1996 SECOND SEMIANNUAL SAMPLING › work › 05 › 155846.pdfAqua Tech Environmental Laboratories,...

APPENDIX A.

1996 SECOND SEMIANNUAL SAMPLING

ANALYTICAL RESULTSAND FIELD MEASUREMENTS

__ ^ _ TABLE A-J"REMGN7 LANDFILL FIELD

MONITORING

ij 10/09/96 MW-1R !MW-3RMW-4 ;MW-6DMW-7S ;MW-7DMW-8SMW-8D :WS96-62WS96-62dup. ;

Ii/26/96 ! MW-8D

MW-3R

30.4520.2644.0 /49,281111i i.L i

I00.9Q28.9073.8312, ?7

32,37

74.28

/J.fid^r> -• •MS.JL-t

983,19987.94984.36

1025.471029.541000.581032.77988,00

1025.361025,36

987.55

7.576.607.697.907.917,767.767.017,827.82

7.24

8541023636688744681689936707703

800

11.9

10.6-^ i -?1 1 i

12.1

11.912.211.010,6

U.5

-l Q

Client*: 10107

ATELAqua Tech Environmental Laboratories, Inc.

CERTIFICATE OF ANALYSIS (REPRINT) -

Eagon & Associates inc

100 Old Wilson Bridge RdSuite 320WortfaJngton, OH 43085

Attn: Frank Majchszak

Our Lab #: MAR96-26776Date Logged-In: 10/11/96

Matrix: WaterProjects

Report Date: 27-Nov-96

Original Report Date: 30-Oct-96

Phone: (614)888-5760 Ext:FAX: (614)888-5763

YoarSampkH): MW-1RSample Source: RCRA

Client ProjectsDate Submitted to Lab: 10/10/96

PO#: Tremont Landfill

- COLLECTION INFORMATION -

TestGronDate/Time/By: 10/9/96

EPA Method Test625PM HEINK

Units

NH3V|f\9NO3

CL-ICSO4-ICPH-LABTDSALKTURBCOND-LSB-GFAAAS-GFAABA-ICPBE-ICPCTMiFAACO-ICPCU-ICPPB-GFAANI-ICPSE-GFAAAG-GFAATL-GFAAV-ICP

350.1 Nitrogen. Ammonia (as N)D3867-90A/9200 Nitrate + Nitrite N

300.0300.0

D1293-84/9040160.1

SM2300B180.1

25108/905031I3B/704I31 138/7060200.7/6010200.7/601031138^7131200.7/6010200.7/6010

3II3B/742I200.7/60103 1 138/77403113B/776I31 138/7841200.7/6010

Chloride, ClSul6te.SO4pH,Lab

Residue. Filterable (DissolviAlkalinity. TotalTurbidityConductivity, LabAntimony, SbArsenic, AsBarium. BaBeryllium. BeCadmium. CdCobalt, CoCopper, CuLead,PbNickel. NiSelenium, ScSilverThallium, TlVanadium. V

WS#

0.060.07

968

7.055614090.6

868<3.0<3.0

156<0.5<OJ<10<10

<2.0<20

<3.0<1.0<1.0<20

MG/LMG/LMOT,MG/LS.U.

MG/LMG/LNTU

uMHOUG/L\\nnUU/L

UG/LUG/LUG/LUG/LUG/LUG/LUGflLUGA.IKVLUG/LUG/L

10/15/9610/17/9610/23/9610/23/9610/10/9610/16/9610/14/9610/10/9610/15/9610/16/9610/19/96I (VI 5/96

10/15/9610/18/9610/15/9610/15/9610/18/9610/15/961071/9610/15/9610/19/9610/15/96

RJARJABKHBKHMDORJASKSDKJKRGSMMROHSMMSMMROHSMMSMMJEL

SMMROHROHROHSMM

555598742

.742512588564527554607639557557625557557627557

660565638557

1776 MARION WALDO RD.PHONE 614-389-5991

MAR96-26776:Page I

BOX 436 MARION, OH 43301-0436•* —— —— FAX 614-389-1410


- CERTIFICATE OF ANALYSIS (REPRINT)-

Test Group EPA Method Test

Lab Number MAR96-26776 -Continuedfrom Previous PageAnalysis

Result Units D,te Analyst WS#

ZN-1CPNA-1CPMG-ICPCA-ICPK.-ICPFE4CPMN-ICPCOD-LOCR-QFAA

200.7/6010200.7/6060200.7/6010200.7/6010200.7/6010200.7/6010200,7/6010410.2/71963113B/7191

Ztac.ZnSodium. MaMagnesium. MgCalcium, CaPotassiuoi. 1CIroo,FeManganese, MnCOD, Low LevelChromium, Cr

<IO93

40.61011.150

769<8

<5.0

Report Approved By:

UG/LMG/LMG/LMG/LMG/LUG/LUG/LMG/LUG/L

^

10/15/9610/15/9610/15/9610/15/9610/15/9610/15/9610/15/9610/11/9610/24/96

A' / ^io*A /*'

SMMSMMSMMSMMSMMSMMSMMBKHJEL

'*£%£

V

557557557557557557557545734

t*•"—*

Lab Number MAK96-26776:Page 2

1776 MARION WALDO RD. P.O. BOX 436 MARION, OH 43301-0436PHONE 614-389-5991 1-800-873-2835 FAX 614-389-1410

Aqua Tech Environmental Laboratories, Inc.

Client* EAGON 6 ASSOCIATES INCATBL Sample No.: 96-14271-MELDate Sampled: 10/09/96Date Receivedt 10/11/96Date Analyzed 8260: 10/15/96Date Analyzed 8240: 10/21/96Client ID: MW-1R

Method: SW-846; 8260, 8240(SIM)Sample Type: WATERPercent Solids:Analyst: SPH/JSMProject No.rTREMONT LANDFILL

Compound Concentration - ug/1 (ppb)

Acetone <Acrylonitrile (SIM) <Benzene <Bromochlorome thane <Bronodlchloromethane <Broaofona «Carbon Disulfide <Carbon Tetrachloride <Chlorobenzene <Chloroe thane <Chloroform <Dlbromochloromethane *it 2 -Dlbromo -3 -chloropropane «lf 2 -Dibrotmoe thane <o -Dichlorobenzene «-p-Dichlorobenzene <-trans-l,4-Dichloro-2-Butene <.1,1 -Dichloroe thane «JL,2-Dichloroethane - <J., 1-Dichloroe thene «cis-l,2-Dichloroethene «trans -1,2 -Dichloroe thene <1,2 -Dichloropropane <eis- 1,3 -Dichloropropene <trans -1,3 -Dichloropropene <Xthyl Benzene <2 -Hexanone «Bromome thane «£hlorome thane «Dibromome thane «itethylene Chloride <

: 5.0: 5.0: 1.0: 1.0: 1.0: 1.0: 5.0: 1.0: 1.0: 1.0: 0.5: 1.0: 1.0c 1.0: 1.0: 1.0: 1.0: 0.5: 0.5: 0.5: 0.5: 0.5: 1.0: 1.0: 1.0: 1.0: 10.0c 1.0: 1.0c 1.0c 1.0

2 -Butanone

4 -Methyl - 2 - Pen tan oneStyrene1,1,1,2- Tetrachloroethane1, 1, 2, 2 -TetrachloroethaneTetrachloroe theneToluene1, 1, 1-Trichloroe thane1,1,2 -Trichloroe thaneTrichloroe theneTrichlorof luorome thane1,2,3 -TrichloropropaneVinyl AcetateVinyl ChlorideTotal Xylenes

Surrogate Data: % Rec<

Bromofluorobenzene 94Toluene -d8 106Benzene-d6 105

< 10.0< 10.0< 20.0< 1.0< 1.0< 1.0< 1.0< 1.0< 1.0< 1.0< 0.5< 1.0< 1.0< 10.0< 1.0< 2.0

jvery

(70-115)(86-115)(88-110)(75-120)

6878 S. STATE ROUTE 100 • P.O. BOX 76 • MELMORE. OH 44845-9999PHONE 419-397-2659 • 1-800-858-8869 • FAX 419-397-2229


- CERTIFICATE OF ANALYSIS (REPRINT) -Client #: 10107

Eagon & Associates Inc

100 Old Wilson Bridge RdSuite 320Worthington, OH 43085



Matrix: WaterProject #:

Your Sample ID: MW-3RSample Source: RCRA

Client Project «fcDate Submitted to Lab: 10/10/96

Report Date: 27-Nav-96


Phone: (614)888-5760 Ext:FAX: (614)888-5763

Tremont Landfill

- COLLECTION INFORMATION -Date/Tirae/By: 10/9/96 10 JO AM HED4K

TestGron

NH3NO3CL4CSO4-ICPH-LABTDSALKTURBCOND-LSB-GFAAAS-GFAABA-ICPBE-ICPCD-GFAACO-ICPCIMCPPB-GFAANHCPSE-GFAAAG-GFAATL-GFAAV-1CP

EPA Method

350.1D3867-90A/9200

300.0300.0

D1293-84/9040160.1

SM2300B180.1

2510B/90503113B/70413113B/7060200.7/6010200.7/60103U3B/7131200.7/6010200.7/60103113B/7421200.7/60103H3B/77403I13B/776I3II3B/784I200.7/6010

Test

Nitrogen, Ammonia (as N)Nitrate + Nitrite NChloride. ClSulfete,SO4pH,LabResidue, Filterable (Dissolved Solids)Alkalinity, TotalTurbidityConductivity, LabAntimony, SbArsenic, AsBarium, BaBeryllium, BeCadmium, CdCobalt, CoCopper, CuLead,PbNickel, NiSelenium, SeSilverThallium, TlVanadium, V

Result

<0.05<0.05

1250

6.82620500

181020<3.0<3.0273

<0.5<OJ<10<10<2.0<20<3.0<l.O<1.0<20

UBltS

MG/LMG/LMG/LMG/LS.U.

MG/LMG/LNTU

uMHOUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/L

AmaryibDate A

10/15/9610/17/9610/23/9610/23/9610/10/9610/16/9610/14/9610/10/9610/15/9610/16/9610/19/9610/15/9610/15/9610/18/9610/15/9610/15/9610/18/96

10/15/9610/16/96

10/15/9610/19/9610/15/96

analyst

RJARJABKHBKHMDORJASKSDKJKRGSMMROHSMM "SMMROHSMMSMMJEL

SMMROHROHROHSMM

WS#

555598742742512588564527554607639557557625557557627557579565638557

Lab Number MAR96-26777.Page I


ATELLatmatorieSi /JK.

-CERTIFICATE OP ANALYSIS (REPRINT).

Test Group

ZN-fCPNA-ICPMG-JCPCA-ICTK4CPFB4CPMN-ICPCOD-LOCR-OFAA

EPA Method

200.7/6010200.7/6060200.7/6010200.7/6010200.7/6010200.7/6010200.7/60104IOJ/71963113B/7I91

TestZinc,ZnSodiwn,NaMafDesfnm. MgCUdum.CaPoftrathim, KIron, PeMang*Dese.MnCOD. Low LevelChromium, Cr

Resolt UaJti

IKVLMG/LMO/LMG/LMG/LUG/LU01MOT.

UCVL

11.84621101.9

2780110

9<5.0

AaalvsbPate

10/15/9610/13/9610/15^610/15/9610/15>9610/15/9610/15/9610/11/9610/24/96

Previous Page

Analyst


WS#

557557557557557557557545734

R*port Approved By:

LabNu

1776 MARION WALDO RO. P.O. BOX 436 MARION, OH 43301-0436PHONE 614-389-5991 1-800-873-2835 FAX 614-389-1410

lab Number MAR96-26777:Pagc 2


Clients EAGON & ASSOCIATES INCATEL Sample No. t 96-14272-MELDate Sampled: 10/09/96Date Received! 10/11/96Date Analyzed 8260s 10/15/96Date Analyzed 8240: 10/21/96Client ID: MW-3R

Method: SW-846} 8260, 8240(SIM)Sample Type: MATERPercent Solids:Analys t: SPH/JSMProject No.:TREMQHT LANDFILL


AcetoneAcrylonitrile (SIM)BenzeneHTV"nnnrt Vi 1 r\T-flmfk*-Vi«iTi«»BronK>(lichToroiniwt:hiiP*»BromoformCarbon DisulfideCarbon TetrachlorideChlorobenzeneChloroethaneChloroformPj*1?ronK>chloTC>w3t!' |g'T>**1,2 -Dibromo - 3 - chloropropane1, 2 -Dibromoethaneo -DichlorobenzeneT> - Pi r?hl r>ToV>°Ti Kflnfltrans- 1, 4-Dichloro-2 -Butene1, 1 -Dichloroe thane1,2 -Dichloroe thane —1, 1 -Dichloroe thenecis-1, 2 -Dichloroethenetrans -1,2 -Dichloroethene1,2 -Dichloropropanecis -1,3 -Dichloropropenetrans- 1, 3 -DichloropropeneEthyl Benzene2-HexanoneBrtjmoin© t ha n f?ChlorooMst"- " *"*DibromomethaneMethylene Chloride

<<<

<<<<<<<<<<<<<<<<<<<<<<<<<<<

5.05.01.01.01.01.05.01.01.01.00.51.01.01.01.01.01.00.50.50.50.50.51.01.01.01.010.01.01.01.01.0

2-Butanone < 10.0«^ —-•_,., _ 4-.m »•»« n ^ «| f\ t\iV/OwUlTTTr IrT***** ^ 1 Ip _ 11

4-Methyl-2-Pentanone < 20.0Styrene < 1.01,1, 1,2 -Tetrachloroe thane < 1.01,1, 2, 2 -Tetrachloroe thane < 1.0Tetrachloroethene < 1.0Toluene < 1.01,1,1 -Trichloroethane < 1.01,1, 2 -Trichloroe thane < 1.0Trichloroethene < 0.5Trichlorof luoromethane < 1.01,2,3-Trichloropropane < 1.0Vinyl Acetate < 10.0Vinyl Chloride < 1.0Total Xvlenes < 2.0

Surrogate Data: % Recovery— _

Dibromof luoromethane 98 (70-115)Bromofluorobenzene 93 (86-115)Toluene-d8 93 (88-110)Benzene-d6 103 (75-120)

6878 S. STATE ROUTE 100 • P.O. BOX 76 • MELMORE, OH 44845-9999PHONE 419-397-2659 • 1-800-858-8869 • FAX 419-397-2229


- CERTIFICATE OF ANALYSIS -Client* 10107 Report Date: IS-Dec-96

Bagon & Associates Inc100 OW Wilson Bridge RdSuite 320Wortbingtan, OH 43085 Phone:(614)888-5760 Ext:

Attn: Chris Cobel FAX: (614)888-5763

Our Lab #: MAR96-32409 Your Sample ID: MW-3RDate Logged-In: 12/17/96 Sample Soarce: Groundwater Monitoring

Matrix: Water Client Project ft POfcProject <fc TREMONTLA Date Submitted to Lab: 12/16796

- COLLECTION INFORMATION -Date/Time/By: 12/16/96 COBEL

AnalysisTest Group EPA Method Test Result Units Date Analyst WS#

COD-LO 410.2/7196 COD, Low Level <8 MG/L 12/17/96 BSR 1548End of Report

Report Approved By:

Lab Number MAR96-32409:Page I

1776 MARION WALDO RD. P.O. BOX 436 MARION, OH 43301-0436PHONE 614-389-5991 1400-873-2835 FAX 614-389-1481



Eagon&A iates Inc

100 OW Wilson Bridge RdSuite 320Worthington,OH 430S5


Our Lab #: MAR96-26778Date Logged-la: 10/11/96


Your Sample ID: MW-4Sample Source: RCRA

Client Project*:Date Submitted to Lab: 10/10/96

Report Date: 27-Nav-96Original Report Date: 30-Oct-96

Phone: (614)888-5760 Ext:FAX: (614)888-5763

POfe Tremont Landfill

- COLLECTION INFORMATION -Date/Time/By: 10/9/96 6:00 PM HED4K

TestGron EPA Method Test Remit UnitsAnalysis

Date Analyst WS#

NH3NO3CL4CSO4-ICPH-LABIDSALKTURBCOND-LSB-GFAAAS-OFAABA-ICP~BE4CPCO-OFAACO-ICPCU-ICPPB-OFAANMCPSE-GFAAAG-OFAATL-OFAAV-ICP

350.1D3867-90A/9200

300.0300.0

D1293-S4/9040160.1

SM2300B180.1

2510B/905031I3B/70413113B/7060200.7/6010200.7/60103113B/7131200.7/6010200.7/60103113B/7421200.7/60103113B/77403113B/T7613113B/7841200.7/6010

Nitrogen, Ammonia (as N)Nitrate + Nitrite NChloride, ClSulfete,SO4pH,LabResidue, Filterable (Dissolved Solids)Alkalinity, TotalTurbidityConductivity, LabAntimony, SbArsenic, AsBarium, BaBeryllium, BeCadmium, CdCobalt, CoCopper, CuLead,PbNickel, NiSelenium, SeSilverThallium, TlVanadium, V

0.08<0.05

6IS

7.29381348

16638

<3.03.2244

<OJ<0.5<10<10<2.0<20<3.0<1.0<1.0<20


MG/LMG/LKTU

uMHOUO/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/L

10/15/9610/17/9610/23/9610/23/9610/10/9610/16/9610/14/9610/10/9610/15/9610/16/9610/19/9610/15/9610/15/9610/18/9610/15/9610/15/9610/18/9610/15/96

10/16/9610/15/9610/19/9610/15/96


SMMROHROHROHSMM

555598742742512588564527554607639557557625557557627557579565638557




- CERTIFICATE OF ANALYSIS (REPRINT) -

Test Group

ZN-ICPNA-ICPMG-ICPCA-ICPK-ICPFE4CPMN-ICPCOD-LOCR-GFAA

EPA Method

200.7/6010200.7/6060200.7/6010200.7/6010200.7/5010200.7/6010200.7/6010410.2/7196

3113B/7191

Test

Zinc,ZnSodium. MaMagnesium, MgCakhmvCaPotassium,KIroo,FcManganese, MnCOD, Low LevelChromium, Cr

Result• •M^m

<IO10.629.271.41.1

11906712

<5.0

UntoUO/LMG/LMG/LMG/LMG/LUG/LUG/LMG/LUG/L

AnalysisDate '«~«>_«MI10/15/9610/15/9610/15/9610/15/9610/15/9610/15/9610/15/9610/11/9610/24/96

taafyst—— —— .


WS#•— •— —

557557557557557557557545734

Report Approved By:

LOO NU

1776 MARION WALDO RD. P.O. BOX 436 MARION, OH 43301-0436PHONE 614-389-5991 1-800-87*4835 FAX 614-389-1410

Lab Number MAR96-26778:Page 2

^[^LMm^^jR^Sz^SiSjjSjs^j^^^^^^^^

Aqua Ikefe Environmental Laboratories, Inc.

Client: BAGON ft ASSOCIATES INCATEL Sample No.s 96-14273-MELDate Sampled: 10/09/96Date Received: 10/11/96Date Analyzed 8260s 10/15/96Date Analyzed 8240: 10/21/96Client IDs MW-4

Compound

Method: SW-846j 8260, 8240(SIM)Sample Types WATERPercent SolidssAnalysts SPH/JSMProject Ho.sTRBUQNT LANDFILL

Concentration - ug/1 (ppb)

Acetone «Acrylonitrile (SIM) «Benzene «T*T* TflBll f r {JiC TWI ^ T fl T n *^ T OBOi ^ * • 1 1 TT THM ^ I ^ ^ *Broao£orm <Carbon Disulf ide <Carbon Tetrachloride <Chlorobenzene «Chloroethane «Chloroform <PlbrowQchl OT*onM»thiMH? *l,2-Dibromo-3-chloropropane <1,2 -Dibromoe thane «o -Dichlorobenzene <P -Dichlorobenzene «trans-1, 4-Dichloro-2-Butene «lff 1-Dichloroethane «1, 2 -Dichloroe thane «If 1-Dichloroethene <cis -1,2 -Dichloroethene «trans -1,2 -Dichloroethene «1,2 -Diohloropropane «cis-1, 3 -Dichloropropene <trans -1,3 -Dichloropropene <Ethyl Benzene «2 -Hexanone «Bromomethane «ChlOT'Wlf fhPTT* «T»4 V»i»r«inom«t-Vi»Ti«Methylene Chloride «

: 5.0: 5.0: 1.0: 1.0: 1.0: 1.0: 5.0: 1.0c 1.0: 1.0: 0.5: 1.0: 1.0: 1.0; 1.0: 1.0c 1.0: 0.5c 0.5: 0.5: 0.5: 0.5: 1.0: 1.0c 1.0: 1.0c 10.0; 1.0: 1.0I n. u

c 1.0

2-Butanone < 10.0Tri^rnnat-VmnA «- 1 O fl

4-Methyl-2-Pentanone < 20.0Styrene < 1.01,1,1,2 -Tetrachloroethane < 1.01,1, 2,2 -Tetrachloroe thane < 1.0Tetrachloroethene < 1.0Toluene < 1.01,1, 1-Trichloroe thane < 1.01,1,2-Trichloroethane < 1.0Trichloroethene < 0.5Trichlorof luoromethane < 1.01,2,3 -Trichloropropane < 1.0Vinyl Acetate < 10.0Vinyl Chloride < 1.0Total Xylenes < 2.0

Surrogate Data: % Recovery-. —Dibronof luoromethane 98 (70-115)Bromofluorobenzene 90 (86-115)Toluene-d8 99 (88-110)Benzene -d6 105 (75-120)

6878 S. STATE ROUTE 100 • P.O. BOX 76 • MELMORE. OH 44845-9999419-397-2659 • 1-800-858-8869 • FAX 419-397-2229

Client #: 10107


CERTIFICATE OF ANALYSIS (REPRINT)


100 Old Wilson Bridge RdSuite 320Wortfaington, OH 43085


Our Lab #: MAR96-26781Date Logged-Ia: 10/11/96

Matrix: WaterProject*:



Pnone: (614)888-5760 Ext:FAX: (614)888-5763

Yo«r Sample ID: MW-6DSample Source: RCRA

Client Project ftDate Submitted to Lab: 10/10/96

- COLLECTION INFORMATION -Date/nme/By: 10/9/96 430PM HEINK

TestGrou EPA Method Test

Tranom Landfill

Result Units *£* ^^

NH3NO3CL-ICSO4-ICPH-LABTDSALKTURBCOND-LSB-OFAAAS-OFAABA-ICPBE4CPCD-GFAACO-ICPCU-ICPPB-GFAANHCPSE-GFAAAO-OFAATL-OFAAV-ICP

350.1D3867-90A9200

300.0300.0

D1293-849040160.1

SM2300B180.1

2510B90503I13B/70413113B/7060200.7«010200.7/6010 |3113B/713I i200.7/6010 <200.7/6010 (31I3B/7421 I200.7/6010 r

3I13B/7740 S31I3B/7761 S3I13B/7841 T200.7/6010 V

Nitrogen, Ammonia (as N)Nitrate+Nitrite NChloride, aSulfide.S04PH,Lab

Residue, Filterable (Dissolved Solids)Alkalinity, TotalTuibidityConductivity, LabAntimony, SbArsenic. AsBarium, BaBeryllium, BeCadmium, CdCobalt, CoCopper, CuLead.PbNickel, NiSelenium, SeSilverThallium. TlVanadium, V

ws#

0.17<0.05

<510

7.273843701.8

649<3.0<3.0262

<0.5<0.5<10< I O

<2.0<20<3.0<1.0<1.0<20

MGVLMGA,M.&LMG/LS.U.

M&LM&LNTU

uMHOUG^LUG^L

"~IKMLUG/LUG/LUG/LUG/LUG/LUG/LUG/L

UG/LUG/LUG/L

10/159610/179610/23/9610/239610/109610/169610/14/9610/109610/159610/169610/199610/159610/159610/189610/159610/159610/189610/159610/169610/159610/199610/1596


SMMROHROHROHSMM

555598742742512588564527554607639557557625557557627557579565638557


Lab Number UAR96-2678l:Page I


- CERTIFICATE OF ANALYSIS (REPRINT)-


Lab Number MAR96-26781 -Continued/root Previous Page

Result UntoAnalysis

rj,te Analyst WS#

ZN-ICPNA-ICPMG4CPCA-ICPK-ICPFE-ICPMN-ICPCOD-LOCR-OFAA

200.7/6010200.7/6060200.7/6010200.7/6010200.7/6010200.7/6010200.7/6010410.2/71963113B/7191

Hnc.ZnSodium, NaMagnesium, MgCalcium, CaPotassium, KIron,FeManganese, MnGOD. Low LevelChromium, Cr

•

<108.1

29.670.3

<1.0155138<8

<5.0

Report Approved By: f


A

10/15/9610/15/9610/15/9610/15/9610/15/9610/15/9610/15/9610/11/9610/24/96

E»

^^


idofRjon

Mtr*w**7

557557557557557557.557545734

f

«— J

Lab Number MAR96-2678l:Page 2



Clients EAOQN & ASSOCIATES INCATBL Saaple No.s 96-14276-MELDate Sampled* 10/09/96Date Receiveds 10/11/96Date Analyzed 8260s 10/15/96Date Analyzed 8240s 10/21/96Client IDs MW-6D

Methods SH-846; 8260, 8240(SIM)Saaple Types WATERPercent SolidssAnalysts SPH/JSMProject No.sTREMONT LANDFILL


Acetone <Acrylonitrile (SIM) <Benzene <

BronodichlorcniethanQ 'Bromoform <Carbon Disulfide <Carbon Tetrachloride <Chlorobenzene <Chloroe thane <Chloroform <DibroHiofrliT.QroMieHiwnf* *l,2-Dibramo-3-chloropropane <1,2- Dibromoe thane «o- Dichlorobenzene <p -Dichlorobenzene <trails- 1, 4 -Dichloro-2-Butene <1, l-Diohloroethane «1,2-Dichloroethane <1,1 -Dichloroethene <cis-1, 2 -Dichloroethene «trans -1,2 -Dichloroethene «1,2 -Dichloropropane «cis-1, 3 -Dichloropropene <trans -1,3 -Dichloropropene <Ethyl Benzene <2 -Hexanone <B7*O9IK>lfl*'t'l1?*T"* 'Chloromethane «Dibromomethane <Methylene Chloride «

: 5.0: 5.0: 1.0I n. V

: 1.0: 1.0: 5.0: 1 . 0: 1.0: 1.0: 0.5: 1.0: 1.0: 1.0: 1.0c 1.0: 1.0: 0.5: 0.5: 0.5: 0.5; 0.5: 1.0: 1.0: 1.0: 1.0: 10.0: 1.0£ 1.0c 1.0c 1.0

2 -ButanoneTodonw *•*•«'"*»4 -Methyl - 2 - Pen tanoneStyrene1, 1, 1,2-Tetrachloroethane1,1,2,2 -Tetrachloroe thaneTetrachloroetheneToluene1 , 1 , 1 - Trichloroe thane1,1, 2 -Trichloroe thaneTrichloroe theneTrlchlorofluorome thane1,2,3 -TrichloropropaneVinyl AcetateVinyl ChlorideTotal Xylenes

Surrogate Data: % Race.._

Dibromofluorome thane 102Bromofluorobenzene 95Toluene -d8 97Benzene -d6 102

< 10.0< 10.0< 20.0< 1.0< 1.0< 1.0< 1.0< 1.0< 1.0< 1.0< 0.5< 1.0< 1.0< 10.0< 1.0< 2.0

>very

(70-115)(86-115)(88-110)(75-120)




Eagon&A

100 Old Wilson Bridge RdSuite 320Worthington,OH 43085


Our Lab ft MAR96-26782Date Logged-la: 10/11/96


Your Sample ID: MW-7SSample Source: RCRA

Client Project #:DateSabmittedtoLab: 10/10/96

Report Date: 27-Nav-96


Phone: (614)888-5760 Ext:FAX: (614)888-5763


- COLLECTION INFORMATION -Date/Time/By: 10/9/96 330PM HEINK

TestGrou EPA Method Test Result UnitsAnalysis

Date Analyst WS#

NH3NO3CL-ICSO4-ICPH-LABTDSALKTURBCOND-LSB-QFAAAS-GFAABA-ICPBE-ICPCD-GFAACO-ICPCU-ICPPB-GFAANHCPSE-OFAAAG-GFAA

TL-GFAAV-ICP

350.1D3867-90A/9200

300.0300.0

D1293-84/9040160.1

SM2300B180.1

2310B/90503113B/70413113B/7060200.7/6010200.7/6010311.38/7131200.7/6010200.7/601031I3B/7421200.7/601031I3B/77403U3B/77613U3B/7841200.7/6010

Nitrogen, Ammonia (as N)Nitrate + Nitrite NChloride, ClSulfcte,SO4pH.LabResidue, Filterable (Dissolved Solids)Alkalinity, TotalTutidityConductivity. LabAntimony, SbArsenic, AsBarium. BaBeryllium, BeCadmium, CdCobalt, CoCopper, CuLcad,PbNickel, NiSelenium, SeSilverThallium, TlVanadium, V

lutO<0.05

<5<2

6.96411419110711

<3.010

407<OJ<0^<IO<10

2.2<20<3.0<1.0<1.0<20


MG/LM&LNTU

uMHOUGA,UG/LUGA-~IKVLUG/LUG/LIKWLUGA,UG/LUGA.UG/LUG/LUG/L

10/15/9610/17/9610/23/9610/23/9610/10/9610/16/9610/14/9610/10/9610/13/9610/16/9610/19/9610/15/9610/15/9610/18/9610/15/9610/15/9610/18/9610/15/9610/16/9610/15/9610/19/9610/15/96


SMMROHROHROHSMM

555598742742512588564527554607639557557625557557627557579565638557

Lab Number M4R96-267S2:Page I



CERTIFICATE OF ANALYSIS (REPRINT) -

Test Group•ZFWCPNA-ICPMG-ICPCA-ICPK-ICPFB-ICPMN-ICPCODiOCR-GFAA

EPA Method-

200.7/6010200.7/6060200.7/6010200.7/6010200.7/6010200.7/6010200.7/6010410.2/7196

3113B/719I

Test•— — —— __

Snc.ZnSodium. N.Magnesium, MgCaJduin.CaPotassium, KIroo,FcManganese, MnCOD. Low LevelChromJom, Cr

^ MAR96-267S2 -Conli^fr^

A ^Analyst ws#

K*P«rt Approved By:



Clients EAGON 6 ASSOCIATES INCATBL Sample No.t 96-14277-MELDate Sampled: 10/09/96Date Received: 10/11/96Date Analyzed 8260s 10/15/96Date Analyzed 8240s 10/21/96Client IDs MW-7S

Method: SW-846j 8260, 8240(SIM)Sample Types HATERPercent SolidssAnalysts SPH/JSMProject No.sTREHDNT LANDFILL

Conpound Concentration - ug/1 (ppb)

AcetoneAcrylonitrile (SIM)BenzeneBroaxxrtiloTomQ thaneBronodJ.cliloronie thaneBromoformCarbon Disulf ideCarbon TetrachlorideChlorobenzeneChloroethaneChloroform

1,2 -Dibromo - 3 - chloropropane1,2-Dibromoethaneo -Dichlorobenzenep-Dichlorobenzenetrans-1, 4-Dichloro-2-Butene1, 1-Dichloroethane1,2 -Dichloroe thane1, 1 -Dichloroetheneois-1, 2 -Dichloroethenebrans- 1, 2 -DichloroetheneL, 2 -Dichloropropanesis-1, 3 -Dichloropropenebrans -1,3 -DichloropropeneSthyl Benzene2 -Hexanone

""hToroiBfs thane)ibromome thanelethylene Chloride

<<<<<<<<<<<

<<<

<<<<<

<<<<

<<<

5.05.01.01.01.01.05.01.01.01.00.51.01.01.01.01.01.00.50.50.50.50.51.01.01.01.010.01.01.01.01.0

2-Butanone < 10.0lodomethane < 10.04-Methyl-2-Pentanone < 20.0Styrene < 1.01,1,1, 2 -Tetraohloroe thane < 1.01,1,2,2-Tetrachloroethane < 1.0Tetrachloroethene < 1.0Toluene < 1.01,1,1-Trichloroe thane < 1.01,1,2 -Trichloroethane < 1.0Trichloroethene < 0.5Triohlarofluoromethftpe *• i-O1,2,3- Tr i chloropropane < 1.0Vinyl Acetate < 10.0Vinyl Chloride < 1.0Total Xylenes < 2.0

Surrogate Data: % Recovery

Dibromofluoromethane 105 (70-115)Bromofluorobenzene 94 (86-115)Toluene-d8 89 (88-110)Benzene -d6 103 (75-120)


Client #: 10107


CERTIFICATE OF ANALYSIS (REPRINT)






Yonr Sample ID: MW-7DSample Sovree: RCRA

CUeat Project ftD*te Submitted to Ub: 10/10/96

Report Date: 27.Nm.96Original Report Date: 30-Oct-96

Plume: (614) 888-5760FAX: (614)888-5763

WMfe Tremont Landfill

TestGroD

NH3.NO3CL-ICS04-ICPH-LABTDSALKTURBCOND-LSB-GFAAAS-OFAABA-1CPBE-ICPCD-OFAACO-ICPCU-ICPPB-GFAANHCPSE-OFAAAO-OFAATL-GFAAV-ICP

Date/Tlme/By: 10/9/96

EPA Method Test

- COLLECTION INFORMATION -3:40 PM HEINK

Result Units AnalysisDate Analyst

350.1

D3867-90A/9200300.0

300.0

D1293-84/9040160.1

SM2300B180.1

2510B/905031138^04131I3E7060200.7/6010200.7/60103113B/7131200.7/6010200.7/6010

3I13B/742I200.7/601031138^4031138^6131138^841200.7/6010

Nitrogen, Ammonia (as N)Nitrate + Nitrite NChloride. CISulfcte,SO4pH,Lab

Residue, Filterable (Dissolved Solids)Alkalinity, TotalTurbidity

Conductivity, LabAntimony, SbArsenic, AsBarium, BaBeryllium, BeCadmium, CdCobalt, CoCopper, CuLead,PbNickel, NiSelenium, SeSilverThallium, TlVanadium, V

WS#

1.10<0.05

<5<2

736390402

12691

<3.05.4

579<0.5<0.5<10<IO

<2.0<20

<3.0<I.O<1.0<20

MG/LMG/LMO/LMG/LS.U.

MG/LMG/LNTU

uMHOUQTLUG/Lvan.UQ/LUG/LUG/LUG/LUG/LUG/LUG/LU&Lvan.UCWL

10/15^610/17/961003/9610/23/9610/10/9610/16/9610/14/9610/10/9610/15/9610/16/9610/22/9610/15/9610/15/9610/18/9610/15/9610/15/9610/18/9610/15/96

10/21/9610/15/9610/19/9610/15/96

RJARJABKHBKHMDORJASKSDKJKRGSMMSMMSMMSMMROHSMMSMMJEL

SMM

ROHROHROHSMM

555598742742512588564527554607682557557625557557627557660565638557







Result U»te D^ Analyst WS#

ZH4CPNA-ICPMG-ICPCA-ICPK-ICPFE4CPMN4CPCOD-LOCR-GFAA

200.7/6010200.7/6060200.7/6010200.7/6010200.7/6010200.7/6010200.7/6010410.2/719631I3B/719I

Zuc.ZnSodium. MaMagnesium, MgCalcium, CaPotassium, KIron,Fe

COD. Low LevelChromium, Cr

<1011.629.151.6U

89188

<8<5.0


10/15/9610/15/9610/15/9610/15/9610/15/9610/15/9610/15/9610/11/9610/24/96


557557557557557557557545734

End of Reportr\ . * i J iReport Approved By: ^ / vrAA' /'*.., £6»~!*-»


1776 MARION WALDO RD. P.O. BOX 436 MARION, OH 43301-0436ounup K-1A^89^9fi1 1400-873-2835 FAX


Clients EAGON & ASSOCIATES INCAXEL Sample No.r 96-14278-MELDate Sampled: 10/09/96Date Received: 10/11/96Date Analyzed 8260: 10/15/96Date Analyzed 8240s 10/21/96Client IDs MW-7D

Methods SW-846; 8260, 8240(SIM)Sample Types MATERPercent SolidssAnalys t s SPH/JSMProject No.sTREHONT LANDFILL


AcetoneAcrylonitrile (SIM)BenzeneBromoohlorome t han eBroaodichloromethaneBromof ormCarbon DisulfideCarbon TetrachlorideChlorobenzeneChloroethaneChloroform

lt 2 -Dibromo- 3 -ohlorppropaue1,2-Dibromoethaneo-Dichlorobenzenep-Diohlorobenzenetrans-l,4-Dichloro-2-Butene1, 1-Dichloroe thane1,2-Dichloroethane1,1-Dichloroetheneci0-l,2-Dichloroethenetrans-l,2-Dichloroethene1,2 -Dichloropropanecis-l,3-Dichloropropenetrails -1,3 -DichloropropeneEthyl Benzene2-HexanoneBromomethaneChlorome thane

Methylene Chloride

5.05.01.01.01.01.05.01.01.01.00.51.01.01.01.01.01.00.50.50.5

< 0.5< 0.5< 1.0< 1.0< 1.0< 1.0< 10.0< 1.0< 1.0< 1.0< 1.0

2-Butanone < 10.0lodomethane < 10.04-Methyl-2-Pentanone < 20.0Styrene < 1.01,1,1,2-Tetrachloroethane < 1.01,1,2,2-Tetrachloroethane < 1.0Tetrachloroethene < 1.0Toluene < 1.01.1.1-Trichloroethane < 1.01.1.2-TriChloroethane < 1.0Trichloroethene < 0.5Trichlorofluoromethane < 1.01,2,3-Trichloropropane < 1.0Vinyl Acetate < 10.0Vinyl Chloride < 1.0Total Zylenes < 2.0


Dibromofluoromethane 102 (70-115)Bromofluorobenzene 91 (86-115)Toluene-d8 96 (88-110)Benzene-d6 104 (75-120)

6878 S. STATE ROUTE 100 • P.O. BOX 76 • MELMORE. OH 44845-9999PHONE 419-397-2659 • 1*800-058-8869 • FAX 419-397-2229



Bagon & Associates Inc100 Old Wilson Bridge RdSuite 320Worthington,OH 43085

Attn: Frank Majcfaszak

Our Lab*: MAR96-26784Date Logged-In: 10/11/96




Phone: (614)888-5760 Ext:FAX: (614)888-5763

Your Sample ID: MW-8SSample Source: RCRA

CUeat Project IkDate Submitted to Lab: 10/10/96

PO#: Trcmont Landfill

- COLLECTION INFORMATION -Date/Ilme/By: 10/9/96


1:05 PM HEINKAnalysis

Result Units Date Analyst WS#

NH3 350.1 Nitrogen, Ammonia (as N)NO3 D3867-90A/9200 Nitrate*Nitrite NCL-IC 300.0 Chloride, ClSO4-IC 300.0 Sulftte,SO4PH-LAB D1293-84/9040 pH.LabIDS 160.1 Residue, Filterable (Dissolved Solids)ALK SM2300B Alkalinity, TotalTURB 180.1 TurbidityCOND-L 2310B/9050 Conductivity, LabSB-QFAA 3113B/7041 Antimony. SbAS-OFAA 3113B/7060 Arsenic, AsBA-ICP 200.7/6010 Barium, BaBE-ICP 200.7/6010 Beryllium, BeCD-GFAA 3113B/7131 Cadmium, CdCO-1CP 200.7/6010 Cobalt, CoCU-ICP 200.7/6010 Copper, CuPB-GFAA 3113B/7421 Lead, PbNl-tCP 200.7/6010 Nickel, NiSE-GFAA 3113B/7740 Selenium, SeAG-GFAA 3113B/7761 SilverTL-GFAA 31I3B/7841 Thallium, TlV-1CP 200.7/6010 Vanadium, V

0.47<0.05

<520

7^739236424

687<3.0

5.058

<OJ<0.5<10<IO<2.0<20<3.0<1.0<1.0<20

MO/LM(VLMOO,MO/LS.U.

MG/LMG/LNTU

uMHOUG/LUG/LUG/LUCtfLixyLUG/LV&LUGA,UGrt.UGrt,UG/LUG/LUG/L

10/15/9610/17/961003/9610/23/9610/10/9610/16/9610/14/9610/10/9610/15/9610/16/9610/19/9610/15/9610/15/9610/18/9610/13/9610/15/9610/18/9610/15/9610/21/96

10/15/9610/22/9610/15/96

RJARJABKHBKHMDORJASKSDKJKRGSMMROMSMMSMMROHSMMSMMJEL

SMMROHROHRLHSMM

555598742742512588564527554607639557557625557557627557660565675557

Lab Number MAR96-26784:Pagf I

1776 MARION WALDO RD. P.O. BOX 436 MARION, OH 43301-0436Dunup ft14-.tAa.59S1 1-800-873-2835 FAX 614-3ft9-14in

Test Group

ZN-ICPKA4CPMO-1CPCA-ICPK-1CPFE-ICPMN-ICPCOD-LOCR-OFAA

EPA Method

200.7/6010200.7/6060200.7/6010200.7/6010200.7/6010200.7/6010200.7/6010410.2/71963II3B/7191

Test

ZHIC.ZBSodium. NaMnanmium j^/.Calcium. CaPotassium, KIron,FeManganese, MnCOD.LowLevdChnxniun], Or

ATELAqua Tech Envtowtmeittal Laboratories, Inc.

- CERTIFICATE ClF ANALYSIS (REPRINT)-

Lab Number MAR96-26784 -Continuedfrom Previous PageA __t——1_

Result Uiits

25 U&L4J7 MCVL26J MO/L67.4 MQfL

<1.0 MG/L825 U&L679 UQ^

11 MQA.<5.0

lQflSt9610/15/96IO/IS«610/15/9610/15/9610/15/9610/15/9610/11/9610/24/96


WS#

557557557557557557557545734

Report Approved By:

Lot Number MAR96-26784:Pagc 2

PPHONE MARION, OH 43301-04361-800473-2835 FAX 614-389-1410


Clients BASON & ASSOCIATES ZNCAXIL Sanple No.: 96-14279-MELDate Saapleds 10/09/96Date Received: 10/11/96Date Analyzed 8260: 10/15/96Date Analyzed 8240s 10/21/96Client IDs MW-8S

Methods SN-846; 8260, 8240(SIM)Sample Types MATERPercent SolidssAnalysts SPH/JSMProject No.iTREMOHT LANDFILL


AcetoneAcrylonitrile (SIM)BenzeneBroMOGhToroHicf1"*1**Broaodiohlorome thaneBronof omCarbon Disulf ideCarbon TetrachlorideChlorobenzeneChloroethaneChloroformp-jy>Trf>nw» 'h'j r>roinftt~bi|'ri<*1,2 -Dibromo - 3 - ohloropropane1,2 -Dibromoe thaneo -Dichlorobenzenep -Dichlorobenzenetrans -1,4 -Dichloro - 2 - Buteneig 1-Dichloroethane1,2-Dichloroethane —1, 1 -Dichloroethenecis-1, 2 -Dichloroethenetrans -1,2 -Dichloroethene1,2 -Dichloropropanecis -1,3 -Dichloropropenetrans -1, 3 -DichloropropeneEthyl Benzene2 -HexanoneBromome thaneCh.lorompt'rTvT*Dibromome thaneMethylene Chloride

<<<<<<<<<<<

<<<<<<<<<<<<<<<<

<<

5.05.01.01.01.01.05.01.01.01.00.51.01.01.01.01.01.00.50.50.50.50.51.01.01.01.010.01.01.01.01.0

2 -ButanoneTo/ ogiftl-ViiinA4 -Methyl - 2 - PentanoneStyrene1,1,1, 2 -Tetrachloroe thane1,1,2,2 -Tetrachloroe thaneTetrachl oroetheneToluene1,1, 1 - Tr i Chloroethane1 , 1 , 2 -Trichloroe thaneTrichloroetheneTrichloro f luorome thane1,2,3 -TrichloropropaneVinyl AcetateVinyl ChlorideTotal Xylenes

Surrogate Data: % Recc—~

Dibromofluoromethane 101Bromofluorobenzene 90Toluene-d8 104Benzene- d6 100

< 10.0< 10.0< 20.0< 1.0< 1.0< 1.0< 1.0< 1.0< 1.0< 1.0< 0.5< 1.0< 1.0< 10.0< 1.0< 2.0

>very

(70-115)(86-115)(88-110)(75-120)


Client #: 10107Eagon & Associates Inc






Matrix: WaterProject^:

Report Date: 27-Nav-96Original Report Date: 30-Oct-96

Phone: (614)888-5760FAX: (614)888-5763

Yow Sample ID: MW-8DSa«pk Scarce: RCRA

COeat Project*:DateSalMdttedtoLab: 10/10/96


- COLLECTION INFORMATION -Date/Time/By: 10/9/96 11:45 AM HEINK

TestGrou EPA Method TestResnlt Units Analyst WS#

NH3NO3CWCSO4-ICPH-LABTDSALKTURBOOND-LSB-GFAAAS-OFAABA-ICP

BB-ICPCDOFAACQ-ICPCU-ICPPB-GFAANI-ICPSE-OFAAAG-GFAA

TL-OFAAV-ICP

350.1

D3867-90A/9200300.0300.0

Dl 293-84/9040160.1

SM2300B180.1

2510B/905031I3B/7041

3I13B/7060200.7/6010200.7/60103U3B/7I3I200.7/6010200.7/6010

3I13B/7421200.7/6010

3II3B/77403II3B/776I

3II3BA784I200.7/6010

Nitrogen, Ammonia (as N)Nitrate* Nitrite NChloridc,aSu»&tc,SO4pH.Lab


Conductivity, LabAntimony, SbAiscjiJc,AsBanum, BaBeryllium, BeCadmiom,CdCobalt, CoCopper. CuLead,PbNickel, NiSdenium.SeSilverThallium. Tl

1776

Vanadium, V

MARION WALDO RD. P.O. BOX 436 MARION, OH 43301-0436PHONE 614-389-5991 1-800-873-2835 FAX 614489-1410

<0.05<0.05

5022

7.0452441910.0919

<3.0<3.0224

<0.5<0.5<10<10

<2.0<20

<3.0<1.0<I.O<20

MG/L

MG/LMG/LMG/LS.U.

MG/LMG/LNTU


10/15/9610/17/9610/23/9610/23/96

10/10/9610/16/9610/14/9610/10/9610/15/9610/1679610/19/96

10/15/96

10/15/9610/18/9610/15/9610/15/9610/18/9610/15/96

10/21/9610/15/9610/22/96

10/15/96


SMMROHROHRLHSMM

555598742742512588564527554607639557557625557557627557660565675557




TotGnmp EPA Method Test

Lab Number MAR96-2678S -Continuedfrom Previous PageAnalysis

Result Uatts D.te Analyst WS#

ZN-ICPNA4CPMO-ICPCA-ICPK4CPFE4CPMN-KPCOD-LOCR-OFAA

200.7/6010200.7/6060200.7/6010200.7/6010200.7/6010200.7/6010200.7/6010410.2/71963113B/7191

Zinc,ZnSodium, NaMagnesium, MgCaldum,CaPotassium, KIron,FeManganese, MnCOD. Low LevelChromium, Cr

4715.435J86J1.2

845479

<5.0

Report Approved By:

UG/LMG/LMG/LMG/LMO/LUG/LUGA,MG/LIKVL

A

10/15/9610/15/9610/15/9610/15/9610/15/9610/15/9610/15/9610/11/9610/24/96

A

*/^


•fflr*^"A*-/7

557557557557557557557545734

ra"-*

-1678S:Page 2

1776 MARION WALDO RO. P.O. BOX 436 MARION, OH 433014436PHONE 614-389-5991 1400-873-2835 FAX 614-389-1410

Jjl ^ fc^J^^Aqua Tech Environmental Laboratories, Inc.

Clients EAGON & ASSOCIATES INCA.TBL Sample No. i 96-14280-MBLDate Sampled: 10/09/96Date Received: 10/11/96Date Analyzed 8260: 10/15/96Date Analyzed 8240: 10/21/96Client ID: MSC-8D

Method: SW-846; 8260, 8240(SIM)Sanple Type: WATERPercent Solids:Analysts SPH/JSMProject NO.:TREMONT LANDFILL

Confound Concentration - ug/1 (ppb)

AcetoneAcrylonltrile (SIM)BenzeneBromochl orome thaneBroaodi chl orome thaneBronoformCarbon DisulfideCarbon TetrachlorideChlorobenzeneChloroethaneChloroform

I/ 2 -Dlbromo -3 -chloropropane1,2-Dibromoethaneo-Dlchlorobenzenep-Dichlorobenzenetrans-1, 4 -Dichloro-2 -Butane1.1-Dichloroe thane1.2-Dichloroethane1,1-Dichloroetheneeis-l,2-Dichloroethenetrans-1, 2 -Dichloroethene1,2 -Dichloropropanecis - 1 , 3 - Di chloropropenetrans-1, 3 -DichloropropeneEthyl Benzene2 -HexanoneBromome thaneChlorome thaneDibromomethaneMethylene Chloride

5.05.01.01.01.01.05.01.01.01.00.51.01.01.01.01.01.00.50.50.50.50.51.01.01.01.0

< 10.0< 1.0< 1.0< 1.0< 1.0

2-Butanone <lodomethane <4-Uethyl-2-Pentanone <Styrene <1,1,1, 2 -Tetrachloroe thane <1,1,2,2-Tetrachloroethane <Tetrachloroethene <Toluene <1.1.1-Trlchloroethane <1.1.2-Trichloroethane <Trichloroethene <Trichlorofluoromethane <1,2,3- Trichloropropane <Vinyl Acetate <Vinyl Chloride <Total Xylenes <

10.010.020.01.01.01.01.01.01.01.00.5

0,0

1.1,

10.01.02.0





- CERTIFICATE OF ANALYSIS -Client #: 10107 Report Date: 12-Dec-96


Attn:Phone: (614)888-5760 Ext:

FAX: (614)888-5763

Our Lib* MAR96-30655Date Logged-In: 11/27/96

Matrix: WaterProject*

Your Sample ID: MW-8DSample Source: Groundwater Monitoring

Client Project^ POfeDate Submitted to Lab: 11/26/96

• COLLECTION INFORMATION -Date/Time/By: 11/26/96 10:00 AM VINS

Tot Group EPA Method Test ResultAnalysts

Units Date Analyst WS#

ZN-ICPCL-ICNA-ICP

200.7/6010300.0

200.7/6060

Ztnc,ZnChloride, ClSodium, Na

<10 UG/L48 MG/L

17.8 MG/L

12/3/9612/6/9612/3/96

RGB 1340BKH 1385RGB 1340

End of Report

Report Approved By:Lana L. Jackson




- CERTIFICATE OF ANALYSIS -Client ft 10107 Report Date: 19-Dec~96

Eagon & Associates Inc100 Old Wilson Bridge RdSuite 320Worthingtoo, OH 43085 Phone:(614)888-5760 tot:

Attn: Chris Cobel PAX: (614)888-5763

Our Lab ft MAR96-32410 Your Sample ID: MW-8DDate Logged-In: 12/17/96 Sample Source: Groundwater Monitoring

Matrix: Water Clkat Project ft POftProject ft TREMONTLA Date Submitted to Lib: 12/16/96

• COLLECTION INFORMATION -Date/Time/By: 12/16/96 COBEL

AnalysisTest Group EPA Method Test Result Units Date Analyst WS#

COD-LO 410.2/7196 COD, Low Level <8 MG/L 12/17/96 BSR 1548End of Report

r\.Report Approved By:

Lab Number MAR96-324IO:Page I

1776 MARION WALDO RO. P.O. BOX 436 MARION, OH 43301-0436PHONE 614-389-5991 1400473-2835 FAX 614-389-1481


- CERTIFICATE OF ANALYSIS (REPRINT) -Client*: 10107






Report Date: 27-Hw-96


Phone: (614)888-5760 Ext:FAX: (614)888-5763

Your Sample ID: FB-1Sample Source: RCRA

Client Project*Date Submitted to Lab: 10/10/96

POfc Trtmont Landfill

- COLLECTION INFORMATION -Date/Time/By: 10/97%


5:45 PM HEINKAnalysis

Result Units Date Analyst WS#

NH3 350.1 Nitrogen. Ammonia (as N)NO3 . D3867-90A/9200 Nitrate + Nitrite NCL-IC 300.0 Chloride, aSO4-1C 300.0 Sulfitte.S04PH-LAB D1293-84/9040 pH, LabTDS 160.1 Residue, Filterable (Dissolved Solids)

ALK SM2300B Alkalinity, TotalTURB 180.1 TwttdityCOND-L 25IOB/9050 Conductivity, LabSB-OFAA 3113B/7041 Antimony, SbAS-OFAA 3113B/7060 Arsenic, AsBA-icP 200.7/6010 Barium, BaBE-1CP 200.7/6010 Beryllium, BeCD-OFAA 3113B/7131 Cadmium, CdCO-1CP 200.7/6010 Cobalt, CoCU-1CP 200.7/6010 Copper, CuPB-OFAA 3113B/7421 Lead, PbNI-ICP 200.7/6010 Nickel, NiSE-GFAA 3113B/7740 Selenium. SeAG-OFAA 3113B/7761 SilverTL-GFAA 3U3B/784I Thallium. TlV-ICP 200.7/6010 Vanadium, V

<0.05<0.05

<5<2

6^3<20<50.1

2<3.0<3.0<10<0.5<0.5< I O<10<2.0<20<3.0<l.O<1.0<20

MO/LMG/LMQ/LMG/LS.U.

MO/LMO/LNTU

uMHOUQ/LUG/LIXVLUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/L

10/15/9610/17/9610/23/9610/23/961G/10/9610/16/9610/14/9610/10/9610/15/9610/169610/22/9610/15/9610/15/9610/18/9610/15/9610/15/9610/189610/15/9610/21/96tO/15/%10/19/9610/15/96

RJARJABKHBKHMDORJASKSDKJKRGSMMSMMSMMSMMROHSMMSMMJBL

SMMROHROHROHSMM

555598742742512588564527554607682557557625557557627557

660565638557


1776 MARION WALDO RD. P.O. BOX 436 MARION, OH 43301-0436PHHMF 614-389*5991 1-800-873-2835 FAX 614-389-1410

ATELAqua Tech Environmental laboratories, Inc.

-CERTIFICATE&*ANALYSIS (REPRINT)-

Text Group EPA Method Test


Result Uaite D,te Analyst WS#

ZN-ICPNA4CPMCMCPCA-ICPK4CPFE4CPMN-ICPCOD-LOCR-OFAA

200.7/6010200.7/6060200.7/6010200.7/6010200.7/6010200.7/6010200.7/6010410.2/71963113B/7191

Zmc.ZnSodium, MiMagnesium. MgCalcium, CaPotassium. KIron,FcMflogancse. MnCOD. Low LevelChromium, Cr

<IO UO/L<0.40 MO/L<0.10 MO/L

0.11 MO/L<1.0 MO/L<40 UO/L<10 UO/L<8 MO/L

<5.0 UO/L

Report Approved By: „£&&*

10/15/9610/15/9610/15/9610/15/9610/15/9610/15/9610/15/9610/11/9610/24/96

£>

' / 444A' /!•


rtoftyPfnXZ2LttfrrV**tf

557557557557557557557545734

f

•a"-*


1776 MARION WALDO RO. P.O. BOX 436 MARION, OH 43301-0436PHONE 614489-5991 1-800-873-2835 FAX 614-389-1410


Clients EAOON & ASSOCIATES INCATKL Saaple Ho.s 96-14281-MELDate Sampled: 10/09/96Date Received: 10/11/96Date Analysed 8260s 10/15/96Date Analyzed 8240s 10/21/96Client ID: FB-1

Methods SW-846; 8260, 8240(SIM)Saaple Types HATERPercent SolidssAnalysts SPH/JSMProject No.sTREMONT LANDFILL


AcetoneAcrylonitrile (SIM)BenzeneBromoohlorome thaneBroonodl chl oromw thanBromoformCarbon Disulf ideCarbon TetrachlorideChlorobenzeneChloroe thaneChloroformDibromQchloTonM'itlvMie1,2 -Dibromo - 3 - chloropropane1, 2 -Dibromoethaneo - Dichlorobenzenep -Dichlorobenzenetrans -1,4 -Dichloro - 2 - Butene1, 1-Dichloroethane1,2 -Dichloroethane1, 1-bichloroethenecis- 1, 2 -Dichloroethenetrans- 1 , 2 -Dichloroethene1,2 -Dichloropropanecis -1,3 -Dichloropropenetrans -1,3 -DichloropropeneEthyl Benzene2 -HexanoneBTonw7ini=>*" >a'n*»Chlorome thaneDiforomoine't"*1*1'"'*Methylene Chloride

<<<<<<<<<<<<<<<<<<<~<<<<<<<<<<<<

5.05.01.01.01.01.05.01.01.01.00.51.01.01.01.01.01.00.50.50.50.50.51.01.01.01.0

10.01.01.01.01.0

2-Butanonelodomethane4 -Methyl - 2 - PentanoneStyrene1,1,1,2 -Tetrachloroe thane1,1,2,2 -Tetrachloroe thaneTetrachloroetheneToluene1, 1, 1-Trichloroe thane1,1, 2 -Trichloroe thaneTrichloroetheneTrichlorof luorome thane1,2,3 -TrichloropropaneVinyl AcetateVinyl ChlorideTotal Xylenes

Surrogate Data: % Recc• *DlbmOTotlTioimiiethane 5.06Bromof luorobenzene 99Toluene-d8 104Benzene -d6 101

< 10.0< 10.0< 20.0< 1.0< 1.0< 1.0< 1.0

1.2< 1.0< 1.0< 0.5< 1.0< 1.0< 10.0< 1.0< 2.0

>very

(70-115)(86-115)(88-110)(75-120)

6878 S. STATE ROUTE 100 • P.O. BOX 76•-Mi nc xio_iQ7.0RRQ

MELMORE. OH 44845-9999FAY

Client ft: 10107

ATELvtrotunentalLal

CERTIFICATE OF ANALYSIS (REPRIN^ .Inc.

Eagon A Associates Inc

100 Old Wilson Bridge RdSuite 320Wortfaingtoo, OH 43085

Attn: Frank Majcfaszak

Oar Lab #: MAR96-26792Date Logged-In: 10/11/96


Report Date: 27-ftov-96


Phone: (614)888-5760 Ext:FAX: (614)888-5763

Year Sunpfe ID: WS96-62Sample Scarce: RCRA

Client Project*:DateSnbmittedtoLnb: 10/10/96 PO#: Tremont Landfill

- COLLECTION INFORMATION -Date/Tine/By: 10/9/96

TestGrou EPA Method Test6:40 PM HEINK

Result Units A^fa Analyst ^

NH3N03CL-ICSO4-ICPH-LABTDSALKTURBCOND-LSBXJFAA

. AS-OFAABA-ICPBB4CPCD-OFAACO-ICPCU-ICPPB-GFAANI-ICPSE-OFAAAG-GFAATL-GFAAV-ICP

350.1

D3867-90A/9200300.0300.0

D1293-84/9040160.1

SM2300B180.1

25IOB/905031138)704131I3B/7060200.7/6010200.7/6010

3I13B/7I31200.7/6010200.7/6010

3I13B/7421200.7/6010

3I13B/77403113B/77613II3B/7841200.7/6010

Nitrogen, Ammonia (as N)Nitrate + Nitrite NChloride, ClSulfate,SO4pH.Lab


Conductivity. LabAntimony, SbArsenic, AsBarium, BaBeryllium, BeCadmium, CdCobalt. CoCopper, CuLead.PbNickel, NiSdenium.SeSilverThallium, TlVanadium, V

1776

<0.05<0.05

628

7.22392371680716

<3.05.4143

<0.5<0.5< I O

2514

<20<3.0<I.O<I.O<20

MOT.

MGA.

MG/L

MG/LS.U.

MG/LMGA,NTU

uMHOUGA,UGA,UGA.UGA.UGA.UGA.UGA,UGA,UGA.

UGA,UGA,UGA,UGA.

10/18/9610/17/9610/23/9610/23/96

10/10/9610/16/9610/21/9610/10/9610/15/9610/16/9610/22/9610/15/9610/15/9610/18/9610/15/9610/15/9610/22/9610/15/9610/24/9610/15/9610/19/9610/15/96

RJARJABKHBKHMDORJAKVSDKJKRGSMMSMMSMMSMMROHSMMSMMSMMSMMROHROHROHSMM

615598742742512588637527554607682557557625557557680557724565638557





Lab Number MAR96-26792 -Continuedfrom Previous PageAutysb

Renlt Units rj e Analyst WS#

ZN-ICPNA-1CPMG-ICPCA-1CPK-ICPFE-ICPMN-ICPCOD-LOCR-GFAA

200.7/6010200.7/6060200.7/6010200.7/6010200.7/6010200.7/6010200.7/60104102/71963113B/7191

Zinc,ZnSodium, NaMagnesium, MgCalcium, CaPotassium, KIroo,FcMm— -,--,^-_ »*_

nfflFllllvfffri Prill

COD, Low LevelChromium, Cr

5742

39.092.122

11900239

178.4


10/15/9610/15/9610/15/9610/15/9610/15/9610/15/9610/15/9610/11/9610/24/96


557557557557557557557545734

A /ft^f*/"

Report Approved By: JM> —————— i&*""

ff -*T~*


1776 MARION WALDO RD. P.O. BOX 436 MARION, OH 433014)436^oa eao-i


Clients EAGON ft ASSOCIATES INCATKL Sanple No.s 96-14283-MELDate Sampled: 10/09/96Date Received: 10/11/96Date Analyzed 8260s 10/15/96Date Analyzed 8240s 10/22/96Client IDs WS96-62

Methods SW-846; 8260, 8240(SIM)Sanple Types HATERPercent SolidssAnalysts SPH/JSMProject No.sTRBMONT LANDFILL


AcetoneAcrylonitrile (SIM)BenzeneBronoohlorome thanePronodl i. <?h I o roflM? t ha n £•BronoformCarbon DisulfldeCarbon TetracblorideChlorobenzeneChloroethaneChloroformDibronochlorooiethane1, 2 -Dibromo- 3 -obloropropane1, 2 •Dibromoethaneo -Dichlorobenzenep-Dichlorobenzenetrana -1,4 -Dichloro - 2 - Butene1, 1-Dichloroethane1,2-Dichloroethane1, 1-Dichloroetheneois-1, 2 -Dichloroethenetrans-1, 2 -Dichloroethene1,2 -Dichloropropaneois-1, 3 -Dichloropropenetrans - 1 , 3 - Di chloropropeneBthyl Benzene2-HexanoneBronome thane(7hlOTCX>W*t" H>TT**Dlbronorae thaneMethylene Chloride

<<<<<<<<<<<<

<<<<<<<<<<<<<<<

<<

5.05.01.01.01.01.05.01.01.01.00.51.01.01.01.01.01.00.50.50.50.50.51.01.01.01.0

10.01.01.01.01.0

2 -Butanonelodome thane4 -Methyl - 2 - Pen tanoneStyrene1,1,1,2- TO t?T*a<?h 1 Q?**>g f-h* rt at1,1,2,2 -Tetrachloroe thaneTetrachloroe theneToluene1,1, 1-Tri chloroethane1,1,2 -Trichloroe thaneTrichloroe theneTri ohlorof? luQiXMBel" * « <»1,2,3- TriohloropropaneVinyl AcetateVinyl ChlorideTotal Xylenes

Surrogate Da tat % Recc-~Dibromofluoromethane 104Bronofluorobenzene 105Toluene -d8 104Benzene -d6 100

< 10.0< 10.0< 20.0< 1.0< 1.0< 1.0< 1.0< 1.0< 1.0< 1.0< 0.5< 1.0< 1.0< 10.0< 1.0< 2.0

>very

(70-115)(86-115)(88-110)(75-120)

6876 & STATE ROUTE 100 • P.O. BOX 76 • MELMORE, OH 44845-9999PHONE 419-397-2659 • 1-800^58-8869 • FAX 419-397-2229


- CERTIFICATE OF ANALYSIS (REPRINT) -Client*: 10107






Report Date: 27-Nov~96Original Report Date: 30-Oct-96

Phone: (614)888-5760 Ext:FAX: (614)888-5763

Yomr Sanple ID: WS96-62 DUPSample Sowce: RCRA

Client Project #: PO#: Tremont LandfillDateSnbmittedtoLab: 10/10/96

- COLLECTION INFORMATION -Date/Tlme/By: 109/96 6:45 PM HEINK

TestGrou EPA Method Test Result UnitsAnalysis

Analyst WS#

NH3NO3CL-1CSO4-ICPH-LABTDSALKTURBCOND-LSB-GFAAAS-GFAABA4CPBE-ICPCD-GFAACX>-ICPCU-ICPPB-GFAANMCPSE-GFAAAG-GFAATL-GFAAV-ICP

350.1D3867-90A/9200

300.0300.0

D1293-84/9040160.1

SM2300B180.1

2510B/90503113B/70413113B/7060200.7/6010200.7/601031I3B/7131200.7/6010200.7/60103I13B/7421200.7/6010

3113B/77403I13B/776131I3B/7841200.7/6010

Nitrogen, Amroooia (as N)Nitrate •*• Nitrite NChloride, ClSulfcte,SO4pH,LabResidue, Fdterobte (Dissolved Solids)Alkalinity, TotalTumidityConductivity, LabAntimony, Sb

_Araeaic,AsBarium, BaBeryllium, BeCadmium, CdCobalt, CoCopper, CuLead.PbNickel, NiSeknhHn.SeSilverThallium, TlVanadium, V

<0.05<0.05

626

7^1393367600716

<3.05.7160

<0.5<OJ<10

239.9

<20<3.0<1.0<1.0<20

MO/LMQ/LMG/LMGA,S.U.

MQ/L •MG/LNTU

uMHOUG/LIKVL _UGILUGrt.UG/LUGA,UG/LUGfl-UGA,UG/LIKVLUG/LUG/L

10/18/9610/17/9610/23/9610/23/9610/10/9610/16/9610/21/9610/10/9610/15/9610/16/9610/22/9610/1579610/15/9610/18/9610/1579610/15/9610/22/9610/15/9610/24/96

10/15/9610/19/96JO/15/%

RJARJABKHBKHMDORJAKVSDKJKRGSMMSMMSMMSMMROHSMMSMMSMMSMMROHROHROHSMM

615598742742512588637527554607682557557625557557679557

724565638557





Tot Group

ZN-KPNA-ICPMCMCPCA-ICPK-ICPFE-IGPMN-ICPCOD-LOCIMJFAA

EPA Method Test

200.7/6010 Ztac,Zn200.7/6060 Sodium, Ma200.7/6010 Magnesium. Mg200.7/6010 Calcium, Ca200.7/6010 Potassium. K200.7/6010 Iron.Fe200.7/6010 Manganese. Mn410.2/7196 COD. Low Level

3I13B/7191 Chromium, Cr

K* Nunber MAR96-26793 -Continedfro* Prevlous Pagg

».__.. .. . Analyib•^ «* *y78

Report Approved By:

MAR96-26793:Page 2


Clients EAQON 6 ASSOCIATES INCATBL Saaple Ho.s 96-14284-MELDate Sampled! 10/09/96Date Received: 10/11/96Date Analyzed 8260s 10/15/96Date Analyzed 8240s 10/22/96Client IDs WS96-62 DUP

Methods SW-846; 8260, 8240(SIM)Sample Types WATERPercent SolidssAnalysts SPH/JSMProject No.sTREMQNT LANDFILL


AcetoneAcrylonitrile (SIM)BenzeneBroaochloromethaneBroaodichloromethaneBroaoformCarbon Disulf ideCarbon TetrachlorideChlozobenzeneChloroe thaneChloroformPU>roBK>qhlorCTB£'t'*>>*'"c>1 , 2 -Dlbromo - 3 - chloropropane1,2 -Dibromoe thaneo -Dichlorobenzenep-Diohlorbbenzenetrans-l,4-Diohloro-2-ButeneJL, 1-Dichloroe thane4.,2-Dichloroethane1, 1-Dichloroethenecis -1,2 -Dichloroethenetrans-1, 2 -Dichloroethene1,2 -Dichloropropanecis-1, 3 -Dichloropropenetrans -1,3 -DichloropropeneEthyl Benzene2 -HwJMiTioni?i-omfM aam - iypaiChlOTomo ttmp ADibronomethaneHethylene Chloride

<<<<<<<<<<<<

<<<<<<<<<<<<<^

<<<<

5.05.01.01.01.01.05.01.01.01.00.51.01.01.01.01.01.00.50.50.50.50.51.01.01.01.010.01.01.01.01.0

2-ButanoneTo<iomflt" |J*T|e*4 -Methyl - 2 - PentanoneStyrene1,1,1,2 -Tetrachloroe thane1,1,2,2 - Tetrachloroe thaneTetrachloroetheneToluene1,1, 1-Trichloroe thane1,1,2- Tr ichloroe thaneTrichloroetheneTr 4 ohloroU luorouift th ATI ft1,2,3 -TrichloropropaneVinyl AcetateVinyl ChlorideTotal Xylenes

Surrogate Data: % Recc— -Dibromofluoromethane 98Bromofluorobenzene 95Toluene -d8 99Benzene -d6 97

< 10.0< 10.0< 20.0< 1.0< 1.0< 1.0< 1.0< 1.0< 1.0< 1.0< 0.5< 1.0< 1.0< 10.0< 1.0< 2.0

>very

(70-1(86-1(88-1(75-1

RRTRR STATE ROUTE 100 - P.O. BOX 76 • MELMORE. OH 44845-9999


Clients EAGON & ASSOCIATES INCATKL Sample HO.J 96-14285-MBLDate Sampled: 10/09/96Date Received: 10/11/96Date Analysed 8260s 10/15/96Date Analyzed 8240s 10/22/96Client IDs TRIP BLANK

Methods SH-846; 8260, 8240(SIM)Sanple Types MATERPercent SolidssAnalysts SPH/JSMProject No.sTRBMONT LANDFILL


Acetone <Acxylonitrile (SIM) <Benzene <Bromochlorome thane <Bromodichlorome thane <Bronof orm <Carbon Disulfide <Carbon Tetrachloride <Chlorobenzene <Chloroethane <Chloroform <Dibromochlorome than e <1,2 -Dibromo- 3 -cllloropropane <1,2-Dibromoethane <o-Diohlorobenzene <p-Dichlorobenzene <trans-l,4-Dichloro-2-Butene <1,1-Dichloroe thane1, 2 -Dionloroethane1.1-Dichloroetheneois-l,2-Dichloroethenetran0-l,2-Dichloroethene1.2-Dichloropropaneoi«-l,3-Dichloropropenetrans -1,3 -DiohloropropeneKtnyl Benzene2-Hexanone

ChloromethaneDlbromome thaneMethylene Chloride

<<<<<<<<<<<<<<

5.05.01.01.01.01.05.01.01.01. 00.51.01.01.01.01.01.00.50.50.50.50.51.01.01.01.0

10.01.01.01.01.0

,0.0.0,0

2-Butanone < 10.0lodomethane < 10.04-Methyl-2-Pentanone < 20.0Styrene < 1.1,1,1,2-Tetrachloroethane < 1.1,1,2,2-Tetrachloroethane < 1.Tetrachloroethene < 1.Toluene < 1.01.1.1-Trichloroethane < 1.01.1.2-Trlohloroethane < 1.0Trichloroethene < 0.5Trichlorofluoromethane < 1.01,2,3-Triohloropropane < 1.0Vinyl Acetate < 10.0Vinyl Chloride < 1.0Total Xylenes < 2.0

Surrogate Datat % Recovery




EAGON ft ASSOCIATES INC100 OLD WILSON BRIDGE RD

,OH 43085

CLIENTS

ATTNs FRANK MAJCHSZAK

| PROJECT NO.s TREMONT L.F. | DATE OF INT.

| PURCHASE ORDERS TREMONT LANDFILL |

1

| ATEL NO.

J96-14271-MEL

| 96 -14272 -MEL

| 96-14273 -MEL

| 96 -14274 -MEL

| 96 -14275 -MEL

{96-1427 6 -MEL

(96-14277 -MEL

(96-1427 8 -MEL

| 96 -14279 -MEL

(96 -14280 -MEL

(96-14281-MEL

(96 -142 83 -MEL

(96 -142 84 -MEL

(96 -142 85 -MEL

SAMPLE

| CLIENT NO.

| MW-1R

| MW-3R

1 KN-4

| MN-5D

| MW-5DD

| MN-6D

| MN-7S

| MW-7D

| MW-8S

| MW-8D ~

| FB-1

| WS96-62

| WS96-62 DUP

| TRIP BLANK

INVENTORY

DIAL RECEIPT AT* 10/11/96

| METHOD (S)

| SW-846;

1 SW-846;

| SW-846;

| SW-846;

| SW-846>

| SW-846;

| SW-846;

| SW-846 i

| SW-846;

| SW-846;

| SW-846 1

| SW-846;

| SW-846;

| SW-846;

8260,

8260,

8260,

8260,

8260,

8260,

8260,

8260,

8260,

8260,

8260,

8260,

8260,

8260,

8240 (SIM)

8240 (SIM)

8240 (SIM)

8240 (SIM)

8240 (SIM)

8240 (SIM)

8240 (SIM)

8240 (SIM)

8240 (SIM)

8240 (SIM)

8240 (SIM)

8240 (SIM)

8240 (SIM)

8240 (SIM)

AUTHORIZED SIGNATURE: f.ORGANIC SECTION CH

**«IEF

6878 S. STATE ROUTE 100 • P.O. BOX 76 • MELMORE. OH 44845-9999—..-..._ i^^ nn-r necn . 4 O/WOCO-OOCn . CAV *<n nn-r

CHAIN-OF-CUSTODY ".otdj


Client Name:

Project Name: •

Project No.

Sampler

TF /- J.in

/700 «/ --*cL1736 •"71 / •"06 .

AW -

Mvo

SEND RESULTS TO:Person:Company:Street:City:Phone:ATEL Quote #:

loo

tern. Fax:

: OH So:

Company PO #:

Relinquished byj

Relinquished by:

Date/Tune

Date/Time

Received by:

Received by:

Date/Time

Date/Tune

Relinquished by: Date/Time

CommenU: Method of Shipment

Cooler Temperature:

Canton: 5300 Fulton Drive HW Marion: 1776 Marion-Waldo Rd Sanford: 936 N Hocner BoulevudCanton. Ohio 44718 Marion. Ohio 43502 Sanfori. North Carolina 27331800-635-3222 fax 216-494-2961 800-873-2835 fax 614-389-1481 800-522-2832 fax 919-774-7068

Tncson: 2700 E Bilby Rd. Bidg. A Melmorc: 6878 S State RL 100 Mission 27531 ChanUga DriveTucson. Arizona 85706 Melmore, Ohio 44845 VIejo: Mission Viqo, California 92692800-879-2835 fax 520-573-6550 800-858-8869 fax 419-397-2229 800-263-2261 fax 714-348-1922

CHAIN-OF-CUSTODY


Client Name:

Project Ni

Project No.

Fb- Uft-b•*.r j -la Aft**"-*I /" ' AAf.

S - l r

Wlo

N3o 3

SEND RESULTS TO:Person:Company:Street:

City:Phone:ATEL Quote #:

*p Suik. 32.0

Fax:State:(6

Zip:.

Company PO #:_

Relinquished by: ~*- S

Relinquished by.

Relinquished by:

Date/Time

Date/Time

Date/Time

Received by:

Received by: .~tr._ -

Received at Laboratory by:

JZ S^bs h-~Comments:

J

Date/Time

Date/Time ..

Date/Time.

Method of Shipment .krtftjb d^«Vtr H i-rtb

Cooler Temperature: ., )]0/ 1

Canton: 5300 Fulton Drive NW Marion: 1776 Marion-Waldo Rd Sanfonl: 936 N Homer BoulevardCanton. Ohio 44718 Marion. Ohio 43502 Sanfotd, North Carolina 27331800-635-3222 fax 216-494-2961 800-873-2835 fax 614-389-1481 800-522-2832 fax 919-774-7068

Tucson: 2700 E Bilby Rd. Bldg. A Meunore: 6878 S Stale RL 100 Mission 27531 Chantaga DriveTucson, Arizona 85706 Melmore. Ohio 44845 Vlejo: Mission Viejo. California 92692800-879-2835 fax 520-573-6550 800-858-8869 fax 419-397-2229 800-263-2261 fax 714-348-1922

fCHAIN-OF-CUSTODY


Client Name:

Project Name:

TfojectNo.

Sampler

t'/w/n £rer~"* *•/*-*« /-7«f

fiat.

^/fr" V

"• ^ • V — NICS .

C- *^^

t '

SEND RESULTS TO:Person:Company:Street:City:Phone:ATEL-Quote #:

'r* /

^

G/Y-g- **T"State: Zip:.

Fax:

Company PO#:

Dale/Time Received by:

Relinquished by: Dale/Time Received Date/Time

Relinquished by: Date/Time Received at

MetKbd of Shipment / '/- ftl x*«/f •"/••»

Cooler Temperature: /i Of~\

Canton: 5300 FUtton Drive NW Marion: 1776 Marion-Waldo Rd Suiford: 936 N Homer BoulevardCanton. Ohio 44718 Marion. Ohio 43.W2 Sanford. North Carolina 27.130800-63J-3222 fax 216-494-2961 800-873-2835 fax 614-389-1481 800-522-2832 fax919-774-7068

Tucson: 2700 E Bilby Rd. BIdg. A Melmore: 6878 S Stale RL 100 Mission 27531 OunUga DriveTucson. Arizona 83706 Melmore, Ohio 44845 Vicjo: Mission Vicjo, California 92692800-879-2835 fax 520-573-6550 800-858-8869 fax 419-397-2229 800-263-2261 fax 714-348-1922

CHAIN-OF-CUSTODY


SEND RESULTS TO:Person:Company:Street:City:Phone:ATEL Quote #:

dhi* State: fitf Zap:61/ Fax: " J 7<> 5

XICompany HO #: 'fovrts*^ J+n/A//

Relinquished b<

Date/Time

Date/Tune pfevedby: Date/Time

Relinquished by: Date/Time at Laboratory

Comments: /T-n

Method of Shipment

Cooler Temperature:

Date/Tune

°CCuiton: 5300 Fulton Drive NW Marion: 1776 Marion-WildoRd Sanford: 936 N Homer Boulevard

Canton. Ohio 44718 Marion. Ohio 43302 Sanford, North Carolina 27330800-635-3222 fax 216^94-2961 800-873-2835 fax614-389-I481 800-522-2832 fax 919-774-7068

Tucson: 2700 E Bilby Rd. Bldg. A Melmorc: 6878 S State RL 100 Mission 27531 Chantaga DriveTucson, Arizona 85706 Mclmore, Ohio 44845 Vltjo: Mission Viejo. California 92692800-879-2835 fax 520-573-6550 800-858-8869 fax 419-397-2229 800-263-2261 fax 714-348-1922


QUALITY CONTROL REPORTPrinted: 10/30/96

QCWS* Lab# Test ID Code Result

625 MAR96-26770S CD-GFAA627 MAR96-26770S PB-GFAA565 MAR96-26776D AG-GFAA564 MAR96-26776D ALK639 MAR96-26776D AS-GFAA557 MAR96-26776D BA-ICP557 MAR96-26776D B6-ICP557 MAR96-26776D CA-ICP625 MAR96-26776D CD-GFAA742 MAR96-26776D CL-IC557 MAR96-26776D CCMCP734 MAR96-26776D CR-GFAA557 MAR96-26776D CR-ICP557 MAR96-26776D CU-ICP557 MAR96-26776D FE-TCP557 MAR96-26776D K-ICP557 MAR96-26776D MG-ICP557 MAR96-26776D MN-ICP557 MAR96-26776D NA-ICP557 MAR96-26776D NI-ICP627 MAR96-26776D PB-GFAA607 MAR96-267760 SB-GFAA660 MAR96-26776D SE-GFAA742 MAR96-26776D SO4-IC588 MAR96-26776D TDS638 MAR96-267760 TL-GFAA527 MAR96-26776D TUR8557 MAR96-26776D V-ICP557 MAR96-26776D ZN-4CP565 MAR96-26776S AG-GFAA639 MAR96-26776S AS-GFAA625 MAR96-26776S CD-GFAA742 MAR96-26776S CL-IC734 MAR96-26776S CR-GFAA627 MAR96-26776S PB-GFAA

S 1.14S 12.7D .110 409.8D -1.07D 144.77D .77D 93.00759D 0D 8.668D -.7D .98D 4.63D .66D 28.56D .81967D 37.43168D 710.48D 8.570580 8.12D .70 .91D -.72D 67.845D 560D .08D .616D -1.83D .96S 1.51S 11.96S 1.18S 24.355S 12.5S 11.43

QC Code Legend

True ~ QC Calculations -Units Added QC1

UC/U 0.95 108 %R:UG/L 9.5 107 %R:0«A- 533 %D *MG/L 0 %DOCA- 56 %D *MCA. 8 %DMG/U 0 %DMCA- 6 %DUGA_ 200 %D •MG/L 1 %D**S/L 550 %D *UG/L 63 %D *VAA. 144 %D •

HASA. 200 %D *MCA. - 55 %D •NKA. 33 %D *»»S/L 8 %DMCA. 8 %D•ASA. 8 %DWCA. 12 %DUG/L 4 %DUGA. 41 %D •IXA. 73 %D *MGA. 0 %DMG/L 0 %0USA- 100 %D •NTU 1 %DMC/l 1 %DkMVt. o %oUfiA- 1-81 86 %R:UG/L 12.2 103 %R:IX t- 0-95 122 %R:MGA. 20 79 %R:UGA. 12.2 98 %R:UGA. 9.5 113 %R:

IB Blanks K Calibration Checks S SpikesC Control Samples M Matrix Spike DuplicatesD Duplicates R Surrogates

- QC Calculations - Lower UpperQC2 Umlt Limit

75 12575 125

2080 20

20202020

80 202020202020202020202020202020202020

80 202020

75 12575 12575 12575 12575 12675 12:




QCWS* Lab# Test ID Code Result units

607 MAR96-26776S SB-GFAA660 MAR96-26776S SE-GFAA638 MAR96-26776S TL-GFAA557 MAR96-26777 BA-ICP627 MAR96-26777 PB-GFAA565 MAR96-26777S AG-GFAA639 MAR96-26777S AS-GFAA625 MAR96-26777S CD-GFAA734 MAR96-26777S CR-GFAA627 MAR96-26777S PB-GFAA607 MAR96-26777S SB-GFAA579 MAR96-26777S SE-GFAA638 MAR96-26777S TL-GFAA565 MAR96-26778S AG-GFAA557 MAR96-26778S AS-GFAA639 MAR96-26778S AS-GFAA557 MAR96-26778S BA-ICP639 MAR96-26778S BA-ICP557 MAR96-26778S BE-ICP639 MAR96-26778S BE-ICP625 MAR96-26778S CD-GFAA557 MAR96-26778S CCWCP639 MAR96-26778S CO-ICP734 MAR96-26778S CR-GFAA557 MAR96-26778S CR-ICP639 MAR96-26778S CR-ICP557 MAR96-26778S CLWCP639 MAR96-26778S CIMCP557 MAR96-26778S FE-ICP639 MAR96-26778S FE-ICP557 MAR96-26778S K-ICP639 MAR96-26778S K-ICP557 MAR96-26778S MG-ICP639 MAR96-26778S MG-ICP557 MAR96-26778S MN-ICP

S 24.62 UG/LS 24.05 UG/LS 9.04 US/U

273.26 KKrt.44 UGA.

S 1.43 UC/LS 15.49 U/LS 1.04 UVtS 11.91 UGA.S 10.51 UGA.S 24.38 UGA.S 22.39 UC/US 8.62 U/uS 1.42 U/LS 16.24 us/«_S 16.24 U&/LS 2637.14 I*S/LS 2637.14 H&/LS 22.88 MC/LS 22.88 MS/US 1.08 USA.S 863.13 M6A_S 863.13 M6A-S 11.05 UGA.S 860.31 Mfirt.S 860.31 *B/LS 895.12 M«/uS 895.12 »WLS 3238.05 MO/uS 3238.05 IAC/US 10.40612 AM/LS 10.40612 «AS/LS 32.02589 Mtf/cS 32.02589 AAS/LS 926.45 I </L

QC Code Legend

True ~ QC Calculations —Added QC1

24 100 %R:24 107 %R;9.5 93 %R:

1.81 64 %R: *12 111 %R:0.95 113 %R:12.2 87 %R:9.5 111 %R;24 101 %R:24 91 %R:9.5 88 %R:

1.81 91 %R:12.2 107 %R:12.2 107 %R:

2500 96 %R:2500 96 %R:

20 111 %R:20 111 %R:

0.95 119 %R:1000 86 %R:1000 86 %R:12^ 85 %R;1000 86 %R:1000 86 %R;1000 --90 %R:1000 90 %R:2500 82 %R:2500 82 %R:

10 93 %R:10 93 %R:5 57 %R: •5 57 %R: •

1000 86 %R:

B Blanks K Calibration Checks S SpikesC Control Samples M Matrix Spike DuplicatesD Duplicates R Surrogates

- QC Calculations - LowerQC2 Limit

757575

757575757575757575757575757575757575757575757575757575757575

UpperLimit

125125125

125125125125125125125125125125125125125125125125125125125125125125125125125125125125125125




QCWS# Lab# Test ID Code Result Units

639 MAR96-26778S MN-ICP657 MAR96-26778S NA-ICP639 MAR96-26778S NA-ICP557 MAR96-26778S NI-ICP639 MAR96-26778S NHCP627 MAR96-26778S PB-GFAA607 MAR96-26778S SB-GFAA579 MAR96-26778S SE-GFAA638 MAR96-26778S TL-GFAA657 MAR96-26778S V-ICP639 MAR96-26778S V-ICP557 MAR96-26778S ZN-ICP639 MAR96-26778S ZN-ICP742 MAR96-26779D CL-IC598 MAR96-26779D NO3565 MAR96-26779S AG-GFAA639 MAR96-26779S AS-GFAA625 MAR96-26779S CD-GFAA742 MAR96-26779S CL-IC734 MAR96-26779S CR-GFAA598 MAR96-26779S NO3627 MAR96-26779S PB-GFAA607 MAR96-26779S SB-GFAA579 MAR96-26779S SE-GFAA638 MAR96-26779S TL-GFAA565 MAR96-26780S AG-GFAA639 MAR96-26780S AS-GFAA625 MAR96-26780S CD-GFAA734 MAR96-26780S CR-GFAA627 MAR96-26780S PB-GFAA607 MAR96-26780S SB-GFAA579 MAR96-26780S SE-GFAA638 MAR96-26780S TL-GFAA565 MAR96-26781S AG-GFAA639 MAR96-26781S AS-GFAA

S 926.45 M6/L.

True ~ QC Calculations -Added QC1

1000 86 %R:S 14.95458 Mfl/t- 5 88 %R:S 14.95458 MM-S 855.33 VKS/LS 855.33 NC/US 10.8 UG/LS 24.31 UG/LS 24.52 ICA.S 8.81 UJ/L

5 88 %R:1000 86 %R:1000 86 %R:

9.5 110 Wt24 98 %R;24 110 %R:9.5 92 %R:

S 787.17 Mfi/L 1000 79 %R:S 787.17 Mfi/uS 822.17 AW/i-S 822.17 VGA.D 9.644 MG/LD .011 MG/LS 1.98 06/LS 19.25 UftA.S 1.1 USA.S 26.326 MG/LS 11.25 UG/LS 1.167 MG/LS 10.56 UG/LS 22.28 UG/LS 29.32 VGfl,S 9.28 UfiA-S 1.99 Wtt.S 12.41 VC/Ls 1.1 uy<_S 11.15 UGA.S 10.4 UGA.S 24.64 UGA.S 26.75 IXSfiS 9.08 t&LS 1.71 tX/uS 14.37 UC/U

QC Code LegendB Blanks KC Control Samples MD Duplicates R

1000 79 %R:1000 82 %R:1000 82 %R:

1 %D119 %D *

1.81 93 %R:12.2 90 %R:0.95 116 %R;

20 84 %R:12.2 84 %R;

1 112 %R:9.5 105 %R:24 91 %R:24 124 %R:

9.5 95 %R:1.81 100 %R;12.2 106 %R:0.95 116 %R;12.2 85 %R:9.5 105 %R:24 100 %R:24 121 %R:9.5 91 %R:

1.81 93 %R:12.2 112 %R:

Calibration Checks S SpikesMatrix Spike DuplicatesSurrogates


75757575757575757575757575

807575757575757575757575757575757575757575

UpperLimit

1251251251251251251251251251251251251252020125125125125125125125125125125125125125125125125125125125125




QCWS# Lab* Test ID Code Result

625 MAR96-26781S CD-GFAA734 MAR96-26781S CR-GFAA627 MAR96-26781S PB-GFAA607 MAR96-26781S SB-GFAA579 MAR96-26781S SE-GFAA638 MAR96-26781S TL-GFAA565 MAR96-26782S AG-GFAA639 MAR96-26782S AS-GFAA625 MAR96-26782S CD-GFAA734 MAR96-26782S CR-GFAA627 MAR96-26782S PB-GFAA607 MAR96-26782S SB-GFAA579 MAR96-26782S SE-GFAA638 MAR96-26782S TL-GFAA545 MAR96-26783D COD-LO554 MAR96-26783D COND-L555 MAR96-26783D NH3565 MAR96-26783S AG-GFAA682 MAR96-26783S AS-GFAA625 MAR96-26783S CD-GFAA545 MAR96-26783S COD-LO734 MAR96-26783S CR-GFAA555 MAR96-26783S NH3627 MAR96-26783S PB-GFAA607 MAR96-26783S SB-GFAA660 MAR96-26783S SE-GFAA638 MAR96-26783S TL-GFAA625 MAR96-26784 CD-GFAA742 MAR96-26784D SO4-IC565 MAR96-26784S AG-GFAA639 MAR96-26784S AS-GFAA625 MAR96-26784S CD-GFAA734 MAR96-26784S CR-GFAA627 MAR96-26784S PB-GFAA607 MAR96-26784S SB-GFAA

S 1.1S 11.98S 10.67S 24.91S 23.93S 9.36S 1.97S 20.96S 1.06S 12.26S 12.12S 23.22S 23.77S 9.37D 8.0898D 692D 1.201S 1.85S 19.11S 1.03S 57.0236S 10.45S 2.068S 10.58S 24.5S 22.63S 8.73

.12D 19.32S 1.83S 15.46S .98S 11.3S 12.48S 25.2

QC Code Legend

Units

CC/i.UG/LUG/LUG/Luc/uUtf-wrt.ua<-UtfLUG/LUG/LUG/LUJ/Lve/LMG/LuMHOMG/L1%/U

UG/LU6/LMG/LUG/LMG/LUG/LUG/LU6A-UViUG/LMG/LUG/l,

ue/Lu«>A-UG/LUG/LUG/L

B Blanks KC Control Samples MD Duplicates R


0.95 127 %R: *12.2 91 %R:9.5 109 %R:24 104 %R:24 103 %R:

9.5 98 %R:1.81 103 %R;12^ 89 %Ft0.95 124 %R:12.2 80 %R:9.5 104 KR:24 96 %R:24 100 %R:9.5 95 %R:

3 %D0 %D9 %D

1.81 87 %R;12.2 112 %R:0.95 115 %R:47.6 103 %R:12.2 78 %R:

1 97 %R:9.5 105 %R:24 97 %R:24 93 %R:9.5 90 %R:

1 %D1.81 94 %R;12.2 86 %R:0.95 103 %R:12.2 77 %R:9.5 117 %R:24 103 %R:

ICalibration Checks S SpikesMatrix Spike DuplicatesSurrogates

- QC Calculations — LowerQC2 Umlt

7575757575757575757575757575

75757575757575757575

757575757575

UpperUmlt

125125125125125125125125125125125125125125202020125125125125125125125125125125

20125125125125125125



QUALITY CONTROL REPORT -Printed: 10/30/96

QCWS* Lab* Test ID Code Result

660 MAR96-26784S SE-GFAA675 MAR96-26784S TL-GFAA512 MAR96-26785D PH-LAB565 MAR96-26785S AG-GFAA639 MAR96-26785S AS-GFAA625 MAR96-26785S CD-GFAA734 MAR96-26785S CR-GFAA627 MAR96-26785S PB-GFAA607 MAR96-26785S SB-GFAA660 MAR96-26785S SE-GFAA675 MAR96-26785S TL-GFAA564 MAR96-26786D ALK588 MAR96-26786D TDS627 MAR96-26786D TURB565 MAR96-26786S AG-GFAA682 MAR96-26786S AS-GFAA557 MAR96-26786S BA-ICP557 MAR96-26786S BE-ICP557 MAR96-26786S CA-JCP625 MAR96-26786S CD-GFAA557 MAR96-26786S CO-iCP734 MAR96-26786S CR-GFAA557 MAR96-26786S CR-ICP557 MAR96-26786S CU-ICP557 MAR96-26786S FE-ICP557 MAR96-26786S K-ICP557- MAR96-26786S MG-ICP557 MAR96-26786S MN-iCP557 MAR96-26786S NA-ICP557 MAR96-26786S NI-ICP627 MAR96-26786S PB-GFAA607 MAR96-26786S SB-GFAA660 MAR96-26786S SE-GFAA638 MAR96-26786S TL-GFAA557 MAR96-26786S V-1CP

S 17.17S 5.47D 7.05S 1.79S 13.2S .91S 10.38S 11.28S 24.7S 17.55S 5.47D 1.6D 3D .121S 1.57S 11.22S 9806S 235.05S 24.05068S 1.12S 2394.84S 11.99S 947.91S 1211.24S 4723.4S 24.44358S 24.39803S 2394.82S 25.09955S 2391.02S 9.41S 22.92S 14.38S 9.18S 2412.11

QC Code Legend


U&A- 24 76 %R:Utf/L 9.5 51 %R:S.U. 0 %DU6/L 1.81 86 %R;UfirV 12.2 96 %R;US/L 0.95 98 %R:UGA. 12.2 77 %R:UGA. 9.5 119 %R:UGA. 24 101 %R:y«A- 24 72 %R: *Ufi/L 13 37 %R: *MG/L 0 %DMG/L 0 %DNTU 2 %DUfiA- 1.81 85 %R:UGA, 12.2 104 %R:MC/L 10000 98 %R;t*G/L 250 94 %R;**eA- 25 96 %R:U^ 0.95 121 %R:M4<- 2500 96 %R:UG/L 12.2 95 %R:N6/U 1000 95 %R:*A«/U 1250 97 %R:Mfi/U 5000 95 %R:Mfl/u 25 98 %R:*M/u 25 97 %R:MO/u 2500 96 %R:•Wt. 25 100 %R:M4/u 2500 96 %R:UGA. 9.5 99 %R:UGA. 24 94 %R;ttf/L 24 63 %R: *i /L 9.5 96 %R:f^/c. 2500 96 %R:



7575

757575757575757580

80757575757575757575757575757575757575757575

UpperLimit

125

20125125125125125125125125202020125125125125125125125125125125125125125125125125125125125125125




QCWS« Lab* Test ID Code Result

557 MAR96-26786S ZN-ICP565 MAR96-26787D AG-GFAA639 MAR96-26787D AS-GFAA557 MAR96-26787D BA-ICP557 MAR96-26787D BE-ICP557 MAR96-26787D CA-ICP625 MAR96-26787D CD-GFAA557 MAR96-26787D CO-ICP734 MAR96-26787D CR-GFAA557 MAR96-26787D CR-ICP557 MAR96-26787D CU-ICP557 MAR96-26787D FE-ICP557 MAR96-26787D K-ICP557 MAR96-26787D MG-ICP557 MAR96-26787D MN-ICP557 MAR96-26787D NA-ICP557 MAR96-26787D NI-ICP679 MAR96-26787D PB-GFAA607 MAR96-26787D SB-GFAA660 MAR96-26787D SE-GFAA638 MAR96-26787D TL-GFAA557 MAR96-26787D V-ICP557 MAR96-26787D ZN-ICP565 MAR96-26787S AG-GFAA639 MAR96-26787S AS-GFAA625 MAR96-26787S CO-GFAA734 MAR96-26787S CR-GFAA734 MAR96-26787S CR-GFAA*679 MAR96-26787S PB-GFAA607 MAR96-26787S SB-GFAA660 MAR96-26787S SE-GFAA638 MAR96-26787S TL-GFAA557 MAR96-26788 BA-ICP565 MAR96-26788S AG-GFAA639 MAR96-26788S AS-GFAA

S 2431.01D .13D -.16D 101.87D .74D 67.31385D .01D -.65D .4D 1.71D 1.93D 60.56D 1.78797D 28.14398D 14.11D 10.31832D 6.82D 6.79D .33D 1.66D .11D .04D 2.28S 1.77S 12.48S .96

12.49S 10.61S 12.9S 24.54S 24.77S 8.9

100.24S 1.75S 12.55

QC Code Legend


UflA- 2500 97 %R:uart-. 378 %D *ufiA. 446 %D 'Mfi/L 5 %DMfi/t 0 %DMG/L 2 %DMtft. 600 %D *Mfr/L 883 %D •UG/L 50 %D *M«4. 120 %D *M«/U 101 %D *MC/u 49 %D *Mtfu 2 %DfAC/L 3 %DfteJu 0 %Dr«£/u 4 %Dt*Gtl- 33 %D *UGA. 82 %D *UGA. 6 %D•UGTu 281 %D *ue/L 200 %D ••*WC/L 55 %D *HAfi/u 104 %D *W6/U 1.81 100 %R:UGA. 12.2 99 %R:IX/l- 0.95 103 %R:UGA. 12.2UGA. 12.2 81 %R-UGA. 9.5 106 %R:UGA. 24 101 %R:UC/U 24 104 %R:oa/u 9.5 94 %R:MCA.UQ'u 1.81 93 %R:UC/U 12.2 99 %R:


- QC Calculations - Lower UpperQC2 Limit Limit

75 1252020202020

80 2020202020202020202020202020

80 202020

75 12575 12575 12575 12575 12575 12575 12575 12575 125

75 12575 125




ws#625734679607660638742565639625742734679607724638565682625734679607724638639625734679607724638734565682625

Lab*

MAR96-26788SMAR96-26788SMAR96-26788SMAR96-26788SMAR96-26788SMAR96-26788SMAR96-26789DMAR96-26789SMAR96-26789SMAR96-26789SMAR96-26789SMAR96-26789SMAR96-26789SMAR96-26789SMAR96-26789SMAR96-26789SMAR96-26790SMAR96-26790SMAR96-26790SMAR96-26790SMAR96-26790SMAR96-26790SMAR96-26790SMAR96-26790SMAR96-26791SMAR96-26791SMAR96-26791SMAR96-26791SMAR96-26791SMAR96-26791SMAR96-26791SMAR96-26792MAR96-26792SMAR96-26792SMAR96-26792S

QCTest ID Code Result

CD-GFAACR-GFAAPB-GFAASB-GFAASE-GFAATL-GFAACL-ICAG-GFAAAS-GFAACD-GFAACL-ICCR-GFAAPB-GFAASB-GFAASE-GFAATL-GFAAAG-GFAAAS-GFAACD-GFAACR-GFAAPB-GFAASB-GFAASE-GFAATL-GFAAAS-GFAACD-GFAACR-GFAAPB-GFAASB-GFAASE-GFAATL-GFAACR-GFAAAG-GFAAAS-GFAACD-GFAA

S .88S 9.86S 9.91S 25.4S 22.03S 8.06D 16.906S 1.93S 12.34S .87S 31.772S 11.08S 18.1S 24.88S 27.13S 8.76S 2.8S 14.25S .9S 10.89S 10.3S 23.96S 20.64S 8.22S 12.2S .97S - 11.97S 16.75S 25.77S 22.35S 8.12S 18.8S 1.66S 16.77S 1.15

QC Code Legend

Units

Ufi/uUG/LUG/LUG/LOG/uUG/L

MG/LusA.U L

i*VLMG/LUG/LUG/LUG/LUG/LUSA.Uaft-UG/Ltt/L

UG/LUG/LUG/LUG/LueA-ueA-oe/t.UG/LUG/LUG/LUG/LC£/CUG/LtJC/t.

UG/LU6/U

B Blanks KC Control Samples MD Duplicates R

True - QC Calculations - - QC Calculations - LowerAdded QC1 QC2 Um't

0.9512.29.524249.5

1.8112.20.95

2012.29.52424

9.51.8112.20.9512.29.524

19.29.5

12.20.9512.29.524249.5

12.21.8112.20.95

1

102 %R:75 %R:

105 %R:103 %R:96 %R:83 %R:

200 %D *87 %R:

100 %R:87 %R:

159 %R: *89 %R:99 %R:

103 %R:112 %R:90 %R:QA <W.R-«7*T /Orx.

124 %R:Q7 %R*9* /Orx.

87 %R:108 %R:99 %R:

103 %R:OQ Q/.D>OO /Orx.

82 %R:100 %R:

Q"> CULD.9O TDfx.

97 %R:104 %R:89 %R:QC 0/D-OO 7Qr\.

86 %R:89 %R:94 %R:86 %R:

757575757575

75757575757575757575757575757575757575757575757575757575

UpperLimit

12512512512512512520125125125125125125125125125125125125125125125125125125125125125125125125125125125125

Calibration Checks S Spikes !Matrix Spike DuplicatesSurrogates |




QCWS* Lab# Test ID Code Result

607 MAR96-26792S SB-GFAA724 MAR96-26792S SE-GFAA638 MAR96-26792S TL-GFAA554 MAR96-26793D COND-L565 MAR96-26793S AG-GFAA682 MAR96-26793S AS-GFAA625 MAR96-26793S CD-GFAA734 MAR96-26793S CR-GFAA679 MAR96-26793S PB-GFAA607 MAR96-26793S SB-GFAA724 MAR96-26793S SE-GFAA638 MAR96-26793S TL-GFAA545 MAR96-26794D COD-LO742 MAR96-26794D SO4-IC565 MAR96-26794S AG-GFAA682 MAR96-26794S AS-GFAA625 MAR96-26794S CD-GFAA734 MAR96-26794S CR-GFAA679 MAR96-26794S PB-GFAA607 MAR96-26794S SB-GFAA724 MAR96-26794S SE-GFAA638 MAR96-26794S TL-GFAA512 MAR96-26795D PH-LAB724 MAR96-26795D SE-GFAA565 MAR96-26795S AG-GFAA682 MAR96-26795S AS-GFAA625 MAR96-26795S CD-GFAA734 MAR96-26795S CR-GFAA679 MAR96-26795S PB-GFAA607 MAR96-26795S SB-GFAA724 MAR96-26795S SE-GFAA638 MAR96-26795S TL-GFAA615 MAR96-26796D NH3588 MAR96-26796D TDS527 MAR96-26796D TURB

S 22.52S 20.58S 8.93D 716S 1.58S 19.17S 1.2S 21.22S 19.16S 18.66S 20.21S 8.74D 83.7388D 64.294S 1.66S 18.24S .92S 11.8S 11.87S 20.59S 17.97S 8.16D 6.82D -.81S 2.75S 18.69S 1.54S 14.04S 10.35S 21.76S 25.22S 7.31D .239D 1146D 9.45

QC Code Legend

Units

UGA.UGA.ue/upMHOl*A-UGA.

UtflUGA.UGA.UGA.UGA.utfcMGA.MGA.IX/LUGA.06/LUGA.UGA.UGA.UGA.OCA.S.U.UGA.

wsA,UGA.U6/LUGA.UGA.UGA.UGA.U6/LMGA.MGA.NTU

8 Blanks KC Control Samples MD Duplicates R


24 91 %R;24 77 %R:

9.5 91 %R:0 %D

1.81 90 %R;12.2 110 %R;0.95 89 %R;12.2 103 %R:9.5 98 %R:24 76 %R:24 80 %R:9.5 86 %R:

2 %D4 %D

1.81 86 %R:12.2 107 %R;0.95 102 %R:12.2 88 %R;9.5 106 %R;24 84 %R:24 76 %R:9.5 86 %R:

0 %0172 %D *

1.81 88 %R:12.2 106 %R;0.95 93 %R:12.2 109 %R:9.5 102 %R:24 89 %R;24 105 %R:

9.5 78 %R:5 %D2 %D0 %D

Calibration Checks S SpikesMatrix Spike DuplicatesSurrogates


757575

7575757575757575

7575757575757575

7575757575757575

80

UpperLimit

1251251252012512512512512512512512520201251251251251251251251252020125125125125125125125125202020


APPENDIX B.

SPECIAL PURPOSE SAMPLING RESULTS

TABLES-3TREMONT LANDFILL FIELD MEASUREMENTS

SPECIAL PURPOSE WELLS

10/09/96 MW-5DMW-5DDWS 96-61

33.7534.1327.50

1025.711025.281025.37

7.667.32

8991114

11.211.2

/tremont/fldmeas2.wk3;13 - Dec - 96 Eagon & Associates, Inc.







Matrix: WaterProject#:

Your Sample ID: MW-5DSample Source: RCRA

Client Project #:Date Submitted to Lab: 10/10/96



Phone: (614)888-5760 Ext:FAX: (614)888-5763


- COLLECTION INFORMATION -Date/Time/By: 10/9/96 5:00 PM HEINK

Test Grou EPA Method Test Result UnitsAnalysis

Date Analyst WS#

NH3NO3

CL-ICSO4-ICPH-LABTDSALKTURBCOND-LSB-GFAAAS-GFAABA-ICPBE-ICPCD-GFAACO-ICPCU-ICPPB-GFAANI-ICPSE-GFAAAG-GFAATL-GFAAV-ICP

350.1D3867-90A/9200

300.0300.0

D1293-84/9040160.1

SM 2300B180.1

251 OB/90503113B/70413I13B/7060200.7/6010200.7/601031I3B/7131200.7/6010200.7/60103I13B/7421200.7/60103M3B/77403U3B/776131I3B/784I200.7/6010

Nitrogen, Ammonia (as N)Nitrate + Nitrite NChloride, ClSulfate, SO4pH,LabResidue, Filterable (Dissolved Solids)Alkalinity, TotalTurbidityConductivity, LabAntimony, SbArsenic, AsBarium, BaBeryllium, BeCadmium, CdCobalt, CoCopper, CuLead,PbNickel. NiSelenium, SeSilverThallium. TlVanadium, V

0.10<0.05

1024

6.92595484110882

<3.08.3321

<0.5<0.5<10<10

<2.0<20

<3.0<I.O<1.0<20


MG/LMG/LNTU


10/15/9610/17/9610/23/9610/23/9610/10/9610/16/9610/14/9610/10/9610/15/9610/1679610/19/9610/15/9610/15/9610/18/9610/15/9610/15/9610/18/9610/15/9610/16/9610/15/9610/19/9610/15/96


SMMROH

ROHROHSMM

555598742742512588564527554607639557557625557557627557579565638557




• CERTIFICATE OF ANALYSIS (REPRINT) -


Lab Number MAR96-26779 -Continuedfrom Previous Page

WS#Analysis

Result Units Date Analyst

ZN-ICPNA-ICPMG-ICPCA-ICPK-ICPFE-ICPMN-ICPCOD-LOCR-GFAA

200.7/6010200.7/6060200.7/6010200.7/6010200.7/6010200.7/6010200.7/6010410.2/7196

31I3B/7191

Zinc,ZnSodium, NaMagnesium, MgCalcium, CaPotassium, KIron,FcManganese, MnCOD, Low LevelChromium, Cr

<106.3

46.199.9<1.0

104007411

<5.0


10/15/9610/15/9610/15/9610/15/9610/15/9610/15/9610/15/9610/11/9610/24/96


557557557557557557557545734

_ EndofReoortn/ . & /J—Report Approved By: M / r\lOSc /I •

/frfis**"-^7




Client: EAGON & ASSOCIATES INCATEL Sample No.: 96-14274-MELDate Sampled: 10/09/96Date Received: 10/11/96Date Analyzed 8260: 10/15/96Date Analyzed 8240: 10/21/96Client ID: MW-5D

Method: SW-846; 8260, 8240(SIM)Sample Type: WATERPercent Solids:Analyst: SPE/JSMProject No.:TREMONT LANDFILL


AcetoneAcrylonitrile (SIM)BenzeneBromochloromethaneBromodichl or ome thaneBromofonnCarbon DisulfideCarbon TetrachlorideChlorobenzeneChloroethaneChloroformDibromochloromethanel,2-Dibromo-3-chloropropane1,2-Dibromoethaneo-Dichlorobenzenep-Dichlorobenzenetrans-l,4-Dichloro-2-Butene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenecis-l,2-Dichloroethenetrans-l,2-Dichloroethene1.2-Dichloropropanecis-l,3-Dichloropropenetrans-1,3-DichloropropeneEthyl Benzene2-HexanoneBromome thaneChloromethaneDibromome thaneMethy1ene Chloride

5.1,1.1.

5.05.01.01.01.01.0

0000

0.51.01.01.01.01.0

< 1.01.0

< 0 . 5< 0.5< 0.5< 0.5< 1.0< 1.0< 1.0< 1.0< 10.0< 1.0< 1.0< 1.0< 1.0

2-Butanone < 10.0lodomethane < 10.04-Methyl-2-Pentanone < 20.0Styrene < 1.01,1,1,2-Tetrachloroethane < 1.01,1,2,2-Tetrachloroethane < 1.0Tetrachloroethene < 1.0Toluene < 1.01.1.1-Trichloroethane < 1.01.1.2-Trichloroethane < 1.0Trichloroethene < 0.5Trichlorofluoromethane < 1.01,2,3-Trichloropropane < 1.0Vinyl Acetate < 10.0Vinyl Chloride < 1.0Total Xylenes < 2.0







Lab Number MAR96-26780 -Continuedfrom Previous Page

WS#Analysis

Result Units Date Analyst

ZN-ICPNA-ICPMG-ICPCA-ICPK-ICPFE-ICPMN-ICPCOD-LOCR-GFAA

200.7/6010200.7/6060200.7/6010200.7/6010200.7/6010200.7/6010200.7/6010410.2/719631I3B/7191

Zinc,ZnSodium, NaMagnesium, MgCalcium, CaPotassium, KIron,FcManganese, MnCOD, Low LevelChromium, Cr

<106.7

57.61341.165

1220<8

<5.0

Report Approved By:


^

10/15/9610/15/9610/15/9610/15/9610/15/9610/15/9610/15/9610/11/9610/24/96

£>

J i f f


idofRepon

ft/***7

557557557557557557557545734

rr~->




Client: EAGON & ASSOCIATES INCATEL Sample No.: 96-14275-MELDate Sampled: 10/09/96Date Received: 10/11/96Date Analyzed 8260: 10/15/96Date Analyzed 8240: 10/21/96Client ID: MW-5DD

Method: SW-846; 8260, 8240(SIM)Sample Type: WATERPercent Solids:Analys t: SPH/JSMProject No.:TREMONT LANDFILL


Acetone <Acrylonitrile (SIM) <Benzene <Bromochloromethane <Bromodichloromethane <Bromoform <Carbon Bisulfide <Carbon Tetrachloride <Chlorobenzene <Chloroethane <Chloroform <Dibromochloromethane <l,2-Dibromo-3-chloropropane <1,2-Dibromoethane <o-Dichlorobenzene <p-Dichlorobenzene <trans-l,4-Dichloro-2-Butene <1.1-Dichloroethane1.2-Dichloroethane <1.1-Dichloroethene <cis-1,2-Dichloroethene <trans-1,2-Dichloroethene <1.2-Dichloropropane <cis-1,3-Dichloropropene <trans-1,3-Dichloropropene <Ethyl Benzene <2-Hexanone <Bromome thane <Chloromethane <Dibromomethane <Hethylene Chloride <

5.5.1.1.1.1.5.1.1.1.0.1.1.1.1.1.I.1.0.0.0.0.1.1.1.1.

10.01.01.01.01.0

Surrogate Data:

2-Butanone < 10.0lodomethane < 10.04-Methyl-2-Pentanone < 20.0Styrene < 1.01,1,1,2-Tetrachloroethane < 1.01,1,2,2-Tetrachloroethane < 1.0Tetrachloroethene < 1.0Toluene < 1.01.1.1-Trichloroethane < 1.01.1.2-Trichloroethane < 1.0Trichloroethene < 0.5Trichlorofluoromethane < 1.01,2,3-Trichloropropane < 1.0Vinyl Acetate < 10.0Vinyl Chloride < 1.0Total Xylenes < 2.0

% Recovery



TABLE B-l.WATER-QUALITY RESULTS SUMMARY

WELL MW-5DTREMONT LANDFILL

x"::::::::::;:;x::;:;:::::::"

1 Antimony (total)2 Arsenic (total)3 Barium (total)4 Beryllium (total)5 Cadmium (total)6 Chromium (total)7 Cobalt (total)8 Copper (total)9 Lead (total)

10 Nickel (total)11 Selenium (total)12 Silver (total)13 Thallium (total)14 Vanadium (total)15 Zinc (total)63 Ammonia64 Chloride65 Sodium66 Chemical Oxygen Demand

Sfc&iWSSKSs:::

iliiillugtfug/€ug/€ugtfugtfugtfugtfug/€ugtfug/ûg/<ug/ûg/fug/€ug/€mg/^mg/^mg/€mg/€

:B:ssips:j«

•1<3.0

92.3240<5.0<OJ<5.0

<20.0<10.0<2.0

<20.0<3.0<1.0<1.0

<20.0<10.0

0.118J8565<8

sSiig;?: !?;?!;:;;;

<3.08.2

330.0<05<OS<5.0

<10.0<10.0<10

<20.0<3.0<1.0<1.0

<20.0<10.0

0.1412.10

5.8<8

$$%xa®.

<3.092

327.0<05<05<5.0

<20.0<10.0

<2.0<20.0

<3.0<1.0<1.0

<20.0<10.0

0.1211.00

5.6<8

wmmm

•I

<3.014.0

332.0<0^<OJ<5.0

<20.0<10.0

<2.0<20.0

<3.0<1.0<1.0

<20.0<10.0

0301130

5.4<8

•

i:::;¥:?5i|::?:?S:;SS:::

iliPilP;|i 95i:iiliilli Iiliilli

mmmm

mmmm

MKismtti

<3.010.0

327.0<OJ<05<5.0

<20.0<10.0<2.0

<20.0<3.0<1.0<1.0

<20.0<10.0

0.118.725.6<8

mmmm

liiiil::::::::::-::::::::xtt::;:;::::x:::::v:::v::::::::::::::;;:v:vX;:;::

<3.08.8

323.0<0.5<OJ<5.0

<20.0<10.0

<2.0<20.0

<3.0<1.0<1.0

<20.0<10.0

0.1016.90

6.5<8

<3.083

321.0<OJ<0.5<5.0

<10.0<10.0

<2.0<20.0

<3.0<1.0<1.0

<20.0<10.0

0.1010.06311

mmmm

mtffvotfi^mlllfllilillli'0t>siii*iliiiSni:s

7777777777777777777

\tremont\wqtables\mw5dwqd.wk3; 19-Dec-96 Page 1 of2 jEaôn <ft Associates, Inc.

TABLE B-l.WATER-QUALITY RESULTS SUMMARY (cont'd)

WELL MW-5DDTREMONT LANDFILL

1 Antimony (total)2 Arsenic (total)3 Barium (total)4 Beryllium (total)5 Cadmium (total)6 Chromium (total)7 Cobalt (total)8 Copper (total)9 Lead (total)

10 Nickel (total)11 Selenium (total)12 Silver (total)13 Thallium (total)14 Vanadium (total)15 Zinc (total)63 Ammonia64 Chloride65 Sodium66 Chemical Oxygen Demand

XC :-:-v':: " '':• •. ^^'t'*'^?ttftttfX}^^

ugtfug/fugtfugtfugtfugtfugtfugtfugtfugtfugtfugtfugtfugtfug/€mg/€mg/€mg/€mg/€

t>mmm?ii.

•<3.0<3.0

422.0<5.0<0^<5.0

<20.0<10.0

2.0<20.0<3.0<1.0<1.0

<20.0<10.0<0.05

6.776^<8

::??;SSSS:::::::;s;;*:-

•

<3.0<3.0

435.0<Q5<Q5<5.0

<10.0<10.0

<2.Q<20.0<3.0<1.0<1.0

<20.0<10.0

0.056.735.1<8

•<3.0<3.0

414.0<OJ<05<5.0

<20.0<10.0<2.0

<20.0<3.0<1.0<1.0

<20.0<10.0

0.077.026.0<8

WMSimm

<3.0<3.0

402.0<05<OJ<5.0

<20.0<10.0<2.0

<20.0<3.0<1.0<1.0

<20.0<10.0

0.186.445.6<8

::':::::::::;::i:;:::::::;:::>;::-:'::::: ;:;:;:;:|x::::|:j:o:;;i:;:|:;:;:>i:;:

SKSS'SSi iSSS

i^^^llii

•

;:;::;::::;;;::;:;:;:::;:;:::::::;:;x:::

liiiiiii

:-i':-;'::::;::; :; ••; 'i-i^v'-'- '••'•';-

i i iS^^

<3.0<3.0355.0<OJ<0.5<5.0

<20.0<10.0<2.0

<20.0<3.0<1.0<1.0

<20.0<10.0

0.076.4363<8

ilSiiiffi*?;"?

liiii<3.0<3.0393.0<0.5<0^<5.0

<20.0<10.0<2.0

<20.0<15.0<1.0<1.0

<20.0<10.0

0.068.115.6<8

;v:':':-:'::x::':::::::o::::;v;v

iiiiiiliiiiiii<3.0<3.0

454.0<OJ<OJ<5.0

<10.0<10.0<2.0

<20.0<3.0<1.0<1.0

<20.0<10.0

0.0610.06.7<8

35:::¥S:::;:S5S:SS

lilf^^lllObservations

7777777777777777777

\tremont\wqtables\mw5ddwqd.wk3; 19-Dec-96 Page 2 of2 Eagoa & Associates, Inc.

TABLE B-2.VOC DETECTIONS

TREMONT LANDFILL

•g^&fM&m&m&mmmmmmmmmWell Number

MW-5D

MW-5DD

mm$*^mmmiillJateiifl

10/03/94

11/28/94

02/01/95

04/05/95

07/28/95

10/06/95

04/02/96

10/09/96

10/03/94

11/28/94

02/01/95

04/05/95

07/28/95

10/06/95

04/02/96

10/09/96

lifiiiilflil

Illillillllil^mmemim5.8

<1.0

5.1

4.8

55

6.2

<1.0

<1.0

5.9

<1.0

4.2

3.1

4.8

5.9

3.1

<1.0

1.4

15

1.9

13

1.9

1.7

1.6

1.0

2.0

1.7

1.8

1.4

2.0

2.0

1.6

1.6

I JO

0.9

1.2

0.7

\2

1.0

<05

<05

1.2

13

15

1.0

1.8

2.2

<05

<05

lliiseiiiiil

<20.0

<5.0

<5.0

22.6

<5.0

<20.0

<5.0

<5.0

<20.0

<5.0

<5.0

45.0

<5.0

<20.0

<5.0

<5.0

Aremont/vocdec2.wk3; 13 - Dec-96 Eagon & Associates, Inc.

APPENDIX C.

TREND PLOTS

TREHONT LANDFILJLArsenic, total Oct 03, 1994 To Oct 09, 1996

/•S

J3

~i I i i i ! i i i i i i i i i i i i i i i i i i i i i i I i

2.4900 -

1.6600 -

0.8300 -

0.0000-

12/15/94 05/12/95 10/06/95 03/01/96 07/27/9610/03/94 02/27/95 07/24/95 12/19/95 05/14/96 10/08/96

+ MU-1R X MW-3R MW-7D aMW-8D

TKXHONT LAHDFILJLBariun, total Oct 03, 1994 To Oct 09, 1996

,«.J5

n

759.0000

683.1000

607.2000

531.2999

455.3999

379.5000

303.6000

227.7000

151.8000

75.9000

0.0000i I i i i I i i i i i i i i i i i I i i i i i i i i i i i i i i i I i i i i i i i i

12X15/94 05/12X95 10/06/95 03/01/96 07/27/9610/03/94 02/27/95 07/24/95 12/19/95 05/14/96 10/08/96

+ MW-1R XMU-3R D MM-7D MU-8D Sanple Dates

TREHONT LANDFILLLead, total Oct 03, 1994 To Oct 09, 1996

3.6000

3.2400

2.8800

2.5200

2.1600

1.8000

1.4400

1.0800

0.7200

0.3600

0.0000i I i i i I i i i i i i i i i i i I i i i i i i i i i i i i i i i I i i i i i i i i

12/15/94 05/12/95 10/06/95 03/01/96 07/27/9610/03/94 02/27/95 07/24/95 12/19/95 05/14/96 10/08/96

MW-1R X MW-3R D MU-7D » MW-8DSanple Dates

TREHONT LAHDFIIX.Silver, total Oct 03, 1994 To Oct 09, 1996

tn(I

1.3000

1.1700

1.0400

0.9100

0 .7800

0.6500

0.5200

0.3900

0.2600

0.1300

0.0000i I i i i I i i i i i i i i i i i i i i i i i i i i i i i i I i i i i i i i i

12/15/94 05/12/95 10/06/95 03/01/96 07/27/9610/03/94 02/27/95 07/24/95 12/19/95 05/14/96 10/08/96

MU-1R X MW-3R D MM-7D oMU-8DSanple

LAMDFIU.Zinc, total Oct 03, 1994 To Oct 09, 1996

/•»J5

N

11.0000

9.9000

8.8000

7.7000

6.6000

5.5000

4.4000

3.3000

2.2000

1.1000

0.0000

-

^

-

-

—

-

- 1

_

—

_

^

"I

3 ——— B-

1 1 I1

1 ——— D —

1 1 1

—— B ——

1 1 1

—————

...........1 I 1

T

DBBB I

1 1 I

1 —————

i i t i i i i

i — B ———

............' i l l 1 1 1

————— 1

I I I

1

|12/15/94 05/12/95 18/86/95 83/01/96 07/27/96

10/03/94 82/27/95 87/24/95 12/19/95 85/14/96 18/08/96

+ MW-iR X MW-3R D MU-7D MU-8DSanple Dates

TRD1ONT LAHDFILJLAnnonia. Nitrogen Oct 03, 1994 To Oct 09, 1996

/N

a.V

z

0£<X

1.8100

1.6290

1.4480

1.2670

1.0860

0.9050

0.7240

0.5430

0.3620

0.1810

0.0000i I i i i i i i i i i i i i i i i I i i i i i i i i i i i i i i i I ii i i i i i i i

12/J15/94 05/12/95 10/06/95 03/01/96 07/27/9610/03/94 I 02/27/95 07/24/95 12/19/95 05/14/96 10/08/96

•f MU-1R X MU-3R D MU-7D MU-8D A MI4-7S Z MMDates-8S

TREHONT LfiKWIlI.Chloride Oct 03, 1994 To Oct 09, 1996

A

01-c• HJ-0p-

u

47.9999

43.1999

38.3999

33.5999

28.8000

24.0000

19.2000

14.4000

9.6000

4 .8000

0.0000'I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I

12/15/94 05/12/95 10/06/95 03/01/96 07/27/9610/03/94 02/27/95 07/24/95 12/19/95 05/14/96 10/08/96

MU-1R X MU-3R D MU-7D MU-8DSample DatesA MH-7S X MW-8S

TREMONT LAHDFILI.Sodiun Oct 03, 1994 To Oct 09, 1996

15.4000 -

I I I I I I I I I I I I I I I I I I I I I0.0000 -

12/15/94 05/12/95 10/06/95 03/01/96 07/27/9610/03/94 02/27/95 07/24/95 12/19/95 05/14/96 10/08/96

MU-1R X MM-3R D MW-7D oMW-8D Sanple DatesA MU-7S X MW-8S

IKEHONT LAMDQFILI.Chenical Oxygen Denand Oct 03, 1994 To Oct 09, 1996

ino

ffaoouou£0<hU)

•«H

2.5649

2.3084

2.0519

1.7954

1.5389

1.2824

1.0259

0.7694

0.5129

0.2564

0.0000"i I I I I I I I I i I I I i I I I I I I I i t i i i I

12/15/94 05/12/95 10/06/95 03/01/96 07/27/9610/03/94 02/27/95 07/24/95 12/19/95 05/14/96 10/08/96

+ MU-IR X MH-3R MU-7D sanpie DatesMM-8D AMW-7S X MW-8S

APPENDIX D.

CONTROL CHARTS

Report Printed: 12-12-1996 10:44

Facility:TREMONT TREMONT LANDFILL

Address:3108 SNYDER DOMER RD

ST:OH Zip:45502City:SPRINGFIELDCounty:CLARK

Contact:ROD CHRISTENPhone:( ) -

Permit Type:(* No Permit Type Specified *)

MCL: 0.000 ppbACL: 0.000 ppb

Detect Limit: 0.000 ppb

Start Date:Oct 06 1995End Date:Oct 09 1996

Mean (/z) :Std Deviation (a):

Decision Internal Value (h):Reference Value (k):

Shewart Control Limit (SCL):

4.980.095.001.004.50

(Ln)pp(Ln)pp Mean and Std Deviation

based on 8 readingsprior to Oct 06,1995

* Indicates out-of-control process via (Zi>SCL) or (Si>h)

Oct 06Apr 01Oct 09

123

111

4.885.095.05

-1.271.290.77

•2.27-0.29•0.23

0.000.290.06

COMB IKED Sheuavt-OISUH CHARTTREHONT LANDFILL UelI:MU-1R Oct 06, 1995 To Oct 09, 1996

•*»tfl

0>H•*»

01u0u

5.0000-

4.3000-

3.6000-

-2.0000 -

+-SCL

10/06/9504/07/96

10/09/96

-f-CUSUMDStand*Y>dlized MeanSanpltnsr Pemtod




City:SPRINGFIELD ST:OH Zip:45502County:CLARK



MCL:ACL:

Detect Limit:

0.000 ppm0.000 ppm0.000 ppm


Mean (/*) :Std Deviation (a):




£.051A

•

•

*

•

/ \J470000Rn

{uu}(Ln)

ffPP Mean and

based onprior to

Std

Oct

Deviation8 readings06,1995

Oct 06Apr 01Oct 09

123

111

-2.81--2.81-2.81

•0.25•0.25•0.25

•1.25•1.25•1.25

0.4Q0.000.00

COMBINED Shewart—CUSUH CHftRTTREMONT LANDFILL Well:MW-lR Oct 06, 1995 To Oct 09, 1996

H3•cv

r0

u0u

0££

<Z

4. :000

4.4000

3 on A Ok.8O0O

2.6000

2 AAA A.0000

1.4000

e octctn

0.4000

I omckct

i

--

_^

—

_.

„

—_-

Lrf

_

-

0/0

1

...........................................................

•

1 1 1 104/0

6/95

...........................................................

——————————————————————————————rL

1 1 1 17/96

10/04

D

9/9«

*-SCL

+ CUSUMDStAr»dArdi2ed Mean Pemiod







MCL:ACL:

Detect Limit:

6.000 ppm0.000 ppm0.000 ppm


•.-: v.----*:-K-.'.w>.-.v--"- .-.-.--•.-.•.•.•:•.•,•.-.• .•.-.--•.-.-.•.•.•.•.•.•.•.•.•.•.•.•.•.•.•.v

MeanStd Deviation (a):



6.20 ppm2.24 ppm5.001.004.50

Mean and Std Deviationbased on 8 readingsprior to Oct 06,1995


Oct 06Apr 01Oct 09

123

111

6.179.779.00

-0.011.601.25

-1.010.600.25

0.000.600.85

COMBINED SheiiCTt-CIISIM CHARTTREMONT LANDFILL Mell:MM-lR Oct 86, 1995 To Oct 89, 1996

•8*>VI

C0

*>S010

00

0

4.:888

4.4888

3.8888

3.2888

2.6888

2.8888

1.4888

8.8888

8.2888

-8.4888

-1.8888

18X86X9584X87X96

«-SCL

18X89X96

+ CUSUMQst*nd*r-d.ized Me ATISanpl i ing Peri od




City .'SPRINGFIELD ST:OH Zip: 4 55 02County:CLARK

Contact:ROD CHRISTENPhone:( )


MCL:ACL:

Detect Limit:

0.000 ppm0.000 ppm0.000 ppm





2.21 (Ln)pp0.14 (Ln)pp5.001.004.50



Oct 06Apr 01Oct 09

123

111

1.962.212.23

-1.690.020.17

-2.69-0.98-0.83

0.000.000.00

COMBINED SKeuai-t-CUSUM CHARTTREMONT LANDFILL Uell:MU-lR Oct 06, 1995 To Get 09, 1996

(A

£

£0•r>V*

aioou

5.0000

4.3000

3.6000

2.9000

2.2000

1.5000

0.8000

0.1000

-0.6000

-1.3000

-2.0000

10/06/9504/07/96

*-SCL

10/09/96

Peri od







HKvKwS-SwSv:?MCL:ACL:

Detect Limit:

0.000 ppb0.000 ppb0.000 ppb

Start Date:Oct 06 1995End Date:Oct 09 1996IPlPlliiii$£j!%m!!/Mi3&®mm

Mean (/*):Std Deviation (a):



5.81 (Ln)pp0.03 (Ln)pp5.001.004.50



OctAprOct

060109

123

111

5.5.5.

61 -3661

-5.-13.-6.

896200

-6.-14.-7.

896200

0.0.0.

00-0000

COMBINED Sheuart—CUSUM CHARTTREMONT LANDFILL Mel l :MM-3R Oct 06, 1995 To Oct 09, 1996

(ft*»•ftC

*

01000

•8n

4.:000

3.0999

1.2000

-0.7000

-2.6000

-4.5000

-6.4000

-8.3000

-10.2000

-12.1000

-14.0000

4-SCL

10X06X9504X07X96

10X09X96

+CUSUMDstartdar'dize<dl Mean' Per*i od







mS*

MCL:ACL:

Detect Limit:

0.000 ppm0.000 ppm0.000 ppm


Std Deviation (<r) :Decision Internal Value (h):

Reference Value (k):Shewart Control Limit (SCL):

2.60 (Ln)pp0.03 (Ln)pp5.001.004.50



Oct 06Apr 01Oct 09

123

111

2.502.732.48

-2.944.25

•3.45

-3.943.25

-4.45

0.00-3.250.00

COMBINED Skewai-t-OISUn CHARTTREMONT LANDFILL Uell:MU-3R Oct 06, 1995 To Oct 89, 1996

•S•*»

otrft»*J.

01u0u01•a•HJ.O^*

U

5.0000

4.1000

3.2000

2.3000

1.4000

0.5000

-0.4000

-1.3000

-2.2000

-3.1000

-4.0000

10/06/9304/07/96

4-SCL

10/09/96

4-CUSUMDstAHdardized Mean Sanpltnsr Perl od




ST:OH Zip:45502City .'SPRINGFIELDCounty:CLARK



MCL:ACL:

Detect Limit:

0.000 ppm0.000 ppm0.000 ppm

Start Date:Oct 06 1995End Date:0ct 09 1996

Mean (p.) :Std Deviation (a) :



2.58 (Ln)pp0.06 (Ln)pp5.001.004.50



Oct 06Apr 01Oct 09

123

111

2.462.262.47

-1.92-5.07-1.79

-2.92-6.07-2.79

0.000.000.00

COMBINED Shewart-CUSlin CHARTTREMONT LANDFILL Well:MH-3R Oct 06, 1995 To Oct 09, 1996

•8*>\flf

0

0000

4.:000

3.9000

2.8000

1.7000

0.6000

-0.5000

-1.6000

-2.7000

-3.8000

-4.9000

-6.0000

10X06X9504X07X96

*-SCL

10X09X96

Sanpli ng Peri od

Printed: 12-12-1996 10:58






ACL:Detect Limit:

0.000 ppb0.000 ppb

Start Date:0ct 06 1995End Date:Oct 09 1996

MeanStd Deviation (a)

Decision Internal Value (h)Reference Value (k)

Shewart Control Limit (SCL)

1.93 (Ln)pp0.14 (Ln)pp5.001.004.50



Oct 06Apr 01Oct 09

123

111

1.811.841.69

-0.87-0.63-1.77

-1.87-1.63-2.77

0.000.000.00

COMBINED SKeuAT»t-CUSUH GHftRTTREMONT LANDFILL Uell:MW-7D Oct 06, 1995 To Oct 09, 1996

Of0

0u

5.0000

4.3000

3.6000

2.9000

2.2000

1.5000

0.8000

0.1000

-0.6000

-1.3000

-2.0000

4-SCL

10/06/9504/07/96

10/09/96

Meari SAMP! i r»5f Peri od







MCL:ACL:

Detect Limit:

0.000 ppb0.000 ppb0.000 ppb


MeanStd Deviation (a) :

Decision Internal Value (h) :Reference Value (k) :

Shewart Control Limit (SCL) :

6.530.06 (Ln)pp5.001.004.50


* Indicates out-of -control process via (Zi>SCL) or (Si>h)

Oct 06Apr 01Oct 09

123

111

6.506.566.36

-0.490.47-2.78

-1.49-0.53-3.78

0.000.000.00

COMBINED Skewai-t—CUSUM CHARTTREMONT LANDFILL Well:MU-7D Oct 06, 1995 To Oct 09, 1996

•«*>(ft

c

0•f

01u0u

5.0000

4.2000

3.4000

2.6000

1.8000

0.:000

0.2000

-0.6000

-1.4000

-2.2000

-3.0000

+-SCL

10/06/9504/07/96

10/09/96

+CUSUM[I]St«!mdUr<Hzed Mean Sattpl i nsr Pevl odl







'•^•tt>£#&ttt&?&&^%&$#^

MCL: 0.000 ppmACL: 0.000 ppm

Detect Limit: 0.000 ppm





0.290.085.001.004.50

(Ln)pp Mean and Std Deviationbased on 8 readingsprior to Oct 06,1995


Oct 06Apr 01Oct 09

123

11

0.200.260.10

-1.14-0.33-2.44

-2.14-1.33-3.44

0.000.000.00

COMBINED ShewMTt-CUSUM CHARTTREMONT LANDFILL Uell:MU-7D Oct 06, 1995 To Oct 09, 1996

•C

0)u0u

ao

i

5.0000

4.2000

3.4000

2.6000

1.8000

0.:000

0.2000

-0.6000

-1.4000

-2.2000

-3.0000

10X06X9504X07X96

<-SCL

10X09X96

Mean SAMP I i nsr Peri od







MCL:ACL:

Detect Limit:

0.000 ppm0.000 ppm0.000 ppm





1.510.715.001.004.50

ppmppm Mean and Std Deviation



Oct 06Apr 01Oct 09

123

111

2.052.502.50

0.761.401.40

-0.240.400.40

0.000.400.80







MCL:ACL:

Detect Limit:

0.000 ppm0.000 ppm0.000 ppm


Mean (p.) :Std Deviation (a) :

Decision Internal Value (h) :Reference Value. (k) :


0.05 (Ln)pp5.001.004.50



Oct 06Apr 01Oct 09

123

111

2.582.612.45

-0.050.54

-2.62

-1.05-0.46-3.62

0.000.000.00

COHBINED Shewart-CIISUH CHARTTREMONT LANDFILL Uell:MW-7D Oct 06, 1995 To Oct 09, 1996

0

£01u0u0)•s

u

5.0000

4 .5000

4.0000

3.5000

3.0000

2.5000

2.0000

1.5000

1.0000

0.5000

0.0000

10X06X9504X07X96

4-SCL

10X09X96

-fCUSUMQstanaaraizea tl Sanpli ng Peri







MCL:ACL:

Detect Limit:

0.000 ppb0.000 ppb0.000 ppb





380.25 ppb171.81 ppb5.001.004.50



WaSJHWSRv

OctAprOct

060109

123

1-11

223222224

.00

.00

.00

-0.-0.-0.

929291

o:w::::WK?ft:i

-1.-1.-1.

929291

000

.00

.00

.00

GDHBINED SKeuai-t-CUSUH CHARTTREMONT LANDFILL Uell :MW-7D Get 06, 1995 To Oct 09, 1996

co

Ofu0u

5.0000

4.2000

3.4000

2.6000

1.8000

0.:000

0.2000

-0.6000

-1.4000

-2.2000

-3.0000

10X06X95

+CUSUMnst*ncJUrdized Mean

04X07X96

4-SCL

10X09X96

Per>i od

COHBINKD Sheuart-CUSUM CHARTTREMONT LANDFILL Mell:MW-8D Oct 06, 1995 To Oct 09, 1996

•8•*»Ml

J.t»P01U

0

4. :000

4 . 4000

S onnet• 0000

3 AAAA.2000

. O000

2CtCkCfeCt

1 . 4000

0 OCfeCIC%

0 . 4000

1.0000

-

-

_...

-

mm,

-

-

_

_

-

-

-

1

J....... ............. .................... ..... ...Di i i i

:.........................................................£i i i i

1

10/06/95'04/07/96

10/09/96

Pey-t oa






Permit Type:Detection

MCL:ACL:

Detect Limit:

0.000 ppb0.000 ppb0.000 ppb


MeanStd Deviation (cr)




JL

1

51A

•

•

«

•

~J\J

060000Rn

ff"ppb Mean

basedprior

andonto

Std

Oct


Oct 06Apr 01Oct 09

123

111

1.002.001.00

-0.530.41-0.53

1.530.591.53

0.000.000.00

COMBINED SHewai-t-CUSUtl GHARTTREMONT LANDFILL Well:MW-8D Oct 06, 1995 To Oct 09, 1996

o

010

0u

4. :000

4.4000

3.8000

3.2000

2.6000

2.0000

1.4000

0.8000

0.2000

-0.4000

-1.0000

10X06X9304X07X96

4-SCL

10X09X96

4-COSUMDstAndardlized Mean Period

Report'"'Printed: 12-12-1996 11:16






MCL:ACL:

Detect Limit:

0.000 ppm0.000 ppm0.000 ppm


JvJwSKw.vT':-.-.': •:•.•-•:•"•;-.-. vS* -,v.v.v.v.-.v




12.277.68 ppm5.001.004.50



Oct 06Apr 01*Oct 09

123

111

19.6046.1048.00

0.96-4.414.65

-0.043.413.65

0.003.417.06

COMB IKED SKetKn-t-CUSUM CHARTTREMONT LANDFILL MelI :MU-8D Oct 06, 1995 To Oct 09, 1996

(fl•*»iH

3

•tf•>\ft

s•H

0

01u0u01•s

8.0000

7.2000

6.4000

5.6000

4.8000

4.0000

3 .2000

2.4000

1.6000

0.8000

0.0000

10X06X9504X07X96

4-SCL

10X09X96

-f CUSUMOStandardized Mean Sanplinsr Peiri od




City .'SPRINGFIELD ST:OH Zip: 4 55 02County:CLARK



MCL: 0.000 ppmACL: 0.000 ppm

Detect Limit: 0.000 ppm


Mean (/x) :Std Deviation (a):



2.01 (Ln)pp0.10 (Ln)pp5.001.004.50



Oct 06Apr 01*0ct 09

123

111

2.. 092.272.73

0.802.647.36

•0.201.646.36

.0.001.647.99

COMBINED Shetrart-CUSUH CHARTTREMONT LANDFILL Well :MM-8D Oct 06, 1995 To Oct 09, 1996

ifl•*»•i*

0

01u00

8.0000

7.2000

6.4000

5.6000

4.8000

4.0000

3.2000

2.4000

1.6000

0.8000

0.0000

10X06X9504X07X96

*-SCL

10X09X96

-j-CUSUMQstandardized Mean Sanpl i nsr Peyi od

Report '"Printed: 12-12-1996 11:19






MCL:ACL:

Detect Limit:

0.000 ppm0.000 ppm0.000 ppm





0.48 (Ln)pp0.07 (Ln)pp5.001.004.50



Oct 06Apr 01Oct 09

123

111

0.41 ._0.360.18

-1.08-1.65-4.20

-2.08-2.65-5.20

0.000.000.00

TREMONT LftNDF I S'Bel'PWl-78*0121 06, 1995 To Oct 09, 1996

3•8•**<fi

0

J.•**f010

0u

•H

0c<r

5.0000

4.0000

3.0000

2.0000

1.0000

0.0000

-1.0000

-2.0000

-3.0000

-4.0000

-5.0000

10X06X9504X07X96

+-SCL

10X09X96

+CUSUMQStandardized Mean Saitpl i nsr Peri od




City .'SPRINGFIELD ST:OH Zip:45502County:CLARK



MCL:ACL:

Detect Limit:

liiiiid.boo ppmo.ooo ppmo.ooo ppm


Mean (/LI)Std Deviation (a)



0.71 (Ln)pp0.79 (Ln)pp5.001.004.50



OctAprOct

060109

123

111

000

.72

.92

.92

0.0.0.

OL2626

-0.-0.-0.

ivwAW,\:vK-

997474

0.0.0.

000000

COMBINED Skewai-t-CUSUtl CHARTTREMONT LANDFILL Uell:MW-7S Oct 06, 1995 To Oct 09, 1996

auo

J.0ft

U

5.0000

4.5000

4.0000

3.5000

3.0000

2.5000

2.0000

1.5000

1.0000

0.5000

0.0000

«-SCL

10/06/9504/07/96

10/09/96

-f-CUSUMQst*nd*rdized MeanSanpli ng Peri od







TMCL:ACL:

Detect Limit:

6.000 ppm0.000 ppm0.000 ppm





2.470.055.001.004.50

(Ln)pp(Ln)pp Mean and Std Deviation



Oct 06Apr 01Oct 09

-0.02-3.23-5.90

0.020.000.00

COHBIHED Shewart-CUSUtf CHARTTREMONT LANDFILL Uell:MM-7S Oct 06, 1995 To Oct 09, 1996

•*»p010

0u

5.0000

4 .0000

3.0000

2.0000

1.0000

0.0000

-1.0000

-2.0000

-3.0000

-4.0000

-5.0000

+-SCL

10/06/9504X07/96

10/09/96

+CUSUMDstAr>dai~di2ed MeanPeriod







MCL:ACL:

Detect Limit:

0.000 ppm0.000 ppm0.000 ppm

Start Date:0ct 06 1995End Date:0ct 09 1996




1.49 (Ln)pp0.29 (Ln)pp5.001.004.50



«WV9Cwvvvv»

OctAprOct

vMwiyfffK-.vvK'xy

060109

123

111

1.1.2.

.•KWi iwWKwiv.'.-:-:*

39-3956

-0-0

3

KiK-X-r-K^-X-KC-X-X-X

.35

.35

.75

-1.-1.2.

353575

002

.00

.00

.75

COMB IKED Skewart-CUStlH CHARTTREMONT LANDFILL «ell:MW-7S Oct 06, 1995 To Oct 89, 1996

•Hg

0

0u0u

oou

4.:888

4.4880

3.8088

3.2888

2.6888

2.8888

1.4888

8.8888

8.2000

-0.4888

-1.0000

10/86/9584/87/96

+-SCL

10/09/96

Mean Peiri od







MCL:ACL:

Detect Limit:

0.000 ppm0.000 ppm0.000 ppm






\j . •* /0.125.001.004 . (?n

ffluppm Mean and

based onprior to

Std

Oct


>:-:•:•:•:-:-mOct 06Apr 01Oct 09

-123

i>:-W3«Ov«vM»WW»X'«-»K;

111

0.370.550.47

-0.890.66

-0.03

-1.89-0.34-1.03

0.000.000.00

USUM OIARTCOMBINED Slvewart-CUSUM TTREMONT LANDFILL Mell:MM-8S Get 06, 1995 To Dot 09, 1996

•Hc

TJ•**vn

o

4$-•*»7.01u0u

0c

4.:00e

4.4000

3.8000

3.2000

2.6000

2.0000

1.4000

0.8000

0.2000

-0.4000

-1.0000

10X06X95

-f-CUSUMnst*ndArdized Mean

+-SCL

04X07X96

Sar»plir»sr Pemi od

10X09X96







MCL:ACL:

Detect Limit:

0.000 ppm0.000 ppm0.000 ppm


Mean (p.) :Std Deviation (a):

Decision Internal Value (h):Reference Value (Jc):


2.400.675.001.004.50

ppmppm Mean and Std Deviation



Oct 06Apr 01Oct 09

1 12 13 1

3.122.502.50

1.080.150.15

0.08-0.85•0.85

0.080.000.00

TREMONTCOMBINED CHART

Oct 09, 1996

-a

o

4•*>C010

0

01•s•H

0»-

u

5.0000

4.5000

4.0000

3.5000

3.0000

2.5000

2.0000

1.5000

1.0000

0.5000

0.0000

10X06X95

+CUSUMnst*ruA*Y*dized Mean

*-SCL

04X07X96

Sanpl i nsr Peri od

10X09X96







MCL:ACL:

Detect Limit:

0.000 ppm0.000 ppm0.000 ppm


nWPlliPiHPirinîlÛ Ct %*• Cy ''JT1 Utfili t?':»'~ J' tvlJ J wXit' VtV'd 1A £?.' TM 'TJf ,«'''W >S W*





X. / t

0.175.001.006. Rn

VUiiypp(Ln)pp Mean and

based onprior to

Std

Oct


Oct 06Âpr 01Oct 09

123

111

1.761.861.52

0.69-1.30

-0.89-0.31-2.30

0.000.000.00

COMB IKED ShewCTt-CUSUM CHARTTREMONT LANDFILL Uell:MU-8S Oct 06, 1995 To Oct 09, 1996

0

j:01o0u

5.0000

4.3000

3.6000

2.9000

2.2000

1.5000

0.8000

0.1000

-0.6000

-1.3000

-2.0000

10X06X9504X07X96

«-SCL

10X09X96

+CUSUMQst*nd*rdized Mean Sanpling Peiriod



Address:3108 SNYDER DOMER RO




MCL:ACL:

Detect Limit:

0.000 ppm0.000 ppm0.000 ppm


Mean (/*)Std Deviation (a)



5.13 ppm2.10 ppm5.001.004.50



Oct 06Apr 01Oct 09

123

111

4.004.0011.00

-0.54 .. -1.54-0.54 -1.542.80 1.80

0.000.001.80

1996 SECOND SEMIANNUAL SAMPLING › work › 05 › 155846.pdfAqua Tech Environmental Laboratories,...

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Transcript of 1996 SECOND SEMIANNUAL SAMPLING › work › 05 › 155846.pdfAqua Tech Environmental Laboratories,...