1 2 3 4 5 ANALYTICAL REPORT 6 · 2017. 1. 12. · 2-Methylnaphthalene 1.5 0.037 0.0068 mg/Kg 1...
Transcript of 1 2 3 4 5 ANALYTICAL REPORT 6 · 2017. 1. 12. · 2-Methylnaphthalene 1.5 0.037 0.0068 mg/Kg 1...
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ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Chicago2417 Bond StreetUniversity Park, IL 60484Tel: (708)534-5200
TestAmerica Job ID: 500-69043-1Client Project/Site: 3450 E 2056th Wedron IL
For:CDM Smith, Inc.125 South Wacker DriveSuite 600Chicago, Illinois 60606
Attn: Chris Albrecht
Authorized for release by:1/8/2014 5:02:42 PMEric Lang, Manager of Project Management(708)[email protected]
Designee for
Bonnie Stadelmann, Senior Project Manager(708)[email protected]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accreditedparameters, exceptions are noted in this report. This report may not be reproduced except in full,and with written approval from the laboratory. For questions please contact the Project Managerat the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: CDM Smith, Inc.Project/Site: 3450 E 2056th Wedron IL
TestAmerica Job ID: 500-69043-1
Page 2 of 152TestAmerica Chicago
1/8/2014
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 90QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 91Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 98QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 101Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 138Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 147Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 148Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 152
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Case NarrativeClient: CDM Smith, Inc. TestAmerica Job ID: 500-69043-1
Project/Site: 3450 E 2056th Wedron IL
Job ID: 500-69043-1
Laboratory: TestAmerica Chicago
Narrative
Job Narrative
500-69043-1
Comments
No additional comments.
Receipt
The samples were received on 12/20/2013 5:15 PM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperatures of the 2 coolers at receipt time were 2.6º C and 2.9º C.
GC/MS VOA
Method(s) 8260B: The following samples were diluted to bring the concentration of target analytes within the calibration range:
GP-01B-131219 (500-69043-2), GP-02B-131219 (500-69043-4), GP-03B-131219 (500-69043-6), GP-05B-131219 (500-69043-8),
GP-11B-131220 (500-69043-20), GP-11B-131220D (500-69043-21). Elevated reporting limits (RLs) are provided.
Method(s) 8260B: The following samples were diluted due to the abundance of non-target analytes: GP-04B-131220 (500-69043-27),
GP-06B-131219 (500-69043-12), GP-06B-131219D (500-69043-13), GP-07A-131220 (500-69043-23), GP-07B-131220 (500-69043-24),
GP-07B-131220D (500-69043-25), GP-08B-131219 (500-69043-10). Elevated reporting limits (RLs) are provided.
Method(s) 8260B: The following samples submitted for volatiles analysis was received with insufficient preservation (pH >2): Trip Blank
121913 (500-69043-14), Trip Blank 122013 (500-69043-22).
Method(s) 8260B: Surrogate recovery for the following samples were outside control limits: GP-06B-131219 (500-69043-12),
GP-08B-131219 (500-69043-10). Evidence of matrix interference is present; therefore, re-analysis was not performed.
Method(s) 8260B: Surrogate recovery for the following sample was outside control limits: GP-01B-131219 (500-69043-2), GP-02B-131219
(500-69043-4), GP-03B-131219 (500-69043-6), GP-05B-131219 (500-69043-8), GP-11B-131220 (500-69043-20). Evidence of matrix
interference is present. Re-analysis was performed at a dilution for target compounds, with all surrogates meeting QC limits.
Method(s) 8260B: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for batches 218334 and 218482 were outside control
limits. Sample matrix interference is suspected because the associated laboratory control samples (LCS) recovery were within
acceptance limits.
Method(s) 8260B: The %RPD of the matrix spike (MS) and matrix spike duplicate (MSD) samples for preparation batches 218455 and
218482 recovered outside control limits.
No other analytical or quality issues were noted.
GC/MS Semi VOA
Method(s) 8270D: The following samples were diluted due to the abundance of target and non-target analytes: GP-02B-131219
(500-69043-4), GP-05B-131219 (500-69043-8). Elevated reporting limits (RLs) are provided.
Method(s) 8270D: 500-69043-4 had 2-Fluorobiphenyl at 122% (25%-119%). All other surrogate recoveries were within limits. No further
action was required.GP-02B-131219 (500-69043-4)
Method(s) 8270D: Two matrix spike and one matrix spike duplicate (MS/MSD) recoveries for batch 218462 were outside control limits.
There were 2 RPD's > 30%. Sample matrix interference is suspected because the associated laboratory control sample (LCS) recovery
was within acceptance limits.GP-04A-131220 (500-69043-26 MS), GP-04A-131220 (500-69043-26 MSD)
Method(s) 8270D: Two matrix spike / matrix spike duplicate (MS/MSD) recoveries for batch 218463 were outside control limits. Sample
matrix interference is suspected because the associated laboratory control sample (LCS) recovery was within acceptance
limits.GP-06A-131219 (500-69043-11 MS), GP-06A-131219 (500-69043-11 MSD)
No other analytical or quality issues were noted.
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Case NarrativeClient: CDM Smith, Inc. TestAmerica Job ID: 500-69043-1
Project/Site: 3450 E 2056th Wedron IL
Job ID: 500-69043-1 (Continued)
Laboratory: TestAmerica Chicago (Continued)
GC VOA
Method(s) 8260B: The laboratory control sample (LCS) for batch 218642 recovered outside control limits for the following analytes:
1,1,1-Trichloroethane. These analytes were biased high in the LCS and were not detected in the associated samples; therefore, the data
have been reported.
No other analytical or quality issues were noted.
Metals
Method(s) 6010B: The matrix spike (MS) precision for sample 500-69043-11 was outside control limits for Pb. The associated laboratory
control sample (LCS) precision met acceptance criteria, therefore the data has been reported. The %RPD for the MS/MSD was outside
control limits for Pb.
Method(s) 6010B: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for sample 500-69043-26 were outside control limits for
Pb. The associated laboratory control sample (LCS) recovery was within acceptance limits, therefore the data has been reported
No other analytical or quality issues were noted.
Organic Prep
No analytical or quality issues were noted.
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Detection SummaryTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Client Sample ID: GP-01A-131219 Lab Sample ID: 500-69043-1
☼Acetone
RL
0.0046 mg/Kg
MDL
0.0020
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10.0049 8260B
☼Lead 0.48 mg/Kg0.14 Total/NA16.2 B 6010B
Client Sample ID: GP-01B-131219 Lab Sample ID: 500-69043-2
☼Toluene
RL
0.14 mg/Kg
MDL
0.063
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA5004.6 8260B
☼Ethylbenzene - DL 1.4 mg/Kg0.69 Total/NA5000220 8260B
☼Xylenes, Total - DL 2.8 mg/Kg0.38 Total/NA5000890 8260B
☼Acenaphthene 0.037 mg/Kg0.0067 Total/NA10.012 J 8270D
☼Benzo[a]anthracene 0.037 mg/Kg0.0050 Total/NA10.0089 J 8270D
☼Benzo[a]pyrene 0.037 mg/Kg0.0072 Total/NA10.0090 J 8270D
☼2,4-Dimethylphenol 0.37 mg/Kg0.14 Total/NA10.19 J 8270D
☼Fluoranthene 0.037 mg/Kg0.0069 Total/NA10.021 J 8270D
☼Fluorene 0.037 mg/Kg0.0052 Total/NA10.038 8270D
☼2-Methylnaphthalene 0.037 mg/Kg0.0068 Total/NA11.5 8270D
☼Naphthalene 0.037 mg/Kg0.0057 Total/NA10.93 8270D
☼Phenanthrene 0.037 mg/Kg0.0052 Total/NA10.10 8270D
☼Pyrene 0.037 mg/Kg0.0074 Total/NA10.034 J 8270D
☼Lead 0.51 mg/Kg0.15 Total/NA114 B 6010B
Client Sample ID: GP-02A-131219 Lab Sample ID: 500-69043-3
☼Acetone
RL
0.0045 mg/Kg
MDL
0.0019
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10.021 8260B
☼Lead 0.49 mg/Kg0.15 Total/NA13.6 B 6010B
Client Sample ID: GP-02B-131219 Lab Sample ID: 500-69043-4
☼Ethylbenzene
RL
1.3 mg/Kg
MDL
0.64
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA5000440 8260B
☼Toluene 1.3 mg/Kg0.58 Total/NA50006.1 8260B
☼Xylenes, Total - DL 25 mg/Kg3.5 Total/NA500001700 8260B
☼Fluoranthene 0.17 mg/Kg0.032 Total/NA50.063 J 8270D
☼Fluorene 0.17 mg/Kg0.025 Total/NA50.12 J 8270D
☼2-Methylnaphthalene 0.17 mg/Kg0.032 Total/NA55.5 8270D
☼Naphthalene 0.17 mg/Kg0.027 Total/NA55.3 8270D
☼Phenanthrene 0.17 mg/Kg0.024 Total/NA50.24 8270D
☼Pyrene 0.17 mg/Kg0.035 Total/NA50.10 J 8270D
☼Lead 0.52 mg/Kg0.15 Total/NA17.4 B 6010B
Client Sample ID: GP-03A-131219 Lab Sample ID: 500-69043-5
☼Acetone
RL
0.0048 mg/Kg
MDL
0.0021
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10.011 8260B
☼Lead 0.56 mg/Kg0.17 Total/NA14.1 B 6010B
Client Sample ID: GP-03B-131219 Lab Sample ID: 500-69043-6
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
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Detection SummaryTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Client Sample ID: GP-03B-131219 (Continued) Lab Sample ID: 500-69043-6
☼Toluene
RL
0.028 mg/Kg
MDL
0.013
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1001.8 8260B
☼Ethylbenzene - DL 0.28 mg/Kg0.14 Total/NA100079 8260B
☼Xylenes, Total - DL 0.56 mg/Kg0.076 Total/NA1000210 8260B
☼2,4-Dimethylphenol 0.37 mg/Kg0.14 Total/NA10.40 8270D
☼Fluoranthene 0.037 mg/Kg0.0069 Total/NA10.0090 J 8270D
☼Fluorene 0.037 mg/Kg0.0052 Total/NA10.020 J 8270D
☼2-Methylnaphthalene 0.037 mg/Kg0.0068 Total/NA11.8 8270D
☼Naphthalene 0.037 mg/Kg0.0057 Total/NA11.6 8270D
☼Phenanthrene 0.037 mg/Kg0.0052 Total/NA10.024 J 8270D
☼Lead 0.51 mg/Kg0.15 Total/NA16.2 B 6010B
Client Sample ID: GP-05A-131219 Lab Sample ID: 500-69043-7
☼Acetone
RL
0.0048 mg/Kg
MDL
0.0021
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10.022 8260B
☼Methyl Ethyl Ketone 0.0048 mg/Kg0.0017 Total/NA10.0054 8260B
☼Lead 0.46 mg/Kg0.14 Total/NA13.3 B 6010B
Client Sample ID: GP-05B-131219 Lab Sample ID: 500-69043-8
☼Ethylbenzene
RL
0.012 mg/Kg
MDL
0.0059
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA505.8 8260B
☼Toluene 0.012 mg/Kg0.0054 Total/NA500.13 8260B
☼Xylenes, Total - DL 0.23 mg/Kg0.032 Total/NA50018 8260B
☼Di-n-octyl phthalate 0.91 mg/Kg0.30 Total/NA50.63 J 8270D
☼Fluorene 0.18 mg/Kg0.025 Total/NA50.15 J 8270D
☼2-Methylnaphthalene 0.18 mg/Kg0.033 Total/NA55.8 8270D
☼Naphthalene 0.18 mg/Kg0.028 Total/NA53.5 8270D
☼Phenanthrene 0.18 mg/Kg0.025 Total/NA50.19 8270D
☼Pyrene 0.18 mg/Kg0.036 Total/NA50.052 J 8270D
☼Lead 0.51 mg/Kg0.15 Total/NA18.9 B 6010B
Client Sample ID: GP-08A-131219 Lab Sample ID: 500-69043-9
☼Acetone
RL
0.0047 mg/Kg
MDL
0.0020
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10.0069 8260B
☼Lead 0.47 mg/Kg0.14 Total/NA12.5 B 6010B
Client Sample ID: GP-08B-131219 Lab Sample ID: 500-69043-10
☼Ethylbenzene
RL
0.012 mg/Kg
MDL
0.0059
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA502.4 8260B
☼Toluene 0.012 mg/Kg0.0054 Total/NA500.027 8260B
☼Xylenes, Total 0.024 mg/Kg0.0032 Total/NA504.1 8260B
☼2-Methylnaphthalene 0.035 mg/Kg0.0064 Total/NA10.29 8270D
☼Naphthalene 0.035 mg/Kg0.0054 Total/NA10.20 8270D
☼Lead 0.47 mg/Kg0.14 Total/NA15.8 B 6010B
Client Sample ID: GP-06A-131219 Lab Sample ID: 500-69043-11
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
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Detection SummaryTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Client Sample ID: GP-06A-131219 (Continued) Lab Sample ID: 500-69043-11
☼Acetone
RL
0.0053 mg/Kg
MDL
0.0023
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10.028 8260B
☼Methyl Ethyl Ketone 0.0053 mg/Kg0.0019 Total/NA10.0072 8260B
☼Toluene 0.0053 mg/Kg0.00075 Total/NA10.0030 J 8260B
☼Lead 0.46 mg/Kg0.14 Total/NA12.6 B 6010B
Client Sample ID: GP-06B-131219 Lab Sample ID: 500-69043-12
☼Ethylbenzene
RL
0.13 mg/Kg
MDL
0.067
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA5000.90 8260B
☼Toluene 0.13 mg/Kg0.061 Total/NA5000.17 8260B
☼Xylenes, Total 0.27 mg/Kg0.037 Total/NA5001.5 8260B
☼Acenaphthene 0.036 mg/Kg0.0065 Total/NA10.032 J 8270D
☼Benzo[a]anthracene 0.036 mg/Kg0.0049 Total/NA10.028 J 8270D
☼Benzo[a]pyrene 0.036 mg/Kg0.0070 Total/NA10.015 J 8270D
☼Benzo[b]fluoranthene 0.036 mg/Kg0.0078 Total/NA10.021 J 8270D
☼Benzo[g,h,i]perylene 0.036 mg/Kg0.012 Total/NA10.013 J 8270D
☼Chrysene 0.036 mg/Kg0.0099 Total/NA10.018 J 8270D
☼Fluoranthene 0.036 mg/Kg0.0067 Total/NA10.12 8270D
☼Fluorene 0.036 mg/Kg0.0051 Total/NA10.059 8270D
☼2-Methylnaphthalene 0.036 mg/Kg0.0067 Total/NA12.2 8270D
☼Naphthalene 0.036 mg/Kg0.0056 Total/NA10.099 8270D
☼Phenanthrene 0.036 mg/Kg0.0051 Total/NA10.19 8270D
☼Pyrene 0.036 mg/Kg0.0072 Total/NA10.088 8270D
☼Lead 0.50 mg/Kg0.15 Total/NA14.0 B 6010B
Client Sample ID: GP-06B-131219D Lab Sample ID: 500-69043-13
☼Ethylbenzene
RL
0.13 mg/Kg
MDL
0.064
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA5000.24 8260B
☼Xylenes, Total 0.25 mg/Kg0.035 Total/NA5000.44 8260B
☼Benzo[a]anthracene 0.035 mg/Kg0.0048 Total/NA10.012 J 8270D
☼Benzo[a]pyrene 0.035 mg/Kg0.0069 Total/NA10.0088 J 8270D
☼Benzo[b]fluoranthene 0.035 mg/Kg0.0077 Total/NA10.0097 J 8270D
☼Bis(2-ethylhexyl) phthalate 0.18 mg/Kg0.065 Total/NA10.26 8270D
☼Fluoranthene 0.035 mg/Kg0.0066 Total/NA10.040 8270D
☼2-Methylnaphthalene 0.035 mg/Kg0.0065 Total/NA10.51 8270D
☼Naphthalene 0.035 mg/Kg0.0055 Total/NA10.0085 J 8270D
☼Phenanthrene 0.035 mg/Kg0.0049 Total/NA10.035 8270D
☼Pyrene 0.035 mg/Kg0.0070 Total/NA10.033 J 8270D
☼Lead 0.49 mg/Kg0.15 Total/NA14.7 B 6010B
Client Sample ID: Trip Blank 121913 Lab Sample ID: 500-69043-14
No Detections.
Client Sample ID: GP-09A-131220 Lab Sample ID: 500-69043-15
☼Di-n-octyl phthalate
RL
0.18 mg/Kg
MDL
0.059
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.12 8270D
☼Lead 0.49 mg/Kg0.15 Total/NA15.1 B 6010B
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
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Detection SummaryTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Client Sample ID: GP-09B-131220 Lab Sample ID: 500-69043-16
☼Di-n-octyl phthalate
RL
0.18 mg/Kg
MDL
0.059
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.073 8270D
☼Lead 0.52 mg/Kg0.16 Total/NA13.5 B 6010B
Client Sample ID: GP-10A-131220 Lab Sample ID: 500-69043-17
☼Acetone
RL
0.0051 mg/Kg
MDL
0.0022
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10.0076 8260B
☼Benzo[a]anthracene 0.039 mg/Kg0.0053 Total/NA10.013 J 8270D
☼Benzo[a]pyrene 0.039 mg/Kg0.0076 Total/NA10.012 J 8270D
☼Benzo[b]fluoranthene 0.039 mg/Kg0.0085 Total/NA10.019 J 8270D
☼Chrysene 0.039 mg/Kg0.011 Total/NA10.018 J 8270D
☼Fluoranthene 0.039 mg/Kg0.0073 Total/NA10.027 J 8270D
☼2-Methylnaphthalene 0.039 mg/Kg0.0072 Total/NA10.035 J 8270D
☼Phenanthrene 0.039 mg/Kg0.0055 Total/NA10.032 J 8270D
☼Pyrene 0.039 mg/Kg0.0078 Total/NA10.023 J 8270D
☼Lead 0.60 mg/Kg0.18 Total/NA118 B 6010B
Client Sample ID: GP-10B-131220 Lab Sample ID: 500-69043-18
☼Acetone
RL
0.0057 mg/Kg
MDL
0.0025
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10.019 8260B
☼Methyl Ethyl Ketone 0.0057 mg/Kg0.0021 Total/NA10.0056 J 8260B
☼Toluene 0.0057 mg/Kg0.00080 Total/NA10.0037 J 8260B
☼Bis(2-ethylhexyl) phthalate 0.17 mg/Kg0.062 Total/NA10.063 J 8270D
☼Lead 0.53 mg/Kg0.16 Total/NA12.0 B 6010B
Client Sample ID: GP-11A-131220 Lab Sample ID: 500-69043-19
☼Acetone
RL
0.0052 mg/Kg
MDL
0.0022
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10.012 8260B
☼Toluene 0.0052 mg/Kg0.00073 Total/NA10.0033 J 8260B
☼Lead 0.48 mg/Kg0.14 Total/NA12.3 B 6010B
Client Sample ID: GP-11B-131220 Lab Sample ID: 500-69043-20
☼Ethylbenzene - DL
RL
1.4 mg/Kg
MDL
0.72
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA5000160 8260B
☼Toluene - DL 1.4 mg/Kg0.66 Total/NA500039 8260B
☼Xylenes, Total - DL 2.9 mg/Kg0.39 Total/NA5000940 8260B
☼Naphthalene 0.036 mg/Kg0.0056 Total/NA12.2 8270D
☼Phenanthrene 0.036 mg/Kg0.0051 Total/NA10.041 8270D
☼Pyrene 0.036 mg/Kg0.0073 Total/NA10.0081 J 8270D
☼2-Methylnaphthalene - DL 0.18 mg/Kg0.034 Total/NA54.1 8270D
☼Lead 0.49 mg/Kg0.14 Total/NA14.0 B 6010B
Client Sample ID: GP-11B-131220D Lab Sample ID: 500-69043-21
☼Ethylbenzene
RL
0.14 mg/Kg
MDL
0.072
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA50065 8260B
☼Toluene 0.14 mg/Kg0.066 Total/NA5004.2 8260B
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
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Detection SummaryTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Client Sample ID: GP-11B-131220D (Continued) Lab Sample ID: 500-69043-21
☼Xylenes, Total - DL
RL
2.9 mg/Kg
MDL
0.39
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA5000310 8260B
☼Acenaphthene 0.036 mg/Kg0.0064 Total/NA10.026 J 8270D
☼Fluoranthene 0.036 mg/Kg0.0066 Total/NA10.019 J 8270D
☼Fluorene 0.036 mg/Kg0.0050 Total/NA10.049 8270D
☼Phenanthrene 0.036 mg/Kg0.0050 Total/NA10.23 8270D
☼Pyrene 0.036 mg/Kg0.0071 Total/NA10.025 J 8270D
☼2-Methylnaphthalene - DL 0.71 mg/Kg0.13 Total/NA2020 8270D
☼Naphthalene - DL 0.71 mg/Kg0.11 Total/NA2016 8270D
☼Lead 0.51 mg/Kg0.15 Total/NA17.6 B 6010B
Client Sample ID: Trip Blank 122013 Lab Sample ID: 500-69043-22
No Detections.
Client Sample ID: GP-07A-131220 Lab Sample ID: 500-69043-23
☼Fluoranthene
RL
0.039 mg/Kg
MDL
0.0073
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.029 8270D
☼2-Methylnaphthalene 0.039 mg/Kg0.0073 Total/NA10.48 8270D
☼Naphthalene 0.039 mg/Kg0.0061 Total/NA10.31 8270D
☼Phenanthrene 0.039 mg/Kg0.0055 Total/NA10.074 8270D
☼Pyrene 0.039 mg/Kg0.0079 Total/NA10.018 J 8270D
☼Lead 0.58 mg/Kg0.17 Total/NA110 B 6010B
Client Sample ID: GP-07B-131220 Lab Sample ID: 500-69043-24
☼Ethylbenzene
RL
1.5 mg/Kg
MDL
0.76
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA50008.4 8260B
☼Xylenes, Total 3.0 mg/Kg0.41 Total/NA50009.2 8260B
☼Fluoranthene 0.039 mg/Kg0.0073 Total/NA10.013 J 8270D
☼2-Methylnaphthalene 0.039 mg/Kg0.0072 Total/NA11.7 8270D
☼Naphthalene 0.039 mg/Kg0.0060 Total/NA10.55 8270D
☼Phenanthrene 0.039 mg/Kg0.0055 Total/NA10.045 8270D
☼Pyrene 0.039 mg/Kg0.0078 Total/NA10.0091 J 8270D
☼Lead 0.62 mg/Kg0.18 Total/NA111 B 6010B
Client Sample ID: GP-07B-131220D Lab Sample ID: 500-69043-25
☼Ethylbenzene
RL
0.012 mg/Kg
MDL
0.0062
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA503.7 8260B
☼Toluene 0.012 mg/Kg0.0057 Total/NA500.016 8260B
☼Xylenes, Total 0.025 mg/Kg0.0034 Total/NA505.3 8260B
☼Fluoranthene 0.036 mg/Kg0.0066 Total/NA10.019 J 8270D
☼2-Methylnaphthalene 0.036 mg/Kg0.0066 Total/NA11.1 8270D
☼Naphthalene 0.036 mg/Kg0.0055 Total/NA10.57 8270D
☼Phenanthrene 0.036 mg/Kg0.0050 Total/NA10.040 8270D
☼Pyrene 0.036 mg/Kg0.0071 Total/NA10.011 J 8270D
☼Lead 0.55 mg/Kg0.17 Total/NA18.5 B 6010B
Client Sample ID: GP-04A-131220 Lab Sample ID: 500-69043-26
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
Page 9 of 152 1/8/2014
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Detection SummaryTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Client Sample ID: GP-04A-131220 (Continued) Lab Sample ID: 500-69043-26
☼Ethylbenzene
RL
0.0051 mg/Kg
MDL
0.0010
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10.028 8260B
☼Toluene 0.0051 mg/Kg0.00071 Total/NA10.0043 J 8260B
☼Xylenes, Total 0.010 mg/Kg0.00046 Total/NA10.067 8260B
☼Phenanthrene 0.037 mg/Kg0.0052 Total/NA10.0082 J 8270D
☼Lead 0.49 mg/Kg0.15 Total/NA17.9 B 6010B
Client Sample ID: GP-04B-131220 Lab Sample ID: 500-69043-27
☼Ethylbenzene
RL
1.4 mg/Kg
MDL
0.72
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA500051 8260B
☼Xylenes, Total 2.8 mg/Kg0.39 Total/NA5000130 8260B
☼Acenaphthene 0.035 mg/Kg0.0064 Total/NA10.061 8270D
☼Anthracene 0.035 mg/Kg0.0059 Total/NA10.050 8270D
☼Benzo[a]anthracene 0.035 mg/Kg0.0048 Total/NA10.014 J 8270D
☼Benzo[a]pyrene 0.035 mg/Kg0.0069 Total/NA10.0070 J 8270D
☼Benzo[b]fluoranthene 0.035 mg/Kg0.0076 Total/NA10.0088 J 8270D
☼Benzo[g,h,i]perylene 0.035 mg/Kg0.011 Total/NA10.012 J 8270D
☼Chrysene 0.035 mg/Kg0.0097 Total/NA10.0097 J 8270D
☼Fluoranthene 0.035 mg/Kg0.0066 Total/NA10.053 8270D
☼Fluorene 0.035 mg/Kg0.0050 Total/NA10.10 8270D
☼Naphthalene 0.035 mg/Kg0.0055 Total/NA11.6 8270D
☼Phenanthrene 0.035 mg/Kg0.0049 Total/NA10.25 8270D
☼Pyrene 0.035 mg/Kg0.0070 Total/NA10.068 8270D
☼2-Methylnaphthalene - DL 0.18 mg/Kg0.033 Total/NA55.2 8270D
☼Lead 0.56 mg/Kg0.17 Total/NA18.1 B 6010B
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
Page 10 of 152 1/8/2014
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Method SummaryTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Method Method Description LaboratoryProtocol
SW8468260B Volatile Organic Compounds (GC/MS) TAL CHI
SW8468270D Semivolatile Organic Compounds (GC/MS) TAL CHI
SW8466010B Metals (ICP) TAL CHI
EPAMoisture Percent Moisture TAL CHI
Protocol References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534-5200
TestAmerica Chicago
Page 11 of 152 1/8/2014
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Sample SummaryTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
500-69043-1 GP-01A-131219 Solid 12/19/13 09:30 12/20/13 17:15
500-69043-2 GP-01B-131219 Solid 12/19/13 09:45 12/20/13 17:15
500-69043-3 GP-02A-131219 Solid 12/19/13 10:30 12/20/13 17:15
500-69043-4 GP-02B-131219 Solid 12/19/13 10:45 12/20/13 17:15
500-69043-5 GP-03A-131219 Solid 12/19/13 11:30 12/20/13 17:15
500-69043-6 GP-03B-131219 Solid 12/19/13 11:45 12/20/13 17:15
500-69043-7 GP-05A-131219 Solid 12/19/13 13:30 12/20/13 17:15
500-69043-8 GP-05B-131219 Solid 12/19/13 13:45 12/20/13 17:15
500-69043-9 GP-08A-131219 Solid 12/19/13 15:45 12/20/13 17:15
500-69043-10 GP-08B-131219 Solid 12/19/13 16:00 12/20/13 17:15
500-69043-11 GP-06A-131219 Solid 12/19/13 14:45 12/20/13 17:15
500-69043-12 GP-06B-131219 Solid 12/19/13 14:50 12/20/13 17:15
500-69043-13 GP-06B-131219D Solid 12/19/13 14:55 12/20/13 17:15
500-69043-14 Trip Blank 121913 Water 12/19/13 00:00 12/20/13 17:15
500-69043-15 GP-09A-131220 Solid 12/20/13 08:45 12/20/13 17:15
500-69043-16 GP-09B-131220 Solid 12/20/13 08:55 12/20/13 17:15
500-69043-17 GP-10A-131220 Solid 12/20/13 09:45 12/20/13 17:15
500-69043-18 GP-10B-131220 Solid 12/20/13 10:00 12/20/13 17:15
500-69043-19 GP-11A-131220 Solid 12/20/13 11:20 12/20/13 17:15
500-69043-20 GP-11B-131220 Solid 12/20/13 11:30 12/20/13 17:15
500-69043-21 GP-11B-131220D Solid 12/20/13 11:45 12/20/13 17:15
500-69043-22 Trip Blank 122013 Water 12/20/13 00:00 12/20/13 17:15
500-69043-23 GP-07A-131220 Solid 12/20/13 13:30 12/20/13 17:15
500-69043-24 GP-07B-131220 Solid 12/20/13 13:45 12/20/13 17:15
500-69043-25 GP-07B-131220D Solid 12/20/13 13:55 12/20/13 17:15
500-69043-26 GP-04A-131220 Solid 12/20/13 14:25 12/20/13 17:15
500-69043-27 GP-04B-131220 Solid 12/20/13 14:35 12/20/13 17:15
TestAmerica Chicago
Page 12 of 152 1/8/2014
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Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-1Client Sample ID: GP-01A-131219Matrix: SolidDate Collected: 12/19/13 09:30
Percent Solids: 91.3Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone 0.0049 0.0046 0.0020 mg/Kg ☼ 12/21/13 06:55 12/31/13 17:53 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0046 0.00063 mg/Kg 12/21/13 06:55 12/31/13 17:53 1☼Benzene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-1Client Sample ID: GP-01A-131219Matrix: SolidDate Collected: 12/19/13 09:30
Percent Solids: 91.3Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
Benzo[b]fluoranthene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-1Client Sample ID: GP-01A-131219Matrix: SolidDate Collected: 12/19/13 09:30
Percent Solids: 91.3Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
N-Nitrosodi-n-propylamine
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-2Client Sample ID: GP-01B-131219Matrix: SolidDate Collected: 12/19/13 09:45
Percent Solids: 88.9Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-2Client Sample ID: GP-01B-131219Matrix: SolidDate Collected: 12/19/13 09:45
Percent Solids: 88.9Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS) - DL (Continued)
Toluene-d8 (Surr) 102 75 - 120 12/19/13 09:45 01/01/14 19:54 5000
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8270D - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene 0.012 J 0.037 0.0067 mg/Kg ☼ 01/02/14 07:08 01/03/14 14:02 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.037 0.0049 mg/Kg 01/02/14 07:08 01/03/14 14:02 1☼Acenaphthylene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-2Client Sample ID: GP-01B-131219Matrix: SolidDate Collected: 12/19/13 09:45
Percent Solids: 88.9Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
2-Methylphenol
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-3Client Sample ID: GP-02A-131219Matrix: SolidDate Collected: 12/19/13 10:30
Percent Solids: 91.5Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone 0.021 0.0045 0.0019 mg/Kg ☼ 12/21/13 06:55 12/31/13 18:16 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0045 0.00061 mg/Kg 12/21/13 06:55 12/31/13 18:16 1☼Benzene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-3Client Sample ID: GP-02A-131219Matrix: SolidDate Collected: 12/19/13 10:30
Percent Solids: 91.5Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
Benzo[b]fluoranthene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-3Client Sample ID: GP-02A-131219Matrix: SolidDate Collected: 12/19/13 10:30
Percent Solids: 91.5Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
N-Nitrosodi-n-propylamine
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-4Client Sample ID: GP-02B-131219Matrix: SolidDate Collected: 12/19/13 10:45
Percent Solids: 91.4Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-4Client Sample ID: GP-02B-131219Matrix: SolidDate Collected: 12/19/13 10:45
Percent Solids: 91.4Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS) - DL (Continued)
Toluene-d8 (Surr) 104 75 - 120 12/19/13 10:45 01/01/14 20:49 50000
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8270D - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-4Client Sample ID: GP-02B-131219Matrix: SolidDate Collected: 12/19/13 10:45
Percent Solids: 91.4Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
2-Methylphenol
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-5Client Sample ID: GP-03A-131219Matrix: SolidDate Collected: 12/19/13 11:30
Percent Solids: 88.6Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone 0.011 0.0048 0.0021 mg/Kg ☼ 12/21/13 06:55 12/31/13 18:38 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0048 0.00066 mg/Kg 12/21/13 06:55 12/31/13 18:38 1☼Benzene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-5Client Sample ID: GP-03A-131219Matrix: SolidDate Collected: 12/19/13 11:30
Percent Solids: 88.6Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
Benzo[b]fluoranthene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-5Client Sample ID: GP-03A-131219Matrix: SolidDate Collected: 12/19/13 11:30
Percent Solids: 88.6Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
N-Nitrosodi-n-propylamine
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-6Client Sample ID: GP-03B-131219Matrix: SolidDate Collected: 12/19/13 11:45
Percent Solids: 86.6Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-6Client Sample ID: GP-03B-131219Matrix: SolidDate Collected: 12/19/13 11:45
Percent Solids: 86.6Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS) - DL (Continued)
Toluene-d8 (Surr) 104 75 - 120 12/19/13 11:45 01/01/14 21:43 1000
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8270D - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-6Client Sample ID: GP-03B-131219Matrix: SolidDate Collected: 12/19/13 11:45
Percent Solids: 86.6Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
2-Methylphenol
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-7Client Sample ID: GP-05A-131219Matrix: SolidDate Collected: 12/19/13 13:30
Percent Solids: 92.3Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone 0.022 0.0048 0.0021 mg/Kg ☼ 12/21/13 06:55 12/31/13 19:01 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0048 0.00066 mg/Kg 12/21/13 06:55 12/31/13 19:01 1☼Benzene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-7Client Sample ID: GP-05A-131219Matrix: SolidDate Collected: 12/19/13 13:30
Percent Solids: 92.3Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
Benzo[b]fluoranthene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-7Client Sample ID: GP-05A-131219Matrix: SolidDate Collected: 12/19/13 13:30
Percent Solids: 92.3Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
N-Nitrosodi-n-propylamine
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-8Client Sample ID: GP-05B-131219Matrix: SolidDate Collected: 12/19/13 13:45
Percent Solids: 91.1Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-8Client Sample ID: GP-05B-131219Matrix: SolidDate Collected: 12/19/13 13:45
Percent Solids: 91.1Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS) - DL (Continued)
Toluene-d8 (Surr) 104 75 - 120 12/19/13 13:45 01/02/14 12:51 500
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8270D - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-8Client Sample ID: GP-05B-131219Matrix: SolidDate Collected: 12/19/13 13:45
Percent Solids: 91.1Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
2-Methylphenol
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-9Client Sample ID: GP-08A-131219Matrix: SolidDate Collected: 12/19/13 15:45
Percent Solids: 94.5Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone 0.0069 0.0047 0.0020 mg/Kg ☼ 12/21/13 06:55 12/31/13 19:24 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0047 0.00065 mg/Kg 12/21/13 06:55 12/31/13 19:24 1☼Benzene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-9Client Sample ID: GP-08A-131219Matrix: SolidDate Collected: 12/19/13 15:45
Percent Solids: 94.5Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
Benzo[b]fluoranthene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-9Client Sample ID: GP-08A-131219Matrix: SolidDate Collected: 12/19/13 15:45
Percent Solids: 94.5Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
N-Nitrosodi-n-propylamine
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-10Client Sample ID: GP-08B-131219Matrix: SolidDate Collected: 12/19/13 16:00
Percent Solids: 90.6Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-10Client Sample ID: GP-08B-131219Matrix: SolidDate Collected: 12/19/13 16:00
Percent Solids: 90.6Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
Benzo[b]fluoranthene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-10Client Sample ID: GP-08B-131219Matrix: SolidDate Collected: 12/19/13 16:00
Percent Solids: 90.6Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
N-Nitrosodi-n-propylamine
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-11Client Sample ID: GP-06A-131219Matrix: SolidDate Collected: 12/19/13 14:45
Percent Solids: 94.5Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone 0.028 0.0053 0.0023 mg/Kg ☼ 12/21/13 06:55 12/31/13 19:46 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0053 0.00073 mg/Kg 12/21/13 06:55 12/31/13 19:46 1☼Benzene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-11Client Sample ID: GP-06A-131219Matrix: SolidDate Collected: 12/19/13 14:45
Percent Solids: 94.5Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
Benzo[b]fluoranthene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-11Client Sample ID: GP-06A-131219Matrix: SolidDate Collected: 12/19/13 14:45
Percent Solids: 94.5Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
N-Nitrosodi-n-propylamine
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-12Client Sample ID: GP-06B-131219Matrix: SolidDate Collected: 12/19/13 14:50
Percent Solids: 90.8Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-12Client Sample ID: GP-06B-131219Matrix: SolidDate Collected: 12/19/13 14:50
Percent Solids: 90.8Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
Benzo[b]fluoranthene 0.021 J 0.036 0.0078 mg/Kg ☼ 01/02/14 07:08 01/03/14 19:44 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.036 0.012 mg/Kg 01/02/14 07:08 01/03/14 19:44 1☼Benzo[g,h,i]perylene 0.013 J
0.036 0.011 mg/Kg 01/02/14 07:08 01/03/14 19:44 1☼Benzo[k]fluoranthene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-12Client Sample ID: GP-06B-131219Matrix: SolidDate Collected: 12/19/13 14:50
Percent Solids: 90.8Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
N-Nitrosodi-n-propylamine
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-13Client Sample ID: GP-06B-131219DMatrix: SolidDate Collected: 12/19/13 14:55
Percent Solids: 90.3Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-13Client Sample ID: GP-06B-131219DMatrix: SolidDate Collected: 12/19/13 14:55
Percent Solids: 90.3Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
Benzo[b]fluoranthene 0.0097 J 0.035 0.0077 mg/Kg ☼ 01/02/14 07:08 01/03/14 20:03 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.035 0.011 mg/Kg 01/02/14 07:08 01/03/14 20:03 1☼Benzo[g,h,i]perylene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-13Client Sample ID: GP-06B-131219DMatrix: SolidDate Collected: 12/19/13 14:55
Percent Solids: 90.3Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
N-Nitrosodi-n-propylamine
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-14Client Sample ID: Trip Blank 121913Matrix: WaterDate Collected: 12/19/13 00:00
Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-15Client Sample ID: GP-09A-131220Matrix: SolidDate Collected: 12/20/13 08:45
Percent Solids: 90.3Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-15Client Sample ID: GP-09A-131220Matrix: SolidDate Collected: 12/20/13 08:45
Percent Solids: 90.3Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
Benzo[b]fluoranthene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-15Client Sample ID: GP-09A-131220Matrix: SolidDate Collected: 12/20/13 08:45
Percent Solids: 90.3Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
N-Nitrosodi-n-propylamine
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-16Client Sample ID: GP-09B-131220Matrix: SolidDate Collected: 12/20/13 08:55
Percent Solids: 88.8Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-16Client Sample ID: GP-09B-131220Matrix: SolidDate Collected: 12/20/13 08:55
Percent Solids: 88.8Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
Benzo[b]fluoranthene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-16Client Sample ID: GP-09B-131220Matrix: SolidDate Collected: 12/20/13 08:55
Percent Solids: 88.8Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
N-Nitrosodi-n-propylamine
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-17Client Sample ID: GP-10A-131220Matrix: SolidDate Collected: 12/20/13 09:45
Percent Solids: 80.1Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone 0.0076 0.0051 0.0022 mg/Kg ☼ 12/21/13 06:55 12/31/13 21:17 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0051 0.00070 mg/Kg 12/21/13 06:55 12/31/13 21:17 1☼Benzene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-17Client Sample ID: GP-10A-131220Matrix: SolidDate Collected: 12/20/13 09:45
Percent Solids: 80.1Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
Benzo[b]fluoranthene 0.019 J 0.039 0.0085 mg/Kg ☼ 01/02/14 07:08 01/08/14 11:55 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.039 0.013 mg/Kg 01/02/14 07:08 01/08/14 11:55 1☼Benzo[g,h,i]perylene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-17Client Sample ID: GP-10A-131220Matrix: SolidDate Collected: 12/20/13 09:45
Percent Solids: 80.1Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
N-Nitrosodi-n-propylamine
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-18Client Sample ID: GP-10B-131220Matrix: SolidDate Collected: 12/20/13 10:00
Percent Solids: 92.7Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone 0.019 0.0057 0.0025 mg/Kg ☼ 12/21/13 06:55 12/31/13 21:40 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0057 0.00078 mg/Kg 12/21/13 06:55 12/31/13 21:40 1☼Benzene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-18Client Sample ID: GP-10B-131220Matrix: SolidDate Collected: 12/20/13 10:00
Percent Solids: 92.7Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
Benzo[b]fluoranthene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-18Client Sample ID: GP-10B-131220Matrix: SolidDate Collected: 12/20/13 10:00
Percent Solids: 92.7Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
N-Nitrosodi-n-propylamine
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-19Client Sample ID: GP-11A-131220Matrix: SolidDate Collected: 12/20/13 11:20
Percent Solids: 95.1Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone 0.012 0.0052 0.0022 mg/Kg ☼ 12/21/13 06:55 01/02/14 13:16 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0052 0.00071 mg/Kg 12/21/13 06:55 01/02/14 13:16 1☼Benzene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-19Client Sample ID: GP-11A-131220Matrix: SolidDate Collected: 12/20/13 11:20
Percent Solids: 95.1Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
Benzo[b]fluoranthene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-19Client Sample ID: GP-11A-131220Matrix: SolidDate Collected: 12/20/13 11:20
Percent Solids: 95.1Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
N-Nitrosodi-n-propylamine
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-20Client Sample ID: GP-11B-131220Matrix: SolidDate Collected: 12/20/13 11:30
Percent Solids: 87.9Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-20Client Sample ID: GP-11B-131220Matrix: SolidDate Collected: 12/20/13 11:30
Percent Solids: 87.9Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS) - DL (Continued)
Toluene-d8 (Surr) 102 75 - 120 12/20/13 11:30 01/03/14 11:34 5000
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8270D - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-20Client Sample ID: GP-11B-131220Matrix: SolidDate Collected: 12/20/13 11:30
Percent Solids: 87.9Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
3 & 4 Methylphenol
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-21Client Sample ID: GP-11B-131220DMatrix: SolidDate Collected: 12/20/13 11:45
Percent Solids: 88.4Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-21Client Sample ID: GP-11B-131220DMatrix: SolidDate Collected: 12/20/13 11:45
Percent Solids: 88.4Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS) - DL (Continued)
Toluene-d8 (Surr) 105 75 - 120 12/20/13 11:45 01/03/14 12:01 5000
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8270D - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene 0.026 J 0.036 0.0064 mg/Kg ☼ 01/02/14 07:08 01/08/14 13:33 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.036 0.0047 mg/Kg 01/02/14 07:08 01/08/14 13:33 1☼Acenaphthylene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-21Client Sample ID: GP-11B-131220DMatrix: SolidDate Collected: 12/20/13 11:45
Percent Solids: 88.4Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
3 & 4 Methylphenol
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-22Client Sample ID: Trip Blank 122013Matrix: WaterDate Collected: 12/20/13 00:00
Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-23Client Sample ID: GP-07A-131220Matrix: SolidDate Collected: 12/20/13 13:30
Percent Solids: 81.0Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-23Client Sample ID: GP-07A-131220Matrix: SolidDate Collected: 12/20/13 13:30
Percent Solids: 81.0Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
Benzo[b]fluoranthene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-23Client Sample ID: GP-07A-131220Matrix: SolidDate Collected: 12/20/13 13:30
Percent Solids: 81.0Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
N-Nitrosodi-n-propylamine
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-24Client Sample ID: GP-07B-131220Matrix: SolidDate Collected: 12/20/13 13:45
Percent Solids: 80.4Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-24Client Sample ID: GP-07B-131220Matrix: SolidDate Collected: 12/20/13 13:45
Percent Solids: 80.4Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
Benzo[b]fluoranthene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-24Client Sample ID: GP-07B-131220Matrix: SolidDate Collected: 12/20/13 13:45
Percent Solids: 80.4Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
N-Nitrosodi-n-propylamine
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-25Client Sample ID: GP-07B-131220DMatrix: SolidDate Collected: 12/20/13 13:55
Percent Solids: 88.8Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-25Client Sample ID: GP-07B-131220DMatrix: SolidDate Collected: 12/20/13 13:55
Percent Solids: 88.8Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
Benzo[b]fluoranthene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-25Client Sample ID: GP-07B-131220DMatrix: SolidDate Collected: 12/20/13 13:55
Percent Solids: 88.8Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
N-Nitrosodi-n-propylamine
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-26Client Sample ID: GP-04A-131220Matrix: SolidDate Collected: 12/20/13 14:25
Percent Solids: 86.1Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-26Client Sample ID: GP-04A-131220Matrix: SolidDate Collected: 12/20/13 14:25
Percent Solids: 86.1Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
Benzo[b]fluoranthene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-26Client Sample ID: GP-04A-131220Matrix: SolidDate Collected: 12/20/13 14:25
Percent Solids: 86.1Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
N-Nitrosodi-n-propylamine
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-27Client Sample ID: GP-04B-131220Matrix: SolidDate Collected: 12/20/13 14:35
Percent Solids: 89.2Date Received: 12/20/13 17:15
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-27Client Sample ID: GP-04B-131220Matrix: SolidDate Collected: 12/20/13 14:35
Percent Solids: 89.2Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
Benzo[b]fluoranthene 0.0088 J 0.035 0.0076 mg/Kg ☼ 01/02/14 07:04 01/07/14 22:51 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.035 0.011 mg/Kg 01/02/14 07:04 01/07/14 22:51 1☼Benzo[g,h,i]perylene 0.012 J
0.035 0.010 mg/Kg 01/02/14 07:04 01/07/14 22:51 1☼Benzo[k]fluoranthene
-
Client Sample ResultsTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Lab Sample ID: 500-69043-27Client Sample ID: GP-04B-131220Matrix: SolidDate Collected: 12/20/13 14:35
Percent Solids: 89.2Date Received: 12/20/13 17:15
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
N-Nitrosodiphenylamine
-
Definitions/GlossaryTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Qualifiers
GC/MS VOA
Qualifier Description
X Surrogate is outside control limits
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
F1 MS and/or MSD Recovery exceeds the control limits
F2 MS/MSD RPD exceeds control limits
* LCS or LCSD exceeds the control limits
GC/MS Semi VOA
Qualifier Description
F1 MS and/or MSD Recovery exceeds the control limits
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
F2 MS/MSD RPD exceeds control limits
X Surrogate is outside control limits
Metals
Qualifier Description
B Compound was found in the blank and sample.
Qualifier
F1 MS and/or MSD Recovery exceeds the control limits
F2 MS/MSD RPD exceeds control limits
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤ Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Chicago
Page 90 of 152 1/8/2014
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QC Association SummaryTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
GC/MS VOA
Prep Batch: 217834
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035500-69043-1 GP-01A-131219 Total/NA
Solid 5035500-69043-3 GP-02A-131219 Total/NA
Solid 5035500-69043-5 GP-03A-131219 Total/NA
Solid 5035500-69043-7 GP-05A-131219 Total/NA
Solid 5035500-69043-9 GP-08A-131219 Total/NA
Solid 5035500-69043-11 GP-06A-131219 Total/NA
Solid 5035500-69043-11 MS GP-06A-131219 Total/NA
Solid 5035500-69043-11 MSD GP-06A-131219 Total/NA
Solid 5035500-69043-15 GP-09A-131220 Total/NA
Solid 5035500-69043-16 GP-09B-131220 Total/NA
Solid 5035500-69043-17 GP-10A-131220 Total/NA
Solid 5035500-69043-18 GP-10B-131220 Total/NA
Solid 5035500-69043-19 GP-11A-131220 Total/NA
Solid 5035500-69043-26 GP-04A-131220 Total/NA
Solid 5035500-69043-26 MS GP-04A-131220 Total/NA
Solid 5035500-69043-26 MSD GP-04A-131220 Total/NA
Prep Batch: 218172
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035500-69043-2 - DL GP-01B-131219 Total/NA
Solid 5035500-69043-2 GP-01B-131219 Total/NA
Solid 5035500-69043-4 GP-02B-131219 Total/NA
Solid 5035500-69043-4 - DL GP-02B-131219 Total/NA
Solid 5035500-69043-6 - DL GP-03B-131219 Total/NA
Solid 5035500-69043-6 GP-03B-131219 Total/NA
Solid 5035500-69043-8 - DL GP-05B-131219 Total/NA
Solid 5035500-69043-8 GP-05B-131219 Total/NA
Solid 5035500-69043-10 GP-08B-131219 Total/NA
Solid 5035500-69043-10 MS GP-08B-131219 Total/NA
Solid 5035500-69043-10 MSD GP-08B-131219 Total/NA
Solid 5035500-69043-12 GP-06B-131219 Total/NA
Solid 5035500-69043-13 GP-06B-131219D Total/NA
Solid 5035500-69043-20 GP-11B-131220 Total/NA
Solid 5035500-69043-20 - DL GP-11B-131220 Total/NA
Solid 5035500-69043-21 GP-11B-131220D Total/NA
Solid 5035500-69043-21 - DL GP-11B-131220D Total/NA
Solid 5035500-69043-23 GP-07A-131220 Total/NA
Solid 5035500-69043-24 GP-07B-131220 Total/NA
Solid 5035500-69043-25 GP-07B-131220D Total/NA
Solid 5035500-69043-27 GP-04B-131220 Total/NA
Analysis Batch: 218334
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260B 217834500-69043-1 GP-01A-131219 Total/NA
Solid 8260B 217834500-69043-3 GP-02A-131219 Total/NA
Solid 8260B 217834500-69043-5 GP-03A-131219 Total/NA
Solid 8260B 217834500-69043-7 GP-05A-131219 Total/NA
Solid 8260B 217834500-69043-9 GP-08A-131219 Total/NA
Solid 8260B 217834500-69043-11 GP-06A-131219 Total/NA
Solid 8260B 217834500-69043-11 MS GP-06A-131219 Total/NA
Solid 8260B 217834500-69043-11 MSD GP-06A-131219 Total/NA
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QC Association SummaryTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
GC/MS VOA (Continued)
Analysis Batch: 218334 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260B 217834500-69043-16 GP-09B-131220 Total/NA
Solid 8260B 217834500-69043-17 GP-10A-131220 Total/NA
Solid 8260B 217834500-69043-18 GP-10B-131220 Total/NA
Solid 8260BLCS 500-218334/6 Lab Control Sample Total/NA
Solid 8260BMB 500-218334/5 Method Blank Total/NA
Analysis Batch: 218369
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B500-69043-14 Trip Blank 121913 Total/NA
Water 8260BLCS 500-218369/4 Lab Control Sample Total/NA
Water 8260BMB 500-218369/6 Method Blank Total/NA
Analysis Batch: 218455
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260B 218172500-69043-2 GP-01B-131219 Total/NA
Solid 8260B 218172500-69043-2 - DL GP-01B-131219 Total/NA
Solid 8260B 218172500-69043-4 GP-02B-131219 Total/NA
Solid 8260B 218172500-69043-4 - DL GP-02B-131219 Total/NA
Solid 8260B 218172500-69043-6 GP-03B-131219 Total/NA
Solid 8260B 218172500-69043-6 - DL GP-03B-131219 Total/NA
Solid 8260B 218172500-69043-8 GP-05B-131219 Total/NA
Solid 8260B 218172500-69043-10 GP-08B-131219 Total/NA
Solid 8260B 218172500-69043-10 MS GP-08B-131219 Total/NA
Solid 8260B 218172500-69043-10 MSD GP-08B-131219 Total/NA
Solid 8260B 218172500-69043-12 GP-06B-131219 Total/NA
Solid 8260B 218172500-69043-13 GP-06B-131219D Total/NA
Solid 8260BLCS 500-218455/11 Lab Control Sample Total/NA
Solid 8260BMB 500-218455/6 Method Blank Total/NA
Analysis Batch: 218482
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260B 217834500-69043-15 GP-09A-131220 Total/NA
Solid 8260B 217834500-69043-19 GP-11A-131220 Total/NA
Solid 8260B 217834500-69043-26 GP-04A-131220 Total/NA
Solid 8260B 217834500-69043-26 MS GP-04A-131220 Total/NA
Solid 8260B 217834500-69043-26 MSD GP-04A-131220 Total/NA
Solid 8260BLCS 500-218482/6 Lab Control Sample Total/NA
Solid 8260BLCSD 500-218482/7 Lab Control Sample Dup Total/NA
Solid 8260BMB 500-218482/5 Method Blank Total/NA
Analysis Batch: 218487
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260B 218172500-69043-8 - DL GP-05B-131219 Total/NA
Solid 8260B 218172500-69043-20 GP-11B-131220 Total/NA
Solid 8260B 218172500-69043-21 GP-11B-131220D Total/NA
Solid 8260BLCS 500-218487/4 Lab Control Sample Total/NA
Solid 8260BMB 500-218487/6 Method Blank Total/NA
Analysis Batch: 218488
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B500-69043-22 Trip Blank 122013 Total/NA
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QC Association SummaryTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
GC/MS VOA (Continued)
Analysis Batch: 218488 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260BLCS 500-218488/4 Lab Control Sample Total/NA
Water 8260BMB 500-218488/6 Method Blank Total/NA
Analysis Batch: 218601
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260B 218172500-69043-23 GP-07A-131220 Total/NA
Solid 8260B 218172500-69043-24 GP-07B-131220 Total/NA
Solid 8260B 218172500-69043-25 GP-07B-131220D Total/NA
Solid 8260B 218172500-69043-27 GP-04B-131220 Total/NA
Solid 8260BLCS 500-218601/4 Lab Control Sample Total/NA
Solid 8260BMB 500-218601/6 Method Blank Total/NA
Analysis Batch: 218642
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260B 218172500-69043-20 - DL GP-11B-131220 Total/NA
Solid 8260B 218172500-69043-21 - DL GP-11B-131220D Total/NA
Solid 8260BLCS 500-218642/4 Lab Control Sample Total/NA
Solid 8260BMB 500-218642/6 Method Blank Total/NA
GC/MS Semi VOA
Prep Batch: 218462
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3541500-69043-23 GP-07A-131220 Total/NA
Solid 3541500-69043-24 GP-07B-131220 Total/NA
Solid 3541500-69043-25 GP-07B-131220D Total/NA
Solid 3541500-69043-26 GP-04A-131220 Total/NA
Solid 3541500-69043-26 MS GP-04A-131220 Total/NA
Solid 3541500-69043-26 MSD GP-04A-131220 Total/NA
Solid 3541500-69043-27 GP-04B-131220 Total/NA
Solid 3541500-69043-27 - DL GP-04B-131220 Total/NA
Solid 3541LCS 500-218462/2-A Lab Control Sample Total/NA
Solid 3541MB 500-218462/1-A Method Blank Total/NA
Prep Batch: 218463
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3541500-69043-1 GP-01A-131219 Total/NA
Solid 3541500-69043-2 GP-01B-131219 Total/NA
Solid 3541500-69043-3 GP-02A-131219 Total/NA
Solid 3541500-69043-4 GP-02B-131219 Total/NA
Solid 3541500-69043-5 GP-03A-131219 Total/NA
Solid 3541500-69043-6 GP-03B-131219 Total/NA
Solid 3541500-69043-7 GP-05A-131219 Total/NA
Solid 3541500-69043-8 GP-05B-131219 Total/NA
Solid 3541500-69043-9 GP-08A-131219 Total/NA
Solid 3541500-69043-10 GP-08B-131219 Total/NA
Solid 3541500-69043-11 GP-06A-131219 Total/NA
Solid 3541500-69043-11 MS GP-06A-131219 Total/NA
Solid 3541500-69043-11 MSD GP-06A-131219 Total/NA
Solid 3541500-69043-12 GP-06B-131219 Total/NA
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QC Association SummaryTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
GC/MS Semi VOA (Continued)
Prep Batch: 218463 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3541500-69043-13 GP-06B-131219D Total/NA
Solid 3541500-69043-15 GP-09A-131220 Total/NA
Solid 3541500-69043-16 GP-09B-131220 Total/NA
Solid 3541500-69043-17 GP-10A-131220 Total/NA
Solid 3541500-69043-18 GP-10B-131220 Total/NA
Solid 3541500-69043-19 GP-11A-131220 Total/NA
Solid 3541500-69043-20 GP-11B-131220 Total/NA
Solid 3541500-69043-20 - DL GP-11B-131220 Total/NA
Solid 3541500-69043-21 GP-11B-131220D Total/NA
Solid 3541500-69043-21 - DL GP-11B-131220D Total/NA
Solid 3541LCS 500-218463/2-A Lab Control Sample Total/NA
Solid 3541MB 500-218463/1-A Method Blank Total/NA
Analysis Batch: 218566
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270D 218462LCS 500-218462/2-A Lab Control Sample Total/NA
Solid 8270D 218463LCS 500-218463/2-A Lab Control Sample Total/NA
Solid 8270D 218462MB 500-218462/1-A Method Blank Total/NA
Solid 8270D 218463MB 500-218463/1-A Method Blank Total/NA
Analysis Batch: 218651
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270D 218463500-69043-1 GP-01A-131219 Total/NA
Solid 8270D 218463500-69043-2 GP-01B-131219 Total/NA
Solid 8270D 218463500-69043-3 GP-02A-131219 Total/NA
Solid 8270D 218463500-69043-5 GP-03A-131219 Total/NA
Solid 8270D 218463500-69043-6 GP-03B-131219 Total/NA
Solid 8270D 218463500-69043-7 GP-05A-131219 Total/NA
Solid 8270D 218463500-69043-9 GP-08A-131219 Total/NA
Solid 8270D 218463500-69043-10 GP-08B-131219 Total/NA
Solid 8270D 218463500-69043-11 GP-06A-131219 Total/NA
Solid 8270D 218463500-69043-11 MS GP-06A-131219 Total/NA
Solid 8270D 218463500-69043-11 MSD GP-06A-131219 Total/NA
Solid 8270D 218463500-69043-12 GP-06B-131219 Total/NA
Solid 8270D 218463500-69043-13 GP-06B-131219D Total/NA
Solid 8270D 218463500-69043-16 GP-09B-131220 Total/NA
Analysis Batch: 218873
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270D 218462500-69043-23 GP-07A-131220 Total/NA
Solid 8270D 218462500-69043-24 GP-07B-131220 Total/NA
Solid 8270D 218462500-69043-25 GP-07B-131220D Total/NA
Solid 8270D 218462500-69043-26 GP-04A-131220 Total/NA
Solid 8270D 218462500-69043-26 MS GP-04A-131220 Total/NA
Solid 8270D 218462500-69043-26 MSD GP-04A-131220 Total/NA
Solid 8270D 218462500-69043-27 GP-04B-131220 Total/NA
Analysis Batch: 219013
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270D 218463500-69043-4 GP-02B-131219 Total/NA
Solid 8270D 218463500-69043-8 GP-05B-131219 Total/NA
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QC Association SummaryTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
GC/MS Semi VOA (Continued)
Analysis Batch: 219013 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270D 218463500-69043-15 GP-09A-131220 Total/NA
Solid 8270D 218463500-69043-17 GP-10A-131220 Total/NA
Solid 8270D 218463500-69043-18 GP-10B-131220 Total/NA
Solid 8270D 218463500-69043-19 GP-11A-131220 Total/NA
Solid 8270D 218463500-69043-20 GP-11B-131220 Total/NA
Solid 8270D 218463500-69043-20 - DL GP-11B-131220 Total/NA
Solid 8270D 218463500-69043-21 GP-11B-131220D Total/NA
Solid 8270D 218463500-69043-21 - DL GP-11B-131220D Total/NA
Solid 8270D 218462500-69043-27 - DL GP-04B-131220 Total/NA
Metals
Prep Batch: 218329
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3050B500-69043-1 GP-01A-131219 Total/NA
Solid 3050B500-69043-2 GP-01B-131219 Total/NA
Solid 3050B500-69043-3 GP-02A-131219 Total/NA
Solid 3050B500-69043-4 GP-02B-131219 Total/NA
Solid 3050B500-69043-5 GP-03A-131219 Total/NA
Solid 3050B500-69043-6 GP-03B-131219 Total/NA
Solid 3050B500-69043-7 GP-05A-131219 Total/NA
Solid 3050B500-69043-8 GP-05B-131219 Total/NA
Solid 3050B500-69043-9 GP-08A-131219 Total/NA
Solid 3050B500-69043-10 GP-08B-131219 Total/NA
Solid 3050B500-69043-11 GP-06A-131219 Total/NA
Solid 3050B500-69043-11 DU GP-06A-131219 Total/NA
Solid 3050B500-69043-11 MS GP-06A-131219 Total/NA
Solid 3050B500-69043-11 MSD GP-06A-131219 Total/NA
Solid 3050B500-69043-12 GP-06B-131219 Total/NA
Solid 3050B500-69043-13 GP-06B-131219D Total/NA
Solid 3050B500-69043-15 GP-09A-131220 Total/NA
Solid 3050B500-69043-16 GP-09B-131220 Total/NA
Solid 3050B500-69043-17 GP-10A-131220 Total/NA
Solid 3050B500-69043-18 GP-10B-131220 Total/NA
Solid 3050B500-69043-19 GP-11A-131220 Total/NA
Solid 3050B500-69043-20 GP-11B-131220 Total/NA
Solid 3050B500-69043-21 GP-11B-131220D Total/NA
Solid 3050BLCS 500-218329/2-A Lab Control Sample Total/NA
Solid 3050BMB 500-218329/1-A Method Blank Total/NA
Prep Batch: 218336
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3050B500-69043-23 GP-07A-131220 Total/NA
Solid 3050B500-69043-24 GP-07B-131220 Total/NA
Solid 3050B500-69043-25 GP-07B-131220D Total/NA
Solid 3050B500-69043-26 GP-04A-131220 Total/NA
Solid 3050B500-69043-26 DU GP-04A-131220 Total/NA
Solid 3050B500-69043-26 MS GP-04A-131220 Total/NA
Solid 3050B500-69043-26 MSD GP-04A-131220 Total/NA
Solid 3050B500-69043-27 GP-04B-131220 Total/NA
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QC Association SummaryTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Metals (Continued)
Prep Batch: 218336 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3050BLCS 500-218336/2-A Lab Control Sample Total/NA
Solid 3050BMB 500-218336/1-A Method Blank Total/NA
Analysis Batch: 218473
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6010B 218336500-69043-23 GP-07A-131220 Total/NA
Solid 6010B 218336500-69043-24 GP-07B-131220 Total/NA
Solid 6010B 218336500-69043-25 GP-07B-131220D Total/NA
Solid 6010B 218336500-69043-26 GP-04A-131220 Total/NA
Solid 6010B 218336500-69043-26 DU GP-04A-131220 Total/NA
Solid 6010B 218336500-69043-26 MS GP-04A-131220 Total/NA
Solid 6010B 218336500-69043-26 MSD GP-04A-131220 Total/NA
Solid 6010B 218336500-69043-27 GP-04B-131220 Total/NA
Solid 6010B 218336LCS 500-218336/2-A Lab Control Sample Total/NA
Solid 6010B 218336MB 500-218336/1-A Method Blank Total/NA
Analysis Batch: 218474
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6010B 218329500-69043-1 GP-01A-131219 Total/NA
Solid 6010B 218329500-69043-2 GP-01B-131219 Total/NA
Solid 6010B 218329500-69043-3 GP-02A-131219 Total/NA
Solid 6010B 218329500-69043-4 GP-02B-131219 Total/NA
Solid 6010B 218329500-69043-5 GP-03A-131219 Total/NA
Solid 6010B 218329500-69043-6 GP-03B-131219 Total/NA
Solid 6010B 218329500-69043-7 GP-05A-131219 Total/NA
Solid 6010B 218329500-69043-8 GP-05B-131219 Total/NA
Solid 6010B 218329500-69043-9 GP-08A-131219 Total/NA
Solid 6010B 218329500-69043-10 GP-08B-131219 Total/NA
Solid 6010B 218329500-69043-11 GP-06A-131219 Total/NA
Solid 6010B 218329500-69043-11 DU GP-06A-131219 Total/NA
Solid 6010B 218329500-69043-11 MS GP-06A-131219 Total/NA
Solid 6010B 218329500-69043-11 MSD GP-06A-131219 Total/NA
Solid 6010B 218329500-69043-12 GP-06B-131219 Total/NA
Solid 6010B 218329500-69043-13 GP-06B-131219D Total/NA
Solid 6010B 218329500-69043-15 GP-09A-131220 Total/NA
Solid 6010B 218329500-69043-16 GP-09B-131220 Total/NA
Solid 6010B 218329500-69043-17 GP-10A-131220 Total/NA
Solid 6010B 218329500-69043-18 GP-10B-131220 Total/NA
Solid 6010B 218329500-69043-19 GP-11A-131220 Total/NA
Solid 6010B 218329500-69043-20 GP-11B-131220 Total/NA
Solid 6010B 218329500-69043-21 GP-11B-131220D Total/NA
Solid 6010B 218329LCS 500-218329/2-A Lab Control Sample Total/NA
Solid 6010B 218329MB 500-218329/1-A Method Blank Total/NA
General Chemistry
Analysis Batch: 217924
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture500-69043-1 GP-01A-131219 Total/NA
Solid Moisture500-69043-2 GP-01B-131219 Total/NA
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QC Association SummaryTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
General Chemistry (Continued)
Analysis Batch: 217924 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture500-69043-3 GP-02A-131219 Total/NA
Solid Moisture500-69043-4 GP-02B-131219 Total/NA
Solid Moisture500-69043-5 GP-03A-131219 Total/NA
Solid Moisture500-69043-6 GP-03B-131219 Total/NA
Solid Moisture500-69043-7 GP-05A-131219 Total/NA
Solid Moisture500-69043-8 GP-05B-131219 Total/NA
Solid Moisture500-69043-9 GP-08A-131219 Total/NA
Solid Moisture500-69043-10 GP-08B-131219 Total/NA
Solid Moisture500-69043-11 GP-06A-131219 Total/NA
Solid Moisture500-69043-11 DU GP-06A-131219 Total/NA
Solid Moisture500-69043-11 MS GP-06A-131219 Total/NA
Solid Moisture500-69043-11 MSD GP-06A-131219 Total/NA
Solid Moisture500-69043-12 GP-06B-131219 Total/NA
Solid Moisture500-69043-13 GP-06B-131219D Total/NA
Solid Moisture500-69043-15 GP-09A-131220 Total/NA
Solid Moisture500-69043-16 GP-09B-131220 Total/NA
Solid Moisture500-69043-17 GP-10A-131220 Total/NA
Solid Moisture500-69043-18 GP-10B-131220 Total/NA
Solid Moisture500-69043-19 GP-11A-131220 Total/NA
Solid Moisture500-69043-20 GP-11B-131220 Total/NA
Solid Moisture500-69043-21 GP-11B-131220D Total/NA
Solid Moisture500-69043-23 GP-07A-131220 Total/NA
Solid Moisture500-69043-24 GP-07B-131220 Total/NA
Solid Moisture500-69043-25 GP-07B-131220D Total/NA
Solid Moisture500-69043-26 GP-04A-131220 Total/NA
Solid Moisture500-69043-26 DU GP-04A-131220 Total/NA
Solid Moisture500-69043-26 MS GP-04A-131220 Total/NA
Solid Moisture500-69043-26 MSD GP-04A-131220 Total/NA
Solid Moisture500-69043-27 GP-04B-131220 Total/NA
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Surrogate SummaryTestAmerica Job ID: 500-69043-1Client: CDM Smith, Inc.
Project/Site: 3450 E 2056th Wedron IL
Method: 8260B - Volatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (70-122) (75-120) (70-134) (75-122)
BFB DBFM 12DCE TOL
103 100 103 95500-69043-1
Percent Surrogate Recovery (Acceptance Limits)
GP-01A-131219
89 101 100 96500-69043-3 GP-02A-131219
98 104 104 97500-69043-5 GP-03A-131219
91 102 102 98500-69043-7 GP-05A-131219
96 100 91 98500-69043-9 GP-08A-131219
93 98 87 99500-69043-11 GP-06A-131219
95 90 86 104500-69043-11 MS GP-06A-131219
92 94 83 104500-69043-11 MSD GP-06A-131219
92 97 87 95500-69043-15 GP-09A-131220
96 97 86 98500-69043-16 GP-09B-131220
94 96 91 99500-69043-17 GP-10A-131220
92 94 90 96500-69043-18 GP-10B-131220
94 101 94 96500-69043-19 GP-11A-131220
89 92 81 103500-69043-26 GP-04A-131220
90 92 80 101500-69043-26 MS GP-04A-131220
88 93 85 103500-69043-26 MSD GP-04A-131220
101 99 102 103LCS 500-218334/6 Lab Control Sample
93 97 85 102LCS 500-218482/6 Lab Control Sample
88 93 82 103LCSD 500-218482/7 Lab Control Sample Dup
89 94 91 96MB 500-218334/5 Method Blank
92 94 80 101MB 500-218482/5 Method Blank
Surrogate Legend
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane
12DCE = 1,2-Dichloroethane-d4 (Surr)
TOL = Toluene-d8 (Surr)
Method: 8260B - Volatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (75-120) (75-120) (75-125) (75-120)
BFB DBFM 12DCE TOL
101 91 186 X 105500-69043-2
Percent Surrogate Recovery (Acceptance Limits)
GP-01B-131219
101 95 115 102500-69043-2 - DL GP-01B-131219
100 94 131 X 104500-69043-4 GP-02B-131219
102 93 108 104500-69043-4 - DL GP-02B-131219
101 89 133 X 102500-69043-6 GP-03B-131219
98 96 109 104500-69043-6 - DL GP-03B-131219
99 93 127 X 101500-69043-8 GP-05B-131219