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raising standards worldwide NO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAW BSI Standards Publication BS EN ISO 13123:2011 Metallic and other inorganic coatings — Test method of cyclic heating for thermal- barrier coatings under temperature gradient (ISO 13123:2011) This is a preview of "BS EN ISO 13123:2011". Click here to purchase the full version from the ANSI store.

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raising standards worldwide™

NO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAW

BSI Standards Publication

BS EN ISO 13123:2011

Metallic and other inorganiccoatings — Test method ofcyclic heating for thermal-barrier coatings undertemperature gradient (ISO13123:2011)

This is a preview of "BS EN ISO 13123:2011". Click here to purchase the full version from the ANSI store.

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BS EN ISO 13123:2011 BRITISH STANDARD

National foreword

This British Standard is the UK implementation of EN ISO13123:2011.

The UK participation in its preparation was entrusted to TechnicalCommittee STI/40, Thermally sprayed inorganic finishes.

A list of organizations represented on this committee can beobtained on request to its secretary.

This publication does not purport to include all the necessaryprovisions of a contract. Users are responsible for its correctapplication.

© The British Standards Institution 2012

ISBN 978 0 580 67283 5

ICS 25.220.20

Compliance with a British Standard cannot confer immunity fromlegal obligations.

This British Standard was published under the authority of theStandards Policy and Strategy Committee on 31 January 2012.

Amendments issued since publication

Date Text affected

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EUROPEAN STANDARD

NORME EUROPÉENNE

EUROPÄISCHE NORM

EN ISO 13123

December 2011

ICS 25.220.20

English Version

Metallic and other inorganic coatings - Test method of cyclic heating for thermal-barrier coatings under temperature gradient

(ISO 13123:2011)

Revêtements métalliques et autres revêtements inorganiques - Méthode d'essai de cyclage thermique de

systèmes barrière thermique sous gradient de température (ISO 13123:2011)

Metallische und andere anorganische Überzüge - Prüfverfahren für Wärmedämmschichten unter

Temperaturwechselbeanspruchung bei gleichzeitigem Temperaturgradienten (ISO 13123:2011)

This European Standard was approved by CEN on 14 December 2011. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.

EUROPEAN COMMITTEE FOR STANDARDIZATION C O M I T É E U R O P É E N D E N O R M A LI S A T I O N EUR OP ÄIS C HES KOM ITEE FÜR NOR M UNG

Management Centre: Avenue Marnix 17, B-1000 Brussels

© 2011 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members.

Ref. No. EN ISO 13123:2011: E

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BS EN ISO 13123:2011EN ISO 13123:2011 (E)

3

Foreword

This document (EN ISO 13123:2011) has been prepared by Technical Committee ISO/TC 107 "Metallic and other inorganic coatings" in collaboration with Technical Committee CEN/TC 240 “Thermal spraying and thermally sprayed coatings” the secretariat of which is held by DIN.

This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by June 2012, and conflicting national standards shall be withdrawn at the latest by June 2012.

Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent rights.

According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom.

Endorsement notice

The text of ISO 13123:2011 has been approved by CEN as a EN ISO 13123:2011 without any modification.

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BS EN ISO 13123:2011ISO 13123:2011(E)

© ISO 2011 – All rights reserved iii

Contents Page

Foreword ............................................................................................................................................................ iv 

Introduction ......................................................................................................................................................... v 

1  Scope ...................................................................................................................................................... 1 

2  Normative references ............................................................................................................................ 1 

3  Terms and definitions ........................................................................................................................... 1 

4  Principle ................................................................................................................................................. 2 

5  Test piece ............................................................................................................................................... 2 

6  Test method ........................................................................................................................................... 3 6.1  Test equipment ...................................................................................................................................... 3 6.1.1  General ................................................................................................................................................... 3 6.1.2  Test block ............................................................................................................................................... 5 6.1.3  Heating unit ............................................................................................................................................ 6 6.1.4  Cooling unit ............................................................................................................................................ 6 6.1.5  Controller ............................................................................................................................................... 6 6.1.6  Measuring instruments and sensor ..................................................................................................... 6 6.1.7  Chamber ................................................................................................................................................. 7 6.2  Testing .................................................................................................................................................... 7 6.2.1  General ................................................................................................................................................... 7 6.2.2  Procedure ............................................................................................................................................... 7 6.3  Calculation ............................................................................................................................................. 8 6.4  Evaluation .............................................................................................................................................. 9 6.4.1  General ................................................................................................................................................... 9 6.4.2  Evaluating the thermal-barrier performance ...................................................................................... 9 6.4.3  Cyclic heat resistance ......................................................................................................................... 10 

7  Test report ............................................................................................................................................ 10 

Annex A (informative) Calculation of temperature at the bottom side of the top coat .............................. 13 

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BS EN ISO 13123:2011ISO 13123:2011(E)

iv © ISO 2011 – All rights reserved

Foreword

ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.

International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2.

The main task of technical committees is to prepare International Standards. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote.

Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights.

ISO 13123 was prepared by Technical Committee ISO/TC 107, Metallic and other inorganic coatings.

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BS EN ISO 13123:2011ISO 13123:2011(E)

© ISO 2011 – All rights reserved v

Introduction

Thermal-barrier coatings (TBCs) are refractory coatings which provide thermal insulation for turbine blades and vanes, as well as for combustion chamber liners in power generation, aviation gas turbines and rocket combustors. They allow operation at substantially higher surface temperatures than is possible with bare metal, and thus TBCs have been used to extend the life of components that suffer from severe heat load cyclically during operation.

Conventional isothermal test methods are not suitable for evaluating the TBC under high heat load with a large temperature-gradient condition. Standardization of a cyclic heating test method for determination of their thermal-barrier performance and cyclic heat resistance under a temperature gradient field is required.

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BS EN ISO 13123:2011

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BS EN ISO 13123:2011

INTERNATIONAL STANDARD ISO 13123:2011(E)

© ISO 2011 – All rights reserved 1

Metallic and other inorganic coatings — Test method of cyclic heating for thermal-barrier coatings under temperature gradient

1 Scope

This International Standard applies to the test method of cyclic heating to evaluate the thermal-barrier performance and cyclic heat resistance of the thermal-barrier coatings provided for high-temperature components, such as burners, rotor and stator blades, etc. of power-generation gas turbines used in thermal power plants, aircraft engines and rocket engines.

2 Normative references

The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.

ISO 1463, Metallic and oxide coatings — Measurement of coating thickness — Microscopical method

ISO 2063, Thermal spraying — Metallic and other inorganic coatings — Zinc, aluminium and their alloys

ISO 2178, Non-magnetic coatings on magnetic substrates — Measurement of coating thickness — Magnetic method

ISO 14917, Thermal spraying — Terminology, classification

ISO 80000-1, Qualities and units — Part 1: General

IEC 60584-1:1995, Thermocouples — Part 1: Reference tables

IEC 60584-2:1982, Thermocouples — Part 2: Tolerances

IEC 60584-3:2007, Thermocouples — Part 3: Extension and compensating cables —Tolerances and identification system

3 Terms and definitions

For the purposes of this document, the terms and definitions given in ISO 2063, ISO 14917 and the following apply.

3.1 temperature gradient temperature gradient caused by heating and cooling of both material surfaces of a test piece with thermal-barrier coatings

3.2 cyclic-heating testing testing in which a temperature gradient is applied cyclically to the test piece with a thermal-barrier coating

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