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    Coating Technology forFlexible Packaging

    Lee A. Ostness

    Product Manager - Coating & Drying Systems

    Flexible Packaging is widely used in todays world. It is used to package

    a multitude of products such as: processed meat, processed cheese,

    fresh red meat, bulk liquids, cereals, cake mix, coffee, medical device

    films, snacks and many others. There are many different substrates and

    coatings used to create these packages to produce the various levels of

    barrier protection. see ch rt

    SUBSTRATES COATINGS

    PET 1 10 mil Primers 0.04 0.4 gsm

    PE 1 8 mil Adhesives 3.25 6.5 gsm

    Al Foil 20 60 PVDC 1.6 6.5 gsm

    BOPP/OPP 0.4 2 mil Wash-coats 0.8 1.5 gsm

    CPP 1 4 mil PVOH 0.5 gsm

    Nylon 0.4 2 mil Lacquers 5.0 gsm

    MetPET 1 10 mil Varnishes 0.02 0.04 gsm

    Cellophane 0.8 1 mil Acrylic Polyurethanes 0.3 gsm

    A typical package may be constructed of several layers of substrates and

    coatings. Two typical constructions are illustrated below. The beveragepackage is constructed with PET/Printed/Primer coating/LDPE/Foil/LDPE heatseal).

    The Retort Package is a different construction requiring two coatings,

    PET/Printed/Adhesive coating/Foil/Primer coating/LDPE. The foil is a barrier

    layer and may be substituted with Metalized PET, Nylon, or EVOH

    depending on the amount or type of barrier required. see illustr tion

    PET 12.6

    (PRINT)

    FOIL 6.3

    LDPE 12.6

    LDPE (Heat Seal) 25

    PRIMER 0.04

    Beverage Package

    PET 12.6

    (PRINT)

    FOIL 6.3ADHESIVE 3.25 6.5

    LDPE 25

    PRIMER 0.04

    Retort Package

    PET 12.6

    (PRINT)

    FOIL 6.3

    LDPE 12.6

    LDPE (Heat Seal) 25

    PRIMER 0.04

    PET 12.6

    (PRINT)

    FOIL 6.3

    LDPE 12.6

    LDPE (Heat Seal) 25

    PRIMER 0.04

    Beverage Package

    PET 12.6

    (PRINT)

    FOIL 6.3ADHESIVE 3.25 6.5

    LDPE 25

    PRIMER 0.04

    Retort Package

    PET 12.6

    (PRINT)

    FOIL 6.3ADHESIVE 3.25 6.5

    LDPE 25

    PRIMER 0.04

    PET 12.6

    (PRINT)

    FOIL 6.3ADHESIVE 3.25 6.5

    LDPE 25

    PRIMER 0.04

    Retort Package

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    The constructions incorporate the use of solution coating(s) to enhance

    either the barrier and/or the adhesion properties. The focus of this paper

    is to discuss how these coatings are applied.

    A solution coating is a liquid with solids dispersed in the liquid to assist

    the wetting of the substrate it is applied to. The

    liquid can be a combination of solvents or water

    determined by its ability to maintain the dispersion

    of the solids. The solution coating is applied to a

    continuous web with a Coater and then passed

    through a Dryer to remove the liquid leaving a thin

    layer of solids on the substrate. The coater will beeither a gravure type or a smooth roll type. The

    dryers are normally a roll support design or a

    floatation design. The roll support dryer consist of

    rolls supporting the web with opposing impingement nozzles drying the

    web. The floatation dryer consist of nozzles on both sides of the web

    creating a sign wave affect to float the web.

    Coating heads have a variety of applications, strengths and weaknesses.

    How do you objectively select the right coating head? There are 50 plus

    coater configurations available to apply an infinite number of coating

    solutions. To select the coater for your needs you first need to know

    your coating and substrates properties, then match these properties with

    the coaters abilities/limitations.

    Coating Substrate Coater

    % Solids Absorbency Speed Range

    Viscosity Surface Tension Coat Weight Range

    pH Tear Strength Solids Range

    Shear Stability Smoothness Viscosity Range

    Density Caliper Appearance

    Solvent/Water Based Melt Point

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    There are four main coater configurations used in the Flex Package

    construction. The four types are Direct Gravure, Reverse Gravure, Offset

    Gravure and Smooth Roll. The

    gravure coaters utilize steel rolls

    with patterns engraved into the

    face of the roll. This pattern

    determines how much coating is

    carried to the web. The coating is

    applied to the gravure, metered off the surface, leaving coating only in

    the engraved pattern, then transferred to the web that is supported by

    the rubber covered back-up roll. The smooth roll coater applies the

    coating from an open pan, picking up the coating with a smooth steel rollpartially immersed into the pan, then the web is pressed against the steel

    roll with the rubber covered back-up roll. The speed of the steel roll and

    amount of pressure against the steel roll combine to control the amount

    of coating applied to the web.

    The gravure roll is a steel roll with a precise pattern engraved into the

    surface of the roll. There are several gravure vendors, each with their

    own names for these patterns. The picture shows one vendors patterns

    and the names associated

    with them. The patterns

    are called from left to

    right; Tri-Helical, Pyramid, Quadrangular, and Hexagonal. The amount

    of coating in each cell (pattern) is measured and referred to as Billion

    Cubic Microns (BCM). To select the correct gravure pattern for your

    application, you need to reference a coat weight chart provided by most

    gravure vendors. On this chart locate your coat weight under the percent

    solids column that matches your formulation. Then follow the row to the

    left and it determines the volume required to deliver the desired coating

    to the substrate.

    Direct

    Gravure

    Reverse

    Gravure

    Offset

    Gravure

    Smooth

    Roll

    Direct

    Gravure

    Reverse

    Gravure

    Offset

    Gravure

    Smooth

    Roll

    Direct

    Gravure

    Reverse

    Gravure

    Offset

    Gravure

    Smooth

    Roll

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    This chart is setup for the Direct Gravure method. The Reverse Gravure

    method will need to add approximately 20% to the desired coat weight

    and for Offset Gravure method add approximately 75%. This will be

    explained as we discuss each type of coater and their operating

    parameters.

    The chart is only a starting point to get you close to your target. A large

    amount of the time the gravure pattern will need to be adjusted to

    achieve the correct coat weight due to the different coating and/or

    substrate characteristics.

    Direct Gravure Coater:

    The Direct Gravure Coater consists of a rubber

    covered back-up roll, a gravure roll, and a coating

    applicator. The back-up roll is covered with a rubber

    compound and is used to transport the web through

    the coating process. The back-up roll is pressed

    against the gravure roll creating a slight nip which pulls the coating out

    of the gravure cells and deposits the coating onto the web. The gravure

    roll is a steel roll with a pattern engraved into the face of the roll. These

    cells are filled with the coating and doctored of the surface of the roll

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    GSM

    150%50% 100%

    Gravure Speed

    GSM

    95% 100% 105%

    Gravure Speed

    leaving a precise amount of coating on the gravure roll. The roll then

    transports the coating to the nip where it is transferred to the web. The

    coating applicator is either an enclosed chamber with two doctor blades

    or an open pan with a doctor blade assembly to remove the excess

    coating. In the Direct Gravure mode the gravure roll and

    the web are moving in the same direction at the point of

    contact. The speed of the gravure roll is usually the same

    as the web but it may be adjusted to 10% of the web

    speed. The coat weight is determined by the gravure

    volume and the coating solids.

    Reverse Gravure Coater:

    The Reverse Gravure Coater consists of the same

    equipment as the Direct Gravure coater. In this

    method the gravure roll runs in the opposite

    direction to the web and varies in speed from 50%

    to 150% of web speed. The most common

    operating speed is 110% to 120%. The coat weight

    in this mode when plotted will create a bell shaped curved by running the

    gravure roll from 50 to 150% of web speed measuring the coat weight

    every 10%. If the same gravure pattern from the Direct gravure is used

    the highest coat weight will only be about 80% of the direct

    gravure methods. The coat weight is determined by the

    gravure pattern, the coating solids, and by the speed of the

    gravure roll. This method will lay the coating down with a

    smoother appearance because of the shearing action

    created at the nip. The appearance created by the direct

    gravure method is a rougher texture because at matched speeds and in

    the same direction you are virtually printing the pattern onto the web.

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    10% 60% 100%

    Gravure Speed

    GSM

    Offset Gravure Coater:

    The Offset GravureCoater consist of a steel back-up

    roll, a rubber covered applicator roll, a gravure roll,

    and a coating applicator. The back-up roll is chrome

    plated steel roll used to transport the web through

    the coating process and create the nip between the

    web and the applicator roll. The Applicator roll is a

    rubber covered roll used to transfer the coating from

    the gravure roll to applicator roll, to the web. The gravure roll is a steel

    roll with a pattern engraved into its surface. The coating applicator is

    either an enclosed chamber with two doctor blades to an open pan with a

    doctor blade assembly to remove the excess coating. In this method allthe rolls are turning in the same direction at the point of contact at each

    nip. The back-up roll is operating at line speed, the applicator roll most

    usually is operating at 98% of line speed (5%), and the gravure roll

    operates at 25 to 35% of line speed. With this method

    the coat weight curve when plotted would be a steady

    incline then level off to a fairly straight plain. The curve

    would be generated by varying the speed of the gravure

    roll from 5% to 100 % in increments of 5%. The coat

    weight usually levels off when the gravure roll reaches

    about the 60% of line speed. The shearing action created by the

    differential speeds and the two nip points generally apply a smooth

    coating.

    Smooth Roll Coater:

    The Smooth RollCoaterconsist of a rubber covered back-

    up roll, a steel chrome plated pick-up roll, sling guards

    and a coating pan. The back-up roll is covered with a

    rubber compound and is used to transport the web

    through the coating process. The back-up roll is pressed

    against the pick-up roll creating a slight nip. The pick-up roll is

    immersed into the coating pan and transports the coating to the nip

    between the web and the pick-up roll. The coating is applied to the web

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    10% 100%

    Pick-up Speed

    GSM

    at this nip point. The amount of coating applied is dependent on the

    hydraulic forces at the coater nip created by the speed of the pick-up roll

    and the nip force. The coating pan is filled with a solution coating and in

    most cases it has an overflow weir so the coating may be recirculated.

    The rubber compound selected has to consider several operational

    conditions. The parameters consist of the durometer, surface tension,

    resilience, tear resistance. The durometer needs to be based on the

    speed of the machine line and the viscosity of the coating. With this

    method the coat weight increases with higher speed and higher viscosity.

    The surface tension is selected based on the compound of the rubber.

    This method requires the rubber to repel the coating, so only the web will

    be coated. The resilience and tear strength are required due to the highforces and different web widths. The coat weight is determined by the nip

    width and the pick-up roll speed and the curve will be a line

    with a slow incline and then when the hydraulic forces

    overcome the nip the line transitions into a steep incline.

    The wider the nip the lower on the graph the curve is

    generated.

    The gravure coater requires the rubber

    rolls to be undercut slightly narrower than

    the web width whereas in the smooth roll

    method the rubber rolls are full width.

    When the coating is transferred to the

    web or applicator roll from the gravure cells it only needs to be

    transferred at the width of the web. If the rubber is not undercut the

    coating would form a flooded nip outside the area of the web and

    gradually move into the web area, creating a hydraulic force that would

    increase the coat weight to unacceptable levels in these areas. If the

    rubber was undercut, the area outside the width of the web would

    continue to travel around and back into the coating applicator. The

    smooth roll coater requires a full width rubber roll to create the flooded

    nip. If the nip was not flooded across the entire web, some areas would

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    have either too little coating or none at all. This flooded nip also requires

    sling guards at the end of the rolls to catch and return into the pan any of

    the slinging coating.

    A nip is required between the coating rolls in all of the methods listed

    above. What is a nip? A nip is the amount of contact that is generated

    between the rolls when they are pressed together. The softer the rubber

    durometer, the wider the nip will be with the same pressure. As the

    pressure increases the nip width increases. How do you measure the nip

    width? There are several methods available using

    carbon nip paper, aluminum foil, liquid coating and

    piece of paper, a computerized nip blanket. What allthese methods have in common is you must place

    something between the two rolls before you close

    them together.

    In review, the coat weight control of each coater as depicted in the charts

    show that the only coater that cannot adjust coat weight is the Direct

    Gravure (shown s forw rd gr vure in the illustr tion).

    GSM

    150%5 0% 1 00 %

    Gravure Speed

    Reverse

    Gravure

    GSM

    95 % 10 0% 1 05%

    Gravure Speed

    Forward

    Gravure

    10% 60% 100%

    Gravure Speed

    GSM

    Offset

    Gravure

    10% 100%

    Pick-up Speed

    GSM

    Smooth

    Transfer

    GSM

    150%5 0% 1 00 %

    Gravure Speed

    Reverse

    Gravure

    GSM

    150%5 0% 1 00 %

    Gravure Speed

    Reverse

    Gravure

    150%5 0% 1 00 %

    Gravure Speed

    Reverse

    Gravure

    GSM

    95 % 10 0% 1 05%

    Gravure Speed

    Forward

    Gravure

    10% 60% 100%

    Gravure Speed

    GSM

    Offset

    Gravure

    10% 100%

    Pick-up Speed

    GSM

    Smooth

    Transfer

    GSM

    95 % 10 0% 1 05%

    Gravure Speed

    Forward

    Gravure

    10% 60% 100%

    Gravure Speed

    GSM

    Offset

    Gravure

    10% 60% 100%

    Gravure Speed

    GSM

    Offset

    Gravure

    10% 100%

    Pick-up Speed

    GSM

    Smooth

    Transfer

    10% 100%

    Pick-up Speed

    GSM

    Smooth

    Transfer

    The smooth roll coater can control coat weight until the hydraulic force

    over comes the coater nip and then the coat weight climbs dramatically.

    The Gravure coaters offer excellent coat weight control and are stable

    through out all line speeds but require an undercut rubber roll for each

    web width. A sleeve system may be used in the rubber roll location. The

    sleeve system allows the rubber undercut sleeve to be changed in less

    than 15 minutes. This system still requires a sleeve for each web width.

    The smooth roll coater offers coat weight control but needs adjustment

    going from low to high line speeds. This is referred to as unstable, as

    IMPRESSION

    PAPER

    TORQUE SHAFT

    SHOULD BE

    LEVELED

    RUBBER

    COVERED

    ROLL

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    the line speed increases so does the amount of coating supplied. The

    result is much of the coated web during speed-up and slow down is

    waste. The advantage to the smooth roll coater is it only requires one

    rubber roll for all web widths.

    GSM

    Line Speed

    Gravure

    Smooth Roll

    GSM

    Line Speed

    Gravure

    Smooth Roll

    The Direct Gravure coater is used primarily on substrates that are fragile,

    like metalized PET or printed webs. If the roll applying the coating to

    these two examples were operated in the reverse direction or at a

    differential speed, then that roll could damage the print layer or pick off

    the foil. Operating the roll in the forward direction with matched speeds

    will apply the coating without damage. The smooth roll coater can adjust

    coat weights and apply coatings without damage to the layers. The limit

    on this coater is the flooded nip. This application works well on films or

    coated papers, BUT on open face paper the coat weight cannot be

    controlled. Passing the open faced paper through the flooded nip will

    saturate the web and apply excessive coating.

    Take all the parameters from this paper and create a chart, now you can

    select the correct coater for your process.

    Coater Selection

    Direct

    Gravure

    Reverse

    Gravure

    Offset

    Gravure

    Smooth

    Roll

    Ability to Adjust Coat Weight No Yes Yes Yes

    Ability to Coat Paper Yes Yes Yes No

    Ability to Coat Film Yes Yes Yes Yes

    Stable at all Line Speeds Yes Yes Yes No

    Requires Under Cut Rubber Roll Yes Yes Yes No

    Ability to Coat Printed Film Yes No Yes Yes

    Ability to Coat Foil Yes No Yes Yes

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    2006 PLACE

    Conference

    September 17-21

    Cincinnati, Ohio

    Coating TechnologyforFlexible Packaging

    Presented by:

    Lee A. Ostness

    Product ManagerCoating & Drying Systems

    Black Clawson Converting Machinery

    Typical Products

    ProductProcessed Meat

    Processed Cheese

    Fresh Red Meat

    Bulk Liquids

    Cereal/Cake Mix

    Medical Devices Films

    Coffee

    Fresh Produce

    Snacks

    Package TypePouches, Vacuum Packages

    Pouches, Wraps

    Barrier, Shrink Bags

    Pouches, Bag in Box

    Inner Liners

    Pouches, Thermal Formed

    Brick Packs, Pouches

    Breathable Bags

    Bags

    Flex-Pack Components

    Substrates

    PET 1-10 mil

    PE 1-8 mil

    Al foil 20-60

    BOPP/OPP 0.4-2 mil

    CPP 1-4 mil

    Nylon 0.4-2 mil

    METPET 1-10 mil

    Cellophane 0.8-1 mil

    Coatings

    Primers 0.04-0.4 gsm

    Adhesives 3.25-6.5 gsm

    PVDC 1.6-6.5 gsm

    Wash-coats 0.8-1.5 gsm

    PVOH 0.5 gsm

    Lacquer 5.0 gsm

    Acrylic Polyurethane 0.3 gsm

    Varnish 0.02 0.04 gsm

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    Typical Product Structures

    PET 12.6

    (PRINT)

    FOIL 6.3

    LDPE 12.6

    LDPE (Heat Seal) 25

    PRIMER 0.04

    Beverage Package

    PET 12.6

    (PRINT)

    FOIL 6.3

    ADHESIVE 3.25 6.5

    LDPE 25

    PRIMER 0.04

    Retort Package

    Note: The foil is a barrier layer and may be substituted with METPET, Nylon, or EVOH

    depending on the amount or type of barrier layer needed.

    COATER/DRYER

    Coater

    Smooth roll

    Backing Roll not Undercut

    Pan Fed

    Direct Gravure

    Backing Roll Undercut

    Sleeve

    Pan Fed

    Enclosed Applicator

    Dryer

    Air Floatation Nozzles

    Roll Support

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    FLEX-PACK COATERS

    Direct

    Gravure

    Reverse

    Gravure

    Offset

    Gravure

    Smooth

    Roll

    Methodology of Application

    Gravure Coater Smooth Roll Coater

    Gravure Engraved Patterns

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    Volume

    BCMBillion Cubic Microns

    The formula is based onink technology. Many of

    today's coatings are of

    an unique composition.Use this formula for a

    better understanding ofhow the cell volumes are

    achieved. Coat weights

    may vary when different

    coatings are applied withthe same cell volume.

    formula from Consolidated Engravers

    DIRECT GRAVURE: is 80 % of what the chart displays

    REVERSE GRAVURE: is generally 80% of Direct GravureDIFFERENTIAL OFFSET GRAVURE: is generally 25% of Direct Gravure

    CHARTSREFERENCE DFROM:

    PAMARCO,INC.

    2 00 0 . 00 08 2 . 6 0 .2 1 0 . 26 0 .3 2 0 . 47 0 .7 0 2 00 0 . 00 12 5 . 7 0 .2 2 0 . 32 0 .4 8 0 .7 1 1 .0 5 1 .3 1 1 20 0 .0 02 2 1 8. 0 0 .6 4 0 .9 5 1 .4 0 2 .0 7 3 .0 7 3 .8 0 ARCINDUSTRIES, INC.

    1 80 0 . 00 09 3 . 2 0 .2 3 0 . 29 0 .3 6 0 . 53 0 .7 9 1 90 0 . 00 15 7 . 5 0 .2 7 0 . 40 0 .6 0 0 .8 9 1 .3 1 1 .6 3 1 10 0 .0 02 5 2 0. 3 0 .7 3 1 .0 8 1 .6 0 2 .3 7 3 .5 1 4 .3 5 AMERICANENGRAVINGAND MACHINECO.

    1 65 0 . 00 10 3 . 4 0 .2 6 0 . 32 0 .4 0 0 . 59 0 .8 8 1 80 0 . 00 18 9 . 4 0 .3 3 0 . 48 0 .7 2 1 .0 7 1 .5 8 1 .9 6 9 5 0 .0 03 2 2 6. 2 0 .9 4 1 .3 9 2 .0 5 3 .0 3 4 .4 9 5 .5 7 MODERNENGRAV INGAND MACHINE CO.

    1 50 0 . 00 20 7 . 5 0 .5 1 0 . 64 0 .8 0 1 . 18 1 .7 5 1 65 0 . 00 22 1 0 .9 0 .3 0 0 . 49 0 .8 0 1 .3 0 1 .9 3 2 .3 9 9 0 0 .0 03 5 2 8. 8 1 .0 3 1 .5 2 2 .2 5 3 .3 3 4 .9 3 6 .1 1

    1 42 0 . 00 22 8 . 2 0 .5 6 0 . 70 0 .8 8 1 . 30 1 .9 2 1 50 0 . 00 25 1 3 .3 0 .4 6 0 . 68 1 .0 0 1 .4 8 2 .1 9 2 .7 2 8 4 0 .0 03 9 3 2. 3 1 .1 4 1 .6 9 2 .5 0 3 .7 0 5 .4 8 6 .7 9

    1 32 0 . 00 25 9 . 7 0 .6 4 0 . 80 1 .0 0 1 . 48 2 .1 9 1 40 0 . 00 28 1 5 .0 0 .5 1 0 . 76 1 .1 2 1 .6 6 2 .4 5 3 .0 5 7 9 0 .0 04 0 3 2. 7 1 .1 8 1 .7 5 2 .5 8 3 .8 1 5 .6 4 6 .9 9

    1 20 0 . 00 30 1 1 .0 0 .7 7 0 . 96 1 .2 0 1 . 78 2 .6 3 1 30 0 . 00 30 1 6 .0 0 .5 5 0 . 8 1 1 . 20 1 .7 8 2 .6 3 3 .2 6 7 2 0 .0 04 5 3 6. 8 1 .3 2 1 .9 5 2 .8 8 4 .2 6 6 .3 0 7 .8 1

    1 16 0 . 00 32 1 1 .9 0 .8 1 1 . 02 1 .2 8 1 . 89 2 .8 0 1 20 0 . 00 32 1 7 .2 0 .5 9 0 . 8 7 1 . 28 1 .8 9 2 .8 0 3 .4 8 6 4 0 .0 05 1 4 1. 8 1 .5 0 2 .2 2 3 .2 8 4 .8 5 7 .1 8 8 .8 9

    1 08 0 . 00 33 1 2 .2 0 .8 5 1 . 06 1 .3 2 1 . 95 2 .8 9 1 10 0 . 00 39 2 1 .4 0 .7 1 1 . 0 5 1 . 56 2 .3 1 3 .4 2 4 .2 4 5 9 0 .0 05 5 4 5. 0 1 .6 1 2 .3 9 3 .5 3 5 .2 2 7 .7 3 9 .5 7

    1 00 0 . 00 35 1 3 .9 1 .0 3 1 . 20 1 .4 0 2 . 07 3 .0 7 9 6 0 . 00 44 2 6 .3 0 .8 0 1 . 1 9 1 . 76 2 .6 1 3 .8 5 4 .7 9 5 4 0 .0 06 0 4 9. 0 1 .7 6 2 .6 0 3 .8 5 5 .7 0 8 .4 4 1 0. 46

    9 0 0 . 00 38 1 6 .0 0 .9 8 1 . 22 1 .5 2 2 . 25 3 .3 3 8 5 0 . 00 49 3 0 .0 0 .9 0 1 . 32 1 .9 6 2 .9 0 4 .2 9 5 .3 3 5 0 0 .0 06 5 5 3. 3 1 .9 1 2 .8 3 4 .1 8 6 .1 8 9 .1 5 1 1. 34

    8 0 0 . 00 40 1 7 .3 1 .0 2 1 . 28 1 .6 0 2 . 37 3 .5 0 7 5 0 . 00 54 3 2 .0 0 .9 8 1 . 4 6 2 . 16 3 .2 0 4 .7 3 5 .8 8 4 5 0 .0 07 3 5 9. 6 2 .1 4 3 .1 7 4 .6 8 6 .9 2 1 0. 25 1 2. 70

    7 0 0 . 00 45 1 8 .0 1 .1 5 1 . 44 1 .8 0 2 . 66 3 .9 4 6 5 0 . 00 60 3 5 .4 1 .1 0 1 . 6 2 2 . 40 3 .5 5 5 .2 6 6 .5 3 4 2 0 .0 07 5 6 1. 5 2 .1 9 3 .2 5 4 .8 0 7 .1 0 1 0. 52 1 3. 04

    6 5 0 . 00 50 2 0 .4 1 .2 8 1 . 60 2 .0 0 2 . 96 4 .3 8 5 5 0 . 00 65 4 0 .4 1 .1 9 1 . 7 6 2 . 60 3 .8 5 5 .6 9 7 .0 7 3 6 0 .0 09 0 7 3. 3 2 .6 4 3 .9 1 5 .7 8 8 .5 5 1 2. 66 1 5. 68

    6 0 0 . 00 58 2 4 .4 1 .4 9 1 . 86 2 .3 2 3 . 43 5 .0 8 4 5 0 . 00 68 4 4 .5 1 .2 4 1 . 8 4 2 . 72 4 .0 3 5 .9 6 7 .4 0 3 5 0 .0 09 3 7 6. 0 2 .8 0 4 .0 9 5 .9 8 8 .7 4 1 3. 10 1 6. 23

    5 5 0 . 00 62 2 6 .6 1 .5 8 1 . 98 2 .4 8 3 . 67 5 .4 3 3 5 0 . 00 70 4 6 .6 1 .2 8 1 . 8 9 2 . 80 4 .1 4 6 .1 3 7 .6 2 3 3 0 .0 09 6 7 8. 2 2 .8 1 4 .1 6 6 .1 5 9 .1 0 1 3. 48 1 6. 70

    5 0 0 . 00 76 3 3 .7 1 .9 4 2 . 42 3 .0 2 4 . 47 6 .6 1 3 0 0 . 00 90 5 8 .7 1 .6 4 2 . 4 3 3 . 60 5 .3 3 7 .8 8 9 .7 9 2 8 0 .0 11 0 9 0. 0 3 .2 2 4 .7 7 7 .0 5 1 0. 43 1 5. 45 1 9. 15

    4 5 0 . 0 09 0 4 1. 0 2 . 3 0 2 . 8 8 3 . 60 5 .3 3 7 . 8 8 2 5 0 . 0 12 0 8 1 .0 2 . 19 3 . 25 4 . 80 7 . 10 1 0 .5 1 1 3 .0 6 2 6 0 .0 1 30 1 0 6. 5 3 . 81 5 .6 3 8 . 33 1 2 .3 2 1 8 .2 5 2 2 .6 14 0 0 . 0 10 4 4 8. 0 2 . 6 7 3 . 3 3 4 . 16 6 .1 5 9 . 1 1 1 6 0 . 0 17 0 11 7 .0 3 . 1 1 4 . 6 0 6 . 80 1 0 .0 6 1 4 .8 9 1 6 .5 0 2 4 0 .0 1 40 1 1 5. 0 4 . 09 6 .0 5 8 . 95 1 3 .2 4 1 9 .6 2 2 4 .3 1

    DIRECT FORWARD GRAVURE

    0 .0 00 8 2. 6 0 . 17 0 . 21 0 . 26 0 . 38 0 . 56 0 .0 01 2 5. 7 0 . 18 0 . 26 0 . 38 0 .5 7 0 .8 4 1 .0 5 0 .0 01 2 5 .7 0 .2 0 0 . 30 0 .4 4 0 . 6 5 0 .9 7 1 .2 1 0 .0 02 2 1 8. 0 0 . 51 0 .7 6 1 .1 2 1 .6 6 2 .4 6 3 .0 4

    0 .0 00 9 3. 2 0 . 19 0 . 23 0 . 29 0 . 42 0 . 63 0 .0 01 5 7. 5 0 . 22 0 . 32 0 . 48 0 .7 1 1 .0 5 1 .3 0 0 .0 01 5 7 .5 0 .2 5 0 . 37 0 .5 5 0 . 8 2 1 .2 1 1 .5 0 0 .0 02 5 2 0. 3 0 . 58 0 .8 6 1 .2 8 1 .9 0 2 .8 1 3 .4 8

    0 .0 01 0 3. 4 0 . 20 0 . 26 0 . 32 0 . 47 0 . 70 0 .0 01 8 9. 4 0 . 26 0 . 39 0 . 58 0 .8 6 1 .2 6 1 .5 7 0 .0 01 8 9 .4 0 .3 0 0 . 45 0 .6 6 0 . 9 8 1 .4 5 1 .8 0 0 .0 03 2 2 6. 2 0 . 75 1 .1 1 1 .6 4 2 .4 2 3 .5 9 4 .4 6

    0 .0 02 0 7. 5 0 . 41 0 . 51 0 . 64 0 . 94 1 . 40 0 .0 02 2 10 .9 0 . 24 0 . 39 0 . 64 1 .0 4 1 .5 4 1 .9 1 0 .0 02 2 1 0. 9 0 . 28 0 .4 5 0 . 74 1 .2 0 1 .7 8 2 .2 0 0 .0 03 5 2 8. 8 0 . 82 1 .2 2 1 .8 0 2 .6 6 3 .9 4 4 .8 9

    0 .0 02 2 8. 2 0 . 45 0 . 56 0 . 70 1 . 04 1 . 54 0 .0 02 5 13 .3 0 . 37 0 . 54 0 . 80 1 .1 8 1 .7 5 2 .1 8 0 .0 02 5 1 3. 3 0 . 42 0 .6 2 0 . 92 1 .3 6 2 .0 1 2 .5 0 0 .0 03 9 3 2. 3 0 . 91 1 .3 5 2 .0 0 2 .9 6 4 .3 8 5 .4 3

    0 .0 02 5 9. 7 0 . 51 0 . 64 0 . 80 1 . 18 1 . 75 0 .0 02 8 15 .0 0 . 41 0 . 60 0 . 90 1 .3 3 1 .9 6 2 .4 4 0 .0 02 8 1 5. 0 0 . 47 0 .7 0 1 . 03 1 .5 3 2 .2 5 2 .8 1 0 .0 04 0 3 2. 7 0 . 95 1 .4 0 2 .0 6 3 .0 5 4 .5 1 5 .5 9

    0 .0 03 0 11 .0 0 . 61 0 . 77 0 . 96 1 . 42 2 . 10 0 .0 03 0 16 .0 0 . 44 0 . 6 5 0 .9 6 1 . 42 2 .1 0 2 .6 1 0 .0 03 0 1 6. 0 0 . 5 0 0 .7 4 1 . 10 1 .6 4 2 .4 2 3 .0 0 0 .0 04 5 3 6. 8 1 .0 5 1 . 56 2 .3 0 3 .4 1 5 .0 4 6 .2 5

    0 .0 03 2 11 .9 0 . 65 0 . 82 1 . 02 1 . 51 2 . 24 0 .0 03 2 17 .2 0 . 47 0 . 6 9 1 .0 2 1 . 51 2 .2 4 2 .7 8 0 .0 03 2 1 7. 2 0 . 5 4 0 .8 0 1 . 18 1 .7 4 2 .5 8 3 .2 0 0 .0 05 1 4 1. 8 1 .2 0 1 . 77 2 .6 2 3 .8 8 5 .7 4 7 .1 1

    0 .0 03 3 12 .2 0 . 68 0 . 85 1 . 06 1 . 56 2 . 31 0 .0 03 9 21 .4 0 . 57 0 . 8 4 1 .2 5 1 . 85 2 .7 4 3 .3 9 0 .0 03 9 2 1. 4 0 . 6 5 0 .9 7 1 . 44 2 .1 3 3 .1 5 3 .9 0 0 .0 05 5 4 5. 0 1 .2 9 1 . 91 2 .8 2 4 .1 8 6 .1 8 7 .6 6

    0 .0 03 5 13 .9 0 . 82 0 . 96 1 . 12 1 . 66 2 . 46 0 .0 04 4 26 .3 0 . 64 0 . 9 5 1 .4 1 2 . 09 3 .0 8 3 .8 3 0 .0 04 4 2 6. 3 0 . 7 4 1 .0 9 1 . 62 2 .4 0 3 .5 4 4 .4 1 0 .0 06 0 4 9. 0 1 .4 1 2 . 08 3 .0 8 4 .5 6 6 .7 5 8 .3 7

    0 .0 03 8 16 .0 0 . 78 0 . 98 1 . 22 1 . 80 2 . 66 0 .0 04 9 30 .0 0 . 72 1 . 0 6 1 .5 7 2 . 32 3 .4 3 4 .2 6 0 .0 04 9 3 0. 0 0 . 8 2 1 .2 2 1 . 80 2 .6 7 3 .9 5 4 .9 0 0 .0 06 5 5 3. 3 1 .5 3 2 . 26 3 .3 4 4 .9 4 7 .3 2 9 .0 7

    0 .0 04 0 17 .3 0 . 82 1 . 02 1 . 28 1 . 90 2 . 80 0 .0 05 4 32 .0 0 . 79 1 . 1 7 1 .7 3 2 . 56 3 .7 8 4 .7 0 0 .0 05 4 3 2. 0 0 . 9 1 1 .3 4 1 . 99 2 .9 4 4 .3 5 5 .4 1 0 .0 07 3 5 9. 6 1 .7 1 2 . 53 3 .7 4 5 .5 4 8 .2 0 1 0. 16

    0 .0 04 5 18 .0 0 . 92 1 . 15 1 . 44 2 . 13 3 . 15 0 .0 06 0 35 .4 0 . 88 1 . 3 0 1 .9 2 2 . 84 4 .2 1 5 .2 2 0 .0 06 0 3 5. 4 1 . 0 1 1 .4 9 2 . 21 3 .2 7 4 .8 4 6 .0 1 0 .0 07 5 6 1. 5 1 .7 6 2 . 60 3 .8 4 5 .6 8 8 .4 2 1 0. 43

    0 .0 05 0 20 .4 1 . 02 1 . 28 1 . 60 2 . 37 3 . 50 0 .0 06 5 40 .4 0 . 95 1 . 4 0 2 .0 8 3 . 08 4 .5 5 5 .6 6 0 .0 06 5 4 0. 4 1 . 0 9 1 .6 2 2 . 39 3 .5 4 5 .2 3 6 .5 0 0 .0 09 0 7 3. 3 2 .1 1 3 . 13 4 .6 2 6 .8 4 1 0. 13 1 2. 54

    0 .0 05 8 24 .4 1 . 19 1 . 49 1 . 86 2 . 74 4 . 06 0 .0 06 8 44 .5 0 . 99 1 . 4 7 2 .1 8 3 . 22 4 .7 7 5 .9 2 0 .0 06 8 4 4. 5 1 . 1 4 1 .6 9 2 . 50 3 .7 1 5 .4 8 6 .8 1 0 .0 09 3 7 6. 0 2 .2 4 3 . 27 4 .7 8 6 .9 9 1 0. 48 1 2. 98

    0 .0 06 2 26 .6 1 . 26 1 . 58 1 . 98 2 . 94 4 . 34 0 .0 07 0 46 .6 1 . 02 1 . 5 1 2 .2 4 3 . 31 4 .9 0 6 .1 0 0 .0 07 0 4 6. 6 1 . 1 8 1 .7 4 2 . 58 3 .8 1 5 .6 4 7 .0 1 0 .0 09 6 7 8. 2 2 .2 5 3 . 33 4 .9 2 7 .2 8 1 0. 78 1 3. 36

    0 .0 07 6 33 .7 1 . 55 1 . 94 2 . 42 3 . 58 5 . 29 0 .0 09 0 58 .7 1 . 31 1 . 9 5 2 .8 8 4 . 26 6 .3 0 7 .8 3 0 .0 09 0 5 8. 7 1 . 5 1 2 .2 4 3 . 31 4 .9 0 7 .2 5 9 .0 1 0 .0 11 0 9 0. 0 2 .5 8 3 . 81 5 .6 4 8 .3 4 1 2. 36 1 5. 32

    0 .0 09 0 41 .0 1 . 8 4 2 .3 0 2 . 88 4 .2 6 6 . 30 0 .0 12 0 81 .0 1 . 76 2 .6 0 3 . 84 5 .6 8 8 .4 1 1 0. 45 0 .0 12 0 8 1. 0 2 .0 2 2 . 99 4 .4 2 6 .5 3 9 .6 7 1 2. 02 0 .0 13 0 1 06 .5 3 .0 5 4 . 51 6 .6 6 9 . 86 1 4 .6 0 18 .0 90 .0 10 4 4 8. 0 2 . 13 2 .6 6 3 . 33 4 .9 2 7 . 29 0 .0 17 0 11 7. 0 2 .4 9 3 . 68 5 .4 4 8 .0 5 1 1. 91 1 3. 20 0 .0 17 0 1 17 .0 2 .8 6 4 .2 3 6 .2 6 9 .2 6 1 3. 70 1 5. 18 0 .0 14 0 1 15 .0 3 .2 7 4 . 84 7 .1 6 1 0. 59 1 5 .7 0 1 9. 45

    DIRECT REVERSEGRA VURE

    0 .0 00 8 2. 6 0 . 14 0 . 17 0 . 20 0 . 30 0 . 45 0 .0 01 2 5. 7 0 . 14 0 . 21 0 . 31 0 .4 5 0 .6 7 0 .8 4 0 .0 01 2 5 .7 0 .1 6 0 . 24 0 .3 5 0 . 5 2 0 .7 7 0 .9 6 0 .0 02 2 1 8. 0 0 . 41 0 .6 1 0 .9 0 1 .3 2 1 .9 6 2 .4 3

    0 .0 00 9 3. 2 0 . 15 0 . 19 0 . 23 0 . 34 0 . 51 0 .0 01 5 7. 5 0 . 17 0 . 26 0 . 38 0 .5 7 0 .8 4 1 .0 4 0 .0 01 5 7 .5 0 .2 0 0 . 30 0 .4 4 0 . 6 6 0 .9 6 1 .2 0 0 .0 02 5 2 0. 3 0 . 47 0 .6 9 1 .0 2 1 .5 2 2 .2 5 2 .7 8

    0 .0 01 0 3. 4 0 . 16 0 . 20 0 . 26 0 . 38 0 . 56 0 .0 01 8 9. 4 0 . 21 0 . 31 0 . 46 0 .6 8 1 .0 1 1 .2 5 0 .0 01 8 9 .4 0 .2 4 0 . 36 0 .5 3 0 . 7 9 1 .1 6 1 .4 4 0 .0 03 2 2 6. 2 0 . 60 0 .8 9 1 .3 1 1 .9 4 2 .8 7 3 .5 6

    0 .0 02 0 7. 5 0 . 33 0 . 41 0 . 51 0 . 76 1 . 12 0 .0 02 2 10 .9 0 . 19 0 . 32 0 . 51 0 .8 3 1 .2 4 1 .5 3 0 .0 02 2 1 0. 9 0 . 22 0 .3 6 0 . 59 0 .9 6 1 .4 2 1 .7 6 0 .0 03 5 2 8. 8 0 . 66 0 .9 7 1 .4 4 2 .1 3 3 .1 6 3 .9 1

    0 .0 02 2 8. 2 0 . 36 0 . 45 0 . 56 0 . 83 1 . 23 0 .0 02 5 13 .3 0 . 29 0 . 43 0 . 64 0 .9 5 1 .4 0 1 .7 4 0 .0 02 5 1 3. 3 0 . 34 0 .5 0 0 . 74 1 .0 9 1 .6 1 2 .0 0 0 .0 03 9 3 2. 3 0 . 73 1 .0 8 1 .6 0 2 .3 7 3 .5 1 4 .3 5

    0 .0 02 5 9. 7 0 . 41 0 . 51 0 . 64 0 . 95 1 . 40 0 .0 02 8 15 .0 0 . 33 0 . 48 0 . 72 1 .0 6 1 .5 7 1 .9 5 0 .0 02 8 1 5. 0 0 . 38 0 .5 6 0 . 82 1 .2 2 1 .8 0 2 .2 4 0 .0 04 0 3 2. 7 0 . 76 1 .1 2 1 .6 5 2 .4 4 3 .6 1 4 .4 7

    0 .0 03 0 11 .0 0 . 49 0 . 61 0 . 77 1 . 14 1 . 68 0 .0 03 0 16 .0 0 . 35 0 . 5 2 0 .7 7 1 . 14 1 .6 8 2 .0 9 0 .0 03 0 1 6. 0 0 . 4 0 0 .6 0 0 . 88 1 .3 1 1 .9 4 2 .4 0 0 .0 04 5 3 6. 8 0 .8 4 1 . 25 1 .8 4 2 .7 3 4 .0 3 5 .0 0

    0 .0 03 2 11 .9 0 . 52 0 . 65 0 . 82 1 . 21 1 . 79 0 .0 03 2 17 .2 0 . 38 0 . 5 5 0 .8 2 1 . 21 1 .7 9 2 .2 3 0 .0 03 2 1 7. 2 0 . 4 3 0 .6 4 0 . 94 1 .3 9 2 .0 6 2 .5 6 0 .0 05 1 4 1. 8 0 .9 6 1 . 42 2 .1 0 3 .1 0 4 .6 0 5 .6 9

    0 .0 03 3 12 .2 0 . 54 0 . 68 0 . 84 1 . 25 1 . 85 0 .0 03 9 21 .4 0 . 46 0 . 6 7 1 .0 0 1 . 48 2 .1 9 2 .7 1 0 .0 03 9 2 1. 4 0 . 5 2 0 .7 8 1 . 15 1 .7 0 2 .5 2 3 .1 2 0 .0 05 5 4 5. 0 1 .0 3 1 . 53 2 .2 6 3 .3 4 4 .9 5 6 .1 2

    0 .0 03 5 13 .9 0 . 66 0 . 77 0 . 90 1 . 32 1 . 96 0 .0 04 4 26 .3 0 . 51 0 . 7 6 1 .1 3 1 . 67 2 .4 6 3 .0 7 0 .0 04 4 2 6. 3 0 . 5 9 0 .8 7 1 . 30 1 .9 2 2 .8 3 3 .5 3 0 .0 06 0 4 9. 0 1 .1 2 1 . 66 2 .4 6 3 .6 5 5 .4 0 6 .6 9

    0 .0 03 8 16 .0 0 . 63 0 . 78 0 . 97 1 . 44 2 . 13 0 .0 04 9 30 .0 0 . 57 0 . 8 5 1 .2 5 1 . 86 2 .7 5 3 .4 1 0 .0 04 9 3 0. 0 0 . 6 6 0 .9 7 1 . 44 2 .1 3 3 .1 6 3 .9 2 0 .0 06 5 5 3. 3 1 .2 2 1 . 81 2 .6 8 3 .9 6 5 .8 6 7 .2 6

    0 .0 04 0 17 .3 0 . 66 0 . 82 1 . 02 1 . 52 2 . 24 0 .0 05 4 32 .0 0 . 63 0 . 9 3 1 .3 8 2 . 05 3 .0 3 3 .7 6 0 .0 05 4 3 2. 0 0 . 7 2 1 .0 7 1 . 59 2 .3 6 3 .4 8 4 .3 3 0 .0 07 3 5 9. 6 1 .3 7 2 . 03 3 .0 0 4 .4 3 6 .5 6 8 .1 3

    0 .0 04 5 18 .0 0 . 74 0 . 92 1 . 15 1 . 70 2 . 52 0 .0 06 0 35 .4 0 . 70 1 . 0 4 1 .5 4 2 . 27 3 .3 7 4 .1 8 0 .0 06 0 3 5. 4 0 . 8 1 1 .1 9 1 . 77 2 .6 1 3 .8 7 4 .8 1 0 .0 07 5 6 1. 5 1 .4 0 2 . 08 3 .0 7 4 .5 4 6 .7 3 8 .3 5

    0 .0 05 0 20 .4 0 . 82 1 . 02 1 . 28 1 . 89 2 . 80 0 .0 06 5 40 .4 0 . 76 1 . 1 2 1 .6 6 2 . 46 3 .6 4 4 .5 2 0 .0 06 5 4 0. 4 0 . 8 7 1 .2 9 1 . 91 2 .8 3 4 .1 9 5 .2 0 0 .0 09 0 7 3. 3 1 .6 9 2 . 50 3 .7 0 5 .4 7 8 .1 0 1 0. 04

    0 .0 05 8 24 .4 0 . 95 1 . 19 1 . 48 2 . 20 3 . 25 0 .0 06 8 44 .5 0 . 79 1 . 1 7 1 .7 4 2 . 58 3 .8 1 4 .7 4 0 .0 06 8 4 4. 5 0 . 9 1 1 .3 5 2 . 00 2 .9 7 4 .3 9 5 .4 5 0 .0 09 3 7 6. 0 1 .7 9 2 . 62 3 .8 3 5 .5 9 8 .3 8 1 0. 39

    0 .0 06 2 26 .6 1 . 01 1 . 27 1 . 59 2 . 35 3 . 48 0 .0 07 0 46 .6 0 . 82 1 . 2 1 1 .7 9 2 . 65 3 .9 2 4 .8 8 0 .0 07 0 4 6. 6 0 . 9 4 1 .3 9 2 . 06 3 .0 5 4 .5 1 5 .6 1 0 .0 09 6 7 8. 2 1 .8 0 2 . 66 3 .9 4 5 .8 2 8 .6 3 1 0. 69

    0 .0 07 6 33 .7 1 . 24 1 . 55 1 . 93 2 . 86 4 . 23 0 .0 09 0 58 .7 1 . 05 1 . 5 6 2 .3 0 3 . 41 5 .0 4 6 .2 7 0 .0 09 0 5 8. 7 1 . 2 1 1 .7 9 2 . 65 3 .9 2 5 .8 0 7 .2 1 0 .0 11 0 9 0. 0 2 .0 6 3 . 05 4 .5 1 6 .6 8 9 .8 9 1 2. 26

    0 .0 09 0 41 .0 1 . 47 1 . 84 2 . 30 3 . 41 5 . 04 0 .0 12 0 81 .0 1 . 40 2 . 0 8 3 .0 7 4 . 54 6 .7 3 8 .3 6 0 .0 12 0 8 1. 0 1 . 6 1 2 .3 9 3 . 53 5 .2 3 7 .7 4 9 .6 1 0 .0 13 0 1 06 .5 2 .4 4 3 . 60 5 .3 3 7 .8 8 1 1. 68 1 4. 470 .0 10 4 4 8. 0 1 . 71 2 .1 3 2 . 66 3 .9 4 5 . 83 0 .0 17 0 11 7. 0 1 .9 9 2 . 94 4 .3 5 6 .4 4 9 .5 3 1 0. 56 0 .0 17 0 1 17 .0 2 .2 9 3 .3 8 5 .0 0 7 .4 0 1 0. 96 1 2. 14 0 .0 14 0 1 15 .0 2 .6 2 3 . 87 5 .7 3 8 . 47 1 2 .5 6 1 5. 56

    0 .0 00 8 2. 6 0 . 06 0 . 07 0 . 08 0 . 12 0 . 18 0 .0 01 2 5. 7 0 . 06 0 . 09 0 . 13 0 .1 9 0 .2 8 0 .3 5 0 .0 01 2 5 .7 0 .0 7 0 . 10 0 .1 5 0 . 2 2 0 .3 2 0 .4 0 0 .0 02 2 1 8. 0 0 . 17 0 .2 5 0 .3 7 0 .5 5 0 .8 1 1 .0 0

    0 .0 00 9 3. 2 0 . 06 0 . 08 0 . 10 0 . 14 0 . 21 0 .0 01 5 7. 5 0 . 07 0 . 11 0 . 16 0 .2 3 0 .3 5 0 .4 3 0 .0 01 5 7 .5 0 .0 8 0 . 12 0 .1 8 0 . 2 7 0 .4 0 0 .4 9 0 .0 02 5 2 0. 3 0 . 19 0 .2 9 0 .4 2 0 .6 3 0 .9 3 1 .1 5

    0 .0 01 0 3. 4 0 . 07 0 . 08 0 . 11 0 . 16 0 . 23 0 .0 01 8 9. 4 0 . 09 0 . 13 0 . 19 0 .2 8 0 .4 2 0 .5 2 0 .0 01 8 9 .4 0 .1 0 0 . 15 0 .2 2 0 . 3 2 0 .4 8 0 .6 0 0 .0 03 2 2 6. 2 0 . 25 0 .3 7 0 .5 4 0 .8 0 1 .1 9 1 .4 7

    0 .0 02 0 7. 5 0 . 14 0 . 17 0 . 21 0 . 31 0 . 46 0 .0 02 2 10 .9 0 . 08 0 . 13 0 . 21 0 .3 4 0 .5 1 0 .6 3 0 .0 02 2 1 0. 9 0 . 09 0 .1 5 0 . 24 0 .3 9 0 .5 9 0 .7 3 0 .0 03 5 2 8. 8 0 . 27 0 .4 0 0 .5 9 0 .8 8 1 .3 0 1 .6 1

    0 .0 02 2 8. 2 0 . 15 0 . 18 0 . 23 0 . 34 0 . 51 0 .0 02 5 13 .3 0 . 12 0 . 18 0 . 26 0 .3 9 0 .5 8 0 .7 2 0 .0 02 5 1 3. 3 0 . 14 0 .2 1 0 . 30 0 .4 5 0 .6 6 0 .8 3 0 .0 03 9 3 2. 3 0 . 30 0 .4 5 0 .6 6 0 .9 8 1 .4 5 1 .7 9

    0 .0 02 5 9. 7 0 . 17 0 . 21 0 . 26 0 . 39 0 . 58 0 .0 02 8 15 .0 0 . 13 0 . 20 0 . 30 0 .4 4 0 .6 5 0 .8 1 0 .0 02 8 1 5. 0 0 . 15 0 .2 3 0 . 34 0 .5 0 0 .7 4 0 .9 3 0 .0 04 0 3 2. 7 0 . 31 0 .4 6 0 .6 8 1 .0 1 1 .4 9 1 .8 5

    0 .0 03 0 11 .0 0 . 20 0 . 25 0 . 32 0 . 47 0 . 69 0 .0 03 0 16 .0 0 . 14 0 . 2 1 0 .3 2 0 . 47 0 .6 9 0 .8 6 0 .0 03 0 1 6. 0 0 . 1 7 0 .2 5 0 . 36 0 .5 4 0 .8 0 0 .9 9 0 .0 04 5 3 6. 8 0 .3 5 0 . 51 0 .7 6 1 .1 2 1 .6 6 2 .0 6

    0 .0 03 2 11 .9 0 . 21 0 . 27 0 . 34 0 . 50 0 . 74 0 .0 03 2 17 .2 0 . 15 0 . 2 3 0 .3 4 0 . 50 0 .7 4 0 .9 2 0 .0 03 2 1 7. 2 0 . 1 8 0 .2 6 0 . 39 0 .5 7 0 .8 5 1 .0 6 0 .0 05 1 4 1. 8 0 .4 0 0 . 59 0 .8 7 1 .2 8 1 .9 0 2 .3 5

    0 .0 03 3 12 .2 0 . 22 0 . 28 0 . 35 0 . 51 0 . 76 0 .0 03 9 21 .4 0 . 19 0 . 2 8 0 .4 1 0 . 61 0 .9 0 1 .1 2 0 .0 03 9 2 1. 4 0 . 2 2 0 .3 2 0 . 47 0 .7 0 1 .0 4 1 .2 9 0 .0 05 5 4 5. 0 0 .4 3 0 . 63 0 .9 3 1 .3 8 2 .0 4 2 .5 3

    0 .0 03 5 13 .9 0 . 27 0 . 32 0 . 37 0 . 55 0 . 81 0 .0 04 4 26 .3 0 . 21 0 . 3 1 0 .4 6 0 . 69 1 .0 2 1 .2 6 0 .0 04 4 2 6. 3 0 . 2 4 0 .3 6 0 . 53 0 .7 9 1 .1 7 1 .4 5 0 .0 06 0 4 9. 0 0 .4 6 0 . 69 1 .0 2 1 .5 0 2 .2 3 2 .7 6

    0 .0 03 8 16 .0 0 . 26 0 . 32 0 . 40 0 . 59 0 . 88 0 .0 04 9 30 .0 0 . 24 0 . 3 5 0 .5 2 0 . 77 1 .1 3 1 .4 1 0 .0 04 9 3 0. 0 0 . 2 7 0 .4 0 0 . 60 0 .8 8 1 .3 0 1 .6 2 0 .0 06 5 5 3. 3 0 .5 0 0 . 75 1 .1 0 1 .6 3 2 .4 2 2 .9 9

    0 .0 04 0 17 .3 0 . 27 0 . 34 0 . 42 0 . 63 0 . 92 0 .0 05 4 32 .0 0 . 26 0 . 3 8 0 .5 7 0 . 84 1 .2 5 1 .5 5 0 .0 05 4 3 2. 0 0 . 3 0 0 .4 4 0 . 66 0 .9 7 1 .4 4 1 .7 9 0 .0 07 3 5 9. 6 0 .5 7 0 . 84 1 .2 4 1 .8 3 2 .7 1 3 .3 5

    0 .0 04 5 18 .0 0 . 30 0 . 38 0 . 48 0 . 70 1 . 04 0 .0 06 0 35 .4 0 . 29 0 . 4 3 0 .6 3 0 . 94 1 .3 9 1 .7 2 0 .0 06 0 3 5. 4 0 . 3 3 0 .4 9 0 . 73 1 .0 8 1 .6 0 1 .9 8 0 .0 07 5 6 1. 5 0 .5 8 0 . 86 1 .2 7 1 .8 7 2 .7 8 3 .4 4

    0 .0 05 0 20 .4 0 . 34 0 . 42 0 . 53 0 . 78 1 . 16 0 .0 06 5 40 .4 0 . 31 0 . 4 6 0 .6 9 1 . 02 1 .5 0 1 .8 7 0 .0 06 5 4 0. 4 0 . 3 6 0 .5 3 0 . 79 1 .1 7 1 .7 3 2 .1 5 0 .0 09 0 7 3. 3 0 .7 0 1 . 03 1 .5 3 2 .2 6 3 .3 4 4 .1 4

    0 .0 05 8 24 .4 0 . 39 0 . 49 0 . 61 0 . 91 1 . 34 0 .0 06 8 44 .5 0 . 33 0 . 4 8 0 .7 2 1 . 06 1 .5 7 1 .9 5 0 .0 06 8 4 4. 5 0 . 3 8 0 .5 6 0 . 83 1 .2 2 1 .8 1 2 .2 5 0 .0 09 3 7 6. 0 0 .7 4 1 . 08 1 .5 8 2 .3 1 3 .4 6 4 .2 8

    0 .0 06 2 26 .6 0 . 42 0 . 52 0 . 65 0 . 97 1 . 43 0 .0 07 0 46 .6 0 . 34 0 . 5 0 0 .7 4 1 . 09 1 .6 2 2 .0 1 0 .0 07 0 4 6. 6 0 . 3 9 0 .5 7 0 . 85 1 .2 6 1 .8 6 2 .3 1 0 .0 09 6 7 8. 2 0 .7 4 1 . 10 1 .6 2 2 .4 0 3 .5 6 4 .4 1

    0 .0 07 6 33 .7 0 . 51 0 . 64 0 . 80 1 . 18 1 . 75 0 .0 09 0 58 .7 0 . 43 0 . 6 4 0 .9 5 1 . 41 2 .0 8 2 .5 8 0 .0 09 0 5 8. 7 0 . 5 0 0 .7 4 1 . 09 1 .6 2 2 .3 9 2 .9 7 0 .0 11 0 9 0. 0 0 .8 5 1 . 26 1 .8 6 2 .7 5 4 .0 8 5 .0 6

    0 .0 09 0 41 .0 0 . 61 0 . 76 0 . 95 1 . 41 2 . 08 0 .0 12 0 81 .0 0 . 58 0 . 8 6 1 .2 7 1 . 87 2 .7 7 3 .4 5 0 .0 12 0 8 1. 0 0 . 6 7 0 .9 9 1 . 46 2 .1 6 3 .1 9 3 .9 7 0 .0 13 0 1 06 .5 1 .0 1 1 . 49 2 .2 0 3 .2 5 4 .8 2 5 .9 7

    0 .0 10 4 48 .0 0 . 7 0 0 .8 8 1 . 10 1 .6 2 2 . 41 0 .0 17 0 11 7. 0 0 .8 2 1 . 21 1 . 80 2 .6 6 3 .9 3 4 .3 6 0 .0 17 0 1 17 .0 0 .9 4 1 . 40 2 .0 6 3 .0 5 4 .5 2 5 .0 1 0 .0 14 0 1 15 .0 1 .0 8 1 . 60 2 .3 6 3 . 50 5 .1 8 6 . 42

    TRI-HELICAL CELLCHART #11

    PYRAMIDCELLCHART #12 QUADRANGULAR CELLCHART #13 QUADRANGULAR CHANNELED CELLCHART #14 TRI-HELICAL CELLCHART #15

    QUADRANGULAR CHANNELED CELLCHART#6

    5%

    SOLIDS

    15%

    SOLIDS

    25%

    SOLIDS

    35%

    SOLIDS

    35%

    SOLIDS

    45%

    SOLIDS

    50%

    SOLIDSVOLUME

    5%

    SOLIDS

    15%

    SOLIDS

    25%

    SOLIDS

    45%

    SOLIDS

    50%

    SOLIDS CELL DEPTH

    5%

    SOLIDS

    15%

    SOLIDS

    25%

    SOLIDS

    35%

    SOLIDS

    50%

    SOLIDS CELL DEPTH VOLUME

    15%

    SOLIDS

    25%

    SOLIDS

    35%

    SOLIDS

    45%

    SOLIDS

    CELL

    DEPTH VOLUME

    5%

    SOLIDS

    15%

    SOLIDS

    25%

    SOLIDS

    35%

    SOLIDS

    45%

    SOLIDS

    CELL

    DEPTH VOLUME

    5%

    SOLIDS

    35%

    SOLIDS

    45%

    SOLIDS

    50%

    SOLIDS

    OFFSET GRAVURE OFFSET GRAVURE OFFSET GRAVURE OFFSET GRAVURE

    VOLUME 5%

    SOLIDS

    15%

    SOLIDS

    25%

    SOLIDS

    45%

    SOLIDS

    50%

    SOLIDS CELL DEPTH

    5%

    SOLIDS

    15%

    SOLIDS

    25%

    SOLIDS

    35%

    SOLIDS

    50%

    SOLIDS CELL DEPTH VOLUME

    15%

    SOLIDS

    25%

    SOLIDS

    35%

    SOLIDS

    45%

    SOLIDS

    CELL

    DEPTH VOLUME

    5%

    SOLIDS

    15%

    SOLIDS

    25%

    SOLIDS

    35%

    SOLIDS

    45%

    SOLIDS

    CELL

    DEPTH VOLUME

    5%

    SOLIDS

    PYRAMIDCELLCHART #8 QUADRANGULAR CELLCHART #9 QUADRANGULAR CHANNELED CELLCHART#10

    35%

    SOLIDS

    45%

    SOLIDSCELL DEPTH

    5%

    SOLIDS

    15%

    SOLIDS

    25%

    SOLIDS

    35%

    SOLIDS

    50%

    SOLIDS

    DIRECT REVERSE GRAVURE DIRECT REVERSE GRAVURE DIRECT REVERSE GRAVURE

    VOLUME 5%

    SOLIDS

    15%

    SOLIDS

    25%

    SOLIDS

    45%

    SOLIDS

    50%

    SOLIDS

    50%

    SOLIDS CELL DEPTH VOLUME

    15%

    SOLIDS

    25%

    SOLIDS

    35%

    SOLIDS

    45%

    SOLIDS

    CELL

    DEPTH VOLUME

    5%

    SOLIDS

    15%

    SOLIDS

    25%

    SOLIDS

    35%

    SOLIDS

    45%

    SOLIDS

    CELL

    DEPTH VOLUME

    5%

    SOLIDS

    TRI-HELICAL CELLCHART #7

    6.CHOOSETHEROLL FROM ANY VENDORCHART THAT

    MATCHES THE VOLUME AND CELL TYPE.

    D IR EC T F OR WA RD G RA VU RE D IR EC T F OR WA RD G RA VU RE D IR EC T F OR WA RD G RA VU RE

    PYRAMIDCELLCHART #4 QUADRANGULAR CELLCHART #5

    2.DETERMINETYPEOF GRAVURECOATER

    3.DETERMINETYPEOF GRAVURECELL

    4.FIND THE DESIREDCOATWEIGHT IN THECHART

    5.TRACETHATROLL OVERTO THE VOLUMEINTHESAMECHART

    45%

    SOLIDS

    50%

    SOLIDS

    NOTE: THISISFOR CHROME PLATED GRAVURE ROLLS ONLY!

    1.DETERMINESOLIDS

    50%

    SOLIDS NUMBER CELL DEPTH VOLUME

    15%

    SOLIDS

    25%

    SOLIDS

    35%

    SOLIDS

    45%

    SOLIDSNUMBER

    CELL

    DEPTH VOLUME

    5%

    SOLIDS

    15%

    SOLIDS

    25%

    SOLIDS

    35%

    SOLIDS

    45%

    SOLIDSNUMBER

    CELL

    DEPTH VOLUME

    5%

    SOLIDS

    ENGRAVINGCOATING CHARTWEIGHT INPOUNDSDRYSOLIDS PERREAM - 432,000SQUARE INCHES

    WEIGHT OF MATERIAL 8 LBS. PERGALLONINSOLUTION

    PYRAMIDCELLCHART #1 QUADRANGULAR CELLCHART #2 TRI-HELICAL CELLCHART#3

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    DIRECT GRAVURE

    BACKING; LINESPEED

    Undercut Required

    BACKING/GRAVURE = 3/8 NIP

    GRAVURE; 90% to 110% LINESPEED

    USUALLY REQUIRES POST SMOOTHING

    REVERSE GRAVURE

    BACKING; LINESPEED

    Undercut required

    BACKING/GRAVURE = 3/8 NIP

    GRAVURE; 50% to 150% OF LINESPEED

    OFFSET GRAVURE

    BACKING; LINESPEED

    BACKING/OFFSET =3/8 NIP

    OFFSET; 95% to 105% OF LINESPEED

    Undercut Required

    OFFSET/GRAVURE = 3/8 NIP

    GRAVURE; 10% to 25% OF LINESPEED

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    SMOOTH ROLL

    BACKING; LINESPEED

    NOUndercut Required

    BACKING/PICKUP = VARY NIP

    PICKUP;20% to 150% LINESPEED

    COAT WEIGHT

    NIP WIDTH & ROLL SPEEDCoat weight control is dependent upon the relationship of

    linespeed vs. nip width and pickup roll speed

    By increasing pickup roll speed the coat weight increases

    By decreasing the pickup roll footprint the coat weight

    increases

    Other coat weight variables

    coating solids

    coating viscosity

    Transfer Roll Coater

    Roll vs. Speed

    Roll speed

    Coatweight

    1/2" nip

    3/8" nip

    3/4" nip

    CHECKING NIP

    IMPRESSIONS

    STEEL ROLL

    LOAD

    RUBBERCOVEREDROLL

    FOOTPRINT

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    Coat Weight Curves

    Gravure Volume

    Coating Solids

    Roll Speed

    Coating Viscosity

    GSM

    150%50% 100%

    Gravure Speed

    Reverse

    Gravure

    GSM

    95% 100% 105%

    Gravure Speed

    Forward

    Gravure

    10% 60% 100%

    Gravure Speed

    GSM

    Offset

    Gravure

    10% 100%

    Pick-up Speed

    GSM

    Smooth

    Transfer

    Factors That Affect Coat Weight

    Nip Width

    COAT WEIGHT STABILITYEffects of speed on coatweight

    Differential Offset Gravure -STABLE

    Direct/Reverse Gravure -STABLE

    Smooth Roll -UNSTABLE

    GSM

    Line Speed

    Gravure

    Smooth Roll

    Yesesoes

    bility to Coat Foil

    bility to Coat Foil

    Yesesoes

    bility to Coat

    bility to Coat

    Printed Film

    rinted Film

    Noeseses

    equires Undercut

    equires Undercut

    Rubber Roll

    ubber Roll

    Noeseses

    table at ll Line

    table at ll Line

    Speeds

    peeds

    Yesesesesbility to Coatbility to Coat

    Film

    ilm

    Noeseses

    bility to Coat

    bility to Coat

    Paper

    aper

    Yeseseso

    bility to djust

    bility to djust

    Coat Weight

    oat Weight

    Smooth

    mooth

    Roll

    oll

    Offset

    ffset

    Gravure

    ravure

    Reverse

    everse

    Gravure

    ravure

    Direct

    irect

    Gravure

    ravure

    Coater

    oater

    Selection

    election

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    Thank You

    PRESENTED BY

    Lee A. OstnessProduct ManagerCoating & Drying Systems

    Black Clawson Converting [email protected]

    Please remember to t urn

    in you r evaluation sheet...