 800
DS 0
SWH 29761.904 Hz
FIDRES 1.389185 Hz
AQ 0.3599232 sec
RG 128
DW 16.800 usec
DE 7.96 usec
TE 295.0 K
D1 3.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D20 200.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 125.7716224 MHz
NUC1 13C
P1 8.90 usec
P13 2000.00 usec
P26 500.00 usec
PLW1 125.00000000 W
SPNAM[5] Crp60comp.4
SPOAL5 0.500
SPOFFS5 0 Hz
SPW5 15.12800026 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 15.12800026 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 262144
SF 125.7577651 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
9 8 7 6 5 4 3 2 1 ppm
0.94
0.95
1.47
1.48
1.49
1.50
1.50
1.51
1.51
1.52
1.53
1.54
1.55
1.78
1.79
1.81
1.82
1.83
1.83
1.84
1.84
1.85
1.86
1.87
2.41
2.41
2.42
2.43
2.43
2.44
2.44
2.45
2.46
2.46
2.47
2.48
2.48
2.49
2.49
2.50
2.51
2.51
3.29
3.30
3.31
3.31
3.32
3.32
3.33
3.34
4.50
7.27
7.27
7.28
7.29
7.29
7.30
7.30
7.30
7.30
7.31
7.33
7.34
7.34
7.36
7.36
7.37
7.37
9.76
9.77
9.77
3.0
1
1.0
2
2.0
5
1.9
7
2.0
0
2.0
0
4.8
2
0.9
0
Current Data Parameters
NAME 08232013-17-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130824
Time 4.59
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 101
DW 71.400 usec
DE 11.40 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 500.1330008 MHz
NUC1 1H
P1 10.35 usec
PLW1 24.00000000 W
F2 - Processing parameters
SI 65536
SF 500.1300083 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
200 180 160 140 120 100 80 60 40 20 ppm
17.10
26.11
33.25
41.78
73.25
75.48
76.98
77.23
77.48
127.75
127.77
128.57
138.71
202.98
Current Data Parameters
NAME 08232013-17-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130824
Time 5.54
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG udeft
TD 21424
SOLVENT CDCl3
NS 800
DS 0
SWH 29761.904 Hz
FIDRES 1.389185 Hz
AQ 0.3599232 sec
RG 128
DW 16.800 usec
DE 7.96 usec
TE 295.0 K
D1 3.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D20 200.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 125.7716224 MHz
NUC1 13C
P1 8.90 usec
P13 2000.00 usec
P26 500.00 usec
PLW1 125.00000000 W
SPNAM[5] Crp60comp.4
SPOAL5 0.500
SPOFFS5 0 Hz
SPW5 15.12800026 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 15.12800026 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 262144
SF 125.7577654 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
9 8 7 6 5 4 3 2 1 ppm
1.41
1.41
1.43
1.43
1.44
1.45
1.46
1.47
1.47
1.48
1.56
1.58
1.60
1.61
1.63
1.65
1.66
1.68
3.45
3.46
3.48
3.64
3.65
3.67
3.81
4.44
6.87
6.88
6.88
6.89
6.90
6.90
7.25
7.26
7.27
7.28
3.6
9
4.2
7
2.0
3
2.0
7
3.0
8
2.0
0
2.0
2
2.5
9
Current Data Parameters
NAME 07092013-44-michaelM
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130709
Time 18.07
INSTRUM AVII400
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 5597.015 Hz
FIDRES 0.085404 Hz
AQ 5.8545494 sec
RG 362
DW 89.333 usec
DE 6.50 usec
TE 295.9 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 400.1324008 MHz
NUC1 1H
P1 12.50 usec
PLW1 15.04800034 W
F2 - Processing parameters
SI 32768
SF 400.1300056 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
22.65
29.67
32.73
55.49
63.07
70.20
72.80
76.91
77.23
77.55
113.97
129.47
130.86
159.33
Current Data Parameters
NAME 07092013-44-michaelM
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130710
Time 5.35
INSTRUM AVII400
PROBHD 5 mm PABBO BB/
PULPROG deptqgpsp.2
TD 65536
SOLVENT CDCl3
NS 800
DS 4
SWH 24038.461 Hz
FIDRES 0.366798 Hz
AQ 1.3631488 sec
RG 2050
DW 20.800 usec
DE 6.50 usec
TE 295.9 K
CNST2 145.0000000
CNST12 1.5000000
D1 2.00000000 sec
D2 0.00344828 sec
D12 0.00002000 sec
D16 0.00020000 sec
D28 1.50000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 100.6238364 MHz
NUC1 13C
P1 8.50 usec
P13 2000.00 usec
PLW0 -1.00000000 W
PLW1 55.73500061 W
SPNAM[5] Crp60comp.4
SPOAL5 0.500
SPOFFS5 0 Hz
SPW5 6.15259981 W
======== CHANNEL f2 ========
SFO2 400.1316005 MHz
NUC2 1H
CPDPRG[2 waltz16
P0 18.00 usec
P3 12.00 usec
P4 24.00 usec
PCPD2 90.00 usec
PLW2 15.04800034 W
PLW12 0.26752999 W
PLW13 0.21670000 W
====== GRADIENT CHANNEL =====
GPNAM[1] SINE.100
GPNAM[2] SINE.100
GPNAM[3] SINE.100
GPZ1 31.00 %
GPZ2 31.00 %
GPZ3 31.00 %
P16 1000.00 usec
F2 - Processing parameters
SI 32768
SF 100.6127487 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
9 8 7 6 5 4 3 2 1 ppm
1.37
1.37
1.38
1.38
1.39
1.40
1.40
1.41
1.41
1.42
1.43
1.44
1.46
1.54
1.55
1.56
1.57
1.59
1.60
1.62
1.64
1.65
3.43
3.45
3.46
3.62
3.63
3.65
3.81
4.44
6.87
6.87
6.88
6.89
6.90
6.90
7.25
7.26
7.26
7.27
7.27
7.28
7.29
4.1
2
1.1
2
4.1
7
2.0
0
2.0
5
3.0
4
2.0
0
2.0
0
2.2
0
Current Data Parameters
NAME 07092013-43-michaelM
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130709
Time 18.02
INSTRUM AVII400
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 5597.015 Hz
FIDRES 0.085404 Hz
AQ 5.8545494 sec
RG 144
DW 89.333 usec
DE 6.50 usec
TE 295.9 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 400.1324008 MHz
NUC1 1H
P1 12.50 usec
PLW1 15.04800034 W
F2 - Processing parameters
SI 32768
SF 400.1300057 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
25.77
26.21
29.91
32.90
55.48
63.12
70.22
72.73
76.91
77.23
77.55
113.94
129.45
130.91
159.30
Current Data Parameters
NAME 07092013-43-michaelM
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130710
Time 4.45
INSTRUM AVII400
PROBHD 5 mm PABBO BB/
PULPROG deptqgpsp.2
TD 65536
SOLVENT CDCl3
NS 800
DS 4
SWH 24038.461 Hz
FIDRES 0.366798 Hz
AQ 1.3631488 sec
RG 2050
DW 20.800 usec
DE 6.50 usec
TE 296.0 K
CNST2 145.0000000
CNST12 1.5000000
D1 2.00000000 sec
D2 0.00344828 sec
D12 0.00002000 sec
D16 0.00020000 sec
D28 1.50000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 100.6238364 MHz
NUC1 13C
P1 8.50 usec
P13 2000.00 usec
PLW0 -1.00000000 W
PLW1 55.73500061 W
SPNAM[5] Crp60comp.4
SPOAL5 0.500
SPOFFS5 0 Hz
SPW5 6.15259981 W
======== CHANNEL f2 ========
SFO2 400.1316005 MHz
NUC2 1H
CPDPRG[2 waltz16
P0 18.00 usec
P3 12.00 usec
P4 24.00 usec
PCPD2 90.00 usec
PLW2 15.04800034 W
PLW12 0.26752999 W
PLW13 0.21670000 W
====== GRADIENT CHANNEL =====
GPNAM[1] SINE.100
GPNAM[2] SINE.100
GPNAM[3] SINE.100
GPZ1 31.00 %
GPZ2 31.00 %
GPZ3 31.00 %
P16 1000.00 usec
F2 - Processing parameters
SI 32768
SF 100.6127500 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
9 8 7 6 5 4 3 2 1 ppm
1.65
1.65
1.66
1.66
1.67
1.67
1.68
1.68
1.69
1.70
1.70
1.70
1.71
1.71
1.72
1.73
1.74
1.74
1.75
1.76
1.76
1.77
1.78
2.44
2.44
2.46
2.46
2.47
2.48
3.45
3.46
3.48
3.81
4.43
6.87
6.88
6.88
6.89
6.90
6.91
6.92
6.94
7.25
7.25
7.26
7.27
7.27
9.76
9.77
9.77
4.5
5
1.7
8
2.0
0
3.0
3
2.0
0
1.9
9
2.4
9
0.8
4
Current Data Parameters
NAME 07022013-16-michaelM
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130702
Time 15.20
INSTRUM AVII400
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 5597.015 Hz
FIDRES 0.085404 Hz
AQ 5.8545494 sec
RG 362
DW 89.333 usec
DE 6.50 usec
TE 295.3 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 400.1324008 MHz
NUC1 1H
P1 12.50 usec
PLW1 15.04800034 W
F2 - Processing parameters
SI 32768
SF 400.1300056 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
200 180 160 140 120 100 80 60 40 20 ppm
19.17
29.34
43.81
55.49
69.65
72.81
76.91
77.23
77.55
113.98
129.48
130.72
159.35
202.80
Current Data Parameters
NAME 07022013-34-michaelM
EXPNO 12
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130703
Time 2.17
INSTRUM AVII400
PROBHD 5 mm PABBO BB/
PULPROG udeftnoe.and
TD 8650
SOLVENT CDCl3
NS 1024
DS 4
SWH 24038.461 Hz
FIDRES 2.779013 Hz
AQ 0.1799200 sec
RG 203
DW 20.800 usec
DE 6.50 usec
TE 295.9 K
D1 2.00000000 sec
D6 0.03000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D15 0.00302000 sec
D20 1.53362894 sec
D21 0.21294050 sec
D24 0.10000000 sec
L4 1
======== CHANNEL f1 ========
SFO1 100.6238364 MHz
NUC1 13C
P1 8.50 usec
P12 40000.00 usec
P26 500.00 usec
PLW1 55.73500061 W
SPNAM[2] Q3.1000
SPOAL2 0.500
SPOFFS2 0 Hz
SPW2 0.00043873 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 6.15259981 W
======== CHANNEL f2 ========
SFO2 400.1316005 MHz
NUC2 1H
CPDPRG[2 waltz16
PCPD2 90.00 usec
PLW2 15.04800034 W
PLW13 0.21670000 W
F2 - Processing parameters
SI 32768
SF 100.6127491 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
9 8 7 6 5 4 3 2 1 ppm
1.41
1.42
1.43
1.43
1.44
1.44
1.45
1.46
1.56
1.58
1.59
1.61
1.61
1.63
1.65
1.65
1.66
1.67
1.69
2.42
2.42
2.44
2.44
2.46
2.46
3.43
3.45
3.46
3.81
4.43
6.87
6.88
6.88
6.89
6.90
6.90
7.25
7.25
7.26
7.27
7.27
7.28
9.76
9.77
9.77
2.3
1
4.9
0
1.8
0
2.0
1
3.0
4
2.0
0
1.9
9
2.9
3
0.8
7
Current Data Parameters
NAME 07022013-15-michaelM
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130702
Time 15.13
INSTRUM AVII400
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 5597.015 Hz
FIDRES 0.085404 Hz
AQ 5.8545494 sec
RG 406
DW 89.333 usec
DE 6.50 usec
TE 295.1 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 400.1324008 MHz
NUC1 1H
P1 12.50 usec
PLW1 15.04800034 W
F2 - Processing parameters
SI 32768
SF 400.1300057 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
200 180 160 140 120 100 80 60 40 20 ppm
22.11
26.06
29.73
44.07
55.50
69.94
72.81
76.91
77.23
77.55
113.97
129.47
130.84
159.35
202.94
Current Data Parameters
NAME 07022013-33-michaelM
EXPNO 12
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130703
Time 1.42
INSTRUM AVII400
PROBHD 5 mm PABBO BB/
PULPROG udeftnoe.and
TD 8650
SOLVENT CDCl3
NS 1024
DS 4
SWH 24038.461 Hz
FIDRES 2.779013 Hz
AQ 0.1799200 sec
RG 203
DW 20.800 usec
DE 6.50 usec
TE 295.8 K
D1 2.00000000 sec
D6 0.03000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D15 0.00302000 sec
D20 1.53362894 sec
D21 0.21294050 sec
D24 0.10000000 sec
L4 1
======== CHANNEL f1 ========
SFO1 100.6238364 MHz
NUC1 13C
P1 8.50 usec
P12 40000.00 usec
P26 500.00 usec
PLW1 55.73500061 W
SPNAM[2] Q3.1000
SPOAL2 0.500
SPOFFS2 0 Hz
SPW2 0.00043873 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 6.15259981 W
======== CHANNEL f2 ========
SFO2 400.1316005 MHz
NUC2 1H
CPDPRG[2 waltz16
PCPD2 90.00 usec
PLW2 15.04800034 W
PLW13 0.21670000 W
F2 - Processing parameters
SI 32768
SF 100.6127483 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
9 8 7 6 5 4 3 2 1 ppm
1.54
1.54
1.55
1.56
1.57
1.58
1.59
1.60
1.63
1.65
1.66
1.68
1.69
1.70
1.72
1.73
1.73
1.74
1.75
1.76
1.77
1.77
1.79
2.47
2.47
3.45
3.47
3.48
3.81
4.37
4.37
4.38
4.38
4.39
4.40
4.44
6.87
6.88
6.88
6.89
6.90
6.90
7.26
7.26
7.27
7.28
7.28
8.4
9
0.9
4
1.9
9
3.0
0
0.9
8
1.9
9
1.9
6
4.3
7
Current Data Parameters
NAME 09272013-19-doh-mc410-F
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130927
Time 21.16
INSTRUM spect
PROBHD 5 mm QNP 1H/13
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 812.7
DW 71.400 usec
DE 6.00 usec
TE 292.6 K
D1 1.00000000 sec
TD0 1
SFO1 499.9029994 MHz
NUC1 1H
P1 10.50 usec
PLW1 -1.00000000 W
F2 - Processing parameters
SI 65536
SF 499.9000044 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
22.01
29.48
37.55
55.49
62.42
70.02
72.81
73.16
76.98
77.23
77.48
85.05
113.97
129.49
130.80
159.33
Current Data Parameters
NAME 09282013-30-doh-mc410-F
EXPNO 10
PROCNO 1
F2 - Processing parameters
SI 262144
SF 125.6999303 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
9 8 7 6 5 4 3 2 1 ppm
1.48
1.48
1.49
1.49
1.50
1.50
1.51
1.52
1.60
1.62
1.63
1.65
1.66
1.68
1.70
1.71
1.71
1.72
1.73
1.74
1.75
1.75
1.76
1.77
1.79
2.46
2.47
3.44
3.45
3.46
3.81
4.35
4.36
4.37
4.37
4.38
4.38
4.44
6.87
6.88
6.88
6.89
6.90
6.90
6.91
7.26
7.27
7.27
7.28
4.4
0
2.2
7
2.1
6
1.4
8
0.9
4
2.1
5
3.6
3
1.0
0
2.2
1
2.3
8
2.6
8
Current Data ParametersNAME 03072014-8-doh-mc410-AEXPNO 10PROCNO 1
F2 - Acquisition ParametersDate_ 20140307Time 17.54INSTRUM spectPROBHD 5 mm PABBO BB/PULPROG zg30TD 65536
SOLVENT CDCl3NS 8DS 2SWH 7002.801 HzFIDRES 0.106854 HzAQ 4.6792703 secRG 90.5DW 71.400 usecDE 11.40 usecTE 295.0 KD1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========SFO1 500.1330008 MHzNUC1 1HP1 10.35 usecPLW1 24.00000000 W
F2 - Processing parametersSI 65536SF 500.1300065 MHzWDW EM
SSB 0LB 0.30 HzGB 0PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
25.03
26.06
29.83
37.77
55.49
62.44
70.13
72.74
73.09
76.98
77.23
77.48
85.14
113.95
129.46
130.89
159.30
Current Data ParametersNAME 03072014-8-doh-mc410-AEXPNO 11PROCNO 1
F2 - Acquisition ParametersDate_ 20140308Time 8.51INSTRUM spectPROBHD 5 mm PABBO BB/PULPROG udeftTD 21424SOLVENT CDCl3
NS 800DS 0SWH 29761.904 HzFIDRES 1.389185 HzAQ 0.3599232 secRG 128DW 16.800 usecDE 7.96 usecTE 295.0 KD1 3.00000000 secD11 0.03000000 secD12 0.00002000 sec
D20 200.00000000 secTD0 1
======== CHANNEL f1 ========SFO1 125.7716224 MHzNUC1 13CP1 8.90 usecP13 2000.00 usecP26 500.00 usecPLW1 125.00000000 WSPNAM[5] Crp60comp.4SPOAL5 0.500
SPOFFS5 0 HzSPW5 15.12800026 WSPNAM[8] Crp60,0.5,20.1SPOAL8 0.500SPOFFS8 0 HzSPW8 15.12800026 W
======== CHANNEL f2 ========SFO2 500.1320005 MHzNUC2 1HCPDPRG[2 waltz65PCPD2 80.00 usecPLW2 24.00000000 WPLW12 0.39015001 W
F2 - Processing parametersSI 262144SF 125.7577649 MHzWDW EMSSB 0LB 2.00 HzGB 0PC 1.40
9 8 7 6 5 4 3 2 1 ppm
1.62
1.63
1.64
1.65
1.65
1.66
1.68
1.76
1.78
1.79
1.80
1.81
1.82
2.62
2.63
2.65
3.22
3.46
3.47
3.48
3.82
4.44
6.89
6.91
6.91
7.27
7.28
7.28
2.2
0
2.0
8
0.9
2
2.0
2
3.0
4
2.0
0
1.9
8
2.2
9
Current Data Parameters
NAME 09192013-41-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130919
Time 16.59
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 101
DW 71.400 usec
DE 11.40 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 500.1330008 MHz
NUC1 1H
P1 10.35 usec
PLW1 24.00000000 W
F2 - Processing parameters
SI 65536
SF 500.1300034 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
20.77
29.06
45.31
55.48
69.57
72.78
76.97
77.23
77.48
78.60
81.62
113.97
129.47
130.72
159.34
187.45
Current Data Parameters
NAME 09192013-41-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130919
Time 23.59
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG udeft
TD 21424
SOLVENT CDCl3
NS 800
DS 0
SWH 29761.904 Hz
FIDRES 1.389185 Hz
AQ 0.3599232 sec
RG 128
DW 16.800 usec
DE 7.96 usec
TE 295.0 K
D1 3.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D20 200.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 125.7716224 MHz
NUC1 13C
P1 8.90 usec
P13 2000.00 usec
P26 500.00 usec
PLW1 125.00000000 W
SPNAM[5] Crp60comp.4
SPOAL5 0.500
SPOFFS5 0 Hz
SPW5 15.12800026 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 15.12800026 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 262144
SF 125.7577660 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
9 8 7 6 5 4 3 2 1 ppm
1.37
1.39
1.40
1.40
1.41
1.42
1.43
1.44
1.45
1.58
1.59
1.61
1.63
1.64
1.66
1.68
1.70
1.71
1.72
1.74
2.58
2.60
2.62
3.20
3.43
3.45
3.46
3.81
4.43
6.87
6.87
6.88
6.89
6.90
6.90
7.24
7.25
7.26
7.27
2.2
0
5.5
8
2.0
6
0.9
4
1.9
7
3.0
0
1.9
8
2.0
1
3.4
6
Current Data Parameters
NAME 10042013-23-michaelM
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131005
Time 6.46
INSTRUM AVII400
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 5597.015 Hz
FIDRES 0.085404 Hz
AQ 5.8545494 sec
RG 322
DW 89.333 usec
DE 6.50 usec
TE 296.4 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 400.1324008 MHz
NUC1 1H
P1 12.50 usec
PLW1 15.04800034 W
F2 - Processing parameters
SI 32768
SF 400.1300058 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
23.76
25.80
29.66
45.59
55.50
69.93
72.80
76.91
77.23
77.55
78.55
81.64
113.98
129.46
130.85
159.35
187.59
Current Data Parameters
NAME 10042013-23-michaelM
EXPNO 12
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131005
Time 7.47
INSTRUM AVII400
PROBHD 5 mm PABBO BB/
PULPROG udeftnoe.and
TD 8650
SOLVENT CDCl3
NS 1024
DS 4
SWH 24038.461 Hz
FIDRES 2.779013 Hz
AQ 0.1799200 sec
RG 203
DW 20.800 usec
DE 6.50 usec
TE 297.1 K
D1 2.00000000 sec
D6 0.03000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D15 0.00302000 sec
D20 1.53362894 sec
D21 0.21294050 sec
D24 0.10000000 sec
L4 1
======== CHANNEL f1 ========
SFO1 100.6238364 MHz
NUC1 13C
P1 8.50 usec
P12 40000.00 usec
P26 500.00 usec
PLW1 55.73500061 W
SPNAM[2] Q3.1000
SPOAL2 0.500
SPOFFS2 0 Hz
SPW2 0.00043873 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 6.15259981 W
======== CHANNEL f2 ========
SFO2 400.1316005 MHz
NUC2 1H
CPDPRG[2 waltz16
PCPD2 90.00 usec
PLW2 15.04800034 W
PLW13 0.21670000 W
F2 - Processing parameters
SI 32768
SF 100.6127483 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
9 8 7 6 5 4 3 2 1 ppm
1.63
1.64
1.67
1.68
1.68
1.69
1.70
1.72
1.72
1.74
1.75
1.77
1.78
2.02
2.03
2.05
2.06
2.06
2.07
2.08
2.09
2.09
2.11
2.75
2.76
2.77
3.46
3.47
3.48
3.82
4.45
6.88
6.90
7.26
7.27
7.28
3.7
3
1.6
9
0.7
8
1.9
8
3.0
5
2.0
0
2.0
0
2.3
1
Current Data Parameters
NAME 09212013-46-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130921
Time 17.55
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 101
DW 71.400 usec
DE 11.40 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 500.1330008 MHz
NUC1 1H
P1 10.35 usec
PLW1 24.00000000 W
F2 - Processing parameters
SI 65536
SF 500.1300087 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
19.80
19.83
19.86
29.21
38.79
38.99
39.20
55.49
69.60
72.84
75.30
75.36
75.41
76.45
76.77
76.98
77.10
77.23
77.48
112.62
113.99
114.47
116.33
129.46
130.72
159.37
Current Data Parameters
NAME 09212013-46-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130921
Time 20.20
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG udeft
TD 21424
SOLVENT CDCl3
NS 800
DS 0
SWH 29761.904 Hz
FIDRES 1.389185 Hz
AQ 0.3599232 sec
RG 128
DW 16.800 usec
DE 7.96 usec
TE 295.0 K
D1 3.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D20 200.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 125.7716224 MHz
NUC1 13C
P1 8.90 usec
P13 2000.00 usec
P26 500.00 usec
PLW1 125.00000000 W
SPNAM[5] Crp60comp.4
SPOAL5 0.500
SPOFFS5 0 Hz
SPW5 15.12800026 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 15.12800026 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 262144
SF 125.7577649 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
-50 -60 -70 -80 -90 -100 -110 ppm
-83.99
Current Data Parameters
NAME 03042014-17-doh-mc410-F
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20140304
Time 11.05
INSTRUM spect
PROBHD 5 mm QNP 1H/13
PULPROG zgfhigqn
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37593.984 Hz
FIDRES 0.573639 Hz
AQ 0.8716288 sec
RG 1625.5
DW 13.300 usec
DE 6.00 usec
TE 293.9 K
D1 1.00000000 sec
d11 0.03000000 sec
d12 0.00002000 sec
TD0 1
SFO1 470.3383309 MHz
NUC1 19F
P1 12.15 usec
PLW1 -1.00000000 W
SFO2 0 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 -1.00000000 W
PLW12 -1.00000000 W
F2 - Processing parameters
SI 65536
SF 470.3759460 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
-83.2 -83.4 -83.6 -83.8 -84.0 -84.2 -84.4 -84.6 -84.8 ppm
-84.03
-84.02
-84.00
-83.98
-83.96
-83.95
Current Data Parameters
NAME 03042014-17-doh-mc410-F
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20140304
Time 11.08
INSTRUM spect
PROBHD 5 mm QNP 1H/13
PULPROG zgflqn
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37593.984 Hz
FIDRES 0.573639 Hz
AQ 0.8716288 sec
RG 1024
DW 13.300 usec
DE 6.00 usec
TE 293.8 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
NUC1 19F
P1 12.15 usec
PL1 -5.00 dB
SFO1 470.3383309 MHz
F2 - Processing parameters
SI 65536
SF 470.3759460 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
9 8 7 6 5 4 3 2 1 ppm
1.56
1.57
1.58
1.59
1.59
1.60
1.62
1.62
1.64
1.65
1.66
1.67
1.99
2.00
2.01
2.01
2.02
2.03
2.04
2.04
2.05
2.06
2.07
2.08
2.08
2.09
2.10
2.74
2.75
2.76
3.44
3.46
3.47
3.82
4.44
6.87
6.88
6.88
6.90
6.90
6.91
7.26
7.26
7.27
7.27
7.28
7.29
6.6
4
1.7
9
0.8
2
1.9
9
3.1
8
2.0
0
2.1
8
2.4
5
Current Data Parameters
NAME 10182013-12-michaelM
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131018
Time 18.02
INSTRUM AVII400
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 5597.015 Hz
FIDRES 0.085404 Hz
AQ 5.8545494 sec
RG 181
DW 89.333 usec
DE 6.50 usec
TE 296.1 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 400.1324008 MHz
NUC1 1H
P1 12.50 usec
PLW1 15.04800034 W
F2 - Processing parameters
SI 32768
SF 400.1300058 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
22.67
22.70
22.73
25.83
29.67
38.97
39.18
39.38
55.48
69.89
72.79
75.23
75.28
75.33
76.48
76.81
76.97
77.14
77.23
77.48
112.66
113.97
114.51
116.36
129.45
130.83
159.33
Current Data Parameters
NAME 10252013-9-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131026
Time 0.16
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG udeft
TD 21424
SOLVENT CDCl3
NS 1600
DS 0
SWH 29761.904 Hz
FIDRES 1.389185 Hz
AQ 0.3599232 sec
RG 128
DW 16.800 usec
DE 7.96 usec
TE 295.0 K
D1 3.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D20 200.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 125.7716224 MHz
NUC1 13C
P1 8.90 usec
P13 2000.00 usec
P26 500.00 usec
PLW1 125.00000000 W
SPNAM[5] Crp60comp.4
SPOAL5 0.500
SPOFFS5 0 Hz
SPW5 15.12800026 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 15.12800026 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 262144
SF 125.7577649 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
-50 -60 -70 -80 -90 -100 -110 ppm
-84.49
Current Data Parameters
NAME 10182013-12-michaelM
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131018
Time 18.07
INSTRUM AVII400
PROBHD 5 mm PABBO BB/
PULPROG zgfhigqn.baseopt
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 29761.904 Hz
FIDRES 0.454131 Hz
AQ 1.1010048 sec
RG 2050
DW 16.800 usec
DE 9.42 usec
TE 296.4 K
D1 1.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 376.4682461 MHz
NUC1 19F
P1 13.20 usec
PLW1 15.53699970 W
======== CHANNEL f2 ========
SFO2 400.1316005 MHz
NUC2 1H
CPDPRG[2 waltz16
PCPD2 90.00 usec
PLW2 15.04800034 W
PLW12 0.26752999 W
F2 - Processing parameters
SI 65536
SF 376.4985513 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
-84.25 -84.30 -84.35 -84.40 -84.45 -84.50 -84.55 -84.60 -84.65 ppm
-84.53
-84.52
-84.49
-84.48
-84.45
-84.44
Current Data Parameters
NAME 10182013-12-michaelM
EXPNO 12
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131018
Time 18.11
INSTRUM AVII400
PROBHD 5 mm PABBO BB/
PULPROG zg30.baseopt
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 29761.904 Hz
FIDRES 0.454131 Hz
AQ 1.1010048 sec
RG 2050
DW 16.800 usec
DE 9.42 usec
TE 296.2 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 376.4682461 MHz
NUC1 19F
P1 13.20 usec
PLW1 15.53699970 W
F2 - Processing parameters
SI 65536
SF 376.4985513 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
9 8 7 6 5 4 3 2 1 ppm
0.96
0.96
0.97
0.97
1.45
1.47
1.48
1.50
1.55
1.56
1.57
1.58
1.59
1.59
1.60
1.61
1.62
1.64
1.65
1.67
1.71
1.73
1.73
1.74
1.74
1.75
1.75
1.78
1.79
1.80
1.81
1.83
1.84
1.85
2.03
2.04
2.06
2.07
3.32
3.32
3.32
3.33
3.33
3.34
3.34
3.45
3.47
3.48
3.83
4.41
4.41
4.42
4.43
4.45
4.52
6.89
6.91
6.91
6.92
7.27
7.29
7.29
7.30
7.30
7.31
7.32
7.34
7.35
7.36
7.36
7.37
3.2
5
1.2
6
2.3
4
10.1
3
2.0
6
2.1
4
2.0
3
3.0
0
0.9
6
1.9
3
2.1
7
1.9
9
8.9
4
Current Data Parameters
NAME 08262013-23-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130826
Time 23.44
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 128
DW 71.400 usec
DE 11.40 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 500.1330008 MHz
NUC1 1H
P1 10.35 usec
PLW1 24.00000000 W
F2 - Processing parameters
SI 65536
SF 500.1300008 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
2030405060708090100110120130140150160170180190 ppm
17.29
17.36
22.79
22.82
22.84
25.79
29.21
29.23
29.62
33.28
33.35
34.71
34.77
39.00
39.21
39.42
55.48
62.30
62.40
69.90
72.77
73.25
75.76
76.98
77.23
77.48
77.92
78.04
78.14
78.24
88.06
88.11
88.17
88.23
88.28
113.11
113.98
114.95
116.80
127.73
127.77
127.79
128.57
129.50
130.74
138.73
138.75
159.34
Current Data Parameters
NAME 09132013-2-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130913
Time 23.29
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG udeft
TD 21424
SOLVENT CDCl3
NS 800
DS 0
SWH 29761.904 Hz
FIDRES 1.389185 Hz
AQ 0.3599232 sec
RG 128
DW 16.800 usec
DE 7.96 usec
TE 295.0 K
D1 3.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D20 200.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 125.7716224 MHz
NUC1 13C
P1 8.90 usec
P13 2000.00 usec
P26 500.00 usec
PLW1 125.00000000 W
SPNAM[5] Crp60comp.4
SPOAL5 0.500
SPOFFS5 0 Hz
SPW5 15.12800026 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 15.12800026 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 262144
SF 125.7577656 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
-55 -60 -65 -70 -75 -80 -85 -90 -95 ppm
-83.10
-83.09
Current Data Parameters
NAME 08252013-60-michaelM
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130825
Time 14.02
INSTRUM AVII400
PROBHD 5 mm PABBO BB/
PULPROG zgfhigqn.baseopt
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 29761.904 Hz
FIDRES 0.454131 Hz
AQ 1.1010048 sec
RG 2050
DW 16.800 usec
DE 9.42 usec
TE 295.7 K
D1 1.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 376.4682461 MHz
NUC1 19F
P1 13.20 usec
PLW1 15.53699970 W
======== CHANNEL f2 ========
SFO2 400.1316005 MHz
NUC2 1H
CPDPRG[2 waltz16
PCPD2 90.00 usec
PLW2 15.04800034 W
PLW12 0.26752999 W
F2 - Processing parameters
SI 65536
SF 376.4985513 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
-83.10 ppm
-82.6 -82.7 -82.8 -82.9 -83.0 -83.1 -83.2 -83.3 -83.4 ppm
-83.16
-83.14
-83.11
-83.09
-83.05
-83.04
Current Data Parameters
NAME 09122013-13-michaelI
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130912
Time 18.50
INSTRUM av300
PROBHD 5 mm QNP 1H/13
PULPROG zg30
TD 131072
SOLVENT CDCl3
NS 64
DS 4
SWH 22522.523 Hz
FIDRES 0.171833 Hz
AQ 2.9097984 sec
RG 2580.3
DW 22.200 usec
DE 6.00 usec
TE 295.2 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
NUC1 19F
P1 8.50 usec
PL1 -3.00 dB
SFO1 282.3817627 MHz
F2 - Processing parameters
SI 131072
SF 282.4044991 MHz
WDW EM
SSB 0
LB 0.50 Hz
GB 0
PC 1.00
9 8 7 6 5 4 3 2 1 ppm
0.95
0.97
1.45
1.46
1.48
1.48
1.49
1.55
1.56
1.57
1.58
1.58
1.60
1.61
1.61
1.63
1.64
1.66
1.67
1.80
1.82
1.83
1.84
1.85
1.85
1.86
1.87
1.88
1.88
1.89
2.08
2.09
2.11
2.67
2.67
2.68
2.68
2.69
2.69
2.70
2.70
3.29
3.30
3.31
3.32
3.33
3.34
3.35
3.45
3.46
3.48
3.83
4.45
4.51
6.89
6.89
6.90
6.91
6.91
7.27
7.29
7.30
7.31
7.32
7.32
7.34
7.35
7.36
7.37
7.37
7.39
3.3
6
9.7
7
2.3
2
1.8
4
2.0
0
2.1
8
2.0
1
3.0
0
2.0
3
2.1
9
2.0
1
10.2
7
Current Data Parameters
NAME 08262013-14-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130826
Time 14.09
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 128
DW 71.400 usec
DE 11.40 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 500.1330008 MHz
NUC1 1H
P1 10.35 usec
PLW1 24.00000000 W
F2 - Processing parameters
SI 65536
SF 500.1299997 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
2030405060708090100110120130140150160170180190 ppm
17.12
22.49
22.51
22.54
25.82
27.58
29.63
33.03
38.74
38.94
39.14
43.38
55.48
69.82
72.79
73.23
75.36
76.97
77.23
77.48
80.46
80.79
81.13
82.53
82.59
82.64
112.76
113.97
114.62
116.49
127.76
128.57
129.44
130.78
138.65
159.34
186.48
Current Data Parameters
NAME 09132013-3-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130914
Time 0.25
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG udeft
TD 21424
SOLVENT CDCl3
NS 800
DS 0
SWH 29761.904 Hz
FIDRES 1.389185 Hz
AQ 0.3599232 sec
RG 128
DW 16.800 usec
DE 7.96 usec
TE 295.0 K
D1 3.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D20 200.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 125.7716224 MHz
NUC1 13C
P1 8.90 usec
P13 2000.00 usec
P26 500.00 usec
PLW1 125.00000000 W
SPNAM[5] Crp60comp.4
SPOAL5 0.500
SPOFFS5 0 Hz
SPW5 15.12800026 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 15.12800026 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 262144
SF 125.7577661 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
-55 -60 -65 -70 -75 -80 -85 -90 -95 -100 -105 ppm
-85.49
Current Data Parameters
NAME 08262013-14-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130826
Time 14.13
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zgfhigqn.3.and
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37500.000 Hz
FIDRES 0.572205 Hz
AQ 0.8738133 sec
RG 128
DW 13.333 usec
DE 7.77 usec
TE 295.0 K
D1 1.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 470.5547296 MHz
NUC1 19F
P1 13.00 usec
PLW1 55.00000000 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 65536
SF 470.5923770 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
-85.2 -85.4 -85.6 -85.8 -86.0 -86.2 -86.4 -86.6 -86.8 ppm
-86.04
-85.98
-85.93
Current Data Parameters
NAME 09122013-14-michaelI
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130912
Time 19.00
INSTRUM av300
PROBHD 5 mm QNP 1H/13
PULPROG zg30
TD 131072
SOLVENT CDCl3
NS 64
DS 4
SWH 22522.523 Hz
FIDRES 0.171833 Hz
AQ 2.9097984 sec
RG 2298.8
DW 22.200 usec
DE 6.00 usec
TE 295.1 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
NUC1 19F
P1 8.50 usec
PL1 -3.00 dB
SFO1 282.3817627 MHz
F2 - Processing parameters
SI 131072
SF 282.4044991 MHz
WDW EM
SSB 0
LB 0.50 Hz
GB 0
PC 1.00
9 8 7 6 5 4 3 2 1 ppm
0.97
0.98
1.42
1.43
1.44
1.45
1.46
1.47
1.48
1.49
1.55
1.57
1.57
1.58
1.60
1.61
1.63
1.64
1.66
1.67
1.73
1.74
1.75
1.75
1.76
1.76
1.78
1.79
1.83
1.84
1.86
1.87
2.03
2.05
2.06
2.08
2.09
2.10
2.11
2.12
2.13
2.14
2.15
2.17
3.30
3.31
3.32
3.32
3.33
3.33
3.34
3.34
3.36
3.45
3.46
3.48
3.82
4.45
4.52
6.89
6.91
7.27
7.28
7.29
7.30
7.32
7.32
7.34
7.36
7.37
7.38
3.1
6
7.4
2
1.0
8
0.9
2
4.0
3
2.0
1
2.0
6
3.0
0
1.9
6
2.0
0
1.9
6
7.1
8
Current Data Parameters
NAME 09162013-38-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130917
Time 5.45
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 57
DW 71.400 usec
DE 11.40 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 500.1330008 MHz
NUC1 1H
P1 10.35 usec
PLW1 24.00000000 W
F2 - Processing parameters
SI 65536
SF 500.1300057 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
17.04
22.47
22.49
22.52
25.78
26.48
26.50
26.52
29.62
33.03
36.42
36.62
36.82
38.70
38.90
39.10
55.46
69.82
72.79
73.25
75.29
76.97
77.23
77.48
78.75
78.81
78.86
78.90
79.09
79.14
79.19
79.24
79.43
79.48
79.53
79.58
112.47
112.63
113.96
114.34
114.51
116.20
116.37
127.73
127.75
128.57
129.44
130.78
138.67
159.33
Current Data Parameters
NAME 09162013-38-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130917
Time 6.39
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG udeft
TD 21424
SOLVENT CDCl3
NS 800
DS 0
SWH 29761.904 Hz
FIDRES 1.389185 Hz
AQ 0.3599232 sec
RG 128
DW 16.800 usec
DE 7.96 usec
TE 295.0 K
D1 3.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D20 200.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 125.7716224 MHz
NUC1 13C
P1 8.90 usec
P13 2000.00 usec
P26 500.00 usec
PLW1 125.00000000 W
SPNAM[5] Crp60comp.4
SPOAL5 0.500
SPOFFS5 0 Hz
SPW5 15.12800026 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 15.12800026 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 262144
SF 125.7577675 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
-50 -60 -70 -80 -90 -100 -110 ppm
-114.54
-85.61
-85.60
-85.59
-85.47
-85.46
-85.45
-84.05
-84.04
-84.03
-84.00
-84.00
-83.98
-83.98
-83.85
-83.84
1.9
6
2.0
0
0.4
0
0.3
2
Current Data Parameters
NAME 08272013-22-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130827
Time 16.05
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zgfhigqn.3.and
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37500.000 Hz
FIDRES 0.572205 Hz
AQ 0.8738133 sec
RG 128
DW 13.333 usec
DE 7.77 usec
TE 295.0 K
D1 1.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 470.5547296 MHz
NUC1 19F
P1 13.00 usec
PLW1 55.00000000 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 65536
SF 470.5923770 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
-85.4 -85.6 ppm
-85.1 -85.2 -85.3 -85.4 -85.5 -85.6 -85.7 -85.8 ppm
-85.60
-85.58
-85.57
-85.56
-85.55
-85.54
-85.53
-85.52
-85.51
-85.43
-85.42
-85.41
-85.39
-85.38
-85.37
-85.36
-85.35
-85.34
2.1
1
2.0
0
Current Data ParametersNAME 04232014-3-doh-mc410-AEXPNO 10PROCNO 1
F2 - Acquisition ParametersDate_ 20140423Time 15.34INSTRUM spectPROBHD 5 mm PABBO BB/PULPROG zgflqnTD 65536
SOLVENT CDCl3NS 64DS 4SWH 37500.000 HzFIDRES 0.572205 HzAQ 0.8738133 secRG 128DW 13.333 usecDE 7.77 usecTE 295.0 KD1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========SFO1 470.5547296 MHzNUC1 19FP1 13.00 usecPLW1 55.00000000 W
F2 - Processing parametersSI 65536SF 470.5923770 MHzWDW EM
SSB 0LB 0.30 HzGB 0PC 1.00
9 8 7 6 5 4 3 2 1 ppm
1.61
1.62
1.71
1.72
1.73
1.75
1.76
1.76
1.77
1.78
1.81
1.82
1.84
1.85
1.86
1.88
2.04
2.05
2.07
2.08
2.08
2.10
2.11
2.12
2.13
2.14
2.15
2.16
3.28
3.29
3.30
3.31
3.31
3.32
3.34
3.34
3.35
3.36
3.64
3.65
3.66
4.51
7.27
7.28
7.29
7.30
7.31
7.31
7.33
7.34
7.35
7.36
7.38
2.9
1
7.9
4
1.2
1
0.9
6
4.1
4
2.0
1
1.9
8
2.0
0
4.9
2
Current Data Parameters
NAME 09162013-39-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130917
Time 7.34
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 80.6
DW 71.400 usec
DE 11.40 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 500.1330008 MHz
NUC1 1H
P1 10.35 usec
PLW1 24.00000000 W
F2 - Processing parameters
SI 65536
SF 500.1300090 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
17.02
22.47
22.50
22.52
25.27
26.50
26.52
26.55
32.46
33.03
36.42
36.62
36.82
38.69
38.89
39.09
62.71
73.28
75.32
76.98
77.23
77.49
78.82
78.88
79.12
79.16
79.21
79.26
79.49
79.54
112.46
112.65
114.33
114.52
116.20
116.38
127.76
127.79
128.60
138.64
Current Data Parameters
NAME 09162013-39-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130917
Time 20.03
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG udeft
TD 21424
SOLVENT CDCl3
NS 800
DS 0
SWH 29761.904 Hz
FIDRES 1.389185 Hz
AQ 0.3599232 sec
RG 128
DW 16.800 usec
DE 7.96 usec
TE 295.0 K
D1 3.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D20 200.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 125.7716224 MHz
NUC1 13C
P1 8.90 usec
P13 2000.00 usec
P26 500.00 usec
PLW1 125.00000000 W
SPNAM[5] Crp60comp.4
SPOAL5 0.500
SPOFFS5 0 Hz
SPW5 15.12800026 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 15.12800026 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 262144
SF 125.7577652 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
-50 -60 -70 -80 -90 -100 -110 ppm
-114.61
-85.56
-85.55
-85.54
-85.39
-85.38
-85.37
-84.02
-84.02
-83.94
-83.93
-83.91
-83.90
-83.82
-83.81
2.0
1
2.0
0
0.1
7
0.4
9
Current Data Parameters
NAME 08292013-38-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130829
Time 18.02
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zgfhigqn.3.and
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37500.000 Hz
FIDRES 0.572205 Hz
AQ 0.8738133 sec
RG 128
DW 13.333 usec
DE 7.77 usec
TE 295.0 K
D1 1.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 470.5547296 MHz
NUC1 19F
P1 13.00 usec
PLW1 55.00000000 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 65536
SF 470.5923770 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
-85.2 -85.4 -85.6 -85.8 ppm
-85.1 -85.2 -85.3 -85.4 -85.5 -85.6 -85.7 -85.8 ppm
-85.60
-85.58
-85.57
-85.56
-85.55
-85.54
-85.53
-85.52
-85.51
-85.43
-85.42
-85.41
-85.39
-85.38
-85.37
-85.36
-85.35
-85.34
Current Data Parameters
NAME 04232014-3-doh-mc410-AEXPNO 10PROCNO 1
F2 - Acquisition ParametersDate_ 20140423Time 15.34INSTRUM spectPROBHD 5 mm PABBO BB/PULPROG zgflqnTD 65536
SOLVENT CDCl3NS 64DS 4SWH 37500.000 HzFIDRES 0.572205 HzAQ 0.8738133 secRG 128DW 13.333 usecDE 7.77 usecTE 295.0 KD1 1.00000000 secTD0 1
======== CHANNEL f1 ========SFO1 470.5547296 MHzNUC1 19FP1 13.00 usecPLW1 55.00000000 W
F2 - Processing parametersSI 65536SF 470.5923770 MHzWDW EMSSB 0LB 0.30 HzGB 0PC 1.00
9 8 7 6 5 4 3 2 1 ppm
1.69
1.71
1.72
1.74
1.75
1.77
1.78
1.79
1.81
1.82
1.83
1.85
1.86
1.87
2.03
2.04
2.05
2.06
2.07
2.08
2.09
2.10
2.11
2.12
2.13
2.14
2.15
2.17
2.18
2.38
2.39
2.41
3.30
3.32
3.32
3.33
3.34
3.35
3.36
3.37
4.53
7.27
7.28
7.29
7.30
7.31
7.32
7.33
7.34
7.35
7.36
7.38
2.9
7
0.9
8
5.2
4
1.0
6
4.0
7
2.0
4
1.9
7
2.0
0
4.9
6
Current Data Parameters
NAME 10172013-1-doh-mc410-A_2
EXPNO 14
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131017
Time 20.06
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 128
DW 71.400 usec
DE 11.40 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 500.1330008 MHz
NUC1 1H
P1 10.35 usec
PLW1 24.00000000 W
F2 - Processing parameters
SI 65536
SF 500.1300077 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
16.92
22.16
22.19
22.22
24.07
26.47
26.50
26.52
33.00
33.49
36.41
36.61
36.81
38.37
38.57
38.77
73.24
75.26
76.97
77.23
77.48
78.84
78.94
79.00
79.04
79.18
79.31
79.38
112.32
112.62
114.17
114.48
116.04
116.36
127.87
128.62
138.42
177.32
Current Data Parameters
NAME 10252013-8-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131025
Time 22.30
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG udeft
TD 21424
SOLVENT CDCl3
NS 3200
DS 0
SWH 29761.904 Hz
FIDRES 1.389185 Hz
AQ 0.3599232 sec
RG 128
DW 16.800 usec
DE 7.96 usec
TE 295.0 K
D1 3.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D20 200.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 125.7716224 MHz
NUC1 13C
P1 8.90 usec
P13 2000.00 usec
P26 500.00 usec
PLW1 125.00000000 W
SPNAM[5] Crp60comp.4
SPOAL5 0.500
SPOFFS5 0 Hz
SPW5 15.12800026 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 15.12800026 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 262144
SF 125.7577639 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
-50 -60 -70 -80 -90 -100 -110 ppm
-85.43
-85.42
-85.40
-85.39
-85.33
-85.32
-85.32
-83.91
-83.90
-83.86
-83.85
1.9
6
2.0
0
0.2
9
Current Data Parameters
NAME 10172013-1-doh-mc410-A_2
EXPNO 12
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131017
Time 16.46
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zgfhigqn.3.and
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37500.000 Hz
FIDRES 0.572205 Hz
AQ 0.8738133 sec
RG 128
DW 13.333 usec
DE 7.77 usec
TE 295.0 K
D1 1.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 470.5547296 MHz
NUC1 19F
P1 13.00 usec
PLW1 55.00000000 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 65536
SF 470.5923770 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
-85.2 -85.4 -85.6 ppm
-85.1 -85.2 -85.3 -85.4 -85.5 -85.6 ppm
-85.45
-85.44
-85.43
-85.42
-85.40
-85.39
-85.38
-85.37
-85.36
-85.35
-85.33
-85.32
-85.32
-85.31
-85.29
-85.28
4.0
0
Current Data Parameters
NAME 10172013-1-doh-mc410-A_2
EXPNO 13
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131017
Time 16.49
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zgflqn
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37500.000 Hz
FIDRES 0.572205 Hz
AQ 0.8738133 sec
RG 128
DW 13.333 usec
DE 7.77 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 470.5547296 MHz
NUC1 19F
P1 13.00 usec
PLW1 55.00000000 W
F2 - Processing parameters
SI 65536
SF 470.5923770 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
9 8 7 6 5 4 3 2 1 ppm
1.55
1.56
1.59
1.60
1.62
1.63
1.63
1.64
1.65
1.67
1.68
1.70
1.71
1.81
1.82
1.83
1.85
1.86
1.88
1.90
1.91
1.92
1.93
1.96
1.98
2.00
2.00
2.03
2.05
2.06
2.07
2.08
2.33
2.35
2.36
3.49
3.50
3.68
7.27
3.0
0
1.0
9
7.4
8
4.1
4
3.7
2
2.0
0
2.0
0
2.9
9
Current Data Parameters
NAME 09192013-26-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130919
Time 15.39
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 71.8
DW 71.400 usec
DE 11.40 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 500.1330008 MHz
NUC1 1H
P1 10.35 usec
PLW1 24.00000000 W
F2 - Processing parameters
SI 65536
SF 500.1300087 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
22.04
22.07
24.74
25.74
25.77
25.81
29.10
29.14
29.31
29.35
29.52
29.55
33.93
34.34
34.54
34.74
35.53
36.43
36.63
36.83
51.81
67.99
76.97
77.23
77.48
122.48
122.75
124.39
124.67
126.31
126.59
174.00
Current Data Parameters
NAME 09192013-42-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130920
Time 1.10
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG udeft
TD 21424
SOLVENT CDCl3
NS 800
DS 0
SWH 29761.904 Hz
FIDRES 1.389185 Hz
AQ 0.3599232 sec
RG 128
DW 16.800 usec
DE 7.96 usec
TE 295.0 K
D1 3.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D20 200.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 125.7716224 MHz
NUC1 13C
P1 8.90 usec
P13 2000.00 usec
P26 500.00 usec
PLW1 125.00000000 W
SPNAM[5] Crp60comp.4
SPOAL5 0.500
SPOFFS5 0 Hz
SPW5 15.12800026 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 15.12800026 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 262144
SF 125.7577653 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
-50 -60 -70 -80 -90 -100 -110 ppm
-99.90
-99.81
0.9
9
1.0
0
Current Data Parameters
NAME 09132013-33-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130913
Time 16.35
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zgfhigqn.3.and
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37500.000 Hz
FIDRES 0.572205 Hz
AQ 0.8738133 sec
RG 128
DW 13.333 usec
DE 7.77 usec
TE 295.0 K
D1 1.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 470.5547296 MHz
NUC1 19F
P1 13.00 usec
PLW1 55.00000000 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 65536
SF 470.5923770 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
-99.7 -99.8 -99.9 -100.0 ppm
-99.6 -99.7 -99.8 -99.9 -100.0 -100.1 ppm
-99.97
-99.94
-99.91
-99.87
-99.85
-99.81
-99.78
-99.74
4.0
0
Current Data ParametersNAME 04232014-4-doh-mc410-AEXPNO 10PROCNO 1
F2 - Acquisition ParametersDate_ 20140423Time 15.40INSTRUM spectPROBHD 5 mm PABBO BB/PULPROG zgflqnTD 65536
SOLVENT CDCl3NS 64DS 4SWH 37500.000 HzFIDRES 0.572205 HzAQ 0.8738133 secRG 128DW 13.333 usecDE 7.77 usecTE 295.0 KD1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========SFO1 470.5547296 MHzNUC1 19FP1 13.00 usecPLW1 55.00000000 W
F2 - Processing parametersSI 65536SF 470.5923770 MHzWDW EM
SSB 0LB 0.30 HzGB 0PC 1.00
9 8 7 6 5 4 3 2 1 ppm
0.94
0.95
1.23
1.25
1.26
1.28
1.29
1.30
1.31
1.31
1.32
1.33
1.34
1.35
1.37
1.52
1.54
1.55
1.55
1.56
1.57
1.57
1.58
1.62
1.63
1.64
1.66
1.67
1.67
1.68
1.69
1.70
1.72
1.73
1.75
1.79
1.80
1.82
1.83
1.85
1.87
1.87
1.88
1.90
1.91
1.92
1.93
1.94
1.94
1.96
1.97
1.98
1.99
2.00
2.01
2.02
2.03
2.06
2.07
2.08
2.39
2.40
2.42
3.49
3.50
3.51
3.52
3.53
3.54
3.55
7.27
3.0
0
2.1
3
2.3
5
4.4
2
4.1
5
3.6
0
2.0
0
2.0
9
Current Data Parameters
NAME 09282013-28-doh-mc410-F
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130928
Time 18.33
INSTRUM spect
PROBHD 5 mm QNP 1H/13
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 574.7
DW 71.400 usec
DE 6.00 usec
TE 293.0 K
D1 1.00000000 sec
TD0 1
SFO1 499.9029994 MHz
NUC1 1H
P1 10.50 usec
PLW1 -1.00000000 W
F2 - Processing parameters
SI 65536
SF 499.9000044 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
21.99
22.03
24.45
25.84
25.88
25.91
29.04
29.08
29.29
29.32
29.47
29.49
33.54
34.23
34.43
34.63
35.48
36.19
36.39
36.59
68.08
76.97
77.23
77.48
122.57
122.80
124.48
124.71
126.39
126.64
177.53
Current Data Parameters
NAME 10022013-4-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131004
Time 2.19
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG udeft
TD 21424
SOLVENT CDCl3
NS 1600
DS 0
SWH 29761.904 Hz
FIDRES 1.389185 Hz
AQ 0.3599232 sec
RG 128
DW 16.800 usec
DE 7.96 usec
TE 295.0 K
D1 3.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D20 200.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 125.7716224 MHz
NUC1 13C
P1 8.90 usec
P13 2000.00 usec
P26 500.00 usec
PLW1 125.00000000 W
SPNAM[5] Crp60comp.4
SPOAL5 0.500
SPOFFS5 0 Hz
SPW5 15.12800026 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 15.12800026 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 262144
SF 125.7577644 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
-50 -60 -70 -80 -90 -100 -110 ppm
-99.23
-98.86
-98.85
2.0
0
1.9
8
Current Data Parameters
NAME 04242014-27-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20140424
Time 15.59
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zgfhigqn.3.and
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37500.000 HzFIDRES 0.572205 Hz
AQ 0.8738133 sec
RG 128
DW 13.333 usec
DE 7.77 usec
TE 295.0 K
D1 1.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 470.5547296 MHz
NUC1 19F
P1 13.00 usec
PLW1 55.00000000 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 65536
SF 470.5923770 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
-98.8 -99.0 -99.2 ppm
-98.7 -98.8 -98.9 -99.0 -99.1 -99.2 -99.3 -99.4 ppm-99.30
-99.26
-99.23
-99.19
-99.16
-98.93
-98.90
-98.88
-98.86
-98.85
-98.83
-98.82
-98.78
2.0
0
2.0
4
Current Data ParametersNAME 04232014-5-doh-mc410-AEXPNO 10PROCNO 1
F2 - Acquisition ParametersDate_ 20140423Time 15.45INSTRUM spectPROBHD 5 mm PABBO BB/PULPROG zgflqnTD 65536
SOLVENT CDCl3NS 64DS 4SWH 37500.000 HzFIDRES 0.572205 HzAQ 0.8738133 secRG 128DW 13.333 usecDE 7.77 usecTE 295.0 KD1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========SFO1 470.5547296 MHzNUC1 19FP1 13.00 usecPLW1 55.00000000 W
F2 - Processing parametersSI 65536SF 470.5923770 MHzWDW EM
SSB 0LB 0.30 HzGB 0PC 1.00
9 8 7 6 5 4 3 2 1 ppm
0.97
0.99
1.15
1.17
1.22
1.33
1.34
1.34
1.35
1.36
1.37
1.38
1.41
1.42
1.42
1.44
1.45
1.49
1.50
1.52
1.54
1.55
1.57
1.58
1.59
1.60
1.61
1.63
1.72
1.73
1.74
1.75
1.77
1.78
1.81
1.82
1.84
1.86
1.88
1.88
1.89
1.90
1.91
1.91
1.93
1.95
1.96
1.98
2.00
2.03
2.04
2.36
2.37
2.37
2.39
2.40
2.41
2.46
2.47
2.48
2.49
2.50
2.50
3.75
3.78
3.79
4.19
4.20
4.22
4.22
7.27
3.0
2
16.9
1
2.0
4
1.0
0
1.0
2
Current Data Parameters
NAME 09262013-32-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130926
Time 14.22
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 128
DW 71.400 usec
DE 11.40 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 500.1330008 MHz
NUC1 1H
P1 10.35 usec
PLW1 24.00000000 W
F2 - Processing parameters
SI 65536
SF 500.1300088 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
28.10
28.13
28.18
28.21
28.26
28.32
28.36
28.38
28.40
28.43
28.47
28.54
28.57
28.60
28.63
28.65
28.70
31.35
31.55
31.75
32.26
34.12
34.32
34.42
34.52
67.93
76.98
77.23
77.48
123.29
123.63
125.20
125.54
127.12
127.46
173.07
Current Data Parameters
NAME 06112013-18-doh-mc410-A
EXPNO 12
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130611
Time 21.42
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG udeft
TD 21424
SOLVENT CDCl3
NS 800
DS 0
SWH 29761.904 Hz
FIDRES 1.389185 Hz
AQ 0.3599232 sec
RG 128
DW 16.800 usec
DE 7.96 usec
TE 295.0 K
D1 3.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D20 200.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 125.7716224 MHz
NUC1 13C
P1 8.90 usec
P13 2000.00 usec
P26 500.00 usec
PLW1 125.00000000 W
SPNAM[5] Crp60comp.4
SPOAL5 0.500
SPOFFS5 0 Hz
SPW5 15.12800026 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 15.12800026 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 262144
SF 125.7577653 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
-50 -60 -70 -80 -90 -100 -110 ppm
-92.49
-91.96
-91.36
-91.04
-91.01
-90.83
0.2
7
0.7
4
0.7
4
1.9
8
0.2
8
Current Data Parameters
NAME 09262013-32-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130926
Time 14.26
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zgfhigqn.3.and
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37500.000 Hz
FIDRES 0.572205 Hz
AQ 0.8738133 sec
RG 128
DW 13.333 usec
DE 7.77 usec
TE 295.0 K
D1 1.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 470.5547296 MHz
NUC1 19F
P1 13.00 usec
PLW1 55.00000000 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 65536
SF 470.5923770 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
-90.5 -91.0 -91.5 -92.0 -92.5 ppm
-92.49
-91.96
-91.36
-91.04
-91.01
-90.83
0.2
7
0.7
4
0.7
4
1.9
8
0.2
8
Current Data Parameters
NAME 09262013-32-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130926
Time 14.26
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zgfhigqn.3.and
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37500.000 Hz
FIDRES 0.572205 Hz
AQ 0.8738133 sec
RG 128
DW 13.333 usec
DE 7.77 usec
TE 295.0 K
D1 1.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 470.5547296 MHz
NUC1 19F
P1 13.00 usec
PLW1 55.00000000 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 65536
SF 470.5923770 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
-90.5 -91.0 -91.5 -92.0 -92.5 ppm
-92.55
-92.53
-92.51
-92.50
-92.48
-92.47
-92.45
-92.43
-92.02
-92.00
-91.97
-91.95
-91.93
-91.90
-91.42
-91.39
-91.37
-91.35
-91.32
-91.30
-91.10
-91.07
-91.04
-91.02
-90.99
-90.96
-90.90
-90.87
-90.85
-90.82
-90.80
-90.77
-90.73
-90.70
0.2
8
0.7
6
0.8
6
2.0
0
0.4
7
Current Data Parameters
NAME 04232014-56-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20140423
Time 14.31
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zgflqn
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37500.000 HzFIDRES 0.572205 Hz
AQ 0.8738133 sec
RG 128
DW 13.333 usec
DE 7.77 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 470.5547296 MHz
NUC1 19F
P1 13.00 usec
PLW1 55.00000000 W
F2 - Processing parameters
SI 65536SF 470.5923770 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
9 8 7 6 5 4 3 2 1 ppm
0.95
0.95
0.96
0.96
1.27
1.28
1.29
1.30
1.31
1.32
1.34
1.51
1.52
1.53
1.54
1.55
1.55
1.56
1.57
1.58
1.59
1.60
1.61
1.61
1.62
1.63
1.64
1.65
1.66
1.66
1.80
1.81
1.82
1.84
1.85
2.46
2.47
2.48
2.48
2.49
2.74
2.75
2.76
2.77
2.90
2.91
2.91
3.27
3.28
3.29
3.29
3.30
3.30
3.31
3.32
3.33
3.33
3.35
4.51
7.27
7.28
7.28
7.29
7.29
7.30
7.31
7.34
7.35
7.35
7.36
7.37
3.0
2
1.0
8
3.3
0
1.0
3
0.9
9
1.0
1
0.9
9
2.0
0
2.0
0
4.8
5
Current Data Parameters
NAME 09192013-40-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130919
Time 16.55
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 80.6
DW 71.400 usec
DE 11.40 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 500.1330008 MHz
NUC1 1H
P1 10.35 usec
PLW1 24.00000000 W
F2 - Processing parameters
SI 65536
SF 500.1300088 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
17.17
17.21
29.94
29.96
30.13
30.18
33.46
33.51
47.28
47.41
52.68
52.72
73.21
73.23
75.83
76.97
77.23
77.48
127.68
127.74
128.54
138.86
Current Data Parameters
NAME 09192013-40-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130919
Time 22.48
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG udeft
TD 21424
SOLVENT CDCl3
NS 800
DS 0
SWH 29761.904 Hz
FIDRES 1.389185 Hz
AQ 0.3599232 sec
RG 128
DW 16.800 usec
DE 7.96 usec
TE 295.0 K
D1 3.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D20 200.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 125.7716224 MHz
NUC1 13C
P1 8.90 usec
P13 2000.00 usec
P26 500.00 usec
PLW1 125.00000000 W
SPNAM[5] Crp60comp.4
SPOAL5 0.500
SPOFFS5 0 Hz
SPW5 15.12800026 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 15.12800026 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 262144
SF 125.7577667 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
9 8 7 6 5 4 3 2 1 ppm
0.93
0.94
0.94
0.95
1.49
1.50
1.50
1.51
1.52
1.52
1.53
1.53
1.54
1.55
1.56
1.57
1.57
1.59
1.60
1.61
1.62
1.63
1.64
1.65
1.66
1.66
1.67
1.68
1.70
1.78
1.80
1.81
2.00
2.02
2.03
2.05
2.06
2.42
2.43
2.43
2.44
2.46
2.47
2.48
3.29
3.30
3.30
3.31
3.32
3.45
3.46
3.47
3.76
3.77
3.78
3.81
4.44
4.51
6.88
6.90
7.26
7.27
7.27
7.29
7.29
7.30
7.31
7.33
7.34
7.35
7.37
3.1
0
1.2
2
7.2
7
1.4
4
1.0
3
2.1
3
2.0
9
1.9
9
2.1
8
1.0
3
3.0
3
2.0
0
2.0
0
2.0
2
7.3
1
Current Data Parameters
NAME 10112013-9-doh-mc410-A
EXPNO 12
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131011
Time 22.01
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 80.6
DW 71.400 usec
DE 11.40 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 500.1330008 MHz
NUC1 1H
P1 10.35 usec
PLW1 24.00000000 W
F2 - Processing parameters
SI 65536
SF 500.1300081 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
17.25
17.31
20.09
27.39
27.57
29.19
29.67
29.71
33.41
33.61
33.89
33.92
39.04
39.26
39.46
55.48
69.62
69.93
70.12
72.81
73.24
73.27
75.78
75.90
76.16
76.22
76.49
76.54
76.98
77.23
77.48
85.42
85.47
113.19
113.98
115.04
116.88
127.71
127.74
127.79
127.81
128.56
129.48
130.67
138.74
138.79
159.35
Current Data Parameters
NAME 10112013-9-doh-mc410-A
EXPNO 13
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131011
Time 22.56
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG udeft
TD 21424
SOLVENT CDCl3
NS 800
DS 0
SWH 29761.904 Hz
FIDRES 1.389185 Hz
AQ 0.3599232 sec
RG 128
DW 16.800 usec
DE 7.96 usec
TE 295.0 K
D1 3.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D20 200.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 125.7716224 MHz
NUC1 13C
P1 8.90 usec
P13 2000.00 usec
P26 500.00 usec
PLW1 125.00000000 W
SPNAM[5] Crp60comp.4
SPOAL5 0.500
SPOFFS5 0 Hz
SPW5 15.12800026 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 15.12800026 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 262144
SF 125.7577662 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
-50 -60 -70 -80 -90 -100 -110 ppm
-81.27
-81.25
Current Data Parameters
NAME 10112013-9-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131011
Time 17.24
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zgfhigqn.3.and
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37500.000 Hz
FIDRES 0.572205 Hz
AQ 0.8738133 sec
RG 128
DW 13.333 usec
DE 7.77 usec
TE 295.0 K
D1 1.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 470.5547296 MHz
NUC1 19F
P1 13.00 usec
PLW1 55.00000000 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 65536
SF 470.5923770 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
-81.2 -81.3 ppm
-81.15 -81.20 -81.25 -81.30 -81.35 ppm
-81.31
-81.30
-81.29
-81.27
-81.26
-81.25
-81.24
-81.23
-81.22
-81.21
Current Data Parameters
NAME 10112013-9-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131011
Time 17.28
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zgflqn
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37500.000 Hz
FIDRES 0.572205 Hz
AQ 0.8738133 sec
RG 128
DW 13.333 usec
DE 7.77 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 470.5547296 MHz
NUC1 19F
P1 13.00 usec
PLW1 55.00000000 W
F2 - Processing parameters
SI 65536
SF 470.5923770 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
9 8 7 6 5 4 3 2 1 ppm
0.95
0.96
0.97
1.50
1.51
1.52
1.52
1.54
1.54
1.56
1.57
1.58
1.59
1.60
1.61
1.62
1.64
1.65
1.66
1.66
1.68
1.69
1.80
1.81
1.94
1.95
1.97
2.43
2.45
2.45
2.46
2.46
2.47
3.29
3.30
3.31
3.32
3.32
3.33
3.34
3.35
3.45
3.47
3.48
3.67
3.67
3.68
3.83
4.45
4.52
5.59
5.62
5.84
5.86
6.89
6.89
6.90
6.91
6.91
6.92
7.27
7.29
7.29
7.30
7.30
7.31
7.32
7.35
7.36
7.36
7.37
3.0
3
1.2
0
9.2
5
1.1
4
1.9
2
1.8
7
2.0
3
2.4
2
1.0
6
3.0
0
1.9
7
2.0
4
0.9
6
0.9
3
1.9
8
7.4
5
Current Data Parameters
NAME 11062013-16-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131107
Time 3.13
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 80.6
DW 71.400 usec
DE 11.40 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 500.1330008 MHz
NUC1 1H
P1 10.35 usec
PLW1 24.00000000 W
F2 - Processing parameters
SI 65536
SF 500.1300003 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
17.32
17.41
19.40
19.43
19.46
29.59
29.77
29.82
33.53
33.71
34.68
34.75
36.25
36.41
38.21
38.42
38.63
55.48
69.77
71.70
71.93
72.80
73.20
73.24
75.84
75.98
76.98
77.23
77.48
113.97
120.82
122.73
124.63
126.71
126.75
126.92
126.97
127.14
127.18
127.68
127.70
127.78
127.80
128.54
129.46
130.74
134.08
134.10
134.13
134.15
134.17
134.19
138.81
138.86
159.34
Current Data Parameters
NAME 11062013-16-doh-mc410-A
EXPNO 12
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131107
Time 4.58
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG udeft
TD 21424
SOLVENT CDCl3
NS 1600
DS 0
SWH 29761.904 Hz
FIDRES 1.389185 Hz
AQ 0.3599232 sec
RG 128
DW 16.800 usec
DE 7.96 usec
TE 295.0 K
D1 3.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D20 200.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 125.7716224 MHz
NUC1 13C
P1 8.90 usec
P13 2000.00 usec
P26 500.00 usec
PLW1 125.00000000 W
SPNAM[5] Crp60comp.4
SPOAL5 0.500
SPOFFS5 0 Hz
SPW5 15.12800026 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 15.12800026 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 262144
SF 125.7577661 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
-50 -60 -70 -80 -90 -100 -110 ppm
-91.00
-90.98
-90.47
-90.45
-90.42
-89.92
-89.89
Current Data Parameters
NAME 11052013-32-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131105
Time 13.49
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zgfhigqn.3.and
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37500.000 Hz
FIDRES 0.572205 Hz
AQ 0.8738133 sec
RG 128
DW 13.333 usec
DE 7.77 usec
TE 295.0 K
D1 1.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 470.5547296 MHz
NUC1 19F
P1 13.00 usec
PLW1 55.00000000 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 65536
SF 470.5923770 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
-90.0 -90.5 ppm
-89.8 -90.0 -90.2 -90.4 -90.6 -90.8 -91.0 ppm
-91.04
-91.01
-90.98
-90.95
-90.92
-90.52
-90.49
-90.46
-90.43
-90.40
-90.37
-89.96
-89.93
-89.90
-89.87
-89.84
0.0
2
1.0
0
0.0
2
Current Data Parameters
NAME 11062013-16-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131106
Time 17.56
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zgflqn
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37500.000 Hz
FIDRES 0.572205 Hz
AQ 0.8738133 sec
RG 128
DW 13.333 usec
DE 7.77 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 470.5547296 MHz
NUC1 19F
P1 13.00 usec
PLW1 55.00000000 W
F2 - Processing parameters
SI 65536
SF 470.5923770 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
9 8 7 6 5 4 3 2 1 ppm
0.92
0.94
1.45
1.47
1.48
1.54
1.56
1.57
1.57
1.58
1.59
1.62
1.63
1.64
1.66
1.67
1.67
1.75
1.76
1.76
1.77
1.78
1.79
1.89
1.91
1.92
2.45
2.46
2.47
2.48
2.49
2.50
3.29
3.29
3.30
3.30
3.42
3.42
3.43
3.43
3.44
3.45
3.46
3.47
3.81
4.44
4.49
6.04
6.88
6.88
6.89
6.90
6.90
7.25
7.26
7.27
7.27
7.28
7.28
7.29
7.29
7.29
7.30
7.30
7.33
7.33
7.34
7.35
7.35
7.36
7.37
3.0
9
7.8
0
1.7
2
2.7
9
1.9
9
3.4
6
3.0
0
1.9
4
1.9
9
0.7
3
0.8
3
1.9
7
7.1
7
Current Data Parameters
NAME 11072013-10-doh-mc410-F
EXPNO 12
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131107
Time 22.27
INSTRUM spect
PROBHD 5 mm QNP 1H/13
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 114
DW 71.400 usec
DE 6.00 usec
TE 293.3 K
D1 1.00000000 sec
TD0 1
SFO1 499.9029994 MHz
NUC1 1H
P1 10.50 usec
PLW1 -1.00000000 W
F2 - Processing parameters
SI 65536
SF 499.9000044 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
200 180 160 140 120 100 80 60 40 20 ppm
17.19
19.27
19.30
19.33
27.76
29.55
33.21
38.01
38.22
38.43
40.55
41.58
55.47
69.70
72.81
73.20
75.64
76.98
77.23
77.48
113.97
120.70
122.61
124.51
126.86
127.07
127.28
127.70
127.77
128.54
129.05
129.09
129.13
129.44
130.73
138.77
159.35
207.75
Current Data Parameters
NAME 11072013-10-doh-mc410-F
EXPNO 13
PROCNO 1
F2 - Processing parameters
SI 262144
SF 125.6999325 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
-50 -60 -70 -80 -90 -100 -110 ppm
-91.88
Current Data Parameters
NAME 11072013-10-doh-mc410-F
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131107
Time 22.23
INSTRUM spect
PROBHD 5 mm QNP 1H/13
PULPROG zgfhigqn
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37593.984 Hz
FIDRES 0.573639 Hz
AQ 0.8716288 sec
RG 1625.5
DW 13.300 usec
DE 6.00 usec
TE 293.5 K
D1 1.00000000 sec
d11 0.03000000 sec
d12 0.00002000 sec
TD0 1
SFO1 470.3383309 MHz
NUC1 19F
P1 12.15 usec
PLW1 -1.00000000 W
SFO2 0 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 -1.00000000 W
PLW12 -1.00000000 W
F2 - Processing parameters
SI 65536
SF 470.3759460 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
-91.2 -91.4 -91.6 -91.8 -92.0 -92.2 ppm
-91.93
-91.92
-91.89
-91.89
-91.86
-91.83
-91.82
Current Data Parameters
NAME 11072013-10-doh-mc410-F
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131107
Time 22.26
INSTRUM spect
PROBHD 5 mm QNP 1H/13
PULPROG zgflqn
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37593.984 Hz
FIDRES 0.573639 Hz
AQ 0.8716288 sec
RG 1149.4
DW 13.300 usec
DE 6.00 usec
TE 293.3 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
NUC1 19F
P1 12.15 usec
PL1 -5.00 dB
SFO1 470.3383309 MHz
F2 - Processing parameters
SI 65536
SF 470.3759460 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
9 8 7 6 5 4 3 2 1 ppm
0.94
0.96
0.98
0.98
0.99
1.16
1.18
1.23
1.55
1.56
1.57
1.58
1.59
1.59
1.60
1.61
1.62
1.64
1.64
1.65
1.67
1.68
1.78
1.79
1.81
1.82
1.83
1.86
1.88
1.89
1.91
1.93
1.94
2.85
2.85
2.87
2.87
3.30
3.30
3.31
3.31
3.32
3.32
3.33
3.44
3.45
3.47
3.81
4.44
4.51
5.80
6.88
6.89
6.90
6.90
7.26
7.27
7.28
7.28
7.29
7.30
7.30
7.31
7.33
7.34
7.35
7.36
7.36
7.37
7.37
7.38
2.8
9
6.4
9
4.4
4
1.9
1
1.9
2
2.0
5
3.0
0
1.9
9
2.0
3
0.6
9
0.7
6
1.9
9
7.3
8
Current Data Parameters
NAME 11072013-11-doh-mc410-F
EXPNO 12
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131108
Time 1.16
INSTRUM spect
PROBHD 5 mm QNP 1H/13
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 HzFIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 114
DW 71.400 usec
DE 6.00 usec
TE 293.3 K
D1 1.00000000 sec
TD0 1
SFO1 499.9029994 MHz
NUC1 1H
P1 10.50 usec
PLW1 -1.00000000 W
F2 - Processing parameters
SI 65536
SF 499.9000045 MHz
WDW EMSSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
17.09
19.28
19.31
19.34
26.01
26.04
26.07
29.56
33.34
33.95
34.14
34.34
35.50
35.71
35.92
38.10
38.31
38.52
55.47
69.71
72.82
73.23
75.56
76.97
77.23
77.48
113.98
120.58
122.28
122.49
124.20
124.39
126.12
127.70
127.75
128.20
128.25
128.29
128.34
128.55
129.44
130.75
138.79
159.36
Current Data Parameters
NAME 11072013-11-doh-mc410-F
EXPNO 13
PROCNO 1
F2 - Processing parameters
SI 262144
SF 125.6999317 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
-50 -60 -70 -80 -90 -100 -110 ppm
-98.51
-91.77
1.0
5
1.0
0
Current Data ParametersNAME 11012013-6-doh-mc410-FEXPNO 11PROCNO 1
F2 - Acquisition ParametersDate_ 20131101Time 15.35INSTRUM spectPROBHD 5 mm QNP 1H/13PULPROG zgfhigqnTD 65536
SOLVENT CDCl3NS 64DS 4SWH 37593.984 HzFIDRES 0.573639 HzAQ 0.8716288 secRG 1625.5DW 13.300 usecDE 6.00 usecTE 295.5 KD1 1.00000000 sec
d11 0.03000000 secd12 0.00002000 secTD0 1SFO1 470.3383309 MHzNUC1 19FP1 12.15 usecPLW1 -1.00000000 WSFO2 499.9019996 MHzNUC2 1HCPDPRG[2 waltz65PCPD2 80.00 usecPLW2 -1.00000000 W
PLW12 -1.00000000 W
F2 - Processing parametersSI 65536SF 470.3759460 MHzWDW EMSSB 0LB 0.30 HzGB 0PC 1.00
-92 -93 -94 -95 -96 -97 -98 ppm
-98.58
-98.54
-98.51
-98.47
-98.44
-91.81
-91.78
-91.75
-91.72
1.0
6
1.0
0Current Data ParametersNAME 11012013-6-doh-mc410-FEXPNO 12PROCNO 1
F2 - Acquisition ParametersDate_ 20131101Time 15.38INSTRUM spectPROBHD 5 mm QNP 1H/13PULPROG zgflqnTD 65536
SOLVENT CDCl3NS 64DS 4SWH 37593.984 HzFIDRES 0.573639 HzAQ 0.8716288 secRG 812.7DW 13.300 usecDE 6.00 usecTE 295.5 KD1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========NUC1 19FP1 12.15 usecPL1 -5.00 dBSFO1 470.3383309 MHz
F2 - Processing parametersSI 65536SF 470.3759460 MHzWDW EM
SSB 0LB 0.30 HzGB 0PC 1.00
9 8 7 6 5 4 3 2 1 ppm
0.94
0.95
1.27
1.28
1.31
1.33
1.34
1.35
1.36
1.37
1.38
1.64
1.65
1.67
1.68
1.69
1.70
1.77
1.79
1.80
1.81
1.82
1.84
1.85
1.85
1.87
1.88
1.89
1.89
1.90
1.95
1.96
1.96
1.98
1.99
2.00
2.01
2.02
2.03
2.04
2.42
2.44
2.45
2.82
2.84
2.86
2.87
2.87
2.89
2.90
3.31
3.32
3.33
4.52
5.67
5.70
5.82
5.83
5.85
5.86
7.27
7.28
7.29
7.29
7.30
7.31
7.31
7.33
7.35
7.36
7.37
3.1
0
1.2
5
1.2
2
7.8
3
2.3
9
1.7
9
1.9
1
1.9
5
0.9
5
1.0
0
5.0
1
Current Data Parameters
NAME 12082013-54-doh-mc410-F
EXPNO 12
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131208
Time 16.29
INSTRUM spect
PROBHD 5 mm QNP 1H/13
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 114
DW 71.400 usec
DE 6.00 usec
TE 293.2 K
D1 1.00000000 sec
TD0 1
SFO1 499.9029994 MHz
NUC1 1H
P1 10.50 usec
PLW1 -1.00000000 W
F2 - Processing parameters
SI 65536
SF 499.9000043 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
17.05
17.59
17.62
17.65
26.02
26.05
26.08
33.29
33.34
33.96
34.16
34.35
35.46
35.67
35.88
37.31
37.52
37.73
73.22
75.54
76.98
77.23
77.48
120.21
122.12
122.21
124.02
124.13
126.06
127.75
127.81
128.07
128.28
128.49
128.56
128.60
128.66
128.71
128.75
129.76
138.65
178.85
Current Data Parameters
NAME 12082013-54-doh-mc410-F
EXPNO 13
PROCNO 1
F2 - Processing parameters
SI 262144
SF 125.6999321 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
-50 -60 -70 -80 -90 -100 -110 ppm
-98.44
-92.05
2.0
8
2.0
0
Current Data Parameters
NAME 12082013-54-doh-mc410-F
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131208
Time 16.25
INSTRUM spect
PROBHD 5 mm QNP 1H/13
PULPROG zgfhigqn
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37593.984 Hz
FIDRES 0.573639 Hz
AQ 0.8716288 sec
RG 812.7
DW 13.300 usec
DE 6.00 usec
TE 293.6 K
D1 1.00000000 sec
d11 0.03000000 sec
d12 0.00002000 sec
TD0 1
SFO1 470.3383309 MHz
NUC1 19F
P1 12.15 usec
PLW1 -1.00000000 W
SFO2 0 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 -1.00000000 W
PLW12 -1.00000000 W
F2 - Processing parameters
SI 65536
SF 470.3759460 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
-91 -92 -93 -94 -95 -96 -97 -98 -99 ppm
-98.51
-98.48
-98.44
-98.41
-98.37
-92.09
-92.06
-92.03
-92.00
1.7
8
2.0
0
Current Data Parameters
NAME 12082013-54-doh-mc410-F
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131208
Time 16.28
INSTRUM spect
PROBHD 5 mm QNP 1H/13
PULPROG zgflqn
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37593.984 Hz
FIDRES 0.573639 Hz
AQ 0.8716288 sec
RG 574.7
DW 13.300 usec
DE 6.00 usec
TE 293.3 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
NUC1 19F
P1 12.15 usec
PL1 -5.00 dB
SFO1 470.3383309 MHz
F2 - Processing parameters
SI 65536
SF 470.3759460 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
-92.0 -92.1 ppm
-98.4 -98.6 ppm
9 8 7 6 5 4 3 2 1 ppm
1.65
1.66
1.67
1.68
1.69
1.70
1.71
1.72
1.77
1.80
1.81
1.81
1.82
1.83
1.83
1.84
1.85
1.86
1.86
1.87
1.88
1.89
1.90
1.91
1.92
1.93
1.93
1.94
1.95
2.38
2.39
2.41
3.48
3.49
3.50
3.51
3.51
3.52
3.53
3.54
3.69
7.27
3.3
9
1.8
9
3.5
2
4.4
8
10.3
0
2.0
0
2.1
0
3.0
0
Current Data Parameters
NAME 12122013-13-doh-mc410-F
EXPNO 12
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131213
Time 2.32
INSTRUM spect
PROBHD 5 mm QNP 1H/13
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 16
DS 2
SWH 7002.801 HzFIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 574.7
DW 71.400 usec
DE 6.00 usec
TE 293.1 K
D1 1.00000000 sec
TD0 1
SFO1 499.9029994 MHz
NUC1 1H
P1 10.50 usec
PLW1 -1.00000000 W
F2 - Processing parameters
SI 65536
SF 499.9000044 MHzWDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
15.70
16.55
17.97
18.01
18.05
25.73
25.76
25.80
33.53
33.94
34.14
34.34
35.57
35.78
35.83
35.92
36.03
36.12
36.23
36.32
51.88
68.04
76.98
77.23
77.48
124.78
125.18
173.68
Current Data Parameters
NAME 12122013-13-doh-mc410-F
EXPNO 13
PROCNO 1
F2 - Processing parameters
SI 262144
SF 125.6999291 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
121122123124125126127128 ppm
122.87
123.27
124.78
125.18
126.70
127.10
Current Data Parameters
NAME 12152013-21-doh-mc410-F
EXPNO 10
PROCNO 1
F2 - Processing parameters
SI 262144
SF 125.6999287 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
-50 -60 -70 -80 -90 -100 -110 ppm
-98.64
-98.48
1.9
7
2.0
0
Current Data Parameters
NAME 12122013-13-doh-mc410-F
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131213
Time 2.27
INSTRUM spect
PROBHD 5 mm QNP 1H/13
PULPROG zgfhigqn
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37593.984 Hz
FIDRES 0.573639 Hz
AQ 0.8716288 sec
RG 1625.5
DW 13.300 usec
DE 6.00 usec
TE 293.6 K
D1 1.00000000 sec
d11 0.03000000 sec
d12 0.00002000 sec
TD0 1
SFO1 470.3383309 MHz
NUC1 19F
P1 12.15 usec
PLW1 -1.00000000 W
SFO2 0 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 -1.00000000 W
PLW12 -1.00000000 W
F2 - Processing parameters
SI 65536
SF 470.3759460 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
-98.4 -98.5 -98.6 -98.7 ppm
-98.3 -98.4 -98.5 -98.6 -98.7 -98.8 ppm
-98.70
-98.67
-98.64
-98.60
-98.57
-98.55
-98.52
-98.48
-98.45
-98.41
1.9
5
2.0
0
Current Data Parameters
NAME 12122013-13-doh-mc410-F
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131213
Time 2.30
INSTRUM spect
PROBHD 5 mm QNP 1H/13
PULPROG zgflqn
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37593.984 Hz
FIDRES 0.573639 Hz
AQ 0.8716288 sec
RG 1149.4
DW 13.300 usec
DE 6.00 usec
TE 293.2 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
NUC1 19F
P1 12.15 usec
PL1 -5.00 dB
SFO1 470.3383309 MHz
F2 - Processing parameters
SI 65536
SF 470.3759460 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
9 8 7 6 5 4 3 2 1 ppm
0.94
0.95
1.27
1.28
1.31
1.33
1.34
1.35
1.36
1.37
1.38
1.64
1.65
1.67
1.68
1.69
1.70
1.77
1.79
1.80
1.81
1.82
1.84
1.85
1.85
1.87
1.88
1.89
1.89
1.90
1.95
1.96
1.96
1.98
1.99
2.00
2.01
2.02
2.03
2.04
2.42
2.44
2.45
2.82
2.84
2.86
2.87
2.87
2.89
2.90
3.31
3.32
3.33
4.52
5.67
5.70
5.82
5.83
5.85
5.86
7.27
7.28
7.29
7.29
7.30
7.31
7.31
7.33
7.35
7.36
7.37
3.1
0
1.2
5
1.2
2
7.8
3
2.3
9
1.7
9
1.9
1
1.9
5
0.9
5
1.0
0
5.0
1
Current Data Parameters
NAME 12082013-54-doh-mc410-F
EXPNO 12
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131208
Time 16.29
INSTRUM spect
PROBHD 5 mm QNP 1H/13
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 114
DW 71.400 usec
DE 6.00 usec
TE 293.2 K
D1 1.00000000 sec
TD0 1
SFO1 499.9029994 MHz
NUC1 1H
P1 10.50 usec
PLW1 -1.00000000 W
F2 - Processing parameters
SI 65536
SF 499.9000043 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
17.05
17.59
17.62
17.65
26.02
26.05
26.08
33.29
33.34
33.96
34.16
34.35
35.46
35.67
35.88
37.31
37.52
37.73
73.22
75.54
76.98
77.23
77.48
120.21
122.12
122.21
124.02
124.13
126.06
127.75
127.81
128.07
128.28
128.49
128.56
128.60
128.66
128.71
128.75
129.76
138.65
178.85
Current Data Parameters
NAME 12082013-54-doh-mc410-F
EXPNO 13
PROCNO 1
F2 - Processing parameters
SI 262144
SF 125.6999321 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
-50 -60 -70 -80 -90 -100 -110 ppm
-98.44
-92.05
2.0
8
2.0
0
Current Data Parameters
NAME 12082013-54-doh-mc410-F
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131208
Time 16.25
INSTRUM spect
PROBHD 5 mm QNP 1H/13
PULPROG zgfhigqn
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37593.984 Hz
FIDRES 0.573639 Hz
AQ 0.8716288 sec
RG 812.7
DW 13.300 usec
DE 6.00 usec
TE 293.6 K
D1 1.00000000 sec
d11 0.03000000 sec
d12 0.00002000 sec
TD0 1
SFO1 470.3383309 MHz
NUC1 19F
P1 12.15 usec
PLW1 -1.00000000 W
SFO2 0 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 -1.00000000 W
PLW12 -1.00000000 W
F2 - Processing parameters
SI 65536
SF 470.3759460 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
-91 -92 -93 -94 -95 -96 -97 -98 -99 ppm
-98.51
-98.48
-98.44
-98.41
-98.37
-92.09
-92.06
-92.03
-92.00
1.7
8
2.0
0
Current Data Parameters
NAME 12082013-54-doh-mc410-F
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131208
Time 16.28
INSTRUM spect
PROBHD 5 mm QNP 1H/13
PULPROG zgflqn
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37593.984 Hz
FIDRES 0.573639 Hz
AQ 0.8716288 sec
RG 574.7
DW 13.300 usec
DE 6.00 usec
TE 293.3 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
NUC1 19F
P1 12.15 usec
PL1 -5.00 dB
SFO1 470.3383309 MHz
F2 - Processing parameters
SI 65536
SF 470.3759460 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
-92.0 -92.1 ppm
-98.4 -98.6 ppm
9 8 7 6 5 4 3 2 1 ppm
1.58
1.77
1.78
1.79
1.80
1.81
1.82
1.83
1.85
1.85
1.86
1.87
1.88
1.89
1.90
1.91
1.92
1.93
1.95
1.96
1.98
1.99
2.01
2.02
2.40
2.42
2.43
2.43
2.44
2.46
2.49
2.50
2.51
2.52
2.53
2.54
3.84
3.85
3.86
3.88
4.18
4.19
4.21
4.21
7.27
3.1
0
4.3
3
11.4
7
1.0
5
1.0
5
1.0
0
1.0
0
Current Data Parameters
NAME 11262013-30-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131127
Time 1.26
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 101
DW 71.400 usec
DE 11.40 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 500.1330008 MHz
NUC1 1H
P1 10.35 usec
PLW1 24.00000000 W
F2 - Processing parameters
SI 65536
SF 500.1300076 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
17.98
18.02
18.96
19.01
19.05
25.78
25.82
25.87
30.73
30.94
31.14
31.80
33.54
33.75
33.93
33.95
34.05
34.14
34.26
34.34
34.46
67.16
76.98
77.23
77.48
123.64
124.19
125.55
126.10
127.47
128.01
172.65
Current Data Parameters
NAME 11262013-30-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131127
Time 3.11
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG udeft
TD 21424
SOLVENT CDCl3
NS 1600
DS 0
SWH 29761.904 Hz
FIDRES 1.389185 Hz
AQ 0.3599232 sec
RG 128
DW 16.800 usec
DE 7.96 usec
TE 295.0 K
D1 3.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D20 200.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 125.7716224 MHz
NUC1 13C
P1 8.90 usec
P13 2000.00 usec
P26 500.00 usec
PLW1 125.00000000 W
SPNAM[5] Crp60comp.4
SPOAL5 0.500
SPOFFS5 0 Hz
SPW5 15.12800026 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 15.12800026 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 262144
SF 125.7577640 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
-50 -60 -70 -80 -90 -100 -110 ppm
-92.07
-91.54
-91.49
-90.99
-90.96
0.0
4
0.9
4
0.9
4
2.0
0
Current Data Parameters
NAME 11262013-2-doh-mc410-F
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131126
Time 13.52
INSTRUM spect
PROBHD 5 mm QNP 1H/13
PULPROG zgfhigqn
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37593.984 Hz
FIDRES 0.573639 Hz
AQ 0.8716288 sec
RG 1290.2
DW 13.300 usec
DE 6.00 usec
TE 293.7 K
D1 1.00000000 sec
d11 0.03000000 sec
d12 0.00002000 sec
TD0 1
SFO1 470.3383309 MHz
NUC1 19F
P1 12.15 usec
PLW1 -1.00000000 W
SFO2 499.9019996 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 -1.00000000 W
PLW12 -1.00000000 W
F2 - Processing parameters
SI 65536
SF 470.3759460 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
-90.2 -90.4 -90.6 -90.8 -91.0 -91.2 -91.4 -91.6 -91.8 -92.0 ppm
-92.07
-91.54
-91.49
-90.99
-90.96
0.0
4
0.9
4
0.9
4
2.0
0
Current Data Parameters
NAME 11262013-2-doh-mc410-F
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131126
Time 13.52
INSTRUM spect
PROBHD 5 mm QNP 1H/13
PULPROG zgfhigqn
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37593.984 Hz
FIDRES 0.573639 Hz
AQ 0.8716288 sec
RG 1290.2
DW 13.300 usec
DE 6.00 usec
TE 293.7 K
D1 1.00000000 sec
d11 0.03000000 sec
d12 0.00002000 sec
TD0 1
SFO1 470.3383309 MHz
NUC1 19F
P1 12.15 usec
PLW1 -1.00000000 W
SFO2 499.9019996 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 -1.00000000 W
PLW12 -1.00000000 W
F2 - Processing parameters
SI 65536
SF 470.3759460 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
-90.8 -91.0 -91.2 -91.4 -91.6 -91.8 -92.0 ppm
-92.13
-92.10
-92.07
-92.04
-92.00
-91.60
-91.57
-91.54
-91.52
-91.51
-91.49
-91.46
-91.43
-91.06
-91.02
-90.99
-90.96
-90.93
0.0
5
1.9
2
2.0
0
Current Data Parameters
NAME 11262013-2-doh-mc410-F
EXPNO 12
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131126
Time 13.55
INSTRUM spect
PROBHD 5 mm QNP 1H/13
PULPROG zgflqn
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37593.984 Hz
FIDRES 0.573639 Hz
AQ 0.8716288 sec
RG 1149.4
DW 13.300 usec
DE 6.00 usec
TE 293.4 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
NUC1 19F
P1 12.15 usec
PL1 -5.00 dB
SFO1 470.3383309 MHz
F2 - Processing parameters
SI 65536
SF 470.3759460 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
9 8 7 6 5 4 3 2 1 ppm
0.93
0.95
1.15
1.15
1.16
1.17
1.17
1.18
1.19
1.20
1.22
1.31
1.32
1.33
1.34
1.34
1.35
1.35
1.40
1.41
1.42
1.42
1.43
1.44
1.45
1.46
1.47
1.47
1.48
1.49
1.49
1.50
1.53
1.55
1.56
1.56
1.56
1.57
1.57
1.58
1.58
1.59
1.60
1.75
1.76
1.78
1.79
1.80
3.25
3.26
3.27
3.28
3.32
3.33
3.33
3.35
3.63
3.64
3.66
4.51
7.27
7.28
7.29
7.29
7.30
7.30
7.34
7.34
7.35
7.36
7.37
3.1
6
7.2
9
1.5
8
1.0
0
1.0
0
2.0
0
2.0
0
4.8
3
Current Data Parameters
NAME 09132013-5-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130914
Time 1.24
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 90.5
DW 71.400 usec
DE 11.40 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 500.1330008 MHz
NUC1 1H
P1 10.35 usec
PLW1 24.00000000 W
F2 - Processing parameters
SI 65536
SF 500.1300090 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
17.28
23.29
33.22
33.60
33.65
63.18
73.18
76.05
76.97
77.23
77.48
127.65
127.75
128.53
138.94
Current Data Parameters
NAME 09132013-5-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130914
Time 2.19
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG udeft
TD 21424
SOLVENT CDCl3
NS 800
DS 0
SWH 29761.904 Hz
FIDRES 1.389185 Hz
AQ 0.3599232 sec
RG 128
DW 16.800 usec
DE 7.96 usec
TE 295.0 K
D1 3.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D20 200.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 125.7716224 MHz
NUC1 13C
P1 8.90 usec
P13 2000.00 usec
P26 500.00 usec
PLW1 125.00000000 W
SPNAM[5] Crp60comp.4
SPOAL5 0.500
SPOFFS5 0 Hz
SPW5 15.12800026 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 15.12800026 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 262144
SF 125.7577661 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
9 8 7 6 5 4 3 2 1 ppm
0.94
0.96
1.15
1.16
1.16
1.17
1.17
1.18
1.18
1.19
1.19
1.20
1.20
1.21
1.46
1.47
1.48
1.48
1.49
1.49
1.50
1.50
1.52
1.53
1.56
1.57
1.59
1.60
1.60
1.61
1.61
1.62
1.62
1.63
1.64
1.68
1.68
1.69
1.70
1.72
1.72
1.73
1.77
1.78
1.80
1.81
2.42
2.43
2.45
3.27
3.28
3.28
3.30
3.30
3.32
3.32
3.33
4.51
7.27
7.28
7.29
7.29
7.30
7.30
7.33
7.34
7.35
7.37
9.77
9.77
9.77
3.0
4
1.0
9
4.6
5
1.7
8
0.9
9
0.9
8
2.0
0
4.7
8
0.8
3
Current Data Parameters
NAME 09182013-19-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130918
Time 18.01
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 114
DW 71.400 usec
DE 11.40 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 500.1330008 MHz
NUC1 1H
P1 10.35 usec
PLW1 24.00000000 W
F2 - Processing parameters
SI 65536
SF 500.1300088 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
200 180 160 140 120 100 80 60 40 20 ppm
17.15
19.74
33.36
33.59
44.37
73.24
75.80
76.97
77.23
77.48
127.71
127.77
128.56
138.86
203.01
Current Data Parameters
NAME 09202013-22-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130921
Time 1.58
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG udeft
TD 21424
SOLVENT CDCl3
NS 800
DS 0
SWH 29761.904 Hz
FIDRES 1.389185 Hz
AQ 0.3599232 sec
RG 128
DW 16.800 usec
DE 7.96 usec
TE 295.0 K
D1 3.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D20 200.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 125.7716224 MHz
NUC1 13C
P1 8.90 usec
P13 2000.00 usec
P26 500.00 usec
PLW1 125.00000000 W
SPNAM[5] Crp60comp.4
SPOAL5 0.500
SPOFFS5 0 Hz
SPW5 15.12800026 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 15.12800026 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 262144
SF 125.7577636 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
9 8 7 6 5 4 3 2 1 ppm
1.47
1.47
1.48
1.50
1.50
1.51
1.53
1.54
1.56
1.57
1.59
1.60
1.61
1.63
1.64
1.66
1.95
1.95
1.96
2.18
2.19
2.20
2.20
2.21
2.22
3.44
3.46
3.47
3.81
4.44
6.88
6.90
7.26
7.27
7.28
6.3
9
0.9
3
2.0
3
2.0
2
3.0
6
2.0
0
1.9
9
2.2
9
Current Data Parameters
NAME 09122013-3-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130912
Time 18.09
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 80.6
DW 71.400 usec
DE 11.40 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 500.1330008 MHz
NUC1 1H
P1 10.35 usec
PLW1 24.00000000 W
F2 - Processing parameters
SI 65536
SF 500.1300085 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
18.58
25.61
28.52
29.47
55.48
68.42
70.11
72.76
76.98
77.23
77.49
84.76
113.95
129.44
130.89
159.30
Current Data Parameters
NAME 09122013-3-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130913
Time 0.32
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG udeft
TD 21424
SOLVENT CDCl3
NS 800
DS 0
SWH 29761.904 Hz
FIDRES 1.389185 Hz
AQ 0.3599232 sec
RG 128
DW 16.800 usec
DE 7.96 usec
TE 295.0 K
D1 3.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D20 200.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 125.7716224 MHz
NUC1 13C
P1 8.90 usec
P13 2000.00 usec
P26 500.00 usec
PLW1 125.00000000 W
SPNAM[5] Crp60comp.4
SPOAL5 0.500
SPOFFS5 0 Hz
SPW5 15.12800026 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 15.12800026 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 262144
SF 125.7577661 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
9 8 7 6 5 4 3 2 1 ppm
0.94
0.95
1.14
1.15
1.16
1.17
1.44
1.45
1.46
1.47
1.47
1.48
1.49
1.49
1.50
1.51
1.52
1.55
1.57
1.58
1.60
1.61
1.62
1.64
1.65
1.72
1.73
1.74
1.75
1.75
1.76
1.77
1.79
1.80
2.35
2.36
2.37
2.50
2.51
2.52
2.52
2.53
2.54
3.25
3.26
3.27
3.28
3.30
3.31
3.32
3.33
3.44
3.45
3.46
3.81
4.43
4.50
6.87
6.88
6.89
7.26
7.27
7.28
7.29
7.29
7.30
7.33
7.34
7.34
7.35
7.37
3.0
5
1.0
4
11.1
2
2.0
0
2.0
5
0.9
9
1.0
1
1.9
8
3.0
0
2.0
1
2.0
1
1.9
9
8.0
8
Current Data Parameters
NAME 09212013-47-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130921
Time 17.59
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 128
DW 71.400 usec
DE 11.40 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 500.1330008 MHz
NUC1 1H
P1 10.35 usec
PLW1 24.00000000 W
F2 - Processing parameters
SI 65536
SF 500.1300090 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
180 160 140 120 100 80 60 40 20 ppm
17.16
19.13
21.75
25.78
27.79
29.40
33.14
33.55
45.95
55.49
69.94
72.81
73.21
75.89
76.97
77.23
77.48
81.16
94.24
113.97
127.67
127.73
128.54
129.45
130.80
138.90
159.34
188.57
Current Data Parameters
NAME 09212013-47-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130921
Time 21.32
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG udeft
TD 21424
SOLVENT CDCl3
NS 800
DS 0
SWH 29761.904 Hz
FIDRES 1.389185 Hz
AQ 0.3599232 sec
RG 128
DW 16.800 usec
DE 7.96 usec
TE 295.0 K
D1 3.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D20 200.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 125.7716224 MHz
NUC1 13C
P1 8.90 usec
P13 2000.00 usec
P26 500.00 usec
PLW1 125.00000000 W
SPNAM[5] Crp60comp.4
SPOAL5 0.500
SPOFFS5 0 Hz
SPW5 15.12800026 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 15.12800026 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 262144
SF 125.7577653 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
9 8 7 6 5 4 3 2 1 ppm
0.94
0.96
1.19
1.19
1.20
1.46
1.46
1.47
1.48
1.49
1.50
1.51
1.52
1.53
1.54
1.55
1.56
1.57
1.59
1.60
1.60
1.61
1.63
1.64
1.65
1.79
1.80
1.98
1.99
1.99
2.00
2.01
2.02
2.25
2.26
2.26
2.27
2.28
2.29
2.30
3.27
3.28
3.29
3.30
3.31
3.32
3.33
3.34
3.44
3.45
3.47
3.81
4.44
4.51
6.88
6.89
6.90
6.90
6.91
7.26
7.27
7.28
7.29
7.30
7.30
7.31
7.34
7.35
7.35
7.36
7.38
3.1
1
1.0
9
9.3
5
1.1
0
1.8
8
1.8
9
2.0
6
2.0
3
3.0
0
2.0
1
2.0
5
2.0
0
7.2
0
Current Data Parameters
NAME 09272013-17-doh-mc410-F
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130927
Time 17.29
INSTRUM spect
PROBHD 5 mm QNP 1H/13
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 114
DW 71.400 usec
DE 6.00 usec
TE 292.4 K
D1 1.00000000 sec
TD0 1
SFO1 499.9029994 MHz
NUC1 1H
P1 10.50 usec
PLW1 -1.00000000 W
F2 - Processing parameters
SI 65536
SF 499.9000040 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
17.10
18.53
20.61
25.67
27.87
29.39
33.12
33.53
39.65
39.86
40.07
55.46
69.96
72.77
73.21
73.95
74.27
74.59
75.89
76.97
77.23
77.48
88.56
88.61
88.66
113.36
113.95
115.19
117.03
127.67
127.71
128.54
129.44
130.81
138.87
159.31
Current Data Parameters
NAME 09272013-17-doh-mc410-F
EXPNO 11
PROCNO 1
F2 - Processing parameters
SI 262144
SF 125.6999329 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
-45 -50 -55 -60 -65 -70 -75 -80 -85 -90 -95 ppm
-82.23
-81.52
-81.50
-80.79
0.0
2
0.9
4
1.0
0
0.0
2
Current Data Parameters
NAME 09242013-29-michaelM
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130924
Time 13.15
INSTRUM AVII400
PROBHD 5 mm PABBO BB/
PULPROG zgfhigqn.baseopt
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 29761.904 Hz
FIDRES 0.454131 Hz
AQ 1.1010048 sec
RG 2050
DW 16.800 usec
DE 9.42 usec
TE 296.3 K
D1 1.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 376.4682461 MHz
NUC1 19F
P1 13.20 usec
PLW1 15.53699970 W
======== CHANNEL f2 ========
SFO2 400.1316005 MHz
NUC2 1H
CPDPRG[2 waltz16
PCPD2 90.00 usec
PLW2 15.04800034 W
PLW12 0.26752999 W
F2 - Processing parameters
SI 65536
SF 376.4985513 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
-81.0 -81.5 -82.0 ppm
-80.4 -80.6 -80.8 -81.0 -81.2 -81.4 -81.6 ppm
-81.63
-81.60
-81.56
-81.07
-81.06
-81.04
-81.03
-81.02
-81.01
-81.00
-80.98
-80.96
-80.95
-80.46
-80.43
-80.40
Current Data Parameters
NAME 09242013-11-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130924
Time 17.58
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zgflqn
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37500.000 Hz
FIDRES 0.572205 Hz
AQ 0.8738133 sec
RG 128
DW 13.333 usec
DE 7.77 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 470.5547296 MHz
NUC1 19F
P1 13.00 usec
PLW1 55.00000000 W
F2 - Processing parameters
SI 65536
SF 470.5923770 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
9 8 7 6 5 4 3 2 1 ppm
0.94
0.95
1.17
1.18
1.19
1.19
1.20
1.22
1.46
1.47
1.48
1.48
1.49
1.50
1.50
1.51
1.52
1.53
1.54
1.55
1.56
1.57
1.57
1.59
1.59
1.60
1.60
1.62
1.63
1.77
1.79
1.80
1.81
1.96
1.97
1.98
1.99
1.99
2.01
2.01
2.02
2.03
2.27
2.28
2.28
2.29
2.30
2.30
2.32
3.27
3.28
3.29
3.30
3.32
3.32
3.34
3.63
3.65
3.66
4.51
7.27
7.28
7.28
7.29
7.29
7.30
7.31
7.33
7.35
7.36
7.37
3.1
2
1.1
0
10.6
2
1.0
7
1.9
4
1.9
5
1.9
9
2.0
2
2.0
0
4.8
5
Current Data Parameters
NAME 09252013-7-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130926
Time 4.08
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 4
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 128
DW 71.400 usec
DE 11.40 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 500.1330008 MHz
NUC1 1H
P1 10.35 usec
PLW1 24.00000000 W
F2 - Processing parameters
SI 65536
SF 500.1300091 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
17.12
18.55
20.69
25.18
27.79
32.30
33.17
33.57
39.67
39.88
40.09
62.84
73.25
74.07
74.39
74.71
75.94
76.97
77.23
77.48
88.46
88.51
88.56
113.37
115.21
117.05
127.71
127.76
128.56
138.83
Current Data Parameters
NAME 09252013-7-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130926
Time 4.06
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG udeft
TD 21424
SOLVENT CDCl3
NS 800
DS 0
SWH 29761.904 Hz
FIDRES 1.389185 Hz
AQ 0.3599232 sec
RG 128
DW 16.800 usec
DE 7.96 usec
TE 295.0 K
D1 3.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D20 200.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 125.7716224 MHz
NUC1 13C
P1 8.90 usec
P13 2000.00 usec
P26 500.00 usec
PLW1 125.00000000 W
SPNAM[5] Crp60comp.4
SPOAL5 0.500
SPOFFS5 0 Hz
SPW5 15.12800026 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 15.12800026 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 262144
SF 125.7577653 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
-45 -50 -55 -60 -65 -70 -75 -80 -85 -90 -95 ppm
-82.25
-81.55
-81.48
-80.77
0.0
4
1.0
0
1.0
2
0.0
4
Current Data Parameters
NAME 09242013-55-michaelM
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130924
Time 17.21
INSTRUM AVII400
PROBHD 5 mm PABBO BB/
PULPROG zgfhigqn.baseopt
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 29761.904 Hz
FIDRES 0.454131 Hz
AQ 1.1010048 sec
RG 2050
DW 16.800 usec
DE 9.42 usec
TE 296.5 K
D1 1.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 376.4682461 MHz
NUC1 19F
P1 13.20 usec
PLW1 15.53699970 W
======== CHANNEL f2 ========
SFO2 400.1316005 MHz
NUC2 1H
CPDPRG[2 waltz16
PCPD2 90.00 usec
PLW2 15.04800034 W
PLW12 0.26752999 W
F2 - Processing parameters
SI 131072
SF 376.4985513 MHz
WDW no
SSB 0
LB 0 Hz
GB 0
PC 1.00
-80.5 -81.0 -81.5 -82.0 -82.5 ppm
-80.6 -80.8 -81.0 -81.2 -81.4 -81.6 -81.8 -82.0 -82.2 -82.4 ppm
-82.29
-82.28
-82.26
-82.25
-82.24
-82.23
-82.21
-82.20
-82.19
-81.58
-81.57
-81.56
-81.54
-81.53
-81.52
-81.51
-81.49
-81.48
-81.47
-81.45
-81.44
-81.43
-81.42
-80.81
-80.80
-80.78
-80.77
-80.76
-80.74
-80.73
-80.72
-80.71
Current Data Parameters
NAME 10022013-37-michaelM
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131002
Time 15.54
INSTRUM AVII400
PROBHD 5 mm PABBO BB/
PULPROG zg30.baseopt
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 29761.904 Hz
FIDRES 0.454131 Hz
AQ 1.1010048 sec
RG 2050
DW 16.800 usec
DE 9.42 usec
TE 296.4 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 376.4682461 MHz
NUC1 19F
P1 13.20 usec
PLW1 15.53699970 W
F2 - Processing parameters
SI 65536
SF 376.4985513 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
9 8 7 6 5 4 3 2 1 ppm
0.93
0.95
1.15
1.16
1.17
1.18
1.18
1.19
1.21
1.23
1.50
1.50
1.52
1.54
1.54
1.55
1.56
1.57
1.59
1.60
1.61
1.62
1.63
1.65
1.73
1.74
1.75
1.76
1.77
1.77
1.79
1.79
1.81
1.96
1.98
1.98
1.99
2.01
2.01
2.02
2.29
2.30
2.30
2.31
2.32
2.32
2.33
2.37
2.39
2.40
3.27
3.29
3.29
3.30
3.30
3.31
3.32
3.33
4.52
7.27
7.28
7.28
7.29
7.30
7.30
7.31
7.33
7.35
7.35
7.36
7.37
3.2
2
1.4
5
5.3
0
3.1
1
2.0
6
2.0
0
2.0
7
1.9
8
2.0
0
4.9
9
Current Data Parameters
NAME 09272013-18-doh-mc410-F
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130927
Time 19.23
INSTRUM spect
PROBHD 5 mm QNP 1H/13
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 Hz
FIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 512
DW 71.400 usec
DE 6.00 usec
TE 292.9 K
D1 1.00000000 sec
TD0 1
SFO1 499.9029994 MHz
NUC1 1H
P1 10.50 usec
PLW1 -1.00000000 W
F2 - Processing parameters
SI 65536
SF 499.9000045 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
17.10
18.32
20.73
23.96
27.28
33.16
33.39
33.56
39.66
39.87
40.08
73.23
74.38
74.69
75.01
75.89
76.98
77.23
77.48
87.86
87.91
87.97
113.32
115.16
117.00
127.75
127.81
128.57
138.72
178.17
Current Data Parameters
NAME 09282013-29-doh-mc410-F
EXPNO 10
PROCNO 1
F2 - Processing parameters
SI 262144
SF 125.6999303 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
-50 -60 -70 -80 -90 -100 -110 ppm
-81.91
-81.34
-81.08
-80.51
0.1
7
0.9
8
1.0
0
0.1
8
Current Data Parameters
NAME 09262013-31-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20130926
Time 14.18
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zgfhigqn.3.and
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37500.000 Hz
FIDRES 0.572205 Hz
AQ 0.8738133 sec
RG 128
DW 13.333 usec
DE 7.77 usec
TE 295.0 K
D1 1.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 470.5547296 MHz
NUC1 19F
P1 13.00 usec
PLW1 55.00000000 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 65536
SF 470.5923770 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
-80.5 -81.0 -81.5 ppm
-80.8 -81.0 -81.2 -81.4 -81.6 -81.8 -82.0 -82.2 -82.4 ppm
-82.52
-82.51
-82.50
-82.48
-82.47
-82.46
-82.44
-82.43
-82.42
-81.81
-81.80
-81.79
-81.77
-81.76
-81.75
-81.73
-81.72
-81.71
-81.68
-81.67
-81.65
-81.64
-81.63
-81.62
-81.60
-81.59
-81.58
-80.97
-80.96
-80.94
-80.93
-80.92
-80.90
-80.89
-80.88
-80.87
0.0
8
1.0
0
1.0
0
0.0
8
Current Data Parameters
NAME 10022013-38-michaelM
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131002
Time 16.01
INSTRUM AVII400
PROBHD 5 mm PABBO BB/
PULPROG zg30.baseopt
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 29761.904 Hz
FIDRES 0.454131 Hz
AQ 1.1010048 sec
RG 2050
DW 16.800 usec
DE 9.42 usec
TE 296.3 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 376.4682461 MHz
NUC1 19F
P1 13.20 usec
PLW1 15.53699970 W
F2 - Processing parameters
SI 65536
SF 376.4985513 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
9 8 7 6 5 4 3 2 1 ppm
0.93
0.94
1.12
1.12
1.13
1.14
1.15
1.15
1.16
1.16
1.17
1.17
1.19
1.20
1.21
1.22
1.36
1.37
1.37
1.40
1.41
1.43
1.43
1.44
1.45
1.45
1.46
1.47
1.48
1.50
1.50
1.53
1.54
1.55
1.56
1.57
1.58
1.59
1.60
1.62
1.62
1.64
1.64
1.64
1.65
1.66
1.68
1.69
1.76
1.77
1.78
1.79
1.80
1.81
1.82
1.83
1.84
1.84
1.85
2.35
2.36
2.38
3.45
3.46
3.47
3.48
3.50
3.51
3.52
3.53
7.27
3.0
4
1.0
3
12.8
6
4.2
5
2.0
9
2.0
0
Current Data Parameters
NAME 10042013-4-doh-mc410-F
EXPNO 12
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131004
Time 17.28
INSTRUM spect
PROBHD 5 mm QNP 1H/13
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 0 Hz
FIDRES 0 Hz
AQ 1.#INF000 sec
RG 256
DW 1.#IO usec
DE 6.00 usec
TE 292.6 K
D1 1.00000000 sec
TD0 1
SFO1 0 MHz
NUC1 1H
P1 10.50 usec
PLW1 -1.00000000 W
F2 - Processing parameters
SI 65536
SF 499.9000043 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
16.64
19.96
19.99
20.03
22.25
22.29
22.32
24.63
28.92
29.11
33.01
34.04
35.72
36.19
36.39
36.52
36.59
36.72
36.92
68.25
76.97
77.23
77.48
123.55
125.46
127.37
179.29
Current Data Parameters
NAME 10042013-4-doh-mc410-F
EXPNO 13
PROCNO 1
F2 - Processing parameters
SI 262144
SF 125.6999307 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
-50 -60 -70 -80 -90 -100 -110 ppm
-97.75
Current Data Parameters
NAME 10042013-4-doh-mc410-F
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131004
Time 17.23
INSTRUM spect
PROBHD 5 mm QNP 1H/13
PULPROG zgfhigqn
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37593.984 Hz
FIDRES 0.573639 Hz
AQ 0.8716288 sec
RG 1625.5
DW 13.300 usec
DE 6.00 usec
TE 292.8 K
D1 1.00000000 sec
d11 0.03000000 sec
d12 0.00002000 sec
TD0 1
SFO1 470.3383309 MHz
NUC1 19F
P1 12.15 usec
PLW1 -1.00000000 W
SFO2 0 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 -1.00000000 W
PLW12 -1.00000000 W
F2 - Processing parameters
SI 65536
SF 470.3759460 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
-97.2 -97.4 -97.6 -97.8 -98.0 -98.2 ppm
-97.82
-97.78
-97.75
-97.71
-97.68
Current Data Parameters
NAME 10042013-4-doh-mc410-F
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131004
Time 17.26
INSTRUM spect
PROBHD 5 mm QNP 1H/13
PULPROG zgflqn
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37593.984 Hz
FIDRES 0.573639 Hz
AQ 0.8716288 sec
RG 812.7
DW 13.300 usec
DE 6.00 usec
TE 292.5 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
NUC1 19F
P1 12.15 usec
PL1 -5.00 dB
SFO1 470.3383309 MHz
F2 - Processing parameters
SI 65536
SF 470.3759460 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
9 8 7 6 5 4 3 2 1 ppm
0.96
0.98
1.34
1.36
1.37
1.38
1.39
1.40
1.41
1.41
1.43
1.44
1.44
1.45
1.46
1.47
1.48
1.48
1.49
1.50
1.51
1.59
1.63
1.65
1.67
1.67
1.67
1.69
1.71
1.76
1.77
1.78
1.79
1.80
1.81
1.82
1.84
1.85
1.87
1.87
1.88
1.89
1.90
1.90
1.91
1.92
1.92
1.93
1.93
1.94
1.95
1.96
2.34
2.36
2.36
2.38
2.38
2.40
2.40
2.42
2.42
2.44
3.77
3.79
3.80
3.82
4.11
4.12
4.14
4.15
7.27
3.0
7
10.4
7
2.1
3
5.1
7
2.0
6
0.9
9
1.0
0
Current Data Parameters
NAME 10092013-58-michaelM
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131009
Time 17.49
INSTRUM AVII400
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 5597.015 Hz
FIDRES 0.085404 Hz
AQ 5.8545494 sec
RG 181
DW 89.333 usec
DE 6.50 usec
TE 296.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 400.1324008 MHz
NUC1 1H
P1 12.50 usec
PLW1 15.04800034 W
F2 - Processing parameters
SI 32768
SF 400.1300057 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
17.74
19.87
19.92
19.98
20.12
20.17
20.22
24.28
26.07
26.50
31.55
32.14
32.40
32.64
32.78
34.83
35.03
35.09
35.34
68.04
76.91
77.23
77.55
124.35
126.73
129.12
173.97
Current Data Parameters
NAME 10092013-58-michaelM
EXPNO 14
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131010
Time 3.02
INSTRUM AVII400
PROBHD 5 mm PABBO BB/
PULPROG udeftnoe.and
TD 8650
SOLVENT CDCl3
NS 2048
DS 4
SWH 24038.461 Hz
FIDRES 2.779013 Hz
AQ 0.1799200 sec
RG 203
DW 20.800 usec
DE 6.50 usec
TE 295.6 K
D1 2.00000000 sec
D6 0.03000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
D15 0.00302000 sec
D20 1.53362894 sec
D21 0.21294050 sec
D24 0.10000000 sec
L4 1
======== CHANNEL f1 ========
SFO1 100.6238364 MHz
NUC1 13C
P1 8.50 usec
P12 40000.00 usec
P26 500.00 usec
PLW1 55.73500061 W
SPNAM[2] Q3.1000
SPOAL2 0.500
SPOFFS2 0 Hz
SPW2 0.00043873 W
SPNAM[8] Crp60,0.5,20.1
SPOAL8 0.500
SPOFFS8 0 Hz
SPW8 6.15259981 W
======== CHANNEL f2 ========
SFO2 400.1316005 MHz
NUC2 1H
CPDPRG[2 waltz16
PCPD2 90.00 usec
PLW2 15.04800034 W
PLW13 0.21670000 W
F2 - Processing parameters
SI 32768
SF 100.6127487 MHz
WDW EM
SSB 0
LB 2.00 Hz
GB 0
PC 1.40
-50 -60 -70 -80 -90 -100 -110 ppm
-91.21
-90.69
-90.64
-90.12
0.0
5
0.9
9
1.0
0
0.0
5
Current Data Parameters
NAME 10092013-9-doh-mc410-F
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131009
Time 9.29
INSTRUM spect
PROBHD 5 mm QNP 1H/13
PULPROG zgfhigqn
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37593.984 Hz
FIDRES 0.573639 Hz
AQ 0.8716288 sec
RG 2048
DW 13.300 usec
DE 6.00 usec
TE 293.1 K
D1 1.00000000 sec
d11 0.03000000 sec
d12 0.00002000 sec
TD0 1
SFO1 470.3383309 MHz
NUC1 19F
P1 12.15 usec
PLW1 -1.00000000 W
SFO2 499.9019996 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 -1.00000000 W
PLW12 -1.00000000 W
F2 - Processing parameters
SI 65536
SF 470.3759460 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
-90.5 -91.0 ppm
-90.0 -90.2 -90.4 -90.6 -90.8 -91.0 -91.2 ppm
-91.27
-91.24
-91.24
-91.22
-91.21
-91.18
-91.17
-91.14
-90.76
-90.73
-90.72
-90.70
-90.69
-90.68
-90.66
-90.65
-90.64
-90.61
-90.57
-90.19
-90.15
-90.12
-90.09
-90.05
Current Data Parameters
NAME 10092013-2-doh-mc410-F
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20131009
Time 12.11
INSTRUM spect
PROBHD 5 mm QNP 1H/13
PULPROG zgflqn
TD 65536
SOLVENT CDCl3
NS 64
DS 4
SWH 37593.984 Hz
FIDRES 0.573639 Hz
AQ 0.8716288 sec
RG 812.7
DW 13.300 usec
DE 6.00 usec
TE 293.2 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
NUC1 19F
P1 12.15 usec
PL1 -5.00 dB
SFO1 470.3383309 MHz
F2 - Processing parameters
SI 65536
SF 470.3759460 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
9 8 7 6 5 4 3 2 1 ppm
1.75
1.77
1.77
1.78
1.78
1.80
1.80
1.81
1.81
2.12
2.12
2.13
2.15
2.16
2.16
2.92
2.93
2.94
2.94
2.95
2.96
4.01
4.01
4.03
4.03
4.04
4.04
4.40
4.40
4.42
4.42
4.43
4.44
4.98
5.00
5.03
5.03
5.04
5.06
5.07
5.07
5.77
5.77
5.78
5.78
5.79
5.79
5.80
5.80
5.82
5.82
5.82
5.83
5.83
5.84
5.84
5.85
5.85
7.27
2.0
6
2.0
6
2.0
5
2.0
8
2.0
7
2.0
4
1.0
0
Current Data Parameters
NAME 04232014-14-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20140423
Time 20.47
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 HzFIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 128
DW 71.400 usec
DE 11.40 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 500.1330008 MHz
NUC1 1H
P1 10.35 usec
PLW1 24.00000000 W
F2 - Processing parameters
SI 65536SF 500.1300073 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
23.57
33.20
34.63
42.72
62.23
76.97
77.23
77.48
115.52
138.01
153.74
173.55
Current Data ParametersNAME 04232014-14-doh-mc410-AEXPNO 11PROCNO 1
F2 - Acquisition ParametersDate_ 20140423Time 21.41INSTRUM spectPROBHD 5 mm PABBO BB/PULPROG udeftTD 21424SOLVENT CDCl3
NS 800DS 0SWH 29761.904 HzFIDRES 1.389185 HzAQ 0.3599232 secRG 128DW 16.800 usecDE 7.96 usecTE 295.0 KD1 3.00000000 secD11 0.03000000 secD12 0.00002000 sec
D20 200.00000000 secTD0 1
======== CHANNEL f1 ========SFO1 125.7716224 MHzNUC1 13CP1 8.90 usecP13 2000.00 usecP26 500.00 usecPLW1 125.00000000 WSPNAM[5] Crp60comp.4SPOAL5 0.500
SPOFFS5 0 HzSPW5 15.12800026 WSPNAM[8] Crp60,0.5,20.1SPOAL8 0.500SPOFFS8 0 HzSPW8 15.12800026 W
======== CHANNEL f2 ========SFO2 500.1320005 MHzNUC2 1HCPDPRG[2 waltz65PCPD2 80.00 usecPLW2 24.00000000 WPLW12 0.39015001 W
F2 - Processing parametersSI 262144SF 125.7577642 MHzWDW EMSSB 0LB 2.00 HzGB 0PC 1.40
9 8 7 6 5 4 3 2 1 ppm
1.18
1.19
1.49
1.50
1.50
1.51
1.52
1.53
1.53
1.61
1.84
1.85
1.86
1.86
1.87
1.87
1.89
2.06
2.06
2.07
2.07
2.07
2.08
2.08
2.08
2.08
2.09
2.09
2.09
2.10
2.10
2.11
3.74
3.75
3.76
3.78
4.00
4.01
4.02
4.02
4.02
4.04
4.39
4.40
4.41
4.41
4.42
4.42
4.94
4.94
4.95
4.95
4.95
4.96
4.96
4.97
4.97
4.97
4.99
4.99
5.00
5.00
5.02
5.03
5.03
5.03
5.76
5.78
5.80
5.82
7.27
3.1
4
1.0
3
1.0
3
2.0
5
1.0
0
2.1
2
2.1
1
2.0
2
1.0
0
Current Data Parameters
NAME 04232014-15-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20140423
Time 21.45
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 HzFIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 90.5
DW 71.400 usec
DE 11.40 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 500.1330008 MHz
NUC1 1H
P1 10.35 usec
PLW1 24.00000000 W
F2 - Processing parameters
SI 65536SF 500.1300072 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
17.26
31.58
32.83
37.07
42.99
62.04
76.98
77.23
77.48
115.09
138.25
153.35
177.46
Current Data ParametersNAME 04232014-15-doh-mc410-AEXPNO 11PROCNO 1
F2 - Acquisition ParametersDate_ 20140423Time 22.39INSTRUM spectPROBHD 5 mm PABBO BB/PULPROG udeftTD 21424SOLVENT CDCl3
NS 800DS 0SWH 29761.904 HzFIDRES 1.389185 HzAQ 0.3599232 secRG 128DW 16.800 usecDE 7.96 usecTE 295.0 KD1 3.00000000 secD11 0.03000000 secD12 0.00002000 sec
D20 200.00000000 secTD0 1
======== CHANNEL f1 ========SFO1 125.7716224 MHzNUC1 13CP1 8.90 usecP13 2000.00 usecP26 500.00 usecPLW1 125.00000000 WSPNAM[5] Crp60comp.4SPOAL5 0.500
SPOFFS5 0 HzSPW5 15.12800026 WSPNAM[8] Crp60,0.5,20.1SPOAL8 0.500SPOFFS8 0 HzSPW8 15.12800026 W
======== CHANNEL f2 ========SFO2 500.1320005 MHzNUC2 1HCPDPRG[2 waltz65PCPD2 80.00 usecPLW2 24.00000000 WPLW12 0.39015001 W
F2 - Processing parametersSI 262144SF 125.7577655 MHzWDW EMSSB 0LB 2.00 HzGB 0PC 1.40
9 8 7 6 5 4 3 2 1 ppm
0.93
0.94
0.94
0.95
1.24
1.26
1.26
1.26
1.27
1.27
1.28
1.28
1.29
1.45
1.46
1.46
1.47
1.48
1.55
1.87
1.88
1.90
1.91
2.03
2.04
2.04
2.06
2.10
2.11
3.56
3.56
4.09
4.10
4.11
4.12
4.16
4.17
4.18
4.20
4.23
4.24
4.25
4.27
4.95
4.95
4.95
4.97
4.97
4.97
4.98
4.98
4.99
4.99
5.01
5.02
5.02
5.02
5.74
5.75
5.75
5.77
7.27
7.40
7.41
7.41
7.42
7.42
7.43
7.52
7.53
7.53
3.1
9
1.4
8
1.0
9
1.0
5
2.2
3
3.1
6
0.5
5
0.5
5
0.5
3
0.5
3
2.0
5
1.0
0
3.2
1
2.1
1
Current Data Parameters
NAME 04042014-17-doh-mc410-A
EXPNO 10
PROCNO 1
F2 - Acquisition Parameters
Date_ 20140404
Time 10.58
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zg30
TD 65536
SOLVENT CDCl3
NS 8
DS 2
SWH 7002.801 HzFIDRES 0.106854 Hz
AQ 4.6792703 sec
RG 128
DW 71.400 usec
DE 11.40 usec
TE 295.0 K
D1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 500.1330008 MHz
NUC1 1H
P1 10.35 usec
PLW1 24.00000000 W
F2 - Processing parameters
SI 65536SF 500.1300074 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
16.79
16.82
31.05
32.03
32.05
32.33
32.38
55.64
71.19
71.23
76.98
77.23
77.48
115.02
120.12
122.40
124.70
126.99
127.55
128.62
129.81
132.54
138.45
166.88
Current Data ParametersNAME 04222014-4-doh-mc410-AEXPNO 10PROCNO 1
F2 - Acquisition ParametersDate_ 20140423Time 0.56INSTRUM spectPROBHD 5 mm PABBO BB/PULPROG udeftTD 21424SOLVENT CDCl3
NS 800DS 0SWH 29761.904 HzFIDRES 1.389185 HzAQ 0.3599232 secRG 128DW 16.800 usecDE 7.96 usecTE 295.0 KD1 3.00000000 secD11 0.03000000 secD12 0.00002000 sec
D20 200.00000000 secTD0 1
======== CHANNEL f1 ========SFO1 125.7716224 MHzNUC1 13CP1 8.90 usecP13 2000.00 usecP26 500.00 usecPLW1 125.00000000 WSPNAM[5] Crp60comp.4SPOAL5 0.500
SPOFFS5 0 HzSPW5 15.12800026 WSPNAM[8] Crp60,0.5,20.1SPOAL8 0.500SPOFFS8 0 HzSPW8 15.12800026 W
======== CHANNEL f2 ========SFO2 500.1320005 MHzNUC2 1HCPDPRG[2 waltz65PCPD2 80.00 usecPLW2 24.00000000 WPLW12 0.39015001 W
F2 - Processing parametersSI 262144SF 125.7577638 MHzWDW EMSSB 0LB 2.00 HzGB 0PC 1.40
-71.45 -71.50 -71.55 -71.60 -71.65 ppm
-71.56
-71.54
1.0
3
1.0
0
Current Data Parameters
NAME 04042014-17-doh-mc410-A
EXPNO 11
PROCNO 1
F2 - Acquisition Parameters
Date_ 20140404
Time 11.01
INSTRUM spect
PROBHD 5 mm PABBO BB/
PULPROG zgfhigqn.3.and
TD 131072
SOLVENT CDCl3
NS 64
DS 4
SWH 125000.000 HzFIDRES 0.953674 Hz
AQ 0.5242880 sec
RG 128
DW 4.000 usec
DE 6.95 usec
TE 295.0 K
D1 1.00000000 sec
D11 0.03000000 sec
D12 0.00002000 sec
TD0 1
======== CHANNEL f1 ========
SFO1 470.5359059 MHz
NUC1 19F
P1 13.00 usec
PLW1 55.00000000 W
======== CHANNEL f2 ========
SFO2 500.1320005 MHz
NUC2 1H
CPDPRG[2 waltz65
PCPD2 80.00 usec
PLW2 24.00000000 W
PLW12 0.39015001 W
F2 - Processing parameters
SI 65536
SF 470.5923770 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
9 8 7 6 5 4 3 2 1 ppm
0.94
0.95
1.22
1.24
1.25
1.25
1.26
1.27
1.28
1.28
1.29
1.43
1.44
1.45
1.47
1.56
1.88
1.90
2.01
2.03
2.03
2.05
2.05
2.06
2.08
2.08
2.10
2.10
2.21
2.26
3.56
3.56
4.14
4.15
4.16
4.18
4.18
4.20
4.21
4.22
4.94
4.94
4.94
4.95
4.96
4.96
4.97
4.98
4.98
4.98
5.01
5.02
5.02
5.03
5.72
5.74
5.76
5.78
7.27
7.40
7.40
7.40
7.41
7.41
7.42
7.42
7.43
7.52
7.53
7.54
7.54
3.2
3
1.5
4
1.1
1
1.0
4
2.2
3
3.0
6
2.0
9
2.0
3
1.0
0
3.1
7
2.1
4
Current Data ParametersNAME 04112014-8-doh-mc410-NEXPNO 10PROCNO 1
F2 - Acquisition ParametersDate_ 20140411Time 21.40INSTRUM AV400PROBHD 5 mm PABBO BB-PULPROG zg30TD 65536
SOLVENT CDCl3NS 8DS 2SWH 5592.841 HzFIDRES 0.085340 HzAQ 5.8589182 secRG 228.1DW 89.400 usecDE 6.50 usecTE 296.7 KD1 1.00000000 sec
TD0 1
======== CHANNEL f1 ========NUC1 1HP1 12.00 usecPL1 -3.00 dBPL1W 19.24057770 WSFO1 400.3024018 MHz
F2 - Processing parametersSI 65536SF 400.3000055 MHz
WDW EMSSB 0LB 0.30 HzGB 0PC 1.00
190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 ppm
16.82
31.06
32.05
32.33
55.64
71.19
76.98
77.23
77.48
115.01
120.12
122.40
124.70
127.00
127.55
128.62
129.81
132.54
138.45
166.88
Current Data ParametersNAME 04222014-5-doh-mc410-AEXPNO 10PROCNO 1
F2 - Acquisition ParametersDate_ 20140423Time 1.52INSTRUM spectPROBHD 5 mm PABBO BB/PULPROG udeftTD 21424SOLVENT CDCl3
NS 800DS 0SWH 29761.904 HzFIDRES 1.389185 HzAQ 0.3599232 secRG 128DW 16.800 usecDE 7.96 usecTE 295.0 KD1 3.00000000 secD11 0.03000000 secD12 0.00002000 sec
D20 200.00000000 secTD0 1
======== CHANNEL f1 ========SFO1 125.7716224 MHzNUC1 13CP1 8.90 usecP13 2000.00 usecP26 500.00 usecPLW1 125.00000000 WSPNAM[5] Crp60comp.4SPOAL5 0.500
SPOFFS5 0 HzSPW5 15.12800026 WSPNAM[8] Crp60,0.5,20.1SPOAL8 0.500SPOFFS8 0 HzSPW8 15.12800026 W
======== CHANNEL f2 ========SFO2 500.1320005 MHzNUC2 1HCPDPRG[2 waltz65PCPD2 80.00 usecPLW2 24.00000000 WPLW12 0.39015001 W
F2 - Processing parametersSI 262144SF 125.7577638 MHzWDW EMSSB 0LB 2.00 HzGB 0PC 1.40
-71.45 -71.50 -71.55 -71.60 -71.65 ppm
-71.56
-71.54
Current Data Parameters
NAME 04112014-8-doh-mc410-NEXPNO 12PROCNO 1
F2 - Processing parametersSI 65536SF 376.6583260 MHzWDW EMSSB 0LB 0.30 HzGB 0
PC 1.00
