5 Underwood Court, Delran, NJ 08075 609-461-4003 EPA ... · 5 underwood court, delran, nj 08075...

5 Underwood Court, Delran, NJ 08075 609-461-4003

TECHNICAL ASSISTANCE TEAM FOR EMERGENCY RESPONSE REMOVAL AND PREVENTIONEPA CONTRACT 68-WO-0036

' ','• ?' ••"--'•* • _"..•. ...MEMORANDUM

TO: Jamie Fenske, OSC, EPA Region III TDD #9106-38AWestern Response Section . - PCS #1724

THRU: Mike Zickler, TATL, Region III *, .., l t . ' - . . . -

FROM: Marian Murphy, TAT Regiqn IIIW*-

SUBJECT: laeger Site Transformer Samples Analytical Review

DATE: -August-'14, 1991 / : s

This report covers the review of the analytical data package fortwenty-three (23) transformer oil samples. The samples werecollected from the laeger Site on August 5, 1991. The samples weredelivered to Technical Testing Laboratories, Inc* on August 6,1991. -The analysis requested was PCBs.

ANALYTICAL METHODOLOGY -';V

The samples were analyzed in accordance with EPA Method 8080.

• Signed chain-of-custody^records were received*

•" The samples were analyzed within holding times.

• The calibration curve was acceptable. The method blankwas free of contamination. The surrogate spikerecoveries were acceptable. The matrix spike/matrixspike duplicate recoveries were low (56% and 58%) butwithin acceptable range. The relative percent difference(RPD) values were also acceptable. -;A / -

CONCLUSION

Accept the data as presented.

MM/inr

Roy F. Weston, Inc :: r f: : ( - .- t **/**/MAJOR PROGRAMS DIVISION ' t ftO(\U6 ** '00trfg ,L _ .In Association with Foster Wheeler Envircsponse, Inc jROoy U fifcahons, Inc CC Johnson & Malhotra, F.C.,R.E. Sarriera Assodates, and GRB Environmental ServiBesylnc.

... ROY F. WESTON, INC.

IAEGER SITE-PROJECT 1742

TTL# N4542 through N4565

Please find enclosed with this package tha results and the QA/QC fortha following samples:

TTL/ Station i station LocationN4 5 4 2 ' l TransformerN4543 3 TransformerN4544 4 TransformerN4546 5 TransformerN4547 9 TransformerN4 5 4 8 10 . TransformerN4 54 9 12 TransformerN4550 - 14 ' •• - TransformerN4551 15 TransformerN4552 17 - TransformerN4553 18 TransformerN4554 .19 TransformerN4555 * 20 TransformerN4556 21 TransformerN4557 22 TransformerN4 5 5 8 . 23 TransformerN4559 ' . - 24 ' ' TransformerN4560 25 TransformerN4561 •: 26 . Transformer'N4562 27 TransformerN4563 23, TransformerN4S64 30 TransformerN4565 31 Transformer

If you^hav* any questions concerning this packaga, plaasa feel freeto call us at 304-346-0725. Wa at Technical Tasting Laboratoriesappreciate your business. -'

• • ' \ " • • . . _;--'.)-•: TECHNICAL TEfiTINQ LABORATORIES

ST TECHNICAL TESTING LABORATORIES.. . * DIVISION OF COMMERCIAL TISTINO 4 INGlNEERINO CO.

LABORATORY ANALYSIS REPORT

ftoy F. Ueston-Delran, NJ/Murphy, Marian Laboratory Number N4542 Respectfullyr- / f . <•:-.' ':'-.,. ' • / • - - :' •'•- " " SubmittediSTA. Kl \ TRANSFORMER , : Date Sampled 88/85/91 18:88 _> vW * } 'IAEGER PCB SITE 111784 Date Received 88/86/91

Sampled bv CLIENT 88129ri924

, ANALYSIS FOR REQUESTED PARAMETERSALL RESULTS ARE ON AN AS RECEIVED BASIS

ANALYZED.PARAMETER . - -- RESULT HDL UNITS METHOD - DATE/TIME/ANALYST

PCB(as Aroclor 1868) C11896-82-S3 198 1.8 ug/G SU8888 88/89/91 8Si44 ftLMSURROGATE RECOVERY-PESTICIDE FRACTION , .„ . •Tetrachloro-met«-Xylene<SURR06ATE> 75 -———— % REC SU8888 88/89/91 85i44 .ALHDecachldrobiphenyl-SURR 77 ———— % REC SU8888 88/89/91 85i44 ALH

Extraction Datt — 88/07/91 18188 DT

Method Rftftrtncti USEPAs "Methods for Evaluating Solid Wa«tt"iSU-846<8nd Ed.)

Method Rtferencei OIL-PCB in oil aethodt EPA-688/4-61-845

1256 GREENBRIER STREET. CHARLESTON, WEST VIRGINIA 25311 — TELEPHONE 304 346-0725 v-4 43 BENSON AVENUE. BALTIMORE. MARYLAND 21227 - { Fl0®fi fr ft247"7400 !

4440 GLEN ESTE — WITHAMSVILLE RD.. SUITE 800, CINCINNATI. OHIO 45245 — TELEPHONE 513 752-9696

yS(- -•• TECHNICAL TESTING LABORATORIESW. ~ ~ A DIVISION OP COMMERCIAL TESTING A ENGINEERING CO.

LABORATORY ANALYSIS REPORT ±j

Roy F. Ueston-Delran, NJ/Murphy, Marian Laboratory Number N4S43

3TA. t»3 TRANSFORMER Date Sanpled 08/05/91 1<IAEGER PCB SITE H1784 Date Received 08/06/91

Sampled by CLIENT

PARAMETER

ANALYSISALL RESULTS

PCB (A* Aroelor I860) C 11096-62-33SURROGATE RECOVERY-PESTICIDE FRACTIONTetrachloro-meta-Xylene<SURROGATE>

FOR REQUESTED PARAMETERSARE ON AN AS RECEIVED BASIS

RESULT MDL UNITS METHOD

2.5 1.9 ug/G SU80S0

RespectfullySufanittedt

081291 1934

ANALYZEDDATE/TIME/flNALYST

08/09/91 06101 AL«

08/09/91 06101 ALM

Extraction Date -- 38/87/91 12108 JB

Method Reference! USEPAs"Methods for Evaluatin| Solid, Waste"iS«-846(8nd Ed.)

Method Reference! OIL-PCB in oil methodi EPA-600/4-81-845 •

1250 GREENBRIER STREET, CHARLESTON.,WESTVIRGINIA 25311 — TELEPHON6 304 34*07254643 BENSON AVENUE, BALTIMOR6, MARYLAChaiM-rElPHONE 301 247-7400 '

4440 GLEN ESTE - WITHAMSVILLE RO., SUfTE 900, CINCl NATl.'CHlt) «5245 - TELEPHONE 513 752-9696

TECHNICAL TESTING LABORATORIESA DIVISION Of COMMERCIAL TISDNQ a ENGINEERING CO.


Roy F. Weston-Delranf NJ/Murphy, Marian Laboratory Number N4544 Respectfully... Submitted i

6TA. «4 TRANSFORMER s Date Sampled 08/65/91 18il5 ^ W) V - *;IAEGER PCB SITE M1784 Date Received 08/86/91

Sampled fay CLIENT 681291 1984

ANALYSIS FOR REQUESTED PARAMETERSALL RESULTS ARE ON AN AS RECEIVED BASIS

PARAMETER RESULT HDL UNITS METHOD

PCBUs Aroclor i860) £11096-88-53 77 1.0 ug/G SU8080 08/09/91 06119 ALMSURROGATE RECOVERY-PESTICIDE FRACTION ,Tetraehloro-«eta-XyUne<SURRQGATE> 78 -——— % REC SU8088 08/09/91 66tl9 ALHDecachlorobiphenyl-SURR 77 ————% R£C 8uaa80 08/09/91 86119 ALM

Extraction Date -- 08/07/91 12:06 DT

Method Reference! USEPAs"Hethods for Evaluating Solid UasteHiSU-646(8nd Ed.)

Method Refereneei OIL-PCB in oil aethodi EPA-680/4-81-045

1256 GREENBRIER STREET. CHARLESTON, WEST VIRGINIA 25311 — TELEPHONE 304 346MT725 4643 BENSON AVENUE, BALTIMORE. MARV1AND 21227 — TELEfWeN&«<M 647-7400

4440 QLEN ESTE - WITHAMSVILLE RD.,:SUITE 900, CINCINNATI, OHI fiaW'-r TCCEPHONE 613 752-9696

55 V" TECHNICAL TESTING LABORATORIES* j ^ A DIVISION 0* COMMERCIAL TESTINO 4 ENOlNEEWNO CO.

LABORATORY ANALYSIS REPORT ^

Roy F. U»ston-D»lr*n, NJ/Murphy, M*ri*n Laboratory Nunbtr N4546 RtspvctfullySubmitted t

STA. »5 TRANSFORMER Date S*apl*d 08/05/91 18i20 , /yi , \ f ff iIAEGER PCB SITE H1784 D*t* Recvivtd 08/06/91 7, /|iU/Xl/mAC1 "7JSanpled by CLIENT 081271 1924


PARAMETER : RESULT MDL UNITS METHOD

PCB ND 1.0 UO/0 SU8080SURROGATE RECOVERY-PESTICIDE FRACTIONT*trachloro-m«tA-Xyl»n»<SURROGATE> 73 ———— * REC SU8080na«*a«*h1nvnhinh«nvl-SURR 7ft ...... « per CUAAAa

ANALYZEDDATE/TIME/ANALYST

08/09/91 06i36 ALM

08/09/91 06i36 ALHaA/aQ/Qi ac.*?£ ai M

Extraction Date — 88/07/91 12:09 JB

Method References USEPAi'Tlethods for Evaluatini Solid Waste"iSU-846(2nd Ed.)

Method Referencei OIL-PCB in oil methodI EPA-600/4-81-045

- -, -\ M'1258 GREENBRtEA STREET. CHARLESTON, WEST VIRGINIA 25311 — TELEPHONE 304 346-0725

4643 BENSON AVENUE, BALTIMORE. MARYLAND 21227 - TgLEPtfOM} §3§3*7-74004440 GLEN ESTE - WITHAMSVILLE RD., SUITE 900, CINCINNATI, OHICT45245 - TELEPHONE 513 752-9690

•55 I TECHNICAL TESTING LABORATORIES^ L A DIVISION Of COMMERCIAL TISTINQ 4 INGINEERINQ CO.z mmmv: ———————————————

Roy F. Ueston-Oelran,

STA. H9 TRANSFORMERIAE6ER PCB SITE K1724

Sampled by CLIENT

'LABORATORY

NJ/Murphy, Marian

ANALYSIS REPORT

Laboratory Number N4547

Date Sampled 88/05/91Date Received 06/06/91

RespectfullySubmittedi^

18i35 "; * fa ~- \ ' ft LTl.cjx081291 1924


PARAMETER . ,1 ., _ RESULT MDL UNITS METHOD

PCB Us Arocior 1260) C11096-62-S3 70SURROGATE RECOVERY-PESTICIDE FRACTION. ...„Tetrachloro-meta-Xylene SURROGATE) _ ^7Z

1.0 ug/G SU8080


08/09/91 06154 ALM

08/09/91 06 I 54 ALHaa/nQ/Qi ac*^A ai M

Extraction Date -- 08/07/91 12i00 DT

\J

Method References USEPAi"Method* for Evaluating Solid Waste"iSU-846(2nd Ed.)

Method References OIL-PCB in oil methodiEPA-600/4-61-045

1256 GREENBRIER STREET, CHARLESTON, WEST VIRGINIA 25311 — TELEPHONE 304 34 0725 v4643 BENSON AVENUE, BALTIMORE, MARYLAND 21227 — T&EftHQNK30C&7-7400

4440 GLEN ESTE - WITHAMSVILLE RD.f SUITE 900, CINCINNATI, OHIOT5i« TH£PHONE 513 752-9696

5JV' TECHNICAL TESTING LABORATORIESJ j ^ * DIVISION Of COMMIHCIAL TESTING A ENGINEERING CO.


Roy F. Ueston-Delran,

STA. H10 TRANSFORHERIAEGER PCB SITE M1724

Sampled by CLIENT

PARAMETER

NJ/Hurphy, Marian Laboratory Number N4548

Date Sampled 08/05/91 18Date Received 08/06/91

ANALYSISALL RESULTS

PCB (AS Aroclor 1260) C11096-82-53SURROGATE RECOVERY-PESTICIDE FRACTIONTetrachloro-meta-Xylene<SURROGATE>


RESULT MDL UNITS HETHOD

38 1.0 ug/G SU8080

AO ...... * per QUAflAA

RespectfullySubmitted i

148 U /IA "\ * P 4sf* fl*W"*9(M081291 1924

ANALYZEDDATE/TIHE/ANALYST

08/09/91 97 I 11 ALM

08/09/91 07ill ALIIAA/flQ/OI ft9.11 AIM

Extraction Date — 08/07/91 12:00 JB

Method Referencei USEPAi "Methods for Evaluating Solid Waste" iSy-846 (2nd Ed.)

Method Referencei OIL-PCB in oil method i EPA-60 0/4-8 1-045 :

- 1258 GREENBRIER STREET, CHARLESTON, WEST VIRGINIA 25311 -i TELEPHONE 304 3404372S "4643 BENSON AVENUE. BALTIMORE, MARYLAND 21227 - TB HQNE qj 247-7400 '

4440 GLEN ESTE - WITHAMSVILLE RO., SUITE 900, CINCINNATI, OHIC74d2l TE%PHONE 513 752-9696

TECHNICAL TESTING LABORATORIESA DIVISION Of COMMERCIAL TtSTING a CNQINEERtNQ CO. -

\J • LABORATORY ANALYSIS REPORT

Roy F. Ueston-Delran, NJ/Burphyt Marian Laboratory Number N4549 RespectfullySubmittedi

STA. K12 TRANSFORMER ' Date Sampled 08/05/91 18iS0IAEGER PCB SITE M1724 Date Received 08/06/91

Sampled by CLIENT 08l29ri924


ANALYZEDPARAMETER . ' RESULT MDL UNITS METHOD DATE/TIME/ANALYST

PCB ND 1.0 UG/G SU8080 08/09/91 07128 ALMSURROGATE RECOVERY-PESTICIDE FRACTIONTetrachloro-meta-Xylene<SURROGATE> 76 ———— % REC SU8080 08/89/91 07i88 ALHDecachlorobiphenyl-SURR 79 ———— % REC SU8080 08/09/91 07i28 ALM

Extraction Date -- 08/07/91 12i00 JB

Method Referencei USEPAi"Hethods for .Evaluating Solid Haste" iSU-846 (2nd Ed.)

Method References OIL-PCB in oil methods EPA-608/4-61-045

1256 GREENBR1ER STREET, CHARLESTON, WEST VIRGINIA 25311 - TELEPHONE 304 34*07254643 BENSON AVENUE, BALTIMORE, MARYLAND 2l227JWTHLEFg»gg01 247-7400

4440 GLEN ESTE - WITHAMSVILLE RD., SUITE 000t CINCINNATI, OHIO $245 — TELEPHONE 513 752-9696

TECHNICAL TESTING LABORATORIESA DIVISION OP COMMERCIAL TESTING ft ENGINEERING CO.


>y F. Ueston-DeTran- HJ/Murphyf Marian Laboratory Number N43S9 RespectfullySubmittedi

FA. »14 TRANSFORMER Date Sampled 08/05/91 19il0 ^ \ 'IEGER PCB SITE H1724 Date Received 08/06/91 V y

impled by CLIENT 081291 1924

ANALYSIS FOR REQUESTED PARAMETERSALL RESULTS ARE ON AN A3 RECEIVED BASIS

ANALYZEDiRAMETER RESULT HDL UNITS METHOD DATE/TIME/ANALYST

:B ND 1.0 UG/G SU80S0 08/09/91 07s46 ALMIRROGATE RECOVERY-PESTICIDE FRACTION[trachlOTO-aeta-Xylene<SURROGATE> 76 ———— % REC SU8089 08/09/91 07i46 ALMfcachlorobiphenyl-SURR 80 ———— % REC SU8080 08/09/91 07i46 ALM

[traction Date — 08/07/91 12iB0 DT

thod References USEPAi"Methods for Evaluating Solid Waste"iSW-846(2nd Ed.)

thod Referencei OIL-PCB in oil methods EPA-600/4-81-045

1256 GREENBRIER STREET, CHARLESTON, WEST VIRGINIA 25311 — TELEPHONE 304 34*07254643 BENSON AVENUE, BALTIMORE, MARYLAND 21227 - J QCQja SOC247-7400

4440 GLEN ESTE - WITHAMSVILLE RD., SUITE 900, CINCINNATI, OHIO 45245 — TELEPHONE 513 752-9696

57 V TECHNICAL TESTING LABORATORIES" j ^ * DIVISION OP COMMERCIAL TESTING A ENGINEERING CO.

\J


STA. N15 TRANSFORMERJAEGER PCB SITE Hi 724

Sampled by CLIENT

PARAMETER

PCBSURROGATE RECOVERY-PESTetrach 1 or o-«eta-Xy 1 eniOecachlorobiphenyl-SURI


NJ/Murphy, Marian Laboratory Number N4551 Respectfully, Submitted! "A

Date Sanpled 83/85/91 19il5 u/il'i 1 ' //•Date Received 88/86/91 /-(, //•(/ JyU

ANALYSIS FOR REQUESTED PARAMETERS -ALL RESULTS ARE ON AN AS RECEIVED BASIS

1 . .RESULT MDL UNITS METHOD

NO 1.8 UG/G suseaariCIDE FRACTION

R 83 ———— % REC SU8888

831291 1924


88/89/91 83183 ALM

88/89/91 681 83 ALH88/89/91 88183 ALM

Extraction Date -- 88/87/91 12x00 JB

Method Reference! USEPAs"Methods for Evaluating Solid UasteHsSU-64&(2nd Ed.)

Method Referencei OIL-PCB in oil methods EPA-t00/4-61-845

_______->.IM'JS '-.y_____ ./?<jz>OQ5 >1256 QREENBRIER STREET, CHARLESTON, WEST VIRGINIA 25311 — TELEPHONE 304 346-0725 '

4643 BENSON AVENUE. BALTIMORE. MARYLAND 2122? R- rfVFPfl<9€ 301 247-7400X440 QLEN ESTE - WITHAMSVILLE RD.f %UITE 900, CiNCINNATCOVilO 4S245 - TELEPHONE 513 752-9696

7J'\ TECHNICAL TESTING LABORATORIESTv B BV A 0(VISION Of COMMERCIAL TESTING a ENGINEERING CO.


Roy F. Ueston-Delran, NJ/Murphy, Marian Laboratory Number N4552

STA. H17 TRANSFORMER Date Sampled 08/85/91 19IAE6ER PCB SITE 111724 Date Received 08/06/91

Sampled by CLIENT

PARAMETER

PCB (as Aroclor 1260)SURROGATE RECOVERY-PEiTetrach loro-neta-Xy leinai«.af*h1ni*rthi nh«nvl— Sill


RESULT nDL UNITS METHOD

C11096-82-53 130 1.0 ug/G SU8080STICIDE FRACTIONn» (SURROGATE) 79 ———— % REC SU8080

^RespectfullySubmitted i

«25 - /fa \ * u »fj. /liU&Arfu

031231 1324

ANALYZEDDATE/TIHE/ANALYST

08/09/91 08 I 20 AU1

08/09/91 08i20 ALHflfl/aas<ai aa.oa-Ai M

Extraction Date — 08/87/91 12:88 DT

Method Referencei USEPAi"Methods for Evaluating Solid Waste"iSU-846(2nd Ed.)

Method References OIL-PCS in oil nethodt EPA-688/4-81-845

"1256 GREENBRIEH STREET, CHARLESTON^ WEST VIRGINIA 25311 — TELEPHONE 304 3464)7254643; BENSON AVENUE, BALTIMORE, MARYLAND 21227 - TELEPHONE 3Qlf 47-7400

4440 GLEN ESTE - WITHAMSVILLE RO.. SUITE 900, CINCINNATI. OHl&RsMJU-Q&EPHONB 513 752-9696

TECHNICAL TESTING LABORATORIESA orvisioni or COMMERCIAL TESTING & ENGINEERING do:


Roy F. Ueston-Delran, NJ/Murphy, Marian Laboratory Number N4553 ., Respectfully. Submitted:

STA. Kid TRANSFORMER , Date Sampled 08/03/91 19s30IAEGER PCB SITE K1724 Date Received 08/06/91

Sampled by CLIENT • 08129V1924


ANALYZEDPARAMETER . . . ., . RESULT HDL UNITS METHOD DATE/TIME/ANALYST

PCBCas AroclQT 1260) t11996-82-53' 24 1.0 ug/G SU80S0 08/09/91.0&s38 ALHSURROGATE RECOVERY-PESTICIDE FRACTION , .Tetrachloro-»eta-Xylene<SURROGATE> 76 ———— % REC SU80S0 . 08/09/91 88:36 ALMDecachlorobiphenyl-SURR " " 78 ——— X REC SU8080 08/09/91 08s38-ALM

Extraction Date — 08/07/91 12i00 JB

Method References USEPAi "Methods for Evaluating Solid Uaste"iSU-846(2nd Ed.)'f-~ ^ -• . • > ' ' ' . - , . * ? * : • >• • - -. . • i ; ' - . " • .

Method References OIL-PCB in oil aethodi EPA-600/4-61-84S

1256 GREENBRVEFi feTFteET. CHARLESTON, VEST VIRGINIA 25311 — TELEPHONE 304 346-07254643 BENSON AVENUE, BALtlMORE. MARYLAND 21227 — TELEPHONE 301 247-7400

4440 GLEN ESTE - WITHAMSVILLE RLV'SUITE 900, CINCINNATI, OHIO 45245 -

^Jl TECHNICAL TESTING LABORATORIESf f \ _. ....* DIVISION Of COMMERCIAL TESTING a ENGINEERING CO. -

UBORATORY ANALYSIS REPORT ^/

»y F. Ueston-DeTran-

'A. »19 TRANSFORMERlEGER PCB SITE HI 724

lapled by CLIENT

IRAMETER

NJ/Murphy, Marian Laboratory Number N4554


ANALYSISALL RESULTS

iBUr-Aroclor 1260) C11096-82-53[RROGATE RECOVERY-PESTICIDE FRACTIONitrachloro-meta-Xylsne<SURR06ATE>

- - - -

FOR REQUESTED PARAMETERSARC ON AN AS RECEIVED BASIS

RESULT MDL UNITS METHOD

420 1.0 U9/0 SU8080

RespectfullySubmitted s

19s35 . ** . } * U isi> II » wMAfij'

081291 1324

ANALYZESDATE/TIME/ ANALYST

08/09/91 08s 55 ALM

08/09/91 08 I 55 ALHftfi/aa/ai aa.«« 'AI M

RC

SIIt

3,

Pfi

PCSLTflHi

traction Date -- 08/07/91 12s00 JB

thod References USEP As "Methods for Evaluating Solid Uaste"iSW-846(2nd Ed.)

thod References OIL-PCS in oil method i EPA-600/4-81-045

— 125« GREENBRIER STREET. CHARLESTON, WEST VIRGINIA 25311 — TELEPHONE 304, -4643BENSON AVENUE, BALTIMORE MARYLAND 21227 — TaEPHONE 301 247-7400

4440 GLEN ESTE - WTTHAMSVILLE RD.t SUITE 900, CINCINNATI, OHIO 45245 — TELEPHONE 513 752-9696

Jp I TECHNICAL TESTING LABORATORIESfL*—i A DIVISION OF COMMERCIAL TESTINQ * tNGINEERINO CO.

\J LABORATORY ANALYSIS REPORT


STA. M20 TRANSFORHERIAEGER PCB SITE H1784

Sampled by CLIENT

PARAMETER

NJ/Hurphy, llarlan Laboratory Number N4555


ANALYSISALL RESULTS

PCB(as Aroclor 1260) C 11096-63-53SURROGATE RECOVERY-PESTICIDE FRACTIONTetrachloro-meta-Xylene (SURROGATE)


RESULT HDL UNITS HETHOD

1H0 1.0 ug/G SU8080

7*7 ...... V QCT eUACIAn

RespectfullySubmitted s

19i40 - ** 1 ' ff-L.J.fttjJvfftr

081291 1984


08/09/91 09 i 13 ALH

08/09/91 09il3 ALHGIA/fll4/Q1 fl^il 7 *OI M


Method References USEPAsuHethods for Evaluating Solid UasteMiSU-846(2nd Ed.)

Method References OIL-PCS in oil methods EPA-600/4-81-04S

1256 GREENBRIER STREET, CHARLESTON, WEST VIRGINIA 25311 — TELEPHONE4643 BENSON AVENUE, BALTIMORE, MARYLAND 21227 - TELEPHONE 01 247-7400

4440 GLEN ESTE — WITHAMSVILLE RD., SUITE 900, CINCINNATI, OHIO 45245 — TELEPHONE 513 752-9696

5Jt TECHNICAL TESTING LABORATORIESMX- \ A DIVISION OP COMMERCIAL TESTING a ENGINEERING CO.

LABORATORY ANALYSIS REPORT ^/

Roy F. Ueston-Delran, NJ/Murphy, Marian Laboratory Number N4S56 RespectfullySubmitted!

STA. »ai TRANSFORMER Date Sampled 06/05/91 19MS \ ' 0IAEBER PCB SITE »1724 Date Received 08/06/91 V ^7 l jjoJ J

Sampled by CLIENT 331291 1344


ANALYZEDPARAMETER RESULT MDL UNITS METHOD DATE/TIME/ANALYST

PCBUft a mixture of Aroclor types) 850 1.0 UO/0 SU&080Aroclor Type! 1848

Percentage of type in mixtures 3*Aroclor Types i860

Percentage of type in mixtures 97XSURROGATE RECOVERY-PESTICIDE FRACTIONTetr*chloro-met*-Xylene<SURROGATE> 74 ———— % REC SU8060n«^»nh1,-»frtMnh««vl-Q1iPP Aft —— —— __ < frPP QUAdftfl

08/09/91 09s30 ALH08/09/91 39130 ALM08/09/91 09 i 33 ALH08/09/91 09s30 ALH08/09/91 09(30 ALII

08/09/91 39 i 38 ALMAA/aO/QI ftQt7O Al M

Extraction Date — 98/07/91 12:80

Method Reference! USEPAsnnethods for Evaluatinf Solid Waste" iSU-846 (2nd Ed.)

Method Referencei OIL-PCB in oil method I EPA-680/4-81-045

1256 GREENBR1ER STREET, CHARLESTON, WEST VIRGINIA 25311 — TELEPHONE 304 34W72S4643 BENSON AVENUE, BALTIMORE, MARYLAND 21227 - TEL flCfa ft>n%7«7400

4440 GLEN ESTE - WITHAMSVILLE RD.f SUITE 900, CINCINNATI, OHIO 45245 — TELEPHONE 513 752-9696

TECHNICAL TESTING LABORATORIESA DIVISION Of COMMERCIAL TISTINQ 4 fNQINEERINQ pO.


Roy F. Ueston-Delran, NJ/Murphy, Marian Laboratory Number N45S7 RespectfullySubmitteds

STA. H88 TRANSFORMER . Date Sampled 08/05/91 19i50IAE6ER PCB SITE H1784 , Date Received 08/06/91

Sampled by CLIENT . 081291 1944


. ANALYZEDPARAMETER . : v RESULT MDL UNITS METHOD DATE/TIHE/ANALYST

PCB(as a mixture of Aroclor types) 33 1.0 UG/G SU8080 08/09/91 09s47 ALHAroclor Types 1848 , ' 08/09/91 09s47 ALH

Percentage of type in mixtures 14* 08/09/91 09s47 ALMAroclor Types i860 08/09/91 09s47 ALH

-Percentage of type in mixtures 86% 08/09/91 09s47 ALMSURROGATE RECOVERY-PESTICIDE FRACTIONTetrachloro-met*-Xylene<SURROGATE> .78 ———— % REC SW8080 08/09/91 89I47 ALRDecachlorobiphenyl-SURR 77 ———— % REC SU8080 08/09/91 09s47 ALH

ction Date -- 08/07/91 12)63 DT

Rethod References USEPAT'Methods for Evaluating Solid Waste"sSU-846<8nd Ed.)

Method References OIL-PCS in oil methods EPA-600/4-81-045 . ;, . . ,

*-TELEPH1256 GREENBRIER STREET, CHARLESTON, WEST VIRGINIA 25311 .*- TELEPHONE 304 3464725 -4643 BENSON AVENUE, BALTIMORE. MARYLAND 21227 — TELEPHONE 301247-7400

4440 GLEN ESTE - WITHAMSVILLE RD., SUITE 900, CINCINNATI, OHIO 45245 <- TELEPHONE 513 752-9696

TECHNICAL TESTING LABORATORIESA DIVISION Of COMMERCIAL TESTING a ENGINEERING CO.


Roy F. Ueston-Delran, NJ/Murphy, Marian Laboratory Number N4538 RespectfullySubmitted! ,

STA. H83 TRANSFORMER Date Sampled 08/03/91 19s55IAEGER PCB SITE It 1724 Date Received 08/06/91



ANALYZEDPARAMETER RESULT MDL UNITS METHOD DATE/T IDE/ANALYST

PCB < as a mixture of Aroclor types) 189 1.9 UG/G SU8089 08/09/91 10105 ALtlAroclor Types 1848 08/09/91 10105 ALM

Percentage of type in mixtures 4* 08/09/91 10103 ALIIAroclor Types 1869 08/09/91 10105 ALH

Percentage of type in mixtures 96* 08/09/91 10103 ALIISURROGATE RECOVERY-PESTICIDE FRACTIONTetrachloro-m»ta-Xylene<SURROGATE> 71 ———— % REC SU8089 08/09/91 10105 ALMDecachlorobiphenyl-SURR 81 ———— X REC SU8089 08/09/91 10103 ALM

Extraction Date - 08/07/91 18:00

Method Reference! USEPAi"Method* for Evaluating Solid ya»te":SU-846<2nd Ed.)

Method Referencei OIL-PCB in oil methods EPA-600/4-61-043

1256 GREENBRIER STREET, CHARLESTON, WEST VIRGINIA 25311 —TELEPHONE TO*346X77254649 BENSON AVENUE, BALTIMORE. MARYLAND 21227 — TELEPHONE 301 247-7400

4440 GLEN ESTE - WITHAMSVILLE RD., SUITE 900, CINCINNATI, OHIO 45245 - TELEPHONE 513 732-9696

53 V TECHNICAL TESTING LABORATORIESW 1^———* *• OIVISION Of COMMERCIAL TISTING a CNGINEERIN& CO.

O LABORATORY ANALYSIS REPORT

Roy F. Ueston-Delran, NJ/Hurphy, Marian Laboratory Number N4539 Respectfullyr Submitted s

STA. 1*84 TRANSFORMER : : . Date Sampled 08/03/91 80100 , .-_ • + ' ' Q jLIAEGER PCB SITE *1784 * Date Received 08/06/91 Y Y/. IjJjUUf JfJT

Sampled by CLIENT 'ft08lftl 1953

, ANALYSIS FOR REQUESTED PARAMETERSALL RESULTS ARE ON AN AS RECEIVED BASIS


PCB (as a mixture of Aroclor types) 140 1.0 UG/G SU8080Aroclor Types 1848

Percentage of type in mixtures 6X .Aroclor Types 1860

Percentage of type in mixtures 94XSURROGATE RECOVERY-PESTICIDE FRACTION "Tetr«chloro-meta-Xylene<SURROGATE> 71 - ——— % REC SU8080n*M>AklM»nh4 nhavtwI-QUOe -', 77 ...... « PFP CUAflACt

08/09/91 10188 ALM08/09/91 10s£8 ALH08/09/91 10s 88 ALH08/09/91 10S88 ALR:0S/09/9i 10:22 ALR

' 08/09/91 10122 ALMaA/aq/Qi idiPP 01 M

ction Date — 08/07/91 18:00 JB

Method References USEPAi"Method* for Evaluating Solid UasteMsSU-846(8nd Ed.)

Method References OIL-PCB in oil methods EPA-600/4-61-843

1256 GREENBRIER STREET, CHARLESTON. WEST VIRGINIA 25311 — TELEPHONE 3IM 6&0725 '4643 BENSON AVENUE, BALTIMORE MARYLAND 21227 — TELEPHONE 301rt$WOO

4440 GLEN ESTE - WITHAMSVILLE RD., SUITE 900, CINCINNATI, OHIO 45245 -*TClEPHONE 513 752-9696i

TECHNICAL TESTING LABORATORIESA DIVISION OP COMMERCIAL TESTING ft ENGINEERING CO.


Roy F. Ueston-Dslran, NJ/Murphy, Marian Laboratory Number N4560 RespectfullySubmittedi

STA. »23 TRANSFORMER Date Sampled 08/05/91 £0105IAEGER PCB SITE H17S4 Date Received 08/06/91



ANALYZEDPARAMETER RESULT MDL UNITS METHOD DATE/TIi1E/ANALYST

PCB(as a mixture of Aroclor types) 710 1.0 UG/G SU8080 08/09/91 10i39 ALMAroclor Typei 1842 08/09/91 10i39 ALM

Percentage of type in mixture: 8% 08/09/91 10i39 ALM- , . '. , Aroclor Typei I860 08/09/91 10i39 ALM

Percentage of type in mixture: 98* 08/09/91 13:33 ALMSURROGATE RECOVERY-PESTICIDE FRACTIONTetrachloro-meta-Xylene<SURROGATE> 68 ———— * REC SUS080 08/09/91 10139 ALMDecachlorobiphenyl-SURR 86 ———— % REC SU8080 08/09/91 10s39 ALM

Extraction Date -- 08/07/91 12:00

Method References USEPAi"Methodt for Evaluating Solid Ua»te"iSU-846<2nd Ed.)

Method Referencei OIL-PCB in oil methodi EPA-600/4-81-043

1256 GREENBRIEfl STREET, CHARLESTON, WEST VIRGINIA 25311 —4643 BENSON AVENUE, BALTIMORE, MARYLAND 21227 — TELEPHONE 3OT 247-7400

4440 GLEN ESTE - WITHAMSVILLH RD., SUITE 900, CINCINNATI, OHIO 45245 — TELEPHONE 513 752-9696

7J( TECHNICAL TESTING LABORATORIES*W , L A DfVTSION Of COMMERCIAL TISTING * tNQlN BERING CO.


Roy F. Weston-Delran, NJ/Hurphy, Harian . Laboratory Number N4561 RespectfullySubmitted i , o

STfl. *86 , TRANSFORMER -, Date Sampled 03/03/91 80110 \j /w . V /IAE6ER PCB SITE 111784 Date Received 0S/06/91 X ( //» iPALOflk

Sampled by CLIENT ...'.; 081891 1943


ANALYZEDPARAMETER : RESULT HDL UNITS METHOD DATE/TIME/ ANALYST

PCB (as a mixture of Aroclor types) 870 1.0 UG/G SW30a0Aroclor Typei 1848

; Percentage of type in mixtures 3X . •^ ' _ . " ' , [ Aroclor Typei I860

. Percentage of type in mixtures 97XSURROGATE RECOVERY-PESTICIDE FRACTIONTetrachloro-meta-Xylene<SURROGATE> 70 ———— % REC SUS080n.M.nhl A^^hf nh^Mul .GtlCQ A1 ------ < PCP CUAflAfl

08/03/91 10137 ALH08/09/91 10157 ALM03/09/91 10157 ALM08/09/91 10157 .ALM03/09/91 10157 ALH

08/09/91 10157 ALMflA/flq/^l ifiiS? AIM

E**-raction Date -- 08/07/91 12i00 DT

Method Referencei USEPAi"Methods for Evaluating Solid Waste"iSU-846<8nd Ed.)

Method Reference! OIL-PCB in oil methods EPA-600/4-81-045

A*1256 GREENBRIER STREET, CHARLESTON, WEST VIRGINIA 25311 — THdEfyWNE 304 346-0725 *-

4643 BENSON AVENUE, BALTIMORE, MARYLAND 21227 — TELEPHONE 301 247-74004440 GLEN ESTE - WITHAMSVILLE RD.t SUITE 900, CINCINNATI, OHIO 45245 - TELEPHONE 513 752-9696

TECHNICAL TESTING LABORATORIESA DIVISION Of COMMERCIAL TESTING 4 ENGINEERING CO.


Roy F. Ue«ton~Delran, NJ/flurphy, Marian Laboratory Nunber N4562 RespectfullySufanittedi

STA. »87 TRANSFORMER Date Sampled 08/05/91 30115IAEGER PCB SITE Ml784 Date Received 88/06/91




PCB (as a mixture of Aroclor types) 5800 1.0 UG/0 SU8080 03/09/91 11U4 ALMAroclor Typei 1848 03/09/91 Ilsl4 ALM

Percentage of type in mixtures 4* 03/09/91 Ilal4 ALMAroclor Types i860 03/09/91 111 14 ALM

Percentage of type in mixtures 96* 08/09/91 Ilsl4 ALMSURROGATE RECOVERY-PESTICIDE FRACTIONTetrachloro-met*-Xylene<SURROGATE> 79 ———— % REC SU3080 03/09/91 Us 14 ALMDecachlorobiphenyl-SURR 79 ———— % REC SU8080 08/09/91 Ilsi4 ALM

Extraction Date — 08/07/91 18i00 ;

Method Referencei USEPftiHHethod* for Evaluatini Solid Matte"iSU-fl46<8nd Ed.)

Method Referencei OIL-PCS in oil methodt EPft-600/4-81-045

1256 GREENBRIER STREET, CHARLESTON, WEST VIRGINIA 25311 —TELEPHONE 304 3464)7254643 BENSON AVENUE. BALTIMORE, MARYLAND 21227— TELEPHONE 301 247-7400

4440 GLEN ESTE — WITHAMSVILLE RD., SUITE 900, CINCINNATI, OHIO 45245 — TELEPHONE 513 752-9696

TECHNICAL TESTING LABORATORIESA DIVISION Of COMMERCIAL TESTING a ENGINEERING CO.


Roy F. Weston-Delran, NJ/Murphy, Marian Laboratory Number N4563 RespectfullySubmitted!

STA. »28 TRANSFORMER : Date Sampled 08/05/91 20i20 f \ *IAE3ER PCB SITE Ml724 - Date Received 08/86/91

Sampled ox CLIENT 081291" 1945


ANALYZEDPARAMETER - RESULT HDL UNITS METHOD DATE/TIME/ ANALYST

PCBU* a mixture of Aroclor types) 3300 1.0 UG/G SU8080 08/09/91 Ili31 ALMAroclor Typei 1842 ' . 08/09/91 Ili3l ALM

-Percentage of type in mixturei SX 08/09/91 Ili31 ALM• Aroclor Typei 1260 08/09/91 lli31-ALMPercentage of type in mixtures 95% 08/09/91 11:31 ALM

SURROGATE RECOVERY-PESTICIDE FRACTION . . .Tetrachloro-meta-Xxlene<SURROGATE> 97 ———— X REC SU3080 08/09/91 Ili31 ALHDecachlorobiphenyl-SURR 59 ———— % REC SU8080 08/09/91 Iii31 ALH

£y*--action Date -- 08/07/91 12:03 JB

Method Referencei USEPfli"Method* for Evaluating Solid Ua«tt"iSU-646<2nd Ed.)

Method Referencei OIL-PCB in oil methodi EPA-600/4-81-845

1256 GREENBRIER STREET, CHARLESTON, WEST VIRGINIA 25311 r-4643 BENSON AVENUE, BALTIMORE, MARYLAND 21227— TELEPHOrH01 247-7400

4440 GLEN ESTE — WITHAMSVILLE RD., SUITE 000, CINCINNATI, OHIO 45245 ** TELEPHONE 513 752-9696

TECHNICAL TESTING LABORATORIESI PA DIVISION OP COMMERCIAL TESTING & ENGINEERING CO.


Roy F. Ueston-Delran, NJ/Murphy, Marian- , Laboratory Nuaber N4564 Respectfully

STA. H30 TRANSFORMER Date Sampled 08/05/91IAEGER PCB SITE 111734 Date Received 08/06/91

Sanpled by CLIENT 081291 1945



PCB(as Aroclor 1260) 011096-88-51 5.3 1.0 ug/G SU8080 08/09/91 11149 ALMSURROGATE RECOVERY-PESTICIDE FRACTIONTetrachloro-meta-Xylene<SURRQGATE> 79 ———— % REC SU8080 08/89/91 11i49 ALMOecachlorobiphenyl-SURR 77 ———— % REC SU8080 08/09/91


Method Reference! USEPAi"Method* for Evaluating Solid Waste1*iSU-846<and Ed.)

Method Rtferencei OIL-PCS in oil methodi EPA-600/4-81-045

1256 GREENBR1ER STREET, CHARLESTON. WEST VIRGINIA 25311 - TELEPHONE 304 34*0725464$ BENSON AVENUE. BALTIMORE. MARYLAND 21227 — TELEPHONE 301247-7400

4440 GLEN ESTB — WITHAMSVILLE RD., SUITE 900. CINCINNATI, OHIO,45245 fVft&.BPHONI* 513 752-9696

; 57 I TECHNICAL TESTING LABORATORIES' / / eeeW * DIVISION or COMMERCIAL TESTING a INOINCERINQ co.

; w LABORATORY ANALYSIS REPORT

Roy F. Ueston-Delran, NJ/Hurphy, Marian Laboratory Number N4565

•

Respectfully;Submitted: ' A

STA. tt31 TRANSFORMER Date Sampled 08/05/91 12:28 j \ s jf LIflEGER PCB SITE H1724 Date Received 08/06/91 T [ (jJ XW-

Sampled by CLIENT


PARAMETER RESULT MDL UNITS METHOD

PCB (a* Aroclor I860) C11096-S2-53 3.4 1.0 ug/G SU8080SURROGATE RECOVERY-PESTICIDE FRACTIONTetrachloro-«eta-Xylene<SURROGATE> 74 ———— % REC SW8080nar**/th1nvnh4 nh«Mwl-QIIBO A1 ...... < PPC SUAflAfl

R081291 1957

1


08/09/91 12106 ALH

08/09/91 12:06 ALMGtA/aQ/qi id.ac -at H

Extraction Date -- 08/07/91 12i00 JB

Method References USEPAs"Methods for Evaluating Solid Waste"iSU-846(8nd Ed.)

Method Referencei OIL-PCB in oil nethodi EPA-680/4-81-045

• -:_________ ft I ODdlD

1256 QREENBRIER STREET. CHARLESTON, WEST VIRGINIA 25311 — TELEPHONE 304 3464725 .4643 BENSON AVENUE, BALTIMORE. MARYLAND 21227 -.TELERfKDN£3ai 247-7400

4440 GLEN ESTE - WITHAMSVILLE RD., SUITE 900, CINCINNATI, OK&fi«3iUJ Y&EPHONE 513 752-9696

SAMPLE CHROMATOGRAMS

TECHNICAL TESTING LABORATORIES

PCB

o,,';;

£ZCHROM\8HOS\eH08.014EZCKROM\MeTHODS\pco.met 0.N4S42 no ctil. '

1991 05:44:30

Channel B

' « ! [ • ) 1i «t li 444' * . ! . '! 35i oi o j i

!3j

1 !' • • 1 i ' JI ;l;l i! * f; ;!!i !. ' ; i !

''•''• •' 'k! ' '- » T I

• •• :! ; j 1 * |

ij

t :I?

It

1

11<t!.3j

5*82a

*

i>i?,i

'ii& ;6. '

3fl84g

i.! :

i

-

,7

5 10Minutes

•-'kno r.:er.., . ime Are<*

•1 O.VJ3A 4235737 52 0,396 5053210 63 0.324 260632 04 0.620 ' 2477G3 0* 0.756 59236 06 0.820 73380 07 0.916 42322 08 1-076 2561519 3'•» 1.212 69235 010 i.31A 13720 011 1.368 54512 012 1.496 24535 013 1.564 93380 014 1.724 9429 015 1.844 2876 01.6 I .940 47395 017 1.996 33Q69 018 2.220 47775 019 2.520 138753 020 2.663 14432 021 2.880 64089 0

: 3.032 83801 03.260 812097 1

24 3.476 1270853 123 3.796 18529 0

88100072

Ret, Time Area Area?:

:-:.924, . • -494801 !.4.056" 2494103' 5'•• » x£w6 oZ:tT.i.3':i':;' ';i.520 7210803 3,,732 402237-a 4,.964 942A23:!. 11S.072 4A32I346 ^,.336 690932 15, .464 4244911 fi,?.316 ' 2090815 2

S-390147 .i.292 10S53139 126.588 1232078 . 16.784 1456206 2"'.120 2775410 37-304 328483 O7,69, 3652334 4

PCB ANALYSIS

File : C:\EZCHROM\8H08\8HOS.OiSMethod : C:\EZCHROM\METHODS\pcb.metSample ID t N4543 no dil.Acauired : Aug 09, 1991 06!01:56

Channel B

0.4!

Vat5

1

<21jl;

i

T

i!

j

i- i! Ji

f> •< ii 'f ;5 , '^o0 :r 'bo..:

_

. -

6 .

5 'I7i

1 ••'•'•'"; j] ;..

U .d.2 2 :3|33334S44; ,3 = * | 477^

- ' ' i. e3 99 i• .' * .

i . ti o 2 2EJ fi.ri' 7. • s;j;... .;.. . 9 .. :

tll!!;Hii!!l!!!;]n 91-rfii 3o SiI AS #1

•vW-W-'|3 c : 44<> 42 a

3 10

Minutes

kn o fte t -. 1" i me Ar » A A r ea":

1 0.236 3791324 242 0.324 913073 63 0.396 358001 Z4 0.432 374805 23 0.520 142369 1£ 0.620 119108 17 0.764 27646 OtiJ 0.824 131830 19 1.000 10442 010 1.076 2466708 1311 1.212 43343 012 1.312 10119 013 1.364 44300 014 1.488 24633 013 1.560 127302 116 1.696 30694 017 1.344 3933 018 1.936 63049 019 1.988 81396 120 2.064 18327 O21 2.212 80603 0

2.312 94342 1£.828 236676 1

24 3.032 139872 123 3.180 272887 2

ABiOQ07<t

kno Ret. Time Area Area":26 3.352 74296 027 3.536 16685 0

j.ot>6 28679 05.308 34306 04,, 044 66433 04.212 97266 14.344 46787<*. 308 80684

34 -4,732 '64297.968 271733 25.340 12058 0

37 3.464 42138 036 3.816 115083 139 4.288 101131 1'40 6.576 1307530 94'l. .*:..v3£ 69099 O42 :• « i.0fl 23219 04.3 7.372 6168 0#4 7.,-'120 4399 O43 7.496 36132 04o 7.480 3679101 234V 6.176 139 0'•!8 3.58 484 04? 9., 680 42885 0'."•O 9 ,OG4 ' 69O6 O!-:!. , 9,'212 . &90 0!?2 11.248 1943 0

ANALYSIS

\ C*\EZCHRQM\8H08\SH08.016

.irsa : Auc 09, 1991 06:19s20

Channel B

' .; ., •( ;.' 1 !; tfi. *•

i|

1" 213 4

<i 1,i0 jj. ^ 4 ,t «5

1f

' ———

I

I

\Ii

4 ?

i 1s ertt v oiW] J 7• n: w s i6* ; i i 7 i i 2 1

5 10Minutes

' :'-rio I-?et,. Time

'i. 0-:!.23 6741 o,:': 0.236 4174968 33 0.396 2633706 5

0.524 149227 0'3 0.616 399775 26 0.744 12500 07 0.840 963364 28 1-068- 2450530 5'.;; 1.204 47575 0

-.0 1.376 83925 011 1.456 9546 012 1.556 2Q8583 113 1.704 18530 014 1.336 5108 013 1.924 33392 016 1.980 44798 017 2.196 43351 018 2.50O 97527 019 2.608 ' 7966 0iiO 2.816 56889 0"1 3.00(3 360058 1

3.164 74890 0• 3.232 372327 1

24 3.452 506761 123 3.772 37920 0

Aft 100076

FC3 ANALYSIS

:•'-:• is : ; ; \mCHRQM\3HOQ\8H08 ,O3i

- •rll' c" : V. '09. 199?^

Channel Sj •=•*

. i 11i

; lie'*! ill3?;

• tf1!! Hi•51 !!| i

' jii:l :

. f •'.', ' •

.,, i :; ! ;i,'.. • (I ! '

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1 i1*9 i; !3 • [1 1! " . .

i:ii H'1i,1- ii'sci9 '* *ji1 :*fls

:2; i?.7* 2*« 0c44 73 T8g 73 ;

i,9! * :t 3

irtifi 'i«l11M;

: ljiIfijl!iiiii

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!'•' kn c i\ ** + .. ' i me A re A Area £

6722 0369 924 143213-*2 11776798 01726490O 510639476 32321605 1

8 1.268 145837 09 , ,380 1163368 010 1-344 1*410*14 O11 L.740 642352 012 1..844 33082 O

597842 014 ,2.068 116169 013 2.148 1704228 016 2.238 702010 017 2.388 362270 018 2.504 1021517 019 2.772 663538 020 2-880 722278 021 3.084 476370 022 3«22<5 3902248 1

3.436 5248799 13.752 139912 O

23 3.884 2489262 1

£• kn o Re t . T i me A rs»a A r e a#

. 192 12537081

.. 472 ''i 50492

. .920 231779«4 7

.020 27286462 8

.272 5612347 2,,420 30866828 9«776 33753836 16.240 46797624 13.524 30O3913 l

.064 1 269148 3,444 3137383 1,,632 4056395 1

..296 I5O31 O„376 W800 0..963 2720 0. j'32 536 0.. "'32 "S3 0,.772 15372 0

1629 03267 04 97 0

HRI00078

PCB ANALYSIS^

Fils s C:\EZCHROM\8HOe\8H08.032"leaned : C:\EZCHROM\METHGDS\pcb.met ASamole ID : N4561 no dil. uAcau.ired : Auq 09. 1991 10:57:16

Channel 3

O - '4

o 5riinuces

f kn o Pe t« T :i. me A re A

1 0.236 3801543 32 0.392 2189288 23 0.520 692593 04 0.616 S586469 6& 0.844 3238133 46 .1.064 2378438 2/ 1.196 1(3646 03 1.26(3 21902 0? 1.380 365308 010 1.548 168045 011 1.732 44133 012 1.868 13307 013 1.972 103358 O14 2.080 20417 013 2.156 104378 016 2.292 38537 017 2.396 22078 018 2.304 184574 019 2.784 103343 0'20 2.8BO 72838 0

3.012 106081 0

23 3I444 1679404 124 3.768 67993 O2S 3.892 722974 1

r ftR 100079

i::ikr.o vv>t „ Tim® Area Area":-'-""- ...... .......... .-....- ....._——.._„._ .._._

c6 -,.024 3994886 3

,::':? •:•., •-••: '3547770 6'.:' 4 6->6 5732072 430 ••* .V33 9302331 7', i. :;..O .iJ 10316934 732 .....::S4 1703417 ;-.•:••• :-. 428 10297316 73 J:.,,7;; J 22926310 16.T5- -:i:';.2 18186104 1336 :... 36 1946157 .1.37 .'>../•••"; 2632746 2•;J* , %Oi:iO 3931621 4,:;9 ^.456 1117589 1

/. ::B 3833385 3;>.33:^ 708972 1:i..«r:2 84573 09. 3.;. 6 1233 09 ...376 10720 0y.-flAa 7545 0•'.. ;J-: 45255 0

:;.«.- .,2 - 5048 0..o , ..:.:u 72015 0,0,,^-:-2 17408 0i. ;...;•!:: • 1186 O

AR100080

PCB ANALYSIS

C : \EZCHROK\8HOS\SHOe . 033C:\EZCKROM\ME-HC3S\pcE.met

H -"i4362 i/40; Auq 09, 19? 1 -1: l4i-36

Channel

4 r i-n a -I.. : •*, *! t *• * . j* i _*

; ?**; If!

,3i 14]: s*'• ]-iPI Hi i l l -

jl 2'

l^UzV 2233° i i|! : Miv *v • 1 * 11 i 2 i i • 'i •L tO *^1'"«1^ * it'' I i ' \l '. B '

'!'.

•!?-u28

5 10

"iinutas

1 kr: o Re t.. T i me A re A A re a£

1 0.236 19O3612 3;.; 0.392 1356196 2-.T 0.428 1393715 2'; 0..520 361114 15 0.612 5057202 76 0.844 2166226 3

0.996 30314 0<:? 1.060 67602 07 1.268 36728 010 . .L.380 146996 011 1.548 26892 01.2 1.748 39921 0i.3 1.936 32863 01.4 2.072 2633 015 2.156 105411 016 2.300 364SO 017 2.338 20976 018 2.312 33193 019 2.788 53683 020 2.89.6 50610 021 3.008 16232 0

I 3.100 23871 023 3.240 605441 124 3.436 903200 125 3.912 330304 0

.RR10Q081

Pkno Ret.. Time? Are?a Area";

26 4.040 2204817 327 *„ 216 2442001 3:£& ^.JX>0 ^Uo^IG 7:.:° -^712 ,5467033 530 '4.748 4982191 7'5.1. *•. .044 6126348 9: 2 ?-.. 04 U41436 :!.J>:: •;H44« 3737490 5:':-4 .?.4V2 -J.y9S364 335 e.SOB 12353672 17::SA 6«272 8933416 133X o.5o2 28145 033 - .768 936704 139 7.10O 2568731 4'*O /.,4BO 429098 1•••;•. -..660 93314 0f'2 ••!.-. 363 854 0:-; H,. 300 830 0^4 v.,633 4454 0'*•:: ^0.316 6233 0

PCB ANALYSIS

£ile s C:\EZCHRQM\8HOe\SH08.034 ,_ A: C:\ezCHROM\METHQDS\Dcb.(net Qt ///&3 ~7 (O""***ED J N4363 1/40: Aug 09, 1991 11:31:59

Channel B

W

'<•>Hft

< j

0., ;|

I JsrA ••? "k°- j|&i'.-- ilir,

k

, . nil0.1 { jlji

i l l i* ' !;i ;•:

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. 4: " 4W i1. :,i-2:-2 22,*°e? 3 " *I"i'"'' *"

|«64 3SttW« 8j||'1 i 5 *4048 £24 042 (11y^ ^ ^ 'UJ..p-V«kj*K*V*'Vi*U.!.

4

42N

00

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41

1-*'*• >& '09 £2 !8:

]

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1

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tf

2

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:{l

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} 7 tf 9^ 1 £ *o6 5 I* ^ 4

A* *J.V-V— Hl '5 10Minutss

P Kn o R ® t - T ± m e Area, ft r e A ":

1 0.236 2426516 '*2 0.392 2409063 43 0.423 2420214 44 0,520 536762 15 0.612 5156022 86 0.840 2088044 37 0.996 31497 08 1.052 82050 09 1.260 14383 010 1,376 113862 . 011 1.344 20383 012 1.736 49913 O13 1.860 12796 014 1.944 50930 015 2.068 11880 016 2.148 133398 017 2.288 54109 013 2.392 42718 0'19 2.304 98749 020 2.7QO 63677 O

2.884 43911 02.992 2490 0

23 3.224 462237 124. 3.440 717532 123 3.756 9435 0

ftR|00083

o -v'rat.. "-'i;n& Area

:* ..;,::; 9 2 .r w,?./• ••.- 024 •..::> 6 s:i.o:7:-.> -•• V:.;>o ;;:i37o:7 v,,.;C;4 ie.10': --..^9^ 30:!. IT-2

-4V76317 - 85../3S 10S31Q97 16-..236 7774681 12.'-;.. 20 238969 0ft. A,1 8 1.040438 £7. ,080 2121929 3

••:!. -',,040 7O933 042 :=J.7&3 17279 03 ;;i,,824 8S8 0

3619 03096 ;;

I 0008**

PCS ANALYSIS

ie = ••: = \EZCHROm 3HOS X fl

•••> -:c '_'. i r «c : ->ua 0 , .1 9 t ;. .; s 4? s 20

3

9 as®'i??J!«T 39i*2SOBS** 2 49 i 3'

10Minutes

ime

1 0.172 5331 0V: 0.236 4216687 26:•: ';.3i33 751677 54 :>.616 377241 2

0.764 80697 16 0.844 223150 1

0.936 124707 .tS 1.064 2682462 179 1..304 73516 010 1.352 110891 111 1.344 258646 212 1.724 22674 013 1.820 18O67 014 1.928 17623 013 2.200 170764 116 2.332 - 2732 017 • 2.496 16O668 119 2.632 27890 019 2.832 103798 1' X> 2.996 93113 1V Jmt •? O'Tf'? i OTTEO1 tN—*.k U-. £.*}£. lY/O^l 122 3.372 52394 023 3.660 76766 024 3.852 91149 125 4.004 114892 1

\00085

Pkno Ret., Vim* Are*128346 1 , >7033 0

x:.d -,364 1180B' 0..;•: 'i.^aa 197974 i3'> 4..708 88610 l•":;. 4,932 174152 132 ,.032 106038 l33 5 ..276 13280 034 .,348 41034 03S S.42S 194768 1-•-V .67« 14663 037 '5.792 410237 339 6.260 330340 239 ,. 44 336115 2••1C 6 .,744 #4643 1.•:"". 6..920 '5137 0•••£ 6,988 1168 0'•*5 7. .094 97O24 1^4 ' .352 ^54 045 7 ..388 3270 0'•'• V..464 42519 047 7. .648 3630587 2348 o,136 3437 0•:-;:j 3.380 21 ' 29 0"••''•> ::;,.448 !.475 0'•:.:. • ;.. :::3 4392 0.:•:; o, /1 6 3796 03 "•,. 8:1.6 8633 0

•" >iJ.860 4244 0'•>$ 9. .024 ' -316 O 'r:>6 10. .232 6888 O:.;/ ".1.024 277 O33 I.:!.,. 108 10 93 O•:9 :;.:i. ...'76 68:1.1 0

4346 O

AR I 00086

PCB ANALYSIS

File : C:\EZCHROM\8HQ8\eH08.036Metnoc : Cs\EZCHROM\METHODS\ocb.metSample iD s M4565 no ail.Acquirea : Auq 09, 1991 12s06:44

Channsi B

O.4;

n —— i —————————M 1j i >jh jj S *

il 1! :! .1

'

i.

6i544

1100

a900

3 10Minutss

Ket. Time Area . Area"i

I. 0.116 6643 02 0.236 4517529 293 0.388 469554 34 0.752 76313 O* 0.828 245831 26 0.928 26153 O7 1.064 2515761 168 1.196 44747 09 1.308 12321 01O 1.348 4859s 011 1.476 16806 012 1.548 132016 113 1.752 12576 014 1.912 60926 015 1.976 37968 016 2,196 59182 017 2.492 141174 110 2.640 25284 019 2.864 96483 1

3.000 83581 13.160 116310 1

22 3.436 1695 023 ' 3.632 22870 024 3.768 1650 023 3.856 65190 0

ftRlOOOS?

'Ti o 7'" o x . ." ;. me Area A r e a A;

I- -i.OOlfj 41446 0'.'.'-7 '-,<.:CO- . 43810 0

-3" -.;•:<: :3639 S3.') . ,.9 0 323036

' :v, .-••;;;; 107031 :!.-i,, ',*& S303 0-..7 6 266626 2.-!,.iii"i: 271228 3..,344 1686800 113 ..9 04 2069 0-.',0;.iO 97207 1;,.3I4 :l.269 0?-.46<) 77637 0"',. ••0 3818644 4..j.. .;;4 926 0ri.J300 1O674 0:;;,. ;v^ 134Q 0

••-• •:•., :'.4 2936 0:: :".T:::: 2677 o<•*'•" >• ...••":.; 5421 0^^ •• ..'•• :-l; :!.482 0'-' ^-:v*' 4462 O':•"••• '.'=../:•.;> 996 0

fCONFIRMATION. CHROMATOGRAMS

ARi 00089TESTING LABORATORIES

PCB ANALYSISCONFIRMATION COLUMN

s C 5 \EZCHROM\8H08\8HC8. "01 4: C: \£ZCHROM\METHCDS\pcc .met:D j. N4542 no dil.d s Aug 09, 1.99.1 05: 44; 30

4i

Channel A

(,

;((

i\

;I

1

'C4

.

5»•

80

1

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7

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48

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100090

PCB ANALYSIS^CONFIRMATION COLUMN

File ; Ct\EZCHROM\8HOe\eH08,015.retncc s C:\EZCHROM\METHODS\pcb.metBamals ID : N4543 no dil.Accuired : Ana 09. 1991 06:01:56

0

Channel A

AR100091

:::NF : -'"AT i ON COLUMN;'- j la i •:; 3 ' SZCHROMXSHOeSSHOS , 016:*»str33 i Ci \EZGHROM\nETHODS\ocb .metsamo^e .J s N4544 no dil.Accu '.-sc : '-*uc 09 , j.991 06 : 19 : 20.jeer A co*1" 'i -- ——————— — .————— — —

Channel A

ABI00092

-'C3 ANALYSISN COLUMN

Fj ia a C:\EZCHROM\SHOS\^H03.017hetroa i! C: \c.ZCHROM\METHCi)S\pco.!net

ID s M4-546 no ail.: Anq 09 1991 06:36:40

O.lj !

o.oLi

Channel A

S 10Minutes


F.ila s C:\2ZCHROM\8HOQ\8HOS.OiaM^r.i^uci -i J s \EZCHROM\METHODS\pcb. metSame.a ID s 4347 nn dil.U o e r-^ TIo r * —-»——————.^—.—.—.—^—

Vo

Channel A

ARI0009U-

PCB ANALYSIS^CONFIRMATION COLUMN

File s C:\EZCHROM\8HOa\8H08.019rie-naa : C:\EZCHROM\METHOOS\pcD.metSample ID : N^543 no dil.ttcauireq : Au<g 09, 1*91 07:11:23Operator : ————-——-——————

o

Channel

AR100095

= ATIGN COLUMN

: 3 \EZCHRGM\3HOS\ 8H08 . 020<'"=?r."Qc t Z 3 \EZCHROh\rit i HGDbXpcb . met=*urtpi a A!) s \£?4? ra dil.cc(.ii:*-«G .' HI tc 09 ,: .L991 07:28:47

*m* ' .7- T7 ' l \ . :+i '* ' '™ * *"" *"" **** "™* *~ ** ™~ ** *"" m ~ ™"

V

o.ou

Channel A

0 3 10Minutes

ARI 00096

'-'•",£ ANALYSISCONFIRMATION COLUMN

Ci \EZCHROM\8H08\t3HQS. 021C:\EZCHROM\METHCDSSoco.met

s .'44550 no dil.: Aua 09, 1991 07:46:06

0

Channel A11jf '

1

t 11

ftRI00097


i"i.Ie s C:\EZCHRQM\SH08\SHOQ.022hetnoc s C : \EZCHROM\METHODS\ccb. matSample ID 4 N4351 no dil.Accuirec : uc 09, 1991 09:03:35

0.1

0.0

Channel

O 3 10Minutes

\0009«.

-V ;CB ANALYSISVCONFIRMATICN COLUMNFile ! C s\EZCHROM\eH08\8H08- 023Metnod : S:\EZCHRQM\METHGDS\pcb,matSamoia IS : N45S2 no dil.Accuirsa i Auc 09,, 199.1 08:20:55Caeratar : —————————————

o

Channel A

»00099

/A-ALY -312GN COLUMN

0 : \SZCHRCM\8HOS\8H06 . 024::: \EZCHRQM\METHOD3\ocD.mst: 4c-53 nc dii.

; Aua 09. 1991 03:38:19

O.'O J

Channel A

! !' tjjfi ;: "

: 1• a

iIi

\i: i7 I

' 5 i4 5 |

ARI 001 00

/C3 ANALYSIS•CONFIRMATION COLUMN

:l* : C : \EZCHROM\8H03\5H08.oZr'•*'f*r.r.ac ; C: \EZCHRQM\METHijD53\pcD.me1Samp la ;D ; ;M4354 no dii.AccuireG s 4u 09. 1991 OS:Sii5?

Channel A

5 - - 10

Minutes

HRI80IG!

PCS ANALYSISCONFIRMATION COLUMN

7i 1 3 ; C i \HZCHROM\8HOS\ 8HOS . 026M^tr -ci • •.; ; \EZCHROM\METHQDS\pcD . metSarcp-a ID : M4555 no dil.AcauirflG ; Aug 09 „ 1991 09: 1-3:0 -

O.OLJ

Channel A

0 5 10Minutes

ARI00102

='CB ANALYSISON COLUMNFile ; C : \EZCHROM\8H08\8H08 . 027MethoG : C : \EZCHROM\METHODS\DCD . metSamole :D s N4336 no dil.Acauirfsd t Aug 09, 1991 09:30:24Ooerator : - — — - ———— • ————

o

Channel A

'i « f . f2 5 n bji7

1 :

0 ,3 10

....... Minutes

AH 100103

ATiciM COLUMN•; '.: ; \HZCHRGM\8H08\8H08 . 023s -.-: \jEZCHRQi1\METHuDS\pco . mati i) * -M 4 S 3 7 <-> o d i 1.

---'.i:.r-r-^ -,,....c 09, .'.991 09s47:48

o. o ur

Channel A

ABI0010U

\J'-C2 ANALYSISCONFIRMATION COLUMN;:; \EZCHRCM\8H08\SH08. C*9C:\EZCHROM\PlErHaDS\pcc-niet; N*55S no Gil.

c 09. 1991 ;.0;0 :C7

ftRlOOlOS

PCS ANALYSISCCNFInMAT-CN CCLLMN

Fi I s •: C .; \EZCHROM\8H08\SH08 . 030."I tr.GG ; '.j s > hZCHROM\METHOD5\pco . met3<Affloi;=? IT s N4559 no dil.

rp»c ; Aue 09. 199.1 10:22:31

.Channel A

0 3 10

Minutes

flR100106

•'CB ANALYS 1 3IQN COLUMN

File i C; \HZCHROM\8HC8\8HOe. 031Mgtr.ca : C : \£ZCHROM\METHOD3\pcc . metSajr.oia -C - i456o nc; dil.Accuirec s Aag O9 . 1991 .10:39: 54

lhannel A

•• ;vj COLUMN

:: 3 \£ZCHRCM\3HOS\SHOS - 032- i \EZ2HRCM\METHOD5\ccb ..'net: Ni436i no dil.

i6

Channel A

O.OU 1 ' i10

Minutas

00108

Pkno ffittt . Time

":..S96 1.?T/,17 o--.,032 ::.20'?7';.2 2

.7004,9J6: .-032 2.6 612

0.e.,264 ^5^6213 9-::;,5:52 2144089 4. .748 A379BO

c • ^ - 092 1 £02290 3-V.: 7.464 £52735 :!.4-v ' 7»6£0 3619380 7

£..092 2924 0525 031.9 0

0

*fi100109

ANALYSIS

\i2CHROM\8H08\SH08.017\EZCHROM\METHGDS\DCD.mM4546 no dii.

Ana 09 , 1991 06 : 36 : 40

Channel 3

41 *

! •< "l. • Z 0i*)i 4M; * 4! I0 0

3 10

Minutes

Pkno '".£?•':. riiie Area

T 0-236 3930046 332 O.o03 10183 O3 0.768 66732 1'.'- 0.828 1397954 3:» 0.796 9218 06 1.072 2303899 217 1.364 28708 08 1.47A 15257 09 1.560 258810 210 1.716 9137 011 1.923 23439 012 1.992 46846 013 2.204 1142Q 01*4 3.028 42422 O13 3-180 37193 016 4,976 32301 017 3.336 3587G 018 6.372 379431 319 7.680 3605232 3020 8.904 17781 O21 3". 964 8233 022 9.232 22374 023 9.800 11374 024 11.740 7373 O

ftRlOQUO

FCB ANALYSIS

Pile is C:\EZCHROM\8H08\8H08.Q18: C:\EZCHROM\METHOOS\pcb.metID : N4347 no dil."

Acouired : Aug 09. 1991 06:54:03

Channel 3

0.4,

J

ji •1 a; *i j1 1N1 ;i '1 i

i <i!jiiji !io i

t

'4 j

42. iOi

,3 23

4

708

i

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J:*MU i

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;

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1

i

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i

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.:

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I5

6 9 ,7 2!'

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! i

1

ttI

:i iill. ii s ?i iilll'Jlll Mill ~. ,11 a a

•JlV"*JLWV

3 6 i3 64 « i

5 10Minutes

Pkno Ret. Time Area Arc A":

1 0.236 4236477 100.392 1672732 40.524 259362 10.616 352276 10.752 88760 0

h 0.812 117132 07 0.932 73140 08 1.068 2543408 69 1.208 129642 010 1.308 34898 0Ii 1.356 112926 012 1.552 134778 013 1.728 44922 014 1.316 16366 O15 1.916 30396 016 1.988 41732 017 2.204 80060 018 2.504 96099 019 2.680 6673 0

3.024 118016 03.172 94319 0

22 3.240 373268 123 3.436 434692 124 3.892 172678 023 4.032 1043966

ftat.. Time Area

3368306

^.33£ ""2936360 Sv.. 744 -90427 1/,.092 1036208 2:-..4O4 13:>69 07. ,472 158445 0•.--..c6a 3786477 9;;i,.J!:;6 2V4°3 0:-'...ft&0 7-1.2? 0.0.676 3112 0

ioo i 12

ANALYSIS

* C:\EZCHROM\9HOa\3H08.0l9

9 •;.;•:,-: a .5 : '•I454»3 no dil.--3'-:.irsG : rtug 09, 1991 07:11:22

V J4-

Channel 3

; I, i

i "

1 i l(1

J,'

ifj 1 •

(i

jf

t

1ai ^s;1:n !

11t4 |• , J

« ' 1 i f.

. 1

j i: ij ; s i t i • ~•. :' ' - . L ^ I '

i

•

,

i? o7 i5 26 4!

5 10

Minutes

ime Area

•L 0..236 3944O72 122 0.396 442772 1;.> 0, 24 166899 14 0,620 2099406 63 . 0.760 68537 06 0.832 1917814 67 1.076 2431194 88 1.212 79896 09 1.391: 115785 010 1.564 189386 1ll 1.752 40021 012 1.940 7049 013 1.988 33829 . 014 2.096 1366 015 2.176 63451 016 2.312 18078 017 2.324 113310 01.8 2.812 38991 019 2.908 17217 020 3.056 203112 121 3.236 787439 222 3.46*3 476679 1' 3.800 27133 0

3.920 214846 14.052 949703 3

ft*UQQM3 -

' kn o <~< e t.. T i me Area Area %'• r>O /•• •-»••-• (•s—' K:J..4-O :.;;./ *:,\J / •..' ..;j312 1406308 •''*

',.:'lc 4 R 720 930939 ."J;.:v -,960 1943503 630 5.04O ;?O0714 :"•51 l?..332 108322 0• •;;: ::.4;;>2 636006 233 ' 5.492 326287 1:..:;* S.816 15A7284 '=.35 6.280 1072953 3o* 6,. 572 3992990 12•>"" 7.112 256151 133 7.492 48618 0V-:' 7.680 3790416 12"40 tf.140 5819 0

*3.412 :l.02159 0<••'.£ R..756 1278 0'-••'$ 9-036 12672 0"-.-4 9.796 4177 O^S 10.684 660 0'>•* 11.396 4794 O

PCB ANALYSIS-.File : C:\EZCHROM\8H08\8H08.020Method : C:\eZCHROM\METHDDS\pcb.met „S*mpia ID : N4549 no dil. &.Acquired : MUG 09, 1991 07i2Ss47

Channel 3

0.471

• a

va I 's.1 !0

* 6i57

0.1W

Mi8 ' ;i l :3 . 4. 5 6'> il30® IriH..,- 2 22 2- 3 *4 *^:5 5 • •• -1 « »* ii * *** « ft " *TI 8>ii'|674 (Zsifij;? 2 *I 9^7 4 02 '^^ * i 9

»M** »fSS» I *h** 27 302*|°2 4 * °

3 9

i * I9 22 3 4

0 5 10

Minutes

l"*kno Ret. Time Are* AreA^

:i. 0.236 43O8160 292 0.388 612480 43 0.612 131911 14 0.760 84269 1•3 0.824 312850 26 1.072 2383698 177 1.204 82720 13 1.304 13370 09 1.360 73278 010 1.484 27666 011 1.560 176943 112 1.692 2320 013 1.728 2310 014 1.764 1488 O13 1.848 5471 016 1.924 21994 017 2.208 32539 . 018 2.496 89418 1

2.632 13394 02-. 932 240O 0

21 3.016 134158 1£2 3.176 81259 123 3.472 22221 024 4.028 22737 023 4.220 - 23368 0

(•-•.no :•<<•; x., Time* ttrea

2:14501162731439801368711397750

7.396 153 O<'.49 29206 O7,.680 3735296 23i:5 ..692 15394 09.,023 4378 0•?.,844 51388 O

A R I O O M 6

»C3 ANALYSIS

i: : \EZCHRQM\SH08\SH08 - 021C:\EZCHRGM\METHCDS\CwC.mer.

0 r.o dil.9, 1^91 07:46:06

Channel 3• if'• I '•

' *! Ii i ! i^i 3 5* I fl i

i • '

•

f1

i!.i

i I

00i t ^ ' ^ i s a 8 j ^ I ? t49 ;: ••• I* ° i ' 4! U* y fii ' A | p . * 0/f o* 3

flQ *3 #9« g ?!

Minutes

F.e T. ., T' i me Area A r e&"i

, 0.236 4157774 182 0.664 3972 O

Q-744 89196 0•'i 0.820 879408 4::. l.OOO 20749 0

1.072 2579543 111.208 155993 1

$ 1.308 11448 01.376 99267 0

10 1.560 381347 211 1.708 ' 2(3840 012 1.800 2894 013 1.924 43900 014 1.980 36223 0IS 2.196 54231 016 2.504 91491 017 2.824 46469 018 3.032 232651 1•'9 3.16(3 353S32 2O 3.336 39716 0

3.772 117643 122 4.844 15009 023 4.960 270647 124 5.444 2642 023 5.536 88979 0

i"'k.no K:4>t., Time Arm* Area":26 •,':.. vZ2 3920627 f>».L(J4 1417157:3 6 ,,2.92 571312? 6,536 716180630 '<• .£76 500S531 7 .,220 A1506Q,:;2 '-..6'!i4 376898833 V,-360 3208134 ,:i,,234 45192235 9. ,656 9386936 V.540 473037 9. .740 218503 :l.:;ra 9.730 i324ia i39 9.904 134382 10 -'.0.640 1.330 0

4'i. :.0., 7/ 11823 c4377 O

ARIOOU8

PCS ANALYSIS

: Cs \EZCHROM\8H08\8H08.022 ,.~ ^: C:\EZCHROM\METHODS\pcb.met £./**T'<? "" f

:3<*mole ID 4 N4551 no dil. *^Accuired s Aug 09, 1991 08:03:35

Channel B

0 0

o,. o U5 10

Minutes

'-•no Ret.. Time Ar«* Area";

1 0-236 3962886 282 0.468 18354 03 0 - 588 8006 0£* 0,664 1156 0S 0.728 8O416 1

0.820 1488112 10 .7 0.996 2826 03 1.072 2458217 179 1.312 4929 010 1.368 59893 011 1.464 12944 012 1.560 237722 213 1.720 4996 014 1.848 6389 013 1.988 80607 11.6 2.204 71764 117 2.304 133439 118 2.82Q 96333 1'9 3.012 128321 1

3.172 85327 13.304 32767 0

22 4.364 33109 023 4.964 939O O24 3.328 32749 023 5.892 330 °AR 1

i-.no

26

2358778330

393S530 28W,o9£ 118 0'-'..636 36030 09.680 22377 0••?,8i6 £60296 2

245:!.1365

AR100120

PCS ANALYSIS

il-u : Cs \EZCHROM\8H08\SH08.023rsr.r.o* ; Cs v-^ZCHROM\METHQDS\Dcb.met'':--u:ic is IJ i i'-4552 ."in d i 1."icuirFsa .' A,ig 09, 1.991*"08:20: 5£

Channel 5

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Pknc !",et- " :i.me Area Wrt-3«i"i

O.i'38 1.693 00.236 4381470 60.396 3704327 S

'-'• 0.*.£8 459149 13 0..620 1O754339 3.6 0.768 107937 0y 0.816 124009 08 0.932 99581 09 1.076 2686560 310 1.208 98428 011 1.320 68726 012 1.364 88177 013 1.438 63747 014 1.360 214691 015 1.764 68437 016 1.848 27803 017 1.936 327263 018 2.212 234005 0•"P 2.39.fi 17812 0

2.312 357614 02.660 107522 ' 0

22 2.896 280539 023 3.020 234498 024 3.232 1000736 14l 3 On^/4^ J>* *tw\J/iL jl __. _ • A .... ftfiiooiai

'-' kn r> t:;' •:# t H Time Are & A r e a. "i

2± 3 ,,804 126237 027" .'.j.,924 533799 i^3 .,056 2484062 32? 4 ,.232 2737737 430 4,516 5214529 73.:. 4-638 1211593 2::: ^,732 23O1784 333 --.t-964 6173513 83^ 5-064 4859074 6o!:. 5 ,,323 703622 136 5..46O 31S2199 437 3.488 2361362o3 5..824 116450385'? 6..292 818833040 6..534 1685529 2'1. ..794 1176849 2'•2 /,.:;. 20 2250313 34"" 7 .3G4 :1792 0A4 7,. 500 339300 045 7,692 37628515 5••'6 '::? . 2'.'2 8620 047 S .412 17041. 0<^o tfa,£4 3526 0

ARIOOI22

PCB ANALYSIS..Fila ! C:\EZCHROM\BHOS\8H08.024Metnoa : C:\EZCHRQM\METHQDS\pcb.met:Samola ID : :M45S3 nc Gil.f^cauired : Aag 09, 1991 08:38:19

Channel B

0.4

O.. 31

i 41 |i ii

4j^41i

f it i

IIi

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i 1 1; a 9 ?W 9 « 0 1

G, , « ! « , « • *

i A iTIi ^ • 2i %5^ • *

/ V t1" " .

; 3i650 A 3 3I 205EO « * 2

3 10

Minutes

kno Ret. T i me A re*

1 0.240 4206720 62 0.396 3374266 4- 0.528 316444 04 0.624 467159 1S 0.760 60536 06 0.824 9O18B 07 0.908 45(387 08 1.080 2588739 39 1.216 82026 010 1.312 13657 011 1.363 59449 012 1.300 23604 013 1.368 110250 014 1.724 9712 O13 1.896 8418 016 1.952 16392 017 1.996 367Q1 018 2.328 270357 0',9 2.672 4757 0

. 2.808 138828 021 2.908 63620 022 3.076 139458 023 3.256 1310816 224 3.480 1700813 223 3.812 203331 0 flfi | QQ | 23

Pkno ;et. Time Area Area";

2-6 0..904 912636 127' '•'• .048 2869954 4

47514G? 61160532 J.:

-,740 2619403 J<,V64 6364197 8'-,.064 4410793 6:::...336 690781 1..-*60 3471419 55.30A 1781903 25,700 328244 l,. 24 10429461 14A. 292 7901603 106. 580 1783674 2

'••:;. 6. -,7PC' 1113168 14i.: 7,116 2237396 343 :%496 3782A9 044 7.6S-3 3685205 545 :.;?,,7:l6 930 0^•6 -% .':;:::.2 20728 £^'v '-'M;\JC 5992 0'•is •"' .:-»6c: 3020 o"t? y,4!" 2 1102 05.; '-•' .6-/0 2683 U•;.:!. -,96^- 697 O;r2 :.0..0ro 7103 053 10 .334. 2312 054 11.852 4074 0

ARIOOlZd

PCB ANALYSIS

Cs\EZCHROM\8H08\SH08:023~; \EZCHROM\WETHGDS\pcts, met

:• : H4334 no ail.s fi,.jg 09, 199.-. OS l 33 a 3?

Channel 3

i '! !\ \l! ]|: *4

••i i JJ \"*!* i0 13 tA CIn iH"!-j | i

• !l;• i r

• i.;i21 jii

; !!i MI *Mil!- . I ' i o i: i.ii!!

1 *j T

1 ^*J f 1

1 ;!iii ;

ka!

2

1: : 4BiJ^iJijgS^ yjjijjp"!oiil .tlb W.•j

ii !)'!fl M3il :4H1) !

?i 90u 041 1! 4iiill '!|ij1 i;i iri i!i!

11*

3!

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2

l l 1 !. ' t

4

32'C3 8

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i'«*31

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ao

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1 i

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,

358 M'O 05| 78 ,. ....i .. ! 3? * 480 5791 ! 79 5 77 ? • 8373 J 22 4 6 2 2 4226 . . t r ! • '..yj.j-' • • • • • • j

.L;/;.L.... ..-———-3 10

Minutes

Kno Ket. Time Area rtreA?::i. 0-148 S559 02 0.240 4208729 , 23 0.396 , 6392437 3« 0.528 664840 Oh: 0.620 1051665 1& 0.744 74146 07 0.820 94237 0B 0.900 66173 07 1.076 2543734 110 1.212 117067 011 1.364 60573 012 1.492 49378 013 1.560 116139 014 1.736 17336 013 1.904 11143 016 1.936 8307 O17 1.988 37438 013 2.176 20738 019 2.304 23271 020 2.40,4 4041 0U 2.520 370358 0

2.644 4766 O23 2.796 137438 024 2.900 : 63330 023 3.028 J 94232 0

ft*100125

F' kn o K'w t . T 1 fne A raa A r a a":23 3-108 34236 02™ 3 ,.248 ££82593 :Lv:S 3»4c£J 3694803 229 5..7S3 1921/12 030 3,904 ;!.B98847 :l3:1. 4..044 7242301 4• •'2 4,,:;2£ 'J232907 433 4-SGtf 13A22129 834 ^i../24 10414519 ^

1.9432382 10' 14283374 7

37 5,324 2345521 139 5 ..436 10630717 539 ?.,496 S9A2711 3

5.816 34777020 IS6..2;;K) 2 20(3108 13

"3 .772 4089702 2•••• ^-.108 7404026 4•-:•> 7-4^8 .i. 17 5603 1^-i •-.,676 3732671 24';- 7. .9 72 2492 03 -"' - :.36 >!336 04? S.,624 2418 0^O -:j.&72 9439 0.;. c:-,,?9£ 2080 0:-2 V..404 4473 033 9.676 3327 054 9.1372 1385 03S 1C -092 791 0^6 !0.5tJ4 1 83 0I:.'1? 10.732 3014 0

PCB ANALYSIS

Filtt J C:\EZCHRQM\8H08\8H08.026i e .hoa i C:\EZCHRQM\METHQDS\pcb.ma-c /):-=«mpie ID : N4355 no dil. t/1A-auirea ,i Auq 09, 1991 09:13:04

Channel 3J

i j

°"1iji ^ (

0...3Ji ;

I . i1 . ;

,. ... f ii

'

O.lj ti ;

i l l

o i. i6 i: 7•• i

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i s l24 '

1 i ' • • * •51-* i ••• • 't • .,?5 7T013C 8 v

nMiVl. . i«»ii«.L''A i vi

v

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V

111

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J

1i

7

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1n 0 ft

6 '• I i 5! I i| 3 2 *

, 1 . > .. .

J!W#W5

Minutes

'kno Ret. rime Are*

:i. 0.236 4380837 7£ 0.396 3424197 53 0.328 414077 1•4 0.620 957983 1S 0,752 76333 0> 0.824 143053 O7 1.076 2632063 48 1.212 87649 0'? 1.306 13792 0

:l.0 1.368 68790 011 1.444 13949 012 1.496 28846 O13 1.560 107088 014 1.748 23319 013 1.900 13340 016 1.992 80517 017 2.092 18034 018 2.180 38346 019 2.314 12366 0

2.432 8014 02.524 81893 . 02.808 17404 0

23 3.048 47161 024 3.236 392743 123 3.472 843590 1

ARIOOI27

c'< e? t • 7 i me Area

*•*> 3.792 ' O. -;i5610:'". * 02/ ;S,.72O 359748 12tt 4.032 1968720 ^27 4 H 232 2193617 ~-0 4.512 4304665 73::. 4.729 2915722 432 3.960 S044134 833 '7.060 4098175 6

5223007 n

;:> 6. .23® 6907818, 1337 6.380 1137613, £33 6.780 983620 ?39 7.116 1910429 340 7.496 280682 O41 7.ASS 3646287 642 8.568 14029 • 0•^3 9.128 3S39 , , 0

9.912 1014 0::.0.824 3721 0

PCB ANALYSIS•

Fila : C; \iZCHRQM\8H08\8HOS-027: .:: \EZCHROM\KETHQDS\ocb.mat

•••-•naL- irac ; r^ug 09, 1991 09:30 :2

Channel 3

.,,.,> t

!t :t1 i' 11

1 1

! *<t i! as:! 41'; 414! S!i !,!! II!; 11!. >) ?

i< ti 1: T( 2i: !

J i

1 . !*«. ;

3J

3 i' 02 V* j0 !f

t

r

ii!t

3fji V

i T="il ;1 U»• • VnS 7 903 t l»& i m

ttl

i:i:i •13l*32$ii;1 !|»/ii

5i804

;ii

6

248

1:|7 9* fo j

J i1 1 7:

ii'

. ! :.. ; f ;

o .o..o. '

o i ;i9 7 |' * !

31. ; i : i ' -i: ' < i i t j j i i i i i i MA ~ *i

k.no Ret. T irne rtrea

= • 10

Minutss

1 0.240 4223713 4i2 0.396 - 4467822 43 0.329 593852 1^ 0-620 1413401 1* 0.764 109396 0& 0.828 611010 17 0.992 14912 08 1.072 2507081 29 1.36Q 36222 010 , 1.460 17963 011 1.33A 164920 012 1.696 ' 1130 013 1.732 21773 014 1-832 7O05 013 .1.884 7934 016 1.980 89493 017 2.034 1967? 018 2.168 70642 019 2.300 34460 020 2.420 13861 0 , j21 2.516 186368 022 2.792 97402 - 023 2.896 76107 024 3.016 26223 023 3.112 ; 39306 0 100129

ijV "3 R w t» T .i me A re«i

26 3.240 1132011 '' :l.2" "25° 1737635 22o 3. 7SO 64664 0£* ..J.904 775781 130 4.040 3625872 3H 4.216 4120443 432 4.300 8033602 73S 4.716 5361189 3;'S4 4..944 ,.- . - 95688O7 - 9»3S 3.044 7644833 73& '5.312 1098393 1

. 444 5339074 3,480 3213057 3

39 5.804 18988896 : 1740 6.268 13539223 ' _ 12*1 6..352 336022 0^V- 6,760 1913058 ^ ' ' • 243 7-092 4342977 4** "''-.472 713312 • ; : 1^ . ••'..660 4032260 : 4*<•- 8.0A8 3113 * 047 S.**S2 9173 : 0

a..664 - 6-137 , - 09.300: , - 11061 0•-.616 . • 29896 0•'"•-500 V '234916 : . - 0

'I ' f'\f.'.f - *i /-%-*«*** ' .*i.v.y^2 ; 13o9 • • 011.760 1638 0

-A£

PCB ANALYSIS

File s Ci\EZCHRQM\SHOS\6HOa.028 „netnnd : Ca \EZCHROM\METHODS\pcb.mst Q.Ga.r.Dia tD s MAS37 no dii.Acauirao : Aug 09, 1991 09:47:48

Channel B

Minutes

Pkno Ret. Tim©

1 0.236 4203353 52 0.392 3661893 43 0.320 ' 425273 14- ' 0.612 1067472 13 0.760 71769 06 0.816 398832 07 O.984 3361 08 1.060 2454237 39 1.340 22938 010 1.54* 160063 011 . 1.724 12031 012 1.852 4943 013 1.908 11764 014 1.968 44737 013 2.068 3678 01.6 2.148 ' 10783 017 2.232 467 018 2.288 14040 019 2.396 4881 • 020 2.49<£ 110476 021 2.648 4442 022 2.772 43182 023 2.872 17377 024 3.008 51138 023 3.220 818232 1

flR100131f% *« •« •

'ime , -Area , , ^re

26 3.436 1226200'"-764 36451;-•??? ,. 55578l•'v. Olw 2633243••*,.:!.<;> A 3050021'-.476 :J84678S•in 638 3807677 " ' ' 5•<v.,920-~ - "5 89903" Q• .020 33S6S71 75.;iS4 649159 l£.416 6005308 " - 75-730 13084311 . 16•:>-244 9223202 --' 116.536 879986 ' - 10../32 1257731 - 27 .068 2999852 47 -.- 8 "63973 - 1/-6J6 3643324 ' 4J.392 3331 :oS: ,456 1035 01 - - "i 27300 0

- 220308 02830 0

6R100132

PCB ANALYSIS

C:\eZCHRQM\SH08\8HOS.02?C:\EZCHRaM\METHOD3\pcu.met A: (\4538 no dil.

i 3ua 09 , 1991 3.0 : OS s 07

Channel B

••.!

, t

\ ^

"

! 1

ll

!!;i,

7 ',a:

•I1| M0 0$$f dh

i

1ifri

ii]SItt$• tN2209

i

f*

rii,f30

I

6

fe|4BH

& 7

s iaIL i •'

i M j jfjs i'Jia **• ioUiji w

5 10

Minutes

Pk.no ftet* Time f^rea Area--:

:i 0.236 4O86333 52 0.392 3601909 43 0.520 * 440534 14 0.612 1078140 1'j 0.760 10O643 06 0.320 512117 17 1.060 2407114 3a 1.196 46981 09 1.296 541 010 1.348 31630 011 1.460 4118 012 1.544 163968 013 1.712 26089 .014 t.832 4414 013 1.964 74822 016 2.148 66284 017 2.292 20314 018 2.408 9963 019 2.300 152363 020 2.776 96905 021 2.8*6 74443 0 vv22 3.068 104344 • 023 3.220 987873 . 124 3.440 ' 1307236 223 3.760 63191 0 . 33

I v w .* **

_3.880 " 5578604 - ° l •'•' 6 9 ? *? 1 6;Hf* 3040073" .3941600-

'f- 7170513»"020 S299596o-^SS 681984

5"472 1849552"•780 'L33249236-r f? 9417847

190261613083393048309493400384X968

2* £22 ' 2579 :-?.8/2 ;- (5575

9 4 ,y.540 " • •n R.-t -»XA • f *-J*J^W'.-*-760 227400

PCB ANALYSIS

File : C:\EZCHROM\SH08\aH08.Q3Qa : C:\EZCHROM\METHQDS\pcb.met* ID : ,M4559 no dil.red ; Aug 09, 1991 10:22:31

Channel

V3

t3

Pkna Ret. Time Are*

1 0.236 , 4076223 62 0.392 2224733 33 0.520 390717 1O 0.612 2234259 3-I 0.844 991982 1A 1.06O 2437025 47 1.1*2 34141 08 1.369 103063 09 1.340 93378 01O 1.74O 37440 011 ' 1.832 11310 012 1.960 116608 O13 2.076 20694 014 2.148 143367 013 2.288 66431 016 2.396 45496 017 2.496 126722 018 2.780 73776 019 2.880 61322 020 . 3.220 787173 121 3.436 92O012 122 3.760 23273 023 3.888 333727 124 4.016 2073923 323 4.196 • • - * 2324328 3

Pknc i-::o . Time , Area

-.476 4466819 6•••f.6£>3 3105340 a««V^4 5121790 7!;..020 4560331 7;5™42O 5642075 3:..780 10410340 156 . 244 602072 1 1i.532 1261433 ' 26.732 1063870 . 27.068 2173259 3y.448-- -338938 - - 07.636 3638317 5B.I 12 262 O

=jzr;i=l7-i'!^r:cN CCLUKN7 :. 1 ^ :;: \aZCHRCM\SHOa\a-HOS . '-33

= sm.;:a L2 : N4362 1/40'•••"•=--i:-sa • ;-:i.ic O9. l?9

Vo

0.1

y.oU

:- han n e I

5 10

Minutes

FC3 ANALYSISCOLUMN

il* : H: \EZCHROM\EHOS\SHOS.034I'l tnuu : C: \iZCKROM\METHOD3\pcb.metE^mcla ID s ,-j4e63 1/40Accu M-ec :- '-ii..io 09 , 1991 ii 831 1 39.3 OP ra ror :: ——— - —————————

Channel A

:•i

•

i,i

_. _. . ~. -

< <*7! :i ;' 1\f!•i <it 5 iit , , 1: 7» • 6 Ii :

I!4 • s |ii s! !j *!' * •! . !

.

\

-

•7 \•t&8•ii01 7Q 7! ;

5 10tfinutes

PCS ANALYSISCONFIRMATION COLUMN

File : C:\EZCHROM\8H08\8HOa.035fret he c s C:\EZCHROM\hETNuD5\pciD.frei:•Same Is ID i N4564 no dil.Acquires s Aug 09., 1991 11:49:20

Vo

Channel A

flRlOOl39

U-p. .iMALYSIS...n:\P-PiflAT I CM COLUMN

'"i 1 .:- .- :; : \e2CHROM\3H08\eH08.036rethad i C;\EZCHRaM\hETHQDS\DCG.metja^cis ID f . *S65 r.a dil.

09, 1991 12:06:44

Cnannel A

O S 1 0I * •' I • *"' -

Minutes

AR1001

:'C3 ANALYSISn.NF': NATION COLUMN

i * • C : \£ZCHROM\8HOS\BH08 . 00 tf:,fr.!v::-a ; ;:: \EZCHROM\ME7HODS\oct .meti anno. .= r.) 5 1242 <a 0.2 ug/ml• ccu-.rsd s ;^g 09. 1991 "04:00:22

\

Channel A

AR100 It* I

;CE? ANALYS I S COLUMNFile ; C:\EZCHROM\8HOS\BH08.007rtstpoc : -! \EZCHROM\METHODS\pcb. metSamol* ID : 1242 € 0.5 ug/ml

ed : Auq O*. 1991 03i42s59

I J>.4

0.3

V 1 i

? !li ,Ji

0.0

Channel A

RRIOOU2


Fila s CJ \EZCHrtGM\aHOB\SHO8. 006Method ! -i \EZCHROM\METHCDS\pcto. martSample ID a 1242 Q i.O ug/mlAcquired i Auq 09. 1991 03:23:37

V

.

0.

0.2

o.ii

Channel A

o.oLJ

-'CB ANALYSIS"O'^'i^MATTON COLUMN

": '.- ; C:\EZCHROM\SH08\SHOe.003?••••*+.••••~J? s Cs\EZCHROK\METHODS\pcb,mat

-? iO s 12iO 'S 0.2 uq/ml-EC ; Auq 09, 199t '03:08:13

'-'re-a ".c:- ; ———-—————————

0.1

o.o

Channel A

0.3

64

4

.':../7.'•*;£ inS r v:i:r8itt!!l ?it f-02 4,-

;0 3

Minutes

/

*CE ANALYSISCONFIRMATION COLUMN

,Kvl.= : C:\EZCHRaM\9H08\8H09.004Mstnoa : C:\EZCHRaM\riETHUDS\ccb.mat

e ID : 1260 (S 0.3 uq/mlir*ri s Pag 09. 1991 "02:30:57

Va

0.0 -f

Channel A

ANALYSISuONFIRMATICN COLUMN

File : S:\SZCHRCM\SH08\8HOS.003: C:\EZCKnOK\METHODS\oco.metID s I2i;0 3 1.0 ua/ml

Acau'.irec : Au-7 C9, 1991 'O2i33i34Qoersircr s ——-————•——————

Channel A

• * i

Minutes


File : C:\EZCHROM\SH08\eHC8.009netnoc : C: \l£ZCHROM\METHQDS\pcb.metSa/nole ID : *CB«ur..131/.206Acnuirso =' Aug 09. 1991 04:17:40

Vc

(

0.4

0.3

0.2

0.0

0.100

J

Channel A

yO - g - 1O

Minutes

COLUMN

Fi i- : Ca\eZCHRGM\SH08\BH08.010e-.--c ; C:\EZCHROM\METHODS\ocD.met

3*;f\a.>.e ID : PCBsur. .075/. 103Aca-.ir*d s Auq 09, 1991 04:35:04Cp^i—^T'S;— " -*———————^——————••

O1.

! 4

0.1

O.O v-

Channel A

: n•• I! 3 7

56

0 g 10

Minutes

U-8

FCB ANALYSISCONFIRMATION COLUMN

Fiis j C:\EZCHROM\8HOB\3HOS.01iMfttraa • Os\EZCKRQM\METHGDS\pco.metS&ir.Jie? ID : PCBaur. . 037/ -0513^C3u*rnd ; Aug 09, 1991 04i52:230jsrs.tcr •. ———————————

1 ii

! )! *

0,3

1 ! l!

0.1

0.0 J

00

68il02

Channel A

0 . . . . . . 3 1 0: Minutes

. "-CB ANALYSIS^CONFIRMATION COLUMN

Fils s C:\SZCHROM\3HOS\SHOa.013Motnod s C:\EZCHRQM\METHODS\pcb.metSample ID : Spike iAcquired s Aug 09, 1991 05«27:08Operator s ————————————

0.31

o.oU-

Channel A

3 - , -: 10Minutes


FUs : C:\EZCHROM\aH08\8H08.033na^noa : Us NEZCHROMXMETHODSNpco.metSample iD : Spike 2Acquired s wug O9 , i.991 12 : 41 : 23Operator : —————————————

o

0.4

0,1

Channel A

s5 02 08

3 10

Minutes

"C ' ANALYSIS6NFT ATION COLUMN

Kl2 ; Oa \EZCHROM\SH08\8HOa.012-ler-rc : .-! \EZCHRGM\METHQiJfci\pcD.metS*.7»;,i« ;2 : Jil BlanK t.•-,-q.;-_:-??:: ; ' O9. 1991 03:09:46

; U' 'ii i

J-t

f~* ' '

•r

0.0

'i80

Channel A

0 3 10Minutes


Fils : :iVEZCHROMXeHOS\SH08.037fretnoc ; Cs \EZCHROri\METHGD5\pcb.mot-3a;i:Dls ID s 3il Blank 2A-.3uirsa :- Auq 09. 1991 ;2:2*r04.»j *J ~p- ' W u. I—J i ,»

Channel A

3 10Minutes

fiRIOOISS

INITIAL CALIBRATION

S

1iTESTINQ LABORATORIES

ORGANIC3 INITIAL CALIBRATION DATA

Instrument rn g ____ Calibration Pat* 8/S/9/

Lab File ID: RRF Is.RRF 4*.

COMPOUND '(IT.

1

i

i

V ;

——————————————————————— | ————

1 '

•

b 1,

'- ***•-.,.;! ^

\

——————————————————————— I ————l

1

—— ————— _ ————————— — ——— 1 ————1

^ '

——————————————————————— t ————

O.£

RRF1

•

™SE

RRF2

•.»

.. - -

:

<.-*

',.'

i

;F 2= _ £F 5=

RRF3

•

_

•

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RRF4

: " ;'

,

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RRF 3:

RRF5

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PCD ANALYSIS

.atrssa ? -:s \EZChRQM\METHODS\Dca.ir-oia ii: i t242 £ 0.2 uq/Ttl ,

09. 1991 04i<xi;

.'-hannal B

V

0 , , , 3 . . . . . . . - 10

Minutes

knc ' ..:-;et.- Time ^. _. Area . . Area?i , . . . . . . .

1 0.232 1931396 42£ -0.372 17969 03 0,472 32827 1

.^i ... . ..0.752.;., ... 12144 ..... 0 .- , .t;> Q.79A : 27197 1£ 0.384 11098 0"7, " O.V92 ,-- 33833 1

10843 O. 13884- . o - - - - - - - - . . . . . . . . . . .

10; t.4CSS . 113299 3 ;11• in34& 21863 '0IZr'V"- 1..72C . 134344 J '" 3"'"-13 t.824 18083 ; 0 :1^1 ...........1.928 -—'- 121333 = • - • ' - 3 , , .- . .. . .13! 2.048 20368 : 0 .16 2.128 383324 • 817 ""•*"'2.268 "" 172363 ' ^l V 'ia; 5J.372 139923 319 --------2.492- - 204463 4MO. 2.736 133493 : 321 2.864 ' 137880 322 3.O64' 37361 1 , -23,: 2T.200 249332 3 i24— - -' 3.476 - • 216253 - - 3 - - - - • -23 3,844 13462 0 -

ime Area.

RR

PCS ANALYSIS

File s C:\EZCHROM\8HOa\8HOB,007hotrod : C:\EZCHROM\METKOD3\pcb.met•jamola *D i 1242 £ 0.5 uc/mlacquired : Au-g 09. 1991 '03:42:59

Channel B

0 S 10Minatea

'kno Ret. Tima Area ATOA":

1 0.232 1889316 182 0,372 16719 0o 0.468 31419 04 0,640 3037 03 0.736 16621 06 0.792 41832 07 0.880 .3389 0tJ 0.984 72817 19 1.17* 34881 110 1.249 < 49936 011 1.40Q: 311971 312 1.35* 53101 113 1.712 397896 414 ' 1.812 38685 113 1.916 329548 316 2.036 64622 117 2.120 999232 1018 2.260 423730 419 2.360 378741 420 2.4QO 380644 621 2.740 423726 422 2.8<8 493O70 323 - 3.048 360298 324 3.180 775689 723 3.456 620854 6

Pkno Ret. Time Area Area";

6 3.732 107077 17 J.320 . 16O608 28 2.936 Io8744 29 4.24S 270338 30 4.684 78130 i1 4.904 73338 12' 6-500 1054226 10

.53 6.e)48 ...24970 -,...- 04 '-"- - 7.i308 367 03 7-852 236 06 7.988 439 07 8.820 2431 0

'i;.7B .--MAUYSI3

=• h a •!;. ; • ; \SZCHRCM\SHCa\8HOB . 006

: 1242* & i.O ua/mlL-.q 09 . 1 99 .1. 05 : 2 S : 37

Cnannsl B

0,44,

'•ii?!l! jiiiSMito™!i:U gs|4ii*JH!|!p|

Are*.1 0.156 6188 0^ 0,232 1717230 11:; C.464 , 32751 0* 0.736 12321 0::- 0.792 25779 0& 0.88O ,4304 0

C.90O 31061 0& 1.135*. 58309 09 1i.24.fc- 92390 110 t.39-4. 606650 411 1.3fi«r 77081 01.2 1.712 749861 313 ' 1.812 103932 114 1-916 645761 413 2.035 126977 116 2.116 1830764 1217 2.256 856550 5IB 2.336 706479 419 2.476 1108592 720 2.740 766810 321 2.8*8 940160 622 S.048 393908 423 3.184 1430432 924 3.436 1191343 823 3.728 164969 1

3 10Minutes

' kn o Ret . r 3 me Area

,--a ,.8?6 6 0276. 504 714374

ftRIOOI6l

ORGAHIC3 INITIAL CALIBRATION DATA

Instrument TP ^ Calibration Data

Lab ?ilo ID: RRJ Is.RB? 49.

COHPOOOT 'AX/?M / ? '£7

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PCB ANALYSIS ... ,,

File ! C:\EZCHROM\8H08\8H08.005Mstnoa : C:\EZCHROM\METHODS\pcb.met

ID t 1260 S 0.2 ug/mlad : Aug 09., 1991 03:08s 15

Channel B

V•TJ1

0.4

0.3

0.2

0.1

0 -. 0

<i:;:!ijij

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0 '*'*j/o°! ii 2?* j - i l ieItf-9 •• i1 i --a5 °<1»?97 54 3 * 7854 8VS744 44 '4 J 44 U A* L9*L fa 7 B .A A f 1 A

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Pkno Ret. Time Area ArraaM

1 0.232 1930277 162 0.372 17523 03 0.464 ' 38431 04 0.636 4818 03 0.724 24724 06 0.788 41594 0? 0.876 6834 08 0.984 43465 09 1.176 68369 110 1.364 28555 011 , 1.664 16546 012 2.992 111297 113 3.136 268071 214 3.408 182139 215 3,744 47784 016 3.840 84358 117 3.980 341717 318 4.156 347740 319 4.440 535653 420 4.6#8 434336 4

4.892 945112 34.952 628278 5

23 5.232 76321 124 5.380 646943 323 5.744 1289687 11

3 10Minutes

m n I ftfi \ &

PCB ANALYSIS

rile * C;\E2CHROM\8H08\8HO8.004: :J .EZCHROM\METHODS\pct:. ro*J : l^&Q & 0.5 urj/mla s *'.iq 09, 1991 "02:30:57

Channel S

3 10Minutes

<n o Re t. r ?. «ie A rea Area?-;

.1. O.I&52 2C60206 9i* 0.304 289928 13 0.372 4 213661 1'* J..463 287364 13 0.632 41204 06 O.728 52338 07 0.788 85591 0CJ 0.876 16128 09 0.984 67333 010 1-i?* 32705 011 . i.464 1757 012 1.336 32370 013 i.660 14569 014 2.736 33536 013 2.964 121571 11.6 3.172 336921 117 3.396 349440 218 3.728 14416 019 3.340 124049 1-0 3.97 752902 3

4.152 804301 44.432 1401347 6

23 4.644 1077876 524 4.880 2005780 925 4.968 1638261 7

F'knc Ret. Tim* Area•" 236 189022 T372 1O39133 3400 699623 3736 3339328 13

30 6.194 2520479 1131 1.4*38 1873016 832 2*.676 317062 i.33 7.,024 603931 3"\4 7.400 169730 I.%"• 7.604 17575 0'36 !:?.648 '418 0o/ l1.284 543 0

PCE ANALYSIS

File : C:\EZCHRQM\8H08\8H08.003Metrod : C:\EZCHROM\METHCDS\pcb.metSample ID s i260 S 1.0 ug/rol

ad i Aug 0^- 1991 02:3-3:34

Channel B

Minutes

Pkno . Ret. ™ime Area Area?:1 0.232 1831037 5£ O.372 221O6 O:$ 0.464 39595 04 0 . 636 4974 03- 0.724 23228 0A 0.792 45160 O7 0.876 7437 08 0.984 4O576 09 1.180 66324 O

.10 1.346 3033 011 1.576 28413 012 1.672 9853 013 1.680 7431 014 2.124 19146 O13 2.468 28833 016 2.760 11028 017 3.008 132349 018 3.180 637174 219 3.412 321251 120 3.732 22882 021 3.834 260366 1**.2 3.992 1437884 4

4.. 164 1529205 424 4.444 2583724 725 4.656 2039764 3

00*67

::st . . Line Area

•'"-. 396 3 32 i 979'• -,V60 303 76-

.-V-'

3214173

',.. 04 3343949 9::..o?2 726976 Z7. .036 '..262923 3:•'.- ':!.o 340612 1''. O-a 25397 o•;L,; o 34497 0


Instrument TP Calibration $1% 1%

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File : C:\EZCHROM\SH08\SH08.0O9C:\EZCHRQM\METHQDS\DCb.met

v ,'-amr,i.s ID : PCBsur. .1517 .206^^*4--cuirsG : Ana 09. i991 04:09. i991 04: 17s40

Channel 2

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5 - 10Minutes

Pxno Ret. Times Area ^ ,

-. 0.232 3937041 242 0.364 13727 O3 0-640 3554 . 04 - 0.740 8333 .- 0

. S 0.792 l 20322 . 06 0.876 3272 O"' 1.O40 4330395 < 288 -1.32O lllOll 19 1.524 19013 010 1.944 45434 , 011 2.96B 3540S ; 012 3.13S 54574 " 013 - 6.S08 385664 214 7.436 60334 , O13 7.608 7189929 4416 8.520 23467 017 8.600 900 0i8 9.220 692 0

/

C.: \iZCHROM\6H08\SHOS . 010w:\ezCHROM\METHaDS\pcb. mat: :-'CSGur. .0757.103

: M.ia 09 . 1991 04: 3£ : 04

Channel B

:' il *v .. • it ,« ". ii i ,>» A i i I A3 3fa , i i • gi et *- ! i i 3 T

5 10Minutes

r~'kna 'rft. Time AroA Area":

1 0-232 3S02316 36l: 0.468 14226 OJ 0.564 6383 04 0.748 5742 05 0.788 ' 6225 06 0.884 2502 07 1.040 2532294 26W 1.324 56452 19 1.328 9419 010 1.946 20962 011 6.3&& 39338 012 7.6£2 3333489 3615 8.668 2272 014 8,804 1647 015 9.372 3025 0

s

-B ANALYSIS

s •-: \S2CHROi-t\METHODS\r; - -CB-sur. ,037/.OS1

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S 10

Minutes

PKn J Ri*t . Time Area Area":

3073247 5111215 O

Z 0.748 6208 0a 0-788 v 10044 0b • 0.8UO 2811 0A 0.972 6710 07 1.036 1186343 20S 1.316 12737 O9 1.33S4. , 13061 010 .3<M' 62431 111 7.6Q0-- 1657373 2712 8.772 1117 013 ' . 8.892 1272 0

173

MATRIX SPIKE/SPIKE DUPLICATE

TECRNttttt*Tfc§TINa LABORATORIES

TECHNICAL TESTING LABORATORIESA DIVISION OF COMMERCIAL TfSTlNQ * tNGINECRINO CO.


Roy F. Ueston-Delran, NJ/Murphy, Marian Laboratory Number N4565 RespectfullySubmittedi

STA. «31 TRANSFORMER Date Saapled 08/05/91 12i30IAEGER PCB SITE #1724 Date Received 08/66/91

Sampled by CLIENT 081M1 194!

MATRIX SPIKE/MATRIX SPIKE DUPLICATE ANALYSIS SUMMARY

' SPIKE PercentParameter Description ;• RESULT LEVEL UNITS Recovery

QC Matrix Spike/Matrix Spike Duplicates

PCB(a* Aroclor 1260) Cil096-6a-53Matrix Spike(Result 1) 81.£ 38.4 * UG/0 56*Matrix Spike Duplicate(Result g) 23.6 44.4 . UG/G 56%Relative % Difference Between Spikes .3.5%

All spike results are corrected for the sample background.

" "' •' . - :. .- RESULT ' - • •Percent Recovery • — ——— —— X 100 r.

. . . C. SPIKE LEVEL- ' ' ' - . - \ : . . , - • - •

CResult 1 - Result £3Relative Percent difference •— — —— - — — --———.— x 100 Expressed AS an absolute value

CResult 1 * Result £3/&

1256 GREENBRIER STREET. CHARLESTON. WEST VIRGINIA 25311 — TELEPHONE 304 346-07254643 BENSON AVENUE. BALT1MORE&lfo$X|jQj$ ?1 7 ~ TELEPHONE 301 247-7400

4440 GLEN ESTE - WITHAMSVILLE RD,, SUITEOOO, CINCINNATI. OHIO 45245 — TELEPHONE 513 752-9696

' 1.' "' ' ' ' *n ' * ** 'i .--an . ,^-iio ;••••;. i?9t

Channel 3

if. <> 116 6630 02 ->,^o 4466888 13-::T 0.3 3 311923 2'4 O.<ul2 s 36884 0» '\.77;: 69094 0.<> '> fci24 247839 1V 0..992 V2319 0R -1.068 2313921 0* :i. -376 30307 " O

.!.<; 1..4 B 15027 011 1.348 169260 112, 1 - 72(3 8374 O13 1-336 3690 014 1.908 18031 0 __ ^ A,15 1 - > 76 63374 0 TV (lO i "f j %16 2-164 3718 O17 2.288 3129 01LJ 2.500 19493 ' 017 , 2,996 28634 -- 020 ; ' -J-2213 208349 121 3.444 328653 122 3.384 123728 023 4.020 739987 2£4 . .. -4.20Q J33368S 325 * W..480 1653410 3

A R100176

' if 0071 £r-Xl3!:>.

r f 16/51.42

V)- . ' f . l 112921 '<* . /' 4 A"•' T -'.. -- - . . .

.-.644 3373381 ; 1e.3ik: ; ?9o o3,332 '40*578 - 0- -

fcft

-*CB ANALYSIS

•rila ; C:\EZCHROM\SHOS\SH08.033"-•-Me s Cs\EZCKRQM\KETHQDS\DCb.met NTO<o"O~ ^Y\\vu J* .J

._.... . *•% - ••* _ - . _ .-t ^^^

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Channel

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Time Area

1. 0.256 4385176 13 fl ,, -» i\ -s.k > ^ /Si 0.338 662178 2 OH O£ - 3\H °G" s O?M*Uv>S/G-; O.A12 116350 0 ^ -*""", 0.772 , 100939 0i* 0.332 329717 1

0.996 1973 0? 1.072 2416358 78 1.260 13623 09 1.364 40934 010 1.472 15324 0II 1.556 163763 012 1.740 7380 013 . 1.924 18480 0 3<V.U14 1.988 37992 0 "llS - G&1$ 2.312 20043 0 - 11,1 iT " ^16 3.012 32178 0 TV"17 3.240 24083118 3.496 393034 117 3.900 159339 0 __ , "71 ° /20 4.036 910140 3 \(? vr\X " I I «t»21 4.24xS 1033139 3 ^" ^22 4.496 2051744 623 4.708 1390727 424 4.940 2591985 725 5.036 2003078 6

e Ar»* Area*5-529 "2S3324 ~"""""T?'£J6 2299173 4--^96 ,. , 43X337* • --.. <

6.532 1687516.792 4436747.084 .1009699

3616433»- 2337V.232

-38 10.256 1467 A'V'"1 .11 j- - « '" "W/ ()*• 11.244 4456 n

11.608 6872 O"'1- 11.700 1086 0

METHOD EXTRACTION BLANKS

LABORATORIES

PCB ANALYSIS

Pile ; C:\EZCHROM\3H08\8H08.012

Acauirea : Aug 09, i?9l 09s09:46

Channel B

0-4

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Minutes

Pknc Ret. Time rtrea Area^1 0.236 4025362 332 0.476 31379 O3 0.756 ' 3084 0*< 0.808 14721 05 0.904 \ . - - , 4046 06 , . 0.938 . , 3384 0 .._-.,7 1.068 ' 2634486 26 "T>r G.O — 758 1.356 31488 0 U^-Or9 1.536 v - f-<-' ', 32745 010 1.988 25739 0 -11 3.012 19563 012 5.336 59236 113 , 7.684 3542566 34

PCB ANALYSIS

File : C:\EZCHRaM\8HOS\8HOS.037

-•icauirea ": Aua 0?, 19? 1 12 5 24:04 O

Channel B

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.- '•' - 3 1CMinutes

'kno Ret.. Time Are* Area's

l 0.236 4011157 37£ 0,472 26984 03 0.808 -- 10433 0^ 0.992 5475 O-< 1.068- 2602998 24 TV I/VN V - "776 1.352 33401 O I Cfn\ '7 1.552 42804 08 1.980 22246 0 y> ^9 2.820 1713 0 T) CO P *"10 £.8$5 14907 011 2.980 23713 012 3.10* 5027 O13 4.424 3271 014 - 4.976 5933 019 5.128 2862 016 5.320 80114 117 6.948 64130 118 7.480 29129 019 7.664 3762996 3520 3.924 1902 021 9.236 1597 . 022 9.3#> 4034 0

CHAXN-of-CUSTODY

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5 Underwood Court, Delran, NJ 08075 609-461-4003 EPA ... · 5 underwood court, delran, nj 08075...

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Transcript of 5 Underwood Court, Delran, NJ 08075 609-461-4003 EPA ... · 5 underwood court, delran, nj 08075...