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N O T E S :* A S R E P O R T E D 3 Y W E S T - P A J N E L A B O R A T O R I E S , I N C . , ' N . D . ' M E A N S B E L O U T r EH T F A C E A M D l f f T S Q F D I - N - B U T ' / L P H T H A L A T E W E R E D F E C T E D .

P H T W L A T E S A R E C a f r i C N L Y F O U N D I H U A T E ? w L ' : R E ^ C P I P E I S U S E D .- H O S A F E D R I N K I N G W A T E R S T A N D A R D S A R E S E " P O R T H E S E P A R A M E T E R S .

•p/ E S T - P A I N EIcUxnctt&u&b I N C .<A—-7979GSRIAVE. • BATON R O U G E , LA 70808

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7 9 7 9 G S R I A V E . • BATON R O U G E . LA 70808

L O U I S I A N A D E P A R T M E N T O F E N V I R O N M E N T A L Q U A L I T YS e p t e m b e r 8, 1986

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S a m p l e s as d e s i g n a t e d b e l ow and on the enc lo s ed c h a i n - o f - c u s t o d y do cumenta t i on werede l iv er ed to W e s t - P a i n e L a b o r a t o r i e s , I n c . on Augus t 21, 1986. The s a m p l e s were a n a l y z e daccording ' t o t h e Environmental Pro t e c t i on Agency protoco l a s shown o n t h e Loui s iana A n a l y s i sResul t s R e p o r t i n g S h e e t s .

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L O U I S I A N A A N A L Y S I S R E S U L T S R E P O R T I N G S H E E TL O U I S I A N A S A M P L E I . D . * A 0 5 8 6 0 S 2 1 - 0 1L A B O R A T O R Y I . D . I 360821-109________D A T E : 08-21-36

N / AS a m p l e P r e p a r a t i o n M e t h o dI f m u l t i p l e m e t h o d s were u s e d , l i s t met f iod" a n d a n a l y s T sp e r f o r m e d .W e r e s p i k e s a d d e d t o t h e s a m p l e , y e s ( X ) n o ( )If yes, a t what s t a g e ? B e f o r e Purging_______

M E T H O D8240

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Paramet erBenzeneB r o m o f o r mC a r b o n t e t r a c h l o r i d eC h l o r o b e n z e n eC h l orod i b r o m o m e t h a n eC h l o r o e t h a n e2 - C h l o r o e t h y l v i n y l e therC h l o r o f o r m1 , 2 - D i c h l o r o b e n z e n e1,4-Di C h l o r o b e n z e n e1 , 3 - D i c h l o r o b e n z e n eDi ch 1 o robrornome thane1 , 1 - D i c h l o r o e t h a n e1 , 2 - O i c h l o r o e t h a n e

S W - 8 4 6T e s tM e t h o d824002403240824032408240.8240824082408 2 / I O324032403 2 / 1 03240

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Parametert r a n s - l . Z - D l c h l . o r o e t h e n e1 , 2 - D i c h l o r o p r o p a n e _______c i s - 1 . 3 - D i c h l o r o p r o p e n et r d n s - l , 3 - D i c h l o r o p r o p e n eE t h y l benzene ________M e t h y l b r o m i d e ________M e t h y l c h l o r i d e _______M e t h y l e n e c h l o r i d e ________1 , 1 . 2 . 2 - T e t r a c h l o r o e t h a n eTe t r a c h 1 oroe t h e n eT o l u ene1 , 1 , 1 - T r i c h l o r o e t h a n e1, 1 , 2 - T r i c h l o r Q e t h a n eTr i c h 1 1 oroe t h e n e _______T r i c h l o r o f l u o r i n e t h a n eV i f i y l c h l o r i d e

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I c e r t i f y t h a t t h e s a m p l e p r e p a r a t i o n m e t h o d ( s ) a n d a n a l y t i c a l t e s t m e t h o d s , ( i n c l u d i n g r e q u i s i t e c a l i b r a t i o n p r o c e d u r e s a n df r e q u e n c y , a n d q u a l i t y c o n t r o l p r o c e d u r e s ) were t h o s e d e s c r i b e d above.

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S W - 8 4 6T e s tM e t h o d8240824082408240824032408 2 / 1 082408240824082408240824082403 2 / 1 0

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P a r a m e t e rt r a n s - l , 2 - D 1 c h _ 1 o r o e t h e n e1 , 2 - D i c h l o r o p r o p a n e ____c i s - l . S - D i c h l o r o p r o p e n et r d n s - l ^ - D i c h l o r o p r o p e n eE t h y l benzene ___________M e t h y l b r o m i d e ________M e t h y l c h l o r i d e _______M e t h y l e n e c h l o r i d e ______1, 1 , 2 , 2 - T e t r a c h l o r o e t h a n eT e t r a c h l o r o e t h e n e _____To l u e n e ___________1. 1 . 1 - T r i c h l o r o e t h a n e1 , 1 , 2 - T r i c h l o r o e t h a n eT r l c h l o r o e t h e n e _________Tr 1 ch 1 oro f 1 uonne th aneV i n y l c h l o r i d e

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I c e r t i f y t h a t t h e s a m p l e p r e p a r a t i o n m e t h o d ( s ) a n d a n a l y t i c a l t e s t m e t h o d s ( i n c l u d i n g r e q u i s i t e c a l i b r a t i o n p r o c e d u r e s a n df r e q u e n c y , a n d q u a l i t y c o n t r o l p r o c e d u r e s ) were t h o s e d e s c r i b e d above.

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L a b o r a t o r yS W - 8 4 § D u p l i c a t e L a b o r a t o r yT e s t R e s u l t R e s u l t B l a n k V a l u eM e t h o d ( U n i t s ) * ( i f a p p l i c a b l e ) ( i f a p p l i c a b l e )8240 <0.0108240 <0.0108240 < 0.0108240 <0.0108240 <0.0108240 <0.0108240 <0.01082^10 <0.0108240 <0.010

• 3240 <0.0108240 <0.0108240 <0.0108210 <0.0103240 <0.0103240 <0.010

A N A L Y S I S


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P a r a m e t e r ,t r a n s - l , 2 - D i c h l . t ) r o e t h e n e1, 2 - D 1 c h l o r o p r q p a n e ____c i s - 1 . 3 - D i c h l o r o p r o p e n et r d n s - l i S - O i c h l o r o p r o p e n eE t h y l benzene ________M e t h y l b r o m i d e ___________M e t h y l c h l o r i d e ___________Me thy 1 ene ch 1 or i de ____1 , 1 , 2 , 2 - T e t r a c h 1 oroe t h a n eT e t r a c h l o r o e t h e n e ________T o l u e n e _______________1 , 1 , 1 - T r i c h l o r o e t h a n e1 , 1 , 2 - T r l c h l o r o e t h a n e

Jr i c h l o r o e t h ene ______ _^T r i c h l o r o f l u o r i i i e t h a n eV i n y l c h l o r i d e

S W - 8 4 6T e s tM e t h o d8240024082408240824082408240824082408240824082408240824082408240

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* A l l r e s u l t s i n P P M u n l e s s o t h e r w i s e n o t e d .M i l l i g r a m s p e r l i t e r .Spike l e v e l - 40 o p b ,

I c e r t i f y t h a t t h e s a m p l e p r e p a r a t i o n m e t h o d ( s ) a n d a n a l y t i c a l t e s t m e t h o d s ( i n c l u d i n g r e q u i s i t e c a l i b r a t i o n p r o c e d u r e s a n df r e q u e n c y , a n d q u a l i t y c o n t r o l p r o c e d u r e s ) were tho s e d e s c r i b e d above.

S i g n a t u r e V i c ' t o ' r J . - ' B - T a n c h ' a r d , I I T 'G e n e r a l M a n a g e r' i t l e

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L O U I S I A N A A N A L Y S I S R E S U L T S R E P O R T I N G S H E E TL O U I S I A N A S A M P L E I . D . #A05S60821-04L A B O R A T O R Y I . D . # 860821-112D A T E : 0 8 - 2 R S B — — — — — — — — — — —N / AS a m p l e P r e p a r a t i o n M e t h o d _____I f m u l t i p l e m e t h o d s were u s e d , l i s t m e t h o c T a n d a n a l y s e sp e r f o r m e d .

M E T H O D8240

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P a r a m e t e rBenzeneB r o m o f o r mCarbon t e t r a c h l o r i d eC h l o r o b e n z e n eC h l o r o d ibromomethaneC h l o r o e t h a n e2 - C h l o r o e t h y l v i n y l e therC h l o r o f o r m1 , 2 - D i c h l o r o b e n z e n e1 , 4 - D i c h l o r o b e n z e n e1 , 3 - D i c h l o r o b e n z e n eD i c h 1 orobromomethane1 , 1 - D i c h l o r o e t h a n e1, 2 - D i c h l o r o e t h a n e1, 1 - D i c h l o r o e t h e n e

S W - 8 4 6T e s tM e t h o d824082408240824082408240824082408240824082408240824082408240

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_ p _ . Q 1 0 _0.010

E S T - P A I N E7 9 7 9 G S R I A V E . • BATON R O U G E , LA 70806

P a r a m e t e rt r a n s - I ^ - D i c h l o r o e t h e n e1 . 2 - D i c h l o r o p r o p a n e _ _ _ _c i s - 1 . 3 - D i c h l o r o p r o p e n et r d n s - l ^ - D i c h l o r o p r o p e n eEthylbenzene________•*M e t h y l b r o m i d e _ _ _ _ _ _ _ _ _ _ _ _ _M e t h y l c h l o r i d e _ _ _ _ _ _ _M e t h y l e n e c h l o r i d e _ _ _ _ _ _ _1, 1 , 2 ^ - T e t r a c h l o r o e t h a n eT e t r a c h l o r o e t h e n e _ _Toluene_________________1 . 1 . 1 - T r i c h 1 o r o e t h a n e1 . 1 . 2 - T r l c h l o r o e t h a n eT r i c h l o r o e t h e n eT r i c h l o r o f l u o n n e t h d n eV i n y l c h l o r i d e

S W - 8 4 6T e s tM e t h o d824082403240824082408240G2408240824082408240

82408240

_824Q_8240

R e s u l t( U n i t s ) *<o.mo<0.010<0.010<0.010< Q . 0 1 Q<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010

L a b o r a t o r yD u p l i c a t eR e s u l t( i f a p p l i c a b l e )L a b o r a t o r yB 1 a n k " V a l u e( i f a p p l i c a b l e )


101

D e t e c t i o nL i m i t0.010~bToio~o7oio0.010

0.0100.0100.0100.0100.010f l . O I Q0.0100.010

0.01* A l l r e s u l t s i n P P M u n l e s s o t h e r w i s e n o t e d .

M i l l i q r a m s p e r l i t e r .S p i k e l ev e l - 40 p o b .I c e r t i f y t h a t t h e s a m p l e p r e p a r a t i o n m e t h o d ( s ) a n d a n a l y t i c a l t e s t m e t h o d s ( i n c l u d i n g r e q u i s i t e c a l i b r a t i o n p r o c e d u r e s a n df r e q u e n c y , a n d q u a l i t y c o n t r o l p r o c e d u r e s ) were t h o s e d e s c r i b e d above.

S i g n a t u r e , :C T a n c h a r dGenera l M a n a g e r

r,I I I

T i t l e

S a m p l e I d e n t i f i c a t i o n ( L o u i s i a n a D N R ] A 0 5 8 6 0 8 2 1 -

L O U I S I A N A A N A L Y S I S R E S U L T S R E P O R T I N G S H E E TL O U I S I A N A S A M P L E 1.0. f A05360821-05L A B O R A T O R Y I . D . # 8 6 0 B Z I - I I 3 ________D A T E : 03-21-86S a m p l e P r e p a r a t i o n M e t h o d M / AI f m u l t i p l e m e t h o d s were u s e d , l i s t me thod a n d a n a l y s i sp e r f o r m e d .

M E T H O D8240

• A N A L Y S I S P E R F O R M E D D I L U T I O N F A C T O R SV o l a t i l e O r g a n i c F r a c t i o n

s. - -

P a r a m e t e rBenzeneBromoformCarbon t e t r a c h l o r i d eC h l o r o b e n z e n eCh 1 orod i b r o m o m e t h a n eC h l o r o e t h a n e2 - C h l o r o e t h y l v i n y l e t h erC h l o r o f o r m1 , 2 - D i c h l o r o b e n z e n e1 , 4-Di ch 1 orobenzene1 , 3 - D i c h l o r o b e n z e n eD i c h l o r o b r o m o m e t h a n e1 , 1 - D i c h l o r o e t h a n e1 , 2-Di ch 1 o ro e thane1 , 1 - D i c h l o r o e t h e n e

S W - 8 4 6T e s tM e t h o d824082408240824082408240824082408240824082^08240824082408240

L a b o r a t o r yD u p l i c a t eR e s u l t R e s u l t( U n i t s ) * ( i f a p p l i c a b l e )<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010

X 0 . 0 1 0<0.010<0.010<0.01Q<0.010


W e r e s p i k e s a d d e d t o t h e s a m p l e , y e s ( X ) n o ( )If yes, at what s t a g e ? B e f o r e Purging______

A N A L Y S I S


100

D e t e c t i o nL i m i tn . o i oo.oioo . o i oQJQo._.o.o i o0.0100.0100.0100.0100.0100.0100.0100.010,0.010

E S T - P A I N E7 9 7 9 G S R I A V 6 . • BATON R O U G E , LA 70808

Parame t e rt r a n s - 1 . 2 - D i c h l Q r Q e t h e n el . 2 - D 1 c h l o r o p r o p a n e _____c i s - 1 . 3 - D i c h l o r o p r o p e n et r d n s - l , 3 - D i c h 1 o r o p r o p e n eE t h y l b e n z e n eM e t h y ] b r o m i d eM e t h y l c h l o r i d eM e t h y l e n e c h l o r i d e1 , 1 , 2 . 2 - T e t r a c h l o r o e t h a n eT e t r a c h l o r o e t h e n eT o l u e n e1 , 1 , 1 - T r i c h l o r o e t h a n e1 . 1 . 2 - T r i c h l o r Q e t h a n eT r i c h l o r o e t h e n eT r i c h l o r o f l u o r i n e t h a n e ____V i n y l c h l o r i d e •

S W - 8 4 6on u-r«T e s tM e t h o d824032403240824082400240S24032408240,3240C24Q824082408240G2408240

R e s u l t( U n i t s ) *<0.010<0.010<0.010<0.01G<0.010<0.010<0.010<0.010<0.010< 0.010<0.010< 0.010<0.010<Q.01Q

_<0.010<0.010

L a b o r a t o r yD u p l i c a t eR e s u l t( i f a p p l i c a b l e )L a b o r a t o r yB l a n k " V a l u e( i f a p p l i c a b l e )


97


~Q100.0100.010

0.010" o T o T f T0.0100.0100.0100.0100.0100.0100.0100.010

* A l l r e s u l t s i n , P P M u n l e s s o t h e r w i s e n o t e d .M i l l i g r a m s p e r l i t e r .S p i k e l e v e l - 4 0 p p b .

I c e r t i f y t h a t t h e s a m p l e p r e p a r a t i o n m e t h o d ( s ) a n d a n a l y t i c a l t e s t m e t h o d s ( I n c l u d i n g r e q u i s i t e c a l i b r a t i o n p r o c e d u r e s a n df r e q u e n c y , a n d q u a l i t y c o n t r o l p r o c e d u r e s ) were t h o s e d e s c r i b e d above.

" S l g T i l t u r e < ^ - " ' V 4 ' c t o r " J . B l a n c h a r d , 1 1 1G e n e r a l M a n a g e r

T i t l e

S a u p l e I d e n t i f i c a t i o n ( L o u i s i a n a D N R ) A05060821-05

L O U I S I A N A A N A L Y S I S R E S U L T S R E P O R T I N G S H E E TL O U I S I A N A S A M P L E I . D . # A 0 5 8 6 0 8 2 1 - 0 6L A B O R A T O R Y I . D . #

S a m p l e P r e p a r a t i o n M e t h o dI f m u l t i p l e m e t h o d s were u s e d ,p e r f o r m e d .M E T H O D8240

N / Al i s t method

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D A T E : 08-21

and a n a l y s i s

P E R F O R M E DO r g a n i c F r a c t i o n

860821-114-86

W e r e s p i k e s a d d e d t cIf yes , a t what s t a c


N.

P a r a m e t e rBenzeneBromoformC a r b o n t e t r a c h l o r i d eC h l o r o b e n z e n eC h l o r o d i b r o m o m e t h a n eC h l o r o e t h a n e2 - C h l o r o e t h y l v i n y l e th erC h l o r o f o r m1 , 2 - D i c h l o r o b e n z e n e1 , 4 - D i c h l o r o b e n z e n e1 , 3 - D i c h l o r o b e n z e n eDi ch 1 o r obromome thane1 , 1 - D i c h l o r o e t h a n e1 , 2 - D i c h l o r o e t h a n e1, 1 - D i c h l o r o e t h e n e

S W - 8 4 6T e s tM e t h o d824082408240824082408240824082408240824082408240824082408240

L a b o r a t o r yD u p l i c a t e L a b o r a t o r yR e s u l t R e s u l t B l a n k V a l u e( U n i t s ) * ( i f a p p l i c a b l e ) ( i f a p p l i c a b l e )<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010

X 0 . 0 1 0<0.010

B e f o r e P u r g i n g

A N A L Y S I S


98

D e t e c t i o nL i m i t0.0100.0100.010

0.0100.010"b~.oio0.0100.0100.0100.0100.0100.0100.010

P A I N E7 9 7 9 G S R I A V E . • BATON R O U G E . LA 70608

P a r a m e t e rt r a n s - l , 2 - 0 i c h l o r o e t h e n e1 , 2 - D i c h l o r o p r o p a n ec i s - l , 3 - D i c h l o r o p r o p e n et r d n s - l , 3 - D i c h l o r o p r o p e n eE t h y l b e n z e n eM e t h y l b r o m i d eM e t h y l c h l o r i d eM e t h y l e n e c h l o r i d e1 , 1 , 2 , 2 - T e t r a c h l o r o e t h a n eT e t r a c h l o r o e t h e n eT o l u e n e1 , 1 , 1 - T r i c h l o r o e t h a n e1 , 1 , 2 - T r i c h l o r o e t h a n eT r i c h l o r o e t h e n eT r i c h l o r o f l u o n n e t h a n eV i n y l c h l o r i d e* A l l r e s u l t s i n P P M u n l e s s

S U - 8 4 6T e s tM e t h o d824082408?408?40824082408240824082408240824082408240824082408240

o t h e r w i s e n o t e d .

R e s u l t( U n i t s ) *<0.010<0.010<0.010<0.010<0.010<0-.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010

L a b o r a t o r yD u p l i c a t eR e s u l t( i f a p p l i c a b l e )L a b o r a t o r yB l a n k " V a l u e( i f a p p l i c a b l e )


94


~0100.010"0.010

0.0100.0100.0100.0100.0100.0100.0100.0100.0100.010

M i l l i g r a m s p e r l i t e r .S p i k e l e v e l - 40 p p b .I c e r t i f y t h a t t h e s a m p l e p r e p a r a t i o n m e t h o d ( s ) a n d a n a l y t i c a l t e s t m e t h o d s ( i n c l u d i n g r e q u i s i t e c a l i b r a t i o n p r o c e d u r e s a n df r e q u e n c y , a n d q u a l i t y c o n t j r o l p r o c e d u r e s ) were t h o s e d e s c r i b e d above.

S i g r i a t u r e V l c t d r J . ' B l a n c h a r d , I I IGeneral M a n a g e r

' i t l e

S a m p l e I d e n t i f i c a t i o n ( L o u i s i a n a D N R ) A05860821-06

" j l T W E S T - P A I N E(^^JaJjotatotieA we.7 S 7 9 G S R I A V E . • BATON R d U G E , LA 70608

S a m p l e P r e p a r a t i o n M e t h o dI f m u l t i p l e m e t h o d s were usedp e r f o r m e d .M E T H O D8270

L O U I S I A N A A N A L Y S I S R E S U L T S R E P O R T I N G S H E E TL O U I S I A N A S A M P L E I . D . # A 0 5 8 6 0 8 2 1 - 0 1LABORATORY I. D. # P , 6 0 8 2 1 - 1 f i 9 ....D A T E : O S -3510, l i s t method and a n a l y s i s

A N A L Y S I S P E R F O R M E DB a s e - N e u t r a l F r a c t i o n

01 Of.i. 1 -1.,-U

Were s p i k e s a d d e d to the s a m p l e , yes ( ) no ( x )If yes, a t what s t a g e ?D I L U T I O N F A C T O R S A N A L Y S I S

9

Paramet erA c e n a p h t h e n eA c e n a p h t h y l e n eA n t h r a c e n eB e n z i d i n eBenzo( a) A n t h r a c e n eB e n z o ( a ) P y r e n e3-4 Benzo F l u o r an theneB e n z o ( g h i ) P e r y l e n eB e n z o ( k ) F l u o r an theneBi s ( 2 - C h l o r o e t h o x y ) M e t h a n eB i s ( 2 - C h l o r o e t h y l ) E t h e rB i s ( 2 - C h l o r o i s o p r o p y l ) E t h e rB i s - ( 2 - E t h y l h e x y l ) P h t h a l a t e4 B r o m o p h e n y l P h e n y l Ether

S W - 8 4 6T e s tM e t h o d8270827082708270827082708270827082708270827082708270R?70

R e s u l t( U n i t s ) *<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010•<o.oio<0.010<0.010<0.010<0.010<0.010

L a b o r a t o r yD u p l i c a t e L a b o r a t o r y S p i k eR e s u l t B l a n k V a l u e Recovery D e t e c t i o n( i f a p p l i c a b l e ) ( i f a p p l i c a b l e ) ( i f a p p l i c a b l e ) L i m i t0.0100.0100.010O . O K Wo.m™0.0100.0100.0100.0100.0100.0100.0100.0100.010

W E S T - P A I N EI N C .7 9 7 9 G S R 1 A V E . • BATON R O U G E , LA 70808

Paramet erButyl Benzyl P h t h a l a t e2 - C h l o r o n a p h t h a l e n e4 - C h l o r o p h e n y l P h e n y l E t h e rC h r y s e n eD i t r e n z o ( a . h ) A n t h r a c e n e1 , 2 - D i c h l o r o b e n z e n e1 , 3 - D i c h l o r o b e n z e n e1, 4-Dich l orob enz ene3 , 3 ' - D i c h l o r o b e n z i d i n eD i e t h y l P h t h a l a t eD i m e t h y l P h t h a l a t eD i - n - B u t y l P h t h a l a t e2 , 4 - D i n i t r o t o l u e n e2 , 6 - D i n t r o t o l u e n eD i - n - O c t y l P h t h a l a t e1 , 2 - D i p h e n y l h y d r a z i n eH e x a c h 1 orobu tad i eneF l u o r a n t h e n eF l u o r e n eH e x a c h 1 orobenzeneH e x a c h 1 orocyc 1 open tad i eneH e x a c h l o r o e t h a n eI n d e n o ( 1 , 2 , 3 - c d ) Pyrene

J ^ s o p h o r o n eN a p t h a l e n eN i t r o b e n z e n e

SW-846T e s tM e t h o d82708270827082708270

•8270 '82708270027082708270827082708270827082700270827082708270027082708270827082708270

R e s u l t( U n i t s ) *<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010

0.020<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010

L a b o r a t o r yD u p l i c a t eR e s u l t LaboratoryB l a n k V a l u e( i f a p p l i c a b l e )S p i k eRecovery( i f a p p l i c a b l e ) D e t e c t i o nL i m i t

0.0100.0100.0100.010

o.o0.0100.0100.0100.0100.0100.0100.0100.0100.010

0.0100.0100.0100-.01Q0.0100.0100.0100.010_0.0100.010

E S T - P A I N EU N C .

7 9 7 9 G S R I A V E . • BATON R O U G E , LA 70BOB

Parameter'N - N i t r o s p d l m e t h y l a m i n eN - N i t r o s o d i - N - P r o p y 1 amineN - N i t r o s o d i p n e n y l a m i n eP h e n a n t h r e n ePyrene1 , 2 , 4 - T r i c h l o r o b e n z e n e

S W - 8 4 6T e s tM e t h o d827082703270827082708270

R e s u l t( U n i t s ) *<0.010<0.010<0.010

X O . O I O<0.010<0.010

Labora toryD u p l i c a t eR e s u l t( i f a p p l i c a b l e )L a b o r a t o r y S p i k eB l a n k V a l u e Recovery( i f a p p l i c a b l e ) ( i f a p p l i c a b l e ) D e t e c t i o nL i m i t

0.010Toi o

0.00.0100.010

* A l l r e s u l t s 1 n P P M u n l e s s o t h e r w i s e n o t e d .M i l l i g r a m s p e r l i t e r .

S u r r o g a t e S t d . Recovery ( % ) D e c a f l u o r o b i n h e n y lF l u o r e n e - d l O 94%1 1 6 SI c e r t i f y that t h e s a m p l e p r e p a r a t i o n m e t h o d ( s ) a n d a n a l y t i c a l te s t m e t h o d s ( i n c l u d i n g r e q u i s i t e c a l i b r a t i o n p r o c e d u r e s a n df r e q u e n c y , and q u a l i t y control p r o c e d u r e s ) were tho s e d e s c r i b e d above.

S i g n a t u r e V f c r b r - d ' . B l a n c n a r c r r lGeneral M a n a g e r

T i t l e

S a m p l e I d e n t i f i c a t i o n ( L o u i s i a n a D N R ) A 0 5 8 6 0 8 2 1 - 0 1

W E S T - P A I N EI N C .7 9 7 9 G S R I A V E . • BATON R O U G E , LA 70608

L O U I S I A N A A N A L Y S I S R E S U L T S R E P O R T I N G S H E E TL O U I S I A N A S A M P L E I . D . I A 0 5 3 6 0 8 2 1 - 0 2L A B O R A T O R Y I . D . I G 6 0 S 2 T - I I UD A T E : 08-21-36S a m p l e P r e p a r a t i o n M e t h o d 3510___l______^______I f m u l t i p l e m e t h o d s were u s e d , l i s t method a n d a n a l y s i sp e r f o r m e d .

M E T H O D3270


•-

ParameterA c e n a p h t h e n eA c e n a p h t h y l e n e -A n t h r a c e n eB e n z i d i n eBenzo( a) Anthrac eneB e n z o ( a ) P y r e n e3-4 Benzo F l u o r a n t h e n eB e n z o ( g h i ) P e r y l e n eB e n z o ( k ) F l u o r a n t h e n eBi s ( 2 - C h l o r o e thoxy ) M e t h a n eB i s ( 2 - C h l o r o e t h y l ) E t h e rB i s ( 2 - C h l o r o i s o p r o p y l ) E t h e rB i s - ( 2 - E t h y l h e x y l ) P h t h a l a t e

SW-846T e s tM e t h o d8270827032708270827082708?70827082708270827082708270

R e s u l t( U n i t s ) *<0.010<0.010< 0 ' . 0 1 0<0.010<0.010<0.010^0.010<0.010<0.010<0.010<0.010<0.010<0.010

W e r e s p i k e s a d d e d to the s a m p l e , yes ( ) no (X )If yes, at what s tage? ____________________D I L U T I O N F A C T O R S A N A L Y S I S

LaboratoryD u p l i c a t eR e s u l t( i f a p p l i c a b l e )LaboratoryB l a n k V a l u e( i f a p p l i c a b l e )

S p i k eRecovery( 1 f a p p l i c a b l e ) D e t e c t i o nL i m i t0.0100.0100.010

4 B r o m o p h e n y l P h e n y l E t h e r 8270 <n.mo

0.0100.0100.0100.0100.0100.0100.0100.0100.010

|̂jr W E S T - P A 1 N E/ £ l p ) JaAvMzt&ueA I N C .\̂ ***5/ Gr^^^~****

7 9 7 9 G S R I A V E . • BATON B O U G E , LA 70808

ParameterButyl Benzyl P h t h a l a t e2 - C h l o r o n a p h t h a l e n e4 - C h l o r o p h e n y l P h e n y l E t h e rChryseneDi l>enzo( a, h ) A n t h r a c e n e1, 2 - D i c h l o r o b e n z e n e1, 3 - D i c h l o r o b e n z e n e1 , 4 - D i c h l o r o b e n z e n e3 , 3 ' - D i c h l o r o b e n z i d i n eD i e t h y l P h t h a l a t eD i m e t h y l P h t h a l a t eD i - n - B u t y l P h t h a l a t e2 , 4 - D i n i t r o t o l u e n e2, 6 - D i n t r o t o l u e n eD i - n - O c t y l P h t h a l a t e1 , 2 - D i p h e n y l h y d r a z i n eH e x a c h l o r o b u t a d i e n eF l u o r a n t h e n eF l u o r e n eH e x a c h l o r o b e n z e n eH e x a c h 1 orocyc 1 o p e n t a d i eneH e x a c h l o r o e t h a n eI n d e n o ( 1 , 2 , 3 - c d ) PyreneI s o p h o r o n eN a p t h a l e n eN i t r o b e n z e n e

S W - 8 4 6T e s tM e t h o d3270

.82708270827082708270827082708270S 2 7 08270827082708270827082708270827082708270827082708270827082708270

L a b o r a t o r yD u p l i c a t e Labora tory S p i k eR e s u l t R e s u l t B l a n k V a l u e Recovery( U n i t s ) * ( i f a p p l i c a b l e ) ( i f a p p l i c a b l e ) ( i f a p p l i c a b l e )<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010

0.029<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010

, (

D e t e c t i o nL i m i t0.010n.o io0.0100.0100.0]| fr0.0™0.0100,0100.0100.0100.0100.0100.0100.0100.010^f-0.0100.0100,0100.0100.0100.010- o . o i o0.0100.010

W E S T - P A I N E-̂•® ^ icLoaicajcru&awc.7 9 7 9 G S R I A V E . « BATON ROUGE. LA 70608

ParameterN - N i t r o s o d i m e t h y l a n f i i n eN - N i t r o s o d 1 - N - P r o p y 1 amineN - H i t r o s o d i p h e n y l a m i n aP h e n a n t h r e n ePyrene1 , 2 , 4 - T r i c h 1 o r o b e n z e n e

S W - 8 4 6T e s tM e t h o d827082708270827032708270

' R e s u l t( U n i t s ) *<0.010<0.010<0.010<0.01Q<0.010<0.010

LaboratoryD u p l i c a t eR e s u l t( i f a p p l i c a b l e )L a b o r a t o r yB l a n k V a l u e( i f a p p l i c a b l e )

S p i k eRecovery( i f a p p l i c a b l e ) D e t e c t i o nL i m i t0,0100.010

0.0100.010

* A T I r e s u l t s I n P P M u n l e s s o t h e r w i s e n o t e d .M i l l i g r a m s p e r l i t e r .S u r r o g a t e S t d . Recovery ( % } D e c a f ! u o r o b i n h e n y l 7 9 %F l u o r o e n e - d l O " 98%

I c e r t i f y that t h e s a m p l e p r e p a r a t i o n m e t h o d ( s ) a n d a n a l y t i c a l te s t m e t h o d s ( i n c l u d i n g r e q u i s i t e c a l i b r a t i o n p r o c e d u r e s a n df r e q u e n c y , and q u a l i t y contro l p r o c e d u r e s ) were tho s e d e s c r i b e d above.

S i g n a t u r e V i c t o r - 3 . B l a n c h a r d , I I IG e n e r a l M a n a q e r

i t l e


we. L O U I S I A N A A N A L Y S I S R E S U L T S R E P O R T I N G S H E E TL O U I S I A N A S A M P L E I . D . # A05860821-03 fV. —— s —7 9 7 9 G S R I A V E . » BATON R O U G E . LA 70808

S a m p l e P r e p a r a t i o n M e t h o dI f m u l t i p l e m e t h o d s were u s e d ,p e r f o r m e d .M E T H O D

327Q

L A B O R A T O R Y I . D . #DATE: OB-3510l i s t method a n d a n a l y s i s


360821-11121-86W e r e s p i k e s a d d e d t oIf yes, at what s t a g


'

ParameterA c e n a p h t h e n eA c e n a p h t h y l e n eA n t h r a c e n eB e n z i d i n eBenzo( a ) A n t h r a c e n eB e n z o ( a ) P y r e n e3-4 Benzo F l u o r a n t h e n eB e n z o ( g h i ) P e r y l e n eB e n z o ( k ) F l u o r a n t h e n eB i s ( 2 - C h l o r o e t h o x y ) M e t h a n eB i s ( 2 - C h l o r o e t h y l ) E t h e rB i s ( 2 - C h l o r o i s o p r o p y l ) E t h e rB i s - ( 2 - E t h y l h e x y l ) P h t h a l a t e4 Bromophenyl P h e n y l Ether

SW-846T e s tM e t h o d327082700270G 2 7 Q8270327082708270827082703270027032708270

R e s u l t( U n i t s ) *<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010

L a b o r a t o r yD u p l i c a t e L a b o r a t o r yR e s u l t B l a n k V a l u e( i f a p p l i c a b l e ) ( i f a p p l i c a b l e )

A N A L Y S I S

S p i k eRecovery( i f a p p l i c a b l e ) D e t e c t i o nL i m i t0.0100.0100.0100.010.010.0100.0100.0100.0100.0100.0100.0100.0100.010

WEST-PAI N EI N C .7979GSRIAVE. • BATON R O U G E . LA 70808

ParameterButyl Benzyl P h t h a l a t e2 - C h l o r o n a p h t h a l e n e4 - C h l o r o p h e n y l Phenyl EtherChrys eneD i benzol a, h) Anthrac ene1 T 2 - D i c h l o r o b e n z e n el f 3 - D i c h l o r o b e n z e n e1 , 4 - D i c h l o r o b e n z e n e3 , 3 ' - D i c h l o r o b e n z i d i n eD i e t h y l P h t h a l a t eD i m e t h y l P h t h a l a t eD i - n - B u t y l P h t h a l a t e2 , 4 - D i n i t r o t o l u e n e2 , 6 - D i n t r o t o l u e n eD i - n - O c t y l P h t h a l a t e1 , 2 - D i p h e n y l h y d r a z i n eH e x a c h 1 orobu tad i eneF l u o r a n t h e n eF l u o r e n eH e x a c h l o r o b e n z e n eH e x a c h 1 orocyc 1 o p e n t a d i eneH e x a c h l o r o e t h a n eI n d e n o ( 1 , 2 , 3 - c d ) PyreneI s o p h o r o n eN a p t h a l e n eN i t r o b e n z e n e

S W - 8 4 6T e s tM e t h o d827082708270827082708270827082708270827082708270827082708270827082708270827082708270

• 8270 •8270827082708270

R e s u l t( U n i t s ) *<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010

0.016<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010

L a b o r a t o r yD u p l i c a t eR e s u l t( i f a p p l i c a b l e )L a b o r a t o r yB l a n k V a l u e( i f a p p l i c a b l e )

S p i k eRecovery( i f a p p l i c a b l e ) D e t e c t i o nL i m i t0.0100.0100.0100.010

o.oi0.0100.0100.0100.0100.0100.0100.0100.0100.01

0.0100.0100.0100.0100.0100.0100.0100.0100.0100.010

•pW E S T - P A I N EI I N C .

7979GSRIAVE. • BATON R O U G E . LA 70808

Paramet erN - N i t r o s o d i m e t h y l a m i n eN - N i t r o s o d i - N - P r o p y l a m i n eN - N - i t r o s o d i p h e n y l a i r r i n eP h e n a n t h r e n ePyrene1 , 2 , 4 - T r i c h l o r o b e n z e n e

S W - 8 4 6T e s tM e t h o d827082708270827082708270

R e s u l t( U n i t s ) *<0.010<0.010<0.010<O.Q10<0.010<0.010

L a b o r a t o r yD u p l i c a t eR e s u l t( i f a p p l i c a b l e )L a b o r a t o r yB l a n k V a l u e( I f a p p l i c a b l e )

S p i k eRecovery( i f a p p l i c a b l e ) D e t e c t i o nL i m i t0.0100.010

0.0100.010

A l l r e s u l t s 1 n P P M u n l e s s o t h e r w i s e n o t e d .M i l l i g r a m s p e r l i t e r .S u r r o q a t e S t d . Recovery ( % ) D e c a f l u o r o b i o h e n y lF l u o r e n e - d - 1 0 90%• 111%

I c e r t i f y that t h e s a m p l e p r e p a r a t i o n m e t h o d ( s ) a n d a n a l y t i c a l test me thod s ( I n c l u d i n g r e q u i s i t e c a l i b r a t i o n proc edure s a n df r e q u e n c y , and q u a l i t y contro l p r o c e d u r e s ) were tho s e d e s c r i b e d above.

S i g n a t u r e V t c t d ' r J r B f a n c h a r d , I I IG e n e r a l M a n a g e rT i t l e


L O U I S I A N A A N A L Y S I S R E S U L T S R E P O R T I N G S H E E TL O U I S I A N A S A M P L E I . D . # A05060821-04"• —— ' •—7 9 7 9 0 S R I A V E . » BATON R O U G E , LA 70808 L A B O R A T O R Y I . D . # 060821-112D A T E : 00-21-86S a m p l e P r e p a r a t i o n M e t h o dI f m u l t i p l e m e t h o d s were u s e d ,p e r f o r m e d .

M E T H O D8270

3510l i s t method a n d a n a l y s i s

A N A L Y S I S P E R F O R M E DB a s e - N e t u r a l F r a c t i o n

Were s p i k e s added to the s a m p l e , yes ( ) no ( x)If yes, at what s t a g e ?D I L U T I O N F A C T O R S A N A L Y S I S

^ ^̂ B

ParameterA c e n a p h t h e n eA c e n a p h t h y l e n eA n t h r a c e n eB e n z i d i n eBenzo( a ) A n t h r a c e n eB e n z o ( a ) P y r e n e3-4 Benzo F l u o r a n t h e n eB e n z o ( g h i ) P e r y l e n eB e n z o ( k ) F l u o r a n t h e n eBi s ( 2-Ch 1 oro e thoxy ) M e t h a n eB i s ( 2 - C h l o r o e t h y 1 ) E t h e rB i s ( 2 - C h l o r o i s o p r o p y l ) EtherB i s - ( 2 - E t h y l h e x y l ) P h t h a l a t e4 B r o m o p h e n y l P h e n y l Ether .

SW-846T e s tMethod82708270827082708270827002708270327082700270827082708270

R e s u l t( U n i t s ) *<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010

L a b o r a t o r yD u p l i c a t e Laboratory S p i k eR e s u l t B l a n k V a l u e Recovery D e t e c t i o n( i f a p p l i c a b l e ) ( i f a p p l i c a b l e ) ( 1 f a p p l i c a b l e ) L i m i t0.0100.0100.010o . o i o j i0.01™0.0100.0100.0100.0100.0100.0100.0100.0100.010

W E S T - P A I N E7 9 7 9 G S R I A V E . • B A T O N M O U G E , L A 70808

ParameterB u t y l Benzyl P h t h a l a t e2 - C h l o r o n a p h t h a l e n e4 - C h l o r o p h e n y l P h e n y l E t h e rC h r y s e n eD i k e n r o ( a , h ) A n t h r a c e n e1, 2 - D i c h l o r o b e n z e n e1 , 3-Di chl orobenzenel ? 4 - D i c h l o r o b e n z e n e3 , 3 ' - D i c h l o r o b e n z i d i n eD i e t h y l P h t h a l a t eD i m e t h y l P h t h a l a t eD i - n - B u t y l P h t h a l a t e2, 4 - D i n i t r o t o l u e n e2 , 6 - D i n t r o t o l u e n eD i - n - O c t y l P h t h a l a t e1 , 2 - D i p h e n y l h y d r a z i n eH e x a c h 1 orobu tad i eneF l u o r a n t h e n eF l u o r e n eH e x a c h 1 orobenzeneH e x a c h 1 orocyc 1 o p e n t a d i eneH e x a c h l o r o e t h a n eI n d e n o ( 1 , 2 , 3 - c d ) PyreneI s o p h o r o n eM a p t h a l e n eN i t r o b e n z e n e

S W - 8 4 6T e s tM e t h o d327082708270

• 8270 •8270827082708270827082700270827082708270827082708270827082708270827082708270827082708270

R e s u l t( U n i t s ) *<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010

L a b o r a t o r yD u p l i c a t eR e s u l t( i f a p p l i c a b l e )L a b o r a t o r y S p i k eBlank" V a l u e Recovery( i f a p p l i c a b l e ) ( 1 f a p p l i c a b l e ) D e t e c t i o nL i m i t

0.0100.010 "0.0100.0100.010o.ol0.0100.0100.0100.010O . Q 1 00.010o.oio"0.0100.010"To"57"b~oioo . o i o 'o . o i o 'o . o i o 'o . o i o ' 'o . o i o 'o . o i o '0.0100.010

pE S T - P A I N EI N C .7979GSRIAVE. • BATON R O U G E , LA 70608

Paramet erN - N i t r o s o d i m e t h y l a m i n eN - N i t r o s o d i - N - P r o p y 1 amineN-N-i t ro sod i p h e n y 1 ami neP h e n a n t h r e n ePyrene1 . 2 . 4 - T r i c h l o r o b e n z e n e

S W - 8 4 6T e s tM e t h o d327082708270327082708270

L a b o r a t o r yD u p l i c a t eR e s u l t R e s u l t( U n i t s ) * ( i f a p p l i c a b l e )<0.010

L a b o r a t o r y S p i k eB l a n k V a l u e Recovery( i f a p p l i c a b l e ) ( i f a p p l i c a b l e )

<0.010<0.010<0.010<0.010<0.010

D e t e c t i o nL i m i t0.0100.0100.010

0.0100.010

* A l l r e s u l t s i n P P M u n l e s s o th erw i s e n o t e d .f l i H i grams p e rS u r r o g a t e S t d . l i t e r .Recovery ( % ) D e c a f l u o r o b i o h e n y l 3 6 %F l u o r e n e - d I O ' 100%

I c e r t i f y that t h e s a m p l e p r e p a r a t i o n m e t h o d ( s ) a n d a n a l y t i c a l test m e t h o d s ( i n c l u d i n g r e q u i s i t e c a l i b r a t i o n p r o c e d u r e s a n df r e q u e n c y , and q u a l i t y control p r o c e d u r e s ) were those d e s c r i b e d above.

S i g n a t u r e J . ^ B T a n c h a r c i , i n

G e n e r a l M a n a g e rT i t l e


E S T - P A I N EI N C . L O U I S I A N A A N A L Y S I S R E S U L T S R E P O R T I N G S H E E T -L O U I S I A N A S A M P L E 1.0. # A05360821-057 9 7 9 G S R I A V E . • BATON ROUGE. LA 70808

S a m o l e P r e p a r a t i o n MethodI f m u l t i p l e m e t h o d s were u s e ' d ,p e r f o r m e d .M E T H O D8270

L A B O R A T O R Y I . D . # 860821-113D A T E :3510l i s t me thod a n d a n a l y s i s


08-21-86Were s p i k e s added to the s a m p l e , yes ( ) no (X)If yes, at what s t ag e?

D I L U T I O N F A C T O R S A N A L Y S I S. . . . . . . . ^ ^V

Paramet erA c e n a p h t h e n eA c e n a p h t h y l e n eA n t h r a c e n eB e n z i d i n eBenzo( a ) A n t h r a c e n eB e n z o ( a ) P y r e n e3-4 Benzo F l u o r a n t h e n eB e n z o ( g h i ) P e r y l e n eB e n z o ( k ) F l u o r a n t h e n eB i s ( 2 - C h l o r o e t h o x y ) M e t h a n eB i s ( 2 - C h l o r o e t h y l ) E t h e rB i s ( 2 - C h l o r o i s o p r o p y l ) E t h e rB i s - ( 2 - E t h y l h e x y l ) P h t h a l a t e4 Bromophenyl Phenyl Ether

S W - 8 4 6T e s tM e t h o d82708270827082708270827032708270827082708270827082708270

R e s u l t( U n i t s ) *<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010

L a b o r a t o r yD u p l i c a t e L a b o r a t o r y S p i k eR e s u l t B l a n k V a l u e Recovery D e t e c t i o n( i f a p p l i c a b l e ) ( i f a p p l i c a b l e ) ( i f a p p l i c a b l e ) L i m i t0.0100.0100.010O . O l Q l f e0.010^0.0100.0100.0100.0100.0100.0100.0100.0100.010

Vx___^ f -*w- —7 9 7 9 G S R I A V E . • BATON R O U G E , LA 70808

Paramet erB u t y l Benzyl P h t h a l a t e2 - C h l o r o n a p h t h a l e n e4 - C h l o r o p h e n y l Phenyl EtherC h r y s e n eD i b £ n z b ( a , h ) A n t h r a c e n e1, 2 - D i c h l o r o b e n z e n e1, 3 - D i c h l o r o b e n z e n e1 , 4 - D i c h l o r o b e n z e n e3 , 3 ' - D i c h l o r o b e n z i d i n eD i e t h y l P h t h a l a t eD i m e t h y l P h t h a l a t eD i - n - B u t y l P h t h a l a t e2, 4 - D i n i t r o t o l u e n e2, 6 - D i n t r o t o l u e n eD i - n - O c t y l P h t h a l a t e1» 2 - D i p h e n y l h y d r a z i n eH e x a c h 1 orobu tad i eneF l u o r a n t h e n eF l u o r e n eH e x a c h l o r o b e n z e n eH e x a c h 1 orocyc 1 o p e n t a d i eneH e x a c h l o r o e t h a n eI n d e n o ( 1 , 2 , 3 - c d ) PyreneI s o p h o r o n eN a p t h a l e n eN i t r o b e n z e n e

S W - 8 4 6T e s tM e t h o d32708270827082708270827032703270827082708270827002703270827082703270827032708270827082703270327082703270

R e s u l t( U n i t s ) *<0..010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010

L a b o r a t o r yD u p l i c a t eR e s u l t Laboratory S p i k eB l a n k ' V a l u e Recovery( i f a p p l i c a b l e ) ( i f a p p l i c a b l e ) D e t e c t i o nL i m i t0.0100.0100.0100.0100.010o.oii0.0100.0100.0100.0100.0100.0100.0100.0100.010

0.010.0100.0100,0100.0100.0100.0100.0100.0100.010

•p/ E S T - P A I N E) < / — ^

7 9 7 9 G S R I A V E . • BATON R O U G E , LA 70806

ParameterN - N i t r o s o d i m e t h y l a m i n eN - N i t r o s o d i - N - P r o p y 1 amineN - M i t r b s o d I p h e n y l a m l n eP h e n a n t h r e n ePyrene1 , 2 , 4 - T r i c h l o r o b e n z e n e

SW-846T e s tM e t h o d827082708270827082708270

R e s u l t( U n i t s ) *<0.010<0.010<0.010<Q.01Q<Q.01Q<0.010

L a b o r a t o r yD u p l i c a t eR e s u l t( i f a p p l i c a b l e )LaboratoryB l a n k V a l u e( 1 f a p p l i c a b l e )

S p i k eRecovery( 1 f a p p l i c a b l e ) D e t e c t i o nL i m i t0.0100.010O . O T jo . o f lO . Q 1 Q0.010

A l l r e s u l t s 1 n P P M u n l e s s o t h e r w i s e n o t e d .f i l m grams p e r l i t e r .S u r r o g a t e S t d . Recovery D e c a f l u o r o b i n h e n y l 94?bF l u o r e n e - d l O ' 110%

I c e r t i f y that t h e s a m p l e p r e p a r a t i o n m e t h o d ( s ) a n d a n a l y t i c a l te s t m e t h o d s ( I n c l u d i n g r e q u i s i t e c a l i b r a t i o n p r o c e d u r e s a n df r e q u e n c y , and q u a l i t y control p r o c e d u r e s ) were those d e s cr i b ed above.

S i g n a t u r e M H c ' t o r - i f . B T a n ' c h a r d T ; I I IGeneral M a n a g e r

T i t l e


•pE S T - P A I N EI N C .7 9 7 9 G S M AVE. • BATON R O U G E , LA 70808

L O U I S I A N A A N A L Y S I S R E S U L T S R E P O R T I N G S H E E TL O U I S I A N A S A M P L E I . D . I A05360821-06L A B O R A T O R Y I . D . I 860821-114D A T E ; 08-21-86_________S a m p l e P r e p a r a t i o n M e t h o d 3510___^_^__^__^_^I f m u l t i p l e me thod s were u s ed , 11st method a n d a n a l y s i sp e r f o r m e d .

M E T H O D8270

A N A L Y S I S P E R F O R M E D D I L U T I O N F A C T O R SB a s e - N e u t r a l F r a c t i o n

•»»

ParameterA c e n a p h t h e n eA c e n a p h t h y l e n eA n t h r a c e n eB e n z i d i n eBenzo( a) AnthraceneB e n z o ( a ) P y r e n e3-4 Benzo F l u o r a n t h e n eB e n z o ( g h i ) P e r y l e n eB e n z o ( k ) F l u o r a n t h e n eB i s ( 2 - C h l o r o e t h o x y ) M e t h a n eB i s ( 2 - C h l o r o e t h y l ) E t h e rB i s ( 2 - C h l o r o i s o p r o p y 1 ) E t h e rB i s - ( 2 - E t h y l h e x y l ) P h t h a l a t e

S W - 8 4 6T e s tM e t h o d8270827082708270827082708270827082708270827082708270

L a b o r a t o r yD u p l i c a t eR e s u l t R e s u l t( U n i t s ) * ( i f a p p l i c a b l e )<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010

L a b o r a t o r yB l a n k V a l u e( i f a p p l i c a b l e )<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010

W e r e s p i k e s added to the s a m p l e , yes (*) no ( )If yes, a t what s t ag e? B e f o r e E x t r a c t i o n _ _ _A N A L Y S I S


102128N . S .

1251 1 1110

9792868988

4 B r o m o p h e n y l P h e n y l E t h e r 8270 <0.010 <0.010 82

D e t e c t i o nL i m i t0.010 :0.010 :

0.0100.010.O . O K0.0100.0100.0100.0100.0100.0100.0100.0100.010

7 9 7 9 G S R I A V E . • B A T O N R O U G E , L A 70608

Paramet erButyl Benzyl P h t h a l a t e2 - C h l o r o n a p h t h a l e n e4 - C h l o r o p h e n y l P h e n y l EtherC h r y s e n eD i trenzo( a, h) A n t h r a c e n e1 , 2 - D i c h l o r o b e n z e n e1 , 3 - D i c h l o r o b e n z e n e1, 4 - D i c h l o r o b e n z e n e3 , 3 ' - D i c h l o r o b e n z i d i n eD i e t h y l P h t h a l a t eD i m e t h y l P h t h a l a t eD i - n - B u t y l P h t h a l a t e2 , 4 - D i n i t r o t o l u e n e2 , 6 - D i n t r o t o l u e n eD i - n - O c t y l P h t h a l a t e1 , 2 - D i p h e n y l h y d r a z i n eH e x a c h 1 orobu tad i eneF l u o r a n t h e n eF l u o r e n eH e x a c h l o r o b e n z e n e .H e x a c h 1 orocyc 1 o p e n t a d i eneH e x a c h l o r o e t h a n eI n d e n o ( 1 , 2 , 3 - c d ) PyreneI s o p h o r o n eN a p t h a l e n eN i t r o b e n z e n e

S W - 8 4 6T e s tM e t h o d0270827082708270827082708270827082708270827082708270827082708270827082708270

• 8270 •827082708270827082708270

R e s u l t( U n i t s ) *<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010<0.010< 0 . 0 ] 0<0.010<0.010<0.010<0.010

• LaboratoryD u p l i c a t eR e s u l t( i f a p p l i c a b l e )Labora t oryB l a n k V a l u e( i f a p p l i c a b l e )

<0.010<0.010<0.010<O.Q10<0.010<0.010<0.010<0.010<0.010<0.010<0.01Q<0.010<0.010<0.010<0.010<0.010< o . p i o<0.010<0.010<0.01Q<0.010<O.Q10<0.010<0.010<0.010<0.010

S p i k eRecovery( i f a p p l i c a b l e )8982859268817679N . S .947878935196N . S .769086

HE66~72~113

90TT

93

D e t e c t i o nL i m i t0.0100.0100.0100.010Q - Q i0.0100:0100.0100.0100.0100.0100.0100.0100.0100.0]"o"7oio~0.0100.0100.. 010o.oTo"0.010~o7oTb~

' o . o i o '0.010"0.010

W E S T - P A I N EI N C .7 9 7 9 G S R I A V 6 . • BATON R O U G E . LA 70608

ParameterN - N i t r o s o d i m e t h y l a m i n eN-Ni t r o s od i -N-Propy 1 ami neN-Ni trosod i p h e n y 1 ami neP h e n a n t h r e n ePyrene1 , 2 , 4 - T r i c h l o r o b e n z e n e

S W - 8 4 6T e s tM e t h o d827082708270827082708270

LaboratoryD u p l i c a t eR e s u l t R e s u l t( U n i t s ) * ( i f a p p l i c a b l e )<0.010<0.010<0.010<0.010<0.010<0.010

L a b o r a t o r yB l a n k V a l u e( i f a p p l i c a b l e )<0.010<0.010<0.010<0.010<0.010<0.010


102869084

D e t e c t i o nL i m i t0.0100.010

" T o T g T "o . o i o ' 'o . o i oo.oio

A l l r e s u l t s i n P P M u n l e s s o t h e r w i s e n o t e d .S p i k e d a t 1 0 0 p p b M i l l i g r a m s n e r l i t e r .N . S . = N o t S o i k e d S u r r o g a t e S t d . Recovery ( % } D e c a f l u o r o b i n h e n y lF l u o r e n e - d l O

I c e r t i f y that t h e s a m p l e p r e p a r a t i o n m e t h o d ( s ) a n d a n a l y t i c a l test m e t h o d s ( i n c l u d i n g r e q u i s i t e c a l i b r a t i o n p r o c e d u r e s a n df r e q u e n c y , and q u a l i t y contro l p r o c e d u r e s ) were tho s e d e s c r i b e d above.

S i g n a t u r e V i c t o r J . B l a n c h a r d , I I IGeneral M a n a g e rT i t l e


•pW E S T - P A I N EI N C .7 9 7 9 G S R I A V E . • BATON R O U G E , LA 70608

L O U I S I A N A A N A L Y S I S R E S U L T S R E P O R T I N G S H E E TL O U I S I A N A S A M P L E I . D . I A 0 5 8 6 0 3 2 1 - 0 1L A B O R A T O R Y I . D . I 860821-109______D A T E nR-?1-86_________

S a m p l e P r e p a r a t i o n M e t h o d 3 5 1 0 _ _ _ _I f m u l t i p l e m e t h o d s were u s e d , l i s t method a n d a n a l y s i sp e r f o r m e d .M E T H O D8270

A N A L Y S I S P E R F O R M E DA c i d E x t r a c t a b l e F r a c t i o n

W e r e s p i k e s a d d e d to the s a m p l e , yes ( ) noIf yes» at what s t a g e ? ____________________D I L U T I O N F A C T O R S A N A L Y S I S

Parameter2 - C h l o r o p h e n o l2-4 D i c h l o r o p h e n o l2-4 D i m e t h y l p h e n o l4-6 D i n i t r o 0-Cresol2-4 D i n i t r o p h e n o l2 - N i t r o p h e n o l _ _ _ _ _ _ _4 - N i t r o p h e n p l _ _ _ _ _P - C h l o r o - M - C r e s o lP e n t a c h l o r o p h e n o lPhenol_________2-4-6 T r i c h l o r o p h e n o l

S W - 8 4 6T e s tM e t h o d02708270827082708270827032708270827082708270


Labora toryB l a n k V a l u e( i f a p p l i c a b l e ) "S p i k eRecovery( i f a p p l i c a b l e )

<0.010<0.010<0.03Q<0.050<0.010<0.040<0.010<0.010<0.010<0.010

D e t e c t i o nL i m i t0.0100.0100.0100.030

D500.0100.0400.0100.010" o T o T o '0.010

* A l l r e s u l t s i n P P M u n l e s s o t h e r w i s e n o t e d .2 - N 1 t r o p h e n o l - d 4 -P e n t a c h l o r o n h e n o l - 84%

W E S T - P A I N E7 9 7 9 G S R I A V E . • B A T O N R O U G E , L A 70fl08

I c e r t i f y tha t t h e s a m p l e p r e p a r a t i o n m e t h o d ( s ) a n d a n a l y t i c a l te s t m e t h o d s ( i n c l u d i n g r e q u i s i t e c a l i b r a t i o n p r o c e d u r e s a n df r e q u e n c y , and q u a l i t y control p r o c e d u r e s ) were tho s e d e s c r i b e d above. -^

S i g n a t u r e wctor J : B l a n c h ' a r a , I I IG e n e r a l M a n a g e r

T i t l e


d r b

'P" W E S T - P A I N E\Ja6otcderue6 I N C .7979 GSRIAVE. • BATON R O U G E , LA 70608

L O U I S I A N A A N A L Y S I S R E S U L T S R E P O R T I N G S H E E TL O U I S I A N A S A M P L E I . D . i t A 0 5 8 6 0 8 2 1 - 0 2L A B O R A T O R Y I . D . ID A T E : 08-21-86S a m p l e P r e p a r a t i o n M e t h o d 3510___ ........ ..t.I f m u l t i p l e m e t h o d s were u s e d , l i s t me thod a n d a n a l y s i sp e r f o r m e d .

M E T H O D827.0


W e r e s p i k e s a d d e d to the s a m p l e , yes ( )If yes, at what s tage? ________ no

D I L U T I O N F A C T O R S A N A L Y S I S

P a r a m e t e r2 - C h l o r o p h e n o l2-4 D i c h l o r o p h e n o l2-4 D i m e t h y l p h e n o l4-6 D i n i t r o Q - C r e s o l2-4 D i n i t r o p h e n o l2 - N i t r o p h e n o l _ _ _ _ _4 - N i t r o p h e n o l _ _ _ _ _P - C h l o r o - M - C r e s o lP e n t a c h l o r o p h e n o lPhenol__________2-4-6 T r i c h l o r o p h e n o l

S W - 8 4 6T e s tM e t h o d82708270827082708270827082708270827082708270


L a b o r a t o r yB l a n k V a l u e( i f a p p l i c a b l e ) "S p i k eRecovery( i f a p p l i c a b l e )

<0.010<0.010<0.030<0.050<0.010<0.040<0.010<0.010<0.010<0.010

D e t e c t i o nL i m i t0.0100.0100.010

0.0100.0400.0100.0100.0100.010

* A l l r e s u l t s i n P P M u n l e s s o t h e r w i s e n o t e d .H i H i grams p e r l i t e r . S u r r o g a t e S t d . Recovery ( % ) - 2 - N i t r o n h e n o l - 1 0 5P e n t a c h l o r o n h e n o l - 84

E S T - P A I N EU N C .

7 9 7 9 G S R I A V E . • BATON ROUGE. LA 70806

I c e r t i f y that t h e s a m p l e p r e p a r a t i o n m e t h o d ( s ) a n d a n a l y t i c a l te s t m e t h o d s ( i n c l u d i n g r e q u i s i t e c a l i b r a t i o n p r o c e d u r e s a n df r e q u e n c y , and q u a l i t y c on t ro l p r o c e d u r e s ) were tho s e d e s c r i b e d above.

S i g n a t u r e V i c t o r J T ' B ' l a n c h a r d , I I IG e n e r a l M a n a g e rT i t l e

S a m p l e I d e n t i f i c a t i o n ( L o u i s i a n a D N R ) A 0 5 8 6 0 8 2 U 0 2

drb


L O U I S I A N A A N A L Y S I S R E S U L T S R E P O R T I N G S H E E TL O U I S I A N A S A M P L E I . D . $ A 0 5 8 6 0 8 2 1 - 0 3L A B O R A T O R Y I . D . # .Rf i fwum_______DATE nft-21-86__________S a m p l e P r e p a r a t i o n M e t h o d 3510I f m u l t i p l e me thod s were u s ed , l i s t method a n d a n a l y s i sp e r f o r m e d .

M E T H O D3270


Were s p i k e s added to the s a m p l e , yes ( ) noI f . y e s , at what s tage? ________________D I L U T I O N F A C T O R S A N A L Y S I S

Parameter2 - C h l o r o p h e n o l2-4 D i c h l o r o p h e n o l2-4 D i m e t h y l p h e n o l4-6 D i n i t r o 0-Creso l2-4 D i n i t r o p h e n o l2 - N i t r o p h e n o l _ _ _ _ _4 - N i t r o p h e n o l _ _ _ _P - C h l o r o - M - C r e s o lP e n t a c h l o r o p h e n o lPhenol_________2-4-6 T r i c h l o r o p h e n o l

S W - 8 4 6T e s tM e t h o d82708270827082708270827082708270827082708270

R e s u l t( U n i t s ) *<0.010<o.oio -<0.010<0.030<n.o50<0.010<0.040xo . o i o<0.010<0.010<0.010

Labora t oryD u p l i c a t eR e s u l t( i f a p p l i c a b l e )L a b o r a t o r yB l a n k V a l u e( i f a p p l i c a b l e )

. S p i k eRecovery( i f a p p l i c a b l e ) D e t e c t i o nL i m i t0.0100.0100.010

330roso0.0100.0400.0100.0100.0100.010

A l l r e s u l t s i n P P M u n l e s s o t h e r w i s e n o t e d .M i l l i g r a m s p e r l i t e r . S u r r o g a t e S t d . Recovery ( " ) 2 - N i t r o p h e n o 1 - d 4 - 9 6P e n t a c h l o r o n h e n o l - 58

I N C .7 9 7 9 G S R I A V E . • BATON ROUGE. LA 70008

I . c e r t i f y that the s a m p l e p r e p a r a t i o n m e t h o d ( s ) and a n a l y t i c a l test me thod s ( i n c l u d i n g r equ i s i t e c a l i b r a t i o n procedure^, andf r e q u e n c y , and q u a l i t y contro l p r o c e d u r e s ) were tho s e d e s c r i b e d above. re«L i

S i g n a t u r e \J .-" B I c t n c n a r a , ill

G e n e r a l M a n a g e rT i t l e


pV V E S T - P A I N EU N C .7 9 7 9 G S R I A V E . • BATON R O U G E . LA 70808

I c e r t f f y that t h e s a m p l e p r e p a r a t i o n m e t h o d ( s ) a n d a n a l y t i c a l test m e t h o d s ( i n c l u d i n g r e q u i s i t e c a l i b r a t i o n procedui^^andf r e q u e n c y , and q u a l i t y contro l p r o c e d u r e s ) were tho s e d e s c r i b e d above.

S i g n a t u r e v i c t or J . " B T a n c h ' a r d , I I IG e n e r a l Manager______T i t l e


drb

pE S T - P A I N EI N C .7 9 7 9 G S R I A V E . • BATON R O U G E , LA 70808

L O U I S I A N A A N A L Y S I S R E S U L T S R E P O R T I N G S H E E TL O U I S I A N A S A M P L E I . D . I A 0 5 8 6 0 8 2 1 - 0 5L A B O R A T O R Y I . D . # 860821-113_______D A T E ; 08-21-86_________3510S a m p l e P r e p a r a t i o n M e t h o d _I f m u l t i p l e m e t h o d s were used,~l i s t method a n d a n a l y s i sp e r f o r m e d .

M E T H O D.3270


W e r e s p i k e s a d d e d to the s a m p l e , yes ( ) no (X )If yes, at what s tage? _______________D I L U T I O N F A C T O R S A N A L Y S I S

Paramet er2 - C h l o r o p h e n o l2-4 D i c h l o r o p h e n o l2-4 D i m e t h y l p h e n o l4-6 D i n i t r o 0-Cresol2-4 D i n i t r o p h e n o l2 - N i t r o p h e n o l _ _ _4 - N i t r o p h e n o l _ _ _ _ _P - C h l o r o - M - C r e s o lP e n t a c h l o r o p h e n o lPhenol_________2-4-6 T r i c h l o r o p h e n o l

S W - 8 4 6T e s tM e t h o d827032703270827082708270.82708270827082708270

R e s u l t( U n i t s ) *<0.010< o . o I F "<o.oio<0.030<0.050<0.01Q<0.040<0.010<0.01Q<0.010<0.010

A l l r e s u l t s i n P P M u n l e s s o t h e r w i s e n o t e d .M i l l i g r a m s p e r l i t e r .

Labora toryD u p l i c a t eR e s u l t( i f a p p l i c a b l e )L a b o r a t o r y S p i k eB l a n k V a l u e Recovery( i f a p p l i c a b l e ) ' ( i f a p p l i c a b l e ) D e t e c t i o nL i m i t

0.0100.0100.010

(l|t|r|30U7050~0.0100.040

. 0.0100.0100.0100.010

S u r r o g a t e S t d . Recovery ( % ) - 2 - N i t r o n h e n o l - d 4 - 1 0 6P e n t a c h l o r o n h e n o l .- 78

W E S T - P A I N E7 9 7 9 G S R I A V E . • BATON R O U G E , LA 70806

I c e r t i f y that t h e s a m p l e p r e p a r a t i o n m e t h o d ( s ) a n d a n a l y t i c a l test m e t h o d s ( i n c l u d i n g r e q u i s i t e c a l i b r a t i o n procedur^andf r e q u e n c y , a n d q u a l i t y c o n t r o l p r o c e d u r e s ) were t ho s e d e s c r i b e d above. ir^L !

S i g n a t u r e ^Vic t o r J . B l a f f c h i a r d , I I I•___________General Manager______T i t l e


d r b

PE S T - P A I N EI N C .7979GSRIAVE. • BATON R O U G E , LA 70806

L O U I S I A N A A N A L Y S I S R E S U L T S R E P O R T I N G S H E E TL O U I S I A N A S A M P L E I . D . I A05860821-06LABORATORY I . D . I 860821-114______D A T E : 08-21-86

S a m p l e P r e p a r a t i o n M e t h o d 3510______________I f m u l t i p l e m e t h o d s were u s e d , l i s t me thod a n d a n a l y s i sp e r f o r m e d .M E T H O D8270


Were s p i k e s added t o th e s a m p l e , ye s (X) no ( )I f yes, a t what s t a g e ? B e f o r e E x t r a c t i o n


Parameter2 - C h l o r o p h e n o l2-4 D i c h l o r o p h e n o l2-4 D i m e t h y l p h e n o l4-6 D i n i t r o Q - C r e s o l2-4 D i n i t r o p n e n o l2 - N i t r o p h e n o l _ _ _ _ _4 - N i t r o p h e n o l _ _ _ _ _P - C h l o r o - M - C r e s o lP e n t a c h l o r o p h e n o lPhenol_________2-4-6 T r i c h l o r o p h e n o l

S W - 8 4 6T e s tM e t h o d82708270827082708270827082708270827082708270

R e s u l tL a b o r a t o r yD u p l i c a t eR e s u l t( U n i t s ) * ( i f a p p l i c a b l e )

<0.010 _____<0.010<0.010<0.030<0.010<0.050<0.040<0.010<0.010<0.010<0.010

L a b o r a t o r yB l a n k V a l u e( i f a p p l i c a b l e ) '<0.010<0.010<0.010<Q.03Q<0 050<0.010<0.040<0.010<0.010<0.01Q<0.010

S p i k eRecovery( i f a p p l i c a b l e )586754m

1 1 6788281

12747

D e t e c t i o nL i m i t0.0100.0100.010

30

78

0.0100.0400.0100.0100.0100.010

A l l r e s u l t s i n P P M u n l e s s o t h e r w i s e no t ed .M i l l i g r a m s p e r l i t e r . S u r r o g a t e S t d . Recoverv ( < $ )S o i k e d at 100 n p b . " 2 ~ N i t r o n h e n o 1 - d 4 - 36P o n t n c h l b r o n l i p n o l - 5

I N C .7 9 7 9 G S R I A V E . • BATON ROUGE, LA 70808

I c e r t i f y that t h e s a m p l e p r e p a r a t i o n m e t h o d ( s ) a n d a n a l y t i c a l te s t m e t h o d s ( i n c l u d i n g r e q u i s i t e c a l i b r a t i o n p r o c e d u r e s a n df r e q u e n c y , and q u a l i t y c on tro l p r o c e d u r e s ) were tho s e d e s c r i b e d above.

S i g n a t u r e c V T c t o r J . B r a n c h a r d , I I IG e n e r a l M a n a g e rT i t l e


drb

we. L O U I S I A N A A N A L Y S I S R E S U L T S R E P O R T I N G S H E E TL O U I S I A N A S A M P L E 1.0. # A 0 5 8 6 0 8 2 1 - 0 1\^ -̂ /0> .̂ —— ~-7 9 7 9 G S R I A V E . • BATON R O U G E , LA 70806

S a n p l e P r e p a r a t i o n M e t h o dI f m u l t i p l e m e t h o d s werep e r f o r m e d .M E T H O D

8080

L A B O R A T O R Y I . D . # P , f i 0 8 ? 1 - 1 0 9D A T E : n n - ? 1 - f t f i3510u s e d , l i s t method a n d a n a l y s i s

A N A L Y S I S P E R F O R M E DP e s t i c i d e / P C B F r a c t i o n

W e r e s p i k e s a d d e d to the s a m p l e , yes (x ) no ( )If yes, a t what s t a g e ? B e f o r e E x t r a c t i o n


" ' ' 9

ParameterA l d r i n ,A l p h a - B H CB e t a - B H CG a m m a - B H CD e l t a - B H CC h l o r d a n e4 , 4 ' - D D T4 , 4 ' -DDE4 , 4 ' - O D DD i e l d r i nA l p h a - E n d o s u l f a nB e t a - E n d o s u l f a nE n d r i nE n d r i n A l d e h y d e

S W - 8 4 6T e s tM e t h o d8080C080H 0 8 080808080808080808080808080808080808080808080

R e s u l t( U n i t s ) *<0.001<0.001<0.001<0.001<0.001<0.001<0.001<0.001<0.001<0.001<0.001<0.001<0.001<0.001

L a b o r a t o r yD u p l i c a t e L a b o r a t o r y S p i k eR e s u l t B l a n k V a l u e Recovery D e t e c t i o n( i f a p p l i c a b l e ) ( i f a p p l i c a b l e ) ( i f a p p l i c a b l e ) L i m i t0.0010.0010.001o.oj^o.Om0.0010.0010.0010 0010.0010.0010.0010.001

_____ 0.001

p—E S T - P A I N E7 9 7 9 G S R I A V E • BATON ROUGE, LA 70808

ParameterH e p t a c h l o rH e p t a c h l o r E p o x i d ePCB-1242PCB-1254PCB-1221PCB-1232PCB-1248PCB-1260PCB-1016T o x a p h e n e

S W - 8 4 6T e s tM e t h o d808080808080

. 8080808080808080808080808080

R e s u l t( U n i t s ) *<0.001<0.001<0.001<0.001<0.001<0.001<0.001<0.001<0.001<0.001

• L a b o r a t o r yD u p l i c a t eR e s u l t( i f a p p l i c a b l e )Labora t oryB l a n k V a l u e( i f a p p l i c a b l e )


86

D e t e c t i o nL i m i t0.0010.0010.001

J h O O l0.0.0010.0010.0010.0010.001

* A l l r e s u l t s i n P P M u n l e s s o t h e r w i s e n o t e d ,f l i H i grams p e r l i t e r .

I c e r t i f y that t h e s a m p l e p r e p a r a t i o n m e t h o d ( s ) a n d a n a l y t i c a l test m e t h o d s ( i n c l u d i n g r e q u i s i t e c a l i b r a t i o n procedure s a n df r e q u e n c y , and q u a l i t y control p r o c e d u r e s ) were tho s e d e s c r i b e d above.

S i g n a t u r e V i c t o r J . B l a n c h a r d , I I IGenera l M a n a g e r

T i t l e


E S T - P A I N EI N C .7979 GSRI AVE. • BATON R O U G E , LA 70808

L O U I S I A N A A N A L Y S I S R E S U L T S R E P O R T I N G S H E E TL O U I S I A N A S A M P L E I . D . I A 0 5 8 6 0 8 2 1 - 0 2L A B O R A T O R Y I . D . # 860821-110_______D A T E : nP,-?1-86_________

S a m p l e P r e p a r a t i o n M e t h o d 3510I f m u l t i p l e m e t h o d s were u s e d , l i s t m e t h o d a n d a n a l y s i sp e r f o r m e d .M E T H O D8080

A N A L Y S I S P E R F O R M E DP e s t i c i d e s / P C B F r a c t i o n

Were s p i k e s a d d e d t o the s a m p l e , ye s ( ) no (X)If yes, a t what s t a g e ? _______________


Parame t e rA l d r i n .A l p h a - B H CB e t a - B H CG a m r n a - B H CD e l t a - B H CC h l o r d a n e4 , 4 ' - D D T4 , 4 ' - D O E4 , 4 ' - D D DD i e l d r i nA l p h a - E n d o s u l f a nB e t a - E n d o s u l f a nE n d r i nE n d r i n A l d e h y d e

S W - 8 4 6T e s tM e t h o d8080808080808080808080808080808080808080

808080808080

L a b o r a t o r yD u p l i c a t eR e s u l t ' R e s u l t( U n i t s ) * ( i f a p p l i c a b l e )<0.001

L a b o r a t o r yB l a n k V a l u e( i f a p p l i c a b l e )S p i k eRecovery( i f a p p l i c a b l e )

<0.001<0.001<0.001<0.001<0.001<0.001<0.001<0.001<0.001<0.001<0.001<0.001<0.001

D e t e c t i o nL i m i t0.0010.0010.001

0.0010.0010.0010.0010.0010.0010.0010.0010.001

I N C .

Parame t e rH e p t a c h l o rH e p t a c h l o r E p o x i d ePCB-1242P C B - 1 2 5 4P t B - 1 2 2 1PCB-1232PCB-1248PCB-1260PCB-1016T o x a p h e n e

S W - 8 4 6T e s tM e t h o d8080808080808080808080808080808080808080

R e s u l t( U n i t s ) *<0.001<0.001<0.001<0.001<0.001<0.001<0.001<0.001<0.001<0.001

L a b o r a t o r yB l a n k V a l u e( i f a p p l i c a b l e )S p i k eRecovery( i f a p p l i c a b l e ) D e t e c t i o nL i m i t

0.0010.001Tooi0.001

"ol0.0010.0010.0010.0010.001

* A l l r e s u l t s i n P P M u n l e s s o t h e r w i s e n o t e d .M i l l i g r a m s p e r l i t e r .

I c e r t i f y that t h e s a m p l e p r e p a r a t i o n m e t h o d ( s ) a n d a n a l y t i c a l test m e t h o d s ( i n c l u d i n g r e q u i s i t e c a l i b r a t i o n procedf r e q u e n c y , and q u a l i t y c o n t r o l p r o c e d u r e s ) were t ho s e d e s c r i b e d above.

S i g n a t u r e

T i t l e

-nnctor 0 ; B T a r i c h a r d , I I IG e n e r a l M a n a g e r


d r h

•pEST-PAIN EI N C .7 9 7 9 G S R I A V E . • BATON R O U G E , LA 70608

S a m p l e P r e p a r a t i o n M e t h o d

L O U I S I A N A A N A L Y S I S R E S U L T S R E P O R T I N G S H E E TL O U I S I A N A S A M P L E I . D . # A05860821-03L A B O R A T O R Y I . D . # 860821-111________D A T E : 08-21-86

3510____ _I f m u l t i p l e m e t h o d s were u s e d , l i s t method a n d a n a l y s i sp e r f o r m e d .M E T H O D

8080A N A L Y S I S P E R F O R M E D

P e s t i c i d e / P C B F r a c t i o n

W e r e s p i k e s a d d e d to the s a m p l e , yes ( ) no (X )If yes, at what s t a g e ? _____________________D I L U T I O N F A C T O R S A N A L Y S I S

Paramet erA l d r i n .A l p h a - B H CB e t a - B H CG a m m a - B H CD e l t a - B H CC h l o r d a n e4 , 4 ' - D D T4 , 4 ' - D D E4 , 4 ' - D D DD i e l d r i n

S W - 8 4 6T e s tM e t h o d80808080808080808080Of"1. i808080800080808080

A l p h a - E n d o s u l f a n 8080B e t a - E n d o s u l f a n 8080E n d r i n 8080


L a b o r a t o r yB l a n k V a l u e( i f a p p l i c a b l e )S p i k eRecovery( i f a p p l i c a b l e )

E n d r i n A l d e h y d e 8080

<0.001<0.001<0.001<0.001<0.001<0.001<0.001<0.001<0.001<0.001<0.001<0.001<0.001

D e t e c t i o nL i m i t0.0010.0010.001

0.0010.0010.0010.0010.0010.001o.ooi0.0010.001

W E S T - P A I N EI N C -7979GSRIAVE. • BATON R O U G E , LA 70808

L O U I S I A N A A N A L Y S I S R E S U L T S R E P O R T I N G S H E E TL O U I S I A N A S A M P L E I . D . # A 0 5 8 6 0 8 2 1 - 0 1 - 0 6L A B O R A T O R Y I . D . # 860821-109-114________

D A T E : _ _ _ _ 0 8 - 2 1 - 8 6S a m p l e P r e p a r a t i o n M e t h o d _ 3020I f m u l t i p l e me thods were u s e d , l i s t me thod a n d a n a l y s i sp e r f o r m e d .

W e r e s p i k e s added to the s a m p l e , yes ( ) no (If y e s , a t what s t a g e ? ________________

M E T H O D A N A L Y S I S P E R F O R M E D D I L U T I O N F A C T O R S A N A L Y S I S

M e t a l s

P a r a m e t e rAntimony

Q u a l i t y A s s u r a n c e D a t a

A r s e n i cB e r y l l i u mCadmiumChromiumC o p p e rLeadMercuryN i c k e lS e l e n i u mS i l v e rT h a l l i u m

0 . 0 2 5 / 00 . 0 2 5 / 00 . 0 0 5 / 0

0.0010/00.010/00.010/00 . 0 2 5 / 0

0 .0100/00 . 5 0 / 0

0 . 0 2 5 / 00 . 0 0 5 / 00 .010/0

.025

.028

.006

.0012

.008

.008

.026

.0101

.51

.025

.004

.010

D a t e / A n a l y s t0 8 - 2 6 / V M0 8 - 2 7 / V M0 9 - 0 3 / V M0 9 - 0 3 / V M0 8 - 2 5 / F D0 9 - 0 3 / V M0 9 - 0 5 / V M0 8 - 2 5 / F D0 8 - 2 7 / F D0 8 - 2 6 / F D0 9 - 0 2 / F D -0 9 - 0 2 / V M

•pE S T - P A I N EI N C .7 9 7 9 G S R I A V E . « BATON ROUGE. LA 70808

ParameterZincBarium

Q u a l i t y Assuranc e Data0 . 2 5 0 / 0 . 2 4 8

2 . 5 0 / 2 . 5 00 8 - 2 5 / F D0 8 - 2 7 / F D

•pE S T - P A I N E7 9 7 9 G S R I A V E . • B A T O N R O U G E . L A 70808

L O U I S I A N A A N A L Y S I S R E S U L T S R E P O R T I N G S H E E TL O U I S I A N A S A M P L E I . D . # A05860821-01_____L A B O R A T O R Y I . D . # 860821-109____________

D A T E : _____08-21-86S a m p l e P r e p a r a t i o n M e t h o d 3020I f m u l t i p l e m e t h o d s were u s e d , l i s t me thod a n d a n a l y s i sp e r f o r m e d .

W e r e s p i k e s a d d e d to the s a m p l e , yes ( ) no (X;If y e s , a t what s t a g e ? ________________


S e e Below M e t a l s

Parame t erA n t i m o n yA r s e n i cB e r y l l i u mC a d m i u mChromiumC o p p e rLeadM e r c u r yN i c k e lS e l e n i u mS i l v e r

S W - 8 4 6T e s t

M e t h o d7041706070917191

T h a l l i u m 7841

R e s u l t s( U n i t s ) *<0.01<0.01<0.001<0.001

0.004<0.001<0.005<0.0002<0.03<0.01<0.001<0.005

L a b o r a t o r yD u p l i c a t e

Result( i f a p p l i c a b l e )

L a b o r a t o r yBlank V a l u e

( i f a p p l i c a b l e )S p i k e

Recovery( i f a p p l i c a b l e )

D e t e c t i o iL i m i t

010.0010.0010.0010.0010.0050.00020.030.010.0010.005

pW E S T - P A I N EI N C .7 9 7 9 G S R I A V E . • BATON R O U G E , LA 70808

ParameterZ i n cBaritun

S W - 8 4 6T e s t

M e t h o d79507080

R e s u l t s( U n i t s ) *

0.006


R e s u l t( i f a p p l i c a b l e )

LaboratoryBlank V a l u e



D e t e c t i o iL i m i t

0.005

* All r e s u l t s in PPM unle s s o th erw i s e n o t e d .M i l l i g r a m s o f m e t a l / l i t e r .

I c e r t i f y that t h e s a m p l e p r e p a r a t i o n m e t h o d ( s ) a n d a n a l y t i c a l t e s t m e t h o d s ( i n c l u d i n g r e q u i s i t e c a l i b r a t i o n p r o c e d u r e sf r e q u e n c y , and q u a l i t y control p r o c e d u r e s ) were tho s e d e s c r i b e d above.

S i g n a t u r e V i c t o r J . B l a n c h a r d , I I I

_____General ManagerT i t l e

S a m p l e I d e n t i f i c a t i o n ( L o u i s i a n a D N R ) . A 0 5 8 6 0 8 2 1 - 0 1

•pE S T - P A I N EI N C .7979GSRIAVE. • BATON R O U G E . LA 70808

L O U I S I A N A A N A L Y S I S R E S U L T S R E P O R T I N G S H E E TL O U I S I A N A S A M P L E I . D . # A 0 5 8 6 0 8 2 1 - 0 2 _ _ _ _ _L A B O R A T O R Y I . D . # 860821-110_________

D A T E : _____08-21-86___________S a m p l e P r e p a r a t i o n M e t h o d 3020I f m u l t i p l e me thod s were u s e d , l i s t method a n d a n a l y s i sp e r f o r m e d .

W e r e s p i k e s added to the s a m p l e , yes ( ) no (X x

If ye s , a t what s t a g e ? ________________



Paramet erA n t i m o n yA r s e n i cB e r y l l i u mC a d m i u mChromiumC o p p e rLeadMercuryN i c k e lS e l e n i u mS i l v e r

S W - 8 4 6T e s t

M e t h o d

T h a l l i u m


<0.01<0.01<0.001<0.001

0.0060.009

<Q.OQ5<0.0002

0.03<0.01<0.001<0.005






D e t e c t i o : |Limit

. 01

0.0010.0010.0010.0050.000?!0.030.010.0010.005

7979GSRIAVE. • BATON R O U G E , LA 70808

ParameterZincBarium

S W - 8 4 6T e s t

M e t h o d7950


0.027080 <0.1



Labora t oryBlank V a l u e



D e t e c t i o tL i m i t

0.005

* All r e s u l t s in PPM unle s s o th erwi s e n o t e d .M i l l i g r a m s o f m e t a l / l i t e r .

I c e r t i f y that th e s a m p l e p r e p a r a t i o n m e t h o d ( s ) and a n a l y t i c a l t e s t m e t h o d s ( i n c l u d i n g r e q u i s i t e c a l i b r a t i o n p r o c e d u r e sf r e q u e n c y , and q u a l ' i t y control p r o c e d u r e s ) were tho s e d e s c r i b e d above.

S i g n a t u r e < ^ x ' V i c ' t o i r J ^ , I I I

General M a n a g e rT i t l e


•pE S T - P A I N E'o6ot,atotieA I N C .7 9 7 9 G S R I A V E . • BATON R O U G E , LA 70808

L O U I S I A N A A N A L Y S I S R E S U L T S R E P O R T I N G S H E E TL O U I S I A N A S A M P L E I . D . # A 0 5 8 6 0 8 2 1 - 0 3 _ _ _ _ _L A B O R A T O R Y I . D . # 860821-111_________

D A T E : _____08-21-86_____________S a m p l e P r e p a r a t i o n M e t h o d 3020I f m u l t i p l e me thods were u s e d , l i s t method a n d a n a l y s i sp e r f o r m e d .

W e r e s p i k e s added to the s a m p l e , yes ( ) no (XIf y e s , a t what s t a g e ? _______________



ParameterA n t i m o n yA r s e n i cB e r y l l i u mC a d m i u mChromiumC o p p e rLeadMercuryN i c k e lS e l e n i u mS i l v e r

S W - 8 4 6T e s t

M e t h o d70417060

7421747075207740

T h a l l i u m

R e s u l t s( U n i t s ) *<0.01<0.01<O.OQ1<O.Q01

0.0040.007

<0.005<O.OOQ2<0.03<0.01<0.001

...<0.025*


Resu l t( i f a p p l i c a b l e )




D e t e c t i oLimit

0.0010.001Q.. 0010.0050.00020.030.01

..0.001

..0.025* M a t r i x E f f e c t

•pE S T - P A I N E7 S 7 9 G S R 1 A V E . • B A T O N R O U G E , L A 70808

ParameterZinc • *-Barium

S W - 8 4 6T e s t

M e t h o d79507080


0.020.10

* All r e s u l t s in PPM u n l e s s o t h e r w i s e n o t e d .M i l l i g r a m s o f m e t a l / l i t e r .


Resu l t( i f a p p l i c a b l e )




D e t e c t i o nLimi t

I c e r t i f y that t h e s a m p l e p r e p a r a t i o n m e t h o d ( s ) a n d a n a l y t i c a l t e s t m e t h o d s ( i n c l u d i n g r e q u i s i t e c a l i b r a t i o n p r o c e d u r e s :f r e q u e n c y , and q u a l i t y control p r o c e d u r e s ) were tho s e d e s c r i b e d above. !

S i g n a t u r e V I r & t o r J . B l a n c h a r d , I I I

Genera l M a n a g e rT i t l e



L O U I S I A N A A N A L Y S I S R E S U L T S R E P O R T I N G S H E E TL O U I S I A N A S A M P L E I . D . # A05860821-04_____L A B O R A T O R Y I . D . # 860821-112_________

D A T E : _____08-21-86____________S a m p l e P r e p a r a t i o n M e t h o d 3020I f m u l t i p l e me thod s were u s e d , l i s t me thod a n d a n a l y s i sp e r f o r m e d .

W e r e s p i k e s a d d e d to the s a m p l e , yes ( ) no (XIf y e s , a t what s t a g e ? _________________



ParameterA n t i m o n yA r s e n i cB e r y l l i u mC a d m i u mChromiumC o p p e rLeadM e r c u r yN i c k e lS e l e n i u mS i l v e rT h a l l i u m

S W - 8 4 6T e s t

M e t h o d704170607091713171917211742174707520774077617841


<0.01<0.01<0.001<0.001

0.004<0.001<0.005<0.0002<0.03<0.01<0.001<0.005






D e t e c t i oL i m i t

o.ooi0.0010.0010.0050.00020.030.010.0010.005

•pE S T - P A I N EI N C .7 9 7 9 G S R I A V E . • BATON R O U G E . LA 70806

ParameterZincBarium

S W - 8 4 6T e s t

M e t h o d79507080


0.09






D e t e c t i o tL i m i t

0.005

* All r e s u l t s in PPM unle s s o t h e r w i s e n o t e d .M i l l i g r a m s o f m e t a l / l i t e r .

I c e r t i f y that the s a m p l e p r e p a r a t i o n m e t h o d ( s ) and ana ly t i ca l t e s t methods ( i n c l u d i n g requisite ca l i b ra t i on procedure sf r e q u e n c y , and q u a l i t y control p r o c e d u r e s ) were tho se d e s c r i b e d above.

S i g n a t u r e V f e t o r " j T s f a n c h a r d , I I I

Genera l ManagerT i t l e

S a m p l e I d e n t i f i c a t i o n (Loui s iana D N R ) . A 0 5 8 6 0 8 2 1 - 0 4

•pW E S T - P A I N E'a6otatotieA I N C .7 9 7 9 G S R I A V E . • BATON R O U G E , LA 70808

L O U I S I A N A A N A L Y S I S R E S U L T S R E P O R T I N G S H E E TL O U I S I A N A S A M P L E I . D . # A 0 5 8 6 0 8 2 1 - 0 5 _ _ _ _ _L A B O R A T O R Y I . D . # 860821-113__________

D A T E : _____08-21-86 ______________S a m p l e P r e p a r a t i o n M e t h o d 3020I f m u l t i p l e m e t h o d s were u s e d , l i s t me thod a n d a n a l y s i sp e r f o r m e d .

W e r e s p i k e s a d d e d to the s a m p l e , yes (X) no (I f y e s , a t what s t a g e ? A f t e r d i g e s t i o n



P a r a m e t e rA n t i m o n yA r s e n i cBeryl l iumCadmiumChromiumC o p p e rLeadMercuryN i c k e lS e l e n i u mS i l v e rT h a l l i u m

S W - 8 4 6T e s t

M e t h o d704170607091713171917211742174707520774077617841

R e s u l t s( U n i t s ) *<0.01<0.01<0.001<Q.OQ1

0.0030.015

<0.005<0.0002<0.03<0.01<0.001<0.005






<0.002 80 %

D e t e c t i cL i m i t

OJ0.0010.0010.0010.0010.0050.0000.030.010.001. 0.00 5

•pW E S T - P A I N EI N C .7979GSRIAVE. • BATON R O U G E . LA 70808

Paramet erZ i n cBarium,

S W - 8 4 6T e s t

M e t h o d7950


0.027080 <0.1

L a b o r a t o r yD u p l i c a t e ^





D e t e c t i o nLimi t

0.005

* All r e s u l t s in PPM unles s o th erwi s e n o t e d .M i l l i g r a m s o f m e t a l / l i t e r .

I c e r t i f y that t h e s a m p l e p r e p a r a t i o n m e t h o d ( s ) a n d a n a l y t i c a l t e s t m e t h o d s ( i n c l u d i n g r e q u i s i t e c a l i b r a t i o n p r o c e d u r e sf r e q u e n c y , and q u a l i t y control p r o c e d u r e s ) were tho s e d e s c r i b e d above.

S i g n a t u r e V i c t o r J . Blanchard, I I I

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I c e r t i f y t h a t t h e s a m p l e p r e p a r a t i o n m e t h o d ( s ) a n d a n a l y t i c a l t e s t m e t h o d s ( i n c l u d i n gr e q u i s i t e c a l i b r a t i o n p r o c e d u r e s a n d f r e q u e n c y , a n d q u a l i t y c o n t r o l p r o c e d u r e s ) weret h o s e d e s c r i b e d above.

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I c e r t i f y t ha t t h e s a m p l e p r e p a r a t i o n m e t h o d ( s ) a n d a n a l y t i c a l t e s t m e t h o d s ( i n c l u d i n gr e q u i s i t e c a l i b r a t i o n p r o c e d u r e s a n d f r e q u e n c y , a n d q u a l i t y c o n t r o l p r o c e d u r e s ) weret h o s e d e s c r i b e d above.

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1 c e r t i f y t h a t t h e s a m p l e p r e p a r a t i o n m e t h o d ( s ) a n d a n a l y t i c a l t e s t n e th c -d s ( U i d u d ir e q u i s i t e c a l i b r a t i o n p r o c e d u r e s a n d f r e q u e n c y , a n d q u a l i t y c o n t r o l p r o c e d u r e s ) woret h o s e d e s c r i b e d above.

S i g n a t u r e V i c t o r , J . B l a n c h a r d , I I IG e n e r a l ? i a r i a f « e r

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00134 - United States Environmental Protection Agency · 2019. 12. 15. · 00134 143950. louisiana...

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Transcript of 00134 - United States Environmental Protection Agency · 2019. 12. 15. · 00134 143950. louisiana...