6 Stainless Steel Wiped-Film Evaporation Plant2019/06/06  · 6” Stainless Steel Wiped-Film...

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6Stainless Steel Wiped-Film Evaporation Plant BW-WFE-6-SS

Transcript of 6 Stainless Steel Wiped-Film Evaporation Plant2019/06/06  · 6” Stainless Steel Wiped-Film...

Page 1: 6 Stainless Steel Wiped-Film Evaporation Plant2019/06/06  · 6” Stainless Steel Wiped-Film Evaporator Throughput capability • Up to 7.0 L/hr • Average 3.0-5.0 L/hr True Continuous

6” Stainless Steel Wiped-Film Evaporation Plant

BW-WFE-6-SS

Page 2: 6 Stainless Steel Wiped-Film Evaporation Plant2019/06/06  · 6” Stainless Steel Wiped-Film Evaporator Throughput capability • Up to 7.0 L/hr • Average 3.0-5.0 L/hr True Continuous

6” Stainless Steel Wiped-Film Evaporator

• Delivers greater consistency, purity, and confidence in every cannabis oil distillation.

• Continuous flow leaves behind less advanced and efficient methods with a dependable input up to 7 liters per hour.

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Page 3: 6 Stainless Steel Wiped-Film Evaporation Plant2019/06/06  · 6” Stainless Steel Wiped-Film Evaporator Throughput capability • Up to 7.0 L/hr • Average 3.0-5.0 L/hr True Continuous

6” Stainless Steel Wiped-Film Evaporator

Throughput capability• Up to 7.0 L/hr• Average 3.0-5.0 L/hr

True Continuous Feed • Peristaltic Inlet pump allows addition of oil while machine is still under vacuum• Outlet pumps allow dispensing of products directly into vessel of choice• Feed rates adjustable from 10mL to 10L/hr

Jacketed body• Thermal fluid circulating through jacketed body for consistent temperature

Precise temperature control• PID temperature controllers on body and all heated lines for creation of precise SOPs

Expert On-Site Training and Installation • Validation with YOUR oil on the day of install• Consultation on how to generate the best SOP for your lab• Sample SOP provided for internal use

Potency up to 99.8% total cannabinoid content

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Specifications

Feed

• 5L or 20L stainless steel feed flask with vacuum inlet line• Peristaltic dosing pump for precise, vacuum-held dosing• Feed line to evaporator is jacketed and PID controlled

Short-Path Evaporator • Max evaporator temperature: 200 °C • 316 Stainless Steel• 316 Stainless Steel Internal condenser (cold finger)• 6 rollers• Easy to adjust drive system speed

Distillate & Residue Discharge Pumps (2 pumps)

• Gear pump in PID controlled heated design (design temperature 100°C), digitally displayed pump speed. Calibration and secret menu options for optimal SOP development

• Check valves used as a pressure lock against the atmosphere

Vacuum System • 21 to 36 CFM Rotary Vane Vacuum pump equipped with

vacuum pump oil• Diffusion vacuum pump for achieving stable vacuum

conditions at low pressures (oil included)• Flanged cold trap & collection vessel for cold trap

Heating & Cooling by Beaker & Wrench/ Polyscience

• 1 independent heating unit for the evaporator (oil circulator)• 1 independent heating unit (silicone pad) for the residue &

distillate line• 1 independent heating unit for the feed tank (silicone pad)• 1 independent cooling unit for the cold trap (immersion

probe)• 1 independent chilling unit for the internal condenser (water

circulator)

Rack/Frame

• Frame constructed of 80/20 aluminium extrusion and equipped with 4 wheels Power supply & power distribution system 1. Voltage: 120V or 220V

• Frequency: 60 Hz 3. Number of Phases: 1 (two hot wires) • Power distribution panel• Control panel for pumps. Included spare parts.• 1 set of rollers• 1 set of static gaskets • 1 set of shaft sealing for rotary transmission • 1 set of bearings for rotary transmission • 1 set of O-rings

Documentation• Operating instructions

Component Certifications See Below• Heaters & Chillers CE/ISO9001 • Vacuum Pumps • Gear Pumps • Wiper Drive • Power Box • Frequency Box • Pressure Gauge

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Page 5: 6 Stainless Steel Wiped-Film Evaporation Plant2019/06/06  · 6” Stainless Steel Wiped-Film Evaporator Throughput capability • Up to 7.0 L/hr • Average 3.0-5.0 L/hr True Continuous

Vacuum Pump Motor (part 1)

Max. Ambient Temperature 40 Degrees CNominal Efficiency 82.4%Nameplate RPM 1725HP 2Overall Length 13-13/16"Phase 1Voltage Compatibility 115, 120, 208, 230, 240, 115/208-230, 115/230, 120/240, 208-230, 208-240Full Load Amps 18.8/10.2-9.4Motor Enclosure Design Totally Enclosed Fan-CooledMotor Design Capacitor-Start/RunNo. of Speeds 1Motor Bearings BallMotor Application General ApplicationIns. Class BFrame 56cMotor Service Factor 1.00Shaft Dia. 5/8”Manufacturers Warranty Length 1 yr.Duty ContinuousHz 60Motor Shaft Rotation CW/CCWVoltage 115/208-230Standards UL (E47479), CSA (258501)RPM Range 1701-1800RPM Group 1701-1800Footnotes 24,51Frame Material SteelMotor Mounting Type FaceLength Less Shaft 11-13/16”Motor Shaft Design Keyed

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Page 6: 6 Stainless Steel Wiped-Film Evaporation Plant2019/06/06  · 6” Stainless Steel Wiped-Film Evaporator Throughput capability • Up to 7.0 L/hr • Average 3.0-5.0 L/hr True Continuous

Vacuum Pump Motor (part 2)

Motor Efficiency Group Energy EfficientShaft Length 1-7/8”Item General Purpose MotorMotor Thermal Protection None

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Page 7: 6 Stainless Steel Wiped-Film Evaporation Plant2019/06/06  · 6” Stainless Steel Wiped-Film Evaporator Throughput capability • Up to 7.0 L/hr • Average 3.0-5.0 L/hr True Continuous

Gear, Peristaltic, Wiper Drive Power Supply

Power Supply Type SwitchingOutput Configuration Single outputOutput Voltage Range 24 VDC (adjustable)Amperage Rating: 10AOutput Power 240WNominal Input Voltage 120/240 VAC or 120-375 VDC Input Voltage Range 85-264 VAC / 120-375 VDC

UL Listed File #: E197592UL Recognized File #: E198298UL Hazardous File #: None

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Page 8: 6 Stainless Steel Wiped-Film Evaporation Plant2019/06/06  · 6” Stainless Steel Wiped-Film Evaporator Throughput capability • Up to 7.0 L/hr • Average 3.0-5.0 L/hr True Continuous

Circulating Heaters

Model H5W/O H15W/O H25W/O H60W/OTiming Continuous operation or timing functionTemperature Range Room: +5 ~ 99(W)/200(O) °C Temperature Control Digital PID +/-0.1 °C, Touch Screen 7 inchPump Speed 0~20 (+/-10%) L/min, adjustableDrain Valve/Port W: Yes, O: NoTank Volume 5.0 L 15.0 L 25.0 L 60.0 LBath Opening 13x13 cm 24x16 cm 24x16 cm 30x28 cmTank Size (cm) 26x14x14 30x24x20 30x25x28 40x40x38 Heating Watts (W) 750W 1000W 1600W 5000WHeating Watts (O) 1000 W 1650 W 2400 W 8000WMax. Pressure 2.5 barProduct Size (cm) 40x35x45 42x45x51 42x45x58 60x60x75Product Weight 25/30 lbs 28/45 lbs 45/55 lbs 100/125 lbs

Tank Size (cm) 26x14x14 30x24x20 30x25x28 40x40x38Heating Watts (W) 750W 1000W 1600W 5000W Heating Watts (O) 1000 W 1650 W 2400 W 8000WAC Voltage & Amp (W/O) 110V 6.5/9.5A 220V 3.5/4.8A Max. Pressure 2.5 barProduct Size (cm) 40x35x45 42x45x51 42x45x58 60x60x75Product Weight 25/30 lbs 28/45 lbs 45/55 lbs 100/125 lbs

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Page 9: 6 Stainless Steel Wiped-Film Evaporation Plant2019/06/06  · 6” Stainless Steel Wiped-Film Evaporator Throughput capability • Up to 7.0 L/hr • Average 3.0-5.0 L/hr True Continuous

Vacuum Gauge

Measurement Method Convection Enhanced PiraniMeasurement Range 1 x 10-4 to 1,000 Torr (1.3 x 10-4 to 1,333 mbar)Communications Interface RS-485/RS-232Temperature (Operating) 0-40° CTemperature (Storage) -40-70° CTemperature (Bakeout) 150° C (gauge only -- electronics removed)Display 4-digit OLED (user-selectable Torr, mbar, or Pa)Materials Exposed to Vacuum Gold-plated tungsten, 304 & 316 stainless steel, glass, nickel, PFPEAccuracy (Typical) 1.0x10-4 to 1.0x10-3 Torr; 0.1 mTorr resolution 1.0x10-3 to 400 Torr; ± 10% of reading 400 to 1,000 Torr; ± 2.5% of readingRepeatability (Typical) ± 2% of readingSet-Point Relays Two SPDT RelaysRelay Response 1A at 30 VDC resistive, or AC non-inductiveMounting/Installation Horizontal recommendedOrientation (Orientation has no effect below 1 Torr)Analog Outputs a) non-linear S-curve 0.375–5.659 VDC b) log-linear 1–8 VDC 1) V/decade 2) linear 0–10 VDC, user scalableInternal Volume 26 cm3 (1.589 in3)

Input Power 12-28 VDC, 2 W, protected against power reversal and transient over-voltages

Connections 9-pin sub-D (male) 15-pin high-density sub-D (male)Compliance & Standards CE compliant, RoHS compliant

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-80C Immersion Probe

Working Temperature Range °F -112° to -40°Working Temperature Range °C -80° to -40°Temperature Control (°F) Fixed at -112°Temperature Control (°C) Fixed at -80°CCleanable Air Filter YesDisplay TemperatureMaximum Ambient Temperature °F 86°Maximum Ambient Temperature °C 30°Overall Dimensions (L x W x H) (inches) 20.1 x 15 x 22.3 inOverall Dimensions (L x W x H) (cm) 51.1 x 38.1 x 56.6 cmRefrigerant R404A & R508BImmersion Probe Type Rigid CoilProbe Diameter (inches) 1.75Probe Diameter (cm) 4.44Probe Length (inches) Probe Length (inches)Probe Length (cm) Coil: 17.8 / Exposed: 41.9Flexible Hose Diameter (inches) 2.83Flexible Hose Diameter (cm) 7.14Flexible Hose Length (feet) 6Flexible Hose Length (m) 1.83Shipping Weight (pounds) 162.0Shipping Weight (kilograms) 73.5Catalog Page Number 114-115

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Wiper Drive Motor

Motor Frame Size NEMA 34 - 3.42 in (86.87 mm) sq.Length 4.63 in (117.60 mm)Input (bus) Voltage Range 24-75 VDC (90 VDC max)Peak Torque (@75 VDC) 605 oz-in (4.3 N-m)Cont. (RMS) Torque (@75 VDC) 141 oz-in (1.0 N-m)Max Speed (@75 VDC) 4150 RPMAchievable Resolution 0.450 degreesRepeatability 0.03 degreesShaft Diameter 0.50 in (12.70 mm)Weight 5.8 lb (2.6 kg)Rotor Inertia 11.4 oz-in² (2.1 kg-cm²)Logic Input Voltage Range 4.0 to 28 VDCMaximum Radial Load 50 lbf (222.4 N)Maximum Thrust Load 10.0 lbf (44.5 N) Environmental Rating Dust & water splash resistantAmbient Temperature 0-70 deg C (derated >40C)Ambient Humidity 0-95%; non-condensingRegulatory Certifications UL recognized; CE; RoHSCountry of Origin USA

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Wiper Drive (part 1)

Current at 5V 7.5mA (min.)Input Current at 28V 12.0mA (min.)HLFB Absolute Maximum Voltage 30VDC (across output terminals)HLFB Output Current, Maximum 9mA (non-inductive load)HLFB Output voltage drop @ 2mA 0.30VDC (+/- 100mV)HLFB Output voltage drop @ 5mA 0.55VDC (+/- 100mV)Motor Bearing, NEMA34:Maximum Radial Load, NEMA34 220N (50-lbs), applied 25mm (1.0in) from front bearingMaximum Thrust Load, NEMA34 44N (10-lbs)Bearing Life, NEMA34 revs (typ., load dependent.) 2.4 x109 to 5.3 x109

Motor Bearing, NEMA23:Maximum Radial Load, NEMA23 110N (25 lbs), applied 25mm (1.0in) from front bearingMaximum Thrust Load, NEMA23 22N (5 lbs)Bearing Life, NEMA23 3.2 x109 to 5.0 x109 revs (typ., load dependent.)Environmental:Shock (peak, maximum) 10G (applied no more than twice)Vibration (RMS, 2 Hz-200 Hz) 1.0G or 0.5mm, whichever is lessMaximum External Shaft Deceleration 250,000 rad/s2Maximum Ambient Operating Temp. For seasonal/intermittent duty 70°C/158°F (RMS torque output de-rated)For continuous long-term use 55°C/122°F (RMS torque output de-rated)For full-rated output speed/torque 40°C/104°FMaximum Body Temp. 100°CMaximum Rear Cover Temp. 70°CStorage Temperature -20°C to 85°CHumidity 0% to 95%, Non-CondensingRecommended Optional Fan, NEMA23 40mm square, 45.25 mm bolt center, >7CFM

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Page 13: 6 Stainless Steel Wiped-Film Evaporation Plant2019/06/06  · 6” Stainless Steel Wiped-Film Evaporator Throughput capability • Up to 7.0 L/hr • Average 3.0-5.0 L/hr True Continuous

Wiper Drive (part 2)

Recommended Optional Fan, NEMA34 60mm square, 70.71 mm bolt center, >14CFMEnvironmental Sealing Front Face, with shaft seal option IP65Front Face, without shaft seal option IP53Body/rear, with dielectric sealing grease in connectors IP55Body/rear, no sealing provisions IP53ComplianceRegulatory Certifications UL recognized, CE, RoHSElectrical Safety UL508C, EN 61010-1EMI EN 61326-1Country of Origin USA

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Page 14: 6 Stainless Steel Wiped-Film Evaporation Plant2019/06/06  · 6” Stainless Steel Wiped-Film Evaporator Throughput capability • Up to 7.0 L/hr • Average 3.0-5.0 L/hr True Continuous

Varian M-2 Water-Cooled Diffusion Pump

Operating Specifications:Optimum Operating Range 2 x 10^-3 torr to less than 3 x 10^-9 torrMaximum Pumping Speed 285 liters/second for airMaximum Forepressure no load: 5.5 x 10^-1 full load: 4.0 x 10^-1Maximum Throughput 0.5 torr liter/secondBackstreaming Rate at Pump Inlet 0.0009 mg/cm^2/min (with cold cap)Aprox. Power Required 450 wattsHeat-up Time 15 minCool-down Time less than 5 min to “break jet” less than 10 min to vent pumpFluid Charge 100cc. For all conventional/high performance pump fluidsCooling Water Requirements 0.1 gpm at 60 deg F to 80 deg F inlet tempFluid Charge 100cc. For all conventional/high performance pump fluidsBacking Pump Size Recommended 5 cfm or larger for optimum throughout

Physical Specifications:Inlet Flange ConnectionOD 6 inchesID 3 11/32 inchesThickness 1/2 inchBolt Circle 4 3/4 diameterNo. of HolesSize of Holes 3/4 diameterOrientation Straddle GLGasket Groove 3 15/32 ID x 13/64 wideGasket O-ring Parket #2-238 Butyl

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Page 15: 6 Stainless Steel Wiped-Film Evaporation Plant2019/06/06  · 6” Stainless Steel Wiped-Film Evaporator Throughput capability • Up to 7.0 L/hr • Average 3.0-5.0 L/hr True Continuous

Diffusion Pump

Foreline ConnectionTubing 0.840 OD*Height 12 11/16 inch - allow additional 3 1/2” for heater removalJet Assembly self-aligning, fractionating design with 3 diffusion stages and one ejector stageForeline Baffle Stacked half moons with snap ring retainerCold Cap Conduction cooledWater Connections 1/8 FPT body and quick cool

Materials of ConstructionBody Stainless SteelFlange Mild SteelJet Assembly Stainless SteelForeline Baffle Stainless SteelCooling Coils Copper, welded to bodyHeater Reflector Polished AluminiumCold Cap Copper, Nickel Plated

Heater: Cartridge TypeSTD Voltage (nom.) 115V 1ΦOption (Nom.) 240V 1ΦPower 450 Watts (approx.)Connector Plug-in, 115V, mates with Hubbell #5269 ( 240V mates with Hubbel #5669)Exterior Finish GreenActual Weight 10 lbsShipping Weight 20 lbs0181-6473-02-150 Heater, 450W, 120V

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