semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II...

303
0001 AUXIER & ASSOCIATES, INC. West Lake NCC ST AND ARD LEVEL IV REPORT OF ANALYSIS WORK ORDER #18-03111-OR May 11, 2018 EBERLINE ANALYTICAL/OAK RIDGE LABO RA TORY OAK RIDGE, TN

Transcript of semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II...

Page 1: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0001

AUXIER & ASSOCIATES, INC.

West Lake NCC

ST AND ARD LEVEL IV REPORT OF ANALYSIS

WORK ORDER #18-03111-OR

May 11, 2018

EBERLINE ANALYTICAL/OAK RIDGE LABO RA TORY

OAK RIDGE, TN

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0002

TABLE OF CONTENTS

SECTION DESCRIPTION PAGE

I Chain of Custody 0004

II Sample Acknowledgement 0009

III Case Narrative 0012

IV Analytical Results Summary 0016

V Analytical Standards 0019

VI Quality Control Sample Results Summary 0037

VII Laboratory Technician's Notes 0044

VIII Analytical Data (Isotopic Uranium) 0060

IX Analytical Data (Isotopic Thorium) 0100

X Analytical Data (Gamma Spectroscopy) 0140

Last Page 0303

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0003

Ea STANDARD OPERATING PROCEDURE INE

Sample Receiving

LABORATORY DATA SUPPORT CHECKLIST

MP-001-3

Eberline Services Work Order # ___ ...... l_a_-~0~3~1~1 _1 ____ _ The checklist items listed below are to be initialed by appropriate staff upon completion/verification.

Date for Partial Initials Date Initials Checklist Items

.s~,J.J-/t ~~ Sample Log-In

lJ//1/;[3 t{tJh Data Compilation

</✓1,t✓/0 ✓-~,;-,,_7 First Technical Data Review

MP-001, Rev. 19 Effective: 2111/18

Page 14 of 15

J-11

1\<(\\,£ 2~ Second Technical Data Review

~I \

Data Entry/Electronic Deliverable G & L) I I )j Case Narrative 5 e, ,e,

,:;]~ I~ 9;1tl /fj '-!(pl /2 Electronic Deliverable Proof

sl,o/,·t. Of&X Samples Analyzed within Holding Time Yes? 1 Y I No?I I

I , r / V iJ)- QA/QC~e~iew 5 110 I 'r I/ - ff:_.~ .• -- Client in Possession of Data

Electronic or Hard Con"

Invoiced by Laboratory

Technical/Clerical Corrections, Signatures Needed, Problems, Etc Date/Initials

Date package approved by: _{;-;, 1 ( Co

Laboratory Manager Date

Copy No. ___ _ Radiochemistry Services

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0004

SECTION I

CHAIN OF CUSTODY

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0005

Chain of ust y Record ~ ~

NO 001 ~ ~ - --------- 0.il( Ridge, TN 37830 EBERLINE

S!!:RV!Cl!:5

- ·-. Project Name: WUr ~ JJtc.- Project Number: E. PA t-u{,'w..,.~ ~I;.}- jfj:/il I I I I I I I I Send Report To: p~ ~&rw Sampler (Pnnt Name):.'1:_ UJl\~..,_ PagLL01_l_

/liti!lt / I , /R~'f M,AR/2 3 2018 Address: GtM:Z: Sampler (Print Name):

Shipment Method: F d ~ 1- I 1/ I / 1 , /~ I ~ - . 1 I I /1~ r ' 1 1 Airbil! Number -=1-:r,e 'OU,i KM ~1 i / I I / I / / Pocchase Phone: laboratory Receiving: , ~ ~ / I / I , I Order ii·

Fax: /~ I I I I I I Sample ! Sample I Sample Number o! / J / I Comments, Speaal Lab Sample ID

l Field Sample 10 ,/ t!J I,;;;, I 1 / / Instructions, etc. I Date I T,me Matrn, Containers (to be romple!ed by lab)

Ae-_j~h- H 1-\ c :}id 1.i 13to &;1 1 ~ '£, ~ I

I

.

l Relinquished by: (Signature) Received by: (Signature) Date: Time: Sample Custodian Remarks (Completed By laboratory):

iJ~~ /Ft;r f'-qti.,:,. .ria/,s 111:o QA/QC level Turnaround Sample Receipt

'l)Feliflquished by: (Signature) ~~by;;;f~ Date: Time: Total# Containers Received?

' Level I 0 Routine O COC Seals Present? _y~·/f il{;tJ Level l! D 24 Hour • GOC Seals intact?

Relinquished by: (Signature) L,/ ,,l'leceiv~tur. Date: Time: Level 111 0 1 Week 0 Received Containers Intact? Other 0 Other -- Temperature?

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0006

EBERLINE SEnv,c:ES

Oak Ridge Laboratory

Internal Chain of Custody

Comments

REPORT ON DRY WEIGHT BASIS.

Location (circle one

Received by ~ ~oughj~p Prep Separations

,,,-. ...----'""'.,\

Relinquished by Sample Storage Rough Prep Prep Separations

Received by Sample Storage Rough Prep Separations

Relinquished by Sample Storage Rough Prep Separations

Received by Sample Storage Rough Prep ~

Relinquished by Sample Storage Rough Prep Prep ~

Received by Sample Storage Rough Prep Prep Separations

Relinquished by Sample Storage Rough Prep Prep Separations

Received by s[~e~~) Rough Prep Prep Separations

Relinquished by Sample Storage Rough Prep Prep Separations

Received by Sample Storage Rough Prep Prep Separations

Relinquished by Sample Storage Rough Prep Prep Separations

Received by Sample Storage Rough Prep Prep Separations

Relinquished by Sample Storage Rough Prep Prep Separations

Work Order#

Lab Deadline

Analysis

Sample Matrix

Sample Fraction

04

Count Room /(30

Count Room o)1S

Count Room

Count Room

Count Room

Count Room

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Count Room

Count Room

Count Room

I

18-03111 4/12/2018

UUISO - Level 4 Soil/Solid

HP 210 / 270 Storage Detector Activity i Location

63 :

Ll.3

Initials Date

\["", ')(./ Jl {I

(,<_? ·~11c:l18 o'1,SD )Cb :s/ao h 9 \ lQ.oo

Printed: 3/23/2018 4.51 PM

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0007

( . .r.;-J\ EBER ~.1,,Nv, _EE···, @ -.. >i......... \ (_, _,_,

· Oak Ridge Laboratory

Internal Chain of Custody

Comments

REPORT ON DRY WEIGHT BASIS.

-l..Pcation (circle one)

Received by )

Rough Prep Prep Separations

Relinquished by Sample Storage

,.;,,:='~ b~p Prep Separations

Received by Sample Storage Rough Prep ~ Separations

Relinquished by Sample Storage Rough Prep Q/_ Separations

Received by Sample Storage Rough Prep Prep

Relinquished by Sample Storage Rough Prep Prep

Received by Sample Storage Rough Prep Prep Separations

Relinquished by Sample Storage Rough Prep Prep Separations

Received by Rough Prep Prep Separations

Relinquished by Sample Storage Rough Prep Prep Separations

Received by Sample Storage Rough Prep Prep Separations

Relinquished by Sample Storage Rough Prep Prep Separations

Received by Sample Storage Rough Prep Prep Separations

Relinquished by Sample Storage Rough Prep Prep Separations

Work Order#

Lab Deadline

Analysis

Sample Matrix !

Sample ! Fraction

04

' '

i

'

18-03111 4/12/2018

ThlSO - Level 4 Soil/Solid

HP 210 / 270 '

Storage Detector Activity Location

63 Ll.3

Initials

Count Room f /?.Jb ~~ s tf\ Count Room

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Printed: 3/2312018 4:51 PM

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0008

. EB ER~.~<~-~

· Oak Ridge Laboratory

Internal Chain of Custody

Comments

REPORT ON DRY WEIGHT BASIS.

21 day ingrowth - Report Ac228, Bi214, K40, Pa231, Pb210/212/214, Ra226 from Bi214, Ra228 from Ac228,Tl208 &

Th234.

Location (circle one)

~ ,/ ·,

Received by ~~p Prep Separations

(;···---, Relinquished by Sample Storage Rough Prep Prep Separations

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e,am~l~~orag_~ Rough Prep Prep Separations

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Received by Sample Storage Rough Prep Prep Separations

Relinquished by Sample Storage Rough Prep Prep Separations

Received by Sample Storage Rough Prep Prep Separations

Relinquished by Sample Storage Rough Prep Prep Separations

Received by Sample Storage Rough Prep Prep Separations

Relinquished by Sample Storage Rough Prep Prep Separations

Received by Sample Storage Rough Prep Prep Separations

Relinquished by Sample Storage Rough Prep Prep Separations

Work Order#

Lab Deadline

Analysis

Sample Matrix

Sample Fraction

04

Count Room // 50

Count Room al ~-s ~o/ eun~~~~"

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18-03111 4/12/2018

Gamma - Level 4 Soil/Solid

1 HP 210 / 270 Storage

Location : Detector Activity :

63 Ll.3

Initials Date

v(1 ) (rj j).J, ( y

h~,., St.1 3, )7,l Y

{r ~ /z;~/28 o[3ec5J 1;p 4/21As dtlcf&

Printed: 3123/2018 4:51 PM

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0009

SECTION II

SAMPLE ACKNOWLEDGEMENT

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0010

Client Name Contract/PO Project Type Date Received Required Turnaround Days .. . ln.u:..i

Auxier & Associates, Inc. WESTLAKE NCC Environmental 03/23/2018 28 18-03111 Project Name Client WO Sample Disp Lab Deadline Internal Deadline I .• •

WESTLAKE NCC WESTLAKE NCC SOIL H 04/12/2018 04/19/2018 04/20/2018 "' 0 0 E

Internal ID Client ID Sample Date Matrix Storage E CJ) CJ) i'='.

"' .c ::J c:J f- ::J

01 LCS 03/23/18 so Ll.3 X X X 3

02 BLANK 03/23/18 so Ll.3 X X X 3

03 DUP 03/23/18 so Ll.3 X X X J

04 AC-SED-11 03/21/18 13:20 so Ll.3 X X X J'

• 0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

Totals Per Analysis (non QA samples) 1 1 1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0

Invoice Accounts Payable Report Data Cecilla Greene

( Auxier & Associates. Inc. Auxier & Associates, Inc

Oak Ridge Laboratory 9821 Cogdill Drive #1 9821 Cogdrl! Road, Suite 1 . EBERLINE 601 Scarboro Rd. Knoxville. TN 37932 Knoxville, TN 37932

~ SERVICES Oak Ridge, TN 37830 Voice 865-675-3669 Voice 865-675-3669

Sample Log In Report Voice: (865) 481-0683 Fax 865-675-3677 Fax 865-675-3677

Fax: (865) 483-4621 Contact Paul Rosasco P E

Voice 303-940-3426

Fax

Printed 3/2312018 4 51 PM

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0011

STANDARD OPERATING PROCEDURE MP-001, Rev. 19 Effective: 2111/18

Page 13 of 15 Sample Receiving

SAMPLE RECEIPT CHECKLIST MP-001-2

WORKORDER#_1 __ 8~--Q~3_1_1_1_ SAMPLE MATRIX/MATRICES:

WERE SAMPLES:

Received in good condition?

If aqueous, properly preserved

WERE CHAIN OF CUSTODY SEALS:

Present on outside of package?

Unbroken on outside of package?

Present on samples?

Unbroken on samples?

Was chain of custody present upon sample receipt?

(CIRCLE ONE OR BOTH)

AQUEOUS c:::::§-AQUEOUS ~ (CIRCLE EITHER YES, NO, ORN/A)

N

y N

Ct> N

~ N

0? N

~ N

(-) N

IF THE RESPONSE TO ANY OF THE ABOVE IS NO, A DISCREPANT SAMPLE RECEIPT REPORT

(DSR) HAS BEEN ISSUED.

REMARKS: ___________________________ _

SIGNA~~ DATE: J~23;-l,Y

Copy No. ___ _ Radiochemistry Services

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0012

SECTION III

CASE NARRATIVE

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0013

EBERLINE

~ EBS-OR-43705

May 11, 2018

Cecilia Greene

SERVICES

Auxier & Associates, Inc. 9821 Cogdill Road #1 Knoxville, TN 37932

SAMPLE RECEIPT

CASE NARRATIVE Work Order# 18-03111-OR

EBERLINE ANALYTICAL C0RF'0f(ATI0~1

601 SCARBOFW R01\ll

OAK RIDGE. TENNESSEE rn:so PHONE (865) L,81--0685

FAX (865) 483-L,621

This work order contains one soil sample received 03/23/2018. Sample was analyzed for Isotopic

Uranium, Thorium-230 and Gamma Spectroscopy.

CLIENT ID

AC-SED-11

ANALYTICAL METHODS

LAB ID

18-03 111-04

Isotopic Uranium was analyzed using EPA Method 908.0 Modified. Thorium-230 was analyzed using

EPA Method 907.0 Modified. Gamma Spectroscopy was performed using EPA Method 901.1 Modified.

ANALYTICAL RES UL TS

Combined Standard Uncertainty is reported at I-sigma value.

Minimum Detectable Activity (MDA) values for data represented in this report are sample-specific.

MDA measurements are determined based on factors and conditions including instrument settings, aliquot

size and matrix type.

SPECIAL CIRCUMSTANCES

Results are reported on a "dry weight" basis.

ISOTOPIC URANITJM

Sample was prepared by removing a representative aliquot followed by mixed acid digestions as

appropriate. Uranium was selectively extracted by ion exchange. Uranium was eluted, micro-precipitated

and mounted on micro-porous filter media. Sample activities were then determined by alpha spectroscopy

using energy specific regions of interest for Uranium-234, Uranium-235 and Uranium-238. Chemical

recovery was determined by the use of a Uranium-232 tracer. Activity of the Uranium-232 tracer was

determined by alpha spectroscopy using an energy specific region of interest.

Page 1 of 3

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0014

ANALYTICAL RESULTS CONTINUED

ISOTOPIC URANIUM CONTINUED

Sample demonstrated acceptable results for all Uranium analyses. Chemical recovery was acceptable for

all samples. The Uranium-234, Uranium-235 and Uranium-238 method blank demonstrated acceptable

results. Results for the Uranium-234 and Uranium-235 duplicate demonstrated a high relative percent

difference; however, normalized difference is within acceptable limits for the analytical technique.

Results for the Uranium-238 duplicate demonstrated an acceptable relative percent difference and

normalized difference. Results for the Uranium-234 and Uranium-238 laboratory control sample

demonstrated an acceptable percent recovery.

THORIUM-230

Sample was prepared by removing a representative aliquot followed by mixed acid digestions as

appropriate. Thorium was selectively extracted by ion exchange. Thorium was eluted, micro-precipitated

and mounted on micro-porous filter media. Sample activities were then determined by alpha spectroscopy

using energy specific regions of interest for Thorium-230. Chemical recovery was determined by the use

of a Thorium-229 tracer. Activity of the Thorium-229 tracer was determined by alpha spectroscopy using

an energy specific region of interest.

Sample demonstrated acceptable results for all Thorium-230 analyses. Chemical recovery was acceptable

for all samples. The Thorium-230 method blank demonstrated acceptable results. Results for the

Thorium-230 duplicate demonstrated an acceptable relative percent difference and normalized difference.

Results for the Thorium-230 laboratory control sample demonstrated an acceptable percent recovery.

GAMMA SPECTROSCOPY

Sample was dried, homogenized and placed into an appropriate gamma spectroscopy geometry container.

Sample was then sealed for 21 days to allow for ingrowth of Radon-222 and progeny. Sample was

counted on High Purity Gennanium (HPGe) gamma ray detectors. Energy lines from Lead-214 and

Bismuth-214 were analyzed for determinations of Radium-226 activity.

Sample demonstrated acceptable results for all gamma-emitting radionuclides as reported. The method

blank demonstrated acceptable results for all radionuclides as reported. Results for the Actinium-228,

Bismuth-214 and Potassium-40 replicate demonstrated an acceptable relative percent difference and

normalized difference. Results for the Cobalt-60 and Cesium-137 laboratory control sample demonstrated

an acceptable percent recovery.

Page 2 of 3

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0015

CERTIFICATION OF ACCURACY

I certify that this data report is in compliance with the terms and conditions of the Purchase Order, both

technically and for completeness, for other than the conditions detailed above. Release of the data

contained in this hard copy data package has been authorized by the cognizant project manager or his/her

signee to be accurate as verified by the following signature.

~;#?..(_,,.(_

M.R. McDougaff--­Laboratory Manager

Date: 5/1I/2018 \

Eberline Analytical wants and encourages your feedback regarding our performance providing radioanalytical services. Please

visit http://cberlineanalytical.com/ to provide us with feedback on our services.

Page 3 of 3

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0016

SECTION IV

ANALYTICAL RESULTS SUMMARY

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0017

Printed: 5/11/2018 9:48 AM Page 1 of 2

Report To: Work Order Details:

Eberline Analytical Cecilia Greene SOG.· 18-03111 "~•·

Auxier & Associates, Inc. Project_ WEST LAKE NCC

Final Report of Analysis r---,- '"""~ ~,,,,,,,, __________ ._ ------ ·--·· ,,,,,,,,_,,__,,

9821 Cogdill Road, Sui!~__:1 Analysis Category: ENVIRONMENTAL

Knoxville, TN 37932 Sample Matrix: so Lab i Sample Client Sample Receipt Analysis Batch Report

ID Type ID Date Date Date ID Analyte Method I Result cu CSU MDA CV

Units

18-03111-01 LCS I KNOWN 03/23/18 00:00 3/23/2018 I 4/17/2018 l 18~03111 Cobalt-60 EPA 901.1 Modified I 1.35E+02 5.27E+00 pCi/g --,-- _,,_,_, ___

18-03111-01 ' LCS i KNOWN 03/23/18 00:00 3/23/2018 4/17/2018 18-03111 Cesium-137 EPA 901.1 Modified 8.44E+01 3.38E+00 pCi/g

··-----·-~·- ~~•"~"""" •••••••••~~~ -•·~···--···

18-03111-01 LCS '

SPIKE 03/23/18 00:00 3/23/2018 4/17/2018 18-03111 Cobalt-60 EPA 901.1 Modified ; 1.32E+02 8.11E+00 1.06E+01 9.45E-01 8.10E-01 pCi/g

------- -· --18-03111-01 LCS SPIKE 03/23/18 00:00 3/23/2018 4/17/2018 18-03111 Cesium-137 EPA 901.1 Modified ' 8.31E+01 7.72E+00 8.82E+00 1.27E+00 6.30E-01 pCi/g

,, __ ____ , ----·--:

i I

•m•~••'-•"•"••~•--•,,,,,_,,,_,,,_m">••-• ,_,, ,,,,,_,, ...

18-03111-02 MBL BLANK 03/23/18 00:00 3/23/2018 4/17/2018 . 18-03111 Actinium-228 EPA 901.1 Modified : 9.58E-03 2.20E-02 2.20E-02 9.02E-02 3.86E-02 pCi/g

18-03111-02 MBL I

BLANK 03/23/18 00:00 3/23/2018 4/17/2018 ' 18-03111 Bismuth-214 EPA 901.1 Modified I

2.99E-02 4.01E-02 4.01E-02 6.90E-02 3.17E-02 pCi/g I

18-03111-02 MBL BLANK 03/23/18 00:00 : 3/23/2018 4/17/2018 18-03111 Potassium-40 EPA 901.1 Modified . 1.62E-01 1.S0E-01 1.S0E-01 3.39E-01 1.45E-01 pCi/g

-·~-~--<-••-,,·--- ·····•···-" 18-03111-02 MBL BLANK 03/23/18 00:00 3/23/2018 4/17/2018 I 18~03111 Protactinium-231 EPA901.1 Modified -4.91E-01 5.96E-01 5.97E-01 7.86E-01 3.60E-01 pCi/g

18-03111-02 MBL i BLANK 03/23/18 00:00 3/23/2018 4/17/2018 : 18-03111 I Lead-210 EPA 901.1 Modified 3.72E-01 3.67E-01 3.67E-01 5.55E-01 2.62E-01 pCi/g

18-03111-02 MBL I BLANK 03/23/18 00:00 3/23/2018 4/17/2018 18-03111 Lead-212 EPA 901.1 Modified 4.19E-02 2.44E-02 2.45E-02 4.68E-02 2.19E-02 pCi/g

-----•-·-· ... ,,,,,,,,,_,,, ____ ~--

18-03111-02 : MBL BLANK 03/23/18 00:00 3/23/2018 4/17/2018 18-03111 Lead-214 EPA 901.1 Modified 2.52E-02 3.78E-02 3.78E-02 6.34E-02 2.94E-02 , pCi/g

·----- ·-18-03111-02 • MBL BLANK 03/23/18 00:00 3/23/2018 41rn2018 - 18-03111 1 Radium-226 EPA 901.1 Modified 2.99E-02 4.01E-02 4.01E-02 6.90E-02 3.17E-02 : pCi/g

18-03111-02 MBL ' BLANK 03/23/18 00:00 3/23/2018 4/17/2018 ; 18~03111 I Radium-228 EPA 901.1 Modified 9.58E-03 2.20E-02 2.20E-02 9.02E-02 3.86E-02 pCi/g

18-03111-02 MBL BLANK 03/23/18 00:00 3/23/2018 4/17/2018 18-03111 Thorium-234 EPA 901.1 Modified 1.08E+00 3.97E-01 4.01E-01 6.57E-01 3.15E-01 pCi/g

18-03111-02 MBL BLANK 03/23/18 00:00 : 3/23/2018 4/17/2018 , 18-03111 I Thallium-208 EPA 901.1 Modified I

-5.60E-03 5.22E-02 5.22E-02 1 7.99E-02 3.58E-02 pCi/g

' I

18-03111-03 i DUP AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 18-03111 I Actinium-228 EPA 901.1 Modified 8.74E-01 2.34E-01 ' 2.38E-01 3.52E-01 1.63E-01 i pCi/g

18-03111-03 I ' AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 18-03111 Bismuth-214 EPA 901.1 Modified 1.06E+00 1.93E-01 2.00E-01 2.46E-01 1.17E-01 I pCi/g

DUP I I

18-03111-03 ; DUP AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 18-03111 ; Potassium-40 EPA 901.1 Modified 1.60E+01 2.13E+00 ' 2.28E+00 1.15E+00 5.25E-01 '

pCi/g __________ ,.

18-03111-03 i DUP AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 18-03111 i Protactinium-231 EPA 901.1 Modified 1.37E+00 : 1.41E+00 1.41E+00 3.33E+00 2.70E+00 pCi/g

18-03111-03 • DUP AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 i 18-03111 ; Lead-210 EPA 901.1 Modified 2.10E+00 1.33E+00 1.33E+00 2.15E+00 ' 1.04E+00 pCi/g

18-03111-03 DUP AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 18-03111 I Lead-212 EPA 901.1 Modified 1.44E+00 2.66E-01 ' 2.76E-01 2.35E-01 1.15E-01 pCi/g

1a-03111-03 l DUP AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 ; 18-03111 I Lead-214 EPA901.1 Modified 1.13E+00 1.98E-01 2.06E-01 2.42E-01 1.16E-01 pCi/g

18-03111-03 i DUP ' AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 I 18-03111 , Radium-226 EPA901.1 Modified 1.06E+00 1.93E-01 2.00E-01 2.46E-01 1.17E-01 pCi/g

18-03111-03 DUP AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 18-03111 Radium-228 EPA 901.1 Modified 8.74E-01 2.34E-01 2.38E-01 3.52E-01 ; 1.63E-01 pCi/g -18-03111-03 DUP I AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 1 18-03111 Thorium-234 EPA 901.1 Modified 1.72E+00 1.49E+00 1.49E+00 1 2.05E+00 1.00E+00 ' pCi/g

18-03111-03 I DUP AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 18-03111 ! Thallium-208 EPA 901.1 Modified 7.74E-01 1.68E-01 1.73E-01 1.34E-01 1.82E-01 pCi/g

CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample; MBL=Slank; DUP=Duplicate; TRG=Normal Sample; DO=Duplicate Original; CV=Critical Value

( . EBERLINE _@ ANALYTiCAL

EBERLINE CAL CORPORATION

601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

Page 18: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0018

Printed: 5/11/2018 9:48 AM Page 2 of2

Report To: Work Order Details:

Eberline Analytical Cecilia Greene SDG.· 18-03111 ···········--·---•·-···-"--~•-, ······- .. "········-·--·--···-- ····--~ .. ••'-•• -·-· ~-- I····· • ••• ,.,,,~,_,,. ·•-❖--••·

Auxier & Associates, Inc. Project: WEST LAKE NCC Final Report of Analysis ~· -----

9821 Cog_qil! Road, Suite 1 Analysis Category: ENVIRONMENTAL - . ---- - -------Knoxville, TN 37932 Sample Matrix: so

Lab Sample Client Sample Receipt Analysis ! Batch Analyte Method Result CSU

I Report

ID Type ID Date Date Date ID ! cu MDA CV

Units

_18-03111-04 : DO AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 : 18-03111 Actinium-228 EPA 901.1 Modified : 1.09E+00 2.60E-01 2.66E-01 3.95E-01 1.84E-01 pCi/g "------

18-03111-04 DO AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 i 18-03111 Bismuth-214 EPA901.1 Modified 1.11E+00 1.95E-01 2.03E-01 2.12E-01 1.01E-01 pCi/g -•••w••• •••-•-'•••~"' "'-•-•~•••"'-•-•m• -

18-03111-04 DO AC-SED-11 03/21/1813:20 3/23/2018 4/17/2018 1 18-03111 , Potassium-40 EPA 901.1 Modified 1.68E+01 2.27E+00 2.42E+00 1.36E+00 6.32E-01 pCi/g

18-03111-04 DO AC-SED-11 03/21/1813:20 I 3/23/2018 4/17/2018 18-03111 Protactinium-231 EPA 901.1 Modified 4.02E-01 1.98E+00 1.98E+00 2.65E+00 1.26E+00 pCi/g

18~03111~04 I DO AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 ; 18-03111 Lead-210 EPA 901.1 Modified 2.01E+00 1.66E+00 1.66E+00 2.74E+00 1.34E+00 pCi/g I 18-03111-04 DO AC-SED-11 03/21/1813:20 3/23/2018 4/17/2018 18-03111 i Lead-212 EPA 901.1 Modified i 1.31E+00 2.57E-01 2.65E-01 2.45E-01 1.19E-01 : pCi/g

18-03111-04 : DO AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 18-03111 Lead-214 EPA 901.1 Modified 1.10E+00 1.94E-01 2.02E-01 2.16E-01 : 1.04E-01 : pCi/g

18-03111-04 DO AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 j 18-03111 ! Radium-226 EPA 901.1 Modified I 1.11E+00 1.95E-01 2.03E-01 2.12E-01 1.01E-01 pCi/g ----~- .,_.,.,_,,

18-03111-04 DO AC-SED-11 03/21/18 13:20 I 3/23/2018 4/17/2018 : 18-03111 I Radium-228 EPA 901.1 Modified 1.09E+00 2.60E-01 2.66E-01 3.95E-01 : 1.84E-01 : pCi/g

18-03111-04 I DO AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 : 18-03111 Thorium-234 EPA901.1 Modified 1.01E+00 1.14E+00 1.14E+00 1.91E+00 9.27E-01 I

pCi/g

18-03111-04 i DO : AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 i 18-03111 Thallium-208 EPA 901.1 Modified •

9.65E-01 1.89E-01 1.95E-01 1.34E-01 1.71E-01 : pCi/g

: ' I : I

18-03111-01 LCS KNOWN 03/23/18 00:00 3/23/2018 3/30/2018 18-03111 Thorium-230 EPA 907 .0 Modified :

5.39E+00 1.45E-01 : pCi/g

18-03111-01 LCS : SPIKE 03/23/18 00:00 3/23/2018 3/30/2018 j 18-03111 : Thorium-230 EPA 907.0 Modified I 6.57E+00 1.01E+00 : 1.30E+00 8.10E-02 7.95E-02 pCi/g

18-03111-02 MBL : BLANK 03/23/18 00:00 3/23/2018 3/30/2018 ! 18-03111 Thorium-230 EPA 907.0 Modified 4.58E-02 i 8.80E-02 8.82E-02 1.63E-01 1.44E-01 pCi/g

18-03111-03 DUP i AC-SED-11 03/21/18 13:20 3/23/2018 3/30/2018 l 18-03111 Thorium-230 EPA 907.0 Modified 1.17E+00 3.38E-01 3.68E-01 8.46E-02 8.67E-02 : pCi/g

18-03111-04 I DO : AC-SED-11 03/21/18 13:20 3/23/2018 313012018 I 18-03111 ; Thorium-230 EPA 907.0 Modified 1.34E+00 4.14E-01 4.47E-01 1.06E-01 1.09E-01 : pCi/g

I : I : I

18-03111-01 i LCS KNOWN 03/23/18 00:00 3/23/2018 313012018 ; 18-03111 I Uranium-234 EPA 908.0 Modified i 7.27E+00 2.62E-01 : pCi/g

18-03111-01 LCS SPIKE 03/23/18 00:00 3/23/2018 3/30/2018 I 18-03111 Uranium-234 EPA 908.0 Modified 6.71E+00 9.02E-01 1.02E+00 7.09E-02 1.22E-02 pCi/g

18-03111-02 I MBL BLANK 03/23/18 00:00 : 3/23/2018 313012018 I 18-03111 , Uranium-234 EPA 908.0 Modified 1.66E-02 4.01E-02 4.01E-02 8.04E-02 1.94E-02 pCi/g

18-03111-03 ; DUP AC-SED-11 03/21/18 13:20 3/23/2018 3/30/2018 18-03111 i Uranium-234 EPA 908.0 Modified 6.S0E-01 1.95E-01 2.00E-01 1.12E-01 4.20E-02 i pCi/g

18-03111-04 DO AC-SED-11 03/21/18 13:20 3/23/2018 3/30/2018 i 18-03111 Uranium-234 EPA 908.0 Modified 9.93E-01 : 2.42E-01 2.52E-01 9.59E-02 ' 2.86E-02 I pCi/g

i

18-03111-01 LCS SPIKE 03/23/18 00:00 3/23/2018 3/30/2018 I 18-03111 1 Uranium-235 EPA 908.0 Modified 4.97E-01 1.78E-01 1.81E-01 9.21E-02 1.34E-02 [ pCi/g

18-03111-02 MBL BLANK 03/23/18 00:00 3/23/2018 3/30/2018 18-03111 ! Uranium-235 EPA 908.0 Modified -5.02E-03 , 3.04E-02 3.04E-02 9.57E-02 1.66E-02 1 pCi/g

18-03111-03 DUP i

AC-SED-11 03/21/1813:20 3/23/2018 3/30/2018 18-03111 i Uranium-235 EPA 908.0 Modified 1.54E-01 1.06E-01 1.06E-01 1.15E--01 2.44E-02 pCi/g I I

18-03111-04 I DO AC-SED-11 03/21/1813:20 3/23/2018 3/30/2018 18-03111 I Uranium-235 EPA 908.0 Modified i 8.12E-02 7.21E-02 7.23E-02 7.76E-02 7.43E-03 : pCi/g

! ·-·~""""

18-03111-01 LCS KNOWN 03/23/18 00:00 3/23/2018 3/30/2018 18-03111 I Uranium-238 EPA 908.0 Modified 7.05E+00 2.54E-01 I pCi/g

18-03111-01 LCS I SPIKE 03/23/18 00:00 3/23/2018 3/30/2018 18-03111 Uranium-238 EPA 908.0 Modified 7.12E+00 9.46E-01 1.07E+00 7.43E-02 1.40E-02 pCi/g

18-03111-02 : MBL BLANK 03/23/18 00:00 3/23/2018 3/30/2018 18-03111 Uranium-238 EPA 908.0 Modified -2.25E-04 2.39E-02 2.39E-02 7.10E-02 1.34E-02 pCi/g

18-03111-03 I DUP AC-SED-11 03/21/1813:20 3/23/2018 3/30/2018 18-03111 Uranium-238 EPA 908.0 Modified : 7.25E-01 2.05E-01 2.12E-01 1.07E-01 3.76E-02 pCi/g

18-03111-04 DO AC-SED-11 03/21/1813:20 3/23/2018 3/30/2018 18-03111 Uranium-238 EPA 908.0 Modified 7.88E-01 2.10E-01 2.17E-01 7.52E-02 1.42E-02 pCi/g

CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample; MBL=Blank; DUP=Duplicate; TRG=Normal Sample; DO=Duplicate Original; CV=Critical Value

( . EBERLINE ~ ANALYTICAL

EBERLINE ALYTICAL ot\J 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/ 483-4621

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0019

SECTIONV

ANALYTICAL STANDARD

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0020

QA/QC REVIEWED CERTIFICATE OF CALIBRATION LL-8

· Date (? q(lnitials Ji£. ALPHA STANDARD SOLUTION

Radionuclide: U-238NAT

Half Life:

Customer:

P.O.No,:

TMA EBERLINE

OR2778

Catalog No.:

(4.468 ± 0.005) x lOA9 years

7338 Reference Date: January 11995 12:00 PST.

Source No.: 479-50 Contained Radioactivity: (Total U) 8.016 µ,Ci

Contained Radioactivity: (fotal U) 297 k:Bq

Description of Solution a. Mass of solution:

b. Chemical form:

65. 2896 g in a 50 ml flame sealed ampoule

Uranyl Nitrate in H20

c. Carrier content: None

d. Density: Approximately 1.3202

Radioimpurities

Radioactive Daughters

Refer to attached technical data sheet

Refer to attached technical data sheet

Radionuclide Concentration

(Total U) 0.1228 Method of Calibration

Activity calculations are based upon known specific activity and mass.

Uncertainty of Measurement a. Systematic uncertainty in instrument calibration:

b. Random uncertainty in assay:

c. Random uncertainty in weighing(s):

d. Total uncertainty at the 99 % confidence level:

NIST Traceability

±3,0%

±0,0%

±2.0%

±3,6%

g/mI @20°c.

µCi/g.

This calibration is implicitly traceable to the National Institute of Standards and Technology.

Leak Test(s)

See reverse side for Leak Test(s) applied to this source.

Notes

1. Nuclear data were taken from "Table of Radioactive Isotopes", edited by Virginia S. Shirley, 1986.

2. IPL participates in an NIST measurement assurance program to "~tablish and maintain implicit traceability for a number of nuclides,

based on the blind as6lly (and later NIST certification) of Standard Reference Materials (As in NRC Regulatory Guide 4.15).

ISOTOPE PRODUCTS LABORATORIES

3017 N. SAN FERNANDO BLVD.

BURBANK, CALIFORNIA 91504

8}8•843•7000 FAX 818•843•6168

lE(Z,lv~

YCONTROL

~ t74::€Mk$ 19:z'f Date Signed

:', ·.,·,·•.···;,,,,,

) j ,,

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0021

~ """"__i,;; BJ;;;~!':!,"' I QUALITY CONTROL PROGRAM

MP-009

Rev.a; 11/01/03 Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES - OAK RIDGE LABORATORY RADIOACTIVE REFERENCE SOLUTIONS PRIMARY DILUTION RECERTIFICATION

MP 009

CURRENT DATE 7/12/20170:00 SOLUTION REFERENCE # .... IP_L_4 ___ 7 __ 9---5-0-··· -------. SOLUTION#"""'·--.. -, .·"""',u.,...;..,...8...,'··'--· -. ---i

Half Life, Years I · .>,4;468E+09!

Radionuclide ' <?&{~U/ Certified Activity . 8t016Ef0O µCi

Certified Concentration · · . µCi per gram

Ampoule /Solution Gross Empty Ampoule

Solution Net Total Activity in Ampoule

Half Life, Days I 1.632E+12!

Reference Date!. · :·•.:1/1119950:0o!

• . 9T6400 Weight, Grams ·· · >32;5020. Weight, Grams

65.1380 Weight, Grams 8.0160 µCl

Chemical Com osition of Standard Solution

Dilution Instructions: Dilution Solvent Used l1MHN. O·· ·.·· .. , .... ' .. 3

Dilute to a volume of! . . 1000;00 ··. j milliliters

Certified Total Activity ofj Which Eauals . 1.780E+07jdpm at the date listed above

• • • . . • • . This activity concentration Is based on the original · And after dilution the act1v1ty of this solution 1s! 1;77955E+04!dpm/m•eference date listed above, All activities are corrected

to the date and time of analysis by the laboratory data processing software.

Expiration Date:! June 28, 2018

Date: 7/12/2017 0:00 -------Date: 7 / 23f( '.) ---,--r--1-----

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0022

Rev.a; 11101103 Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES-OAK RIDGE LABORATORY RADIOACTIVE REFERENCE STANDARD SOLUTIONS

SECONDARY DILUTION RECERTIFICATION

MP-009 Date 7/12/2017 0:00 Solution Reference# IPL479~50 Solution # U-8a< .

Princi al Radionuclide :z34,•2~:2380:

Half Life, Years 1· 4:46$E+MI

Half Life, Days ! . · 1.632E+12I

Radionuclide of Interest, 234; 2~-: 2.~tJ. Reference Date!> •-.j)1i19950:00)

Parent Solution Cone .. 1.7796E+04 · dpmlml

Chemical Com osition of Standard Solution Uranly:Nitrat!:! in 11VF1:!N0i ·· ··

Dilution Instructions: Dilution Solvent Used !_-1MHNo-· :· . . 3 .

SECONDARY VOLUMETRIC DILUTION

Vol. Parent Solution: Total Activity: Final Volume:

NOTES:

)t0000 ml 7.1182E+04 dpm

- 1000;00 ml Final Activity Concentration: I 7.1182E+01!dpm/ml

This activity concentration is based on the original reference date listed above. All activities are corrected to the date and time of analysis by the laboratory data processing software. ------------------------, Isotopic Distribution as:

U-238 Atom % = 48.239 U-235 Atom % = 2.25 U-234 Atom%= 49.501 All values +/- 3.6%

U-238 = 71.182 dpm/rnl X 0.48249 = 34.345 dprn/ml U-235 = 71.182 dpmlrnl X 0.0225 = 1.602 dpm/ml U-238 = 71.182 dpm/ml X 0.49501 = 35.236 dpmlml

Isotopic ratios from manufacturer's data sheet

Verified&Appr~

Expiration Date:I June 28, 2018

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0023

RECORD COf-YY

Tracer Solution for Environmental Analysis & Disequilibrium Studies

Description

(

Product Description & Measurement Certificate

Principal radionuclide: Daughter Nuclide:

uranium 232 (U-232) Th-228

Product code: UDP10050 Batch Number: 92/232/67

Measurement Reference date: 01 March 2000

Accuracy

Radionuclidic Purity

Isotopic Purity

Chemical Composition

Physical Data

Remarks

Approved Signatory

Radioactive concentration U-232 which is equivalent to

6.739E+03 becquerels per gram of solution I.821E-01 microcuries per gram of solution

Volume of solution Total activity of U-232

which is equivalent to

5.035 millilitres 3.6IE+04 becquerels 9.76E-01 microcuries

Method of measurement (see reverse of this certificate) Random uncertainty is:± 0.7% Systematic uncertainty:± 0.5% Overall uncertainty in the radioactive concentration quoted above: ± 1.7% Overall uncertainty is defined on the reverse of this certificate.

Any radioactive impurities measured are listed below, expressed as percentages of the activity of the principle radionuclide at the reference date.

Th-228 and daughter activity removed 2 Feb 2000 U-232 daughters activity will increase with time. By alpha 88% U-232, 12% daughters on 1/3/00

""he isotopic composition, exprP,ssed as atom per cent at the reference date .

,\Jot measured

Calculated weight ofU-232, 4.42E-08 grams, as 2M HN03 solution in a flame sealed glass vial.

This Tracer solution has been produced 'carrier free'.

Recommended halflifo of uranium 232: 6.980E+Ol years Principle energies of alpha emissions (MeV): 5.263 31.7%, 5.320 68.0% Bra..'lching ratio for alpha emission: I 00% Calculated specific activity of uranium 232: 8.167E+05 Bq per microgram U-232.

For safety information and notes to ensure correct usage by all persons handling this radior-tctive Tracer solution please read the instructions accompanying the package.

AEA Technology operates a quality management system which has been independently audited and approved to ISO 9001.

Project Ref. AE:l315

Roger Wiltshire

Prepared and characteri~ed in the UK, for world wide distribution by Isotrak, AEA Technology, QSA.

Trkcert.wps I 0/03/00 AEA Techn1ilogy is the trading name of AEA Technology pie

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0024

,:EBERS~~~

Rev.B; 11/01 /03

QUALITY CONTROL PROGRAM MP-009

Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES - OAK RIDGE LABORATORY RADIOACTIVE REFERENCE SOLUTIONS PRIMARY DILUTION RECERTIFICA TfON

MP009

CURRENT DATE 10/7/2017 0:00 ...-----------. --------1 SOLUTION REFERENCE# AEA/Amersham 92/232/67 SOLUTION # U-10

Princi al Radionuclide 232u

Radionuclide 232U

Half Life, Years

I· 7.200E+o1 I

Certified Activity 9. 760E-01 µCi Certified Concentration µCi per gram .__ ___ __,

Half Life, Days

I 2.630E+04j

Reference Date! ..... ___ 3/_1_/2_0_00_0:_0__.0 I

Ampoule /Solution Gross~Weight, Grams Empty Ampoule Weight, Grams

Solution Net Weight, Grams

Total Activity in Ampoule 0.9760 µCi

Chemical Com osition of Standard Solution

Dilution Instructions: Dilution Solvent Used

Dilute to a volume ofl 1000.00 !milliliters

Certified Total Activity ofl 0.976DlµCi Which Eauals 2.167E+06!dpm at the date listed above

And after dilution the activity of this solution isl 2.167E+03ldp'm/ml This activity concentration is based on tile original reference date listed above. All activities are corrected to the date and time of analysis by the laboratory data processing software.

Expiration Date: i October 4, 2018

Date: 10/7/2017 0:00

Date:

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0025

QUALITY CONTROL PROGRAM MP-009

Rev.8; 11/01/03 Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES - OAK RIDGE LABORATORY · RADIOACTIVE REFERENCE STANDARD SOLUTIONS

SECONDARY DILUTION RECERTIFICATION

MP-009 Date 10/7/20170:00

Solution Reference # AEA/Amersham 92/232/67 Solution # U-1 Oa

Principal Radionuclide Half Life, Years 3 .u I 7 .200E+01 I

Half Life, Days I 2.630E+04I

Radionuclide of Interest 23 U Reference Date.__l ___ 3_/1_/2_0_0_0_0_:o_o.,JI

Parent Solution Cone. 2.167E+03 dpm/ml

Chemical Composition of Standard Solution

Dilution Instructions: Dilution Solvent Used

Vol. Parent Solution: Total Activity: Final Volume:

NOTES:

SECONDARY VOLUMETRIC DILUTION

10.0000 ml 2.1670E+04 dpm

1000.00 ml Final Activity Concentration: I 2.1670E+01 jdpm/ml

This activity concentration is based on the original reference date listed· above. All activities are · corrected to the date and time of analysis by the laboratory data processing software. ·

Expiration Date:I October 4, 2018

10/7/2017 0:00

Date:

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0026

Radionuclide:

Half Life:

CERTIFICATE OF CALIBRATION ALPHA STANDARD SOLUTION

Th-232 Customer:

P.O.No.:

TMA EBERLINE

VH1632

1h-8

Catalog No.:

. (1.405 ± 0.006) x lOA 10 years

7232 Reference Date: November 11993 12:00 PST.

Source No.: 435-104-2 Contained Radioactivity: (Th-232) 0.0933 µCi.

Contained Radioactivity: (Th-232) 3.45 k.Bq.

Description of Solution a. Mass of solution:

b. Chemical form:

c. Carrier content:

11.9712 g (in a 10 ml flame sealed ampoule)

Th(N03)4 in water

None added

d. Density: Approx. 1.21 g/ml@20°C.

Radioimpurities None detected (other than daughters).

Radioactive Daughters Ra-228, Ac-228, Th-228, Ra-224, Rn-220, Po-216, Pb-212, Bi-212, Po-212, Tl-208

Radionuclide Concentration

(Th-232) 0.00779

Method of Calibration Activity calculations are based upon known specific activity and mass.

Uncertainty of Measurement a. Systematic uncertainty in instrument calibration:

b. Random uncertainty in assay:

c. Random uncertainty in weighing(s):

d. Total uncertainty at the 99 % confidence level:

NIST Traceability

±3.0%

±0,0%

±2,0%

±3.6%

This calibration is implicitly traceable to the National Institute of Standards and Technology.

Leak Test(s)

See reverse side for Leak Test(s) applied to this source.

Notes

I. Nuclear data were taken from "'!'.able of Radioactive Isotopes", edited by Virginia S. Shirley, i 986.

µCi/g,

2. IPL participates in an NIST measurement assurance program to establish and maintain implicit traceability for a number of nuclides,

based on the blind assay (and later NIST certification) of Standard Reference Materials (As in NRC Regulatory Guide 4. 15).

ISOTOPE PRODUCTS LABORATORIES

1800 North Keystone Street

Burbank, California 91504

818 843 ~ 7000

QUALITY CONTROL

Date Signed

Page 27: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0027

~Ea EJ¾~!:i!!i I

QUALITY CONTROL PROGRAM MP-009

Rev.8; 1110/03 Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES - OAK RIDGE LABORATORY RADIOACTIVE REFERENCE SOLUTIONS PRIMARY DILUTION RECERTIFICATION

MP009

CURRENT DATE 8/16/2017 0:00 SOLUTION REFERENCE #""'IP""'L_A.,...,3,_,,5....,:::1,.....04,..,.. .. :.-2-, -,,------. SOLUTION # · .. . . .. Th-8

Half Life, Years Half Life, Days ! 1AOSE+10I ! 5.132E+12l

Radionuclide · h · Certified Activity . · 9.330E-'-02 µCi

Reference Date I ..... · . _ _;.1.1..;../.1_1_19..,..9_3_0_: o__,o I Certified Concentration.__ ___ _.µCi per gram

Ampoule /Solution Gross · 18,8415 Weight, Grams Empty Ampoule --=·-··.:6.9296 Weight, Grams

Solution Net 11.9119 Weight, Grams Total Activity in Ampoule 0.0933 µCi

Chemical Composition of Standard Solution

DIiution Instructions: Dilution Solvent Used j1% NitricAcid

Dilute to a volume ofl. 1000,00 ·. I milliliters

Certified Total Activity ofl 0.0933jµCi Which Eauals 2.071 E+OSjdpm at the date listed above

I

And after dilution the activity of this solution isl 2.071E+02jdpm/ml This activity concentration is based on the original reference date listed above. All activities are corrected to the date and time of analysis by the laboratory data processing software.

Expiration Date:! August 11, 2018

R/1R/?017 O·Of)

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0028

Rev.8; 1/10/03 Title: Radioactive Reference Standards· Solutions & Records

EBERLINE SERVICES· OAK RIDGE LABORATORY RADIOACTIVE REFERENCE STANDARD SOLUTIONS

SECONDARY DILUTION RECERTIFICATION

MP-009 Solution Reference# IPL 435:;:.10~2-

Princi al Radionuclide ·· 226&232Th

Radionuclide of Interest ·• ·. 228 & 232Th ·

Half Life, Years ! 1.405E+1DI

Parent Solution Cone. 2.07E+02 ·· dpm/ml

Chemical Composition of Standard Solution

Date 8/16/2017 O;OO Solution # ·. . Jh-,8b

Half Life, Days ! 5.132E+12I

Reference Date! · 1111/199$ o:ooj

Dilution Instructions: Dilution Solvent Used

SECONDARY VOLUMETRIC DILUTION

) 1 % Nitric Acid

Vol. Parent Solution: Total Activity: Final Volume:

NOTES:

• soo:0000 ml 1.0355E+05 dpm

1000.00 ml Final Activity Concentration:! 1.0355E+02!dpm/ml

This activity concentration is based on the original reference date listed above. All activities are corrected to the date and time of analysis by the laboratory data processing software.

Expiration Date: I August 11, 2018

Date: 8/16/2017 0:00 ----,----Date: ~ h0/i:1 -----·7 ~)...._, __

I

Page 29: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0029

RTIFICATE OF CALIBRATIOti.it , LPHA STANDARD SOLUTIO~ \)c', ~:;\\tli

Radionuclide

Half Life:

Th-230 Customer:

P.O.No.:

..1{'~i1t~ ~~ TMA EBE!lLM~ 1,i,t

Catalog No.:

(7 .54 ± 0.03) X 10"4 years

7230 TT4944 \\I~'

Reference Date: November 1 1991 12:00 PST.

Source No.: Contained Radioactivity: 1.036 µCi.

Description of Solution a. Mass of solution:

b. Chemical form:

c. Carrier content:

d. Density:

Radioimpurities

Radioactive Daughters

Radionuclide Concentration

Method of Calibration

5,0042 Th(NO3)4 in 0.lN HNO3

None added 1.0016

See attached technical data sheet

See attached technical data sheet

0.207

Weighed aliquots of the solution were assayed using a liquid scintillation counter.

Uncertainty of Measurement a. Systematic uncertainty in instrument calibration:

b. Random uncertainty in assay:

c. Random uncertainty in weighing(s):

d. Total uncertainty at the 99% confidence level:

NIST Traceability

±2.0% ±0.5% ±0.2% ±2,7%

grams.

gram/ml @ 20°c.

µCi/gram.

This calibration is implicitly traceable to the National Institute of Standards and Technology.

Notes 1. Nuclear data were taken from "Table of Isotopes", Seventh Edition, edited by Virginia S. Shirley.

2. IPL participates in an NIST measurement assurance program to establish and maintain implicit traceability for a number of nuclides, based on the blind assay(and later NIST certification) of Standard Reference Materials. (As in NRC Regulatory Guide 4.15)

ISOTOPE PRODUCTS LABORATORIES 1800 No. Keystone Street., Burbank, California 91504 818 843 - 7000

Page 30: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0030

Rev.14; 10/10/2012

QUALITY CONTROL PROGRAM MP-009

Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES - OAK RIDGE LABORATORY RADIOACTIVE REFERENCE SOLUTIONS

PRIMARY DILUTION RECERTIFICATION MP009

CURRENT DATE 2/10/2018 0:00 SOLUTION REFERENCE #.-IP_L_3_8_8_-1_1_6 ____ _, SOLUTION #1----T-h--1---

Princi al Radionuclide 230Th

Half Life, Years

I 7.540E+04I

Radionuclide l30Thorium

Certified Activity 1.036E+OO µCi Certified Concentration .__ ___ _,µCi per gram

Ampoule /Solution Gross Empty Ampoule

Solution Net Total Activity in Ampoule

Chemical Composition of Standard Solution

Half Life, Days

I 2.754E+07I

Reference Date._! __ 1_1/_1_/1_9_91_0:_o_.ol

9.2660 Weight, Grams 4.6218 Weight, Grams 4.6442 Weight, Grams 1.0360 µCi

Dilution Instructions: Dilution Solvent Used !0.1N HN03

Dilute to a volume of! 1000. 00 I milliliters

Certified Total Activity ofl 1.0360/µCi Which Eauals 2.300E+06ldpm at the date listed above

This activity concentration is based on the original

And after dilution the activity of this solution isl 2.300E+03ldpmhmence date listed above. All activities are corrected to the date and time of analysis by the laboratory data processing software.

Expiration Date: I January 10, 2019

,,,,-· ··--~.~----

Date: 2/10/2018 0:00 --------Date: '3 cg;·

--~,;i.i::.<:.µ....;;.;::;::___

Page 31: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0031

.. ~1;)

)G.,--, ,E B EJ P. LJHN E '~)· '·! ,,,,.,,_'j'.

Rev,14; 10/10/2012

QUALITY CONTROL PROGRAM MP-009

Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES - OAK RIDGE LABORATORY

RADIOACTIVE REFERENCE STANDARD SOLUTIONS SECONDARY DILUTION RECERTIFICATION

MP-009 Date! 2/10/2018 O:OOI

Solution Reference# IPL 388-116 I Solution #I Th-1 b I

Principal Radionuclide Half Life, Years

I 7.540E+04I

Half Life, Days

,ouTh I I 2.754E+07I

Radionuclide of Interest ,ouThorium Reference Date!~ __ 1_1_/1_/1_9_9_1 _0_:o~ol

Parent Solution Cone. 2.30E+03 dpmlml

Chemical Composition of Standard Solution

Dilution Instructions: Dilution Solvent Used j0.1N HNO3

SECONDARY VOLUMETRIC DILUTION

Vol. Parent Solution: 10.0000 ml

Total Activity: 2.2999E+04 dpm

final Volume: 1000.00 ml

NOTES:

Final Activity Concentration: I 2.2999E+01 \dpmlml

This activity concentration is based on the original

reference date listed above. All activities are

corrected to the date and time of analysis by th,e

laboratory data processing software.

Expiration Date:l January 10, 2019 I

Date: 2/10/2018 0:00

Date:

-----,----

s:?, I 31/ ~ I

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0032

-~ Isotope Products Laboratories

An Eckert & Ziegler Company

24937 Avenue Tibbitts Valencia, California 91355

Tel 661•309·1010 Fax 661•257•8303

CERTIFICATE OF CALIBRATION ALPHA STANDARD SOLUTION

Radionuclide: Half-life: Catalog No.:

Th-229 7340 ± 160 years 7229

Customer: P.O.No.: Reference Date:

EBERLINE SERVICES 00009633 15-Jan-02 12:00 PST

Source No.: 867-54 Contained Radioactivity: (Th-229 only)

1.013 µCi 37.48

Physical Description: A. Mass of solution: B. Chemical form:

5.0147 gin 5 ml flame-sealed ampoule Th(NO3) 4 in 0.1 M HNO3

C. Carrier content: 10µg Th/ml D. Density: 1.0016 g/mL@ 20°c.

Radioimpurities:

None detected (daughters in equilibrium)

Radionuclide Concentration: 0.2020 µCi/g, 7.474 kBq/g

Method of Calibration:

This source was prepared from a weighed aliquot of solution whose activity in µCi/g was determined using gamma ray spectrometry. · Peak energy used for integration: 193.5 keV Branching ratio used: 0.0441 gammas per decay

Uncertainty of Measurement: A. Type A (random) uncertainty: B. Type B (systematic) uncertainty: C. Uncertainty in aliquot weighing: D. Total uncertainty at the 99% confidence level:

Notes: - See reverse side for leak test(s) performed on this source.

± 0.7 % ± 3.0 % ± 0.0 % ± 3.1 %

kBq

- IPL participates in a NIST measurement assurance program to establish and maintain implicit traceability for a number of nuclides, based on the blind assay (and later NIST certification) of Standard Reference Materials (As in NRG Regulatory Guide 4.15).

- Nuclear data was taken from IAEA Technical Report Series No. 261. - This solution has a working life of 5 years.

Quality'control Date Signed IPL Ref. No.: 867-54

------------------ ISO 9001 CERTIFIED ------------------

Medical Imaging Laboratory Industrial Gauging Laboratory 24937 Avenue Tibbitts Valencia, California 91355 1800 North Keystone Street Burbank,California 91504

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0033

;: I;. BEIR!,,.~!';'o!/i I QUALITY CONTROL PROGRAM

MP-009

Rev.a; 1/10/03 Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES - OAK RIDGE LABORATORY RADIOACTIVE REFERENCE SOLUTIONS PRIMARY DILUnON RECERTIFICATION

MP 009

CURRENT DATE SOLUTION REFERENCE # .... IP __ L .... ':8 .... 67-~-54.....,•.--,,.------. SOLUTION #1-•· ....,.......,......,,.., ____ _

Half Life, Years 1 · . i340E+03l

Radionuclide ~h . Certified Activity · 1;013E+00 µCi

Certified Concentration.._ ___ _. µCi per gram

Ampoule /Solution Gross Empty Ampoule

Solution Net Total Activity in Ampoule

, .. , .. .,.

Chemical Com osition.of Standard Solution

8.7752 ;3..79~1 5.0161 1.0130

Half Life, Days l 2.681E+06l

Reference Date._! __ 1_/_15_/2_0_0 __ 2_0-'--:0 ...... oj

Weight, Grams Weight, Grams Weight, Grams µCi

Dilution Instructions: Dilution Solvent Used

Dilute to a volume of! • 1000.00C !milliliters

Certified Total Activity ofl 1.0130jµCi Which EQuals 2.249E+06jdpm at the date listed above

This activity concentration is based on the original And after dilution the activity of this solution isl 2.249E+03jdpm/ml reference date listed above. All activities are corrected

to the date and time of analysis by the laboratory data processing software.

Expiration Date: I August 11, 2018 I

n::itA· R/1Rf?n11 n·nn

Date: -.....a~~[(.o+-{t 1-+--

Page 34: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0034

, e; .. a~RL..JN __ E; I auAuTY coMP~T00RoL PROGRAM

~ S~"VIC~'S ""'

Rev.7; 9/29/99 Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES-OAK RIDGE LABORATORY RADIOACTIVE REFERENCE STANDARD SOLUTIONS

SECONDARY DILUTION RECERTIFICATION

MP-009 Solution Reference # IPLB67:-54 •·

Princi al Radionuclide · · 229r11 ·

Radionuclide of Interest · 229th ·

Half Life, Years ! i.340E+03!

Parent Solution Cone. ·· 2.25E+03 .. dpm/ml

Chemical Com osition of Standard Solution TH(N03kin 0.1M HNOi . .· · .

Date 8/16/2017 0:00 Solution # Th-.18a ..

Half Life, Dar I 2.a

Reference Date! ._ __ 11_1 s_/_20_0_2_0_:o_o .... l

Dilution Instructions: Dilution Solvent Used

Vol. Parent Solution: Total Activity: Final Volume:

NOTES:

SECONDARY VOLUMETRIC DILUTION

< 10:0000 ml 2.2490E+04 dpm

10b0:oo ml Final Activity Concentration:! 2.2490E+01 !dpm/ml

This activity concentration is based on the original reference date listed above. All activities are corrected to the date and time of analysis by the laboratory data processing software.

Expiration Date:1 August 11, 2018

::::: ====~=,1=6=:::;:;-7_=7:o_:_o_o __ _

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0035

-4!r t:ckert & Ziegier Analytics

CERTIFICATE OF CALIBRATION Standard Reference Source

SRS Number: 104852

Source Description: Sand in 16 Ounce PP Omega Jar Filled to Capacity

Product Code: 8401-EG-SAN

Customer: Eberline Analytical Corporation

P.O. Number: OR-1610009, Item 4

1380 Seaboard Industrial lllvd. Atlanta, Georgfa 303 lB Tel 404•352•8677

Fax 404•352•2837

www.ezag.com

This standard radionuclide source was prepared from an aliquot measured gravimetrically from a master

radionuclide solution calibrated with a germanium gamma-ray spectrometer system. Additional radionuclides were

added gravimetrically from solutions calibrated by gamma-ray spectrometry, ionization chamber, or liquid

scintillation counting. Calibration and purity were checked using germanium gamma-ray spectrometry. At the time

of calibration no interfering gamma-ray emitting impurities were detected. The gamma-ray emission rates for the

most intense gamma-ray lines are given. Eckert & Ziegler Analytics (EZA) maintains traceability to the National

Institute of Standards and Technology (NIST) through a Measurements Assurance Program as described in USNRC

Regulatory Guide 4.15, Revision 2, July 2007, and compliance with ANSI N42.22-l995, "Traceability of Radioactive

Sources to NIST."

Reference Date: 0l-October-2016

MGSMixture

12:00PMEST

Gamma-Ray Uncertainty Calibration Isotope Energy, keV Half-Life, d Activity, Bq Flux, s-i uA, % u8, % u, %* Method**

~~ .. a'~~~-~111.t~~I Cd-109 88.0 4.614E+02 7.668E+04 2.837E+03 0.5 2.0 4.1 HPGe

~~~~~.,,,-z,~=.-,•"\:;jl,~:E~~"r,W-~- . ... - . -~~1'-~~F~~= ~~~~&~~,~~~ -, .. ' - '. ,_.,. ·~@-~~~ =:-;--;.:;::.,::;l,~~~

Ce--139 165.9 l.376E+02 2.655E+03 Z.124E+03 0.4 1.7 3.6 HPGe -1il~D'.~- _;~.-,: .i,· ~,,-.,,, :,.·~: ·-3

Sn-113 391.7 l.151E+02 4.528E+03 2.942E+03 0.4 1.9 3.9 HPGe • ~ .r.=..~. -~~ ~~··.iv,'.'_•;• ; :,: ~~ ~--· $ • J."'' ;:~--~

Y-88 898.0 l.066E+02 7.415E+03 6.948E+03 0.7 1.7 ~~:1~ • ,,. ' . . ~-~ .•-:· -:; ... - -~~

Co-60 1173.2 l .925E+03 3.562E+03 3.557E+03 ~~~~as~~ ---Mixed Gamma (MGS) master solution is EZA's eight isotope mixture which is calibrated quarterly and consists of

Cd-109, Co-67, Ce-139, Hg-203, Sn-113, Cs-137, Y-88, and Co-60, llrlJncertainty: U -Relative expanded uncertainty,

k = 2. See NIST Technical Note 1297, "Guidelines for Evaluating and Expressing the Uncertainty of NIST

Measurement Results." """Calibration Methods: 4n LS - 4n Liquid Scintillation Counting, HPGe - High Purity

Germanium Gamma-Ray Spectrometer, IC - Ionization Chamber.

(Certificate cont.inued on reve!'$e $ide)

EZA Certificate Program Rev. 0, 07-DEC-201 S Page 1 of 2

Corporate Office laboratory

24937 Avenue Tibbitts Valencia, California 91355 1380 Seaboard Industrial Blvd. Atlanta, Georgia, 30318

Page 36: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0036

-~ Eckert & Ziegler Analytics

1380 Seaboard Industrial Blvd. Atlanta, Georgia 30318 Tel 404•352•8677

Fax 404•352•2837

www.analyticsinc.com

CERTIFICATE OF CALIBRATION Standard Radionuclide Source GAS- ('+D~

98503 Sand in 16 Ounce PP Taral Jar Filled to Capacity

Customer: Eberline Analytical Corporation P.O. No.: OR-1405030, Item 6 Product Code: 8401-EG-SAN

Reference Date: 01-0ct-2014 12:00 PM EST Grams of Master Source: 0.017608

Thls standard radionuclide source was prepared using aliquots measured gravimetrically from master

radionuclide solutions. Additional radionuclides were added gravimetrically from solutions calibrated by

gamma-ray spectrometry, ionization chamber, or liquid scintillation counting. Calibration and purity were

checked using a germanium gamma spectrometer system. At the time of calibration no interfering gamma­

ray emitting impurities were detected. The gamma-ray emission rates for the most intense gamma-ray lines

are given. Eckert & Ziegler Analytics (EZA) maintains traceability to the National Institute of Standards and

Technology through a Measurements Assurance Program as described in USNRC Regulatory Guide 4.15,

Revision 2, July 2007, and compliance with ANSI N42.22-1995, "Traceability of Radioactive Sources to NIST."

EZA is accredited by the Health Physics Society (HPS) for the production of NIST-traceable sources, and this

source was produced in accordance with the HPS accreditation requirements. Customers may report any

concerns with the accreditation program to the HPS Secretariat, 1313 Dolley Madison Blvd., Ste. 402, McLean,

VA 22101.

Master Uncertainty* , %

Gamma-Ray Half-Life, Source* This Source Type Calibration

Nuclide Energy (ke V) Days yps/gram yps UA UB u Method*

Arn-241 69.5 l.580E+05 2.030E+03 0.1 1.8 3.6 -4nLS

Cd-109 88.0 4.614E+02 l.663E+05 2.929E+03 0.5 2.0 4.1 HPGe

Co-57 122.1 2.717E+02 8.913E+04 l.669E+03 0.4 1.7 3.6 HPGe

Ce-139 165.9 l.376E+02 l.241E+05 2.185E+03 0.4 1.7 3.5 HPGe

Hg-203 279.2 4.659E+0l 2.675E+05 4.710E+03 0.3 1.7 3.5 HPGe

Sn-113 391.7 l.151E+02 1.796E+06 3.163E+03 0.4 1.9 3.9 HPGe

Cs-137 661.7 l.099E+04 1.ll 1E+05 1.956E+03 0.7 1.9 4.0 HPGe

Y-88 898.0 l.066E+02 4.223E+06 7.435E+03 0.7 1.7 3.7 HPGe

Co-60 1173.2 l.925E+03 2.091E+05 3.683E+03 0.7 1.8 3.9 HPGe

Co-60 1332.5 l.925E+03 2.094E+05 3.687E+03 0.7 1.8 3.9 HPGe

Y-88 1836.1 l.066E+02 4.471E+05 7.872E+03 0.7 l.7 3.7 HPGe

* Master Source refers to Analytics' 8-isotope mixture which is calibrated quarterly.

Calibration Methods: 4n IB- 4 pi Liquid Scintillation Counting, HPGe. High Purity Germanium Gamma-Ray Spectrometer, IC -

Ionization Chamber. Uncertainty: U - Relative expanded uncertainty, k"' 2. See NIST Technical Note 1297, "Guidelines for

Evaluating and Expressing the Uncertainty of NIST Measurement Results."

(Certificate continued on reverse side)

MGS Certificate Rev 7, 11 September 2014 Page 1 of 2

Corporate Office Laboratory

24937 Avenue Tibbitts Valencia, California 91355 1380 Seaboard Industrial Slvd. Atlanta, Georgia, 30318

Page 37: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0037

SECTION VI

QUALITY CONTROL SAMPLE RESULTS SUMMARY

Page 38: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0038

Eberline Analytical

Analysis Control Chart

WO

18-03111

Analyte

U-234

U-238

Analyte

Analyte

U-234

U-238

U-235

Version

Nonnalized Difference

Analysis

UUISO

LCS I Measured

92.20%

101.10%

MS Actual %Rec

CSU Measured

15.22%

15.08%

Expected MS Result

Duplicate Results

Nonnalized RPD Original

Difference Result

2.09 41.80 9.93E-01

0.41 8.38 7.88E-01

1.11 61.78 8.12E-02

Run Activity Units Aliquot Units

1 pCi g

Laboratory Control Sample

LCS Expected

100.00%

100.00%

Expected MS Uncerl

Original CSU

2.52E-01

2.17E-01

7.23E-02

Uncert. Expected

Known

3.60% 7.27E+00

3.60% 7.0SE+00

Matrix Spike

Actual MS Result

Duplicate Result

6.S0E-01

7.25E-01

1.54E-01

Actual MS CSU

Duplicate CSU

2.00E-01

2.12E-01

1.06E-01

Known Error

2.62E-01

2.54E-01

Sample Result

LCS Relative

Bias

0.92

1.01

Result

6.71E+00

7.12E+00

Sample CSU

LCS¾R

OK

OK

OK

I

CSU

1.02E+00

1.07E+00

Sample Aliquot

Printed: 4/2/2018 8:31 AM Page 1 of 2

Client Name

Auxier & Associates, Inc.

Standard ID

U-Sa

U-8a

Standard ID

Standard ACT(dpm)

3.20E+01

3.10E+01

Standard ACT(dpm)

Standard Error

3.60E+00

3.60E+00

Standard Error%

Standard Added (g)

5.0SE-01

5.0SE-01

Standard Added (g)

QC Summary

I MS¾R I MSND I RepRPD I Rep ND

INV OK

OK OK

NA OK

Page 39: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0039

Eberline Analytical Analysis Control Chart

WO

18-03111

130.00

120.00

110.00

100.00

90.00

80.00

Analysis Run

UUISO 1

LCS % Recovery

L _________ _

Activity Units Ali_g_uot Units

pCi g

40.00

35.00

30.00

25.00

20.00

15.00

10.00

l

Printed: 4/2/2018 8:31 AM Page 2 of 2

Client Name

Auxier & Associates, Inc.

Replicate Sample RPD

l

70.00 ------------------~-----------------~ !

U-234 U-238 5.00

- LowerError 73.38 82.42

- Upper Error 111.03 119.79 o.oo +------,,.=,;-------,----u~ U-234 U-238 I U-235

• %R 92.20 101.10

- -LCL 75 75 - Lower Error

- UpperError

47.55 9.57

I 85.26

36.05 7.19 38.30

--Mean 100 100

- -UCL 125 125 • RPD

--CL

41.80 8.38

I 61.78

35 35 35

Normalized Difference

3.50 No Matrix Spike

3.00

2.50

2.00

1.50

1.00

0.50

0 00 LCS ND MS ND

-U-234 0.00 2.09 0.00

=U-238 0.00 0.41 0.00

= 0.00 0.00 0.00

- UCL 3 3 3

Version

Page 40: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0040

Eberline Analytical

Analysis Control Chart

WO

18-03111

Analyte

TH-228

TH-230

TH-232

Analyte

Analyte

TH-228

TH-230

TH-232

Version

Analysis

ThlSO

LCS CSU Measured Measured

122.00% 18.20%

121.89% I 19.77%

122.44% I 17.88%

Normalized MS Actual Expected

Difference %Rec MS Result

Duplicate Results

Normalized RPD

Original

Difference Result

1.11 27.71 7.91E-01

0.59 13.93 1.34E+00

1.22 30.19 1.12E+00

Run Activit Units Ali uot Units I

1 I pCi I

g I

Laboratory Control Sample

LCS Uncert. Known

Known Result

Expected Expected Error

100.00% 3.60% 5.11E+00 1.84E-01 6.24E+00

100.00% 2.70% 5.39E+00 1.45E-01 6.57E+00

100.00% 3.60% 5.11E+00 1.84E-01 6.26E+00

Matrix Spike

Expected Actual Actual Sample Sample

MS Uncert MS Result MS CSU Result CSU

I Original Duplicate Duplicate LCS Relative

LCS%R I CSU Result CSU Bias

3.04E-01 1.05E+00 3.32E-01 1.22 OK

4.47E-01 1.17E+00 3.68E-01 1.22 OK

3.79E-01 8.29E-01 2.81E-01 1.22 OK

Printed: 3/30/2018 1 :59 PM Page 1 of 2

Client Name

Auxier & Associates, Inc.

CSU Standard Standard Standard Standard

ID ACT(dpm) Error Added (g)

1.14E+00 Th-Sb 1.04E+02 3.60E+00 1.10E-01

1.30E+00 Th-1b 2.35E+01 2.70E+00 5.0SE-01

1.12E+00 Th-Sb 1.04E+02 3.60E+00 1.10E-01

Sample Standard Standard

I Standard

I Standard

Aliquot ID ACT(dpm) Error¾ Added(g)

QC Summary

I MS%R I MSND I RepRPD I Rep ND

INV OK

OK OK

INV OK

Page 41: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0041

Eberline Analytical Analysis Control Chart

WO

18-03111 Analysis Run

ThlSO 1

LCS % Recovery 130,00

120.00

110.00

100,00

r------r------1-90.00

80.00

-----= ----- -~ I H-228 I H-230 TH-232

- Lower Error' 100.21 99.41 100.96

- Upper Error 143.80 144.36 143.91

• %R 122.00 121.89 122.44

- -LCL 75 75 75

--Mean 100 100 100

- -UCL 125 125 I 125

Normalized Difference

3.50 ~-------------------------------

3.00 l-------------------------------2.50 l-------------------------------

2.00 l ______________________________ _ 1.50 +-------------------------------

1.00 +-------------

0.50

0.00 LCS ND MSND

-TH-2281 0.00 1.11 0.00

=TH-2301 0.00 0.59 0.00

- UCL I 3 3 3

Version

Activity Units Aliguot Units

pCi g

40.00

35.00

30.00

25.00

20.00

15.00

10.00

Printed: 3/30/2018 1 :59 PM Page 2 of 2

Client Name

Auxier & Associates, Inc.

Replicate Sample RPD

! -------------7 !

5.00

o.ooL~---r-~c=~~~= - Lower Error

TH-228 TH-230 TH-232

32.51 16.19 35.29

- UpperError 22.91 11.67 25.08

• RPD 27.71 13.93 30.19

--CL 35 35 35

No Matrix Spike

Page 42: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0042

Eberline Analytical Analysis Control Chart

18-03111

Analyte

CO-60

CS-137

Analyte

Analyte

AC-228

81-214

K-40

Version

Normalized Difference

Analysis

Gamma

LCS Measured

97.25%

98.43%

MS Actual %Rec

CSU Measured

8.02%

10.62%

Expected MS Result

Duplicate Results

Normalized RPD Original

Difference Result

1.20 22.27 1.09E+00

0.35 4.66 1.11E+00

0.51 5.25 1.68E+01

Run Activity_ Units Alig_uot Units

1 pCi g

Laboratory Control Sample

LCS Expected

100.00%

100.00%

Expected MS Uncert

Original CSU

2.66E-01

2.03E-01

2.42E+00

Uncert. Known

Expected

3.89% 1.35E+02

4.01% 8.44E+01

Matrix Spike

Actual MS Result

Duplicate Result

8.74E-01

1.06E+00

1.60E+01

Actual MS CSU

Duplicate CSU

2.38E-01

2.00E-01

2.28E+00

Known Error

5.27E+00

3.38E+00

Sample Result

LCS Relative Bias

0.97

0.98

Result

1.32E+02

8.31E+01

Sample CSU

LCS%R

OK

OK

I

CSU

1.06E+01

8.82E+00

Sample Aliquot

Printed: 4/17/2018 8:28 AM Page 1 of 2

Client Name

Auxier & Associates, Inc.

I Standard

ID

GAS-1402

GAS-1402

Standard ID

Standard ACT(dpm)

1.35E+02

8.44E+01

Standard ACT(dpm)

Standard Error

5.27E+00

3.38E+00

Standard Error¾

Standard Added (g)

7.36E+02

7.36E+02

Standard Added(g)

QC Summary

I MS%R I MSND I RepRPD I RepND

<CS-137 AC-228> OK

<CO-60 81-214> OK OK

K-40> OK OK

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0043

Eberline Analytical Analysis Control Chart

WO • 18-03111

130,00

120.00

110.00

100.00

90.00

80.00

Analysis Run

Gamma 1

LCS % Recovery

1 1 I I

70·00

: CO-60 CS-137

- LowerError 85.33 83.81

- Upper Error 109.16 113.05

• %R 97.25 98.43

- -LCL 75 75

--Mean 100 100

- -UCL 125 125

Normalized Difference

3.50

3.00

2.50

2.00

1.50

1.00

0.50

000 LCSND MSND

-

-CO-60 0.00 1.20 0.00

=cs-137 0.00 0.35 0.00

= 0.00 I 0.00 0.00

- UCL 3 I 3 3

Version

Activity_ Units Ali_guot Units

pCi g

40.00

35.00

30.00

25.00

20.00

15.00

10.00

5.00

T • l

Printed: 4/17/2018 8:28 AM Page 2 of 2

Client Name

Auxier & Associates, Inc.

Replicate Sample RPD

• • 0.00 -+--------------~------------~

AC-228 B1-214 K-40

- Lower Error 25.13 5.09 i 5.63

- UpperError

• RPO 19.41 4.22

I 4.87

22.27 4.66 5.25

--CL 35 35 i 35

No Matrix Spike

Page 44: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0044

SECTION VII

LABO RA TORY TECHNICIAN'S NOTES & RUN LOGS

Page 45: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0045

ISOUNOTES

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0046

Printed: 3/28/2018 8:16 AM

,:EBER~~~c~ Work Order Analysis Notes

# Date Dept User

1 03/28/18 08: 15 PREP JHARVEY

Oak Ridge Laboratory

601 Scarboro Rd. Oak RidC1e, TN 37830 Voice: 865.481.0683 www.eberlineservices.com

Page 1 of 1

Internal Work Order 18-03111 ------~--------,-- _____ ,,

Analysis Code UUISO Run Number 1

Notes

ALIQUOTED AND ADDED SPIKES AND TRACERS'-ADDED HF AND DRIED SAMPLES DOWN-ADDED

MIXED ACIDS AND TOOK SAMPLES TO DRYNESS- SUBMITTED SAMPLES TO SEPARATIONS

Page 47: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0047

Printed: 3/29/2018 3:18 PM Page 1 of 1

( Oak Ridge Laboratory Internal Work Order 18-03111 601 Scarboro Rd. 1 .....•• - -· -EBERLINE .... ® SERVICES Oak Ridge, TN 37830 Analysis Code UUISO

Work Order Analysis Notes Voice: 865.481.0683 , .... www.eberlineservices.com Run Number 1

# Date Dept User Notes

1 03/28/18 08:15 PREP JHARVEY ALIQUOTED AND ADDED SPIKES AND TRACERS- ADDED HF AND DRIED SAMPLES DOWN- ADDED

MIXED ACIDS AND TOOK SAMPLES TO DRYNESS- SUBMITTED SAMPLES TO SEPARATIONS

2 03/29/18 15: 18 CHEM JDEMELAS Added concentrated HCI to sample beakers and heated to dryness; Added 20 ml 8N HCL to samples and

transferred to new, labeled C-Tubes, rinsing with 8N HCI to bring volume to ~35 ml; Preconditioned resin

columns with 35 ml 8N HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 ml 8N

HCI, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml 8N HCI - 0.1 N NH4I, 35 ml

of 6.5N HCI- 0.04N HF, and 10 ml of 6.5N HCI; Eluted Uranium with 50 ml of 0.5N HCI into clean, labeled 100

ml beakers; Dried-down samples on hotplate; Dissolved samples in ~10 ml of concentrated HCI; Transferred le

new, labeled C-Tubes with DI H2O. Set samples aside for later precipitation and filtering.

-

Page 48: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0048

Printed: 3/30/2018 4:52 AM Page 1 of 1

~ Oak Ridge Laboratory Internal Work Order 18-03111 601 Scarboro Rd. --EBER~~~c~ Oak Ridge, TN 37830 Analysis Code UUISO Voice: 865,481.0683

Work Order Analysis Notes www.eberlineservices.com 1 Run Number

# Date Dept User Notes

1 03/28/18 08: 15 PREP JHARVEY ALIQUOTED AND ADDED SPIKES AND TRACERS- ADDED HF AND DRIED SAMPLES DOWN- ADDED

MIXED ACIDS AND TOOK SAMPLES TO DRYNESS- SUBMITTED SAMPLES TO SEPARATIONS

2 03/29/18 15:18 CHEM JDEMELAS Added concentrated HCI to sample beakers and heated to dryness; Added 20 ml 8N HCL to samples and

transferred to new, labeled C-Tubes, rinsing with 8N HCI to bring volume to ~35 ml; Preconditioned resin

columns with 35 ml 8N HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 ml 8N

HCI, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml 8N HCI - 0.1 N NH41, 35 ml

of 6.5N HCI- 0.04N HF, and 10 ml of 6.5N HCI; Eluted Uranium with 50 ml of 0.5N HCI into clean, labeled 100

ml beakers; Dried-down samples on hotplate; Dissolved samples in -10 ml of concentrated HCI; Transferred to

new, labeled C-Tubes with DI H2O. Set samples aside for later precipitation and filtering.

m,•,-•-•

3 03/30/18 04:51 CHEM TSMITH Followed steps 12.1.7 to 12.4.5 in AP-005. ( Precipitated and filtered samples for Uranium)

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0049

Eberline Analytical Oak Ridge Laboratory

Q EBERLINE "M> .... ····························· .. SERVICES

Reagents Used in an Analysis

Printed: 3/30/2018 4:58 AM Page 1 of 1

Internal Work Order

18-03111 Analysis Code Run

UUISO 1 ··-·-- -----··-··-·-•-·-··--------· --+-------------,--·-·------··--1-----··-··

Reagent ID

Reagent Name

·············•·····•-··----+-------------------+

019621P Hydrofluoric Acid

Reagent Concentration

Analyst ID

Date Recorded

Reagent Grade JHARVEY 3/28/2018

019673P Nitric Acid Reagent Grade JHARVEY 3/28/2018 ----

019529P Perchloric Acid Reagent Grade JHARVEY 3/28/2018 ··•--············

019351P Sulfuric Acid Reagent Grade JHARVEY 3/28/2018 ····--··········---······-·------·---t-------------------+-····-··-----·····-~

017230P Anion Exchange Resin Reagent Grade JDEMELAS 3/29/2018 --•··-·-···--·--·~····'

019826S HCI - HF 6.5N - 0.04N JDEMELAS 3/29/2018 ----r---- -----

019775D02 Hydrochloric Acid 0.SN JDEMELAS 3/29/2018

019827S Hydrochloric Acid 6.5N JDEMELAS 3/29/2018

019842S Hydrochloric Acid SN JDEMELAS 3/29/2018 --+-----·········---------------------------------+--····•·

019831P Hydrochloric Acid Reagent Grade JDEMELAS 3/29/2018 . ---~-------,~-----·-· ---+----···-·-····----···········-·············----··· ......

019861S HCI - NH4I SN - 0.lM JDEMELAS 3/29/2018 --•••--t--••'"•••~,_,,., __ '<"<¥.,_~••~--"~-•~w•-~•-•-•••->•--------+•

019803S Carbon substrate Solution TSMITH 3/30/2018

019525P Hydrofluoric Acid Reagent Grade TSMITH 3/30/2018

019640S Neodymium Carrier 1 mg/ml TSMITH 3/30/2018 -·····-··+····-·

019599P Reagent Alcohol Reagent Grade TSMITH 3/30/2018

019433P Titanous Chloride Reagent Grade TSMITH 3/30/2018

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0050

5

7 I

----+--------------+------+------1-------1----

---1~----------1--------t------+---+---

----~,1..-----.-----+-------1----->-----+------+---

Page 51: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0051

ISO TH NOTES

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0052

Printed: 3/28/2018 8:15 AM

,: E BER6tt':'c!';; Work Order Analysis Notes

# Date Dept User

1 03/28/18 08: 15 PREP JHARVEY

Oak Ridge Laboratory

601 Scarboro Rd. Oak Ridae, TN 37830 Voice: 865.481.0683 www.eberlineservices.com

Internal Work Order

Analysis Code

Run Number

Notes

Page 1 of 1

18-03111 ThlSO

1

ALIQUOTED AND ADDED SPIKES AND TRACERS- ADDED HF AND ORI Eb SAMPLES DOWN- ADDED

MIXED ACIDS AND TOOK SAMPLES TO DRYNESS- SUBMITTED SAMPLES TO SEPAR.ATIONS

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0053

Printed: 3/29/2018 3:19 PM Page 1 of 1

~ Oak Ridge Laboratory Internal Work Order 18-03111 601 Scarboro Rd. -~'"•·-· ""'"'"" EBERLINE

-~ . . - ... SERV1C:ES Oal< Ridge, TN 37830 Analysis Code ThlSO Voice: 865.481.0683 Work Order Analysis Notes ·--~ --···--··

www.eberlineservices.com Run Number 1

# Date Dept User Notes

1 03/28/18 08: 15 PREP JHARVEY ALIQUOTED AND ADDED SPIKES AND TRACERS-ADDED HF AND DRIED SAMPLES DOWN-ADDED

MIXED ACIDS AND TOOK SAMPLES TO DRYNESS- SUBMITTED SAMPLES TO SEPARATIONS

2 03/29/18 15: 19 CHEM JDEMELAS Added concentrated HNO3 to sample beakers and heated to dryness; Added 20 ml 8N HNO3 to samples and

transferred to new, labeled C-Tubes, adding 8N HNO3 to bring volume to -35 ml; Preconditioned resin

columns with 50 ml 8N HNO3; Centrifuged samples as needed, and passed through columns; Rinsed C-Tubes

with 20 ml 8N HNO3; Centrifuged rinsates and loaded onto columns; Rinsed columns with 40 ml 8N HNO3;

Eluted Thorium with 50 ml of 8N HCI into clean, labeled 100-ml beakers; Dried-down samples on hotplate;

Dissolved samples in -1 O ml of concentrated HCI; Transferred to new, labeled C-Tubes with deiononized

water brinaina volume to -1 Sml. Set samples aside for later orecipitation and filterina.

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0054

Printed: 3/30/2018 4:54 AM Page 1 of 1

~ Oal< Ridge Laboratory Internal Work Order 18-03111 601 Scarboro Rd. . ..•

EBER~~~c~ Oak Ridge, TN 37830 Analysis Code ThlSO Work Order Analysis Notes Voice: 865,481.0683 M•~---•---••••--• ------··-·-~- ··~- -·~·"-""-

www.eberlineservices.com Run Number 1

# Date Dept User Notes

1 03/28/18 08: 15 PREP JHARVEY ALIQUOTED AND ADDED SPIKES AND TRACERS- ADDED HF AND DRIED SAMPLES DOWN- ADDED

MIXED ACIDS AND TOOK SAMPLES TO DRYNESS- SUBMITTED SAMPLES TO SEPARATIONS

2 03/29/18 15: 19 CHEM JDEMELAS Added concentrated HNO3 to sample beakers and heated to dryness; Added 20 ml 8N HNO3 to samples and

transferred to new, labeled C-Tubes, adding 8N HNO3 to bring volume to ~35 ml; Preconditioned resin

columns with 50 ml 8N HNO3; Centrifuged samples as needed, and passed through columns; Rinsed C-Tubes

with 20 ml 8N HNO3; Centrifuged rinsates and loaded onto columns; Rinsed columns with 40 ml 8N HNO3;

Eluted Thorium with 50 ml of 8N HCI into clean, labeled 100-ml beakers; Dried-down samples on hotplate;

Dissolved samples in ~10 ml of concentrated HCI; Transferred to new, labeled C-Tubes with deiononized

water, bringing volume to ~15ml. Set sameles aside for later erecieitation and filtering.

3 03/30/18 04:54 CHEM TSMITH Followed steps 12.2.5 to 12.4.5 in AP-005. ( Precipitated and filtered samples for Thorium)

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0055

Eberline Analytical Oak Ridge Laboratory

Printed: 3/30/2018 4:59 AM Page 1 of 1

-----------N·-----·-·-------~-

Q EBERLINE ® ·······························. SERv1c::Es

Reagents Used in an Analysis

Reagent ID

019621P

019673P

019529P

019351P

Reagent Name

Hydrofluoric Acid

Nitric Acid

Perchloric Acid

Sulfuric Acid

Internal Work Order

18-03111 Analysis Code

·-············---·-···---- ----------

ThISO ----•-•" w -··-··--··-- ,_

Reagent Analyst Concentration ID

Reagent Grade )HARVEY

Reagent Grade JHARVEY

Reagent Grade JHARVEY

Reagent Grade JHARVEY

Run

1 Date

Recorded

3/28/2018

3/28/2018

3/28/2018

3/28/2018 -,-~~-·-··-~···--···-----+--------·--------<------------>---------+---

0l 7230P Anion Exchange Resin Reagent Grade JDEMELAS ·········-·-l---------------+-----------+--

019831P Hydrochloric Acid Reagent Grade

Nitric Acid SN 019841S

019859S

019860S

019673P

·•····+···-····-·•·•···············-···············--------+------····-········-

019803S ···--···-·-----

019578S

Hydrochloric Acid

Nitric Acid

Nitric Acid

Carbon substrate

Cerrium Carrier

SN

SN

Reagent Grade

Solution

0.lmg/ml

JDEMELAS

JDEMELAS

JDEMELAS

JDEMELAS

JDEMELAS

TSMITH

TSMITH ----------+-------------t--------

019525P Hydrofluoric Acid Reagent Grade TSMITH ········-·····················•·····~····-·····-······-·········---·---------+-----

o 19599P Reagent Alcohol Reagent Grade TSMITH

3/29/2018

3/29/2018

3/29/2018

3/29/2018

3/29/2018

3/29/2018

3/30/2018

3/30/2018

3/30/2018

3/30/2018 ··················-·------------~---------~--------'··································'

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0056

u \ < . l_k_(SU_~_· --t--:~~~\--1----"--""·~,::___- ----

l \ l~ ' ~I\,~-...:.. Yi,J.i!. JC12~-----:c.i • l...(.!c) Zh 6--e>;1u}1 'KCi.. & /(P, ·.

&. r-r.o I ·Z-1,rs~ ,-;, · ·p -_ · · ".::;; A-Lev...,. ·~ t"'-1 \3 ;)..k. ... ~ . ...::. y_1,,., l~ W --_,_,

-=--____________,,_--+-----=-U-"-".u.'-'--;;; .:...::..1--., __ -1-------'l:.....J-_ l '-:l_ ~~ . .:- \q) -_-_, v-l ?J J... · t, tSb....: ~~ •---

!LP

~~'.:..__~~e'....!'...2...---------J---'O~-'?~________,____,,"-'--'--'--'-----_,____, -~oe;-

--------"'---'~'---b-"---------------'--""------i------------"~~---+---0""'---=5-o_&l_i--=---'-L__._L..J"'-~- _,____~-----""---------------1---'-----'-----

o00 + i~k-~~~~L_L_c__J.......~~­

-'--'-_,,_,'--------+---~~-----------l- Df§oii_ .z.h_5-01J1k.4----L-'-,.,k-----,__-----+-'(__.::._Y._ L-----------

,1 '(©-/ \-i>

(..1J.. t> o· 5 > -z. h ~1ti't_t1 W. ~ o•:;-fCf 7...bi so ft-11~1 JS~

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0057

GAMMA NOTES

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0058

/ GG\

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0059

f.'------ ------+-------1--------1----+-----I-----

t::,.----------1---------1

~-- ------~----1--------1-----1---~--­

--------.:i-'i; ,§r----

,:it --------.::-f~---t-------+-------i---+------+---------1-----­

:z:

l--+--------+-------1---------+------1---------t...-­

'ffij

--i----------1-----------+------+-----it---------!--------

--------

--------1-------t------+----i-----------------l------------+-

--------t------------+-------------I----

Page 60: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0060

SECTION VIII

ANALYTICAL DATA (ISOTOPIC URANIUM)

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0061

Eberline Analytical Oak Ridge Laboratory

Analysis Sheet

Work Order ... oac I UUISO I

1 Date Received 3/23/2018

Lab Deadline 4/12/2018

Client Auxier & Associates, Inc.

Project WESTLAKE NCC

Report Level 4

Activity Units pCi

Aliquot Units g

Matrix so

Method EPA 908.0 Modified

Instrument Type Alpha Spectroscopy

Radiometric Tracer U-232

Radiometric Sol# U-10a

Tracer Act (dpm/g) 18.21

Carrier

Carrier Cone (mg/ml)

18-03111 UUISO Run 1

Printed: 3/30/2018 4:58 AM Page 1 of 3

! ' !

Internal i Sample i Client I Login I Sample Sample

Fraction Desc [ ID , CPM I Date Aliquot

01 i LCS i LCS I I 03/23/18 00:00 1.0000E+00

02 r MBL r BLANK ---- : 03/23/18 00:00 1.0000E+00

I I --

03 DUP I AC-SED-11 -- _ 63 03/21/1813:20 1.0018E+00

04 DO I AC-SED-11 63 03/21 /18 13:20 1.0080E+00

I

I

I

I I I

i I I

i

I

i

: I I

t------+1

- i I

' I !

I • , I I !

l---~,--~-1 l

i I !

i I ---·-,· -

I

I

i i

* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. "Indicates estimated SAF value.

** Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

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0062

Eberline Analytical Oak Ridge Laboratory Analysis Sheet

Tracer Internal I Sample 1

Fraction I Desc \ Aliquot (g)

01 LCS I i

0.6057

02 MBL I 0.6068

I

03 DUP 0.6077

04 DO 0.6068

I

I

Tracer Total ACT(dpm)

11.0 I

11.0

11.1

11.0

I

I

I Radiometric Tracer {pCi)

l

I

i

I

I

18-03111 UUISO Run 1

Radiometric i Grav Carrier Grav Filter

%Rec I Added (ml) I

Tare (g)

o.ooi I

o.oo[

o.oo[

0.00

'

I I Grav Filter I I Final (g) I

!

i I

I !

I

I

!

I

i ! i I

i I

I

• SAF1 is used for-Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. A Indicates estimated SAF value.

•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

! I

Grav Filter Grav Net(g) %Rec

I

I

I

Printed: 3/30/2018 4:58 AM Page 2 of 3

Mean SAF SAF %Rec 1· 2·

-

I I

I ii

I I I

I

I I

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0063

Eberline Analytical 18-03111 Oak Ridge Laboratory

UUISO Analysis Sheet

Run 1

Internal Sample Rough Prep

I Rough Prep Prep Prep Sep to

Fraction Desc Date By Date By Date/Time i

01 LCS I 03128118 01:s1 I JHARVEY

02 MBL I I 03/28/18 01:57 I JHARVEY

03 DUP I I 03/28/18 07:57 I JHARVEY

04 DO I 03/27/18 06:45 I KSALLINGS I 03/28/18 07:57 I JHARVEY

-

:

I I

i

I I -

• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. ~ Indicates estimated SAF value.

•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

Sep to By

Printed: 3/30/2018 4:58 AM Page 3 of 3

Sep t1 Date/Time

I !

__ I

Sep t1 By

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0064

Eberline Analytical Oak Ridge Laboratory

( Lab I Nuclide Fraction

01 U-234

§ 0:::

i 0 0 -r!! U)

~ QI i:: "(

~, 0

"""'"

0 en -::::> ::::>

CJ C

u, Cl) -ca CJ 0 u, u, <(

ca ... • 5!:? >< ::::, <(

02 U-234

03 U-234

04 U-234

Sample Desc

LCS

MBL

DUP

DO

Preliminary Data Report & Analytical Calculations

Work Order: 18-03111-UUISO-1

Client

I Activity

Results Error Estimate I MDA Identification Units

I I

LCS pCi/g 6.71E+00 9.02E-01 I 7.09E-02

BLANK pCi/g 1.GGE-02 4.01E-02 8.04E-02

AC-SED-11 pCi/g 6.S0E-01 1.95E-01 1.12E-01

AC-SED-11 pCi/g 9.93E-01 2.42E-01 9.59E-02

I

LCS LCS Known %R

7.27E+00 92.20

Printed: 4/2/2018 8:31 AM Page 1 of 3

LCS RPO

I MDA Blank

Flag Flag Flag Flag

OK OK

OK OK

INV OK

OK

Page 65: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0065

Eberline Analytical Oak Ridge Laboratory

( Lab Nuclide

Fraction

01 U-234

§ a::

.g 0 0

-!!! ~ iii C:

c:i:

~I

~

0 en -::, ::,

. CJ C:

tn Cl) ..... . ! CJ 0 tn tn

<3'.: ca ~ Cl)

'>< ::::s

<3'.:

02 U-234

03 U-234

04 U-234

Sample Desc

LCS

MBL

DUP

DO

Preliminary Data Report & Analytical Calculations

Work Order: 18-03111-UUISO-1

Sample Sample Radiometric Grav

I Mean

Date Aliquot % Rec %Rec % Rec

03/23/18 00:00 1.00E+00 140.90 0.00 0.00

03/23/18 00:00 1.00E+00 126.70 0.00 0.00

03/21/18 13:20 1.00E+00 116.92 0.00 0.00

03/21/18 13:20 1.01E+00 112.61 0.00 0.00

SAF I

SeptO Date/Time

Printed: 4/2/2018 8:31 AM Page 2 of 3

Sept1 Date/Time

I

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0066

Eberline Analytical Oak Ridge Laboratory

<( Lab I Nuclide Fraction

01 U-234

§ a::

~ 0 0

-~ ~ ci.i r:: q:

1: Cl)

:::: 0

""'"

0 tn -::::, ::::,

CJ C:

u, Q) --~ CJ 0 u, u,

<C o6 I,.

Q)

>< ::::s

<C

02 U-234

03 U-234

04 U-234

I Sample Desc

LCS

MBL

DUP

DO

Preliminary Data Report & Analytical Calculations

Work Order: 18-03111-UUISO-1

Counting

I Halflife Detect Carrier

Count Counts

DatefTime (days) Time

03/30/18 13:04 A_Spec Alpha_003 170.02 5.66 E+02

03/30/18 13:04 A_Spec Alpha_004 170 1.47 E+00

03/30/18 13: 04 A_Spec Alpha_010 170.02 5.28 E+01

03/30/18 13:04 A_Spec Alpha_011 170.02 8.28 E+01

Bkg CPM

5.00 E-03

9.00 E-03

1.90 E-02

1.30 E-02

I

Printed: 4/2/2018 8:31 AM Page 3 of 3

Eff

15.9

18.5

18.4

19.5

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0067

Eberline Analytical Oak Ridge Laboratory

,: Lab Nuclide Fraction

01 U-238

C: ~ ll:

.g 0 0

-!!? ~ .; C: "(

~I

~

0 en -::, ::,

0 s:: u, Q) -.!2 0 0 u, u, <(

~ ... Q)

>< ::, <(

02 U-238

03 U-238

04 U-238

Sample Desc

LCS

MBL

DUP

DO

Preliminary Data Report & Analytical Calculations

Work Order: 18-03111-UUISO-1

Client Activity Results Error Estimate MDA I

Identification Units I I

LCS pCi/g 7.12E+00 9.46E-01 7.43E-02i

BLANK pCi/g -2.25E-04 2.39E-02 7.10E-02

AC-SED-11 pCi/g 7.25E-01 2.0SE-01 1.07E-01

AC-SED-11 pCi/g 7.SSE-01 2.10E-01 7.52E-02

LCS LCS

I Known %R

7.05E+00 101.10

Printed: 4/2/2018 8:31 AM Page 1 of 3

LCS RPD

I MDA Blank

Flag Flag Flag Flag

OK OK

OK OK

OK OK

OK

Page 68: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0068

Eberline Analytical Oak Ridge Laboratory

( . - Lab Nuclide

Fraction

01 U-238

§ It:

.g 0 u

-!!! ~ iii C: <:(

II

~

0 u, -:::, :::,

(.) C

en Cl) -.! (.)

0 en en <(

~ I.. Cl)

">< :::s <(

02 U-238

03 U-238

04 U-238

Sample Desc

LCS

MBL

DUP

DO

Preliminary Data Report & Analytical Calculations

Work Order: 18-03111-UUISO-1

Sample Sample Radiometric

I Grav Mean

Date Aliquot %Rec %Rec %Rec

03/23/18 00:00 1.00E+00 140.90 0.00 0.00

03/23/18 00:00 1.00E+00 126.70 0.00 0.00

03/21/18 13:20 1.00E+00 116.92 0.00 0.00

03/21118 13:20 1.01E+00 112.61 0.00 0.00

SAF I

SeptO Date/Time

Printed: 4/2/2018 8:31 AM Page 2 of 3

I Sept1

Date/Time

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0069

Eberline Analytical Oak Ridge Laboratory

~ Lab

Nuclide Fraction

01 U-238

C: ::s 0::

i 0 0 ,!!! !g_ ca C: ct

~I

~

0 Cl) -::> ::>

(.) C

(/) Cl) -ns (.)

0 (/) (/) <(

~ a.. -~ >< ::s <(

02 U-238

03 U-238

04 U-238

i Sample Oesc

LCS

MBL

DUP

DO

Preliminary Data Report & Analytical Calculations

Work Order: 18-03111-UUISO-1

Counting

I Halflife

Detect Carrier Count I

Counts Date/Time (days) Time I

03/30/18 13:04 A_Spec Alpha_003 170.02 6.04 E+02

03/30/18 13:04 A_Spec Alpha_004 170 -2.00 E-02

03/30/18 13:04 A_Spec Alpha_010 170.02 5.91 E+01

03/30/18 13:04 A_Spec Alpha_011 170.02 6.60 E+01

8kg CPM

6.00 E-03

6.00 E-03

1.70 E-02

6.00 E-03

Printed: 4/2/2018 8:31 AM Page 3 of 3

Eff

15.9

18.5

18.4

19.5

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0070

Eberline Analytical Oak Ridge Laboratory

~ '\3

C: ::, a:

~ 0 (.)

.r!,!

~ iii C: q;

:: .!l;! u

"'"""

0 en -:::, :::,

0 s:: u, Cl) .... ca 0 0 u, u, <(

~ .... Cl)

'>< :::, <(

Lab Nuclide

Fraction

01 U-235

02 U-235

03 U-235

04 U-235

Sample Desc

LCS

MBL

DUP

DO

Preliminary Data Report & Analytical Calculations

Work Order: 18-03111-UUISO-1

Client

I Activity

Error Estimatel I

Results MDA I Identification Units

LCS pCi/g 4.97E-01 1.78E-01 9.21E-02

BLANK pCi/g -5.02E-03 3.04E-02 9.57E-02

AC-SED-11 pCi/g 1.54E-01 1.0GE-01 1.15E-01

AC-SED-11 pCi/g 8.12E-02 7.21E-02 7.76E-02

LCS I LCS

I Known %R

Printed: 4/2/2018 8:31 AM Page 1 of 3

LCS

I RPD MDA Blank

Flag Flag Flag Flag

OK

OK OK

NA OK

OK

Page 71: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0071

Eberline Analytical Oak Ridge Laboratory

( Lab !

Fraction I Nuclide

01 U-235

§ a:

i 8 -!!? ~ <ii I: q:

C: -~ 0

~

0 u, -=> =>

0 C:

r/) Q) -.! 0 0 r/) r/) <{

06 a.. Q)

">< :::s <{

02 U-235

03 U-235

04 U-235

Sample Desc

LCS

MBL

DUP

DO

Preliminary Data Report & Analytical Calculations

Work Order: 18-03111-UUISO-1

Sample Sample Radiometric Grav Mean

Date Aliquot %Rec %Rec %Rec

03/23/18 00:00 1.00E+00 140.90 0.00 0.00

03/23/18 00:00 1.00E+00 126.70 0.00 0.00

03/21/18 13:20 1.00E+00 116.92 0.00 0.00

03/21/18 13:20 1.01E+00 112.61 0.00 0.00

I Sep to SAF I Date/Time

Printed: 4/2/2018 8:31 AM Page 2 of 3

I Sept1

Date/Time

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0072

Eberline Analytical Oak Ridge Laboratory

( Lab Nuclide Fraction

01 U-235

C: ::i a::

,§ 8 -!!! ~ ;; C: q:

1) 0

""'""

0 en -::::, ::::,

(.) C:

th .s cu (.) 0 th th <(

o6 I.,

Cl)

>< :::s <(

02 U-235

03 U-235

04 U-235

Sample Desc

LCS

MBL

DUP

DO

Preliminary Data Report & Analytical Calculations

Work Order: 18-03111-UUISO-1

Counting Halflife Detect Carrier

Count Counts

Date/Time (days) Time

03/30/18 13:04 A_Spec Alpha_003 170.02 3.40 E+01

03/30/18 13:04 A_Spec Alpha_004 170 -3.60 E-01

03/30/18 13:04 A_Spec Alpha_010 170.02 1.01 E+01

03/30/18 13:04 A_Spec Alpha_011 170.02 5.49 E+00

8kg CPM

6.00 E-03

8.00 E-03

1.10 E-02

3.00 E-03

Printed: 4/2/2018 8:31 AM Page 3 of 3

Eff

15.9

18.5

18.4

19.5

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0073

~ /

4

Count Room Report Client: Auxier Associates, Inc.

Internal Fraction

01

02

03

04

Sample Desc

LCS

MBL

DUP

DO

Client ID

LCS

BLANK

AC-SED-11

AC-SED-11

18-03111-UUISO-1 (pCi/g) in SO Tracer ID: U-1 0a

Printed: 3/30/2018 4:58 AM Page 1 of 1

Sample Date

03/23/18 00:00

Sample Aliquot

Tracer Aliquot (g)

Tracer ACT{dpm)

Radiometric Tracer (pC1J

Radiometric I %Rec I

I

1.0000 o.6057 11.0298 I o.oo

SAF 1·

03/23/18 00:00 1.0000 0.6068 i 11.0498 I 0.00

03/21/1813:20 1.0018 0.6077 I - 11.0662 I 0.00 I

0312111813:20 1.0080 o.6068 I 11.0498 I o.oo

I

SAF 2•

---· .. ~ t ____ I I I I i

!

j_ -~----~-----~--~ __ _j_

- i ' •

I I i ! i

f--------------

---~-·----- --- :

i

--------------·----+------+----------<

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0074

Eberline Analytical Oak Ridge Laboratory

LCS & Matrix Spikes

Isotope Sol#

U-234 U-8a

U-238 U-8a

fraction Isotope

01 U-232

02 U-232

03 U-232

04 U-232

Version 2.0 08/99

Activity dpmlg

32.0001

Solution Date

3/28/2018

31.0ooj 3/28/2018

Tracers

Sol# Activity dpm/g

U-10a 18.210

U-10a i 18.210

U-10a i 18.210 I

U-10a 18.210

Approx Addff:ion

0.550

0.550

I Solution Date

3/28/2018

3/28/2018

3/28/2018

3/28/2018

I

Spike and Tracer Worksheet

Analysis Code

UUISO LCS

Volume Used (g)

0.5046

0.5046

Volume Used(g)

0.6057

0.6068

0.6077

0.6068

I I

MS Volume Used (g)

Approx Addition

0.6600

0.6600

0.6600

0.6600

Date

3/28/2018 7:55

LCSD T MSD Volume I

Volume Used(g) Used(g)

Technician

JHARVEY

T LCS MS -

I Known Error Added

I Error

pCi Estimate pCi Estimate

7.27 0.262 o.ooi 0.000 I

7.05 0.254 o.ooi 0.000

Balance Printer Tapes

Tracer

Page 1 of 1 Printed: 3/28/2018 7:57 AM

Technician Initials Witness Initials

-------CCSD MSD

Known I Added I Error \ Error I pCi Estimate pCi I

Estimate

o.oo/ 0.000 0.00; 0.000 I ------

o.ool 0.000 I

0.001 0.000

LCS

Matrix Spike

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0075

Lab

Eberline Analytical Oak Ridge Laboratory

Auxier & Associates, Inc.

Fraction Client ID

01 LCS 02 BLANK 03 AC-SED-11 04 AC-SED-11

Comments

Analysis Code

UUISO

Sample Muffle Data Ratio

Type Post/Pre

LCS MBL DUP DO

Techn;ciaoc ~ ~ Gl.J\~;:=:;i

Aliquot Worksheet

Rpt Units Lab Deadline

grams 4/12/2018

Dilution Data Aliquot Data

No of Dils Dil Factor Ratio Aliquot Net Equiv

1.0000E+00 1.0000E+00

1.0000E+00 1.0000E+00

1.0018E+00 1.0018E+0O

1.0080E+00 1.0080E+00

Date: ~(@_;~

Technician

JHARVEY

MS Aliquot Data

Printed: 3/28/2018 7:51 AM Page 1 of 1

H-3 Solids Only Water Actcteu H:nnst--

Aliquot Net Equiv (ml) Aliq

i

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0076

Eberline Services - Oak Ridge Prep Logbook Version 2.0 8/1999

Eberline Auxier & Associates, Inc. Fraction Client ID

04 AC-SED-11

Comments

Special Codes

Technician: ¼"27 ,.s·:::::5:

Lab Deadline

4/12/2018

Tare (g) Pan Wt

28.2500

Rough Sample Preparation Log Book

Date Received in Prep Date Sealed

3/26/2018 3/27/2018

Gross (g) Net (g) WetWt. Dry Wt. Wet Wt. I Dry Wt.

1839.8000 1287.5600 , _ 1811.5501- 1259.3100

------

----·- ---------!-----------·----.

---·-· -

----

---------~-------------~----

-----

----

Date Returned

3/28/2018

Percent Liquid r·-· Solid

3o.4s%I 69.52% ___ , !

·----·----•--~-

i

- .. -----~-i--·····---_I•··· I

I

I I I

Printed: 3/27/2018 6:45 AM Page 1 of 1

Technician

KSALLINGS

Gamma Special Dry Wt. LEPS Wt. Info

0.00001 0.0000

.--------

i

-------- ---·- ------·-

I ----

I

'

I

H: Hot, 0: Qrnanic Hazard, e..=_ PCB Haza.-g,~R: Rush,_I:__ Other (see comments)

Date:Analysis: Rough Prep Logbook Analysis: UUISO Page No. 10439

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0077

-11Apex-Alpha'" Sample Description: Spectrum File: Batch Identification:

SPIKE \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002099

1803111A-UU

Sample Identification: Sample Geometry: Procedure Description:

Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:

Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:

Tracer Certificate: Tracer Quantity: Effective Efficiency:

01 Shelf 2 U iso

Alpha_003

3 System Bkgd 211450

<not performed>

l.000E+000 3/30/2018 3/30/2018

170.0

+/- 0.000E+000 gram 6:48:14 AM 1:04:28 PM

minutes 170.0 minutes

0.0121

Counting Efficiency:

U232 UU-l0A 0.606 mL 0.2241 +/-0.1591 +/-1.4090 +/-

0.0028 on 2/16/2018 0.0804

3:44:29 PM

Chem. Recovery Factor:

Control Certificate Name: NatU U-8A Chem. Recov. of Control: U-238 0.889436 +/- 0.065927

Peak Match Tolerance: 0.150 MeV

Nuclide

U-232 T U-234 U-235 U-238

Energy (MeV)

5.268 4.720 4. 371 4.139

PEAK AREA REPORT

Net Pk Area

416.98 566.15

33.98 603.98

Pk Area Error%

9.61 8.24

34.21 7.98

Ambient Backgnd

1.02 0.85 1.02 1.02

Reagent Backgnd

0.00E+000 0.00E+000 0.00E+000 0.00E+000

FWHM (keV)

6.8 4.8 3.0

46.1

T Tracer Peak used for Effective Efficiency

Nuclide

U-232 U-234 U-235 U-238

Id Conf.

0.991 0.988 0.999 0.986

NUCLIDE ANALYSIS RESULTS

Energy (keV)

5302.50* 4761.50* 4385.50* 4184.40*

Activity (pCi/gram

4.94E+000 +!- 5.25E-001 6.71E+000 +!- 9.02E-001 4.97E-001 +!- l.78E-001 7.12E+000 +/- 9.46E-001

I¼ 1/i(rs

MDA (pCi/gram

7.46E-002 +!-7.09E-002 +!-9.21E-002 +!-7.43E-002 +/-

7.93E-003 7.53E-003 9.78E-003 7.89E-003

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0078

60

55

50

45

40

35 V> -I-' C: :::s 8 30

25

20

15

10

5

0 r Ill I I rn IIIIIA Alll!IWl!IIOONVIW\ Ii · , ,1 Ah, ;, du ' · \ MIMI/II I 3500

1 111' \

4000 4500

ROI Type: 1

0000209976.CNF

I ,I I A 1 [PHI II 11111\IYI jl 1 1

5000 Energy(kev)

IM A I IA

5500

Live Time :10201.000 sec Rea 1 Ti me : 10201. 000 sec Start: 1:3496.G(kev) Stop : 1024:6544.G(kev) Acq. start :Fri Mar 30 13:04:28 2018

1 1 Al ! A 1 I I A I I

6000

ROI Type: 3

A I I I

6500

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0079

Channel Data Report 3/30/2018 3:59:09 PM Page 1

******************************************************* ***** s p E C T R A L DAT A R E P O R T ***** *******************************************************

Sample Title: 01

Elapsed Live time: 10201 Elapsed Real Time: 10201

Channell------l-------1-------1-------1-------I-------I-------I-------I 1: 10201 10201 0 0 0 0 0 0

9: 0 0 0 0 0 0 0 0

17: 1 0 0 0 0 0 1 0

25: 0 0 0 0 0 0 0 0

33: 0 0 0 0 0 0 0 1

41: 0 0 0 0 0 0 0 0

49: 0 0 0 0 0 0 0 0

57: 0 0 0 0 1 0 0 0

65: 0 0 1 0 0 0 0 0

73: 1 0 1 0 0 0 1 0

81: 0 0 0 0 0 0 0 0

89: 0 0 0 1 1 0 0 1

97: 2 1 1 0 0 0 0 0

105: 0 1 0 0 0 0 0 0

113: 0 0 0 0 1 0 0 2

121: 0 0 0 2 0 1 0 0

129: 0 1 1 0 1 0 2 0

137: 0 0 1 0 0 0 2 0

145: 0 2 0 1 0 0 1 0

153: 2 1 1 0 1 1 1 0

161: 4 1 2 0 1 0 1 2

169: 1 2 1 1 4 2 2 1

177: 5 2 1 6 3 3 4 2

185: 2 4 5 3 6 5 4 3

193: 6 1 3 3 3 4 7 6

201: 2 6 8 12 7 11 12 7

209: 1 4 10 9 13 13 13 11

217: 16 14 9 19 14 19 16 17

225: 16 16 21 14 17 18 23 15

233: 14 18 9 17 11 9 5 7

241: 0 2 0 2 0 0 0 0

249: 0 0 0 1 0 0 0 0

257: 0 0 1 1 0 0 0 0

265: 1 0 0 0 1 0 0 0

273: 1 1 2 0 1 0 0 1

281: 1 1 1 1 2 1 0 1

289: 1 0 0 0 2 1 0 3

297: 0 0 1 1 2 2 0 0

305: 1 0 1 0 1 1 1 0

313: 0 0 0 0 0 0 0 0

321: 0 0 0 1 0 0 1 1

329: 0 0 0 0 0 0 0 0

337: 0 0 0 0 0 1 0 0

345: 1 0 0 0 1 2 1 0

353: 1 0 1 0 2 1 0 0

361: 1 2 1 0 0 1 5 1

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0080

Channel Data Report 3/30/2018 3:59:09 PM Page 2

369: 1 1 2 1 1 1 2 3

Sample Title: 01

Channell------l-------l-------l-------1-------1-------1-------I-------I 377: 3 4 3 4 1 2 1 3

385: 3 7 5 3 5 11 6 3

393: 10 5 6 4 13 6 4 10

401: 6 9 14 6 8 14 10 8

409: 15 9 9 14 11 13 19 10

417: 24 8 13 17 15 21 17 22

425: 18 21 17 14 12 13 12 7

433: 5 1 3 0 0 0 0 0

441: 0 0 0 0 0 0 0 0

449: 0 0 0 0 0 0 0 0

457: 0 0 0 0 0 0 0 0

465: 0 0 0 0 0 0 0 0

473: 0 0 0 0 0 0 0 0

481: 0 0 0 0 1 0 0 0

489: 0 0 0 0 0 0 0 0

497: 1 0 0 0 0 0 0 0

505: 0 0 0 1 0 0 0 0

513: 1 0 1 0 1 1 1 0

521: 0 0 0 0 0 0 1 2

529: 1 0 0 0 0 0 0 2

537: 0 0 0 1 2 0 1 1

545: 0 0 2 1 0 1 2 1

553: 2 1 0 1 2 4 2 1

561: 0 1 3 5 1 0 2 1

569: 2 4 2 6 7 3 3 4

577: 5 3 3 6 4 5 6 9

585: 5 4 5 5 6 13 7 10

593: 15 16 10 9 6 12 8 9

601: 9 12 9 15 12 15 14 16

609: 5 18 12 7 14 6 5 8

617: 1 4 0 1 0 0 0 0

625: 0 0 0 0 0 0 0 0

633: 0 0 0 0 0 0 0 0

641: 0 1 0 1 0 0 0 0

649: 0 0 0 0 0 1 0 0

657: 0 0 0 0 0 0 0 0

665: 0 0 0 0 0 0 0 0

673: 0 0 0 0 0 0 0 0

681: 0 0 0 0 0 0 0 0

689: 0 0 0 0 0 0 0 0

697: 0 0 0 0 0 0 0 0

705: 0 0 0 0 0 1 0 0

713: 0 0 0 0 0 0 0 0

721: 0 0 0 0 0 0 0 0

729: 0 0 0 0 0 0 0 0

737: 0 0 0 0 0 0 0 0

745: 0 0 0 0 0 0 0 0

753: 0 1 0 0 0 0 0 0

761: 0 0 0 0 0 0 0 0

769: 1 0 0 0 0 0 0 0

777: 0 0 0 0 0 0 0 0

785: 1 0 0 0 0 0 0 0

793: 0 0 0 1 0 0 0 0

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0081

Channel Data Report 3/30/2018 3:59:09 PM Page 3

801: 0 0 0 0 0 0 0 0

Sample Title: 01

Channell------l-------l-------1-------1-------1-------I-------I-------I 809: 0 0 0 0 0 0 0 0

817: 0 0 0 0 0 0 0 0

825: 0 0 0 0 0 0 0 0

833: 0 0 0 0 0 0 0 0

841: 0 0 0 0 0 0 0 0

849: 0 0 0 0 0 0 0 0

857: 0 0 0 0 0 0 0 0

865: 0 0 0 0 0 0 0 0

873: 0 0 0 0 0 0 0 1

881: 0 0 0 0 0 0 0 0

889: 0 0 0 0 0 0 0 0

897: 0 0 0 0 0 0 0 0

905: 0 0 0 0 0 0 0 0

913: 0 0 0 0 0 0 0 0

921: 0 0 0 0 0 0 0 0

929: 0 0 0 0 0 0 0 0

937: 0 0 0 0 0 0 0 0

945: 0 0 0 0 0 0 0 0

953: 1 0 0 0 0 0 0 0

961: 0 0 0 0 0 0 0 0

969: 0 0 0 0 0 0 0 0

977: 0 0 0 0 0 0 0 0

985: 0 0 0 0 0 0 0 0

993: 0 0 0 0 0 0 0 0

1001: 0 0 0 0 0 0 0 0

1009: 0 0 0 0 0 0 0 0

1017: 0 0 0 0 0 0 0 0

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0082

_,A Al h TM ~/-\pex- p a Sample Description: Spectrum File: Batch Identification:

BLANK \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002099

1803111A-UU Sample Identification: Sample Geometry: Procedure Description:

Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:

Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:

Tracer Certificate: Tracer Quantity: Effective Efficiency:

02 Shelf 2 U iso

Alpha_004

4 System Bkgd 211451

<not performed>

l.000E+000 3/30/2018 3/30/2018

+/- 0.000E+000 gram 6:48:14 AM 1:04:29 PM

170.0 minutes 170.0 minutes

U232 UU-l0A 0.607 mL 0.2347 +/- 0.0125

Counting Efficiency: 0.1853 +/- 0.0032 on 2/16/2018 1.2670 +/- 0.0708

3:44:30 PM

Chem. Recovery Factor:

Peak Match Tolerance:

Nuclide

U-232 T U-234 U-235 U-238

Energy (MeV)

5.270 4.680 4.487 4.161

0.150 MeV

PEAK AREA REPORT

Net Pk Area

437.49 1. 47

-0.36 -0.02

Pk Area Error%

9.38 240.74 604.15 10624.

Ambient Backgnd

0.51 1. 53 1. 36 1. 02

Reagent Backgnd

0.00E+000 0.00E+000 0.00E+000 0.00E+000

FWHM (keV)

27.9 2.9 2.9 2.9

T = Tracer Peak used for Effective Efficiency

Nuclide

U-232 U-234 U-235 U-238

Id Con£.

0.992 0.954 0.930 0. 996

NUCLIDE ANALYSIS RESULTS

Energy (keV)

5302.50* 4761.50* 4385.50* 4184.40*

Activity (pCi/gram

4.95E+000 +/- 5.15E-001 1. 66E-002 +/- 4.0lE-002

-5.02E-003 +/- 3.04E-002 -2.25E-004 +/- 2.39E-002

A~ 1(:2((¼

MDA (pCi/gram

5.94E-002 +/-8.04E-002 +!-9.57E-002 +!-7.l0E-002 +/-

6.18E-003 8.37E-003 9.96E-003 7.38E-003

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0083

60

55

50

45

40

35 Vl -I-' C: :::s 8 30

25

20

15

10

5 ~

0000209977.CNF

~ = ~ ' ::,

Live Time :10200.000 sec Real Time :10200.000 sec Start: 1:3488.l(kev) Stop : 1024:6492.S(kev) Acq. Start :Fri Mar 30 13:04:29 2018

0 F 1 1 1 11 'J: I I I i I !1

3500

1 1 i !I\ 'I l. . c ; 1 ! ! ! ! I U [ti ii 1 11

4000 4500 5000 Energy(kev)

I I I ! I I ! 1 I I I I I I I I 5500 6000 6500

ROI Type: 1 ROI Type: 3

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0084

Channel Data Report 3/30/2018 3:59:17 PM Page 1

******************************************************* ***** s p E C T R A L DAT A R E P O R T ***** *******************************************************

Sample Title: 02

Elapsed Live time: 10200 Elapsed Real Time: 10200

Channell------l-------l-------1-------1-------1-------I-------I-------I 1: 10200 10200 0 0 0 0 0 0

9 : 0 0 0 0 0 0 0 0

17: 0 0 0 0 0 0 0 0

25: 0 0 0 0 0 0 0 0

33: 0 0 0 0 0 0 0 0

41: 0 0 0 0 0 0 0 0

49: 0 0 0 0 0 0 0 0

57: 0 0 0 0 0 0 0 0

65: 0 0 0 0 0 0 0 0

73: 0 0 0 0 0 0 0 0

81: 0 0 0 0 0 0 0 0

89: 0 0 0 0 0 0 0 0

97: 0 0 0 0 0 0 0 0

105: 0 0 0 0 0 0 0 0

113: 0 0 0 0 0 0 0 0

121: 0 0 0 0 0 1 0 0

129: 0 0 1 0 0 0 0 0

137: 0 0 0 0 0 0 0 0

145: 0 0 0 0 0 0 0 0

153: 0 0 0 0 0 0 0 0

161: 0 0 0 0 0 0 0 0

169: 0 0 0 0 0 0 0 0

177: 0 0 0 0 0 0 0 0

185: 0 0 0 0 0 0 0 0

193: 0 0 0 0 0 0 0 0

201: 0 0 0 0 0 0 0 0

209: 0 0 0 0 0 0 0 0

217: 0 0 0 0 0 0 0 0

225: 0 0 0 0 0 1 0 0

233: 0 0 0 0 0 0 0 0

241: 0 0 0 0 0 0 0 0

249: 0 0 0 0 0 0 0 0

257: 0 0 0 0 0 0 0 0

265: 0 0 0 1 0 0 0 0

273: 0 0 0 0 0 0 0 0

281: 0 0 0 0 0 0 0 0

289: 0 0 0 0 0 0 0 0

297: 0 0 0 0 0 0 0 0

305: 0 0 0 0 0 0 0 0

313: 0 0 0 0 0 0 0 0

321: 0 0 0 0 0 0 0 0

329: 0 0 0 0 0 0 0 0

337: 0 0 0 0 1 0 0 0

345: 0 0 0 0 0 1 0 0

353: 0 0 0 0 0 0 0 0

361: 0 0 0 0 0 0 0 0

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0085

Channel Data Report 3/30/2018 3:59:17 PM Page 2

369: 0 0 0 1 0 0 0 0

Sample Title: 02

Channell------l-------l-------l-------l-------1-------1-------1-------I 377: 0 0 0 0 0 0 1 0

385: 0 0 0 0 0 0 0 0

393: 0 0 0 0 0 0 0 0

401: 0 0 0 0 0 0 0 1

409: 0 0 0 0 0 0 0 0

417: 0 0 0 0 0 0 0 0

425: 0 0 0 0 0 1 0 0

433: 0 0 0 0 0 0 0 0

441: 0 0 0 0 0 0 0 0

449: 0 0 0 0 0 0 0 0

457: 0 0 0 0 0 1 0 0

465: 0 0 0 0 0 0 0 0

473: 0 0 0 0 1 0 0 0

481: 0 0 0 0 0 0 0 0

489: 0 1 0 0 0 0 0 0

497: 0 0 0 0 0 0 0 0

505: 1 0 0 0 0 0 0 0

513: 0 0 0 0 0 0 0 0

521: 0 0 0 0 0 0 0 0

529: 1 0 0 0 0 0 0 1

537: 0 0 0 0 0 0 1 1

545: 1 0 1 0 0 0 0 3

553: 1 1 2 1 1 2 2 0 561: 1 0 0 1 2 1 2 1

569: 3 0 0 2 3 2 3 2 577: 4 0 1 1 1 2 1 2

585: 2 5 3 3 4 5 7 5 593: 6 6 5 9 7 7 12 7

601: 13 7 7 9 10 13 9 13 609: 13 12 10 8 7 11 13 15 617: 16 12 12 10 15 18 9 16 625: 15 7 7 5 1 0 1 0 633: 0 0 0 0 0 0 0 0 641: 0 0 0 0 0 0 0 0 649: 0 0 0 0 0 0 0 0 657: 0 0 0 0 0 1 0 0 665: 0 0 0 0 0 0 0 0 673: 0 0 0 0 0 0 0 0 681: 0 0 0 0 0 0 0 0 689: 0 0 0 0 0 0 0 0 697: 0 0 0 0 0 0 0 0 705: 0 0 0 0 0 0 0 0 713: 0 0 0 0 0 0 0 0 721: 0 0 0 0 0 0 0 0 729: 0 0 0 0 0 0 0 0 737: 0 0 0 0 0 0 0 0 745: 0 0 1 0 0 0 0 0 753: 0 0 0 0 0 0 0 0 761: 0 0 0 0 0 0 0 0 769: 0 0 0 0 0 0 0 0 777: 0 0 0 0 0 0 0 0 785: 0 0 0 0 0 0 0 0 793: 0 0 0 0 0 0 0 0

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0086

Channel Data Report 3/30/2018 3:59:17 PM Page 3

801: 0 0 0 0 0 0 0 0

Sample Title: 02

Channell------l-------l-------1-------1-------1-------I-------I-------I 809: 0 0 0 0 0 0 0 0

817: 0 0 0 0 0 0 0 0

825: 0 0 0 0 0 0 0 0

833: 0 0 0 0 0 0 0 0

841: 0 0 0 0 0 0 0 0

849: 0 0 0 0 0 0 0 0

857: 0 0 0 0 0 0 0 0

865: 0 0 0 0 0 0 0 0

873: 0 0 0 0 0 0 0 0

881: 0 0 0 0 0 0 0 0

889: 0 0 0 0 0 0 0 0

897: 0 0 0 0 0 0 0 0

905: 0 0 0 0 0 0 0 0

913: 0 0 0 0 0 0 0 0

921: 0 0 0 0 0 0 0 0

929: 0 0 0 0 0 0 0 0

937: 0 0 0 0 0 0 0 0

945: 0 0 0 0 0 0 0 0

953: 0 0 0 0 0 0 0 0

961: 0 0 0 0 0 0 0 0

969: 0 0 0 0 0 0 0 0

977: 0 0 0 0 0 0 0 0

985: 0 0 0 0 0 0 0 0

993: 0 0 0 0 0 0 0 0

1001: 0 0 0 0 0 0 0 0

1009: 0 0 0 0 0 0 0 0

1017: 0 0 0 0 0 0 0 0

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0087

~-~~pex-Alpha,. Sample Description: Spectrum File: Batch Identification:

AC-SED-11 DUP \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002099 1803111A-UU

Sample Identification: Sample Geometry: Procedure Description:

Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:

Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:

Tracer Certificate: Tracer Quantity: Effective Efficiency:

03 Shelf 2 U iso

Alpha_0l0

10 System Bkgd 211452

<not performed>

l.002E+000 +!- 0.000E+000 3/21/2018 6:48:14 3/30/2018 1:04:26

170.0 minutes 170.0 minutes

U232 UU-l0A 0.608 rnL 0.2152 +/- 0.0119

AM PM

gram

Counting Efficiency: Chern. Recovery Factor:

0.1841 +/- 0.0032 on 2/16/2018 1.1692 +/- 0.0675

3:44:30 PM

Peak Match Tolerance:

Nuclide

U-232 T U-234 U-235 U-238

Energy (MeV)

5.281 4.722 4.379 4.147

0.150 MeV

PEAK AREA REPORT

Net Pk Area

401.79 52.77 10.13 59.11

Pk Area Error%

9.81 27.93 67.91 26.21

Ambient Backgnd

2.21 3.23 1. 87 2.89

Reagent Backgnd

0.00E+000 0.00E+000 0.00E+000 0.00E+000

FWHM (keV)

8.6 4.9 2.9 4.9

T Tracer Peak used for Effective Efficiency

Nuclide

U-232 U-234 U-235 U-238

Id Conf.

0.997 0.989 1.000 0.990

NUCLIDE ANALYSIS RESULTS

Energy (keV)

5302.50* 4761.50* 4385.50* 4184.40*

Activity (pCi/grarn

4.95E+000 +!- 5.34E-001 6.50E-001 +/- l.95E-001 l.54E-001 +!- 1. 06E-001 7.25E-001 +!- 2.05E-001

Ni, lf/JftS

MDA (pCi/grarn

9.85E-002 +/-l.12E-001 +!-l.15E-001 +!-1. 07E- 001 +/-

l.06E-002 l.21E-002 l.24E-002 1.16E-002

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0088

60

55

50

45

40

35 V> -I-' C: :::l

8 30

25

20

15

10

5

0000209978.CNF

Live Time 10201.000 sec Rea 1 Ti me 10202. 000 sec Start: 1 3509.l(keV) stop : 1024 6494.S(kev) Acq. Start Fri Mar 30 13:04:26 2018

\1

0 II I !Mlfl ! Im I! Mq ,'\!!,rf.';i,i\'li!i llH'S,1,', ,\[ HH1 i'itfllpfi'!!l\il~A IMl\!11![! ! l~!IW!li:' 11 It!! I I I !I I [! I I ! I I '

4000

ROI Type: 1

4500 5000 Energy(kev)

5500 6000 6500

ROI Type: 3

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0089

Channel Data Report 3/30/2018 3:59:24 PM Page 1

******************************************************* ***** s p E C T R A L DAT A R E P O R T ***** *******************************************************

Sample Title: 03

Elapsed Live time: 10201 Elapsed Real Time: 10202

Channell------l-------1-------1-------1-------I-------I-------I-------I 1: 10202 10201 0 0 0 0 0 0

9 : 0 0 0 0 0 0 0 0

17: 0 0 0 0 0 0 0 0

25: 0 0 0 0 0 0 0 0

33: 0 0 0 0 0 0 0 0

41: 0 0 0 0 0 0 1 0

49: 0 0 0 0 0 0 0 1

57: 0 1 0 0 0 0 0 0

65: 0 0 0 0 0 0 0 0

73: 0 0 1 1 0 0 0 0

81: 0 0 0 0 0 0 0 0

89: 0 1 0 0 0 0 0 0

97: 0 0 0 0 0 0 0 0

105: 0 0 1 0 0 0 0 0

113: 0 1 0 0 0 1 0 0

121: 0 0 0 0 0 0 0 0

129: 0 0 0 0 0 0 0 0

137: 0 0 1 0 0 0 0 0

145: 0 0 0 0 0 0 0 0

153: 1 0 0 1 0 0 0 0

161: 1 0 0 0 0 0 0 0

169: 0 1 0 0 0 0 0 0

177: 0 0 0 0 0 0 0 0

185: 0 0 0 0 0 1 0 0

193: 1 0 1 0 0 2 1 1

201: 0 0 2 0 3 0 0 1

209: 2 1 0 1 1 3 1 1

217: 1 0 2 4 1 0 1 2

225: 0 3 4 2 0 1 3 1

233: 1 1 1 2 0 4 1 0

241: 0 0 2 0 1 0 0 0

249: 0 0 0 0 0 0 0 0

257: 0 0 0 0 0 0 0 0

265: 0 0 0 0 0 0 0 0

273: 0 0 0 0 0 0 1 0

281: 0 0 1 0 0 0 0 0 289: 0 1 0 0 0 2 0 0

297: 1 0 2 0 1 0 0 0

305: 0 1 0 0 0 0 0 0

313: 0 0 1 0 0 0 0 0

321: 0 0 0 0 0 0 0 0

329: 0 0 0 0 0 1 0 0

337: 0 0 0 0 0 0 0 0

345: 0 0 0 0 0 0 0 0

353: 0 0 0 0 0 0 0 1 361: 0 0 0 0 0 1 0 1

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0090

Channel Data Report 3/30/2018 3:59:24 PM Page 2

369: 0 0 0 0 0 0 0 0

Sample Title: 03

Channell------l-------l-------l-------1-------1-------1-------I-------I 377: 1 1 1 0 1 0 0 0

385: 0 0 0 0 0 0 0 0

393: 0 0 0 1 0 0 0 0

401: 0 2 1 0 2 4 1 2

409: 0 1 3 2 0 2 0 4

417: 0 1 0 4 1 2 0 3

425: 2 0 1 2 0 0 0 2

433: 0 2 1 2 1 0 1 0

441: 0 0 0 0 0 0 0 0

449: 0 0 0 0 1 0 0 0

457: 1 0 0 0 0 0 0 0

465: 0 0 0 0 0 0 0 0

473: 0 0 0 0 0 0 0 1

481: 0 0 1 0 0 0 0 0

489: 0 0 1 1 0 0 0 0

497: 0 1 0 0 0 0 0 2

505: 0 0 1 0 0 0 0 0

513: 0 1 0 0 0 0 0 0

521: 0 0 0 0 0 1 0 0

529: 0 0 0 0 0 0 0 0

537: 2 1 0 1 0 0 0 1

545: 0 0 0 0 1 0 0 0

553: 1 0 3 3 0 0 1 0

561: 0 0 1 2 1 2 1 0

569: 0 1 1 1 2 1 4 0

577: 0 5 1 2 3 1 1 2

585: 4 5 3 3 3 4 4 5

593: 5 2 7 4 4 6 7 4

601: 13 5 5 9 4 11 10 11

609: 11 13 13 8 13 6 21 16

617: 11 9 13 16 15 10 12 9

625: 9 11 8 3 2 0 1 2

633: 1 1 0 0 0 0 0 0

641: 0 0 0 0 0 0 0 0

649: 0 1 0 0 0 0 0 0

657: 0 0 0 0 0 0 0 0

665: 0 0 0 0 0 0 0 0

673: 0 0 0 0 0 0 0 0

681: 0 0 0 0 0 0 0 0

689: 0 0 0 0 0 0 0 0

697: 0 0 0 0 0 0 0 0

705: 0 0 0 0 0 0 0 0

713: 0 0 0 0 0 0 0 0

721: 0 0 0 0 0 0 0 0

729: 0 0 0 0 0 0 0 0

737: 0 0 0 0 0 0 0 0

745: 0 0 0 0 0 0 0 0

753: 0 0 0 0 0 0 0 0

761: 0 0 0 0 0 0 0 0

769: 0 0 0 0 0 0 0 0

777: 1 0 0 0 0 0 0 0

785: 0 0 0 0 0 0 0 0

793: 0 0 0 0 0 0 0 0

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0091

Channel Data Report 3/30/2018 3:59:24 PM Page 3

801: 0 0 0 0 0 0 0 0

Sample Title: 03

Channell------l-------l-------l-------1-------1-------1-------I-------I 809: 0 0 0 0 0 0 0 0

817: 0 0 0 0 0 0 0 0

825: 0 0 0 0 0 0 0 0

833: 0 0 0 0 0 0 0 0

841: 0 0 0 0 0 0 0 0

849: 0 0 0 0 0 0 0 0

857: 0 0 0 0 0 0 1 0

865: 0 0 0 0 0 0 0 0

873: 0 0 0 0 0 0 0 0

881: 0 0 0 0 0 0 0 0

889: 0 0 0 0 0 0 0 0

897: 0 0 0 0 0 0 0 0

905: 0 0 0 0 0 0 0 0

913: 0 0 0 0 0 0 0 0

921: 0 0 0 0 0 0 0 0

929: 0 0 0 0 0 0 0 0

937: 0 0 0 0 0 0 1 0

945: 0 0 0 0 0 0 0 0

953: 0 0 0 0 0 0 0 0

961: 0 0 0 0 0 0 0 0

969: 0 0 0 0 0 0 0 0

977: 0 0 0 0 0 0 0 0

985: 0 0 0 0 0 0 0 0

993: 0 0 0 0 0 0 0 0

1001: 0 0 0 0 0 0 0 0

1009: 0 0 0 0 0 0 0 0

1017: 0 0 0 0 0 0 0 0

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0092

~-~~Apex-Alpha™ Sample Description: Spectrum File: Batch Identification:

AC-SED-11 \\OR-ALPHAl\Canberra\Apex.Alpha\Root\Data\00002099

1803111A-UU

Sample Identification: Sample Geometry: Procedure Description:

Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:

Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:

Tracer Certificate: Tracer Quantity: Effective Efficiency:

04 Shelf 2 U iso

Alpha_0ll

11 System Bkgd 211453

<not performed>

l.008E+000 3/21/2018 3/30/2018

+/- 0.000E+000 gram 6:48:14 AM 1:04:27 PM

170.0 minutes 170.0 minutes

U232 UU-l0A 0.607 mL 0.2196 +/- 0.0120

Counting Efficiency: 0.1950 +/- 0.0034 on 2/16/2018 1.1261 +/- 0.0646

3:44:30 PM

Chem. Recovery Factor:

Peak Match Tolerance:

Nuclide

U-232 T U-234 U-235 U-238

Energy (MeV)

5.279 4.729 4.422 4.153

0.150 MeV

PEAK AREA REPORT

Net Pk Area

409.28 82.79

5 .49 65.98

Pk Area Error%

9.73 21.87 88.08 24.35

Ambient Backgnd

2.72 2.21 0.51 1. 02

Reagent Backgnd

0.00E+000 0.00E+000 0.00E+000 0.00E+000

FWHM (keV)

8.8 7.4 2.6 3.5

T Tracer Peak used for Effective Efficiency

Nuclide

U-232 U-234 U-235 U-238

Id Conf.

0. 996 0.993 0.990 0.993

NUCLIDE ANALYSIS RESULTS

Energy (keV)

5302.50* 4761. 50* 4385.50* 4184.40*

Activity (pCi/gram

4.91E+000 +/- 5.26E-001 9.93E-001 +!- 2.42E-001 8.12E-002 +/- 7.21E-002 7.88E-001 +!- 2.l0E-001

~IK

MDA (pCi/gram

l.03E-001 +/-9.59E-002 +/-7.76E-002 +/-7.52E-002 +/-

l.l0E-002 l.03E-002 8.33E-003 8.07E-003

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0093

V) ....,

60

55

50

45

40

35

C: ::::s 8 30

25

20

15

10

5

0000209979.CNF

Live Time :10201.000 sec Real Ti me : 10201. 000 sec Start: 1:3638.?(kev) Stop : 1024: 6325. 9(keV) Acq. Start :Fri Mar 30 13:04:27 2018

0 II I I A! ! n A 11!,\ ,\!U ii,j/i!/,/!jli l!Ji ,I //1 f \; I Ill ,r,n,u,,,1 ll 11 " M! 111 ! ~ A NIWl)lrn1,, ,I, I! A 'A IA I A I Ai I

4000

ROI Type: 1

4500 5000 Energy(kev)

5500 6000

ROI Type: 3

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0094

Channel Data Report 3/30/2018 3:59:31 PM Page 1

******************************************************* ***** s p E C T R A L DAT A R E P O R T ***** *******************************************************

Sample Title: 04

Elapsed Live time: 10201 Elapsed Real Time: 10201

Channell------l-------l-------l-------1-------1-------1-------I-------I 1: 10201 10201 0 0 0 0 0 0

9: 0 0 0 0 0 0 0 0

17: 0 0 0 0 0 0 0 0

25: 0 0 0 0 0 0 0 0

33: 0 0 0 0 0 0 0 0

41: 0 0 0 0 0 0 0 0

49: 0 0 0 0 0 0 0 0

57: 0 0 0 0 0 0 0 0

65: 0 0 0 0 0 0 0 1

73: 0 0 0 0 0 1 0 0

81: 0 0 0 0 0 0 0 0

89: 0 1 0 0 0 0 0 0

97: 0 0 0 0 0 1 0 0

105: 0 0 0 0 0 0 0 0

113: 0 0 0 0 0 0 0 0

121: 0 0 0 0 1 0 0 0

129: 0 0 0 0 0 0 1 0

137: 0 0 0 0 1 0 1 0

145: 0 0 0 0 0 0 1 0

153: 0 0 1 0 1 0 0 0

161: 0 1 0 0 0 0 0 0

169: 1 1 1 0 0 0 0 1

177: 2 0 1 1 1 0 0 0

185: 2 0 1 0 0 0 1 0

193: 0 3 1 4 1 0 2 0

201: 2 2 0 1 2 3 1 2

209: 2 4 2 2 2 4 4 0

217: 2 0 1 1 0 0 0 0

225: 0 0 0 0 0 0 0 0

233: 0 0 0 0 0 0 0 0

241: 0 0 0 0 0 0 0 0

249: 0 0 0 0 0 0 0 0

257: 0 0 0 0 0 0 0 0

265: 0 0 0 0 0 1 0 0

273: 0 0 0 0 0 0 0 0

281: 0 0 0 0 0 1 0 1

289: 0 0 0 0 0 0 0 0

297: 0 0 0 0 0 0 0 0

305: 0 0 0 0 0 1 0 0

313: 0 0 0 0 0 0 1 0

321: 0 0 1 0 0 0 0 0

329: 0 0 0 0 0 0 0 0

337: 0 0 0 0 0 0 0 0

345: 0 0 0 0 0 0 0 0

353: 0 0 0 0 0 0 0 0

361: 1 1 0 0 0 0 0 0

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0095

Channel Data Report 3/30/2018 3:59:31 PM Page 2

369: 0 0 0 0 0 0 1 1

Sample Title: 04

Channell------l-------l-------1-------1-------1-------I-------I-------I 377: 0 1 0 1 1 1 0 0

385: 1 1 0 0 1 1 1 0

393: 1 0 1 1 0 0 1 3

401: 0 0 2 0 0 2 2 0

409: 0 3 3 4 0 1 3 3

417: 3 0 1 1 1 1 3 3

425: 2 1 1 1 3 2 1 2

433: 4 2 1 1 3 1 3 0

441: 1 1 0 0 0 0 0 0

449: 0 0 0 0 0 0 1 0

457: 0 0 0 0 0 0 0 0

465: 0 1 0 1 0 0 0 1

473: 0 0 0 0 0 0 0 0

481: 0 0 0 0 0 0 0 0

489: 1 1 0 0 0 0 0 0

497: 1 0 0 0 0 0 0 0

505: 0 0 0 0 0 0 0 0

513: 0 0 0 0 0 0 0 0

521: 1 0 0 0 0 0 0 0

529: 0 0 0 1 0 0 0 0

537: 0 0 0 0 0 0 1 0

545: 0 2 0 0 1 0 0 0

553: 0 2 0 0 0 1 0 0

561: 2 0 0 1 2 0 1 1

569: 1 1 1 0 0 1 0 0

577: 2 0 1 2 2 1 0 0

585: 0 0 0 2 2 1 3 2

593: 0 3 2 1 1 3 4 3

601: 5 0 3 5 1 5 9 10

609: 9 3 2 2 2 3 5 8

617: 3 8 11 4 10 7 5 8

625: 6 8 11 13 13 13 12 13 633: 11 10 12 4 10 16 13 8

641: 7 14 16 12 10 7 6 3

649: 1 0 0 0 0 0 0 0

657: 0 0 0 0 0 0 0 0

665: 0 0 0 0 0 0 0 0

673: 0 0 0 0 0 0 1 0

681: 0 0 0 0 0 0 0 0

689: 0 0 0 0 0 0 0 0 697: 1 0 0 0 0 0 0 0 705: 0 0 0 0 0 0 1 0 713: 0 0 0 0 0 1 0 0 721: 0 0 0 0 0 0 0 0 729: 0 0 0 0 0 0 0 0 737: 0 0 0 0 0 0 0 0 745: 0 0 0 0 0 0 0 0

753: 0 0 0 0 0 0 0 0 761: 0 0 0 0 0 0 0 0

769: 0 0 0 0 0 0 0 0 777: 0 0 0 0 0 0 0 0 785: 0 0 0 1 0 0 0 0 793: 0 0 0 0 0 0 0 0

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0096

Channel Data Report 3/30/2018 3:59:31 PM Page 3

801: 0 0 0 0 0 0 0 0

Sample Title: 04

Channell------l-------l-------l-------1-------1-------1-------I-------I 809: 0 0 0 0 0 0 0 0

817: 0 0 0 0 0 0 0 0

825: 0 0 0 0 0 0 0 0

833: 0 0 0 0 0 0 0 0

841: 0 0 0 0 0 0 0 0

849: 0 0 0 0 0 0 0 0

857: 0 0 0 0 0 0 0 0

865: 0 0 0 0 0 0 0 0

873: 0 0 0 0 0 0 0 0

881: 0 0 0 0 0 0 0 0

889: 0 0 0 0 0 0 0 0

897: 0 0 0 0 0 0 0 0

905: 0 0 0 0 0 0 0 0

913: 0 0 0 0 0 0 0 0

921: 0 0 0 0 0 0 0 0

929: 0 0 0 0 0 0 0 0

937: 1 0 0 0 0 0 0 0

945: 0 0 0 0 0 0 0 0

953: 0 0 0 0 0 0 0 0

961: 0 0 0 0 0 0 0 0

969: 0 0 0 0 0 0 0 0

977: 0 0 0 0 0 0 0 0

985: 0 0 0 0 0 0 0 0

993: 0 0 0 0 0 0 0 0

1001: 0 0 0 0 0 0 0 0

1009: 0 0 0 1 0 0 0 0

1017: 0 0 0 0 0 0 0 0

Page 97: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0097

r-age I OT L

~Apex-AlphaT] 0-A .C,tlAI/AlARY REPORT

Review Of QA Results - Pulser Check

Date : 3/30/2018 Time : 5:55:22 AM

CHAMBER DEVICE PARAMETER FLAG

Alpha 001 2lf ALL Not Done

Alpha 002 2lf ALL Not Done

Alpha 003 2lf ALL Passed

Alpha 004 2lf ALL Passed

Alpha 005 21f ALL Not Done

Alpha 006 21f ALL Not Done

Alpha 007 21f ALL Not Done

Alpha 008 2lf ALL Not Done

Alpha 009 2lf ALL Not Done

Alpha 010 2lf ALL Passed

Alpha 011 2lf ALL Passed

Alpha 012 21f ALL Passed

Alpha 013 21f ALL Not Done

Alpha 014 2lf ALL Passed

Alpha 015 2lf ALL Not Done

Alpha 016 2lf ALL Not Done

Alpha 033 Alpha Analystl00DC ALL Passed

Alpha 034 Alpha Analvstl00DC ALL Passed

Alpha 035 Alpha Analystl 00DC ALL Passed

Alpha 036 Alpha Analystl 00DC ALL Passed

Alpha 037 Alpha Analystl 00DC ALL Not Done

Alpha 038 Alpha AnalystlO0DC ALL Passed

Alpha 039 Alpha Analystl00DC ALL Not Done

Alpha 040 Alpha Analystl00DC ALL Passed

Alpha 041 Alpha AnalystlO0DC ALL Passed

Alpha 042 Alpha Analystl00DC ALL Passed

Alpha 043 Alpha Analystl00DC ALL Passed

Alpha 044 Alpha Analystl00DC ALL Passed

Alpha 045 Alpha Analystl00DC ALL Passed

Alpha 046 Alpha Analystl00DC ALL Passed

Alpha 047 Alpha Analvstl00DC ALL Not Done

Alpha 048 Alpha Analystl00DC ALL Not Done

Alpha 049 Alpha Analystl00DC ALL Passed

Alpha 050 Alpha Analystl 00DC ALL Passed

Alpha 051 Alpha Analystl00DC ALL Passed

Alpha 052 Alpha Analvstl 00DC ALL Passed

Alpha 053 Alpha Analyst 1 00DC ALL Passed

Alpha 054 Alpha Analystl00DC ALL Passed

Alpha 055 Alpha Analystl00DC ALL Passed

Alpha 056 Alpha Analystl 00DC ALL Passed

Alpha 057 Alpha Arialystl00DC ALL Passed

Alpha 058 Alpha Analystl00DC ALL Passed

3/30/2018 5:55:22 AM

DATE

3/30/2018 5:03:13 AM 3/30/2018 5:03:14 AM

3/30/2018 5:03:15 AM 3/30/2018 5:03:16 AM 3/30/2018 5:03:17 AM

3/30/2018 5:03:18 AM

3/30/2018 5:03:19 AM 3/30/2018 5:03:21 AM 3/30/2018 5:03:22 AM 3/30/2018 5:03:24 AM

3/30/2018 5:03:26 AM

3/30/2018 5:03:28 AM 3/30/2018 5:03:30 AM 3/30/2018 5:03:32 AM 3/30/2018 5:03:34 AM 3/30/2018 5:03:37 AM 3/30/2018 5:03:39 AM 3/30/2018 5:03:42 AM

3/30/2018 5:03:44 AM 3/30/2018 5:03:47 AM 3/30/2018 5:03:49 AM 3/30/2018 5:03:52 AM 3/30/2018 5:03:54 AM 3/30/2018 5:03:57 AM 3/30/2018 5:03:59 AM 3/30/2018 5:04:02 AM

3/30/2018 5:04:05 AM 3/30/2018 5:04:08 AM

Page 98: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0098

Page 2 of 2 Kev1ew ot UA Kesults - t-'u1ser 1.,;necK 3/30/2018 5:55:22 AM

CHAMBER DEVICE PARAMETER FLAG DATE

Alpha 059 Alpha Analvstl00DC ALL Not Done

Alpha 060 Alpha Analyst 1 00DC ALL Not Done

APPROVED BY:

APPROVAL DATE:,~ /3()// 7)

Page 99: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0099

Library Listing Report 6/12/12 12:17:04 PM Page 1

*************************************************************************

***** L I B R A R Y L I S T I N G R E P O R T *****

*************************************************************************

Nuclide Library Title: Uranium

Nuclide Library Description: U-232,-234,-235,-238

Nuclide Half-Life Energy Energy Yield Yield

Name (Seconds) (keV ) Uncert. (keV (%) Uncert. (Abs.+-)

U-232 2.174E+009 5302.500* 0,000 99.8000 0.0000

U-234 7.731E+012 4761.500* 0.000 99.8000 0.0000

U-235 2.221E+016 4385.500* 0.000 80.9000 0.0000

U-238 1.410E+017 4184.400* 0.000 100.2300 0.0000

* = key line

TOTALS: 4 Nuclides 4 Energy Lines

Page 100: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0100

SECTION IX

ANALYTICAL DAT A (ISOTOPIC THORIUM)

Page 101: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0101

Eberline Analytical Oak Ridge Laboratory

Analysis Sheet

Work Order

Analysis Code

Run

18-03111 rhlso~·=7

1

Internal i Sample

Fraction Desc

01 LCS

02 MBL I

18-03111 ThlSO Run 1

Client ID

LCS

BLANK I 1

Login CPM

Printed: 3130/2018 4:59 AM Page 1 of 3

Sample Date

03/23/18 00:00

03/23/18 00:00

Sample Aliquot

1.0000E+00

1.0000E+00

Date Received 3/23/2018 03 DUP [ AC-SED-11 63 03/21/1813:20 9.9780E-01

Lab Deadline 4/12/2018 04 DO I AC-SED-11 63 03/21/18 13:20 1.0036E+00

l ! Client Auxier & Associates, Inc.

Project WESTLAKE NCC

Report Level 4

Activity Units pCi

Aliquot Units g

Matrix so

Method EPA 907.0 Modified

Instrument Type Alpha Spectroscopy

Radiometric Tracer Th-229

Radiometric Sol# Th-18a

Tracer Act (dpm/g) 22.46 I

Carrier

Carrier Cone (mg/ml)

i

i

• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. A Indicates estimated SAF value.

•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

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0102

Eberline Analytical

Oak Ridge Laboratory Analysis Sheet

I

Internal [ Sample Tracer

Fraction i Desc Aliquot(g) I

I 01 LCS 0.4656 I I

02 I

MBL 0.2324 I

03 DUP 0.2329

04 DO 0.2336

I

~

--

----

-----

Tracer Total Radiometric

ACT(dpm) Tracer (pCi)

10.5

5.2

5.2

5.2

18-03111 ThlSO Run 1

I Radiometric/ Grav-Carrier I Grav Filter

[ % Rec [ Added (ml) Tare (g)

I

0.001

o.oo[ I

!

I

I 0.00

0.00

I

I

Grav Filter Final (g)

I I I

• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. A Indicates estimated SAF value.

•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

I i

i

Grav Filter Grav Net (g) %Rec

I i

i I

I

I i

I ! i

I

I

I I I

I

I I !

!

I ! I

I

I

Printed: 313012018 4:59 AM Page 2 of 3

I I Mean SAF SAF %Rec 1· 2·

I

-

Page 103: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0103

Eberline Analytical

Oak Ridge Laboratory

Analysis Sheet

Internal I Sample Fraction Desc

01 LCS

02 MBL

03 DUP

04 DO

I Rough Prep

Date i

03/27 /18 06:45

I

Rough Prep Prep I

By Date I I

03/28/18 07:55

03/28/18 07:55

03/28/18 07:55

KSALLINGS 03/28/18 07:55

I

!

I

i

18-03111 ThlSO Run 1

Prep By

JHARVEY

JHARVEY

JHARVEY

JHARVEY

I Sep to

Date/Time I

• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. "Indicates estimated SAF value.

•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

! Sep to

I By

I I !

---

I

I

l I

I

I I I

!

i ~--· ! I I I

Printed: 3/30/2018 4:59 AM Page 3 of 3

Sep t1 Sep t1 Date/Time By

I

Page 104: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0104

Eberline Analytical Oak Ridge Laboratory

~ Lab I Nuclide

Fraction

01 TH-228

&

~ 0 0 -!!! ~ iii i::: q:

~I

"""""

0 en -.c I-

(J C:

u, Cl) -ca (J 0 u, u, <(

ca ... Cl)

·;;: :::::s <(

02 TH-228

03 TH-228

04 TH-228

Sample Desc

LCS

MBL

DUP

DO

Preliminary Data Report & Analytical Calculations

Work Order: 18-03111-ThlSO-1

Client

I Activity

Results Error Estimate MDA I

Identification Units I

LCS pCi/g 6.24E+00 9.71E-01 8.S0E-02

BLANK pCi/g -7.30E-02 5.48E-02 1.99E-01

AC-SED-11 pCi/g 1.0SE+00 3.17E-01 1.19E-01

AC-SED-11 pCi/g 7.91E-01 2.95E-01 1.34E-01

'

LCS LCS

Known %R

5.11E+00 122.00

Printed: 3/30/2018 1 :59 PM Page 1 of 3

LCS I RPD MDA Blank

Flag I Flag Flag Flag

OK OK

OK OK

INV OK

OK

Page 105: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0105

Eberline Analytical Oak Ridge Laboratory

( Lab Fraction

Nuclide

01 TH-228

C: ::, 0::

.g 0 (.)

,!!! ~ cii C: <t

~I

""""

0 en -.c I-

(.) C:

u, Cl) -ca (.) 0 u, u,

<C otS ...

Cl) ·;;: :::, <C

02 TH-228

03 TH-228

04 TH-228

I Sample Desc

LCS

MBL

DUP

DO

Preliminary Data Report & Analytical Calculations

Work Order: 18-03111-ThlSO-1

Sample Sample

I Radiometric Grav Mean I

Date Aliquot %Rec %Rec %Rec I 03/23/18 00:00 1.00E+00 100.47 0.00 0.00

03/23/18 00:00 1.00E+00 71.21 0.00 0.00

03/21/18 13:20 9.98E-01 92.52 0.00 0.00

03/21/18 13:20 1.00E+00 83.60 0.00 0.00

SAF I

SeptO

Printed: 3/30/2018 1 :59 PM Page 2 of 3

Sept1

Date/Time I Date/Time

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0106

Eberline Analytical Oak Ridge Laboratory

<( Lab Nuclide

Fraction

01 TH-228

C: ::s 0::

{l 0 u .!!,!

~ cu C: ct

C: ,!!! u

~

0 Cl) -.c I-

CJ C

(/) Q) -ns CJ 0 (/) (/) <(

~ a.. Q)

>< :::s <(

02 TH-228

03 TH-228

04 TH-228

Sample Desc

LCS

MBL

DUP

DO

Preliminary Data Report & Analytical Calculations

Work Order: 18-03111-ThlSO-1

Counting Halflife

I Count

Detect Carrier Counts DatefTime (days) Time

03/30/18 08:11 A_Spec Alpha_044 170 4.35 E+02

03/30/18 08:11 A_Spec Alpha_045 170 -3.40 E+00

03/30/18 08:11 A_Spec Alpha_046 170 6.43 E+01

03/30/18 10:29 A_Spec Alpha_049 170 3.88 E+01

Bkg I I

CPM I

0.00 E+00 I

2.00 E-02

1.00 E-02

7.00 E-03

Printed: 3/30/2018 1 :59 PM Page 3 of 3

Eff

18.4

17.4

17.8

15.6

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0107

Eberline Analytical Oak Ridge Laboratory

<\ Lab I Nuclide Fraction I

01 TH-230

§ n:

.g 0 u .!!! ~ iii c::: q:

c:: ~

T"""

0 en -.J:: I-

(.) C: -u, Q) -ca (.) 0 u, u, <(

c6 ... Q)

>< ::::, <(

02 TH-230

03 TH-230

04 TH-230

Sample Desc

LCS

MBL

DUP

DO

Preliminary Data Report & Analytical Calculations

Work Order: 18-03111-ThlSO-1

I

Client Activity Results Error Estimate MDA I Identification Units

LCS pCi/g 6.57E+00 1.01E+00 8.10E-02

BLANK pCi/g 4.58E-02 8.S0E-02 1.63E-01

AC-SED-11 pCi/g 1.17E+00 3.38E-01 8.46E-02

AC-SED-11 pCi/g 1.34E+00 4.14E-01 1.0GE-01

I I LCS LCS

Known %R I

5.39E+00 121.89

Printed: 3/30/2018 1 :59 PM Page 1 of 3

I LCS RPD MDA Blank

Flag Flag Flag Flag

OK OK

OK OK

OK OK

OK

Page 108: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0108

Eberline Analytical

Oak Ridge Laboratory

( Lab

Nuclide Fraction

01 TH-230

C: :, a::

~ 0 (.)

.!(!

~ ;; C: <t

~I

~

0 u, -.c I-

0 r:: -u, .s ca 0 0 u, u, <(

~ ... Cl) ·;: ::s <(

02 TH-230

03 TH-230

04 TH-230

Sample Desc

LCS

MBL

DUP

DO

Preliminary Data Report & Analytical Calculations

Work Order: 18-03111-ThlSO-1

Sample Sample

I Radiometric Grav Mean

I Date Aliquot %Rec %Rec %Rec

03/23/18 00:00 1.00E+00 100.47 0.00 0.00

03/23/18 00:00 1.00E+00 71.21 0.00 0.00

03/21/18 13:20 9.98E-01 92.52 0.00 0.00

03/21/18 13:20 1.00E+00 83.60 0.00 0.00

SAF SeptO

Printed: 3/30/2018 1 :59 PM Page 2 of 3

I Sep t1

Date/Time I Date/Time

Page 109: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0109

Eberline Analytical Oak Ridge Laboratory

<( Lab Nuclide

Fraction

01 TH-230

&

.g 0 (.)

-!!! ~ cii c:: q:

~I

~

0 en -..c I-

(.) C:

ti)

.s ca (.)

0 ti) ti) <(

~ ,_ Q)

'>< :::::s <(

02 TH-230

03 TH-230

04 TH-230

Sample Desc

LCS

MBL

DUP

DO

Preliminary Data Report & Analytical Calculations

Work Order: 18-03111-ThlSO-1

Counting Halflife Carrier I

Count Counts

Date/Time (days) Detect Time

03/30/18 08:11 A_Spec Alpha_044 170 4.57 E+02

03/30/18 08:11 A_Spec Alpha_045 170 2.13 E+00

03/30/18 08:11 A_Spec Alpha_046 170 7.25 E+01

03/30/18 10:29 A_Spec Alpha_049 170 6.65 E+01

! 8kg

I CPM

4.00 E-03

1.10 E-02

3.00 E-03

3.00 E-03

Printed: 3/30/2018 1 :59 PM Page 3 of 3

Eff

18.4

17.4

17.8

15.6

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0110

Eberline Analytical Oak Ridge Laboratory

;: Lab Nuclide

Fraction

01 TH-232

§ a::

.g 0 0 ,!!! ~ cii C: "(

II

""'"

0 Cl) -.c I-

. (.) C -th Q) -cu (.) 0 th th <(

~ lo. Q)

'>< ~ <(

02 TH-232

03 TH-232

04 TH-232

Sample Desc

LCS

MBL

DUP

DO

Preliminary Data Report & Analytical Calculations

Work Order: 18-03111-ThlSO-1

Client Activity Results Error Estimate MDA I Identification Units

LCS pCi/g 6.26E+00 9.74E-01 5.98E-02

BLANK pCi/g -1.S0E-02 4.78E-02 1.58E-01,

AC-SED-11 pCi/g 8.29E-01 2.72E-01 1.14E-01

AC-SED-11 pCi/g 1.12E+00 3.66E-01 9.65E-02

LC$

I LC$

Known %R

5.11E+00 122.44

Printed: 3/30/2018 1 :59 PM Page 1 of 3

LC$

I RPD

I MDA Blank

Flag Flag Flag Flag

OK OK

OK OK

INV OK

OK

Page 111: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0111

Eberline Analytical Oak Ridge Laboratory

~ Lab I Nuclide

Fraction

01 TH-232

c:: :, a:

i 0 0 -!!! ~ iij c:: "(

~I

~

0 u, -.c I-

(.) C:

ti) Cl) -.! (.)

0 ti) ti) <(

oa a.. -~ >< ::::::s <(

02 TH-232

03 TH-232

04 TH-232

Sample Desc

LCS

MBL

DUP

DO

Preliminary Data Report & Analytical Calculations

Work Order: 18-03111-ThlSO-1

Sample Sample Radiometric Grav Mean I Date Aliquot %Rec %Rec %Rec

I

03/23/18 00:00 1.00E+00 100.47 0.00 0.00

03/23/18 00:00 1.00E+00 71.21 0.00 0.00

03/21 /18 13:20 9.98E-01 92.52 0.00 0.00

03/21 /18 13:20 1.00E+00 83.60 0.00 0.00

SAF I I

SeptO

Printed: 3/30/2018 1 :59 PM Page 2 of 3

Sept1

DatefTime DatefTime

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0112

Eberline Analytical Oak Ridge Laboratory

( Lab I Nuclide Fraction

01 TH-232

~

.g 0 0 .!/? ~ cii C: q;

~I

~

0 en -.c I-

(.) C:

u, a, -ns (.)

0 u, u, <(

ca 11,,, a, ·;: ::, <(

02 TH-232

03 TH-232

04 TH-232

Sample Desc

LCS

MBL

DUP

DO

Preliminary Data Report & Analytical Calculations

Work Order: 18-03111-ThlSO-1

Counting Halflife Detect Carrier Count I Counts DatefTime (days) Time

03/30/18 08:11 A_Spec Alpha_044 170 4.37 E+02

03/30/18 08:11 A_Spec Alpha_045 170 -7.00 E-01

03/30/18 08:11 A_Spec Alpha_046 170 5.15 E+01

03/30/18 10:29 A_Spec Alpha_049 170 5.57 E+01

Bkg CPM

1.00 E-03

1.00 E-02

9.00 E-03

2.00 E-03

I

I

Printed: 3/30/2018 1 :59 PM Page 3 of 3

Eff

18.4

17.4

17.8

15.6

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0113

Count Room Report Client: Auxier Associates, Inc.

Internal Fraction

01

I Sample I I Desc j

LCS

Client ID

LCS

18-03111-ThlSO-1 (pCi/g) in SO Tracer ID: Th-18a

Sample Date

Sample Aliquot

Tracer Aliquot (g)

Tracer ACT(dpm)

03/23/18 00:00 1.0000 I 0.4656 10.4574

Radiometric Tracer (pCi)

Printed: 3/30/2018 4:59 AM Page 1 of 1

ii Radiometric ¾Rec

0.00

SAF ! 1*

SAF 2*

\D f 02 MBL BLANK 03/23/18 00:00 1.0000 0.2324 5.2197 0.00

\),.. I

- i

~ 03 DUP AC-SED-11 03/21/18 13:20 ' 0.9978 0.2329 5.2309 0.00 I I _._

i I __J

, 04 DO AC-SED-11 03/21/1813:20 1.0036 0.2336 5.2467 I 0.00 /

,~ . . , 1 l : ~- l i I

. I I I I

,-.-------,.-----+--·

1--------+-----.l--

l I - l 7

I

i I !

i

-----l----+---il--1--1 I ----+----

I ! i

I

i

I

------+--------+[----! ' • ~·~~ -~ ~ -------+--------+-- i I -----,----- ---

·-- - -----f--------------1- ---------~---~---!--- +-- I -·

r·· ---+----+-----+-----+---- ··--·--- -------4--~- +-----t--- i ~·~ -~----

Page 114: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0114

Eberline Analytical Oak Ridge Laboratory

Spike and Tracer Worksheet

Analysis Code

ThlSO

LCS & Matrix Spikes LCS MS

1 ·s 1 # Activity I Solution I Approx Volume Volume

sotope O dpmlg Date I Addition Used (g) Used (g)

Th-228 Th-8b 103.560 3/28/2018[ 0.100 0.1096

Th-230 Th-1b I 23.520 3/28/20181 0.500 0.5084

Th-232 1:'7-8b I 103.560 3/28/20181 0.100 0.1096

Tracers

i I Activity Solution [ Volume

I Approx

fraction Isotope !

Sol# I dpmlg Date 1

Used(g) Addition

01 Th-229 Th-18a 22.460 3/28/2018 0.4656 0.2200

02 Th-229 Th-18a 22.460 3/28/2018 0.2324 0.2200

03 Th-229 Th-18a 22.460 3/28/2018 0.2329 0.2200

04 Th-229 Th-18a 22.460 3/28/2018 0.2336 0.2200

I

I I I

I

Version 2.0 08/99

Date

3/28/2018 7:51

LCSD Volume Used(g)

MSD Volume Used(g)

Technician

JHARVEY

LCS MS Known

pCi

5.11

5.39

5.11

Tracer

\

Error _ Estimate

0.184

0.145

0.184

Added Error pCi Estimate

o.ooi I 0.00!

o.ooi I

0.000

0.000

0.000

Balance Printer Tapes

Page 1 of 1

Printed: 3/28/2018 7:55 AM

Technician Initials

LCSD Known

pCi

0.00

0.00

0.00

Error Estimate

0.000

0.000

0.000

LCS

Matrix Spike

Witness Initials

MSD Added

pCi

0.00

0.00

0.00

Error Estimate

0.000

0.000

0.000

Page 115: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0115

Lab

Eberline Analytical Oak Ridge Laboratory

Auxier & Associates, Inc.

Fraction Client ID

01 LCS

02 BLANK

03 AC-SED-11

04 AC-SED-11

Comments

Technician:

Aliquot Worksheet

Analysis Code Rpt Units Lab Deadline

ThlSO grams 4/12/2018

Sample Muffle Data Dilution Data Aliquot Data

Ratio Type Post/Pre No of Dils Dil Factor Ratio Aliquot Net Equiv

LCS 1.0000E+OO 1.0000E+OO

MBL 1.0000E+OO 1.0000E+OO

DUP 9.9780E-01 9.9780E-01

DO 1.0036E+OO 1.0036E+OO

~f),/0 '7t.-: Date: 3_1@_1--15!,

Technician

JHARVEY

MS Aliquot Data

Printed: 3/28/2018 7:50 AM Page 1 of 1

H-3 Solids Only WaterAaaea R3 UISt

Aliquot Net Equiv (ml) Aliq

I

I

I

Page 116: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0116

Eberline Services - Oak Ridge Prep Logbook Version 2.0 8/1999

Eberline Auxier & Associates, Inc. Fraction Client ID

04 AC-SED-11

Comments

Special Codes

' ~~ / ..

Technician: ' ) ~

Lab Deadline

4/12/2018

Tare (g) Pan Wt

28.2500

Rough Sample Preparation Log Book

Date Received in Prep Date Sealed

3/26/2018 3/27/2018

Gross (g) Net (g) ------

Wet Wt. ! Dry Wt. Wet Wt. Dry Wt.

1839.80001 1287.5600 1811.5500 1259.3100

--·

·--·-·--·--·--- ---·--I

---------·-- ·-·--

----·--

-~---·

-·-···-

..

Date Returned

3/28/2018

Percent Liquid

T Solid

30.48% • 69.52% ··--·- ----+--·-··-··--···· I

I --------

-·-

I ·- --·-·:=1- --·-· ·-·-i ...

,----·

I - ----

i I ·------------

I I

------·--------------~--

I

I

I ---------I I

I

H: Hot, O: Organic Hazard, P: PCB Hazard, R: Rush, T: Other (see comments)

Printed: 3/27/2018 6:45 AM Page 1 of 1

Technician

KSALLINGS

Gamma Special Dry Wt. I LEPS Wt. Info

0.00001 0.0000

1'

l I ·---

. I

I

Date:Analysis: Rough Prep Logbook Analysis: Th ISO Page No, 10439

Page 117: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0117

c&fA Al h TM ~ J-\ p ex- p a Sample Description: Spectrum File: Batch Identification:

SPIKE \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002099

1803111A-TH Sample Identification: Sample Geometry: Procedure Description:

Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:

Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:

Tracer Certificate: Tracer Quantity: Effective Efficiency:

01 Shelf 2 Th iso

Alpha_044 04026481B 84168 System Bkgd 211467

<not performed>

1. 000E+000 3/30/2018 3/30/2018

170.0

+/- 0.000E+000 gram 6:44:48 AM 8:11:12 AM

minutes 170.0 minutes

Th229 S TH-18A

0. 0117

Counting Efficiency:

0.466 mL 0.1849 +/-0.1840 +/-1.0047 +/-

0.0032 on 2/16/2018 0.0660

9:34:19 AM

Chem. Recovery Factor:

Control Certificate Name: NatTh Th-8 Chem. Recov. of Control: TH-232 1.224356 +/- 0.103873

Peak Match Tolerance: 0.175 MeV

Nuclide

TH-227 TH-228 TH-229 T TH-230 TH-232

Energy (MeV)

5.883 5.365 4.851 4.616 3.960

PEAK AREA REPORT

Net Pk Area

2.32 435.00 328.66 457.32 436.83

Pk Area Error%

149.12 9.41

10.82 9.17 9.38

Ambient Backgnd

0.68 0.00 0.34 0.68 0.17

Reagent Backgnd

0.00E+000 0.00E+000 0.00E+000 0.00E+000 0.00E+000

FWHM (keV)

3.0 16.8

4.4 5.1

38.9

T Tracer Peak used for Effective Efficiency

Nuclide

TH-227 TH-228 TH-229 TH-230 TH-232

Id Conf.

0.994 0.994 0.998 0.984 0.993

NUCLIDE ANALYSIS RESULTS

Energy (keV)

5850.00* 5400.00* 4872.00* 4672.00* 3997.00*

Activity (pCi/gram

3.41E-002 +!- 5.l0E-002 6.24E+000 +!- 9.71E-001 4.73E+000 +!- 5.87E-001 6.57E+000 +!- l.0lE+000 6.26E+000 +!- 9.74E-001

~ 3/30/18

MDA (pCi/gram

8.29E-002 +/-8.60E-002 +/-6.88E-002 +/-8.l0E-002 +!-5.98E-002 +/-

l.03E-002 1. 07E-002 8.54E-003 l.00E-002 7.42E-003

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0118

60

55

50

45

40

35 V) .µ C: :::::s

8 30

25

20

15

10

5

g

' er I-

0000209956.CNF

Live Time :10200.000 sec Real Time :10200.300 sec Start: 1:3463.6(kev) Stop : 1024:6522. 9(kev) Acq. Start :Fri Mar 30 08:11:12 2018

0 I j! 11 1 Ml 1111! Mllll/illMI 1 1 , I ' 1 M !MRm rn 1 111i n 11Mv 11 1n1 1 .• 3500 I ,1,1 I I I 1:i11 fU;',P!ii'IJMMl!llll I I I ' ' f II M IW II Ill JI I :: 1 1 ~ , ' I I l!AAN\NU\IVIUIMII\I\ I I' 4000 4500 5000

Energy(kev) 5500 6000 6500

ROI Type: 1 ROI Type: 3

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0119

Channel Data Report 3/30/2018 1:46:48 PM Page 1

******************************************************* ***** s p E C T R A L DAT A R E P O R T ***** *******************************************************

Sample Title: 01

Elapsed Live time: 10200 Elapsed Real Time: 10200

Channe 1 I - - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I 1: 0 0 0 0 0 0 0 0

9 : 0 0 0 0 1 0 0 0

17: 0 1 0 0 0 0 0 0

25: 0 2 0 0 0 1 0 0

33: 0 0 0 0 0 0 0 0

41: 0 1 0 1 0 0 0 0

49: 0 0 0 0 1 1 0 0

57: 2 0 1 0 0 0 1 0

65: 0 0 0 0 0 0 1 0

73: 1 0 0 3 0 0 0 0

81: 0 1 0 1 0 1 1 0

89: 0 0 0 2 1 1 1 0

97: 1 0 1 0 2 2 0 5

105: 3 1 2 1 1 2 1 0

113: 2 3 2 2 1 1 2 1

121: 4 2 2 4 2 1 5 4

129: 7 1 4 7 5 6 5 5

137: 4 5 8 5 5 10 7 6

145: 9 3 6 8 7 9 7 4

153: 12 14 7 16 9 8 11 14

161: 17 14 9 11 15 14 13 11

169: 14 13 14 11 17 21 15 12

177: 10 11 11 10 15 15 4 5

185: 3 3 2 1 0 0 0 0

193: 0 0 0 0 0 0 0 0

201: 0 0 0 0 0 0 0 0

209: 0 0 0 0 0 0 0 0

217: 0 0 0 0 0 0 0 0

225: 1 0 0 1 0 0 0 0

233: 0 0 0 0 0 0 1 0

241: 0 1 0 1 0 0 2 0

249: 0 1 0 0 0 0 0 1

257: 2 0 0 0 0 1 0 1

265: 0 0 0 0 0 0 0 0

273: 0 1 0 0 0 0 2 0

281: 0 0 0 0 0 0 0 0

289: 1 0 0 0 0 0 0 1

297: 0 1 0 1 0 0 0 0

305: 0 0 0 0 0 0 0 0

313: 2 0 0 0 0 0 2 0

321: 0 1 0 0 1 2 1 0

329: 1 2 3 3 0 0 1 1

337: 1 1 1 1 0 2 0 1

345: 0 4 1 1 2 1 3 4

353: 2 2 2 1 5 5 0 2

361: 2 3 6 5 6 10 6 8

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0120

Channel Data Report 3/30/2018 1:46:48 PM Page 2

369: 3 3 11 7 4 6 9 16

Sample Title: 01

Channell------l-------l-------1-------1-------1-------I-------I-------I 377: 3 6 9 8 8 8 8 10

385: 7 17 13 7 9 10 7 9

393: 9 10 9 9 10 9 7 21

401: 10 16 11 9 9 8 7 4

409: 4 4 2 1 0 2 0 0

417: 3 2 0 3 3 2 4 1

425: 2 2 3 2 3 4 1 3

433: 0 3 2 3 6 4 3 8

441: 4 10 4 6 5 4 6 5

449: 6 4 4 7 3 9 3 3

457: 11 4 5 7 6 5 5 7

465: 8 2 4 4 8 3 1 1

473: 2 3 6 4 4 2 3 3

481: 2 6 4 2 6 1 1 3

489: 2 3 2 1 5 2 3 2

497: 0 2 0 0 4 0 2 2

505: 0 2 3 2 1 1 1 2

513: 2 0 1 1 0 1 1 2

521: 1 0 1 0 0 0 0 1

529: 0 0 0 1 0 0 0 0

537: 1 0 0 1 0 1 0 1

545: 1 0 0 0 1 1 0 0

553: 1 0 1 0 0 0 0 0

561: 1 0 0 1 0 2 2 2

569: 1 0 3 0 2 0 1 2

577: 0 0 0 0 3 1 2 1

585: 1 1 1 1 4 1 1 8

593: 0 2 5 4 4 4 5 4

601: 3 3 5 8 4 6 5 6

609: 3 5 10 5 6 5 9 10

617: 6 6 10 11 5 7 9 7

625: 4 7 12 7 16 6 4 6

633: 13 10 10 10 6 14 12 14

641: 15 17 8 12 15 14 12 11

649: 10 14 10 16 12 10 6 4

657: 3 1 2 1 0 0 0 0

665: 0 0 0 0 0 0 0 0

673: 0 0 0 0 0 0 0 0

681: 0 0 1 0 0 0 0 0

689: 0 0 0 0 0 0 2 0

697: 0 0 0 1 0 1 0 0

705: 0 0 0 0 0 0 1 1

713: 1 0 1 0 1 1 1 1

721: 0 0 0 3 1 2 2 0

729: 1 2 3 2 0 4 0 2

737: 1 2 2 0 1 1 2 0

745: 0 0 0 0 0 0 0 0

753: 0 0 0 0 0 0 0 0

761: 0 0 0 0 0 0 0 0

769: 0 0 0 0 0 1 0 0

777: 0 0 0 0 0 0 0 0

785: 0 0 0 0 0 0 0 0

793: 0 0 0 0 0 0 0 0

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0121

Channel Data Report 3/30/2018 1:46:48 PM Page 3

801: 0 0 0 0 0 0 0 0

Sample Title: 01

Channell------l-------l-------1-------1-------1-------I-------I-------I 809: 0 0 0 0 0 0 0 0

817: 0 0 0 0 0 0 1 0

825: 0 0 0 0 0 0 0 0

833: 1 0 0 0 0 0 0 0

841: 0 0 0 0 0 0 0 0

849: 0 0 0 0 0 0 0 0

857: 0 0 0 0 0 0 0 0

865: 0 0 0 0 0 1 0 0

873: 0 0 0 0 0 0 0 0

881: 0 0 0 0 1 0 0 0

889: 0 0 1 0 0 0 1 0

897: 0 0 0 0 1 0 1 1

905: 0 0 0 0 0 0 1 0

913: 1 1 1 0 0 1 1 1

921: 0 0 1 1 0 1 3 1

929: 1 2 1 1 0 3 1 3

937: 0 2 0 2 0 0 0 1

945: 0 0 1 0 0 0 0 0

953: 0 1 1 0 0 1 1 0

961: 0 0 0 0 0 0 0 0

969: 0 0 0 0 0 0 0 0

977: 0 0 0 0 0 0 0 0

985: 0 0 0 0 0 0 0 0

993: 0 0 0 0 0 0 0 0

1001: 0 0 0 0 0 0 0 0

1009: 0 0 0 0 0 0 0 0

1017: 0 0 0 0 0 0 0 0

Page 122: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0122

c&,,A Al h TM ~-~~Mpex- p a Sample Description: Spectrum File: Batch Identification:

BLANK \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002099

1803111A-TH

Sample Identification: Sample Geometry: Procedure Description:

Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:

Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:

Tracer Certificate: Tracer Quantity: Effective Efficiency:

02 Shelf 2 Th iso

Alpha_045 04026482A 91131 System Bkgd 211468

<not performed>

l.000E+000 +!- 0.000E+000 3/30/2018 6:44:48 3/30/2018 8:11:15

170.0 minutes 170.1 minutes

Th229 S TH-18A 0.232 mL 0.1236 +/- 0.0125

AM AM

gram

Counting Efficiency: Chem. Recovery Factor:

0.1735 +/- 0.0031 on 2/16/2018

0.7121 +/- 0.0734 9:34:18 AM

Peak Match Tolerance:

Nuclide

TH-227 TH-228 TH-229 T TH-230 TH-232

Energy (MeV)

5. 912 5.298 4.897 4.647 4.062

0.175 MeV

PEAK AREA REPORT

Net Pk Area

0.79 -3.40

109.62 2.13

-0.70

Pk Area Error%

455.84 72.42 18. 96

191.21 317.90

Ambient Backgnd

2.21 3.40 2.38 1.87 1. 70

Reagent Backgnd

0.00E+000 0.00E+000 0.00E+000 0.00E+000 0.00E+000

FWHM (keV)

3.0 0.0 6.6 3.0 3.0

T = Tracer Peak used for Effective Efficiency

Nuclide

TH-227 TH-228 TH-229 TH-230 TH-232

Id Conf.

0.980 0.947 0.997 0.997 0.978

NUCLIDE ANALYSIS RESULTS

Energy (keV)

5850.00* 5400.00* 4872.00* 4672.00* 3997.00*

Activity (pCi/gram

1. 74E-002 +!- 7.93E-002 -7.30E-002 +/- 5.48E-002

2.36E+000 +/- 4.70E-001 4.58E-002 +/- 8.80E-002

-l.50E-002 +/- 4.78E-002

~ 3/~o!,s

MDA (pCi/gram

1. 76E-001 +!-l.99E-001 +/-l.77E-001 +/-l.63E-001 +/-l.58E-001 +!-

3.50E-002 3.96E-002 3.52E-002 3.24E-002 3.14E-002

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0123

Vl .µ

60

55

50

45

40

35

C: :::s 8 30

25

20

15

10

5

0000209922.CNF

Live Time :10200.000 sec Real Time :10203.600 sec Start: 1: 3510. S(keV) stop : 1024:6578.4(kev) Acq. start :Fri Mar 30 08:11:15 2018

0 I 1 1 i 1'!'1 ' r11111 ,,, I' I h I I l ,. __ ),: u ,G:id lli \ . ~

& I 1! I, !;,ii, 1,1, !11/11 \ 'lil'.i V'lj,1, 11:i, 1! 1 ! 1 ! 1 I I /. I ,'.I,\ I ! I (W\ ! I !t I '

4000

ROI Type: 1

4500 5000 Energy(kev)

5500 6000 6500

ROI Type: 3

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0124

Channel Data Report 3/30/2018 1:27:29 PM Page 1

*******************************************************

***** s p E C T R A L D A T A RE P O R T *****

*******************************************************

Sample Title: 02

Elapsed Live time: 10200 Elapsed Real Time: 10204

Channell------l-------l-------l-------l-------1-------1-------1-------I

1: 0 0 0 0 0 0 0 0

9: 0 0 0 0 0 0 0 0

17: 0 0 0 0 0 0 0 0

25: 0 0 0 0 0 0 0 0

33: 0 0 0 0 0 0 0 0

41: 0 0 0 0 0 0 0 0

49: 0 0 0 0 0 0 0 0

57: 0 0 0 0 0 0 0 0

65: 0 0 0 0 0 0 0 0

73: 0 0 0 0 0 0 0 0

81: 0 0 0 0 0 0 0 0

89: 0 0 0 0 0 0 0 0

97: 0 0 0 0 0 0 0 0

105: 0 0 0 0 0 0 0 0

113: 0 0 0 0 0 0 0 0

121: 0 0 0 0 0 0 0 0

129: 0 0 0 0 0 0 0 0

137: 0 0 0 0 0 0 0 0

145: 0 0 0 0 0 0 0 0

153: 0 0 0 0 0 0 0 0

161: 0 0 0 0 0 0 0 0

169: 0 0 0 0 0 0 0 0

177: 0 0 0 0 0 0 0 0

185: 1 0 0 0 0 0 0 0

193: 0 0 0 0 0 0 0 0

201: 0 0 0 0 0 0 0 0

209: 0 0 0 0 0 0 0 0

217: 0 0 0 0 0 0 0 0

225: 0 0 0 0 1 0 0 0

233: 0 0 0 0 0 0 0 0

241: 0 0 0 0 0 0 0 0

249: 0 0 0 0 0 0 0 0

257: 0 0 0 0 0 0 0 0

265: 0 0 0 0 0 0 0 0

273: 0 0 0 0 0 0 0 0

281: 0 0 0 0 0 0 0 0

289: 0 0 0 0 0 0 0 0

297: 0 0 0 0 0 0 1 0

305: 0 0 0 0 0 0 0 0

313: 0 0 0 0 0 0 0 0

321: 0 0 0 0 0 0 0 0

329: 0 0 0 0 0 0 0 0

337: 0 0 0 0 1 0 0 0

345: 0 0 0 0 0 0 0 0

353: 0 0 0 0 0 0 0 0

361: 0 0 0 0 0 0 0 0

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0125

Channel Data Report 3/30/2018 1:27:29 PM Page 2

369: 0 0 0 0 0 0 0 0

Sample Title: 02

Channell------l-------l-------l-------1-------1-------1-------I-------I 377: 0 0 0 0 0 0 0 0

385: 0 0 1 0 0 0 0 1

393: 0 0 0 0 0 0 0 1

401: 0 0 0 0 0 0 0 0

409: 0 0 0 0 0 2 0 0

417: 1 0 0 0 0 0 0 0

425: 0 0 0 0 1 1 1 0

433: 0 1 0 1 2 1 0 0

441: 3 2 4 1 3 4 5 0

449: 2 2 2 2 2 7 5 2

457: 1 1 0 0 2 2 4 1

465: 2 2 1 1 2 0 1 2

473: 0 2 1 0 0 0 0 1

481: 2 1 1 1 2 2 2 2

489: 2 1 0 1 1 1 0 1

497: 0 0 0 0 1 0 0 0

505: 0 0 0 0 0 0 0 0

513: 0 1 1 0 2 0 0 0

521: 1 1 2 0 0 0 0 0

529: 0 0 0 0 1 0 0 0

537: 0 0 0 0 0 0 0 0

545: 0 0 0 0 0 0 0 0

553: 0 0 0 0 0 0 0 0

561: 0 0 0 0 0 0 0 0

569: 0 0 0 0 0 0 0 0

577: 0 0 0 0 0 0 0 0

585: 0 0 0 0 0 0 0 0

593: 0 0 0 0 0 0 0 0

601: 0 0 0 0 0 0 0 0

609: 0 0 0 0 0 0 0 0

617: 0 0 0 0 0 0 0 0

625: 0 0 0 0 0 0 0 0

633: 0 0 0 0 0 0 0 0

641: 0 0 0 0 0 0 0 0

649: 0 0 0 0 0 0 0 0

657: 0 0 0 0 0 0 0 0

665: 0 0 0 0 0 0 0 0

673: 0 0 0 0 0 0 0 0

681: 0 0 0 0 0 0 0 0

689: 0 1 0 0 0 0 0 0

697: 0 0 0 0 0 0 0 0

705: 0 0 0 0 0 0 0 0

713: 0 0 0 0 0 0 0 0

721: 0 0 0 0 1 0 0 0

729: 0 0 0 0 0 0 0 0

737: 0 0 0 0 0 1 0 0

745: 0 0 0 0 0 0 0 0

753: 0 0 0 0 0 0 0 0

761: 0 0 0 0 0 0 0 0

769: 0 0 0 0 0 0 0 0

777: 0 0 0 0 0 0 0 0

785: 0 0 0 0 0 0 0 0

793: 0 0 0 0 0 0 0 0

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0126

Channel Data Report 3/30/2018 1:27:29 PM Page 3

801: 0 0 0 0 0 0 0 0

Sample Title: 02

Channell------l-------l-------l-------1-------1-------1-------I-------I

809: 0 0 0 0 0 0 0 0

817: 0 0 0 0 0 0 0 0

825: 0 0 1 0 0 0 0 0

833: 0 0 0 1 0 0 0 0

841: 0 0 0 0 0 0 0 0

849: 0 0 0 0 0 0 0 0

857: 0 0 0 0 0 0 0 0

865: 0 0 0 0 0 0 0 0

873: 0 0 0 1 0 0 0 0

881: 0 0 0 0 0 0 0 0

889: 0 0 0 0 0 0 0 0

897: 0 0 0 0 0 0 0 0

905: 0 0 0 0 0 0 0 0

913: 0 0 0 0 0 0 0 0

921: 0 0 0 0 0 0 0 0

929: 0 0 0 1 1 1 2 0

937: 1 0 2 2 1 0 0 0

945: 0 0 0 0 0 0 1 0

953: 0 0 0 0 0 0 0 0

961: 0 0 0 0 0 0 0 0

969: 0 0 0 0 0 0 0 0

977: 0 0 0 0 0 0 0 0

985: 0 0 0 0 0 0 0 0

993: 0 1 0 0 0 0 0 0

1001: 0 0 0 0 0 0 0 0

1009: 0 0 0 0 0 0 0 0

1017: 0 0 0 0 0 0 0 0

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0127

c!!tA Al h TM ~J-\pex- p a Sample Description: Spectrum File: Batch Identification:

AC-SED-11 DUP \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002099

1803111A-TH

Sample Identification: Sample Geometry: Procedure Description:

Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:

Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:

Tracer Certificate: Tracer Quantity: Effective Efficiency:

03 Shelf 2 Th iso

Alpha_046 04026482B 58762 System Bkgd 211469

<not performed>

9.978E-001 3/21/2018 3/30/2018

170.0

+/- 0.000E+000 gram 6:44:48 AM 8:11:18 AM

minutes 170.1 minutes

Th229 S TH-18A 0.233 mL 0.1649 +/- 0.0146

Counting Efficiency: 0.1783 +/- 0.0031 on 2/16/2018

0.9252 +/- 0.0836 9:34:16 AM

Chem. Recovery Factor:

Peak Match Tolerance:

Nuclide

TH-227 TH-228 TH-229 T TH-230 TH-232

Energy (MeV)

5.866 5.384 4.889 4.647 3. 971

0.175 MeV

PEAK AREA REPORT

Net Pk Area

0.47 64.30

146.64 72.49 51.47

Pk Area Error%

626.93 24.82 16.27 23.12 27.79

Ambient Backgnd

1. 53 1. 70 1.36 0.51 1. 53

Reagent Backgnd

0.00E+000 0.00E+000 0.00E+000 0.00E+000 0.00E+000

FWHM (keV)

3.0 8.2

19.1 4.6 4.4

T = Tracer Peak used for Effective Efficiency

Nuclide

TH-227 TH-228 TH-229 TH-230 TH-232

Id Con£.

0.999 0.999 0.998 0.997 0.997

NUCLIDE ANALYSIS RESULTS

Energy (keV)

5850.00* 5400.00* 4872.00* 4672.00* 3997.00*

Activity (pCi/gram

7.77E-003 +!- 4.87E-002 l.05E+000 +!- 3.17E-001 2.37E+000 +!- 4.12E-001 l.17E+000 +/- 3.38E-001 8.29E-001 +!- 2.72E-001

-A~ 3/30/,s

MDA (pCi/gram

1.1 7E- 001 +!-l.19E-001 +!-l.llE-001 +!-8.46E-002 +/-l.14E-001 +!-

2.04E-002 2.07E-002 l.93E-002 l.47E-002 l.99E-002

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0128

0000209923.CNF

Live Time :10200.000 sec

60+ Real Time :10203.600 sec Start: 1:3490.6(kev) Stop : 1024:6554.S(kev) Acq. Start :Fri Mar 30 08:11:18 2018

L 55

50

45

40

35 V) .µ C: :::s 8 30

25

20

15

10

5

Q ~ I I I ! I H I I I I I I

3500 4000 4500 5000 5500 6000 6500 Energy(kev)

ROI Type: 1 ROI Type: 3

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0129

Channel Data Report 3/30/2018 1:27:36 PM Page 1

******************************************************* ***** s p E CTR AL DAT A RE P O R T ***** *******************************************************

Sample Title: 03

Elapsed Live time: 10200 Elapsed Real Time: 10204

Channell------l-------l-------l-------1-------1-------1-------I-------I

1: 0 0 0 0 1 0 0 0

9 : 0 0 0 0 0 0 0 0

17: 0 0 0 0 0 0 0 1

25: 0 0 0 0 0 0 0 0

33: 0 0 0 0 0 0 0 0

41: 0 0 0 0 0 0 0 0

49: 0 0 0 0 0 0 0 0

57: 0 0 0 0 0 0 0 0

65: 0 0 0 0 0 0 0 0

73: 0 0 0 0 0 0 0 0

81: 0 0 1 0 0 0 0 0

89: 0 0 0 0 0 0 0 0

97: 0 0 0 1 0 0 0 0

105: 0 0 0 0 0 0 0 0

113: 0 0 0 0 0 0 0 0

121: 1 0 0 0 1 0 0 0

129: 0 0 0 0 0 0 0 0

137: 1 0 0 1 1 0 0 0

145: 1 0 1 0 1 1 0 1

153: 0 3 0 3 0 2 2 1

161: 1 1 1 1 2 3 1 1

169: 2 5 1 5 1 5 1 0

177: 1 0 0 0 0 0 0 0

185: 0 0 0 0 0 0 0 0

193: 0 0 0 0 0 0 0 0

201: 0 0 0 0 0 0 0 0

209: 0 0 0 0 0 0 0 0

217: 0 0 0 0 0 0 0 0

225: 0 0 0 0 0 0 0 0

233: 0 0 0 0 0 0 0 0

241: 1 0 0 0 0 0 0 0

249: 0 0 0 0 0 0 0 0

257: 0 0 0 0 0 0 0 0

265: 0 0 0 0 0 0 0 0

273: 0 0 0 0 0 0 0 0

281: 1 0 0 0 0 0 0 0

289: 0 0 0 0 0 0 0 0

297: 0 0 0 0 0 0 0 0

305: 0 0 0 0 0 0 0 0

313: 0 0 0 0 0 0 1 0

321: 0 0 0 0 0 0 0 0

329: 0 0 0 0 0 0 0 0

337: 0 0 0 0 0 0 0 0

345: 0 0 0 0 0 0 0 0

353: 0 0 1 0 0 1 0 0

361: 1 1 0 1 0 1 0 0

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0130

Channel Data Report 3/30/2018 1:27:36 PM Page 2

369: 1 2 2 0 2 1 0 1

Sample Title: 03

Channell------l-------l-------l-------l-------1-------1-------1-------I 377: 2 0 1 2 2 1 1 0

385: 2 0 1 0 0 1 2 6

393: 2 3 2 4 10 3 2 5

401: 1 2 1 0 0 0 0 1

409: 0 0 0 0 0 1 0 0

417: 0 0 1 0 0 0 1 0

425: 0 0 0 0 1 0 1 1

433: 0 1 2 1 1 2 2 1

441: 2 2 4 2 3 4 0 4

449: 2 4 4 4 5 5 5 1

457: 2 2 0 3 3 2 0 2

465: 1 0 2 2 1 4 1 1

473: 1 3 2 1 0 1 0 0

481: 1 0 4 1 2 2 1 2

489: 0 1 1 1 0 1 0 1

497: 2 2 3 0 0 0 1 1

505: 3 0 0 1 0 2 2 0

513: 1 3 0 2 1 1 0 1

521: 0 1 0 0 1 1 0 0

529: 0 0 0 0 0 0 0 0

537: 0 0 0 0 0 0 0 0

545: 0 0 0 0 0 0 0 0

553: 1 0 0 0 0 0 0 0

561: 0 0 0 0 0 0 0 0

569: 0 0 0 0 0 0 0 0

577: 0 1 0 2 0 0 0 0

585: 0 0 0 0 0 0 0 0

593: 0 0 0 1 0 0 0 1

601: 1 0 0 0 0 0 0 0

609: 0 0 1 0 1 1 0 1

617: 0 0 1 0 0 1 2 0

625: 0 0 0 0 0 0 3 2

633: 2 0 3 2 5 4 2 2

641: 1 5 3 5 6 2 1 0

649: 3 1 0 0 0 0 0 0

657: 0 0 0 1 0 0 0 1

665: 0 0 0 0 0 0 0 0

673: 0 0 0 0 0 0 0 0

681: 0 0 0 0 0 0 0 0

689: 0 0 0 1 0 0 0 0

697: 0 0 0 1 0 0 0 0

705: 0 0 0 0 0 0 0 0

713: 0 0 1 0 1 0 0 0

721: 0 0 1 0 0 0 0 0

729: 0 0 0 0 0 0 0 0

737: 1 0 0 0 0 0 0 0

745: 0 0 0 0 0 0 0 0

753: 0 1 0 0 0 0 0 0

761: 0 0 0 0 0 0 0 0

769: 0 0 0 0 0 0 0 0

777: 0 0 0 0 0 0 0 0

785: 0 0 0 0 0 0 0 0

793: 0 0 0 0 0 0 0 0

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0131

Channel Data Report 3/30/2018 1:27:36 PM Page 3

801: 0 0 0 0 0 0 0 0

Sample Title: 03

Channell------l-------l-------l-------l-------1-------1-------1-------I

809: 0 0 0 0 0 0 0 0

817: 0 0 0 0 0 0 0 0

825: 0 0 0 0 0 0 0 0

833: 0 1 0 0 0 0 0 0

841: 0 0 0 0 0 0 0 0

849: 0 0 0 0 0 0 0 0

857: 0 0 0 0 0 0 0 0

865: 0 0 0 0 0 0 0 0

873: 0 0 0 0 0 0 0 0

881: 1 0 0 0 0 0 0 0

889: 0 0 0 0 0 0 0 0

897: 0 0 0 0 0 0 0 0

905: 0 0 0 0 0 0 0 0

913: 0 0 0 0 0 0 0 0

921: 0 1 0 0 0 0 0 0

929: 0 1 0 1 1 0 0 0

937: 0 0 0 1 0 0 0 0

945: 0 0 0 0 0 0 0 0

953: 0 0 0 0 0 0 0 0

961: 0 0 0 0 0 0 0 0

969: 0 0 0 0 0 0 0 0

977: 0 0 0 0 0 0 0 0

985: 0 0 0 0 0 0 0 0

993: 0 0 0 0 0 0 0 0

1001: 0 0 0 0 0 0 0 0

1009: 0 0 0 0 0 0 0 0

1017: 0 0 0 0 0 0 0 0

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0132

c!t;'A Al h TM ~-~A!!'l""\pex - p a Sample Description: Spectrum File: Batch Identification:

AC-SED-11 \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002099

1803111A-TH

Sample Identification: Sample Geometry: Procedure Description:

Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:

Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:

Tracer Certificate: Tracer Quantity: Effective Efficiency:

04 Shelf 2 Th iso

Alpha_049 10006121A 49 System Bkgd 211470

<not performed>

l.004E+000 3/21/2018 3/30/2018

170.0

+/- 0.000E+000 gram 6:44:48 AM

10:29:04 AM minutes

170.0 minutes

Th229 S TH-18A 0.234 mL 0.1308 +/- 0.0128

Counting Efficiency: Chem. Recovery Factor:

0.1565 +/- 0.0028 on 2/16/2018 12:37:01 PM

0.8360 +/- 0.0831

Peak Match Tolerance:

Nuclide

TH-227 TH-228 TH-229 T TH-230 TH-232

Energy (MeV)

5.879 5.390 4.887 4.654 3.970

0.175 MeV

PEAK AREA REPORT

Net Pk Area

3.49 38.81

116. 66 66.49 55.66

Pk Area Error%

113. 53 32.02 18.18 24.14 26.37

Ambient Backgnd

0.51 1.19 0.34 0.51 0.34

Reagent Backgnd

0.00E+000 0.00E+000 0.00E+000 0.00E+000 0.00E+000

FWHM (keV)

3.0 5.9 3.6 4.1 3.7

T = Tracer Peak used for Effective Efficiency

Nuclide

TH-227 TH-228 TH-229 TH-230 TH-232

Id Conf.

0.996 0.999 0.999 0.998 0.996

NUCLIDE ANALYSIS RESULTS

Energy (keV)

5850.00* 5400.00* 4872.00* 4672.00* 3997.00*

Activity (pCi/gram

7.23E-002 +/- 8.32E-002 7.91E-001 +/- 2.95E-001 2.37E+000 +!- 4.53E-001 l.34E+000 +!- 4.14E-001 l.12E+000 +/- 3.66E-001

~ c3/3o(<?S

MDA (pCi/gram

1. 09E-001 +/-l.34E-001 +/-9.70E-002 +!-l.06E-001 +/-9.65E-002 +/-

2.08E-002 2.57E-002 1.86E-002 2.03E-002 1.85E-002

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0133

V) ...... C :::J

60

55

50

45

40

35

8 30

25

20

15

10

5

0000209945.CNF

Live Time :10200.000 sec Real Time :10201.000 sec Start: 1:3474.l(kev) stop : 1024:6513.l(kev) Acq. start :Fri Mar 30 10:29:04 2018

i ti. · , ... 1;,;•,,-

0 I. ·, /i

litt I i. _lt1n\/!.\,\1:j ·11 A !, l I , ;\ .. i ; I, "

3500 4000 4500

ROI Type: 1

5000 Energy(kev)

5500 6000

ROI Type: 3

6500

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0134

Channel Data Report 3/30/2018 1:27:44 PM Page 1

******************************************************* ***** s p E C T R A L D A T A R E P O R T ***** *******************************************************

Sample Title: 04

Elapsed Live time: 10200 Elapsed Real Time: 10201

Channell------l-------l-------1-------1-------1-------I-------I-------I

1: 0 0 0 0 0 0 0 0

9 : 0 0 0 0 0 0 0 0

17: 0 0 0 0 0 0 0 0

25: 0 0 0 0 0 0 1 0

33: 0 0 0 0 0 0 0 0

41: 0 1 0 0 0 0 0 0

49: 0 0 0 0 0 0 0 0

57: 0 0 0 0 0 0 0 0

65: 0 0 0 0 0 0 0 0

73: 0 0 0 0 0 0 0 0

81: 0 0 0 0 0 0 0 0

89: 0 0 0 0 0 0 0 0

97: 0 0 0 0 0 0 0 0

105: 0 0 0 0 0 0 0 0

113: 0 0 0 0 0 0 0 0

121: 0 0 0 0 0 1 0 0

129: 0 0 0 0 0 0 0 0

137: 0 2 1 0 0 0 0 0

145: 0 0 1 0 1 0 1 1

153: 2 0 2 0 1 0 2 1

161: 0 2 2 0 2 3 1 0

169: 1 0 1 2 1 1 2 4

177: 1 5 1 0 2 0 1 3

185: 1 1 0 1 1 0 0 0

193: 0 1 0 0 0 0 0 0

201: 0 0 0 0 0 0 0 0

209: 0 0 0 0 0 0 0 0

217: 0 0 0 0 0 0 0 0

225: 0 0 0 0 0 0 0 0

233: 0 0 0 0 0 0 0 0

241: 0 0 0 0 0 0 0 0

249: 0 0 0 0 0 0 0 0

257: 0 0 0 0 0 1 0 0

265: 0 0 0 0 0 0 0 0

273: 0 0 0 0 0 0 0 0

281: 0 0 0 0 0 0 0 0

289: 0 0 1 0 0 0 0 0

297: 0 0 0 0 0 0 0 0

305: 0 0 0 0 0 1 0 0

313: 0 0 0 0 1 0 0 0

321: 1 0 0 0 0 0 0 0

329: 0 0 1 0 0 0 0 0

337: 0 0 0 0 0 0 0 0

345: 0 0 0 0 0 0 0 0

353: 0 0 0 0 0 0 0 0

361: 0 0 0 0 0 0 0 0

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0135

Channel Data Report

369: 0 0 1

Sample Title: 04

3/30/2018

0

1:27:44 PM

1 0 0

Page 2

0

Channell------l-------l-------l-------l-------1-------1-------1-------I 377: 0 0 1 0 2 1 1 0

385: 2 1 1 0 3 2 0 0

393: 0 1 1 4 0 0 1 1

401: 3 1 1 5 3 0 7 3

409: 5 4 2 4 1 1 1 0

41 7: 0 0 0 0 0 0 0 0

425: 1 0 0 0 0 3 1 0

433: 0 0 0 0 0 1 1 0

441: 0 0 0 0 1 1 2 1

449: 1 0 4 1 2 1 1 3

457: 1 6 1 0 1 6 2 4

465: 3 6 2 1 3 2 0 1

473: 0 3 1 3 1 1 1 0

481: 2 2 1 1 1 2 0 0

489: 2 1 2 1 0 0 0 1

497: 2 0 1 1 0 1 1 0

505: 0 0 0 1 0 2 2 0

513: 1 0 0 0 1 0 0 3

521: 0 0 2 1 0 0 2 0

529: 0 0 0 0 1 0 2 1

53 7: 0 0 1 0 0 0 0 0

545: 0 0 1 0 0 1 0 0

553: 0 0 0 0 0 0 0 0

561: 0 0 0 0 0 0 0 0

569: 0 0 0 0 0 0 0 0

577: 0 0 0 0 0 0 0 0

585: 0 0 0 0 0 0 0 0

593: 0 0 0 0 1 0 0 0

601: 0 0 0 0 0 0 0 0

609: 0 0 0 0 0 0 0 0

617: 0 0 0 1 0 1 0 1

625: 0 1 1 0 1 0 0 0

633: 1 0 1 0 1 0 0 1

641: 1 0 0 0 1 3 1 0

649: 0 3 0 2 2 4 2 1

657: 3 0 2 1 1 1 1 0

665: 0 0 0 0 0 0 0 0

673: 0 0 0 0 0 0 0 0

681: 0 0 0 0 0 0 0 0

689: 0 0 0 0 0 0 0 0

697: 0 0 0 0 0 0 0 0

705: 0 0 0 0 0 0 0 0

713: 0 0 0 0 0 0 0 0

721: 0 0 0 0 0 0 0 0

729: 0 0 0 0 0 0 0 0

737: 0 0 0 0 0 0 1 0

745: 0 0 0 0 0 0 0 1

753: 0 0 0 0 0 0 0 0

761: 0 0 0 0 0 0 0 0

769: 0 0 0 0 0 0 0 0

777: 0 0 0 0 0 0 0 0

785: 0 0 0 0 0 1 0 0

7 93: 0 0 0 0 0 0 0 0

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0136

Channel Data Report 3/30/2018 1:27:44 PM Page 3

801: 0 0 0 0 0 0 0 0

Sample Title: 04

Channell------1-------1-------1-------I-------I-------I-------I-------I

809: 0 0 0 0 0 0 0 0

817: 0 0 0 0 0 0 0 0

825: 0 0 0 0 0 0 0 0

833: 0 0 0 0 0 0 0 0

841: 0 0 0 0 0 0 1 0

849: 0 0 0 0 1 0 0 0

857: 0 0 0 0 0 0 0 0

865: 0 0 0 0 0 0 0 0

873: 0 0 0 0 0 0 0 0

881: 0 0 0 0 0 0 0 0

889: 0 0 0 0 0 0 0 0

897: 0 0 0 0 0 0 0 1

905: 0 0 0 0 0 0 0 1

913: 0 0 0 0 0 0 0 0

921: 0 0 0 0 0 0 0 0

929: 0 0 0 0 0 0 0 0

937: 0 0 0 1 0 0 0 0

945: 0 1 0 0 0 0 1 0

953: 0 0 0 0 1 0 0 0

961: 2 0 0 0 0 0 1 0

969: 0 0 0 0 0 0 0 0

977: 0 0 0 0 0 0 0 0

985: 0 0 0 0 0 0 0 0

993: 0 0 0 0 0 0 0 0

1001: 0 0 0 0 0 0 0 0

1009: 0 0 0 0 0 0 0 0

1017: 0 0 0 0 0 0 0 0

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0137

t""age I OT "

f ~Apex-AlphaT]

Date : 3/30/2018

Q_A Sl)A/TAAARY REPORT Review Of QA Results - Pulser Check

Time : 5:55:22 AM

CHAMBER DEVICE PARAMETER FLAG

Alpha 001 2lf ALL Not Done

Alpha 002 21f ALL Not Done

Alpha 003 21f ALL Passed

Alpha 004 21f ALL Passed

Alpha 005 21f ALL Not Done

Alpha 006 21f ALL Not Done

Alpha 007 21f ALL Not Done

Alpha 008 21f ALL Not Done

Alpha 009 21f ALL Not Done

Alpha 010 21f ALL Passed

Alpha 011 21f ALL Passed

Alpha 012 2lf ALL Passed

Alpha 013 21f ALL Not Done

Alpha 014 21f ALL Passed

Alpha 015 21f ALL Not Done

Alpha 016 21f ALL Not Done

Alpha 033 Alpha Analvstl00DC ALL Passed

Alpha 034 Alpha AnalvstlO0DC ALL Passed

Alpha 035 Alpha Analystl00DC ALL Passed

Alpha 036 Alpha Analystl 00DC ALL Passed

Alpha 037 Alpha Analystl 00DC ALL Not Done

Alpha 038 Alpha Analystl00DC ALL Passed

Alpha 039 Alpha Analyst l 00DC ALL Not Done

Alpha 040 Alpha Analystl00DC ALL Passed

Alpha 041 Alpha Analystl00DC ALL Passed

Alpha 042 Alpha Analvstl00DC ALL Passed

Alpha 043 Alpha Analystl 00DC ALL Passed

Alpha 044 Alpha Analystl00DC ALL Passed

Alpha 045 Alpha Analyst l 00DC ALL Passed

Alpha 046 Alpha Analvstl00DC ALL Passed

Alpha 047 Alpha Analvstl 00DC ALL Not Done

Alpha 048 Alpha Analystl00DC ALL Not Done

Alpha 049 Alpha Analystl00DC ALL Passed

Alpha 050 Alpha AnalystlO0DC ALL Passed

Alpha 051 Alpha AnalystlO0DC ALL Passed

Alpha 052 Alpha Analystl 00DC ALL Passed

Alpha 053 Alpha Analystl 00DC ALL Passed

Alpha 054 Alpha Analystl00DC ALL Passed

Alpha 055 Alpha Analystl00DC ALL Passed

Alpha 056 Alpha Analystl 00DC ALL Passed

Alpha 057 Alpha Analvstl 00DC ALL Passed

Alpha 058 Alpha Analvstl00DC ALL Passed

3/30/2018 5:55:22 AM

DATE

3/30/2018 5:03:13 AM 3/30/2018 5:03:14 AM

3/30/2018 5:03:15 AM 3/30/2018 5:03:16 AM 3/30/2018 5:03:17 AM

3/30/2018 5:03:18 AM

3/30/2018 5:03:19 AM 3/30/2018 5:03:21 AM 3/30/2018 5:03:22 AM 3/30/2018 5:03:24 AM

3/30/2018 5:03:26 AM

3/30/2018 5:03:28 AM 3/30/2018 5:03:30 AM 3/30/2018 5:03:32 AM 3/30/2018 5:03:34 AM 3/30/2018 5:03:37 AM 3/30/2018 5:03:39 AM 3/30/2018 5:03:42 AM

3/30/2018 5:03:44 AM 3/30/2018 5:03:47 AM 3/30/2018 5:03:49 AM 3/30/2018 5:03:52 AM 3/30/2018 5:03:54 AM 3/30/2018 5:03:57 AM 3/30/2018 5:03:59 AM 3/30/2018 5:04:02 AM 3/30/2018 5:04:05 AM 3/30/2018 5:04:08 AM

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0138

Page 2 of 2 Kev,ew ot UA Kesults - t-'ulser L;necK 3/30/2018 5:55:22 AM

CHAMBER DEVICE PARAMETER FLAG DATE

Alpha 059 Alpha AnalystlO0DC ALL Not Done

Alpha 060 Alpha AnalvstlO0DC ALL Not Done

APPROVED BY:

APPROVAL DATE:'')/;;()/[ s

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0139

Library Listing Report 6/12/12 12:16:29 PM Page 1

*************************************************************************

***** L I B R A R Y L I S T I N G R E P O R T *****

*************************************************************************

Nuclide Library Title: Thorium

Nuclide Library Description: Th-227,-228,-229,-230,-232

Nuclide Half-Life Energy Energy Yield Yield

Name (Seconds) (keV ) Uncert. (keV (%) Uncert. (Abs.+-)

TH-227 6.873E+008 5850.000* 0.000 97.5000 0.0000

TH-228 6.034E+007 5400.000* 0.000 99.9400 0.0000

TH-229 2.487E+Oll 4872.000* 0.000 99.5200 0.0000

TH-230 2.379E+Ol2 4672.000* 0.000 99.8200 0.0000

TH-232 4.434E+017 3997.000* 0.000 100.0000 0.0000

* = key line

TOTALS: 5 Nuclides 5 Energy Lines

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0140

SECTIONX

ANALYTICAL DATA (GAMMA SPECTROSCOPY)

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0141

Eberline Services Oak Ridge Laboratory Analysis Sheet

Work Order

Analysis Code

Run

Date Received

Lab Deadline

Client

3/23/2018

4/12/2018

Auxier & Associates, Inc.

Internal Sample Fraction Desc

01 LCS

02 MBL

03 DUP

18-03111 Gamma

Run 1

Client ID

LCS

BLANK

AC-SED-11 -----------

AC-SED-11 --~~- D0-r _ _ _ _ _ __ _

Login CPM

Sample Date

Printed: 3/27/2018 7:42 AM Page 1 of 3

Sample Aliquot

03/23/18 00:00 1.0000E+00

1.0000E+00

63 ! 03/21/1813:20 4.7630E+02 ----~-- -- - r~ ---

63 1

03/21/18 13:20 I 4.7630E+02 ------------- -- -+-- ~-- ----·------

1

Repo:':~::: WEST~KE NCC~ I I T ~---- -7 ~ 7- 7 - .

Activity Units I pCi I I I- ~----.~~ . ---------'·· -~::::~:~-~ ... ---~-Aliquot Units I g I I I ~--- I ____ ·"-i __

I

I Matrix I SO 11 ~~-~~~-L-- _______ ~---~--~-~-~ -

1

--~ ~~~~~, Method EPA 901.1 Modified I

I Instrument Type I Gamma Spectroscopy I [ . ·- ---=~~: - +-- [ -~----·~ ~~ ------'------+--------------i ____ .. ________ I ~----

- 1--+ ~·-------~ ~ ~---1 _,, ___ ,,,, _____ _

Radiometric Tracer

Radiometric Sol#

Tracer Act (dpm/g)

Carrier

Carrier Cone (mg/ml)

• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. A Indicates estimated SAF value.

•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

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0142

Eberline Services Oak Ridge Laboratory Analysis Sheet

18-03111 Gamma

Run 1

Printed: 3/27/2018 7:42 AM Page 2 of 3

Internal Fraction

Sample Desc

Tracer Aliquot (g)

Tracer Total ACT(dpm)

Radiometric Tracer (pCi)

Radiometric Grav Carrier ' % Rec I Added (ml)

I

I '1 0.00 Les I

I -- - -------r-- I

Grav Filter Tare (g)

Grav Filter Final (g)

Grav Filter Net (g)

Grav %Rec

Mean %Rec

I SAF SAF

l 1* 2*

01 _ -- - -- -- I 0.00! _ ! -- _ -~ ·········-·--- -- I

_02 I MBL I~ 7 ______ .. --- +- ·~~ I-- I

•-OJlouP-i- ..... -----. -- --1 ----·~--~-:~~I -·i------ I -~- ~-- I I 04 I DO L-~-~- i _____ , -- ~

00 ~~ - - - -- +·~- -- -- i

-[

µ

_I !

I

I I I r- l

I I

I

i I

7 -· L I ---

I I

I I

I

I_ I I

j I

* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. A Indicates estimated SAF value.

** Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

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0143

Eberline Services Oak Ridge Laboratory Analysis Sheet

18-03111 Gamma

Run 1

Printed: 3/27/2018 7:42 AM Page 3 of 3

Internal Fraction

Sample Desc

Rough Prep Date

Rough Prep By

~; I ~-:-:- !,------------------------,-----

-·-·-- - ---·--··-------- --,------ . ··--------·---

03 _ DUP

Prep Date

Prep By

04 i DO i---0-3-/2-7/1_8_06-:4-5-+--K ____ S_A_L--LI-NG-S --------

Sep to Date/Time

Sep to By

Sep t1 Date/Time

Sep t1 By

--- ---,

-----

1'

------

-~- - - +-------- i -----r----~- -r-- --- t--~ ----------+------- - --~ - i

- --------1---~~---+--------,--~~------1 l------+-------1 ~~__,_____---t-~~+---------- ____ J______ I

- I I 1---------+-------+---------------+-----------+--------~---+-------+- I - ,

t-~-- ==== _:

I- I

- ~ I ,

I r---j- . I ~--- I

I

:

• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. "Indicates estimated SAF value.

•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

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0144

Lab Fraction

01 01 02 02 02 02 02 02 02 02 02 02 02 03 03 03 03 03 03 03 03 03 03 03 04 04 04 04 04 04 04 04 04 04 04

Eberline Analytical Oak Ridge Laboratory

Nuclide I Sample

I Desc

CO-60 LCS

CS-137 LCS

AC-228 MBL

Bl-214 MBL

K-40 MBL

PA-231 MBL

PB-210 MBL

PB-212 MBL

PB-214 MBL

RA-226 MBL

RA-228 MBL

TH-234 MBL

TL-208 MBL

AC-228 DUP

Bl-214 DUP

K-40 DUP

PA-231 DUP

PB-210 DUP

PB-212 DUP

PB-214 DUP

RA-226 DUP

RA-228 DUP

TH-234 DUP

TL-208 DUP

AC-228 DO

Bl-214 DO

K-40 DO

PA-231 DO

PB-210 DO

PB-212 DO

PB-214 DO

RA-226 DO

RA-228 DO

TH-234 DO

TL-208 DO

Client

Identification

LCS

LCS

BLANK

BLANK

BLANK

BLANK

BLANK

BLANK

BLANK

BLANK

BLANK

BLANK

BLANK

AC-SED-11

AC-SED-11

AC-SED-11

AC-SED-11

AC-SED-11

AC-SED-11

AC-SED-11

AC-SED-11

AC-SED-11

AC-SED-11

AC-SED-11

AC-SED-11

AC-SED-11

AC-SED-11

AC-SED-11

AC-SED-11

AC-SED-11

AC-SED-11

AC-SED-11

AC-SED-11

AC-SED-11

AC-SED-11

Preliminary Data Report & Analytical Calculations

Work Order: 18-03111-Gamma-1 Activity

I Error LSC LCS LCS

Units Results

Estimate MDA Known %R Flag

pCi/g 1.32E+02 8.11E+00 9.45E-01 1.35E+02 97.25 OK

pCi/g 8.31E+01 7.72E+00 1.27E+00 8.44E+01 98.43 i OK

pCi/g 9.58E-03 2.20E-02 9.02E-02

pCi/g 2.99E-02 4.01E-02 6.90E-02

pCi/g 1.62E-01 1.S0E-01 3.39E-01

pCi/g -4.91E-01 5.96E-01 7.86E-01

pCi/g 3.72E-01 3.67E-01 5.55E-01

pCi/g 4.19E-02 2.44E-02 4.68E-02

pCi/g 2.52E-02 3.78E-02 6.34E-02

pCi/g 2.99E-02 4.01E-02 6.90E-02

pCi/g 9.58E-03 2.20E-02 9.02E-02

pCi/g 1.08E+00 3.97E-01 6.57E-01

pCi/g -5.60E-03 5.22E-02 7.99E-02

pCi/g 8.74E-01 2.34E-01 3.52E-01

pCi/g 1.06E+00 1.93E-01 2.46E-01

pCi/g 1.60E+01 2.13E+00 1.15E+00

pCi/g 1.37E+00 1.41E+00 3.33E+00

pCi/g 2.10E+00 1.33E+00 2.15E+00

pCi/g 1.44E+00 2.66E-01 2.35E-01

pCi/g 1.13E+00 1.98E-01 2.42E-01

pCi/g 1.06E+00 1.93E-01 2.46E-01

pCi/g 8.74E-01 2.34E-01 3.52E-01

pCi/g 1.72E+00 1.49E+00 2.05E+00

pCi/g 7.74E-01 1.68E-01 1.34E-01

pCi/g 1.09E+00 2.60E-01 3.95E-01

pCi/g 1.11E+00 1.95E-01 2.12E-01

pCi/g 1.68E+01 2.27E+00 1.36E+00

pCi/g 4.02E-01 1.98E+00 2.65E+00

pCi/g 2.01E+00 1.66E+00 2.74E+00

pCi/g 1.31E+00 2.57E-01 2.45E-01

pCi/g 1.10E+00 1.94E-01 2.16E-01

pCi/g 1.11E+00 1.95E-01 2.12E-01

pCi/g 1.09E+00 2.60E-01 3.95E-01

pCi/g 1.01E+00 1.14E+00 1.91E+00

pCi/g 9.65E-01 1.89E-01 1.34E-01

RPO

I Sample

Flag Date

03/23/18 00:00

03/23/18 00:00

03/23/18 00:00

03/23/18 00:00

03/23/18 00:00

03/23/18 00:00

03/23/18 00:00

03/23/18 00:00

03/23/18 00:00

03/23/18 00:00

03/23/18 00:00

03/23/18 00:00

03/23/18 00:00

OK 03/21/18 13:20

OK 03/21/18 13:20

OK 03/21/1813:20

03/21/18 13:20

03/21/18 13:20

03/21/18 13:20

03/21/18 13:20

03/21/18 13:20

03/21/1813:20

03/21/18 13:20

03/21/18 13:20

03/21/18 13:20

03/21/18 13:20

03/21/18 13:20

03/21/18 13:20

03/21/18 13:20

03/21/18 13:20

03/21/18 13:20

03/21/18 13:20

03/21/18 13:20

03/21/18 13:20

03/21/18 13:20

Printed: 4/17/2018 8:28 AM Page 1 of 1

Sample

I Counting

Identified Aliquot Date/Time

1.00E+00 04/17/18 05:42 YES

1.00E+00 04/17/18 05:42 YES

1.00E+00 04/17/18 06:13 NO

1.00E+00 04/17/18 06:13 NO

1.00E+00 04/17/18 06:13 NO

1.00E+00 04/17/18 06:13 NO

1.00E+00 04/17/18 06:13 NO

1.00E+00 04/17/18 06:13 NO

1.00E+00 04/17/18 06:13 NO

1.00E+00 04/17/18 06:13 NO

1.00E+00 04/17/18 06:13 NO

1.00E+00 04/17/18 06:13 NO

1.00E+00 04/17/18 06:13 NO

4.76E+02 04/17/18 05:42 YES

4.76E+02 04/17/18 05:42 YES

4.76E+02 04/17/18 05:42 YES

4.76E+02 04/17/18 05:42 YES

4.76E+02 04/17/18 05:42 YES

4.76E+02 04/17/18 05:42 YES

4.76E+02 04/17/18 05:42 YES

4.76E+02 04/17 /18 05:42 YES

4.76E+02 04/17/18 05:42 YES

4.76E+02 04/17/18 05:42 NO

4.76E+02 04/17/18 05:42 YES

4.76E+02 04/17/18 06:44 YES

4.76E+02 04/17/18 06:44 YES

4.76E+02 04/17/18 06:44 YES

4.76E+02 04/17/18 06:44 NO

4.76E+02 04/17/18 06:44 YES

4.76E+02 04/17 /18 06:44 YES

4.76E+02 04/17/18 06:44 YES

4.76E+02 04/17/18 06:44 YES

4.76E+02 04/17/18 06:44 YES

4.76E+02 04/17/18 06:44 YES

4.76E+02 04/17/18 06:44 YES

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0145

Count Room Report Client: Auxier Associates, lnco

Internal Fraction

Sample Desc

Client JD

18-03111-Gamma-1 (pCi/g) in SO Tracer ID:

Sample Sample Tracer

Date Aliquot Aliquot (g) Tracer

ACT(dpm)

Printed: 3/27/2018 7:42 AM Page 1 of 1

1ht Radiometric Radiometric SAF SAF

Tracer (pCi) % Rec 1* 2*

~ I LCS l LCS 03/23/1800:00 1.0000 i ~---------------·····--·•·-------·--··-------- 0.00 1

f7- I MBL , BLANK 03/23/18 00:00 . 1.0000 '

03/23/18 00:00 1.0000 j i

I

I

~, : ---- -ill~ 1--------'----'---------·--· . ----------+-- _ ___J____ - ·----, --~-T--------+.------1

t I · ' • I

1

__ ------ :=--=~=~ 1 ---- ------~! I

f

-- -1 ___ J _________ - I --+--~-

- I !---t-----------1.-------t -- I I

___ ___j_ ··-----

r--------,-7 , I -

I i ' t--_l --~I __ I

Page 146: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0146

Lab

Eberline Analytical Oak Ridge Laboratory

Auxier & Associates, Inc.

Fraction Client ID

01 LCS 02 BLANK 03 AC-SED-11 04 AC-SED-11

Analysis Code

Gamma

Sample Muffle Data Ratio

Type Post/Pre LCS MBL

------·-DUP DO

Aliquot Worksheet

Rpt Units Lab Deadline

grams 4/12/2018

Dilution Data Aliquot Data

No of Dils I Oil Factor7. Ratio Aliquot Net Equiv

I 1.0000E+00 1.0000E+00

i 1.0000E+00 1.0000E+00 i

I 4.7630E+02 4.7630E+02

I 4.7630E+02 4.7630E+02 -·--- .. ------·--··----+· ·- -··--·-------· --··-·--------·-,.·--

____ ! ___

--1-- -- --·-·--·--·-·--

! ---·- ---·-··- :-------·-··----t--- -----··--·~----

i I

! -----·--- ·--~--- ---------·-----

I --····---------- ------------- - I --- -- ----·--· . ---- -----·------ -

'

i

- -·- - --------- -----!- ---

! -·--·--- ------

I I -----!

Comments

')/ 4

Technician: ~/s..r<-f., )?-::::z Date: _3__; JI I / f

Printed: 3/27/2018 7:42 AM Page 1 of 1

Technician

KSALLINGS

MS Aliquot Data H-3 Solids Only

Aliquot Net Equiv wat~~~tea -

1

- H~~t-!

I I . -- -- ------~----

-----

. ----- _______ ,. ...

I - -----------· ---

----~-------- -----

-----··~---

----·--

-·------

Page 147: semspub.epa.gov · 0002 TABLE OF CONTENTS SECTION DESCRIPTION PAGE I Chain of Custody 0004 II Sample Acknowledgement 0009 III Case Narrative 0012 IV Analytical Results Summary 0016

0147

I

Eberline Services - Oak Ridge Prep Logbook Version 2.0 8/1999

Rough Sample Preparation Log Book

Date Received in Prep Date Sealed

3/26/2018 3/27/2018

Date Returned

3/28/2018

Printed: 3/27/2018 6:45 AM Page 1 of 1

Technician

KSALLINGS

Eberline I Auxier & Associates, lnc-j__ Tare (g) Gross (g) 1-- Net (_g) -I·-·- --~e_r~ent Pan Wt Wet Wt. Dry Wt. Wet Wt. Dry Wt. Liquid I Fraction Client ID

Gamma Solid Dry Wt. LEPS Wt.

Special Info

04 AC-SED-11 28.25001 1839.80001 1287.56001 1s11.5500I 1259_31001 30.48%I --·--·t---- . -- .... -- _ .. ~-~:52%1 0.0000 0.00001 I

I --------·· • I I

J - '·-- --- ··t· --· -· -- I

' !

..l

l~j - -~----1-~+---------------+------t-- · t~=-•·-·1-··- -T~~ -- I I I I I I 11-·········-:=[~ ~ ~-~1·~~~1 -----1---1

Comments

Special Codes H: Hot, 0: Organic Hazard, P: PCB Hazard, R: Rush, T: Other (see comments}

Technician: -~_,....,,'7 )t,.;,{ Date:Analysis: Rough Prep Logbook Analysis: Gamma Page No. 10439

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0148

4/17/2018 6:13:23AM

pex-G mma Analysis Report for 1803111-01

GAS-1402

GAMMA SPECTRUM ANALYSIS

Sample Identification

Sample Description

Sample Type

Sample Size

Facility

Sample Taken On

Acquisition Started

Procedure

Operator

Detector Name

Geometry

Live Time

Real Time

Dead Time

Peak Locate Threshold

Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance

Energy Calibration Used Done On

Efficiency Calibration Used Done On

Efficiency Calibration Description

Sample Number

: 1803111-01

: GAS-1402

: SOIL

: 7.360E+02 grams

: Countroom

: 10/1/2014 9:14:17AM

: 4/17/2018 5:42:50AM

: GAS-1602 pCi

: Administrator

: GE1

: GAS-1602

: 1800.0 seconds

: 1821.9 seconds

: 1.20 %

: 2.50

: 1 - 4096

: 17 - 4096

: 1.000 keV

: 2/17/2018

: 2/17/2018

: 64638

PEAK-TO-TOTAL CALIBRATION REPORT

Peak-to-Total Efficiency Calibration Equation

Page 1 of 25

l/ /(l/18

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0149

4/17/2018 6:13:23AM

Analysis Report for 1803111-01

GAS-1402

PEAK LOCATE REPORT

Peak No.

1 2 3 4 5 6 7 8 9

10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33

Peak Locate Performed on

Peak Locate From Channel

Peak Locate To Channel

Peak Search Sensitivity

Energy (keV)

31.75 49.82 55.64 59.34 65.26 84.76 87.94 93.62

121.93 136.49 165.23 187.80 238.60 352.74 518.37 639.07 661.79 666.87

1073.55 1115.79 1121.26 1173.53 1178.72 1332.83 1338.00 1452.45 1835.51 2004.08 2011.16 2273.36 2445.44 2505.69 2614.03

? = Adjacent peak noted

Errors quoted at 2.000sigma

: 4/17/2018 6:13:15AM

: 1 : 4096 : 2.50

Centroid Channel

32.26 50.31 56.12 59.82 65.73 85.22 88.40 94.07

122.35 136.89 165.62 188.16 238.92 352. 96 518.45 639.06 661.76 666.84

1073.24 1115.44 1120.91 1173.15 1178.33 1332.36 1337.52 1451. 91 1834.78 2003.29 2010.37 2272.48 2444.52 2504.75 2613.07

Centroid Uncertainty

0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000

Page 2 of 25

Peak Significance

0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0;00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00

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0150

4/17/2018 6:13:23AM Page 3 of 25

Analysis Report for 1803111-01

GAS-1402

PEAK ANALYSIS REPORT ,.

Peak Analysis Performed on : 4/17/2018 6: 13:15AM

Peak Analysis From Channel : 1

Peak Analysis To Channel : 4096

Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM

No. (keV) start end Centroid Area Uncertainty Counts (keV)

1 31.75 31 - 35 32.26 l.51E+03 225.53 9.73E+03 1. 74

M 2 49.82 45 - 63 50.31 6.00E+03 363.22 l.84E+04 1. 77

m 3 55.64 45 - 63 56.12 6.84E+03 382.93 l.85E+04 1. 78

m 4 59.34 45 - 63 59.82 8.68E+04 686.49 l.87E+04 1. 79

5 65.26 65 - 68 65.73 l.28E+03 248.85 l.38E+04 2.56

M 6 84.76 83 - 91 85.22 6.66E+02 204.69 l.06E+04 2.15

m 7 87.94 83 - 91 88.40 2.11E+04 368.89 l.10E+04 1. 60

8 93.62 93 - 97 94.07 6.09E+02 203.08 8.37E+03 1. 64

9 121.93 119 - 126 122.35 2.83E+03 293.69 l.25E+04 1. 88

10 136.49 134 - 140 136.89 3.62E+02 238.83 l.01E+04 1. 86

11 165.23 164 - 168 165.62 l.93E+02 173.82 6.55E+03 1. 63

12 187.80 186 - 191 188.16 l.79E+02 209.68 8.67E+03 3.83

13 238.60 237 - 241 238.92 2.70E+02 173.72 6.43E+03 1. 50

14 352.74 350 - 356 352. 96 l.70E+02 188.04 6.28E+03 1. 87

15 518.37 515 - 521 518.45 l.53E+02 150.58 4.01E+03 3.75

16 639.07 637 - 642 639.06 l.18E+02 114.71 2.55E+03 2.36

M 17 661.79 655 - 672 661.76 2.98E+04 364.88 2.60E+03 1. 94

m 18 666.87 655 - 672 666.84 l.46E+03 334. 72 4.12E+03 3.36

19 1073.55 1070 - 1076 1073.24 l.43E+02 124.02 2.69E+03 4.21

20 1115.79 1112 - 1119 1115.44 l.08E+02 131.85 2.80E+03 3.04

21 1121.26 1119 - 1123 1120.91 7.llE+0l 84.89 l.54E+03 2.09

M 22 1173.53 1167 - 1183 1173.15 2.38E+04 322.27 l.41E+03 2.21

m 23 1178.72 1167 - 1183 1178.33 l.14E+03 222.49 l.68E+03 3.07

M 24 1332.83 1326 - 1343 1332.36 2.17E+04 298.36 3.43E+02 2.32

m 25 1338.00 132 6 - 1343 1337.52 l.08E+03 212.92 2.50E+02 2.98

26 1452.45 144 9 - 1455 1451.91 2.60E+0l 26.14 l.06E+02 3.00

27 1835.51 1831 - 1840 1834.78 2.28E+0l 28.21 l.02E+02 1. 98

M 28 2004.08 2000 - 2013 2003.29 2.58E+0l 16.85 4.18E+0l 3.42

m 29 2011.16 2000 - 2013 2010.37 2.06E+0l 19.18 3.94E+0l 3.43

30 2273.36 2269 - 2277 2272.48 l.77E+0l 21.99 6.47E+0l 2.52

31 2445.44 2441 - 2448 2444.52 7.85E+00 7.48 4.30E+00 3.44

32 2505.69 2499 - 2512 2504.75 3.36E+02 41.55 4.42E+0l 2.85

33 2614.03 2609 - 2 61 7 2613.07 2.05E+0l 11. 85 9.00E+00 1. 44

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0151

Analysis Report for 1803111-01

GAS-1402

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet

Errors quoted at 2.000sigma

4/17/2018 6:13:23AM

PEAK ANALYSIS REPORT

Peak Analysis Performed on : 4/17/2018 6:13:15AM

Peak Analysis From Channel : 1

Peak Analysis To Channel : 4096

Peak Energy ROI ROI Net Peak Net Area Continuum

No. (keV) start end Area Uncertainty Counts

1 31.75 31 - 35 1.51E+03 225.53 9.73E+03

M 2 49.82 45 - 63 6.00E+03 363.22 1.84E+04

m 3 55.64 45 - 63 6.84E+03 382.93 1.85E+04

m 4 59.34 45 - 63 8.68E+04 686.49 1.87E+04

5 65.26 65 - 68 1.28E+03 248.85 1.38E+04

M 6 84.76 83 - 91 6.66E+02 204.69 1.06E+04

m 7 87.94 83 - 91 2.11E+04 368.89 1.10E+04

8 93.62 93 - 97 6.09E+02 203.08 8.37E+03

9 121.93 119 - 126 2.83E+03 293.69 1.25E+04

10 136.49 134 - 140 3.62E+02 238.83 1.01E+04

11 165.23 164 - 168 1.93E+02 17 3. 82 6.55E+03

12 187.80 186 - 191 1.79E+02 209.68 8.67E+03

13 238.60 237 - 241 2.70E+02 173.72 6.43E+03

14 352.74 350 - 356 1.70E+02 188.04 6.28E+03

15 518.37 515 - 521 1.53E+02 150.58 4.01E+03

16 639.07 637 - 642 1.18E+02 114.71 2.55E+03

M 17 661.79 655 - 672 2.98E+04 364.88 2.60E+03

m 18 666.87 655 - 672 1.46E+03 334. 72 4.12E+03

19 1073.55 1070 - 1076 1.43E+02 124.02 2.69E+03

20 1115.79 1112 - 1119 1.08E+02 131.85 2.80E+03

21 1121.26 1119 - 1123 7. llE+0l 84.89 1.54E+03

M 22 1173.53 1167 - 1183 2.38E+04 322.27 1.41E+03

m 23 1178.72 1167 - 1183 1.14E+03 222.49 1.68E+03

M 24 1332.83 1326 - 1343 2.17E+04 298.36 3.43E+02

m 25 1338.00 1326 - 1343 1.08E+03 212.92 2.50E+02

26 1452.45 144 9 - 1455 2.60E+0l 26.14 1.06E+02

27 1835.51 1831 - 1840 2.28E+0l 28.21 1.02E+02

M 28 2004.08 2000 - 2013 2.58E+0l 16.85 4.18E+0l

m 29 2011.16 2000 - 2013 2.06E+0l 19.18 3.94E+0l

30 2273.36 22 69 - 2277 1.77E+0l 21.99 6.47E+0l

31 2445.44 2 441 - 2448 7.85E+00 7.48 4.30E+00

Page 4 of25

Critical Level

1.74E+02 2.23E+02 2.23E+02 2.25E+02 2.51E+02 1.69E+02 l.72E+02 1.62E+02 2.25E+02 1.94E+02 1.41E+02 1. 71E+02 1.40E+02 1.53E+02 1.22E+02 9.26E+0l 8.38E+0l 1.06E+02 1.00E+02 1.07E+02 6.84E+0l 6.17E+0l 6.74E+0l 3.05E+0l 2.60E+0l 1.98E+0l 2.18E+0l 1.06E+0l 1.03E+0l 1.67E+0l 4.08E+00

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0152

4/17/2018 6:13:23AM Page 5 of 25

Analysis Report for 1803111-01

M

m m

M m

M

m

GAS-1402

Peak Energy ROI

No. (keV) start

32 2505.69 24 99 -33 2614.03 2 609 -

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet

Errors quoted at 2.000sigma

ROI Net Peak Net Area Continuum

end Area Uncertainty Counts

2512 3.36E+02 41. 55 4.42E+0l

2617 2.05E+0l 11.85 9.00E+00

PEAK WITH N/0 REPORT

Peak Analysis Performed on : 4/17/2018 6:13:15AM

Peak Analysis From Channel : 1

Peak Analysis To Channel : 4096

Tentative NID Library

Peak Match Tolerance

Peak Energy

No. (keV)

1 31.75 2 49.82

3 55.64 4 59.34 5 65.26 6 84.76 7 87.94

8 93.62 9 121.93

10 136.49

11 165.23 12 187.80 13 238.60 14 352.74 15 518.37 16 639.07 17 661.79 18 666.87

: \\OR-GAMMA 1 \ApexRoot\Countroom\Library\TMA2.NLB

: 1.000 keV

ROI ROI Peak Net Peak

start end Centroid Area

31 - 35 32.26 l.51E+03 45 - 63 50.31 6.00E+03

45 - 63 56.12 6.84E+03 45 - 63 59.82 8.68E+04 65 - 68 65.73 l.28E+03 83 - 91 85.22 6.66E+02 83 - 91 88.40 2. 11E+04

93 - 97 94.07 6.09E+02

119 - 126 122.35 2.83E+03

134 - 140 136.89 3.62E+02

164 - 168 165.62 l.93E+02

186 - 191 188.16 l.79E+02

237 - 241 238.92 2.70E+02

350 - 356 352. 96 l.70E+02

515 - 521 518.45 l.53E+02

637 - 642 639.06 l.18E+02

655 - 672 661.76 2.98E+04

655 - 672 666.84 l.46E+03

Net Area Continuum Uncertainty Counts

225.53 9.73E+03 363.22 l.84E+04

382.93 l.85E+04 686.49 l.87E+04 248.85 l.38E+04 204.69 l.06E+04 368.89 l.10E+04

203.08 8.37E+03 293.69 l.25E+04

238.83 l.01E+04

173.82 6.55E+03 209.68 8.67E+03 173.72 6.43E+03 188.04 6.28E+03 150.58 4.01E+03 114.71 2.55E+03 364.88 2.60E+03 334.72 4.12E+03

Critical Level

l.61E+0l 6.29E+00

Tentative Nuclide

TE-132 TH-227

AM-241

TH-231 CD-109 SN-126 LU-176 GA-67 CO-57 EU-152 SE-75 CO-57 SE-75 CE-139

PB-212 PB-214

CS-137 SB-126

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4/17/2018 6:13:23AM

Analysis Report for 1803111-01

M m M m

M m

M m m

M m

GAS-1402

Peak Energy ROI

No. (keV) start

19 1073.55 1070 -20 1115.79 1112 -21 1121.26 1119 -

22 1173.53 1167 -23 1178. 72 1167 -24 1332.83 132 6 -25 1338.00 1326 -26 1452.45 14 4 9 -27 1835.51 1831 -28 2004.08 2000 -29 2011.16 2000 -30 2273.36 22 69 -31 2445.44 2441 -32 2505.69 24 99 -33 2614.03 2 60 9 -

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet

Errors quoted at 2.000sigma

ROI Peak Net Peak Net Area

end Centroid Area Uncertainty

1076 1073.24 1.43E+02 124.02 1119 1115.44 1.08E+02 131.85 1123 1120.91 7.llE+0l 84.89

1183 1173.15 2.38E+04 322.27

1183 1178.33 1.14E+03 222.49

1343 1332.36 2.17E+04 298.36 1343 1337.52 l.08E+03 212.92

1455 1451.91 2.60E+0l 26.14 1840 1834.78 2.28E+0l 28.21 2013 2003.29 2.58E+0l 16.85 2013 2010.37 2.06E+0l 19.18 2277 2272.48 l.77E+0l 21.99 2448 2444.52 7.85E+00 7.48 2512 2504.75 3.36E+02 41.55 2617 2613.07 2.05E+0l 11. 85

PEAK EFFICIENCY REPORT

Peak Analysis Performed on : 4/17/2018 6:13:15AM

Peak Energy Net Peak Net Area Peak

No. (keV) Area Uncertainty Efficiency

1 31.75 l.51E+03 225.53 l.00E-02

2 49.82 6.00E+03 363.22 2.14E-02

3 55.64 6.84E+03 382.93 2.38E-02

4 59.34 8.68E+04 686.49 2.49E-02

5 65.26 l.28E+03 248.85 2.63E-02

6 84.76 6.66E+02 204.69 2.84E-02

7 87.94 2 .11E+04 368.89 2.85E-02

8 93.62 6.09E+02 203.08 2.85E-02

9 121.93 2.83E+03 293.69 2.73E-02

10 136.49 3.62E+02 238.83 2.63E-02

11 165.23 l.93E+02 173.82 2.43E-02

12 187.80 l.79E+02 209.68 2. 27E-02

13 238.60 2.70E+02 173.72 l.97E-02

Page 6 of25

Continuum Tentative Counts Nuclide

2.69E+03 2.80E+03 ZN-65 1.54E+03 TA-182

SC-46 BI-214

1.41E+03 CO-60 l.68E+03 3.43E+02 CO-60 2.50E+02 l.06E+02 l.02E+02 Y-88 4.18E+0l 3.94E+0l 6.47E+0l 4.30E+00 4.42E+0l 9.00E+00 TL-208

Efficiency Uncertainty

l.85E-03 l.85E-03 l.85E-03 l.85E-03 l.96E-03 2.35E-03 2.41E-03 2.38E-03 2.21E-03 2.45E-03 2.94E-03 2.88E-03 2.70E-03

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Analysis Report for 1803111-01

M m

M m M m

M m

M m m

M m

GAS-1402

Peak Energy Net Peak Net Area Peak Efficiency

No. (keV) Area Uncertainty Efficiency Uncertainty

14 352.74 1.70E+02 188.04 1.51E-02 2.30E-03

15 518.37 1.53E+02 150.58 1.13E-02 1.56E-03

16 639.07 l.18E+02 114. 71 9.59E-03 9.84E-04

17 661.79 2.98E+04 364.88 9.33E-03 8. 77E-04

18 666.87 1.46E+03 334. 72 9.27E-03 8.85E-04

19 1073.55 1.43E+02 124.02 6.34E-03 7.73E-04

20 1115.79 1.08E+02 131.85 6.15E-03 6.65E-04

21 1121.26 7.llE+0l 84.89 6.12E-03 6.51E-04

22 1173.53 2.38E+04 322.27 5.91E-03 5.18E-04

23 1178.72 1.14E+03 222.49 5.89E-03 5,17E-04

24 1332.83 2.17E+04 298.36 5.35E-03 4.71E-04

25 1338.00 1.08E+03 212.92 5.33E-03 4. 71E-04

26 1452.45 2.60E+0l 26.14 5.0lE-03 4.72E-04

27 1835.51 2.28E+0l 28.21 4.23E-03 4. 77E-04

28 2004.08 2.58E+0l 16.85 3.99E-03 4. 77E-04

29 2011.16 2.06E+0l 19.18 3.98E-03 4.77E-04

30 2273.36 1.77E+0l 21.99 3.69E-03 4. 77E-04

31 2445.44 7.85E+00 7.48 3.54E-03 4. 77E-04

32 2505.69 3.36E+02 41. 55 3.50E-03 4. 77E-04·

33 2614.03 2.05E+0l 11. 85 3.42E-03 4. 77E-04

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet Errors quoted at 2.000 sigma

BACKGROUND SUBTRACT REPORT

Peak Analysis Performed on

Env. Background File

Peak Energy

No. (keV)

1 31.75 2 49.82 3 55.64 4 59.34 5 65.26 6 84.76 7 87.94 8 93.62 9 121.93

10 136.49

: 4/17/2018 6:13:15AM

: \\OR-GAMMA 1\ApexRoot\Countroom\Data\0000063824.CNF

Original Orig. Area Ambient Backgr. Subtracted Subtracted

Area Uncertainty Background Uncert. Area Uncert.

l.51E+03 225.53 l.51E+03 2.26E+02

6.00E+03 363.22 6.00E+03 3.63E+02

6.84E+03 382.93 6.84E+03 3.83E+02

8.68E+04 686.49 8.68E+04 6.86E+02

1.28E+03 248.85 1.28E+03 2. 4 9E+02

6.66E+02 204.69 5.20E+00 1.31E+00 6.60E+02 2.05E+02

2. 11E+04 368.89 1.93E+00 1.15E+00 2.11E+04 3.69E+02

6.09E+02 203.08 6.09E+02 2.03E+02

2.83E+03 293.69 2.83E+03 2.94E+02

3.62E+02 238.83 3.62E+02 2.39E+02

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Analysis Report for 1803111-01

GAS-1402

Peak Energy Original Orig. Area Ambient Backgr. Subtracted

No. (keV) Area Uncertainty Background Uncert. Area

11 165.23 1.93E+02 173.82 1.93E+02

12 187.80 1.79E+02 209.68 1.79E+02

13 238.60 2.70E+02 173.72 1.05E+0l 3.06E+00 2.59E+02

14 352.74 1.70E+02 188.04 3.23E+00 2.56E+00 1.67E+02

15 518.37 1.53E+02 150.58 1.53E+02

16 639.07 1.18E+02 114. 71 1.18E+02

M 17 661.79 2.98E+04 364.88 2.98E+04

m 18 666.87 1.46E+03 334. 72 1.46E+03

19 1073.55 1.43E+02 124.02 1.43E+02

20 1115.79 1.08E+02 131.85 1.08E+02

21 1121.26 7.llE+0l 84.89 7.llE+0l

M 22 1173.53 2.38E+04 322.27 2.38E+04

m 23 1178.72 1.14E+03 222.49 1.14E+03

M 24 1332.83 2.17E+04 298.36 2.17E+04

m 25 1338.00 1.08E+03 212.92 1.08E+03

26 1452.45 2.60E+0l 26.14 2.60E+0l

27 1835.51 2.28E+0l 28.21 2.28E+0l

M 28 2004.08 2.58E+0l 16.85 2.58E+0l

m 29 2011.16 2.06E+0l 19.18 2.06E+0l

30 2273.36 1.77E+0l 21.99 1.77E+0l

31 2445.44 7.85E+00 7.48 7.85E+00

32 2505.69 3.36E+02 41. 55 3.36E+02

33 2614.03 2.05E+0l 11. 85 2.50E+00 8.43E-01 1.80E+0l

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet Errors quoted at 2.000sigma

AREA CORRECTION REPORT REFERENCEPEAKIBKG.SUBTRACT

Peak Analysis Performed on

Ref. Peak Energy

Peak Ratio

: 4/17/2018 6:13:15AM

: 0.00 Reference Date

: 0.00 Uncertainty : 0.00

Background File : \\OR-GAMMA 1 \ApexRoot\Countroom\Data\0000063824.CN F

Corrected Area is: Original * Peak Ratio - Background

Peak Energy Original Orig. Area Ambient Backgr.

No. (keV) Area Uncertainty Background Uncert.

1 31.75 1.51E+03 225.53

M 2 49.82 6.00E+03 363.22

m 3 55.64 6.84E+03 382.93

m 4 59.34 8.68E+04 686.49

5 65.26 1.28E+03 248.85

Corrected Area

1.51E+03 6.00E+03 6.84E+03 8.68E+04 1.28E+03

Subtracted Uncert.

1.74E+02 2.10E+02 1.74E+02 1.88E+02 1.51E+02 1.15E+02 3.65E+02 3.35E+02 l.24E+02 1.32E+02 8.49E+0l 3.22E+02 2.22E+02 2.98E+02 2.13E+02 2.61E+0l 2.82E+0l 1.69E+0l 1.92E+0l 2.20E+0l 7.48E+00 4.15E+0l 1.19E+0l

Corrected Uncert.

2.26E+02 3.63E+02 3.83E+02 6.86E+02 2.49E+02

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Analysis Report for 1803111-01

GAS-1402

Peak Energy Original Orig. Area Ambient Backgr. Corrected Corrected

No. (keV) Area Uncertainty Background Uncert. Area Uncert.

M 6 84.76 6.66E+02 204.69 5.20E+00 1.31E+00 6.60E+02 2.05E+02

m 7 87.94 2.11E+04 368.89 1.93E+00 1.15E+00 2.11E+04 3.69E+02

8 93.62 6.09E+02 203.08 6.09E+02 2.03E+02

9 121. 93 2.83E+03 293.69 2.83E+03 2.94E+02

10 136.49 3.62E+02 238.83 3.62E+02 2.39E+02

11 165.23 l.93E+02 173.82 1.93E+02 1.74E+02

12 187.80 1.79E+02 209.68 l.79E+02 2.10E+02

13 238.60 2.70E+02 173.72 1.05E+0l 3.06E+00 2.59E+02 1.74E+02

14 352.74 1.70E+02 188.04 3.23E+00 2.56E+00 l.67E+02 1.88E+02

15 518.37 1.53E+02 150.58 1.53E+02 l.51E+02

16 639.07 1.18E+02 114.71 1.18E+02 1.15E+02

M 17 661.79 2.98E+04 364.88 2.98E+04 3.65E+02

m 18 666.87 1.46E+03 334. 72 l.46E+03 3.35E+02

19 1073.55 1.43E+02 124.02 1.43E+02 1.24E+02

20 1115.79 l.08E+02 131.85 1.08E+02 1.32E+02

21 1121.26 7. llE+0l 84.89 7.llE+0l 8.49E+01

M 22 1173.53 2.38E+04 322.27 2.38E+04 3.22E+02

m 23 1178.72 l.14E+03 222.49 l.14E+03 2.22E+02

M 24 1332.83 2.17E+04 298.36 2.17E+04 2.98E+02

m 25 1338.00 l.08E+03 212. 92 l.08E+03 2.13E+02

26 1452.45 2.60E+0l 26.14 2.60E+0l 2.61E+0l

27 1835.51 2.28E+0l 28. 21 2.28E+0l 2.82E+0l

M 28 2004.08 2.58E+0l 16.85 2.58E+0l 1.69E+0l

m 29 2011.16 2.06E+0l 19.18 2.06E+0l 1.92E+01

30 2273.36 1.77E+0l 21. 99 1.77E+0l 2.20E+01

31 2445.44 7.85E+00 7.48 7.85E+00 7.48E+00

32 2505.69 3.36E+02 41.55 3.36E+02 4.15E+01

33 2614.03 2.05E+0l 11. 85 2.50E+00 8.43E-0l 1.80E+0l 1.19E+0l

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet

Errors quoted at 2.000sigma

NUCLIDE IDENTIFICATION REPORT

Nuclide Library Used : \ \0 R-GAM MA 1 \Apex Root\Cou ntroom\Library\ TMA2. NLB

IDENTIFIED NUCLIDES

Nuclide Name Id Confidence Energy (keV) Yield(¾) Activity Activity

(pCilgrams) Uncertainty

CO-57 0.890 122.06 * 85.51 6.78E+0l 8.92E+00

136.48 * 10.60 7.26E+01 4.83E+0l

CO-60 0.980 1173.22 * 100.00 1.31E+02 1.17E+0l

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0157

Analysis Report for 1803111-01

GAS-1402

Nuclide Name Id Confidence

CO-60 0.980 ZN-65 0.859 CD-109 0. 961 SN-126 0.978 CS-137 0.997 CE-139 0.605 PB-212 0.894

PB-214 0.365

AM-241 0.994

* == Energy line found in the spectrum.

- == Manually added nuclide.

? == Manually edited nuclide.

Energy Tolerance : 1.000 keV

Nuclide confidence index threshold == 0.30

Errors quoted at 2.000sigma

4/17/2018 6:13:23AM

Energy (keV) Yield(%) Activity

(pCi/grams)

1332.49 * 100.00 1.32E+02

1115.52 * 50.75 2.76E+0l

88.03 * 3. 72 2.80E+03

87.57 * 37.00 4.08E+0l

661.65 * 85.12 8.31E+0l

165.85 * 80.35 1.37E+02

238.63 * 44.60 6.02E-01

300.09 3.41 295.21 19.19 351.92 * 37.19 6.06E-01

59.54 * 35.90 1.99E+02

UNIDENTIFIED PEAKS

M

m

M

m

m m

Peak Locate Performed on

Peak Locate From Channel

Peak Locate To Channel

Peak No. Energy (keV)

1 31.75 2 49.82

3 55.64 5 65.26 6 84.76 8 93.62

12 187.80 15 518.37 16 639.07 18 666.87 19 1073.55 21 1121.26

23 1178.72 25 1338.00 26 1452.45

: 4/17/2018 6:13:15AM

: 1 : 4096

Peak Size (CPS)

8.36269E-01 3.33603E+00

3.80080E+00 7.12556E-01 3.66911E-01 3.38259E-0l 9.93056E-02 8.49036E-02 6. 57231E-02 8.11195E-01 7.92306E-02 3.95080E-02

6.35087E-01 5.98856E-01 1.44374E-02

Peak CPS(%) Uncertainty

7.49 3.02

2.80 9.70

15.50 16.68 58.65 49.27 48.48 11. 4 6 43.48 59.68

9.73 9.88

50.30

Peak Type

Tol.

Tol. D-Esc

Sum

Tol.

Tol.

Sum

Page 10 of25

Activity

Uncertainty

1.18E+0l 3.39E+0l 2.43E+02 3.53E+00 7.88E+00 l.24E+02 4. llE-01

6.90E-01 l.49E+0l

Tolerance Nuclide

TE-132 TH-227

TH-231

SB-126

SC-46 TA-182 BI-214

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0158

Analysis Report for 1803111-01

M m

GAS-1402

Peak No. Energy (keV)

27 1835.51 28 2004.08 29 2011.16 30 2273.36 31 2445.44 32 2505.69 33 2614.03

M = First peak in a multiplet region

m = other peak in a multiplet region

F = Fitted singlet

Errors quoted at 2.000sigma

Peak Size (CPS)

1.26426E-02 l.43245E-02 1.14191E-02 9. 81111E-03 4. 36111E-03 1.86598E-01 l.00000E-02

4/17/2018 6:13:23AM

Peak CPS(%) Peak

Uncertainty Type

61.99 Sum 32.68 46.66 62. 2 6 47.66

6.18 Sum 33.01 Tol.

NUCLIDE IDENTIFICATION REPORT

Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\TMA2.NLB

IDENTIFIED NUCLIDES

Nuclide Id Energy Yield(¾) Activity

Page 11 of25

Tolerance

Nuclide

TL-208

Activity

Name Confidence (keV) (pCilgrams) Uncertainty

CO-57 0.89 122.06 * 85.51 6.78E+0l 8.92E+00

136.48 * 10.60 7.26E+0l 4.83E+0l

CO-60 0.98 1173.22 * 100.00 l.31E+02 1.17E+0l

1332.49 * 100.00 1.32E+02 1.18E+0l

ZN-65 0.85 1115.52 * 50.75 2.76E+0l 3.39E+0l

CD-109 0. 96 88.03 * 3. 72 2.80E+03 2.43E+02

SN-126 0.97 87.57 * 37.00 4.08E+0l 3.53E+00

CS-137 0.99 661.65 * 85.12 8.31E+0l 7.88E+00

CE-139 0.60 165.85 * 80.35 1.37E+02 1. 2 4E+02

PB-212 0.89 238.63 * 44.60 6.02E-01 4.llE-01

300.09 3.41

PB-214 0.36 295.21 19.19 351.92 * 37.19 6.06E-01 6.90E-01

AM-241 0.99 59.54 * 35.90 1.99E+02 1.49E+0l

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0159

Analysis Report for 1803111-01

GAS-1402

* = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity

Energy Tolerance : 1.000 keV

Nuclide confidence index threshold = 0.30

Errors quoted at 2.000sigma

4/17/2018 6:13:23AM

INTERFERENCE CORRECTED REPORT

Nuclide Name

CO-57 CO-60 ZN-65

? CD-109 ? SN-126

CS-137 CE-139 PB-212 PB-214 AM-241

Nuclide Id

Confidence

0.890 0.980 0.859 0. 961 0.978 0.997 0.605 0.894 0.365 0.994

? X

= =

nuclide is part of an undetermined solution

nuclide rejected by the interference analysis

Wt mean Activity

(pCilgrams)

6.79E+0l 1.32E+02 2.76E+0l 2.80E+03 4.08E+0l 8.31E+0l 1.37E+02 6.02E-0l 6.06E-0l 1.99E+02

@ = nuclide contains energy lines not used in Weighted Mean Activity

Errors quoted at 2.000sigma

Wt mean Activity

Uncertainty

8.77E+00 8.28E+00 3.39E+0l 2.43E+02 3.53E+00 7.88E+00 1.24E+02 4. llE-01 6.90E-01 1.49E+0l

Page 12 of25

Comments

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0160

Analysis Report for 1803111-01

M

m

M

m

m m

M

m

GAS-1402

Peak Locate Performed on

Peak Locate From Channel

Peak Locate To Channel

Peak No. Energy (keV)

1 31.75

2 49.82

3 55.64

5 65.26

6 84.76

8 93.62

12 187.80

15 518.37

16 639.07

18 666.87

19 1073.55

21 1121.26

23 1178.72

25 1338.00

26 1452.45

27 1835.51

28 2004.08

29 2011.16

30 2273.36

31 2445.44

32 2505.69

33 2614.03

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet

Errors quoted at 2.000sigma

4/17/2018 6:13:23AM

UNIDENTIFIED PEAKS

: 4/17/2018 6:13:15AM

: 1 : 4096

Peak Size (CPS)

8.36269E-01

3.33603E+00

3.80080E+00

7.12556E-01

3.66911E-01

3.38259E-01

9.93056E-02

8.49036E-02

6.57231E-02

8. 11195E-01

7.92306E-02

3.95080E-02

6.35087E-01

5.98856E-01

1.44374E-02

1.26426E-02

1.43245E-02

l.14191E-02

9. 81111E-03

4. 36111E-03

1.86598E-01

1.00000E-02

Peak CPS(%) Peak

Uncertainty Type

7.49 3.02 Tol.

2.80 9.70

15.50 Tol.

16.68 D-Esc

58.65 49.27 Sum

48.48

11. 46 Tol.

43.48

59.68 Tol.

9.73 9.88 Sum

50.30 61.99 Sum

32.68 46.66

62.26 47.66

6.18 Sum

33.01 Tol.

Page 13 of25

Tolerance Nuclide

TE-132

TH-227

TH-231

SB-126

SC-46 TA-182

BI-214

TL-208

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Analysis Report for 1803111-01

GAS-1402

NUCLIDE MDA REPORT

Nuclide Library Used : \\OR-GAMMA 1\ApexRoot\Countroom\Library\TMA2.NLB

Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA

Name (keV) (pCi/grams) (pCi/grams) (pCi/grams)

+ BE-7 477.59 10.42 -6.60E+05 8.02E+07 8.02E+07

+ NA-22 1274.54 99.94 -4.74E-03 6.79E-01 6.79E-01

+ NA-24 1368.53 99.99 -5.46E-02 7.35E-02 1.78E-01

2754.09 99.86 2.45E-02 7.35E-02

+ AL-26 1808.65 99.76 -1.20E-03 1.73E-01 1.73E-01

+ K-40 1460.81 10.67 1.26E+00 l.90E+00 1.90E+00

+ @ AR-41 1293.64 99.16 1.00E+26 1.00E+26 1.00E+26

+ TI-44 67,88 94.40 1.68E-01 3.07E-01 3.62E-01

78.34 96.00 1.33E-02 3.07E-01

+ SC-46 889.25 98.98 -l.81E+03 2.42E+04 2.49E+04

1120.51 99.90 -1.44E+04 2.42E+04

+ @ V-48 983.52 99.98 1.00E+26 1.00E+26 1.00E+26

@ 1312 .10 97.50 1.00E+26 1.00E+26

+ CR-51 320.08 9.83 5.43E+13 3.96E+14 3.96E+14

+ MN-54 834.83 99.97 2.17E+00 8.79E+00 8.79E+00

+ CO-56 846.75 99. 96 5.34E+04 1.12E+05 1.77E+05

1037.75 14.03 6.00E+05 1.38E+06

1238.25 67.00 2.30E+04 1.51E+05

1771.40 15.51 -3.26E+04 4 .11E+05

2587.48 16.90 -3.00E+04 1.12E+05

+ CO-57 122.06 * 85.51 6.78E+0l 1.08E+0l 1.08E+0l

136.48 * 10.60 7.26E+0l 7.82E+0l

+ CO-58 810.76 99.40 -1.28E+05 1.48E+05 1.48E+05

+ FE-59 1099.22 56.50 -1.22E+08 3.16E+08 5.58E+08

1291.56 43.20 1.43E+07 3.16E+08

+ CO-60 1173.22 * 100.00 1.31E+02 9.45E-01 1.63E+00

1332.49 * 100.00 1.32E+02 9.45E-01

+ ZN-65 1115. 52 * 50.75 2.76E+0l 5.56E+0l 5.56E+0l

+ @ GA-67 93.31 35.70 1.00E+26 1.00E+26 1.00E+26

@ 208.95 2.24 1.00E+26 1.00E+26

@ 300.22 16.00 1.00E+26 1.00E+26

+ SE-75 121. 11 16.70 2.25E+04 6.92E+02 3.06E+03

136.00 59.50 1.24E+03 6.92E+02

264.65 59.80 -5.67E+0l 9.74E+02

27 9. 53 25.20 1.33E+03 2.33E+03

400.65 11. 40 2.19E+03 6.07E+03

+ RB-82 776.52 13.00 -8.34E+14 5.97E+15 5.97E+l5

+ RB-83 520.41 46.00 -1.15E+03 2.83E+04 2.83E+04

529.64 30.30 -2.39E+04 4.17E+04

552.65 16.40 9.53E+03 7.58E+04

+ KR-85 513.99 0.43 7.43E+0l 1.16E+02 1.16E+02

+ SR-85 513.99 99.27 2.63E+05 4.10E+05 4.10E+05

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Analysis Report for 1803111-01

GAS-1402

Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA

Name (keV) (pCi/grams) (pCi/grams) (pCi/grams)

+ Y-88 898.02 93.40 1.78E+03 8.47E+02 2.76E+03

1836.01 99.38 6.12E+02 8.47E+02

+ MO-93 263.06 56.72 8.80E-02 2.24E-01 7.23E-01

684.67 99.68 -8.70E-02 4.96E-01

1477.11 99.08 -2.71E-03 2.24E-01

+ NB-93M 16.57 9.43 -1.83E+09 1.11E+09 1.11E+09

+ NB-94 702.63 100.00 -9.89E-02 4.02E-01 4.02E-01

871.10 100.00 -1.05E-01 5.30E-01

+ NB-95 765.79 99.81 -3.33E+10 5.57E+10 5.57E+10

+ @ NB-95M 235.69 25.00 1.00E+26 1.00E+26 1.00E+26

+ ZR-95 724.18 43.70 -5.26E+05 9.47E+05 1.13E+06

756.72 55.30 -3.08E+05 9.47E+05

+ @ MO-99 181.06 6.20 1.00E+26 1.00E+26 1.00E+26

@ 739.58 12.80 1.00E+26 l.00E+26

@ 778.00 4.50 1.00E+26 1.00E+26

+ TC-99M 140.51 89.00 4.46E-03 2.46E-01 2.46E-01

+ RU-103 497.08 89.00 1.48E+08 3.54E+09 3.54E+09

+ RU-106 621. 84 9.80 -2.02E+0l 4.58E+0l 4.58E+0l

+ AG-108M 433.93 89.90 -4.79E-0l 4.48E-01 4.65E-0l

614.37 90.40 -1.06E-01 4.48E-01

722.95 90.50 -2.22E-02 4.58E-01

+ CD-109 88.03 * 3. 72 2.80E+03 7.45E+0l 7.45E+0l

+ AG-ll0M 657.75 93.14 -3.12E+02 2.75E+0l 4.44E+0l

677.61 10.53 -2.65E+0l 1.36E+02

706.67 16.46 -1.06E+0l 8.93E+0l

763.93 21.98 1. 96E+0l 7.22E+0l

884.67 21. 98 -1.77E+0l 9.00E+0l

1384.27 23.94 -5.88E+00 2.75E+0l

+ CD-113M 263.70 0.02 2.73E+02 1.69E+03 1.69E+03

+ SN-113 255.12 1. 93 -8.10E+03 1.43E+03 3.41E+04

391.69 64.90 3.25E+02 1.43E+03

+ TE-123M 159.00 84.10 2.37E+02 4.86E+02 4.86E+02

+ SB-124 602.71 97.87 -5.79E+05 1.04E+06 1.16E+06

645.85 7.26 -2.26E+06 1.63E+07

722. 7 8 11.10 -5.24E+05 1.08E+07

1691.02 49.00 -2.19E+05 1.04E+06

+ I-125 35.49 6.49 2.92E+07 2.37E+07 2.37E+07

+ SB-125 176.33 6.89 -4.12E+00 3.38E+00 8.l0E+00

427.89 29.33 1.29E-01 3.38E+00

463.38 10.35 5.46E+00 1.07E+0l

600.56 17.80 -1.68E+00 5.25E+00

635.90 11. 32 -1.94E+00 8.51E+00

+ SB-126 414.70 83.30 -2.42E-0l 3.96E-01 4.74E-01

666.33 99.60 -2.0lE+0l 9.07E-01

695.00 99.60 -1.07E-01 3.96E-01

720.50 53.80 1.22E-01 7.60E-01

+ SN-126 87.57 * 37.00 4.08E+0l 1.08E+00 1.08E+00

+ @ SB-127 473.00 25.00 l.00E+26 1.00E+26 1.00E+26

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Analysis Report for 1803111-01

GAS-1402

Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA

Name (keV) (pCi!grams) (pCi!grams) (pCi!grams)

@ SB-127 685.00 35.70 l.00E+26 l.00E+26 l.00E+26

@ 783.80 14.70 l.00E+26 l.00E+26

+ I-129 29.78 57.00 -2.14E+00 l.70E+00 l.70E+00

33.60 13.20 l.83E+00 4. 96E+00

39.58 7.52 -2.46E+0l 6.06E+00

+ @ I-131 284.30 6.05 l.00E+26 l.00E+26 l.00E+26

@ 364.48 81.20 l.00E+26 l.00E+26

@ 636.97 7.26 l.00E+26 l.00E+26

@ 722.89 1. 80 l.00E+26 l.00E+26

+ @ TE-132 49.72 13.10 l.00E+26 l.00E+26 l.00E+26

@ 228.16 88.00 l.00E+26 l.00E+26

+ BA-133 81.00 33.00 -4.40E-01 7.58E-01 l.07E+00

302.84 17.80 -l.50E+00 2.33E+00

356.01 60.00 7.74E-03 7.58E-01

+ @ I-133 529.87 86.30 l.00E+26 l.00E+26 l.00E+26

+ @ XE-133 81.00 38.00 l.00E+26 l.00E+26 l.00E+26

+ CS-134 563.23 8.38 3.52E+00 l.31E+00 l.51E+0l

569.32 15.43 l.60E+00 8.24E+00

604.70 97.60 -l.25E-01 l.31E+00

795.84 85.40 5.64E-01 l.79E+00

801.93 8.73 -8.20E+00 l.76E+0l

+ CS-135 268.24 16.00 6.87E-01 2.04E+00 2.04E+00

+ @ I-135 1131.51 22.50 l.00E+26 l.00E+26 l.00E+26

@ 1260.41 28.60 l.00E+26 l.00E+26

@ 1678.03 9.54 l.00E+26 l.00E+26

+ @ CS-136 153.22 7.46 l.00E+26 l.00E+26 l.00E+26

@ 163.89 4.61 l.00E+26 l.00E+26

@ 176.55 13.56 l.00E+26 l.00E+26

@ 273.65 12.66 l.00E+26 l.00E+26

@ 340.57 48.50 l.00E+26 l.00E+26

@ 818.50 99.70 l.00E+26 l.00E+26

@ 1048.07 79.60 l.00E+26 l.00E+26

@ 1235.34 19.70 l.00E+26 l.00E+26

+ CS-137 661.65 * 85.12 8.31E+0l l.27E+00 l.27E+00

+ LA-138 788.74 34.00 2.32E-01 2.76E-01 l.32E+00

1435.80 66.00 2.81E-02 2.76E-01

+ CE-139 165.85 * 80.35 l.37E+02 2.02E+02 2.02E+02

+ @ BA-140 162.64 6.70 l.00E+26 l.00E+26 l.00E+26

@ 304.84 4.50 l.00E+26 l.00E+26

@ 423.70 3.20 l.00E+26 l.00E+26

@ 437.55 2.00 l.00E+26 l.00E+26

@ 537.32 25.00 l.00E+26 l.00E+26

+ @ LA-140 328.77 20.50 l.00E+26 l.00E+26 l.00E+26

@ 487.03 45.50 l.00E+26 l.00E+26

@ 815.85 23.50 l.00E+26 l.00E+26

@ 1596.49 95.49 l.00E+26 l.00E+26

+ CE-141 145.44 48.40 2.66E+ll 4.47E+ll 4.47E+ll

+ @ CE-143 57.36 11.80 l.00E+26 l.00E+26 l.00E+26

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Analysis Report for 1803111-01

GAS-1402

Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA

Name (keV) (pCi/grams) (pCilgrams) (pCi/grams)

@ CE-143 293.26 42.00 1.00E+26 1.00E+26 1.00E+26

@ 664.55 5.20 1.00E+26 1.00E+26

+ CE-144 133.54 10.80 -8.05E-01 4.78E+0l 4.78E+0l

+ PM-144 476.78 42.00 1.60E+00 4.74E+00 1.23E+0l

618.01 98.60 -3.15E-01 4.76E+00

696. 4 9 99.49 4.24E-01 4:74E+00

+ PM-145 36.85 21. 70 1.99E+00 1.41E+00 2.57E+00

37.36 39.70 6.18E-01 1.41E+00

42.30 15.10 -3.07E+00 3.68E+00

72.40 2.31 -6.58E+00 1.42E+0l

+ PM-146 453.90 39.94 8.19E-01 1.73E+00 1.73E+00

735.90 14.01 1.90E+00 4.77E+00

747.13 13. 10 2.80E+00 5.17E+00

+ @ ND-147 91.11 28.90 1.00E+26 1.00E+26 l.00E+26

@ 531.02 13.10 1.00E+26 1.00E+26

+ @ PM-149 285.90 3.10 1.00E+26 l.00E+26 1.00E+26

+ EU-152 121.78 20.50 1.23E+0l 1.55E+00 l.68E+00

244.69 5.40 3.76E+00 6.21E+00

344.27 19.13 -1.18E+00 2.16E+00

778.89 9.10 9.48E-01 5.93E+00

964.01 10.40 1.15E+00 7.03E+00

1085.78 7.22 -6.52E-01 9.71E+00

1112.02 9.60 3.26E-01 7.25E+00

1407.95 14. 94 1.88E-01 1.55E+00

+ GD-153 97.43 31.30 6.84E-01 2.70E+0l 2.70E+0l

103.18 22.20 5.77E+00 3.86E+0l

+ EU-154 123.07 40.50 6.57E+00 9.35E-01 9.35E-01

723.30 19.70 -l.32E-01 2.73E+00

873.19 11.50 -1.12E+00 6.15E+00

996. 32 10.30 -2.76E-01 7.40E+00

1004.76 17.90 -4.28E-01 4.28E+00

1274.45 35.50 -6.86E-03 9.84E-01

+ EU-155 86.50 30.90 7.66E+0l 1.65E+00 2.91E+00

105.30 20.70 7.67E-02 1.65E+00

+ @ EU-156 811.77 10.40 l.00E+26 1.00E+26 l.00E+26

@ 1153.47 7.20 l.00E+26 1.00E+26

@ 1230.71 8.90 1.00E+26 1.00E+26

+ HO-166M 184.41 72. 60 -1.02E-01 3.45E-01 3.45E-01

280.45 29.60 4.66E-01 1. llE+00

410.94 11.10 7.50E-01 3.60E+00

711.69 54.10 -1.97E-01 7.62E-01

+ TM-171 66. 72 0.14 2.77E+03 9.01E+02 9.01E+02

+ HF-1 72 67.35 5.31 1.07E+0l 7.32E+00 2.31E+0l

125.82 11. 30 -1.42E+00 7.32E+00

+ @ LU-1 72 181.53 20.60 1.00E+26 1.00E+26 l.00E+26

@ 900.72 29.81 1.00E+26 l.00E+26

@ 1093.66 62.50 1.00E+26 l.00E+26

+ LU-173 100.72 5.24 7.97E+00 9.26E+00 2.39E+0l

272 .11 21.20 1.94E+00 9.26E+00

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Analysis Report for 1803111-01

GAS-1402

Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA

Name (keV) (pCilgrams) (pCilgrams) (pCilgrams)

+ HF-175 343.40 84.00 -8.18E+04 l.50E+05 l.50E+05

+ LU-176 88.34 13. 30 l.09E+02 3.03E-01 4.08E+00

201.83 86.00 -2.04E-02 3.03E-01

306.78 94.00 -l.35E-01 3.55E-01

+ HF-181 133.02 41.70 -9.45E+07 7.76E+08 8.03E+08

345.85 17.20 9.27E+08 3.18E+09

482.03 82.80 l.19E+08 7.76E+08

+ TA-182 67.75 41.20 9.39E+02 2.02E+03 2.02E+03

1121.30 34.90 -l.74E+03 3.91E+03

1189.05 16.23 -7.74E+02 6.44E+03

1221. 41 26.98 -9.39E+02 3.09E+03

1231.02 11. 44 -l.37E+03 6.85E+03

+ IR-192 308.46 29.68 l.73E+05 l.72E+05 2.09E+05

468.07 48.10 5.68E+03 l.72E+05

+ HG-203 279.19 77.30 -l.68E+07 9.67E+07 9.67E+07

+ TL-204 374.74 94. 11 8.04E-02 7.42E-01 7.42E-01

899.15 99.16 9.53E-02 l.l0E+00

911. 7 4 91.10 5.73E-01 l.24E+00

+ BI-207 569.67 97. 72 4.53E-03 4.23E-01 4.23E-01

1063.62 74.90 -4.12E-01 8.13E-01

+ TL-208 583.14 30.22 l.07E+00 4.40E-01 l.31E+00

860.37 4.48 l.53E+00 l.17E+0l

2614.66 35.85 4.05E-01 4.40E-01

+ BI-210M 262.00 45.00 6.37E-02 7.27E-0l 7.27E-0l

300.00 23.00 6.83E-01 l.45E+00

+ PB-210 46.50 4.25 -9.55E+0l l.46E+0l l.46E+0l

+ PB-211 404.84 2.90 -7.04E+00 l.33E+0l l.33E+0l

831.96 2.90 l.15E+0l l.72E+0l

+ BI-212 727.17 11. 80 4.65E-01 3.54E+00 3.54E+00

1620.62 2.75 -l.36E+00 6.12E+00

+ PB-212 238.63 * 44.60 6.02E-01 6.58E-01 6.58E-01

300.09 3.41 4.61E+00 9.80E+00

+ BI-214 609.31 46.30 l.03E-02 8.58E-01 8.58E-01

1120.29 15.10 -2.15E+00 3.62E+00

1764.49 15.80 5.83E-01 l.23E+00

2204.22 4.98 -1.0lE+00 3.78E+00

+ PB-214 295.21 19.19 5.19E-01 l.12E+00 l.74E+00

351.92 * 37.19 6.06E-01 l.12E+00

+ RN-219 401.80 6.50 -l.97E+00 5.94E+00 5.94E+00

+ RA-223 323.87 3.88 -4.12E+00 8.76E+00 8.76E+00

+ RA-224 240.98 3.95 -l.29E+00 7.14E+00 7.14E+00

+ @ RA-225 40.00 31.00 l.00E+26 l.00E+26 l.00E+26

+ RA-226 186.21 3.28 l.33E+00 7.80E+00 7.80E+00

+ TH-227 50.10 8.40 3.43E+0l 2.46E+00 7.96E+00

236.00 11. 50 -8.66E-02 2.46E+00

256.20 6.30 -3.44E-01 5.14E+00

+ AC-228 338.32 11. 40 -l.37E+00 2.14E+00 2.99E+00

911. 07 27.70 l.16E+00 2.14E+00

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Analysis Report for 1803111-01

GAS-1402

Nuclide Energy Yield(¾) Activity Nuclide MDA Line MDA

Name (keV) (pCi/grams) (pCilgrams) (pCi/grams)

AC-228 969 .11 16.60 -2.31E-01 2.14E+00 3.55E+00

+ TH-230 48.43 16.90 1.41E+0l 3.76E+00 3.76E+00

62.85 4.60 -6.15E+02 1.25E+0l

67.67 0.37 4.13E+0l 8.89E+0l

+ PA-231 283.67 1.60 1.87E+00 1.43E+0l 2.05E+0l

302.67 2.30 -9.16E+00 1.43E+0l

+ TH-231 25.64 14.70 -2.57E+02 4.92E+00 2.02E+0l

84.21 6.40 -2.50E+02 4.92E+00

+ PA-233 311.98 38.60 8.14E+13 2.36E+l4 2.36E+14

+ PA-234 131.20 20.40 -8.62E-02 1.06E+00 1.06E+00

733.99 8.80 -2.41E-01 4.87E+00

946.00 12.00 -7.02E-01 5.26E+00

+ PA-234M 1001.03 0.92 -5.20E-01 6.28E+0l 6.28E+0l

+ TH-234 63.29 3.80 -5.92E+02 1.0lE+0l 1.0lE+0l

+ U-235 143.76 10.50 2.64E-01 2.12E+00 2.12E+00

163.35 4.70 -1.42E+00 4.90E+00

205.31 4.70 -2.91E+00 5.55E+00

+ NP-237 86.50 12.60 1.15E+02 4.36E+00 4.36E+00

+ @ NP-239 106.10 22.70 l.00E+26 l.00E+26 1.00E+26

@ 228.18 10.70 l.00E+26 l.00E+26

@ 277.60 14.10 l.00E+26 1.00E+26

+ AM-241 59.54 * 35.90 l.99E+02 3.18E+00 3.18E+00

+ AM-243 74.67 66.00 2.77E-01 4.33E-01 4.33E-0l

+ CM-243 209.75 3.29 -3.05E+00 2.55E+00 8.89E+00

228.14 10.60 2. llE+00 2.94E+00

277. 60 14.00 -3.99E-01 2.55E+00

+ = Nuclide identified during the nuclide identification

* = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

NUCLIDE MDA REPORT

Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\TMA2.NLB

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Analysis Report for 1803111-01

GAS-1402

Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level

Name (keV) (pCilgrams) (pCi/grams) (pCilgrams) (pCilgrams)

BE-7 477.59 10.42 8.02E+07 8.02E+07 -6.60E+05 3.97E+07

NA-22 1274.54 99.94 6.79E-0l 6.79E-01 -4.74E-03 3.27E-01

NA-24 1368.53 99.99 1.78E-01 7.35E-02 -5.46E-02 8.40E-02

2754.09 99.86 7.35E-02 2.45E-02 2.85E-02

AL-26 1808.65 99.76 1.73E-01 1.73E-01 -1.20E-03 8.02E-02

K-40 1460.81 10.67 1.90E+00 1.90E+00 1.26E+00 8.96E-01

@ AR-41 1293.64 99.16 l.00E+26 l.00E+26 l.00E+26 1.00E+20

TI-44 67.88 94.40 3.62E-01 3.07E-01 1.68E-01 l.80E-01

78.34 96. 00 3.07E-01 1.33E-02 1.52E-01

SC-46 889.25 98.98 2.49E+04 2.42E+04 -1.81E+03 l.23E+04

1120.51 99.90 2.42E+04 -1.44E+04 1.19E+04

@ V-48 983.52 99.98 l.00E+26 1.00E+26 1.00E+26 1.00E+20

@ 1312.10 97.50 1.00E+26 l.00E+26 1.00E+20

CR-51 320.08 9.83 3.96E+14 3.96E+14 5.43E+13 1.96E+14

MN-54 834.83 99.97 8.79E+00 8.79E+00 2.17E+00 4.33E+00

CO-56 846.75 99. 96 1.77E+05 1.12E+05 5.34E+04 8.74E+04

1037.75 14.03 1.38E+06 6.00E+05 6.81E+05

1238.25 67.00 1.51E+05 2.30E+04 7.29E+04

1771.40 15.51 4 .11E+05 -3.26E+04 1.92E+05

2587.48 16.90 l.12E+05 -3.00E+04 3.95E+04

+ CO-57 122.06 * 85.51 1.08E+0l 1.08E+0l 6.78E+0l 5.39E+00

136.48 * 10.60 7.82E+0l 7.26E+0l 3.88E+0l

CO-58 810.76 99.40 1.48E+05 1.48E+05 -1.28E+05 7.29E+04

FE-59 1099.22 56.50 5.58E+08 3.16E+08 -1.22E+08 2.75E+08

1291.56 43.20 3.16E+08 1.43E+07 l.52E+08

+ CO-60 1173.22 * 100.00 1.63E+00 9.45E-01 1.31E+02 8.l0E-01

1332.49 * 100.00 9.45E-01 1.32E+02 4.64E-01

+ ZN-65 1115.52 * 50.75 5.56E+0l 5.56E+0l 2.76E+0l 2.75E+0l

@ GA-67 93.31 35.70 1.00E+26 1.00E+26 1.00E+26 1.00E+20

@ 208.95 2.24 1.00E+26 1.00E+26 1.00E+20

@ 300.22 16.00 1.00E+26 1.00E+26 l.00E+20

SE-75 121.11 16.70 3.06E+03 6.92E+02 2.25E+04 l.52E+03

136.00 59.50 6.92E+02 1.24E+03 3.43E+02

264.65 59.80 9.74E+02 -5.67E+0l 4.82E+02

279.53 25.20 2.33E+03 1.33E+03 1.15E+03

400.65 11. 40 6.07E+03 2.19E+03 3.01E+03

RB-82 776.52 13.00 5.97E+15 5.97E+15 -8.34E+14 2.94E+15

RB-83 520.41 46.00 2.83E+04 2.83E+04 -1.15E+03 1.40E+04

529.64 30.30 4.17E+04 -2.39E+04 2.06E+04

552.65 16.40 7.58E+04 9.53E+03 3.74E+04

KR-85 513.99 0.43 1.16E+02 1.16E+02 7.43E+01 5.72E+0l

SR-85 513.99 99.27 4.10E+05 4.10E+05 2.63E+05 2.02E+05

Y-88 898.02 93.40 2.76E+03 8.47E+02 1.78E+03 1.36E+03

1836.01 99.38 8.47E+02 6.12E+02 3.94E+02

MO-93 263.06 56.72 7.23E-01 2.24E-01 8.80E-02 3.58E-01

684.67 99.68 4.96E-0l -8.70E-02 2.44E-01

1477.11 99.08 2.24E-01 -2.71E-03 1.05E-01

NB-93M 16.57 9.43 1.11E+09 1.11E+09 -1.83E+09 5.47E+08

NB-94 702.63 100.00 4.02E-01 4.02E-01 -9.89E-02 1.98E-01

871.10 100.00 5.30E-01 -1.05E-01 2.61E-01

NB-95 765.79 99.81 5.57E+10 5.57E+10 -3.33E+10 2.74E+10

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Analysis Report for 1803111-01

GAS-1402

Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level

Name (keV) (pCi/grams) (pCilgrams) (pCilgrams) (pCi/grams)

@ NB-95M 235.69 25.00 1.00E+26 1.00E+26 1.00E+26 l.00E+20

ZR-95 724.18 43.70 1.13E+06 9.47E+05 -5.26E+05 5.54E+05

756. 72 55.30 9.47E+05 -3.08E+05 4.66E+05

@ MO-99 181.06 6.20 1.00E+26 1.00E+26 1.00E+26 1.00E+20

@ 739.58 12.80 1.00E+26 1.00E+26 1.00E+20

@ 778.00 4.50 1.00E+26 1.00E+26 l.00E+20

TC-99M 140.51 89.00 2.46E-01 2.46E-01 4.46E-03 1.22E-01

RU-103 497.08 89.00 3.54E+09 3.54E+09 1.48E+08 l.75E+09

RU-106 621.84 9.80 4.58E+0l 4.58E+0l -2.02E+0l 2.26E+0l

AG-108M 433.93 89.90 4.65E-01 4.48E-01 -4.79E-01 2.30E-01

614.37 90.40 4.48E-01 -l.06E-01 2.21E-01

722.95 90.50 4.58E-01 -2.22E-02 2.25E-01

+ CD-109 88.03 * 3. 72 7.45E+0l 7.45E+0l 2.80E+03 3.71E+0l

AG-ll0M 657.75 93.14 4.44E+0l 2.75E+0l -3.12E+02 2.21E+0l

677.61 10.53 l.36E+02 -2.65E+0l 6.70E+0l

706.67 16.46 8.93E+0l -1.06E+0l 4.40E+0l

763.93 21.98 7.22E+01 1. 96E+01 3.56E+0l

884.67 21.98 9.00E+0l -1.77E+0l 4.44E+0l

1384.27 23.94 2.75E+0l -5.88E+00 1.30E+0l

CD-113M 263.70 0.02 l.69E+03 1.69E+03 2.73E+02 8.39E+02

SN-113 255.12 1. 93 3.41E+04 l.43E+03 -8.10E+03 l.69E+04

391.69 64.90 l.43E+03 3.25E+02 7.07E+02

TE-123M 159.00 84.10 4.86E+02 4.86E+02 2.37E+02 2.41E+02

SB-124 602.71 97.87 l.16E+06 l.04E+06 -5.79E+05 5.71E+05

645.85 7.26 1.63E+07 -2.26E+06 8.02E+06

722.78 11.10 l.08E+07 -5.24E+05 5.32E+06

1691.02 49.00 1.04E+06 -2.19E+05 4.82E+05

I-125 35.49 6.49 2.37E+07 2.37E+07 2.92E+07 1.17E+07

SB-125 176.33 6.89 8.l0E+00 3.38E+00 -4.12E+00 4.0lE+00

427.89 29.33 3.38E+00 1.29E-01 1.67E+00

463.38 10.35 1.07E+0l 5,46E+00 5.30E+00

600.56 17.80 5.25E+00 -1.68E+00 2.59E+00

635.90 11. 32 8.51E+00 -1.94E+00 4.19E+00

SB-126 414.70 83.30 4.74E-01 3.96E-01 -2.42E-01 2.34E-01

666.33 99.60 9.07E-01 -2.0lE+0l 4.51E-0l

695.00 99.60 3.96E-01 -l.07E-01 1.95E-01

720.50 53.80 7.60E-01 l.22E-01 3.74E-01

+ SN-126 87.57 * 37.00 1.08E+00 1.08E+00 4.08E+0l 5.40E-01

@ SB-127 473.00 25.00 l.00E+26 1.00E+26 l.00E+26 1.00E+20

@ 685.00 35.70 1.00E+26 l.00E+26 l.00E+20

@ 783.80 14.70 1.00E+26 l.00E+26 1.00E+20

I-129 29.78 57.00 1.70E+00 1.70E+00 -2.14E+00 8.47E-01

33.60 13.20 4.96E+00 1.83E+00 2.46E+00

39.58 7.52 6.06E+00 -2.46E+0l 3.00E+00

@ I-131 284.30 6.05 1.00E+26 l.00E+26 1.00E+26 l.00E+20

@ 364.48 81.20 l.00E+26 1.00E+26 l.00E+20

@ 636.97 7.26 1.00E+26 1.00E+26 l.00E+20

@ 722.89 1. 80 l.00E+26 1.00E+26 1.00E+20

@ TE-132 49. 72 13.10 l.00E+26 1.00E+26 l.00E+26 1.00E+20

@ 228.16 88.00 1.00E+26 l.00E+26 l.00E+20

BA-133 81.00 33.00 1.07E+00 7.58E-01 -4.40E-01 5.33E-01

302.84 17.80 2.33E+00 -1.50E+00 1.15E+00

356.01 60.00 7.58E-01 7.74E-03 3.75E-01

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Analysis Report for 1803111-01

GAS-1402

Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level

Name (keV) (pCi/grams) (pCi/grams) (pCi/grams) (pCi/grams)

@ I-133 529.87 86.30 1.00E+26 1.00E+26 1.00E+26 1.00E+20

@ XE-133 81.00 38.00 1.00E+26 1.00E+26 1.00E+26 1.00E+20

CS-134 563.23 8.38 1.51E+0l 1.31E+00 3.52E+00 7.44E+00

569.32 15.43 8.24E+00 1.60E+00 4.06E+00

604.70 97.60 1.31E+00 -1.25E-01 6.45E-01

795.84 85.40 1.79E+00 5.64E-01 8.80E-01

801.93 8.73 1.76E+0l -8.20E+00 8.66E+00

CS-135 268.24 16.00 2.04E+00 2.04E+00 6.87E-01 1. 0lE+00

@ I-135 1131.51 22.50 1.00E+26 1.00E+26 1.00E+26 1.00E+20

@ 1260.41 28.60 1.00E+26 1.00E+26 1.00E+20

@ 1678.03 9.54 1.00E+26 1.00E+26 1.00E+20

@ CS-136 153.22 7.46 1.00E+26 1.00E+26 1.00E+26 1.00E+20

@ 163.89 4.61 1.00E+26 1.00E+26 1.00E+20

@ 176.55 13.56 1.00E+26 1.00E+26 1.00E+20

@ 27 3. 65 12.66 l.00E+26 1.00E+26 1.00E+20

@ 340.57 48.50 1.00E+26 1.00E+26 1.00E+20

@ 818.50 99.70 1.00E+26 1.00E+26 1.00E+20

@ 1048.07 79.60 1.00E+26 1.00E+26 1.00E+20

@ 1235.34 19.70 1.00E+26 1.00E+26 1.00E+20

+ CS-137 661.65 * 85.12 1.27E+00 1.27E+00 8.31E+0l 6.30E-01

LA-138 788.74 34.00 1.32E+00 2.76E-0l 2.32E-01 6.50E-01

1435.80 66.00 2.76E-01 2.81E-02 1.30E-01

+ CE-139 165.85 * 80.35 2.02E+02 2.02E+02 1.37E+02 9.99E+01

@ BA-140 162.64 6.70 1.00E+26 1.00E+26 1.00E+26 1.00E+20

@ 304.84 4.50 1.00E+26 1.00E+26 1.00E+20

@ 423.70 3.20 1.00E+26 1.00E+26 l.00E+20

@ 437.55 2.00 1.00E+26 1.00E+26 l.00E+20

@ 537.32 25.00 l.00E+26 1.00E+26 1.00E+20

@ LA-140 328.77 20.50 1.00E+26 1.00E+26 1.00E+26 1.00E+20

@ 487.03 45.50 1.00E+26 1.00E+26 1.00E+20

@ 815.85 23.50 1.00E+26 1.00E+26 1.00E+20

@ 1596.49 95.49 1.00E+26 1.00E+26 1.00E+20

CE-141 145.44 48.40 4.47E+ll 4.47E+ll 2. 66E+ll 2. 21E+ll

@ CE-143 57.36 11. 80 1.00E+26 l.00E+26 l.00E+26 1.00E+20

@ 293.26 42.00 1.00E+26 1.00E+26 1.00E+20

@ 664.55 5.20 1.00E+26 1.00E+26 1.00E+20

CE-144 133.54 10.80 4.78E+0l 4.78E+0l -8.05E-01 2.37E+0l

PM-144 476.78 42.00 1.23E+0l 4.74E+00 1.60E+00 6.07E+00

618.01 98.60 4.76E+00 -3.15E-01 2.34E+00

696. 4 9 99.49 4.74E+00 4.24E-01 2.33E+00

PM-145 36.85 21.70 2.57E+00 1.41E+00 1.99E+00 1.27E+00

37.36 39.70 1.41E+00 6.18E-01 6.99E-01

42.30 15.10 3.68E+00 -3.07E+00 1.83E+00

72.40 2.31 l.42E+0l -6.58E+00 7.03E+00

PM-146 453.90 39.94 1.73E+00 1.73E+00 8.19E-01 8.55E-01

735.90 14.01 4.77E+00 1.90E+00 2.35E+00

747.13 13.10 5.17E+00 2.80E+00 2.55E+00

@ ND-147 91.11 28.90 1.00E+26 1.00E+26 1.00E+26 1.00E+20

@ 531.02 13.10 1.00E+26 1.00E+26 1.00E+20

@ PM-149 285.90 3.10 1.00E+26 1.00E+26 1.00E+26 1.00E+20

EU-152 121.78 20.50 1.68E+00 1.55E+00 1.23E+0l 8.33E-01

244.69 5.40 6.21E+00 3.76E+00 3.07E+00

344.27 19.13 2.16E+00 -1.18E+00 1.07E+00

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Analysis Report for 1803111-01

GAS-1402

Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level

Name (keV) (pCilgrams) (pCilgrams) (pCi/grams) (pCilgrams)

EU-152 778.89 9.10 5.93E+00 l.55E+00 9.48E-01 2.92E+00

964.01 10.40 7.03E+00 l.15E+00 3.47E+00

1085.78 7.22 9. 71E+00 -6.52E-01 4.78E+00

1112.02 9.60 7.25E+00 3.26E-01 3.57E+00

1407.95 14.94 l.55E+00 l.88E-01 7.31E-01

GD-153 97.43 31.30 2.70E+0l 2.70E+0l 6.84E-01 l.34E+0l

103.18 22.20 3.86E+0l 5.77E+00 l.91E+0l

EU-154 123.07 40.50 9.35E-01 9.35E-01 6.57E+00 4.64E-01

723.30 19.70 2.73E+00 -1.32E-01 1.34E+00

873.19 11. 50 6.15E+00 -1.12E+00 3.03E+00

996. 32 10.30 7.40E+00 -2.76E-01 3.65E+00

1004.76 17.90 4.28E+00 -4.28E-01 2. llE+00

1274.45 35.50 9.84E-01 -6.86E-03 4.73E-01

EU-155 86.50 30.90 2.91E+00 1.65E+00 7.66E+0l 1.45E+00

105.30 20.70 1.65E+00 7.67E-02 8.20E-01

@ EU-156 811. 77 10.40 1.00E+26 1.00E+26 l.00E+26 l.00E+20

@ 1153.47 7.20 l.00E+26 1.00E+26 l.00E+20

@ 1230.71 8.90 1.00E+26 l.00E+26 l.00E+20

HO-166M 184.41 72.60 3.45E-01 3.45E-01 -1.02E-01 l.71E-01

280.45 29.60 1.llE+00 4.66E-01 5.52E-01

410.94 11.10 3.60E+00 7.50E-01 1.78E+00

711.69 54.10 7.62E-01 -1.97E-0l 3.75E-01

TM-171 66. 72 0.14 9.01E+02 9.01E+02 2.77E+03 4.48E+02

HF-172 67.35 5.31 2.31E+0l 7.32E+00 1.07E+0l 1.15E+0l

125.82 11. 30 7.32E+00 -1.42E+00 3.63E+00

@ LU-172 181.53 20.60 l.00E+26 l.00E+26 1.00E+26 l.00E+20

@ 900. 72 29.81 1.00E+26 l.00E+26 l.00E+20

@ 1093.66 62.50 l.00E+26 l.00E+26 l.00E+20

LU-173 100. 72 5.24 2.39E+0l 9.26E+00 7.97E+00 l.18E+0l

272.11 21. 20 9.26E+00 1.94E+00 4.59E+00

HF-17 5 343.40 84.00 l.50E+05 l.50E+05 -8. 18E+04 7.44E+04

LU-176 88.34 13.30 4.08E+00 3.03E-01 l.09E+02 2.03E+00

201.83 86.00 3.03E-01 -2.04E-02 1.50E-01

306.78 94.00 3.55E-01 -1.35E-01 1.76E-01

HF-181 133.02 41.70 8.03E+08 7.76E+08 -9.45E+07 3.98E+08

345.85 17.20 3.18E+09 9.27E+08 l.57E+09

482.03 82.80 7.76E+08 1.19E+08 3.84E+08

TA-182 67.75 41. 20 2.02E+03 2.02E+03 9.39E+02 1.00E+03

1121.30 34.90 3.91E+03 -1.74E+03 l.92E+03

1189.05 16.23 6.44E+03 -7.74E+02 3.15E+03

1221.41 26.98 3.09E+03 -9.39E+02 1.50E+03

1231.02 11. 44 6.85E+03 -1.37E+03 3.32E+03

IR-192 308.46 29.68 2.09E+05 1. 72E+05 1.73E+05 l.04E+05

468.07 48.10 1.72E+05 5.68E+03 8.54E+04

HG-203 279.19 77. 30 9.67E+07 9.67E+07 -1.68E+07 4.79E+07

TL-204 374.74 94.11 7.42E-01 7.42E-01 8.04E-02 3.67E-01

899.15 99.16 1.l0E+00 9.53E-02 5.42E-01

911. 74 91.10 1.24E+00 5.73E-01 6.13E-01

BI-207 569.67 97. 72 4.23E-01 4.23E-01 4.53E-03 2.09E-01

1063.62 74.90 8.13E-01 -4.12E-01 4.00E-01

TL-208 583.14 30.22 1.31E+00 4.40E-01 1.07E+00 6.47E-01

860.37 4.48 1.17E+0l 1.53E+00 5.76E+00

2614.66 35.85 4.40E-01 4.05E-01 1.97E-01

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Analysis Report for 1803111-01

GAS-1402

Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level

Name (keV) (pCi!grams) (pCi!grams) (pCi!grams) (pCi!grams)

BI-210M 262.00 45.00 7.27E-01 7.27E-01 6.37E-02 3.60E-01

300.00 23.00 1.45E+00 6.83E-01 7.20E-01

PB-210 46.50 4.25 1.46E+0l 1.46E+0l -9.55E+0l 7.28E+00

PB-211 404.84 2.90 1.33E+0l 1.33E+0l -7.04E+00 6.58E+00

831.96 2.90 1.72E+0l 1.15E+0l 8.48E+00

BI-212 727.17 11. 80 3.54E+00 3.54E+00 4.65E-01 1.74E+00

1620.62 2.75 6.12E+00 -1.36E+00 2.84E+00

+ PB-212 238.63 * 44.60 6.58E-01 6.58E-01 6.02E-01 3.26E-01

300.09 3.41 9.80E+00 4.61E+00 4.85E+00

BI-214 609.31 46.30 8.58E-01 8.58E-01 1.03E-02 4.23E-01

1120.29 15.10 3.62E+00 -2.15E+00 1.78E+00

1764.49 15.80 1.23E+00 5.83E-01 5.75E-01

2204.22 4.98 3.78E+00 -1.0lE+00 1.74E+00

+ PB-214 295.21 19.19 1.74E+00 l.12E+00 5.19E-01 8.61E-01

351.92 * 37.19 1.12E+00 6.06E-01 5.57E-01

RN-219 401.80 6.50 5.94E+00 5.94E+00 -1.97E+00 2.94E+00

RA-223 323.87 3.88 8.76E+00 8.76E+00 -4.12E+00 4.33E+00

RA-224 240.98 3.95 7.14E+00 7.14E+00 -1.29E+00 3.53E+00

@ RA-225 40.00 31.00 1.00E+26 1.00E+26 1.00E+26 1.00E+20

RA-226 186.21 3.28 7.80E+00 7.80E+00 1.33E+00 3.86E+00

TH-227 50.10 8.40 7. 96E+00 2.46E+00 3.43E+0l 3. 96E+00

236.00 11. 50 2.46E+00 -8.66E-02 l.22E+00

256.20 6.30 5.14E+00 -3.44E-01 2.55E+00

AC-228 338.32 11. 40 2.99E+00 2.14E+00 -1.37E+00 1.48E+00

911.07 27. 70 2.14E+00 1.16E+00 1.06E+00

969.11 16.60 3.55E+00 -2.31E-01 1.75E+00

TH-230 48.43 16.90 3.76E+00 3.76E+00 1.41E+0l 1.87E+00

62.85 4.60 1.25E+01 -6.15E+02 6.23E+00

67.67 0.37 8.89E+0l 4.13E+01 4.42E+0l

PA-231 283.67 1. 60 2.05E+0l 1.43E+0l 1.87E+00 1.0lE+0l

302.67 2.30 1.43E+0l -9.16E+00 7.07E+00

TH-231 25.64 14.70 2.02E+0l 4.92E+00 -2.57E+02 1.0lE+0l

84.21 6.40 4.92E+00 -2.50E+02 2.44E+00

PA-233 311.98 38.60 2.36E+14 2.36E+l4 8.14E+13 1.17E+14

PA-234 131.20 20.40 1.06E+00 1.06E+00 -8.62E-02 5.27E-01

733.99 8.80 4.87E+00 -2.41E-01 2.40E+00

946.00 12.00 5.26E+00 -7.02E-01 2.60E+00

PA-234M 1001.03 0.92 6.28E+0l 6.28E+0l -5.20E-01 3.09E+0l

TH-234 63.29 3.80 1.0lE+0l 1.0lE+0l -5.92E+02 5.04E+00

U-235 143.76 10.50 2.12E+00 2.12E+00 2.64E-01 1.05E+00

163.35 4.70 4.90E+00 -1.42E+00 2.43E+00

205.31 4.70 5.55E+00 -2.91E+00 2.75E+00

NP-237 86.50 12.60 4.36E+00 4.36E+00 1.15E+02 2.17E+00

@ NP-239 106.10 22.70 1.00E+26 1.00E+26 1.00E+26 1.00E+20

@ 228.18 10.70 1.00E+26 1.00E+26 1.00E+20

@ 277.60 14.10 1.00E+26 1.00E+26 1.00E+20

+ AM-241 59.54 * 35.90 3.18E+00 3.18E+00 1.99E+02 1.59E+00

AM-243 7 4. 67 66.00 4.33E-01 4.33E-01 2.77E-01 2.15E-01

CM-243 209.75 3.29 8.89E+00 2.55E+00 -3.05E+00 4.40E+00

228.14 10.60 2.94E+00 2.llE+00 1.45E+00

277.60 14.00 2.55E+00 -3.99E-01 1.26E+00

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0172

Analysis Report for 1803111-01

+

>

GAS-1402

= Nuclide identified during the nuclide identification

= Energy line found in the spectrum

= MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

No Action Level results available for reporting purposes.

4/17/2018 6:13:23AM

DATA REVIEW COMMENTS REPORT

Creation Date Comment

No Data Review Comments Entered.

Page 25 of 25

User

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*******************************************************

***** S P E C T R A L D A T A R E P O R T *****

*******************************************************

Sample Title: GAS-1402

Elapsed Live time: 1800 Elapsed Real Time: 1822

Channell------1-------1-------1-------1-------1-------I-------I-------I

1: 0 0 0 0 0 0 0 0

9: 0 0 0 0 0 0 0 0

17: 2 129 1676 1991 7385 33446 23528 5276

25: 11482 7571 2613 1968 1291 1043 1246 1972

33: 1548 835 7 68 1005 1177 961 987 1085

41: 1176 1384 1580 1758 1900 2036 2433 3004

49: 4025 4876 4913 4545 4518 4624 4840 5387

57: 5671 692 6 22551 55117 15932 2034 1735 2043

65: 2513 2621 1713 1344 1390 1436 1302 1291

73: 1311 1357 1437 1333 1443 1351 1413 1360

81: 1340 1354 1393 1431 1567 1510 2830 11531

89: 9385 1618 8 63 964 1105 1238 960 801

97: 688 775 755 738 760 756 803 770

105: 732 753 747 7 68 764 701 740 733

113: 795 786 773 800 774 777 774 855

121: 905 2207 1910 856 786 786 784 733

129: 827 748 742 704 732 724 700 854

137: 956 803 699 67 6 757 718 696 784

145: 693 710 714 708 685 667 691 68 6

153: 692 693 710 645 68 4 694 687 723

161: 654 675 627 676 707 754 663 666

169: 647 653 662 650 669 640 634 654

177: 649 611 623 673 658 671 721 679

185: 685 721 781 756 755 778 723 750

193: 725 736 727 721 727 708 747 688

201: 677 720 736 701 718 672 697 674

209: 666 7 68 717 747 750 786 759 772

217: 794 740 7 61 794 736 763 771 727

225: 711 742 718 7 60 723 708 694 64 6

233: 652 668 685 681 678 717 7 92 666

241: 632 607 625 682 593 650 661 597

249: 610 654 606 577 569 597 573 578

257: 555 587 579 588 587 592 571 568

265: 532 572 567 546 550 552 544 547

273: 548 517 562 526 519 525 547 550

281: 504 524 566 4 97 472 541 519 485

289: 491 510 479 505 506 465 531 500

297: 513 527 501 489 482 494 484 457

305: 451 470 478 502 508 504 516 488

313: 484 454 511 473 477 469 471 491

321: 484 466 469 472 435 4 69 442 503

329: 457 441 447 478 440 444 486 443

337: 443 485 451 411 430 395 453 439

345: 448 423 469 482 472 470 4 67 515

353: 519 441 439 458 406 444 4 61 444

361: 415 446 443 445 470 453 429 435

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369: 416 416 438 436 445 444 425 416

Sample Title: GAS-1402

Channell------l-------l-------l-------l-------l-------1-------1-------1

377: 435 418 420 435 435 454 433 451

385: 420 419 472 456 429 458 441 500

393: 426 430 437 412 423 471 4 67 447

401: 454 429 433 396 421 453 443 438

409: 443 456 477 443 431 455 432 440

417: 430 409 431 456 441 448 429 459

425: 464 405 427 445 471 483 417 458

433: 427 449 427 447 448 480 475 433

441: 440 466 465 437 4 68 431 450 489

449: 4 62 479 423 485 476 477 477 493

457: 511 403 497 481 484 480 516 4 97

465: 489 478 504 455 465 493 461 4 64

473: 445 493 422 451 432 407 420 375

481: 403 402 354 359 364 355 339 403

489: 363 356 340 353 360 322 330 335

497: 336 365 326 334 312 322 300 340

505: 317 344 344 319 307 327 388 366

513: 287 2 95 287 290 331 337 299 319

521: 293 272 285 263 287 311 290 298

529: 295 271 275 266 2 68 315 278 266

537: 306 276 290 254 292 256 271 280

545: 283 288 304 252 259 257 237 274

553: 266 272 250 219 253 239 249 264

561: 239 244 242 261 266 27 6 247 260

569: 273 245 248 232 255 222 251 226

577: 236 235 256 274 233 252 272 276

585: 245 252 227 225 257 244 222 220

593: 216 256 250 246 240 242 255 216

601: 230 205 218 256 239 238 227 248

609: 259 232 231 248 226 243 229 244

617: 242 245 241 232 210 239 237 221

625: 219 241 235 222 221 226 231 234

633: 224 216 230 197 204 245 258 238

641: 229 219 223 229 206 233 217 209

649: 243 235 222 230 252 218 240 231

657: 259 326 409 1696 9430 14484 4 678 637

665: 406 505 586 565 319 206 205 203

67 3: 206 201 207 204 209 191 183 214

681: 204 218 200 182 223 214 174 176

689: 196 200 192 176 173 207 199 200

697: 201 189 202 200 202 197 205 202

705: 178 192 205 211 203 199 186 218

713: 197 212 197 192 225 195 174 224

721: 17 6 187 186 204 174 193 212 187

72 9: 221 216 193 220 222 231 199 198

737: 197 207 200 206 17 6 167 222 206

745: 210 216 235 186 194 212 199 190

753: 211 201 201 201 216 177 213 199

761: 240 192 193 195 189 202 221 190

7 69: 193 206 214 194 210 213 185 226

777: 190 215 204 203 225 203 215 205

785: 182 201 183 197 207 216 208 215

793: 228 180 202 220 214 231 226 193

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801: 211 208 232 204 226 231 228 192

Sample Title: GAS-1402

Channell------l-------l-------l-------1-------1-------1-------I-------I

809: 203 218 218 196 236 193 237 225

817: 222 249 233 252 235 258 235 234

825: 225 224 220 198 237 211 213 217

833: 257 259 225 214 219 225 233 233

841: 233 222 247 247 255 220 260 223

849: 225 266 204 263 2 69 245 233 246

857: 239 241 228 246 255 212 269 252

865: 221 242 226 241 250 266 243 245

873: 231 223 254 263 252 260 243 266

881: 223 251 243 264 265 246 272 251

889: 269 246 272 255 246 270 250 269

8 97: 257 293 2 60 286 270 227 262 270

905: 227 271 243 283 283 2 97 301 279

913: 265 275 270 279 263 273 2 61 305

921: 273 283 283 266 308 281 257 290

929: 284 287 310 289 263 319 340 303

937: 294 282 308 300 311 273 307 274

945: 293 351 275 296 326 334 304 296

953: 347 299 332 315 323 290 269 311

961: 296 304 271 256 288 256 251 255

969: 256 254 248 257 246 241 229 244

977: 198 226 217 194 245 229 232 235

985: 251 223 246 223 239 218 249 243

993: 238 228 231 229 226 226 243 227

1001: 218 250 231 220 250 217 228 219

1009: 245 232 233 233 216 245 215 212

1017: 233 232 224 227 234 219 197 211

1025: 213 194 200 207 209 184 197 208

1033: 185 201 211 230 218 212 17 6 216

1041: 187 211 201 184 205 195 223 203

1049: 201 199 204 203 203 192 203 208

1057: 191 195 226 196 210 200 213 208

1065: 203 172 215 215 198 183 214 216

1073: 238 221 233 185 203 203 184 216

1081: 214 203 218 201 206 210 194 221

1089: 205 205 202 215 199 233 190 211

1097: 191 225 184 195 223 226 235 195

1105: 179 231 208 196 187 207 191 188

1113: 187 199 222 203 199 164 148 182

1121: 196 172 141 163 170 148 146 119

1129: 137 142 147 132 123 127 118 138

1137: 136 111 112 123 129 116 121 122

1145: 140 112 127 105 120 134 93 107

1153: 133 127 110 135 95 129 112 109

1161: 111 130 97 133 124 96 123 133

1169: 17 6 242 822 4614 10329 7021 1405 294

1177: 300 411 436 250 114 99 82 103

1185: 92 91 102 88 69 82 83 101

1193: 84 85 78 61 70 69 70 62

1201: 73 67 69 69 67 56 52 72

1209: 53 78 60 48 56 55 67 55

1217: 65 57 43 64 50 47 54 57

1225: 58 52 53 55 45 45 35 47

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1233: 45 50 41 50 43 35 38 42

Sample Title: GAS-1402

Channell------l-------l-------l-------l-------1-------1-------1-------I

1241: 41 29 39 45 37 35 31 32

1249: 30 46 41 28 32 41 39 31

1257: 36 31 23 37 32 35 20 29

1265: 26 22 40 32 32 31 32 29

1273: 27 44 28 30 30 23 40 34

1281: 28 27 25 24 26 37 29 27

1289: 33 34 22 27 26 33 25 25

1297: 30 24 32 30 26 27 27 27

1305: 25 43 31 30 31 19 29 33

1313: 26 22 27 27 44 24 34 28

1321: 30 26 37 27 32 40 45 108

1329: 139 535 3104 8454 7384 2062 276 197

1337: 308 343 189 56 23 15 14 12

1345: 7 20 17 23 15 18 13 19

1353: 17 12 17 17 15 14 18 12

1361: 8 11 13 15 14 15 6 12

1369: 16 10 13 17 12 11 10 15

1377: 15 15 12 6 15 16 14 12

1385: 9 16 6 24 10 11 12 15

1393: 10 15 14 18 6 14 23 16

1401: 14 11 12 17 15 20 9 11

1409: 9 16 13 15 13 7 18 11

1417: 15 14 19 14 9 12 6 15

1425: 15 8 14 12 10 10 14 9

1433: 13 11 7 14 15 14 8 13

1441: 10 13 6 8 8 15 11 5

1449: 9 8 14 16 15 10 7 9

1457: 13 14 14 17 19 12 12 14

1465: 8 11 10 10 13 8 17 10

1473: 14 15 10 10 13 8 8 11

1481: 10 10 16 11 10 8 13 11

148 9: 7 5 9 3 5 7 6 11

1497: 12 10 11 11 11 8 7 8

1505: 7 11 13 10 15 13 11 13

1513: 5 10 15 2 8 11 11 13

1521: 11 12 15 10 5 5 11 10

1529: 11 12 8 4 10 8 2 11

1537: 7 11 8 10 8 10 7 10

1545: 10 4 5 15 13 12 11 6

1553: 15 12 8 12 14 7 17 5

1561: 5 9 13 10 8 10 17 8

1569: 7 4 10 13 9 6 5 15

1577: 11 6 10 5 9 8 8 9

1585: 8 11 14 10 15 15 9 12

1593: 12 7 6 9 17 8 6 5

1601: 6 11 8 4 13 8 11 7

1609: 11 11 12 8 14 12 9 10

1617: 8 8 8 2 13 10 9 10

1625: 9 9 11 5 8 12 17 9

1633: 7 8 6 11 10 10 5 5

1641: 7 7 3 3 13 9 6 10

1649: 9 6 6 6 9 7 5 9

1657: 8 10 7 7 10 11 4 2

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1665: 7 8 8 4 7 5 6 13

Sample Title: GAS-1402

Channel[------[-------[-------[-------[-------[-------[-------[-------[

1673: 10 9 8 6 9 9 7 5

1681: 12 14 10 12 7 11 6 8

1689: 9 10 9 9 6 10 9 2

1697: 7 6 9 10 7 4 9 10

1705: 12 7 5 7 8 11 5 7

1713: 5 10 5 9 6 5 7 10

1721: 8 4 10 13 7 7 2 10

1729: 12 6 10 10 7 7 3 6

1737: 5 6 8 13 7 5 6 8

1745: 7 14 9 4 10 8 10 6

1753: 9 5 8 8 9 8 5 6

1761: 10 12 12 14 7 8 6 7

1769: 9 9 6 14 8 10 12 11

1777: 8 7 7 9 10 10 6 8

1785: 5 9 8 7 6 8 10 5

1793: 8 5 7 6 5 7 10 7

1801: 7 4 11 11 9 11 8 6

1809: 9 5 4 7 4 9 5 9

1817: 11 7 7 5 8 8 6 7

1825: 10 12 9 6 8 4 4 7

1833: 8 8 11 14 5 7 6 4

1841: 8 4 9 5 7 3 8 8

1849: 7 8 0 8 7 3 5 4

1857: 4 5 4 8 5 2 8 8

1865: 10 7 6 6 7 7 5 11

1873: 7 6 9 8 5 5 8 7

1881: 4 7 4 3 6 3 3 4

1889: 4 5 6 9 6 9 4 6

1897: 3 5 6 4 7 8 9 6

1905: 7 3 7 6 4 10 12 4

1913: 7 8 7 7 6 4 7 9

1921: 6 3 8 5 7 4 3 7

1929: 12 4 7 8 6 4 2 11

1937: 6 4 3 7 3 4 3 8

1945: 4 4 8 9 7 7 10 4

1953: 6 5 13 5 8 5 7 7

1961: 8 4 5 5 9 7 8 8

1969: 5 5 2 6 6 7 3 8

1977: 9 6 9 3 6 10 4 3

1985: 8 9 6 8 7 5 5 5

1993: 3 8 10 4 6 8 4 4

2001: 7 7 5 14 7 4 3 6

2009: 4 11 7 7 2 2 5 8

2017: 7 8 5 12 7 10 3 9

2025: 8 7 9 5 5 6 6 9

2033: 6 4 7 8 3 4 9 6

2041: 4 7 9 0 6 2 3 9

2049: 2 11 4 4 6 6 8 5

2057: 7 5 4 7 3 3 5 6

2065: 7 6 4 5 5 8 5 3

2073: 3 4 5 5 8 7 8 6

2081: 5 2 2 4 3 5 8 4

2089: 5 7 3 6 6 5 3 4

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Channel Data Report 4/17/2018 6:13:44 AM Page 6

2097: 4 6 5 3 6 8 9 6

Sample Title: GAS-1402

Channell------l-------1-------1-------1-------l-------l-------1-------I

2105: 7 2 5 7 3 5 9 6

2113: 10 4 8 4 3 4 6 5

2121: 5 5 3 5 5 5 2 4

2129: 10 2 7 5 5 5 8 4

2137: 5 4 3 10 9 7 4 5

2145: 4 8 9 4 3 1 7 6

2153: 1 4 4 8 1 8 6 2

2161: 3 7 2 2 6 6 3 4

2169: 10 6 3 6 8 4 6 9

2177: 3 4 7 3 2 4 6 3

2185: 6 2 6 7 6 4 3 7

2193: 2 14 7 5 8 4 3 6

2201: 6 4 3 3 10 6 6 7

2209: 6 5 9 5 2 6 9 6

2217: 3 4 4 8 1 4 4 5

2225: 7 5 6 1 2 3 8 6

2233: 6 7 11 4 8 9 5 6

2241: 6 7 2 5 6 4 5 3

2249: 6 2 2 6 3 5 12 5

2257: 6 7 9 8 3 3 5 6

2265: 5 5 6 3 3 4 8 11

2273: 8 6 3 6 1 7 5 8

2281: 7 2 7 4 7 4 5 7

2289: 7 5 4 7 8 4 3 5

2297: 2 3 8 2 3 2 1 2

2305: 6 8 0 5 2 4 1 4

2313: 1 2 7 4 2 5 3 6

2321: 7 4 0 5 3 2 6 0

2329: 2 2 1 2 3 3 3 2

2337: 4 3 7 5 3 2 2 2

2345: 2 2 0 2 3 2 3 6

2353: 0 3 4 1 1 2 3 5

2361: 2 1 3 4 6 1 3 1

2369: 2 4 2 1 2 6 2 0

2377: 2 2 1 4 1 5 3 0

2385: 3 0 3 2 1 2 1 0

2393: 0 1 1 4 0 0 2 2

2401: 0 1 0 3 0 0 2 0

2409: 2 2 1 0 0 1 2 1

2417: 2 0 2 0 1 2 2 2

2425: 0 0 3 0 0 0 1 1

2433: 0 0 1 1 1 0 0 0

2441: 0 0 2 3 2 2 1 0

2449: 1 2 0 2 3 1 2 2

2457: 0 2 1 0 2 0 1 1

2465: 0 1 0 0 1 1 2 0

2473: 0 0 1 1 0 1 0 0

24 81: 2 1 0 0 0 0 1 0

2489: 3 0 1 0 2 1 1 0

2497: 3 2 0 1 6 10 48 85

2505: 109 58 21 6 2 5 4 3

2513: 1 0 1 0 0 1 0 1

2521: 0 0 1 0 0 0 1 0

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Channel Data Report 4/17/2018 6:13:44 AM Page 7

2529: 0 1 0 1 0 0 0 0

Sample Title: GAS-1402

Channell------l-------l-------l-------1-------1-------1-------I-------I

2537: 0 0 0 0 1 0 0 0

2545: 0 0 0 0 0 1 1 0

2553: 1 0 0 0 1 1 0 0

2561: 0 1 0 0 1 0 0 0

2569: 1 0 0 0 0 0 0 1

2577: 0 0 1 0 0 1 0 0

2585: 0 0 0 0 0 2 0 1

2593: 0 0 1 0 0 0 0 0

2601: 0 0 1 0 0 0 0 1

2609: 0 0 2 4 12 4 2 1

2617: 0 1 0 0 0 0 0 0

2625: 0 0 0 0 0 0 0 0

2633: 0 0 0 1 0 0 1 0

2641: 0 1 1 0 0 0 0 0

2649: 0 0 0 0 1 1 0 0

2657: 0 0 0 0 0 0 0 0

2665: 0 1 0 0 0 0 0 0

2673: 1 0 0 0 0 0 0 0

2681: 0 0 0 1 0 0 0 1

2689: 0 0 0 0 0 0 0 0

2697: 1 0 0 0 1 0 0 0

2705: 0 0 0 0 0 1 0 0

2713: 0 0 0 0 1 0 0 0

2721: 0 0 2 0 0 0 0 0

2729: 0 0 0 1 0 0 0 0

2737: 0 2 0 0 0 0 0 0

2745: 0 0 0 0 1 0 1 1

2753: 0 0 1 0 0 0 0 0

2761: 0 0 0 0 0 0 0 0

2769: 0 0 0 0 0 0 0 0

2777: 0 0 0 0 0 0 0 0

2785: 0 0 0 0 0 0 0 0

2793: 1 0 0 0 0 0 0 0

2801: 0 0 0 0 1 0 0 0

2809: 0 1 0 0 0 0 0 0

2817: 0 0 0 0 0 0 0 0

2825: 0 0 0 0 0 0 1 0

2833: 0 1 0 0 0 0 0 0

2841: 1 0 0 0 0 0 0 0

2849: 0 1 0 1 0 0 0 0

2857: 0 0 0 0 0 0 0 0

2865: 0 0 0 0 0 0 0 0

2873: 0 0 0 0 0 0 0 1

2881: 0 0 0 0 0 0 0 0

2889: 0 0 0 0 0 0 0 0

2897: 0 0 0 1 0 0 1 0

2905: 0 0 0 0 0 0 0 0

2913: 0 0 0 0 0 0 0 0

2921: 2 0 2 1 0 0 0 1

2929: 0 0 0 0 0 0 0 0

2937: 0 0 0 0 0 0 0 1

2945: 1 0 0 0 0 1 0 0

2953: 0 0 1 0 0 1 0 0

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Channel Data Report 4/17/2018 6:13:44 AM Page 8

2961: 0 0 1 0 0 0 0 0

Sample Title: GAS-1402

Channell------l-------l-------1-------1-------1-------I-------I-------I

2969: 2 0 0 0 0 0 0 0

2977: 0 0 0 0 0 0 0 0

2985: 0 0 0 0 0 0 0 0

2993: 0 0 2 0 0 0 0 1

3001: 0 0 1 0 0 0 0 1

3009: 0 1 0 0 0 0 0 0

3017: 0 0 0 0 0 0 0 1

3025: 0 0 0 0 0 0 0 0

3033: 0 0 0 0 0 0 0 0

3041: 0 0 0 1 1 0 0 0

3049: 1 0 0 0 2 1 0 1

3057: 0 0 0 0 0 0 0 0

3065: 0 0 0 1 0 0 0 0

3073: 0 0 0 0 0 0 1 0

3081: 0 0 0 0 0 0 2 0

3089: 0 0 0 0 0 0 0 0

3097: 0 0 0 1 1 0 1 0

3105: 0 1 0 0 0 0 0 0

3113: 0 1 0 0 0 0 0 0

3121: 0 0 0 0 0 2 0 0

3129: 1 0 0 0 0 0 1 0

3137: 0 0 0 0 0 0 0 1

3145: 0 0 0 0 0 0 0 0

3153: 1 1 1 0 0 0 0 0

3161: 0 0 0 0 0 0 0 0

3169: 0 0 0 0 0 0 0 0

3177: 1 0 0 0 0 0 0 1

3185: 0 0 0 0 0 0 0 0

3193: 0 0 0 0 0 2 0 0

3201: 1 0 0 0 0 0 0 0

3209: 0 0 0 0 0 0 0 0

3217: 0 0 0 0 0 0 1 0

3225: 0 0 0 0 0 0 1 0

3233: 0 1 0 0 0 0 0 0

3241: 0 0 0 0 0 0 0 0

3249: 0 0 0 0 0 0 0 0

3257: 0 0 0 0 1 0 0 0

3265: 0 0 0 1 0 0 0 0

3273: 0 0 0 0 0 0 0 0

3281: 0 0 0 0 1 0 0 0

3289: 0 0 0 0 0 0 0 0

3297: 0 0 1 0 0 0 0 0

3305: 0 0 0 0 0 0 0 0

3313: 0 0 0 0 0 0 0 0

3321: 0 0 0 0 0 0 0 0

3329: 0 0 0 0 0 0 0 0

3337: 0 0 0 0 0 0 0 1

3345: 0 0 0 0 0 0 0 0

3353: 0 1 0 0 0 0 0 0

3361: 0 0 0 0 0 0 0 0

3369: 1 0 0 0 0 0 0 0

3377: 0 0 0 0 0 0 0 0

3385: 0 0 0 0 1 0 0 1

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Channel Data Report 4/17/2018 6:13:44 AM Page 9

3393: 0 0 0 0 0 0 0 0

Sample Title: GAS-1402

Channell------l-------l-------1-------1-------1-------I-------I-------I

3401: 0 0 0 0 1 0 0 0

3409: 0 0 0 0 0 0 0 0

3417: 0 0 0 0 0 0 0 0

3425: 0 0 0 0 0 0 0 0

3433: 0 0 0 0 0 0 0 0

3441: 0 0 0 0 0 0 0 0

3449: 0 0 0 0 0 0 0 0

3457: 0 0 0 0 0 0 0 0

3465: 0 0 0 0 0 0 0 0

3473: 0 0 0 0 0 0 0 0

3481: 0 1 0 0 0 0 0 0

3489: 0 1 1 1 0 0 0 0

3497: 0 0 0 0 0 0 0 0

3505: 0 0 0 1 0 0 0 0

3513: 0 0 0 0 0 0 0 0

3521: 0 0 0 0 0 1 0 0

3529: 0 0 0 0 0 0 0 0

3537: 0 0 0 0 1 0 0 0

3545: 0 0 1 0 0 0 0 0

3553: 0 0 0 0 0 0 0 1

3561: 0 0 0 0 0 0 0 0

3569: 0 0 0 0 0 0 1 0

3577: 1 0 0 0 1 0 0 0

3585: 0 1 0 0 0 0 0 0

3593: 0 0 0 1 0 0 0 0

3601: 0 0 0 0 0 0 0 0

3609: 0 0 0 0 0 0 0 0

3617: 0 0 0 0 0 0 0 0

3625: 0 0 0 0 0 0 0 0

3633: 0 0 0 0 0 0 0 0

3641: 0 0 0 0 0 0 0 0

3649: 0 1 0 0 0 0 0 0

3657: 0 0 0 0 1 0 0 0

3665: 0 0 0 0 0 0 0 0

3673: 0 0 0 0 0 0 0 1

3681: 0 0 0 0 0 0 0 0

3689: 0 0 0 0 0 0 0 0

3697: 0 0 0 1 0 0 0 0

3705: 0 0 0 1 0 1 0 0

3713: 2 0 0 0 0 0 0 0

3721: 0 0 0 1 0 1 0 0

37 2 9: 0 0 0 0 0 0 0 0

3737: 1 0 0 0 0 0 0 0

3745: 0 1 0 0 0 0 0 0

3753: 1 ' 0 0 0 0 0 0 0

3761: 0 0 0 0 0 0 0 1

37 69: 0 0 0 0 0 0 0 0

3777: 0 0 0 0 0 0 0 0

3785: 0 0 1 0 0 0 0 0

3793: 0 0 0 0 0 0 1 0

3801: 0 0 0 0 0 0 1 0

3809: 0 1 0 0 0 0 0 0

3817: 0 0 0 0 0 0 0 0

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Channel Data Report 4/17/2018 6:13:44 AM Page 10

3825: 0 0 1 1 0 0 0 0

Sample Title: GAS-1402

Channell------l-------1-------l-------1-------1-------l-------1-------I

3833: 0 0 0 0 0 0 0 1

3841: 0 0 0 0 0 0 0 0

3849: 0 0 0 1 0 0 0 0

3857: 0 1 0 0 0 0 0 0

3865: 0 0 1 0 0 0 0 0

3873: 0 0 0 0 0 0 0 0

3881: 0 0 0 0 0 0 0 0

3889: 0 0 0 0 0 0 0 0

3897: 0 0 0 1 0 1 0 0

3905: 0 0 0 0 0 0 0 0

3913: 1 0 0 0 0 0 0 0

3921: 0 0 0 1 1 1 0 0

3929: 0 0 0 0 1 0 0 0

3937: 0 0 0 0 0 0 0 0

3945: 0 0 0 0 0 0 0 0

3953: 1 0 0 0 0 0 0 0

3961: 0 0 0 0 0 0 0 0

3969: 0 0 0 0 0 0 0 0

3977: 0 0 0 0 0 0 1 0

3985: 0 0 0 1 0 0 0 0

3993: 0 0 1 0 0 0 1 0

4001: 0 0 0 0 0 0 0 0

4009: 0 0 0 0 0 0 0 0

4017: 0 0 0 0 0 0 0 0

4025: 0 0 0 0 0 0 0 0

4033: 0 0 0 0 0 0 0 0

4041: 0 0 0 0 0 0 0 0

4049: 0 0 0 0 0 0 0 0

4057: 0 0 0 0 1 0 0 0

4065: 0 0 0 0 0 1 0 0

4073: 0 0 0 0 0 1 0 0

4081: 0 0 0 0 0 0 0 0

4089: 0 0 0 0 0 0 0 0

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0183

105

104

~ 103 ro u V)

en 0 ,­

I V)

-1-' C ::::s 0 u

102

101

_. .._,_

' ;,;

,..__

~ 0 u

cr, ~ ~ _. _. ~ ' ' w "' u ~

,..__ _. ' V,

u ~ 0 u ~

0 u

0000064638.CNF Live Time :1800.000 sec Real Time :1821.900 sec Start: 1: 0.S(kev) Stop : 4096:4096.9(kev) Acq. Start :Tue Apr 17 05:42:50 2018

10°~.l.!...l...J__..l....__.l~...L..lLl_L~~.li__J~r~iL4.~L1-~µ_JL_~~Ul__J_L+__J_L_L_-i-J

500 1000 1500 2000 channel

2500 3000

~ L:.:!..2t::J

3500 4000

~ ROI Type: 1 ROI Type: 2

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0184

4/17/2018 7:13:55AM

pex-Gamma Analysis Report for 1803111-02

BLANK

GAMMA SPECTRUM ANALYSIS

Sample Identification

Sample Description

Sample Type

Sample Size

Facility

Sample Taken On

Acquisition Started

Procedure

Operator

Detector Name

Geometry

Live Time

Real Time

Dead Time

Peak Locate Threshold

Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance

Energy Calibration Used Done On

Efficiency Calibration Used Done On

Efficiency Calibration Description

Sample Number

: 1803111-02

: BLANK

: SOIL

: 7 .834E+02 grams

: Countroom

: 4/16/2018 9:14:44AM

: 4/17/2018 6:13:43AM

: GAS-1602 pCi

: Administrator

: GE1 : GAS-1602

: 3600.0 seconds

: 3600.4 seconds

: 0.01 %

: 2.50

: 1 - 4096

: 19 - 4096

: 1.000 keV

: 2/17/2018

: 2/17/2018

: 64640

PEAK-TO-TOTAL CALIBRATION REPORT

Peak-to-Total Efficiency Calibration Equation

Page 1 of23

l{P lj/;?/18

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Analysis Report for 1803111-02

BLANK

PEAK LOCATE REPORT

Peak No.

1 2 3 4 5 6 7 8 9

10 11 12 13 14 15 16 17 18 19 20

Peak Locate Performed on

Peak Locate From Channel

Peak Locate To Channel

Peak Search Sensitivity

Energy (keV)

59.52 11 7. 32 130.85 142.42 313.97 388.35 452.29 515.40 677.85 681.23 692.28 820.91 860.62 907.03 918.40 940.14

1091.54 1112.88 1224.87 1813.64

? = Adjacent peak noted

Errors quoted at 2.000sigma

: 4/17/2018 7:13:47AM

: 1 : 4096

: 2.50

Centroid Channel

60.00 117.74 131.27 142.82 314.23 388.54 452.43 515.49 677.81 681.19 692.23 820.76 860.45 906.82 918.18 939.91

1091.21 1112.54 1224.45 1812.93

Centroid Uncertainty

0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000

Page 2 of23

Peak Significance

0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00

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0186

M

m M m

4/17/2018 7:13:55AM

Analysis Report for 1803111-02

BLANK

PEAK ANALYSIS REPORT

Peak Analysis Performed on : 4/17/2018 7:13:47AM

Peak Analysis From Channel : 1

Peak Analysis To Channel : 4096

Peak Energy ROI

No. (keV) start

1 59.52 59 -2 11 7. 32 115-3 130.85 12 9 -4 142.42 139 -5 313.97 312 -6 388.35 386 -7 452.29 44 9 -8 515.40 507 -9 677.85 663 -

10 681.23 663 -11 692.28 688 -12 820.91 817 -13 860.62 858 -14 907.03 902 -15 918.40 915 -16 940.14 933 -17 1091.54 1087 -18 1112.88 1109 -19 1224.87 1221 -20 1813.64 1811 -

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet Errors quoted at 2.000sigma

ROI Peak

end Centroid

68 60.00 121 117.74 133 131.27 147 142.82 316 314.23 392 388.54 455 452.43 522 515.49 686 677.81 686 681.19 695 692.23 823 820.76 863 860.45 912 906.82 922 918.18 945 939.91

1094 1091.21 1114 1112.54 1228 1224.45 1815 1812.93

Net Peak Net Area Area Uncertainty

1.80E+0l 14.93 2.57E+0l 30.77 2.50E+0l 23.80 4.80E+0l 39.59 1.30E+0l 16.95 1.35E+0l 15.17 1. 96E+0l 16.32 1.26E+0l 22.63 1.07E+0l 11. 96 8.84E+00 12.29 1.30E+0l 13 .11 1.33E+0l 11. 36 7.78E+00 6.71 1.07E+0l 14.46 9.63E+00 10.58 1.98E+0l 13. 73 8.15E+00 7.48 6.77E+00 8.43 6.83E+00 7.21 6.13E+00 6.67

PEAK ANALYSIS REPORT

Peak Analysis Performed on : 4/17/2018 7:13:47AM

Peak Analysis From Channel : 1

Peak Analysis To Channel : 4096

Page 3 of23

Continuum FWHM Counts (keV)

6.13E+0l 1. 48 1.53E+02 2.71 1.02E+02 2.09 2.12E+02 5.01 5.20E+0l 2.58 3.31E+0l 3.55 3.28E+0l 3.52 4.72E+0l 2. 67 2.00E+0l 2.09 1.91E+0l 2.09 2.00E+0l 2.62 1.35E+0l 2.03 2.44E+00 1. 20 2.26E+0l 3.01 1.28E+0l 3.75 1.25E+0l 6.77 3.70E+00 3.71 8.45E+00 1. 82 4.33E+00 2.91 3.75E+00 2.80

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M

4/17/2018 7:13:55AM Page 4 of23

Analysis Report for 1803111-02

M

m M m

BLANK

Peak Energy ROI

No. (keV) start

1 59.52 59 -2 11 7. 32 115 -3 130.85 12 9 -4 142.42 139 -5 313.97 312 -6 388.35 386 -7 452.29 44 9 -8 515.40 507 -9 677.85 663 -

10 681.23 663 -11 692.28 688 -12 820.91 81 7 -13 860.62 858 -14 907.03 902 -

15 918.40 915 -16 940.14 933 -17 1091.54 1087 -

18 1112.88 1109 -19 1224.87 1221 -20 1813.64 1811 -

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet

Errors quoted at 2.000sigma

ROI Net Peak Net Area Continuum

end Area Uncertainty Counts

68 1.80E+0l 14.93 6.13E+01

121 2.57E+0l 30.77 1.53E+02

133 2.50E+0l 23.80 1.02E+02

147 4.80E+0l 39.59 2.12E+02

316 1.30E+0l 16.95 5.20E+01

392 1.35E+0l 15.17 3.31E+01

455 1.96E+0l 16.32 3.28E+01

522 1.26E+0l 22.63 4. 72E+0l

686 1.07E+0l 11. 96 2.00E+0l

686 8.84E+00 12.29 l.91E+01

695 1.30E+0l 13 .11 2.00E+0l

823 1.33E+0l 11. 36 1.35E+0l

863 7.78E+00 6.71 2.44E+00

912 1.07E+0l 14.46 2.26E+0l

922 9.63E+00 10.58 1.28E+0l

945 1.98E+0l 13.73 1.25E+0l

1094 8.15E+00 7.48 3.70E+00

1114 6.77E+00 8.43 8.45E+00

1228 6.83E+00 7.21 4.33E+00

1815 6.13E+00 6.67 3.75E+00

PEAK WITH NID REPORT

Peak Analysis Performed on : 4/17/2018 7:13:47AM

Peak Analysis From Channel : 1

Peak Analysis To Channel : 4096

Tentative NID Library

Peak Match Tolerance

Peak Energy

No. (keV)

1 59.52 2 11 7. 32 3 130.85

: \\OR-GAMMA 1 \ApexRoot\Countroom\Library\TMA2.NLB

: 1.000 keV

ROI ROI Peak Net Peak

start end Centroid Area

59 - 68 60.00 1.80E+0l

115 - 121 117.74 2.57E+0l

12 9 - 133 131.27 2.50E+0l

Net Area Continuum Uncertainty Counts

14.93 6.13E+0l 30.77 1.53E+02 23.80 1.02E+02

Critical Level

1.29E+0l 2.39E+0l 1.78E+0l 3.05E+0l 1.26E+01 1.09E+01 1.13E+01 l.13E+01 7.36E+00 7.18E+00 9.0lE+00 7.17E+00 3.06E+00 1.06E+0l 7.05E+00 8.60E+00 3.98E+00 5.45E+00 4.08E+00 3.68E+00

Tentative Nuclide

AM-241

PA-234

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Analysis Report for 1803111-02

m M m

M

m M m

BLANK

Peak Energy ROI

No. (keV) start

4 142.42 13 9 -5 313.97 312 -6 388.35 386 -7 452.29 44 9 -8 515.40 507 -9 677.85 663 -

10 681.23 663 -11 692.28 688 -12 820.91 81 7 -13 860.62 858 -14 907.03 902 -15 918.40 915 -16 940.14 933 -17 1091.54 1087 -18 1112.88 1109 -19 1224.87 1221 -20 1813.64 1811 -

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet

Errors quoted at 2.000sigma

ROI Peak Net Peak Net Area

end Centroid Area Uncertainty

147 142.82 4.80E+0l 39.59

316 314.23 1.30E+0l 16.95

392 388.54 1.35E+0l 15.17

455 452.43 1. 96E+0l 16.32

522 515.49 1.26E+0l 22.63

686 677.81 1.07E+0l 11. 96

686 681.19 8.84E+00 12.29

695 692.23 1.30E+0l 13 .11

823 820.76 1.33E+0l 11. 36

863 860.45 7.78E+00 6.71

912 906.82 1.07E+0l 14.46

922 918.18 9.63E+00 10.58

945 939.91 1.98E+0l 13.73

1094 1091.21 8.15E+00 7.48

1114 1112.54 6.77E+00 8.43

1228 1224.45 6.83E+00 7.21

1815 1812.93 6.13E+00 6.67

PEAK EFFICIENCY REPORT

Peak Analysis Performed on : 4/17/2018 7:13:47AM

Peak Energy Net Peak Net Area Peak

No. (keV) Area Uncertainty Efficiency

1 59.52 1.80E+0l 14.93 2.50E-02

2 117.32 2.57E+0l 30.77 2.76E-02

3 130.85 2.50E+0l 23.80 2.67E-02

4 142.42 4.80E+0l 39.59 2.59E-02

5 313.97 1.30E+0l 16.95 1.64E-02

6 388.35 1.35E+0l 15 .17 1.41E-02

7 452.29 1.96E+0l 16.32 1.26E-02

8 515.40 1.26E+01 22.63 l.14E-02

9 677.85 1.07E+01 11. 96 9.15E-03

10 681.23 8.84E+00 12.29 9.12E-03

11 692.28 1.30E+0l 13 .11 9.00E-03

12 820.91 1.33E+01 11. 36 7.85E-03

13 860.62 7.78E+00 6. 71 7.56E-03

Page 5 of23

Continuum Tentative Counts Nuclide

2.12E+02 5.20E+0l 3.31E+0l 3.28E+0l 4.72E+0l 2.00E+0l AG-ll0M 1.91E+0l 2.00E+0l 1.35E+0l 2.44E+00 TL-208 2.26E+0l 1.28E+0l 1.25E+0l 3.70E+00 8.45E+00 EU-152 4.33E+00 3.75E+00

Efficiency Uncertainty

1.85E-03 2.24E-03 2.36E-03 2.56E-03 2.44E-03 2.17E-03 1.87E-03 1.57E-03 9.0lE-04 9.05E-04 9.22E-04 1.llE-03 1.17E-03

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Analysis Report for 1803111-02

M

m M m

BLANK

Peak Energy

Na. (keV)

14 907.03 15 918.40 16 940.14 17 1091.54 18 1112.88 19 1224.87 20 1813.64

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet

Errors quoted at 2.000 sigma

Net Peak Area

l.07E+0l 9.63E+00 l.98E+01 8.15E+00 6.77E+00 6.83E+00 6. 13E+00

Net Area Uncertainty

14.46 10.58 13.73

7.48 8.43 7.21 6.67

Peak Efficiency

7.25E-03 7.18E-03 7.04E-03 6.25E-03 6.16E-03 5.71E-03 4.27E-03

Efficiency Uncertainty

l.20E-03 l.17E-03 1. llE-03 7.27E-04 6.73E-04 5.03E-04 4.77E-04

BACKGROUND SUBTRACT REPORT

Peak Analysis Performed on : 4/17/2018 7:13:47AM

Env. Background File : \\OR-GAMMA 1 \ApexRoot\Countroom\Data\0000063824.CNF

Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted

No. (keV) Area Uncertainty Background Uncert. Area Uncert.

1 59.52 1.80E+0l 14.93 1.80E+0l 1.49E+0l

2 117. 32 2.57E+0l 30.77 2.57E+0l 3.08E+0l

3 130.85 2.50E+0l 23.80 2.50E+0l 2.38E+0l

4 142.42 4.80E+0l 39.59 4.80E+0l 3.96E+0l

5 313.97 1.30E+0l 16.95 1.30E+0l 1.69E+0l

6 388.35 1.35E+0l 15.17 1.35E+0l 1.52E+0l

7 452.29 1.96E+0l 16.32 1.96E+0l 1.63E+0l

8 515.40 1.26E+0l 22.63 1.26E+0l 2.26E+0l

9 677.85 1.07E+0l 11. 96 1.07E+0l 1.20E+0l

10 681. 23 8.84E+00 12.29 8.84E+00 1.23E+0l

11 692.28 1.30E+0l 13 .11 1.30E+0l 1.31E+0l

12 820.91 1.33E+0l 11. 36 1.33E+0l l.14E+0l

13 860.62 7.78E+00 6.71 7.78E+00 6.71E+00

14 907.03 1.07E+0l 14.46 1.07E+0l l.45E+0l

15 918.40 9.63E+00 10.58 9.63E+00 1.06E+0l

16 940.14 1.98E+0l 13. 73 1.98E+0l 1.37E+0l

17 1091.54 8.15E+00 7.48 8.15E+00 7.48E+00

18 1112.88 6.77E+00 8.43 6.77E+00 8.43E+00

19 1224.87 6.83E+00 7.21 6.83E+00 7.21E+00

20 1813.64 6.13E+00 6.67 6.13E+00 6.67E+00

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Analysis Report for 1803111-02

BLANK

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet Errors quoted at 2.000sigma

AREA CORRECTION REPORT

REFERENCE PEAK I 8KG. SUBTRACT

Peak Analysis Performed on

Ref. Peak Energy

Peak Ratio

Background File

: 4/17/2018 7:13:47AM

: 0.00 Reference Date

: 0.00 Uncertainty : 0.00

: \\0 R-GAMMA 1 \ApexRoot\Countroom\Data\0000063824.CN F

Corrected Area is: Original * Peak Ratio - Background

Peak Energy Original Orig. Area Ambient Backgr.

No. (keV) Area Uncertainty Background Uncert.

M 1 59.52 l.80E+0l 14.93

2 117. 32 2.57E+0l 30.77

3 130. 85 2.50E+0l 23.80

4 142.42 4.80E+01 39.59

5 313.97 1.30E+0l 16.95

6 388.35 1.35E+0l 15.17

7 452.29 1. 96E+0l 16.32

m 8 515.40 1.26E+0l 22.63

M 9 677.85 1.07E+0l 11. 96

m 10 681.23 8.84E+00 12.29

11 692.28 1.30E+0l 13 .11

12 820.91 1.33E+0l 11. 36

13 860.62 7.78E+00 6.71

14 907.03 1.07E+01 14.46

15 918.40 9.63E+00 10.58

16 940.14 l.98E+0l 13.73

17 1091.54 8.15E+00 7.48

18 1112.88 6.77E+00 8.43

19 1224.87 6.83E+00 7.21

20 1813.64 6.13E+00 6.67

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet

Errors quoted at 2.000sigma

Corrected Area

1.80E+0l 2.57E+0l 2.50E+0l 4.80E+0l 1.30E+0l 1.35E+0l 1. 96E+0l 1.26E+0l 1.07E+0l 8.84E+00 1.30E+0l 1.33E+0l 7. 78E+00 1.07E+0l 9.63E+00 l.98E+0l 8.15E+00 6.77E+00 6.83E+00 6.13E+00

Corrected Uncert.

l.49E+0l 3.08E+0l 2.38E+0l 3.96E+0l 1.69E+0l 1.52E+0l 1.63E+0l 2.26E+0l 1.20E+0l l.23E+0l 1.31E+0l l.14E+0l 6.71E+00 1.45E+0l 1.06E+0l l.37E+0l 7.48E+00 8.43E+00 7.21E+00 6.67E+00

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Analysis Report for 1803111-02

BLANK

NUCLIDE IDENTIFICATION REPORT

Nuclide Library Used : \\OR-GAMMA 1\ApexRoot\Countroom\Library\TMA2.NLB

IDENTIFIED NUCLIDES

Nuclide Name Id Confidence

PA-234 0.425

AM-241 1.000

* = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

Energy Tolerance : 1.000 keV

Nuclide confidence index threshold = 0.30

Errors quoted at 2.000sigma

Energy (keV)

131. 20 * 733.99 946.00

59.54 *

Yield(%)

20.40 8.80

12.00 35.90

UNIDENTIFIED PEAKS

m M m

Peak Locate Performed on

Peak Locate From Channel

Peak Locate To Channel

Peak No. Energy (keV)

2 117. 32 4 142.42 5 313.97 6 388.35 7 452.29 8 515.40 9 677.85

10 681.23 11 692.28 12 820.91 13 860.62 14 907.03 15 918.40

: 4/17/2018 7:13:47AM

: 1 : 4096

Peak Size (CPS)

7.13508£-03 1.33342£-02 3.60755£-03 3. 73611£-03 5.44753£-03 3. 5071 7E-03 2.96349£-03 2.45691£-03 3.60507£-03 3.68056£-03 2.16049£-03 2. 9671 7E-03 2.67361£-03

Peak CPS(%) Uncertainty

59.90 41.24 65.25 56.41 41.62 89.61 56.04 69.46 50.53 42.86 43.12 67. 67 54.98

Activity

(pCi/grams)

4.40E-02

1.92E-02

Peak Type

Tol.

Tol.

Page 8 of23

Activity

Uncertainty

4.20E-02

1.60E-02

Tolerance Nuclide

AG-ll0M

TL-208

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Analysis Report for 1803111-02

BLANK

Peak No. Energy (ke V)

16 940.14 17 1091.54 18 1112.88 19 1224.87 20 1813.64

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet

Errors quoted at 2.000sigma

Peak Size (CPS) Peak CPS(%) Peak Tolerance

Uncertainty Type Nuclide

5.49145E-03 34. 72 2.26389E-03 45.91 1.88131E-03 62.21 Tol. EU-152

1.89815E-03 52.76 1.70139E-03 54.46

NUCLIDE IDENTIFICATION REPORT

Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\TMA2.NLB

IDENTIFIED NUCLIDES

Nuclide Id Energy

Name Confidence (keV)

PA-234 0.42 131.20 733.99 946.00

AM-241 1.00 59.54

* = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

*

*

@ = Energy line not used for Weighted Mean Activity

Energy Tolerance : 1.000 keV

Nuclide confidence index threshold = 0.30

Errors quoted at 2.000sigma

Yield(%)

20.40 8.80

12.00 35.90

Activity

(pCi!grams)

4.40E-02

1.92E-02

Activity

Uncertainty

4.20E-02

l.60E-02

INTERFERENCE CORRECTED REPORT

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Analysis Report for 1803111-02

BLANK

Nuclide Name

PA-234 AM-241

Nuclide Id

Confidence

0.425 1.000

? nuclide is part of an undetermined solution

X = nuclide rejected by the interference analysis

4/17/2018 7: 13:55AM

Wt mean Wt mean

Activity Activity

(pCilgrams) Uncertainty

4.40E-02 4.20E-02 1.92E-02 1.60E-02

@ = nuclide contains energy lines not used in Weighted Mean Activity

Errors quoted at 2.000sigma

Page 10 of23

Comments

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Analysis Report for 1803111-02

m M

m

BLANK

Peak Locate Performed on

Peak Locate From Channel

Peak Locate To Channel

Peak No. Energy (ke V)

2 11 7. 32

4 142.42

5 313.97

6 388.35

7 452.29

8 515.40

9 677.85

10 681.23

11 692.28

12 820.91

13 860.62

14 907.03

15 918.40

16 940.14

17 1091.54

18 1112.88

19 1224.87

20 1813.64

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet

Errors quoted at 2.000sigma

4/17/2018 7:13:55AM

UNIDENTIFIED PEAKS

: 4/17/2018 7:13:47AM

: 1 : 4096

Peak Size (CPS)

7 .13508E-03

1.33342E-02

3.60755E-03

3. 73611E-03

5.44753E-03

3.50717E-03

2. 9634 9E-03

2.45691E-03

3.60507E-03

3.68056E-03

2.16049E-03

2. 96717E-03

2.67361E-03

5.49145E-03

2.26389E-03

1. 88131E-03

1.89815E-03

1. 70139E-03

Peak CPS(%) Uncertainty

59.90

41.24

65.25

56.41

41.62

89.61

56.04

69.46

50.53

42.86

43.12

67.67

54.98

34.72

45.91

62.21

52.76

54.46

NUCLIDE MDA REPORT

Peak Type

Tol.

Tol.

Tol.

Nuclide Library Used : \\OR-GAMMA 1\ApexRoot\Countroom\Library\TMA2.NLB

Nuclide Name

Energy

(keV)

Yield(%) Activity

(pCilgrams) Nuclide MDA

(pCilgrams)

Line MDA

(pCi/grams)

Page 11 of23

Tolerance Nuclide

AG-ll0M

TL-208

EU-152

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+ BE-7 477.59 10.42 8.60E-03 2.21E-01 2.21E-01

+ NA-22 1274.54 99.94 -1.0lE-02 1.87E-02 1.87E-02

+ NA-24 1368.53 99.99 8.32E-03 2.12E-02 3.18E-02

2754.09 99.86 -9.58E-04 2.12E-02

+ AL-26 1808.65 99.76 6.74E-03 3.57E-02 3.57E-02

+ K-40 1460.81 10.67 1.62E-0l 3.39E-01 3.39E-01

+ AR-41 1293.64 99.16 1.52E+0l 8.58E+01 8.58E+0l

+ TI-44 67.88 94.40 1.76E-03 1.79E-02 1.86E-02

78.34 96. 00 8.90E-04 1.79E-02

+ SC-46 889.25 98.98 5.77E-03 2.07E-02 2.66E-02

1120.51 99.90 -1.58E-02 2.07E-02

+ V-48 983.52 99.98 5.13E-03 2.20E-02 2.20E-02

1312.10 97.50 7.55E-03 2. 27E-02

+ CR-51 320.08 9.83 -4.74E-02 2.19E-01 2.19E-01

+ MN-54 834.83 99.97 7.03E-03 2.78E-02 2.78E-02

+ CO-56 846.75 99. 96 8.91E-03 3.39E-02 3.39E-02

1037.75 14.03 1.02E-01 2.32E-01

1238.25 67.00 -1.59E-02 3.59E-02

1771.40 15.51 0.00E+00 3.89E-02

2587.48 16.90 -2.49E-02 1.79E-01

+ CO-57 122.06 85.51 6.82E-03 1.71E-02 1.71E-02

136.48 10.60 7.57E-03 1.33E-01

+ CO-58 810.76 99.40 -1.38E-03 2.61E-02 2.61E-02

+ FE-59 1099.22 56.50 2. 96E-03 4.15E-02 4.15E-02

1291.56 43.20 -8.21E-03 4.93E-02

+ CO-60 1173.22 100.00 9.59E-03 2.53E-02 2.94E-02

1332.49 100.00 0.00E+00 2.53E-02

+ ZN-65 1115.52 50.75 -1.18E-02 5.59E-02 5.59E-02

+ GA-67 93.31 35.70 l.48E-01 8.16E-02 8.16E-02

208.95 2.24 -3.64E-01 9.08E-01

300.22 16.00 -2.17E-02 1.49E-01

+ SE-75 121.11 16.70 3.49E-02 2.36E-02 8.78E-02

136.00 59.50 -7.44E-03 2.36E-02

264.65 59.80 -5.l0E-03 3.51E-02

279.53 25.20 -9.32E-03 7.14E-02

400.65 11. 40 -1.04E-0l 1.73E-01

+ RB-82 776.52 13. 00 6.96E-02 1.96E-01 1.96E-01

+ RB-83 520.41 46.00 -3.15E-02 4.66E-02 4.66E-02

529.64 30.30 1.97E-03 7.31E-02

552.65 16.40 3.89E-02 1.26E-01

+ KR-85 513.99 0.43 8.44E+00 8.75E+00 8.75E+00

+ SR-85 513.99 99. 27 3.73E-02 3.86E-02 3.86E-02

+ Y-88 898.02 93.40 1.53E-03 1.99E-02 1.99E-02

1836.01 99.38 -2.29E-03 2.75E-02

+ MO-93 263.06 56. 72 9.28E-03 1.99E-02 3.77E-02

684.67 99.68 -9.18E-03 1.99E-02

1477 .11 99.08 5.87E-03 2.35E-02

+ NB-93M 16.57 9.43 -1.17E+00 3.51E+00 3.51E+00

+ NB-94 702.63 100.00 -2.21E-02 2.42E-02 2.42E-02

871.10 100.00 -1.53E-03 2.49E-02

+ NB-95 765.79 99.81 -1.86E-04 2.71E-02 2.71E-02

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Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA

Name (keV) (pCi/grams) (pCi/grams) (pCi/grams)

+ NB-95M 235.69 25.00 -5.63E-02 8.23E-02 8.23E-02

+ ZR-95 724.18 43.70 -8.83E-03 4.69E-02 4.97E-02

756.72 55.30 -l.80E-02 4.69E-02

+ MO-99 181.06 6.20 -1.32E-01 2.21E-0l 3.26E-01

739.58 12.80 3.77E-02 2. 21E-01

778.00 4.50 -2.49E-01 5.90E-01

+ TC-99M 140.51 89.00 -2.79E-04 1.90E-02 l.90E-02

+ RU-103 497.08 89.00 -9.88E-03 2.34E-02 2.34E-02

+ RU-106 621.84 9.80 5.07E-02 2.64E-01 2.64E-01

+ AG-108M 433.93 89.90 2.13E-03 2.39E-02 2.39E-02

614.37 90.40 -4.16E-03 2.97E-02

722.95 90.50 -2.18E-03 2.45E-02

+ CD-109 88.03 3. 72 -3.42E-01 4.48E-0l 4.48E-01

+ AG-ll0M 657.75 93.14 l.l0E-03 2.28E-02 2.28E-02

677.61 10.53 1.54E-01 2.63E-01

706.67 16.46 -l.62E-02 1.74E-01

763.93 21.98 7.90E-02 l.36E-01

884.67 21.98 -3.25E-02 1.22E-01

1384.27 23.94 9.65E-03 9.28E-02

+ CD-113M 263.70 0.02 -1.21E-01 9.06E+0l 9.06E+0l

+ SN-113 255.12 1.93 2.37E-02 3.04E-02 8.78E-01

391.69 64.90 -6.90E-03 3.04E-02

+ TE-123M 159.00 84.10 9.71E-03 2.l0E-02 2.l0E-02

+ SB-124 602.71 97.87 -1.66E-02 2.86E-02 2.86E-02

645.85 7.26 2.03E-01 3.30E-01

722.78 11. 10 -1. 79E-02 2.02E-01

1691.02 49.00 1.54E-02 6.62E-02

+ I-125 35.49 6.49 8.07E-02 4.96E-01 4.96E-01

+ SB-125 176.33 6.89 2.80E-02 6.82E-02 2.37E-01

427.89 29.33 -2.l0E-02 6.82E-02

463.38 10.35 -l.29E-02 2.18E-01

600.56 17.80 4.52E-02 l.64E-01

635.90 11. 32 3.54E-02 2.07E-01

+ SB-126 414.70 83.30 -l.61E-02 2.15E-02 2.15E-02

666.33 99.60 4.15E-03 2.69E-02

695.00 99.60 -3.57E-03 2.58E-02

720.50 53.80 7.66E-03 4.36E-02

+ SN-126 87.57 37.00 -3.43E-02 4.50E-02 4.50E-02

+ SB-127 473.00 25.00 -5.32E-02 6.54E-02 9.64E-02

685.00 35.70 -3.0lE-02 6.54E-02

783.80 14.70 3.55E-02 2. llE-01

+ I-129 29.78 57.00 2.59E-02 9.33E-02 9.33E-02

33.60 13.20 -6.62E-02 2.81E-01

39.58 7.52 4.63E-02 3.64E-01

+ I-131 284.30 6.05 -6.48E-02 2.75E-02 3.09E-01

364.48 81.20 1.82E-03 2.75E-02

636.97 7.26 1.48E-01 3.64E-01

722.89 1. 80 -1.18E-01 l.33E+00

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Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA

Name (keV) (pCi/grams) (pCi!grams) (pCi/grams)

+ TE-132 49. 72 13 .10 -2.95E-01 2.16E-02 1.60E-01

228.16 88.00 -1.50E-03 2.16E-02

+ BA-133 81.00 33.00 -1.14E-02 3.18E-02 5.12E-02

302.84 17.80 -6.35E-02 1.02E-01

356.01 60.00 -2.24E-02 3.18E-02

+ I-133 529.87 86.30 1.41E-03 5. 21E-02 5.21E-02

+ XE-133 81.00 38.00 -1. llE-02 5.00E-02 5.00E-02

+ CS-134 563.23 8.38 -2.03E-02 3.13E-02 2.36E-01

569.32 15.43 -8.03E-02 l.15E-01

604.70 97. 60 2.51E-03 3.15E-02

795.84 85.40 3.49E-04 3.13E-02

801.93 8.73 -2.06E-02 3.08E-01

+ CS-135 268.24 16.00 3.94E-02 1.33E-0l l.33E-01

+ I-135 1131.51 22.50 -8.57E-02 8.56E-01 1.00E+00

1260.41 28.60 8.56E-02 8.56E-01

1678.03 9.54 -4.77E-01 2.55E+00

+ CS-136 153.22 7.46 -1.23E-01 2.94E-02 2.06E-01

163.89 4.61 l.14E-01 3.60E-01

176.55 13.56 1.49E-02 1.26E-01

273.65 12.66 -l.l0E-02 l.73E-01

340.57 48.50 -l.68E-02 4.49E-02

818.50 99.70 -4.27E-04 2.94E-02

1048.07 79.60 8.60E-03 4.05E-02

1235.34 19.70 -8.09E-02 l.18E-01

+ CS-137 661.65 85.12 2.41E-03 2. 71E-02 2.71E-02

+ LA-138 788.74 34.00 -6.95E-03 3.77E-02 7.99E-02

1435.80 66.00 l.44E-02 3.77E-02

+ CE-139 165.85 80.35 -3.77E-03 1.83E-02 l.83E-02

+ BA-140 162. 64 6.70 3.81E-02 9.84E-02 2.54E-01

304.84 4.50 -1.56E-01 4.24E-01

423.70 3.20 2.63E-01 7.39E-01

437.55 2.00 -l.43E-02 1.l0E+00

537.32 25.00 -2.98E-02 9.84E-02

+ LA-140 328.77 20.50 -4.05E-02 2.43E-02 9.58E-02

487.03 45.50 -5.08E-04 5.49E-02

815.85 23.50 4.07E-03 l.06E-01

1596.49 95.49 0.00E+00 2.43E-02

+ CE-141 145.44 48.40 -5. 96E-03 3.46E-02 3.46E-02

+ CE-143 57.36 11. 80 1.00E-01 7.48E-02 2.54E-01

293.26 42.00 -2. 96E-02 7.48E-02

664.55 5.20 l.23E-01 8.08E-01

+ CE-144 133.54 10.80 -3.88E-02 1.30E-01 l.30E-01

+ PM-144 476.78 42.00 -1.27E-02 2.64E-02 5.18E-02

618.01 98.60 -6.19E-03 2.66E-02

696.49 99.49 4.52E-03 2.64E-02

+ PM-145 36.85 21.70 -4. 96E-02 7.54E-02 1.37E-01

37.36 39.70 -1.12E-02 7.54E-02

42.30 15.10 -6.91E-02 1.67E-01

72. 40 2.31 -6.58E-02 7.19E-01

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Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA

Name (keV) (pCilgrams) (pCilgrams) (pCi!grams)

+ PM-146 453.90 39.94 -6.23E-03 5.56E-02 5.56E-02

735.90 14.01 -1.05E-01 1.39E-01

747.13 13.10 -4.99E-02 1.57E-01

+ ND-147 91.11 28.90 1. 72E-01 8.97E-02 8.97E-02

531.02 13.10 -1.40E-02 1.78E-01

+ PM-149 285.90 3.10 -2.09E-02 7.76E-01 7.76E-01

+ EU-152 121.78 20.50 2.83E-02 7.13E-02 7. 13E-02

244.69 5.40 -1.36E-01 3.04E-01

344.27 19 .13 2.29E-02 1.17E-01

778.89 9.10 -1.61E-01 2.42E-01

964.01 10.40 5.76E-02 2.85E-01

1085.78 7.22 -1.06E-02 2.28E-01

1112.02 9.60 4.20E-02 2.94E-01

1407.95 14.94 -2.71E-02 1.35E-01

+ GD-153 97.43 31.30 -2.82E-02 5.03E-02 5.03E-02

103.18 22.20 3.28E-03 6.58E-02

+ EU-154 123.07 40.50 1.83E-03 3.47E-02 3.47E-02

723. 30 19.70 -1.00E-02 1.13E-01

873.19 11. 50 -3.98E-02 2.24E-01

996.32 10.30 -1.26E-03 2.51E-01

1004.76 17.90 -8.15E-02 1.13E-01

1274.45 35.50 -2.84E-02 5.25E-02

+ EU-155 86.50 30.90 1.18E-03 5.55E-02 5.55E-02

105.30 20.70 -l.83E-02 7.02E-02

+ EU-156 811.77 10.40 9.66E-02 2.65E-01 2.65E-01

1153.47 7.20 -5.79E-02 3.67E-01

1230.71 8.90 5.77E-02 3.13E-01

+ HO-166M 184.41 72.60 3.07E-02 3.04E-02 3.04E-02

280.45 29.60 -1.50E-02 5.86E-02

410.94 11.10 l.43E-02 1.83E-01

711.69 54.10 5.66E-03 5.59E-02

+ TM-171 66.72 0.14 -1.64E+0l 1.35E+0l 1.35E+0l

+ HF-1 72 67.35 5.31 3.14E-02 1.29E-01 3.31E-01

125.82 11. 30 -2.58E-03 1.29E-01

+ LU-1 72 181.53 20.60 -1.87E-01 5.07E-02 8.14E-02

900.72 29.81 -1.61E-03 6.82E-02

1093.66 62.50 2.69E-03 5.07E-02

+ LU-173 100. 72 5.24 -2.56E-03 9.83E-02 2.98E-01

272 .11 21. 20 -7.64E-03 9.83E-02

+ HF-175 343.40 84.00 5.25E-03 2.69E-02 2.69E-02

+ LU-176 88.34 13. 30 -3.72E-01 l.88E-02 1.26E-0l

201.83 86.00 -l.22E-02 1.88E-02

306.78 94.00 6.87E-03 2.07E-02

+ HF-181 133.02 41.70 -9.00E-03 2.64E-02 3.61E-02

345.85 17.20 -5. 79E-04 1.33E-01

482.03 82.80 -l.07E-02 2.64E-02

+ TA-182 67.75 41.20 4.05E-03 4.28E-02 4.28E-02

1121. 30 34.90 0.00E+00 7.86E-02

1189.05 16.23 -2.76E-02 1.53E-01

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Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA

Name (keV) (pCi/grams) (pCi/grams) (pCi/grams)

TA-182 1221.41 26.98 -3.12E-03 4.28E-02 8.18E-02

1231.02 11. 44 7.40E-02 2.35E-01

+ IR-192 308.46 29.68 -4.07E-03 4.56E-02 6.58E-02

468.07 48.10 1.70E-04 4.56E-02

+ HG-203 279.19 77. 30 6.45E-03 2.51E-02 2.51E-02

+ TL-204 374.74 94 .11 -3.52E-03 1.99E-02 1.99E-02

899.15 99.16 3.97E-03 1.99E-02

911.74 91.10 2.92E-03 2.64E-02

+ BI-207 569.67 97. 72 -1.55E-02 1.82E-02 1.82E-02

1063.62 74.90 -1.30E-02 2.41E-02

+ TL-208 583.14 30.22 -5.60E-03 7.99E-02 7.99E-02

860.37 4.48 6.36E-02 4.93E-01

2614.66 35.85 7.03E-02 l.30E-01

+ BI-210M 262.00 45.00 -4.19E-03 4.68E-02 4.68E-02

300.00 23.00 -1.25E-02 8.59E-02

+ PB-210 46.50 4.25 3.72E-01 5.55E-01 5.55E-01

+ PB-211 404.84 2.90 -3.48E-01 6.51E-01 6.51E-01

831. 96 2.90 -1.83E-01 8.0lE-01

+ BI-212 727.17 11. 80 -9.39E-02 1.70E-01 1.70E-01

1620.62 2.75 3.77E-01 1.13E+00

+ PB-212 238.63 44.60 4.19E-02 4.68E-02 4.68E-02

300.09 3.41 -8.40E-02 5.80E-01

+ BI-214 609.31 46.30 2.99E-02 6.90E-02 6.90E-02

1120.29 15.10 -l.04E-01 1.36E-01

1764.49 15.80 6.97E-02 l.83E-01

2204.22 4.98 -1.79E-01 5.51E-01

+ PB-214 295.21 19.19 1.37E-02 6.34E-02 l.12E-01

351.92 37.19 2.52E-02 6.34E-02

+ RN-219 401.80 6.50 -1.46E-02 3.16E-01 3.16E-01

+ RA-223 323.87 3.88 2.78E-01 5.68E-01 5.68E-01

+ RA-224 240.98 3.95 2.llE-01 4.98E-01 4.98E-01

+ RA-225 40.00 31.00 1.15E-02 9.04E-02 9.04E-02

+ RA-226 186.21 3.28 9.60E-01 6.87E-01 6.87E-01

+ TH-227 50.10 8.40 -2.29E-02 1.51E-01 2.17E-01

236.00 11. 50 -1.03E-01 1.51E-01

256.20 6.30 -8.07E-03 3.18E-01

+ AC-228 338.32 11. 40 2.70E-03 9.02E-02 l.85E-01

911.07 27.70 9.58E-03 9.02E-02

969 .11 16.60 -4.73E-02 1.52E-01

+ TH-230 48.43 16.90 -4.60E-02 1.16E-01 1.16E-01

62.85 4.60 3.63E-01 5.26E-01

67.67 0.37 4.49E-01 4.74E+00

+ PA-231 283.67 1. 60 -5.23E-02 7.86E-01 1.08E+00

302.67 2.30 -4.91E-01 7.86E-01

+ TH-231 25.64 14.70 -5.91E+00 2.77E-0l 7.13E-01

84.21 6.40 1.38E-01 2.77E-01

+ PA-233 311.98 38.60 -3.85E-03 5.73E-02 5.73E-02

+ PA-234 131.20 * 20.40 4.40E-02 6.72E-02 6. 72E-02

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Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA

Name (keV) (pCilgrams) (pCi/grams) (pCi/grams)

PA-234 733.99 8.80 5.52E-02 6.72E-02 2.55E-01

946.00 12.00 -5.70E-02 1.81E-01

+ PA-234M 1001.03 0.92 3.50E-01 2.93E+00 2.93E+00

+ TH-234 63.29 3.80 1.08E+00 6.57E-01 6.57E-01

+ U-235 143.76 10.50 8.49E-02 1.70E-01 1.70E-01

163.35 4.70 l.06E-01 3.36E-01

205.31 4.70 3.18E-02 3.77E-01

+ NP-237 86.50 12.60 2.89E-03 l.36E-01 l.36E-01

+ NP-239 106.10 22.70 -2.00E-02 8.18E-02 8.18E-02

228.18 10.70 -3.45E-03 l.95E-01

277.60 14.10 1.0lE-01 1.84E-01

+ AM-241 59.54 * 35.90 l.92E-02 7.75E-02 7.75E-02

+ AM-243 74.67 66.00 -7.05E-04 2.59E-02 2.59E-02

+ CM-243 209.75 3.29 -l.13E-01 1.43E-01 5.29E-01

228.14 10.60 -l.03E-02 l.48E-01

277.60 14.00 7.81E-02 1.43E-01

+ = Nuclide identified during the nuclide identification

* = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

NUCLIDE MDA REPORT

Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\TMA2.NLB

Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level

Name (keV) (pCi/grams) (pCilgrams) (pCilgrams) (pCilgrams)

BE-7 477.59 10.42 2.21E-01 2. 21E-01 8.60E-03 1.00E-01

NA-22 1274.54 99.94 l.87E-02 l.87E-02 -1.0lE-02 6.98E-03

NA-24 1368.53 99.99 3.18E-02 2.12E-02 8.32E-03 1.35E-02

2754.09 99.86 2.12E-02 -9.58E-04 6.69E-03

AL-26 1808.65 99.76 3.57E-02 3.57E-02 6.74E-03 1.48E-02

K-40 1460.81 10.67 3.39E-01 3.39E-01 1.62E-01 1.45E-01

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Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level

Name (keV) (pCi/grams) (pCi/grams) (pCi/grams) (pCi/grams)

AR-41 1293.64 99.16 8.58E+0l 8.58E+0l 1.52E+0l 3.47E+0l

TI-44 67.88 94.40 1. 8 6E-02 1.79E-02 1.76E-03 8.76E-03

78.34 96. 00 1.79E-02 8.90E-04 8.49E-03

SC-46 889.25 98.98 2.66E-02 2.07E-02 5.77E-03 1.15E-02

1120.51 99.90 2.07E-02 -1.58E-02 8. 21E-03

V-48 983.52 99.98 2.20E-02 2.20E-02 5.13E-03 9.03E-03

1312.10 97.50 2.27E-02 7.55E-03 8.78E-03

CR-51 320.08 9.83 2.19E-01 2.19E-01 -4.74E-02 1. 0lE-01

MN-54 834.83 99.97 2.78E-02 2.78E-02 7.03E-03 1.22E-02

CO-56 846.75 99. 96 3.39E-02 3.39E-02 8.91E-03 1.53E-02

1037.75 14.03 2.32E-01 1.02E-01 1.02E-01

1238.25 67.00 3.59E-02 -l.59E-02 1.45E-02

1771.40 15.51 3.89E-02 0.00E+00 0.00E+00

2587.48 16.90 1.79E-01 -2.49E-02 6.70E-02

CO-57 122.06 85.51 1.71E-02 l.71E-02 6.82E-03 8.0lE-03

136.48 10.60 1.33E-01 7.57E-03 6.20E-02

CO-58 810.76 99.40 2.61E-02 2.61E-02 -1.38E-03 1.14E-02

FE-59 1099.22 56.50 4.15E-02 4.15E-02 2. 96E-03 1.70E-02

1291.56 43.20 4.93E-02 -8.21E-03 1.91E-02

CO-60 1173.22 100.00 2.94E-02 2.53E-02 9.59E-03 1.25E-02

1332.49 100.00 2.53E-02 0.00E+00 l.02E-02

ZN-65 1115.52 50.75 5.59E-02 5.59E-02 -l.18E-02 2.38E-02

GA-67 93.31 35.70 8.16E-02 8.16E-02 1.48E-01 3.93E-02

208.95 2.24 9.08E-01 -3.64E-01 4.21E-01

300.22 16.00 1.49E-01 -2.17E-02 6.90E-02

SE-75 121.11 16.70 8.78E-02 2.36E-02 3.49E-02 4. llE-02

136. 00 59.50 2.36E-02 -7.44E-03 l.l0E-02

264.65 59.80 3.51E-02 -5.l0E-03 l.64E-02

27 9. 53 25.20 7.14E-02 -9.32E-03 3.28E-02

400.65 11. 40 1.73E-01 -1.04E-01 7.83E-02

RB-82 776.52 13.00 1.96E-0l 1.96E-01 6. 96E-02 8.56E-02

RB-83 520.41 46.00 4.66E-02 4.66E-02 -3.15E-02 2.08E-02

529.64 30.30 7.31E-02 1.97E-03 3. 27E-02

552.65 16.40 1.26E-01 3.89E-02 5.55E-02

KR-85 513.99 0.43 8.75E+00 8.75E+00 8.44E+00 4. llE+00

SR-85 513.99 99. 27 3.86E-02 3.86E-02 3.73E-02 1.82E-02

Y-88 898.02 93.40 1.99E-02 1.99E-02 1.53E-03 8.05E-03

1836.01 99.38 2.75E-02 -2.29E-03 l.07E-02

MO-93 263.06 56. 72 3.77E-02 1.99E-02 9.28E-03 1.76E-02

684.67 99.68 1.99E-02 -9.18E-03 8.53E-03

1477.11 99.08 2.35E-02 5.87E-03 9.l0E-03

NB-93M 16.57 9.43 3.51E+00 3.51E+00 -l.17E+00 1.58E+00

NB-94 702.63 100.00 2.42E-02 2.42E-02 -2. 21E-02 1.06E-02

871.10 100.00 2.49E-02 -1.53E-03 1.07E-02

NB-95 765.79 99.81 2.71E-02 2.71E-02 -1.86E-04 l.19E-02

NB-95M 235.69 25.00 8.23E-02 8.23E-02 -5.63E-02 3.80E-02

ZR-95 724.18 43.70 4.97E-02 4.69E-02 -8.83E-03 2.14E-02

756.72 55.30 4.69E-02 -1. 80E-02 2.06E-02

MO-99 181.06 6.20 3.26E-01 2. 21E-01 -l.32E-01 1.52E-01

739.58 12.80 2.21E-01 3.77E-02 9.57E-02

778.00 4.50 5.90E-01 -2.49E-01 2.51E-01

TC-99M 140.51 89.00 1.90E-02 1.90E-02 -2.79E-04 8.92E-03

RU-103 497.08 89.00 2.34E-02 2.34E-02 -9.88E-03 1.05E-02

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Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level

Name (keV) (pCilgrams) (pCi!grams) (pCi/grams) (pCi/grams)

RU-106 621.84 9.80 2.64E-01 2.64E-01 5.07E-02 1.19E-01

AG-108M 433.93 89.90 2.39E-02 2.39E-02 2.13E-03 1.08E-02

614.37 90.40 2.97E-02 -4.16E-03 1.34E-02

722. 95 90.50 2.45E-02 -2.18E-03 1.06E-02

CD-109 88.03 3. 72 4.48E-01 4.48E-01 -3.42E-01 2.12E-01

AG-ll0M 657.75 93.14 2.28E-02 2.28E-02 1.l0E-03 9.91E-03

677.61 10.53 2.63E-01 1.54E-01 l.18E-01

706.67 16.46 1.74E-01 -1.62E-02 7.82E-02

763.93 21.98 1.36E-01 7.90E-02 6. llE-02

884.67 21.98 1.22E-01 -3.25E-02 5.33E-02

1384.27 23.94 9.28E-02 9.65E-03 3.59E-02

CD-113M 263.70 0.02 9.06E+0l 9.06E+0l -1.21E-01 4.23E+0l

SN-113 255.12 1. 93 8.78E-01 3.04E-02 2.37E-02 4.03E-01

391.69 64. 90 3.04E-02 -6.90E-03 1.37E-02

TE-123M 159.00 84.10 2.l0E-02 2.l0E-02 9.71E-03 9.89E-03

SB-124 602.71 97.87 2.86E-02 2.86E-02 -1.66E-02 1.30E-02

645.85 7.26 3.30E-01 2.03E-01 l.46E-01

722.78 11.10 2.02E-01 -1.79E-02 8.73E-02

1691.02 49.00 6.62E-02 1.54E-02 2.71E-02

I-125 35.49 6.49 4. 96E-01 4. 96E-01 8.07E-02 2.32E-01

SB-125 176.33 6.89 2.37E-01 6.82E-02 2.80E-02 l.l0E-01

427.89 29.33 6.82E-02 -2.l0E-02 3.07E-02

463.38 10.35 2.18E-01 -1.29E-02 9.89E-02

600.56 17.80 1.64E-01 4.52E-02 7.46E-02

635.90 11.32 2.07E-01 3.54E-02 9.15E-02

SB-126 414.70 83.30 2.15E-02 2.15E-02 -1.61E-02 9.58E-03

666.33 99.60 2.69E-02 4.15E-03 1.21E-02

695.00 99.60 2.58E-02 -3.57E-03 1.14E-02

720 .50 53.80 4.36E-02 7.66E-03 1.90E-02

SN-126 87.57 37.00 4.50E-02 4.50E-02 -3.43E-02 2.13E-02

SB-127 473.00 25.00 9.64E-02 6.54E-02 -5.32E-02 4.32E-02

685.00 35.70 6.54E-02 -3.0lE-02 2.80E-02

783.80 14.70 2. llE-01 3.55E-02 9.28E-02

I-129 29.78 57.00 9.33E-02 9.33E-02 2.59E-02 4.40E-02

33.60 13.20 2.81E-0l -6.62E-02 l.32E-01

39.58 7.52 3.64E-01 4.63E-02 1.71E-01

I-131 284.30 6.05 3.09E-01 2.75E-02 -6.48E-02 1.41E-01

364.48 81.20 2.75E-02 1.82E-03 l.26E-02

636.97 7.26 3.64E-01 1.48E-01 l.62E-01

722.89 1. 80 1.33E+00 -l.18E-01 5.76E-01

TE-132 49. 72 13.10 1.60E-01 2.16E-02 -2.95E-01 7.45E-02

228.16 88.00 2.16E-02 -1.50E-03 9.91E-03

BA-133 81.00 33.00 5.12E-02 3.18E-02 -1.14E-02 2.42E-02

302.84 17.80 1.02E-01 -6.35E-02 4.65E-02

356.01 60.00 3.18E-02 -2.24E-02 1.44E-02

I-133 529.87 86.30 5.21E-02 5.21E-02 1.41E-03 2.33E-02

XE-133 81.00 38.00 5.00E-02 5.00E-02 -1. llE-02 2.36E-02

CS-134 563.23 8.38 2.36E-0l 3.13E-02 -2.03E-02 1.04E-01

569.32 15.43 1.lSE-01 -8.03E-02 4. 96E-02

604.70 97.60 3.15E-02 2.51E-03 1.44E-02

795.84 85.40 3.13E-02 3.49E-04 1.38E-02

801.93 8.73 3.08E-01 -2.06E-02 1.36E-01

CS-135 268.24 16.00 1.33E-01 l.33E-01 3.94E-02 6.19E-02

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Nuclide Energy Yield(¾) Line MDA Nuclide MDA Activity Dec. Level

Name (keV) (pCilgrams) (pCilgrams) (pCilgrams) (pCi!grams)

I-135 1131. 51 22.50 1.00E+00 8.56E-01 -8.57E-02 4.l0E-01

1260.41 28.60 8.56E-01 8.56E-02 3.51E-01

1678.03 9.54 2.55E+00 -4.77E-01 9.86E-01

CS-136 153.22 7.46 2.06E-01 2.94E-02 -1.23E-01 9.58E-02

163.89 4.61 3.60E-01 1.14E-01 1.68E-01

176.55 13.56 1.26E-01 1.49E-02 5.87E-02

273.65 12.66 1.73E-01 -1.l0E-02 8.06E-02

340.57 48.50 4.49E-02 -1.68E-02 2.06E-02

818.50 99.70 2.94E-02 -4.27E-04 1.30E-02

1048.07 79.60 4.05E-02 8.60E-03 1.76E-02

1235.34 19.70 1.18E-01 -8.09E-02 4.68E-02

CS-137 661.65 85.12 2.71E-02 2.71E-02 2.41E-03 1.19E-02

LA-138 788.74 34.00 7.99E-02 3.77E-02 -6.95E-03 3.53E-02

1435.80 66.00 3.77E-02 l.44E-02 1.49E-02

CE-139 165.85 80.35 1.83E-02 l.83E-02 -3.77E-03 8.46E-03

BA-140 162.64 6.70 2.54E-01 9.84E-02 3.81E-02 1.19E-01

304.84 4.50 4.24E-01 -1.56E-01 1.94E-01

423.70 3.20 7.39E-01 2.63E-01 3.37E-01

437.55 2.00 1.l0E+00 -1.43E-02 4.98E-01

537.32 25.00 9.84E-02 -2.98E-02 4.43E-02

LA-140 328.77 20.50 9.58E-02 2.43E-02 -4.05E-02 4.37E-02

487.03 45.50 5.49E-02 -5.08E-04 2.49E-02

815.85 23.50 1.06E-01 4.07E-03 4.55E-02

1596.49 95.49 2.43E-02 0.00E+00 9.09E-03

CE-141 145.44 48.40 3.46E-02 3.46E-02 -5.96E-03 1.62E-02

CE-143 57.36 11. 80 2.54E-01 7.48E-02 l.00E-01 1.20E-01

293.26 42.00 7.48E-02 -2. 96E-02 3.46E-02

664.55 5.20 8.08E-01 l.23E-01 3.62E-01

CE-144 133.54 10.80 1.30E-01 1.30E-01 -3.88E-02 6.04E-02

PM-144 476.78 42.00 5.18E-02 2.64E-02 -1.27E-02 2.33E-02

618.01 98.60 2.66E-02 -6.19E-03 1.20E-02

696.49 99.49 2.64E-02 4.52E-03 1.18E-02

PM-145 36.85 21.70 1.37E-01 7.54E-02 -4. 96E-02 6.39E-02

37.36 39.70 7.54E-02 -l.12E-02 3.54E-02

42.30 15.10 1.67E-01 -6.91E-02 7.85E-02

72.40 2.31 7.19E-01 -6.58E-02 3.39E-01

PM-146 453.90 39.94 5.56E-02 5.56E-02 -6.23E-03 2.52E-02

735.90 14.01 1.39E-01 -1.05E-01 5.87E-02

747.13 13.10 1.57E-01 -4.99E-02 6.67E-02

ND-147 91.11 28.90 8.97E-02 8.97E-02 1. 72E-01 4.32E-02

531.02 13.10 1. 78E-01 -1.40E-02 7.95E-02

PM-149 285.90 3.10 7.76E-01 7.76E-01 -2.09E-02 3.57E-01

EU-152 121.78 20.50 7. 13E-02 7.13E-02 2.83E-02 3.33E-02

244.69 5.40 3.04E-01 -1.36E-01 1.39E-01

344.27 19.13 1.17E-01 2.29E-02 5.42E-02

778.89 9.10 2.42E-01 -1.61E-01 1.04E-0l

964.01 10.40 2.85E-01 5.76E-02 1.24E-0l

1085.78 7.22 2.28E-01 -1.06E-02 8.52E-02

1112.02 9.60 2.94E-01 4.20E-02 1.25E-0l

1407.95 14.94 1.35E-01 -2.71E-02 5.04E-02

GD-153 97.43 31.30 5.03E-02 5.03E-02 -2.82E-02 2.37E-02

103.18 22.20 6.58E-02 3.28E-03 3.09E-02

EU-154 123.07 40.50 3.47E-02 3.47E-02 1.83E-03 1.62E-02

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Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level

Name (keV) (pCilgrams) (pCilgrams) (pCilgrams) (pCi/grams)

EU-154 723.30 19.70 l.13E-01 3.47E-02 -l.00E-02 4.87E-02

873.19 11. 50 2.24E-01 -3.98E-02 9.71E-02

996.32 10.30 2.51E-01 -l.26E-03 1.07E-01

1004.76 17.90 1.13E-01 -8.15E-02 4.57E-02

1274.45 35.50 5.25E-02 -2.84E-02 1. 96E-02

EU-155 86.50 30.90 5.55E-02 5.55E-02 1.18E-03 2.63E-02

105.30 20.70 7.02E-02 -l.83E-02 3.29E-02

EU-156 811.77 10.40 2.65E-01 2.65E-01 9.66E-02 l.16E-01

1153.47 7.20 3.67E-01 -5.79E-02 l.52E-01

1230.71 8.90 3.13E-01 5.77E-02 l.30E-01

HO-166M 184.41 72.60 3.04E-02 3.04E-02 3.07E-02 l.44E-02

280.45 29.60 5.86E-02 -1.50E-02 2.68E-02

410.94 11.10 1.83E-01 1.43E-02 8.29E-02

711.69 54.10 5.59E-02 5.66E-03 2.52E-02

TM-171 66.72 0.14 1.35E+0l 1.35E+0l -1.64E+0l 6.42E+00

HF-1 72 67.35 5.31 3.31E-01 1.29E-01 3.14E-02 l.56E-01

125.82 11. 30 1.29E-01 -2.58E-03 6.02E-02

LU-172 181.53 20.60 8.14E-02 5.07E-02 -1.87E-01 3.77E-02

900. 72 29.81 6.82E-02 -1.61E-03 2.76E-02

1093.66 62.50 5.07E-02 2.69E-03 2.17E-02

LU-173 100.72 5.24 2.98E-01 9.83E-02 -2.56E-03 l.40E-01

272.11 21.20 9.83E-02 -7.64E-03 4.58E-02

HF-175 343.40 84.00 2.69E-02 2.69E-02 5.25E-03 1.24E-02

LU-176 88.34 13. 30 1.26E-01 1.88E-02 -3.72E-01 5.98E-02

201.83 86.00 1.88E-02 -l.22E-02 8.73E-03

306.78 94.00 2.07E-02 6.87E-03 9.54E-03

HF-181 133.02 41.70 3.61E-02 2.64E-02 -9.00E-03 1.68E-02

345.85 17.20 1.33E-01 -5.79E-04 6.13E-02

482.03 82.80 2.64E-02 -1.07E-02 1.19E-02

TA-182 67.75 41.20 4.28E-02 4.28E-02 4.05E-03 2.02E-02

1121.30 34.90 7.86E-02 0.00E+00 3.32E-02

1189.05 16.23 l.53E-01 -2.76E-02 6.25E-02

1221.41 26.98 8.18E-02 -3.12E-03 3.25E-02

1231.02 11. 44 2.35E-01 7.40E-02 9.74E-02

IR-192 308.46 29.68 6.58E-02 4.56E-02 -4.07E-03 3.02E-02

468.07 48.10 4.56E-02 l.70E-04 2.06E-02

HG-203 279.19 77.30 2.51E-02 2.51E-02 6.45E-03 l.16E-02

TL-204 374.74 94 .11 1.99E-02 1.99E-02 -3.52E-03 8.98E-03

899.15 99.16 1.99E-02 3.97E-03 8.15E-03

911.74 91.10 2.64E-02 2.92E-03 1.12E-02

BI-207 569.67 97.72 1.82E-02 1.82E-02 -1.55E-02 7.83E-03

1063.62 74.90 2.41E-02 -1.30E-02 9.33E-03

TL-208 583.14 30.22 7.99E-02 7.99E-02 -5.60E-03 3.58E-02

860.37 4.48 4.93E-01 6.36E-02 2.08E-01

2614.66 35.85 1.30E-01 7.03E-02 5.45E-02

BI-210M 262.00 45.00 4.68E-02 4.68E-02 -4.19E-03 2.18E-02

300.00 23.00 8.59E-02 -1.25E-02 3. 96E-02

PB-210 46.50 4.25 5.55E-01 5.55E-01 3.72E-01 2.62E-01

PB-211 404.84 2.90 6.51E-01 6.51E-01 -3.48E-01 2.93E-01

831. 96 2.90 8.0lE-01 -1.83E-01 3.43E-01

BI-212 727.17 11. 80 1.70E-01 1.70E-01 -9.39E-02 7.24E-02

1620.62 2.75 1.13E+00 3.77E-01 4.64E-01

PB-212 238.63 44.60 4.68E-02 4.68E-02 4.19E-02 2.19E-02

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Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level

Name (keV) (pCi/grams) (pCilgrams) (pCilgrams) (pCilgrams)

PB-212 300.09 3.41 5.80E-01 4.68E-02 -8.40E-02 2.67E-01

BI-214 609.31 46.30 6.90E-02 6.90E-02 2.99E-02 3.17E-02

1120.29 15.10 1.36E-01 -1.04E-01 5.39E-02

1764.49 15.80 1.83E-01 6.97E-02 7.25E-02

2204.22 4.98 5.51E-01 -1.79E-01 2.06E-01

PB-214 295.21 19.19 1.12E-01 6.34E-02 1.37E-02 5.21E-02

351.92 37.19 6.34E-02 2.52E-02 2.94E-02

RN-219 401.80 6.50 3.16E-01 3.16E-01 -1.46E-02 1.44E-0l

RA-223 323.87 3.88 5.68E-01 5.68E-0l 2.78E-01 2.63E-01

RA-224 240.98 3.95 4.98E-01 4.98E-01 2. llE-01 2.32E-01

RA-225 40.00 31.00 9.04E-02 9.04E-02 1.15E-02 4.25E-02

RA-226 186.21 3.28 6.87E-01 6.87E-0l 9.60E-01 3.26E-0l

TI-l-227 50.10 8.40 2.17E-01 l.51E-01 -2.29E-02 1.0lE-01

236.00 11. 50 1.51E-01 -l.03E-01 6.97E-02

256.20 6.30 3.18E-01 -8.07E-03 1.48E-01

AC-228 338.32 11. 40 1.85E-01 9.02E-02 2.70E-03 8.52E-02

911.07 27. 70 9.02E-02 9.58E-03 3.86E-02

969.11 16.60 1.52E-01 -4.73E-02 6.48E-02

TI-l-230 48.43 16.90 1.16E-01 1.16E-0l -4.60E-02 5.42E-02

62.85 4.60 5.26E-01 3.63E-01 2.52E-01

67. 67 0.37 4.74E+00 4.49E-01 2.24E+00

PA-231 283.67 1. 60 1.08E+00 7.86E-01 -5.23E-02 4.94E-01

302. 67 2.30 7.86E-01 -4.91E-01 3.60E-01

TI-l-231 25.64 14.70 7.13E-01 2.77E-01 -5.91E+00 3.40E-01

84.21 6.40 2.77E-01 1.38E-01 1.31E-01

PA-233 311.98 38.60 5.73E-02 5.73E-02 -3.85E-03 2.66E-02

+ PA-234 131.20 * 20.40 6. 72E-02 6. 72E-02 4.40E-02 3.12E-02

733.99 8.80 2.55E-01 5.52E-02 l.l0E-01

946.00 12.00 1.81E-01 -5.70E-02 7.50E-02

PA-234M 1001.03 0.92 2.93E+00 2.93E+00 3.50E-01 1.25E+00

TH-234 63. 2 9 3.80 6.57E-01 6.57E-01 1.08E+00 3.15E-01

U-235 143.76 10.50 l.70E-01 l.70E-01 8.49E-02 8.02E-02

163.35 4.70 3.36E-01 1.06E-01 1.57E-01

205.31 4.70 3.77E-01 3.18E-02 1.76E-01

NP-237 86.50 12.60 1.36E-01 l.36E-01 2.89E-03 6.44E-02

NP-239 106.10 22. 70 8.18E-02 8.18E-02 -2.00E-02 3.83E-02

228.18 10.70 1.95E-01 -3.45E-03 8.97E-02

277.60 14.10 1.84E-01 1.0lE-01 8.54E-02

+ AM-241 59.54 * 35.90 7.75E-02 7.75E-02 1.92E-02 3.73E-02

AM-243 74.67 66.00 2.59E-02 2.59E-02 -7.05E-04 l.22E-02

CM-243 209.75 3.29 5.29E-01 1.43E-01 -1.13E-01 2.46E-01

228.14 10.60 1.48E-01 -1.03E-02 6.80E-02

277.60 14.00 1.43E-01 7. 81E-02 6.61E-02

+ = Nuclide identified during the nuclide identification

* = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

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0206

4/17/2018 7:13:55AM Page 23 of23

Analysis Report for 1803111-02

BLANK

No Action Level results available for reporting purposes.

DATA REVIEW COMMENTS REPORT

Creation Date Comment User

No Data Review Comments Entered.

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Channel Data Report 4/17/2018 7:14:12 AM Page 1

*******************************************************

***** S P E C T R A L D A T A R E P O R T *****

*******************************************************

Sample Title: BLANK

Elapsed Live time: 3600 Elapsed Real Time: 3600

Channel[------[-------[-------[-------[-------[-------[-------[-------[

1 : 0 0 0 0 0 0 0 0

9: 0 0 0 0 0 0 0 0

17: 0 0 27 36 49 247 476 70

25: 23 22 18 17 12 20 20 23

33: 14 13 15 15 17 14 13 21

41: 19 15 14 20 18 21 30 16

49: 13 9 5 17 24 13 15 20

57: 20 18 12 27 13 19 43 73

65: 32 27 19 14 23 16 18 17

73: 14 25 19 22 21 23 21 26

81: 14 20 21 22 24 22 25 19

89: 17 18 24 37 98 50 19 15

97: 20 13 27 14 17 13 16 21

105: 15 10 11 17 18 19 10 15

113: 15 8 15 12 17 20 17 13

121: 8 13 17 19 7 15 15 12

12 9: 12 14 21 20 9 9 9 13

137: 15 13 10 18 18 23 17 23

145: 17 15 13 11 16 16 18 10

153: 13 12 14 10 16 16 22 16

161: 14 10 16 15 14 10 6 9

169: 15 9 12 16 11 18 12 11

177: 14 15 12 8 12 16 13 5

185: 27 46 25 12 10 11 7 14

193: 4 12 10 7 13 16 14 7

201: 13 14 9 11 15 17 13 8

209: 10 15 10 17 9 16 15 13

217: 8 12 5 6 12 11 12 9

225: 8 8 7 8 9 11 10 9

233: 11 12 5 9 13 12 28 10

241: 12 5 10 8 9 7 9 14

249: 13 7 12 7 11 2 5 13

257: 12 7 8 15 7 11 10 7

265: 9 10 11 7 8 11 11 8

273: 7 8 9 10 9 12 6 3

281: 6 4 3 6 5 6 9 6

289: 8 9 6 6 6 7 12 9

297: 5 14 6 10 5 6 2 8

305: 4 4 5 10 9 5 6 5

313: 10 7 13 4 6 8 0 7

321: 11 11 7 7 9 5 4 6

329: 6 5 6 5 6 7 6 6

337: 9 6 8 7 4 6 7 6

345: 6 11 11 4 6 6 12 13

353: 6 5 7 2 7 4 3 6

361: 4 3 7 5 5 7 7 5

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Channel Data Report 4/17/2018 7:14:12 AM Page 2

369: 3 8 2 2 5 5 4 8

Sample Title: BLANK

Channell------l-------l-------l-------1-------1-------1-------I-------I

377: 2 4 6 4 2 11 6 5

385: 2 1 5 6 7 6 3 2

393: 4 5 4 6 11 3 6 4

401: 6 6 2 3 6 5 2 3

409: 4 9 7 1 4 3 1 8

417: 2 4 8 0 2 10 5 6

425: 4 6 4 4 3 2 5 3

433: 7 4 3 4 6 3 8 5

441: 1 2 5 5 6 5 4 3

44 9: 4 4 6 7 7 7 1 2

457: 2 4 3 6 6 5 3 7

465: 7 2 2 4 6 5 3 3

473: 4 4 6 0 7 5 1 5

481: 7 5 4 3 2 10 0 4

489: 8 6 5 5 3 3 2 3

497: 3 4 5 3 7 4 3 5

505: 4 2 1 4 8 13 32 13

513: 13 6 7 10 2 5 3 3

521: 3 3 4 3 4 1 3 5

52 9: 1 3 5 3 4 3 5 5

537: 3 7 2 2 6 6 1 3

545: 5 4 3 3 2 4 2 1

553: 2 2 4 4 1 1 5 4

561: 1 3 2 3 2 2 3 2

569: 2 2 1 1 2 7 4 2

577: 4 5 1 2 2 5 6 4

585: 4 2 3 6 2 2 5 2

593: 5 3 2 1 8 3 8 4

601: 4 7 6 4 3 4 6 10

60 9: 9 4 5 5 3 6 3 2

617: 5 4 3 2 8 3 7 1

625: 2 1 3 2 2 2 2 2

633: 2 4 1 3 5 4 1 4

641: 1 2 0 2 5 1 3 7

649: 2 0 0 3 3 1 3 0

657: 2 2 1 3 4 2 2 2

665: 4 7 5 3 2 3 3 3

673: 2 1 2 2 3 7 3 3

681: 6 2 1 2 4 0 3 0

689: 2 2 4 6 5 2 2 0

697: 2 4 7 2 3 2 3 2

705: 3 3 7 4 1 6 7 4

713: 4 6 1 4 1 1 2 4

721: 2 5 1 1 1 0 3 2

729: 2 2 2 4 1 1 3 2

737: 1 1 1 3 4 2 1 1

745: 2 2 3 1 0 2 3 3

753: 4 4 1 5 1 3 0 4

761: 6 2 3 3 2 5 4 1

7 69: 1 3 1 2 1 6 1 2

777: 1 2 3 0 2 2 2 5

785: 1 2 4 4 1 1 4 3

793: 3 3 6 0 2 2 2 0

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0209

Channel Data Report 4/17/2018 7:14:12 AM Page 3

801: 4 3 4 3 2 6 1 1

Sample Title: BLANK

Channell------l-------l-------l-------l-------l-------1-------1-------1

809: 3 2 2 3 2 3 2 1

817: 2 1 2 4 7 4 0 1

825: 2 4 3 1 3 0 2 5

833: 1 0 1 3 2 6 2 3

841: 3 4 5 4 3 2 6 4

849: 4 4 3 0 2 2 1 4

857: 1 0 0 6 2 1 0 0

865: 0 3 0 0 4 0 4 1

873: 1 3 3 2 2 4 2 2

881: 4 1 2 2 2 3 1 1

889: 6 0 2 1 1 1 0 2

897: 1 0 2 1 0 1 0 2

905: 5 1 4 1 2 3 3 0

913: 3 0 0 1 3 3 4 3

921: 1 1 2 1 2 2 4 1

929: 2 1 1 1 1 2 0 2

937: 1 5 3 3 3 1 2 3

945: 0 0 0 1 2 5 1 3

953: 3 2 2 2 2 3 3 2

961: 1 1 4 4 2 3 ·1 1

969: 1 2 3 0 2 2 1 1

977: 4 1 0 2 1 1 0 2

985: 0 1 0 1 2 0 2 0

993: 0 0 1 3 2 2 3 4

1001: 1 2 0 0 1 1 1 1

1009: 2 0 2 0 1 0 1 0

1017: 4 2 2 1 1 1 1 0

1025: 2 0 1 2 1 2 1 2

1033: 2 0 3 3 1 2 5 3

1041: 0 0 1 1 0 2 4 2

1049: 2 3 2 3 1 2 1 2

1057: 1 1 2 0 2 1 1 0

1065: 0 0 2 1 1 2 2 2

1073: 2 3 0 3 3 2 1 2

1081: 1 0 0 2 1 0 0 0

1089: 1 2 2 3 2 0 1 2

1097: 1 1 2 0 0 1 0 2

1105: 0 0 1 2 1 1 1 4

1113: 4 0 0 2 0 1 0 3

1121: 0 1 0 5 1 3 0 0

1129: 3 0 2 1 1 0 2 0

1137: 2 1 1 1 0 3 1 0

1145: 1 0 2 2 2 0 2 0

1153: 1 3 1 1 0 2 1 1

1161: 2 0 2 0 1 1 2 1

1169: 0 1 1 0 1 4 2 2

1177: 2 0 1 2 1 2 1 0

1185: 1 1 1 0 2 2 1 0

1193: 3 1 0 1 2 0 1 1

1201: 0 2 2 1 1 1 3 0

1209: 1 1 0 3 0 0 1 0

1217: 3 0 1 0 0 0 2 2

1225: 3 1 1 0 1 2 2 1

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Channel Data Report 4/17/2018 7:14:12 AM Page 4

1233: 1 1 1 0 1 0 1 3

Sample Title: BLANK

Channell------l-------l-------l-------l-------1-------1-------1-------I

1241: 0 3 2 1 0 1 1 1

1249: 0 2 2 1 4 1 0 2

1257: 1 1 0 0 1 1 3 0

1265: 1 0 2 1 0 2 0 0

1273: 1 0 2 0 0 2 1 3

1281: 0 3 0 1 1 0 0 0

1289: 1 1 0 1 1 0 0 3

1297: 0 1 2 0 1 0 1 1

1305: 1 2 0 0 1 0 0 1

1313: 0 1 1 0 0 1 1 0

1321: 5 1 0 1 2 0 0 3

1329: 1 0 0 1 1 1 2 0

1337: 0 0 0 0 0 1 0 0

1345: 0 1 1 1 0 1 1 0

1353: 1 1 0 0 1 0 0 1

1361: 0 0 1 0 1 1 2 2

1369: 1 2 1 0 2 1 1 1

1377: 3 1 1 1 1 1 0 0

1385: 1 0 1 0 0 1 1 0

1393: 3 2 1 1 5 3 1 1

1401: 1 2 0 1 0 0 0 1

1409: 0 1 1 0 0 0 0 0

1417: 2 0 0 2 0 1 0 0

1425: 2 2 0 1 0 0 0 1

1433: 2 0 0 1 0 1 0 0

1441: 0 0 0 2 0 0 3 1

1449: 1 0 0 1 0 1 1 1

1457: 2 0 5 0 2 0 3 0

1465: 0 2 0 0 1 0 0 1

1473: 0 2 0 1 0 0 0 1

1481: 0 0 0 0 0 1 0 1

1489: 2 0 1 0 1 0 1 1

14 97: 1 0 0 1 1 0 3 0

1505: 0 0 1 1 1 1 2 3

1513: 1 0 1 2 0 0 0 1

1521: 0 0 1 0 1 0 1 0

1529: 1 0 0 0 2 3 1 1

1537: 0 1 0 0 0 0 0 0

1545: 0 2 0 3 1 1 0 0

1553: 1 1 0 1 1 1 1 1

1561: 0 0 0 0 1 0 2 2

1569: 0 0 1 0 1 0 0 0

1577: 1 0 2 1 0 0 0 0

1585: 2 1 1 1 0 0 0 2

1593: 0 0 1 1 1 0 0 0

1601: 0 1 1 0 0 1 0 1

1609: 2 2 1 1 0 1 1 0

1617: 0 1 1 0 2 1 2 0

1625: 0 0 0 1 0 0 1 0

1633: 2 1 1 0 0 3 0 0

1641: 1 0 0 0 1 0 0 1

1649: 0 0 0 0 2 2 0 0

1657: l 2 1 0 0 0 0 1

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Channel Data Report 4/17/2018 7:14:12 AM Page 5

1665: 1 2 0 1 0 0 0 2

Sample Title: BLANK

Channell------l-------l-------l-------l-------l-------1-------1-------1

1673: 1 1 1 0 0 1 0 1

1681: 0 1 0 1 0 1 1 0

1689: 0 2 2 1 1 0 1 2

1697: 2 0 0 3 0 0 0 0

1705: 1 1 0 2 0 0 0 0

1713: 1 0 1 0 0 0 1 1

1721: 0 2 0 0 0 1 0 1

1729: 1 0 0 0 0 0 1 1

1737: 0 0 0 0 1 1 0 2

1745: 0 0 0 0 1 1 2 0

1753: 0 0 1 1 0 2 0 0

1761: 1 0 0 2 2 0 0 0

1769: 0 0 0 0 0 0 0 1

1777: 0 0 0 2 0 1 1 0

1785: 0 1 0 0 0 0 1 0

1793: 0 1 1 1 0 0 0 0

1801: 0 2 0 0 0 1 1 1

1809: 3 2 0 4 1 3 0 0

1817: 0 0 2 0 0 1 0 1

1825: 0 0 1 1 1 0 0 0

1833: 2 1 0 1 0 0 2 0

1841: 2 0 1 1 0 0 0 0

1849: 0 0 0 1 0 1 0 1

1857: 1 0 1 0 1 0 0 1

1865: 2 1 0 1 0 0 1 0

1873: 1 1 0 0 1 2 0 0

1881: 0 1 0 1 1 1 0 0

1889: 1 0 0 0 0 2 1 0

1897: 1 0 0 1 0 0 0 0

1905: 1 2 0 0 0 0 0 1

1913: 0 0 0 2 0 1 1 2

1921: 0 1 0 0 1 1 0 0

192 9: 2 0 0 1 0 0 0 4

1937: 0 0 0 0 0 0 0 0

1945: 0 0 1 0 1 2 0 0

1953: 0 0 0 0 1 0 1 2

1961: 1 0 1 2 0 0 3 0

1969: 2 1 0 0 1 1 0 2

1977: 3 1 1 0 3 1 1 0

1985: 0 0 0 0 0 0 0 1

1993: 0 0 0 1 1 1 1 0

2001: 0 0 0 1 0 0 0 0

2009: 1 1 0 0 0 0 0 0

2017: 0 1 0 0 0 4 0 1

2025: 0 0 0 1 1 0 1 1

2033: 0 1 0 0 0 0 0 1

2041: 1 1 0 0 0 0 0 1

2049: 1 0 0 0 1 0 0 0

2057: 0 1 0 0 0 0 0 1

2065: 0 0 1 0 0 0 0 0

2073: 0 1 1 0 1 1 0 0

2081: 1 0 1 1 1 0 1 0

2089: 0 2 0 0 0 0 1 0

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Channel Data Report 4/17/2018 7:14:12 AM Page 6

2097: 0 0 0 0 0 0 0 1

Sample Title: BLANK

Channell------l-------1-------1-------1-------1-------I-------I-------I

2105: 0 0 0 1 0 0 1 1

2113: 0 0 2 0 0 1 2 0

2121: 0 0 1 0 0 1 0 0

212 9: 0 0 0 1 1 0 0 0

2137: 1 0 0 1 0 0 0 0

2145: 0 0 1 0 0 1 0 0

2153: 0 0 1 0 0 1 0 0

2161: 0 0 0 0 0 1 0 0

2169: 1 0 0 0 0 1 2 1

2177: 0 2 0 0 1 0 0 0

2185: 1 0 0 0 0 0 0 1

2193: 0 0 0 0 1 0 0 0

2201: 0 0 1 1 1 0 0 1

2209: 1 0 0 1 1 1 0 0

2217: 0 0 1 0 0 1 0 0

2225: 0 0 1 1 0 0 0 0

2233: 0 0 0 0 0 0 1 0

2241: 0 0 0 0 0 0 0 0

2249: 0 0 0 4 0 1 0 0

2257: 1 1 0 0 0 1 2 1

2265: 1 0 0 0 0 1 1 1

2273: 0 0 0 0 0 2 0 0

2281: 0 0 0 0 0 0 1 0

2289: 1 0 0 0 0 1 0 2

2297: 1 0 0 0 0 0 0 1

2305: 0 0 0 1 0 0 3 0

2313: 1 1 0 0 0 1 0 0

2321: 0 0 0 0 0 2 0 0

2329: 0 0 1 2 0 0 0 0

2337: 0 0 0 0 0 0 1 0

2345: 1 0 0 0 1 1 0 0

2353: 0 0 1 0 1 0 0 0

2361: 2 0 1 0 2 0 0 1

2369: 0 1 0 1 1 0 0 0

2377: 0 0 1 0 0 0 0 0

2385: 0 0 0 0 0 0 0 0

2393: 0 1 0 1 0 0 0 0

2401: 0 0 0 0 1 2 1 1

2409: 1 0 0 0 0 0 0 1

2417: 0 1 0 0 2 1 0 0

2425: 1 1 1 0 1 0 2 2

2433: 0 0 1 0 0 0 0 0

2441: 0 0 0 0 1 0 0 0

2449: 0 1 0 0 0 0 0 0

2457: 0 0 0 1 0 1 0 0

2465: 0 1 0 0 0 0 0 0

2473: 0 0 0 0 1 0 1 0

2481: 0 1 0 1 0 1 0 0

2489: 2 0 0 1 0 0 0 0

2497: 0 0 0 0 0 1 0 0

2505: 0 0 0 0 0 0 0 0

2513: 0 0 0 0 0 1 1 0

2521: 0 1 1 0 0 0 0 0

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Channel Data Report 4/17/2018 7:14:12 AM Page 7

2529: 1 1 0 0 0 0 0 0

Sample Title: BLANK

Channell------l-------l-------l-------l-------l-------1-------1-------1

2537: 0 1 0 0 0 0 0 0

2545: 1 0 0 0 0 0 0 0

2553: 2 0 0 1 1 0 0 0

2561: 1 0 1 0 0 1 0 0

2569: 0 0 0 0 0 0 0 0

2577: 1 1 0 0 1 0 1 1

2585: 0 0 0 1 0 0 0 1

2593: 0 1 0 1 0 0 0 0

2601: 0 1 0 2 0 2 0 0

2609: 0 0 0 0 2 5 0 1

2617: 0 1 0 0 1 1 0 1

2625: 0 0 0 0 0 0 0 0

2633: 0 0 0 0 1 0 0 0

2641: 0 0 1 0 0 0 0 2

2649: 0 0 0 0 1 0 1 1

2657: 0 0 0 0 0 0 0 0

2665: 0 0 0 0 0 0 1 0

267 3: 0 1 0 0 0 0 0 0

2681: 0 1 0 0 0 0 2 0

2 68 9: 0 0 0 1 0 0 0 0

2697: 0 0 0 1 0 0 0 0

2705: 0 0 0 0 2 0 0 2

2713: 0 0 0 0 2 0 0 0

2721: 0 1 0 0 0 0 0 0

2729: 0 0 1 0 0 0 0 0

2737: 0 0 0 0 0 0 0 0

2745: 0 0 2 0 0 0 1 0

2753: 0 0 0 0 0 0 0 0

2761: 0 1 0 0 0 0 0 1

2769: 1 0 1 0 1 0 0 0

2777: 0 1 0 0 0 0 0 0

2785: 0 0 0 0 0 0 1 0

2793: 0 0 1 0 0 0 0 1

2801: 0 0 0 0 0 0 1 0

2809: 0 0 0 0 1 1 0 0

2817: 0 1 0 1 1 0 1 1

2825: 0 1 0 0 0 0 0 2

2833: 0 1 0 0 0 0 0 0

2841: 1 0 2 0 0 0 0 2

2849: 0 2 0 0 0 0 0 0

2857: 0 1 1 0 0 0 0 0

2865: 1 0 0 0 1 0 0 0

2873: 0 0 0 0 0 0 0 0

2881: 1 0 0 0 0 1 0 0

2889: 0 0 0 0 0 0 0 0

2897: 0 1 0 0 1 0 0 0

2905: 0 1 0 0 0 0 1 0

2913: 0 0 0 0 0 0 1 0

2921: 1 1 1 1 2 1 0 0

292 9: 0 1 0 0 0 0 0 1

2937: 0 0 0 0 0 1 0 0

2945: 0 0 0 0 0 0 0 1

2953: 0 0 0 3 0 0 0 0

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Channel Data Report 4/17/2018 7:14:12 AM Page 8

2961: 0 0 0 1 1 0 0 0

Sample Title: BLANK

Channell------l-------1-------1-------1-------I-------I-------I-------I

2969: 0 0 1 0 0 0 0 1

2977: 0 0 0 0 0 0 0 0

2985: 0 0 0 0 1 0 0 0

2993: 0 0 0 0 1 1 0 0

3001: 0 0 0 0 0 0 0 0

3009: 2 0 0 0 0 0 0 0

3017: 0 0 0 1 0 1 0 0

3025: 0 1 0 0 0 0 0 1

3033: 1 0 0 0 0 1 0 0

3041: 1 0 0 0 0 0 1 0

3049: 0 0 0 0 0 1 0 0

3057: - 0 0 0 0 0 0 0 0

3065: 0 0 0 0 0 0 0 0

3073: 0 1 0 1 0 1 0 0

3081: 0 0 1 0 0 0 0 0

3089: 0 0 0 0 0 0 0 0

3097: 0 0 0 0 0 0 0 0

3105: 0 0 0 0 0 1 0 0

3113: 0 0 0 0 0 0 0 1

3121: 0 0 0 0 0 0 0 0

3129: 0 0 1 0 0 0 0 0

3137: 1 0 0 1 0 1 0 0

3145: 0 0 0 0 0 0 1 0

3153: 0 0 0 0 0 0 0 0

3161: 0 0 0 0 0 0 0 0

3169: 0 1 1 0 0 0 0 0

3177: 0 0 0 1 0 0 0 0

3185: 0 1 0 0 0 0 1 0

3193: 0 0 0 0 0 0 0 0

3201: 0 1 0 0 0 0 0 0

3209: 0 0 0 0 0 0 0 0

3217: 0 0 0 0 0 0 0 0

3225: 0 0 0 2 0 0 0 2

3233: 0 0 1 0 0 2 1 1

3241: 0 0 0 0 1 0 0 1

3249: 0 0 0 0 0 0 0 0

3257: 2 0 0 0 0 0 0 0

3265: 0 0 0 1 0 0 0 0

3273: 0 0 0 0 1 0 1 2

3281: 0 0 0 1 0 0 0 1

3289: 0 0 1 0 0 0 0 0

3297: 0 0 1 0 0 0 0 0

3305: 0 0 1 0 0 0 1 0

3313: 0 0 1 0 0 0 0 0

3321: 0 0 0 0 0 0 0 0

3329: 0 0 0 0 1 0 0 1

3337: 0 0 0 0 0 0 0 0

3345: 0 0 1 0 1 1 0 0

3353: 0 1 0 0 0 0 0 0

3361: 0 0 0 0 0 0 0 0

3369: 0 0 0 1 0 1 0 0

3377: 0 0 0 0 0 0 0 1

3385: 0 0 0 0 0 0 1 1

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Channel Data Report 4/17/2018 7:14:12 AM Page 9

3393: 0 0 0 0 0 0 0 0

Sample Title: BLANK

Channell------l-------l-------1-------1-------1-------I-------I-------I

3401: 0 1 0 1 0 0 0 0

3409: 0 0 0 0 0 0 0 0

3417: 0 0 0 0 0 0 0 1

3425: 1 0 0 0 1 0 0 0

3433: 0 0 0 0 0 0 0 1

3441: 0 0 1 1 1 0 0 0

3449: 1 0 0 0 0 0 1 0

3457: 0 0 0 0 0 1 0 0

3465: 0 0 1 0 0 0 0 0

3473: 1 0 1 1 0 0 1 0

3481: 0 0 0 0 0 0 1 0

3489: 0 0 0 0 0 0 0 0

3497: 0 0 0 0 0 0 1 0

3505: 0 0 0 0 1 0 0 0

3513: 1 0 1 0 0 0 0 0

3521: 0 0 1 0 0 0 0 0

3529: 0 0 0 0 0 0 0 0

3537: 1 0 1 0 1 0 0 0

3545: 0 0 0 0 0 0 1 0

3553: 0 0 0 0 1 0 0 0

3561: 0 0 0 1 0 0 0 0

3569: 0 0 0 0 0 1 1 0

3577: 0 0 0 0 0 0 0 0

3585: 0 0 0 0 0 0 0 1

3593: 0 0 0 0 0 0 1 0

3601: 0 0 1 1 0 0 0 1

3609: 0 0 0 0 0 1 0 0

3617: 0 0 0 0 0 0 0 0

3625: 0 0 0 0 0 0 0 0

3633: 0 0 0 0 1 0 0 1

3641: 0 0 0 0 0 0 0 0

3649: 0 0 0 0 0 0 0 0

3657: 0 0 0 0 0 1 0 0

3665: 0 0 0 0 0 0 0 0

367 3: 0 0 0 0 0 0 0 0

3681: 0 0 0 0 0 0 1 0

3689: 0 0 0 0 0 0 0 0

3697: 0 0 0 0 0 1 0 1

3705: 0 1 0 0 0 1 0 0

3713: 0 0 0 1 0 0 0 0

3721: 0 0 0 0 0 0 1 0

372 9: 1 0 0 0 1 0 0 1

3737: 0 0 0 0 0 0 0 0

3745: 1 1 0 0 0 0 0 0

3753: 0 0 0 0 0 0 0 0

3761: 1 0 1 0 1 0 0 0

3769: 0 1 1 0 0 0 0 0

3777: 1 0 0 0 1 0 0 0

3785: 0 1 0 0 0 0 1 0

3793: 0 0 0 0 1 0 1 0

3801: 0 0 0 0 0 0 1 0

3809: 0 0 0 0 0 0 0 1

3817: 0 0 0 0 0 0 0 2

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Channel Data Report 4/17/2018 7:14:12 AM Page 10

3825: 1 0 1 0 0 0 0 0

Sample Title: BLANK

Channell------l-------1-------1-------1-------I-------I-------I-------I

3833: 0 0 1 0 1 0 0 0

3841: 0 0 0 0 0 0 1 0

384 9: 1 0 0 0 0 1 1 0

3857: 0 0 0 0 0 0 0 0

3865: 0 0 0 0 0 0 0 0

3873: 0 0 1 0 0 1 0 1

3881: 0 0 0 0 0 0 1 0

3889: 0 0 0 0 0 1 0 0

3897: 0 0 0 0 0 0 0 0

3905: 0 0 0 0 0 0 1 0

3913: 0 1 0 0 0 0 0 0

3921: 0 1 0 0 0 0 0 0

3929: 0 0 0 0 0 1 0 0

3937: 0 0 0 0 0 0 1 0

3945: 0 0 0 0 0 0 0 0

3953: 0 1 1 1 0 0 0 0

3961: 0 0 0 0 0 0 0 0

3969: 0 0 0 0 0 0 0 0

3977: 0 0 0 0 0 0 1 3

3985: 0 0 0 0 0 0 0 0

3993: 0 0 0 0 0 0 0 0

4001: 0 0 1 0 0 0 0 0

4009: 0 1 0 1 0 0 0 1

4017: 0 0 0 0 0 0 0 0

4025: 0 0 0 0 0 0 0 0

4033: 0 0 0 0 0 0 0 0

4041: 0 1 0 0 0 0 0 0

4049: 0 0 0 0 0 0 1 0

4057: 0 0 0 0 0 0 0 0

4065: 0 0 0 0 0 0 0 0

4073: 0 0 0 1 0 0 0 0

4081: 0 0 0 0 0 1 0 0

4089: 0 0 0 0 0 0 0 0

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0217

105

104

~ 103 !"CS u V)

O"'I 0 .­

I V)

+-J s:::: :::s 0 u

102

101

0000064640. CNF Live Time :3600.000 sec Real Time :3600.400 sec Start: 1: 0.S(kev) stop : 4096:4096.9(kev) Acq. Start :Tue Apr 17 06:13:43 2018

100 l!Pi\111\ a in~ o 11'.' 11 '·~I I PM qn11 111 11111wm11n11111rnumi111rnnurnm1nu11mw11u1rnumn1mq11 lUll HI rnq1rn11111rn1 DI n unn mmn 11111 iun 10 1 1w11 111 t l 1 1n H\ 1

500 1000

~ ROI Type: 1

1500 2000 channel

2500 3000 r-:;:::m ~

ROI Type: 2

3500 4000

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0218

4/17/2018 6:43:09AM

pex- amm Analysis Report for 1803111-03

AC-SED-11

GAMMA SPECTRUM ANALYSIS

Sample Identification

Sample Description

Sample Type

Sample Size

Facility

Sample Taken On

Acquisition Started

Procedure

Operator

Detector Name

Geometry

Live Time

Real Time

Dead Time

Peak Locate Threshold

Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance

Energy Calibration Used Done On

Efficiency Calibration Used Done On

Efficiency Calibration Description

Sample Number

: 1803111-03

: AC-SED-11

: SOIL

: 4.763E+02 grams

: Countroom

: 3/21/2018 9:15:20AM

: 4/17/2018 5:42:57AM

: GAS-1602 pCi

: Administrator

: GE2

: GAS-1602

: 3600.0 seconds

: 3600.8 seconds

: 0.02 %

: 2.50

: 1 - 4096

: 28 - 4096

: 1.000 keV

: 2/17/2018

: 2/17/2018

: 64639

PEAK-TO-TOTAL CALIBRATION REPORT

Peak-to-Total Efficiency Calibration Equation

Pagel of29 ~p 1//!'1/J8

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0219

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Analysis Report for 1803111-03

AC-SED-11

PEAK LOCATE REPORT

Peak No.

1 2 3 4 5 6 7 8 9

10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42

Peak Locate Performed on

Peak Locate From Channel

Peak Locate To Channel

Peak Search Sensitivity

Energy (ke V)

47.14 76.59 93.65 99.87

185.97 239.38 277.51 295.46 302.20 338.95 352.20 408.80 463.05 477.97 511.42 563.56 583.18 609.34 663.21 750.47 766.58 771.59 795.62 860.86 911.33 932.18 950.24 969.18

1003.27 1098.74 1120.52 1237.76 1327.57 1335.60 1352.42 1377.95 1457.14 1460.90 1510.18 1589.70 1597.80 1639.41

: 4/17/2018 6:43:01 AM

: 1 : 4096 : 2.50

Centroid Channel

46.92 76.35 93.40 99.63

185.68 239.06 277.18 295.12 301.86 338.59 351.83 408.40 462.62 477.54 510.97 563.08 582.70 608.84 662.69 749.89 766.00 771.00 795.02 860.22 910.66 931. 50 949.55 968.48

1002.55 1097.96 1119.73 1236.91 1326.66 1334.67 1351.49 1377.01 1456.14 1459.90 1509.15 1588.61 1596.71 1638.29

Centroid Uncertainty

0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000

Page 2 of 29

Peak Significance

0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00

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0220

Analysis Report for 1803111-03

Peak No.

43 44 45 46 47 48 49 50 51 52

AC-SED-11

Energy (ke V)

1662.23 1729.66 1739.41 1764. 67 1832.00 1887.19 1894.20 2027.45 2203.96 2614.32

? = Adjacent peak noted

Errors quoted at 2.000sigma

Centroid Channel

1661.09 1728.48 1738.22 1763.46 1830.75 1885.90 1892.90 2026.06 2202.44 2612.47

4/17/2018 6:43:09AM

Centroid Uncertainty

0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000

Page 3 of 29

Peak Significance

0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00

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Analysis Report for 1803111-03

AC-SED-11

PEAK ANAL YS/S REPORT

Peak Analysis Performed on : 4/17/2018 6:43:01AM

Peak Analysis From Channel : 1

Peak Analysis To Channel : 4096

Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM

No. (keV) start end Centroid Area Uncertainty Counts (keV)

1 47.14 4 4 - 49 46.92 1.21E+02 58.34 5.78E+02 1. 43

2 76.59 72 - 81 76.35 6.37E+02 116.04 l.53E+03 3.04

3 93.65 91 - 96 93.40 1.40E+02 70.29 8.21E+02 1. 67

4 99.87 97 - 104 99.63 8.19E+0l 70.54 7.80E+02 2.33

5 185.97 181 - 190 185.68 1.64E+02 79.46 8.05E+02 1. 55

6 239.38 234 - 244 239.06 7.01E+02 83.70 5.58E+02 1. 93

7 277.51 27 4 - 281 277.18 5.27E+0l 46.35 3.13E+02 2.35

M 8 295.46 2 91 - 306 295.12 2.16E+02 40.73 1.78E+02 1. 52

m 9 302.20 2 91 - 306 301.86 2.86E+0l 29.65 1.45E+02 1. 53

10 338.95 335 - 343 338.59 1.09E+02 52.38 3.44E+02 1. 79

11 352.20 348 - 355 351.83 3.47E+02 55.79 2.87E+02 1. 42

12 408.80 406 - 411 408.40 2.60E+0l 28.18 1.38E+02 1. 79

13 463.05 4 60 - 466 4 62. 62 3.59E+0l 29.62 l.34E+02 1. 54

14 477.97 4 7 4 - 480 477.54 3.32E+0l 29.42 1.34E+02 2.08

15 511.42 506 - 516 510.97 1.28E+02 41. 25 1.56E+02 2.38

16 563.56 5 61 - 567 563.08 2.09E+0l 23.54 8.82E+0l 1. 96

17 583.18 57 8 - 587 582.70 1.66E+02 43.91 l.82E+02 1. 57

18 609.34 604 - 613 608.84 2.78E+02 46.89 1.56E+02 1. 4 9

19 663.21 657 - 668 662.69 7.14E+01 37.20 1.35E+02 1. 96

20 750.47 7 4 6 - 755 749.89 2.52E+01 28.35 1.02E+02 3.83

M 21 766.58 7 63 - 774 766.00 2.24E+0l 17.27 4.l0E+0l 1. 79

m 22 771.59 763 - 774 771.00 1.63E+0l 19.03 4.36E+0l 1. 7 9

23 795.62 7 92 - 798 795.02 3.24E+0l 22 .11 6.32E+0l 3.25

24 860.86 858 - 863 860.22 2.05E+0l 17.55 4.l0E+0l 2.28

25 911. 33 907 - 913 910.66 9.16E+0l 27. 74 7.27E+0l 1. 74

26 932.18 927 - 938 931.50 3.28E+01 27. 57 8.04E+0l 3.59

27 950.24 94 8 - 952 949.55 1.23E+0l 13. 67 3.15E+0l 2.20

28 969.18 966 - 971 968. 48 4.36E+01 25.73 9.08E+0l 2.26

29 1003.27 994 - 1009 1002.55 4.35E+01 32.37 8.49E+0l 7.38

30 1098.74 1095 - 1103 1097.96 1.66E+01 21. 24 6.08E+0l 3.16

31 1120.52 1116 - 1125 1119.73 3.29E+01 28.77 9.82E+0l 1. 95

32 1237.76 1233 - 1240 1236.91 2.39E+0l 23.41 7.42E+0l 1. 75

33 1327.57 1324 - 1329 1326.66 7.50E+00 8.66 9.00E+00 1. 40

34 1335.60 1330 - 1340 1334.67 2.87E+0l 17.87 2.66E+0l 3.57

35 1352.42 134 7 - 1355 1351.49 1.30E+0l 14.04 2.20E+0l 4. 87

36 1377.95 1373 - 1382 1377.01 2.50E+0l 20.32 4.41E+0l 1. 28

M 37 1457.14 14 53 - 1463 1456.14 1.23E+0l 18.22 2.95E+0l 3.20

m 38 1460.90 1453 - 1463 1459.90 4.57E+02 45.12 2.34E+0l 2.12

39 1510.18 1505 - 1512 1509.15 1.31E+0l 14.00 2.38E+0l 1. 27

40 1589.70 1584 - 1593 1588.61 1.35E+01 14.73 1.89E+0l 4. 91

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0222

Analysis Report for 1803111-03

AC-SED-11

Peak Energy ROI

No. (keV) start

41 1597.80 1594 -42 1639.41 1635 -43 1662.23 1657 -44 1729.66 1724 -45 1739.41 1 735 -46 1764.67 1760 -47 1832.00 1827 -48 1887.19 1881 -49 1894.20 1890 -50 2027.45 2023 -51 2203. 96 2199 -52 2614.32 2607 -

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet

Errors quoted at 2.000sigma

ROI end

1600 1641 1665 1732 1740 1768 1834 1889 1895 2028 2207 2617

4/17/2018 6:43:09AM Page 5 of 29

Peak Net Peak Net Area Continuum FWHM

Centroid Area Uncertainty Counts (keV)

1596.71 6.94E+00 6.95 4. llE+00 1. 59

1638.29 7.50E+00 8.28 7.00E+00 1. 31

1661.09 1.l0E+0l 6.63 0.00E+00 3.22

1728.48 9.50E+00 9.82 9.00E+00 1. 78

1738.22 5.13E+00 7.07 5.75E+00 1. 84

1763.46 3.50E+0l 16.03 1.80E+0l 2.45

1830.75 8.00E+00 5.66 0.00E+00 1.16

1885.90 6. 72E+00 7.50 4.56E+00 2.98

1892.90 1.00E+0l 6.32 0.00E+00 3.65

2026.06 4.50E+00 5.74 3.00E+00 2. 72

2202.44 2.50E+0l 10.00 0.00E+00 4.29

2612.47 5.50E+0l 14.83 0.00E+00 2.25

PEAK ANAL YS/S REPORT

Peak Analysis Performed on : 4/17/2018 6:43:01AM

Peak Analysis From Channel : 1

Peak Analysis To Channel : 4096

Peak Energy ROI ROI Net Peak Net Area Continuum Critical

No. (keV) start end Area Uncertainty Counts Level

1 47.14 44 - 49 1.21E+02 58.34 5.78E+02 4.44E+0l

2 76.59 72 - 81 6.37E+02 116.04 1.53E+03 8.59E+0l

3 93.65 91 - 96 1.40E+02 70.29 8.21E+02 5.44E+0l

4 99.87 97 - 104 8.19E+0l 70.54 7.80E+02 5.60E+0l

5 185.97 181 - 190 1.64E+02 79.46 8.05E+02 6.18E+0l

6 239.38 234 - 244 7.01E+02 83.70 5.58E+02 5.33E+0l

7 277.51 274 - 281 5.27E+0l 46.35 3.13E+02 3.62E+0l

M 8 295.46 2 91 - 306 2.16E+02 40.73 1.78E+02 2.19E+0l

m 9 302.20 2 91 - 306 2.86E+0l 29.65 1.45E+02 1.98E+0l

10 338.95 335 - 343 1.09E+02 52.38 3.44E+02 3.95E+0l

11 352.20 348 - 355 3.47E+02 55.79 2.87E+02 3.42E+0l

12 408.80 40 6 - 411 2.60E+0l 28.18 1.38E+02 2.16E+0l

13 463.05 460 - 466 3.59E+0l 29.62 1.34E+02 2.23E+0l

14 477.97 4 7 4 - 480 3.32E+0l 29.42 1.34E+02 2.23E+0l

15 511.42 506 - 516 l.28E+02 41. 25 l.56E+02 2.84E+0l

16 563.56 561 - 567 2.09E+0l 23.54 8.82E+0l 1.78E+0l

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0223

Analysis Report for 1803111-03

M

m

M

m

AC-SED-11

Peak Energy ROI

No. (keV) start

17 583.18 578 -

18 609.34 604 -19 663.21 657 -20 750.47 74 6 -21 766.58 763 -22 771.59 7 63 -23 795.62 7 92 -24 860.86 858 -25 911.33 907 -26 932.18 927 -27 950.24 948 -28 969.18 966 -29 1003.27 994 -30 1098.74 1095 -31 1120.52 1116 -32 1237.76 1233 -33 1327.57 1324 -34 1335.60 1330 -35 1352.42 134 7 -36 1377.95 1373 -37 1457.14 1453 -38 1460.90 1453 -39 1510.18 1505 -40 1589.70 1584 -41 1597.80 1594 -42 1639.41 1635 -43 1662.23 1657 -44 1729.66 1724 -45 1739.41 1 735 -46 1764.67 17 60 -47 1832.00 1827 -48 1887.19 1881 -49 1894.20 1890 -50 2027.45 2023 -51 2203.96 2199 -52 2614.32 2607 -

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet Errors quoted at 2.000sigma

ROI end

587 613 668 755 774 774 798 863 913 938 952 971

1009 1103 1125 1240 1329 1340 1355 1382 1463 1463 1512 1593 1600 1641 1665 1732 1740 17 68 1834 1889 1895 2028 2207 2617

4/17/2018 6:43:09AM Page 6 of 29

Net Peak Net Area Continuum Critical

Area Uncertainty Counts Level

1.66E+02 43. 91 1.82E+02 2.92E+Ol

2.78E+02 46.89 l.56E+02 2.71E+Ol

7.14E+Ol 37.20 l.35E+02 2.72E+Ol

2.52E+Ol 28.35 1.02E+02 2.18E+Ol

2.24E+Ol 17. 27 4.lOE+Ol 1.05E+Ol

1.63E+Ol 19.03 4.36E+Ol 1.09E+Ol

3.24E+Ol 22 .11 6.32E+Ol 1.56E+Ol

2.05E+Ol 17.55 4.lOE+Ol 1.24E+Ol

9.16E+Ol 27. 74 7.27E+Ol 1.65E+Ol

3.28E+Ol 27.57 8.04E+Ol 2.06E+Ol

1.23E+Ol 13.67 3.15E+Ol 9.66E+OO

4.36E+Ol 25.73 9.08E+Ol l.82E+Ol

4.35E+Ol 32.37 8.49E+Ol 2.43E+Ol

1.66E+Ol 21. 24 6.08E+Ol l.61E+Ol

3.29E+Ol 28.77 9.82E+Ol 2.17E+Ol

2.39E+Ol 23.41 7.42E+Ol 1.75E+Ol

7.50E+OO 8.66 9.00E+OO 5.51E+OO

2.87E+Ol 17.87 2.66E+Ol 1.18E+Ol

1.30E+Ol 14.04 2.20E+Ol 9.91E+OO

2.50E+Ol 20.32 4.41E+Ol l.45E+Ol

1.23E+Ol 18.22 2.95E+Ol 8.94E+OO

4.57E+02 45.12 2.34E+Ol 7.95E+OO

1.31E+Ol 14.00 2.38E+Ol 9.85E+OO

1.35E+Ol 14.73 1.89E+Ol 1.05E+Ol

6.94E+OO 6.95 4.llE+OO 3.72E+OO

7.50E+OO 8.28 7.00E+OO 5.lOE+OO

l.lOE+Ol 6.63 O.OOE+OO O.OOE+OO

9.50E+OO 9.82 9.00E+OO 6.29E+OO

5.13E+OO 7.07 5.75E+OO 4.46E+OO

3.50E+Ol 16.03 1.80E+Ol 8.89E+OO

8.00E+OO 5.66 O.OOE+OO O.OOE+OO

6. 72E+OO 7.50 4.56E+OO 4.45E+00

1.00E+Ol 6.32 O.OOE+OO O.OOE+OO

4.50E+OO 5.74 3.00E+OO 3.18E+OO

2.50E+Ol 10.00 O.OOE+OO O.OOE+OO

5.50E+Ol 14.83 O.OOE+OO O.OOE+OO

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Analysis Report for 1803111-03

M m

M m

AC-SED-11

PEAK WITH N/0 REPORT

Peak Analysis Performed on : 4/17/2018 6:43:01AM

Peak Analysis From Channel : 1

Peak Analysis To Channel : 4096

Tentative NID Library

Peak Match Tolerance

Peak Energy

No. (keV)

1 47.14 2 76.59 3 93.65 4 99.87 5 185.97 6 239.38 7 277.51

8 295.46 9 302.20

10 338.95 11 352.20 12 408.80 13 463.05 14 477.97 15 511 .42 16 563.56 17 583.18 18 609.34 19 663.21 20 750.47 21 766.58 22 771.59 23 795.62 24 860.86 25 911. 33

26 932.18 27 950.24 28 969.18 29 1003.27 30 1098.74 31 1120. 52

32 1237.76 33 1327.57 34 1335.60 35 1352.42 36 1377.95

: \\OR-GAMMA 1 \ApexRoot\Countroom\Library\TMA2.NLB

: 1.000 keV

ROI ROI Peak Net Peak

start end Centroid Area

44 - 49 46.92 1.21E+02 72 - 81 76.35 6.37E+02 91 - 96 93.40 1.40E+02 97 - 104 99.63 8.19E+0l

181 - 190 185.68 1.64E+02 234 - 244 239.06 7.01E+02 27 4 - 281 277.18 5.27E+0l

291 - 306 295.12 2.16E+02 291 - 306 301.86 2.86E+0l

335 - 343 338.59 1.09E+02 348 - 355 351.83 3.47E+02 406 - 411 408.40 2.60E+0l 4 60 - 466 4 62. 62 3.59E+0l 4 7 4 - 480 477.54 3.32E+0l 506 - 516 510.97 1.28E+02 561 - 567 563.08 2.09E+0l 57 8 - 587 582.70 1.66E+02 604 - 613 608.84 2.78E+02 657 - 668 662.69 7.14E+01 746 - 755 749.89 2.52E+0l 7 63 - 774 766.00 2.24E+0l 7 63 - 774 771. 00 1.63E+0l 7 92 - 7 98 795.02 3.24E+0l 858 - 863 860.22 2.05E+0l 907 - 913 910.66 9.16E+0l

927 - 938 931.50 3.28E+0l 948 - 952 949.55 1.23E+0l

966 - 971 968.48 4.36E+0l 994 - 1009 1002.55 4.35E+0l

1095 - 1103 1097. 96 1.66E+0l 1116 - 1125 1119.73 3.29E+0l

1233 - 1240 1236.91 2.39E+0l 1324 - 1329 1326.66 7.50E+00

1330 - 1340 1334. 67 2.87E+0l

134 7 - 1355 1351.49 1.30E+0l

1373 - 1382 1377.01 2.50E+0l

Net Area Uncertainty

58.34 116.04

70.29 70.54 79.46 83.70 46.35

40.73 29.65

52.38 55.79 28.18 29.62 29.42 41.25 23.54 43.91 46.89 37.20 28.35 17.27 19.03 22 .11 17.55 27.74

27.57 13.67 25.73 32.37 21.24 28.77

23.41 8.66

17.87 14.04 20.32

Page 7 of 29

Continuum Tentative Counts Nuclide

5. 78E+02 PB-210 1.53E+03 8.21E+02 GA-67 7.80E+02 LU-173 8.05E+02 RA-226 5.58E+02 PB-212 3.13E+02 CM-243

NP-239 1. 78E+02 PB-214 l.45E+02 PA-231

BA-133 3.44E+02 AC-228 2.87E+02 PB-214 1.38E+02 1.34E+02 SB-125 l.34E+02 BE-7 1.56E+02 8.82E+0l CS-134 1.82E+02 TL-208 1.56E+02 BI-214 1.35E+02 1.02E+02 4.l0E+0l NB-95 4.36E+01 6.32E+0l CS-134 4.l0E+0l TL-208 7.27E+0l AC-228

TL-204 8.04E+0l 3.15E+01 9.08E+0l AC-228 8.49E+0l 6.08E+01 FE-59 9.82E+0l SC-46

BI-214 TA-182

7.42E+0l CO-56 9.00E+00 2.66E+0l 2.20E+0l 4.41E+01

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Analysis Report for 1803111-03

M m

M m

AC-SED-11

Peak Energy ROI

No. (keV) start

37 1457.14 1453 -38 1460.90 1453 -39 1510.18 1505 -40 1589.70 1584 -41 1597.80 1594 -42 1639.41 1635 -43 1662.23 1657 -44 1729.66 1724 -45 1739.41 1 735 -46 1764.67 1760 -47 1832.00 1827 -48 1887.19 1881 -49 1894.20 1890 -50 2027.45 2023 -51 2203.96 2199 -52 2614.32 2 607 -

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet

Errors quoted at 2.000sigma

ROI Peak Net Peak Net Area

end Centroid Area Uncertainty

1463 1456.14 1.23E+0l 18.22

1463 1459.90 4.57E+02 45.12

1512 1509.15 1.31E+0l 14.00

1593 1588.61 1.35E+0l 14.73

1600 1596.71 6.94E+00 6.95

1641 1638.29 7.50E+00 8.28

1665 1661.09 1.l0E+0l 6.63

1732 1728.48 9.50E+00 9.82

1740 1738.22 5.13E+00 7.07

1768 1763.46 3.50E+0l 16.03

1834 1830.75 8.00E+00 5.66

1889 1885.90 6.72E+00 7.50

1895 1892.90 1.00E+0l 6.32

2028 2026.06 4.50E+00 5.74

2207 2202.44 2.50E+0l 10.00

2617 2612.47 5.50E+0l 14.83

PEAK EFFICIENCY REPORT

Peak Analysis Performed on : 4/17/2018 6:43:01AM

Peak Energy Net Peak Net Area Peak

No. (keV) Area Uncertainty Efficiency

1 47.14 1.21E+02 58.34 1.62E-02

2 76.59 6.37E+02 116.04 2.33E-02

3 93.65 1.40E+02 70.29 2.40E-02

4 99.87 8.19E+0l 70.54 2.40E-02

5 185.97 1.64E+02 79.46 1.95E-02

6 239.38 7.01E+02 83.70 1.68E-02

7 277.51 5.27E+0l 46.35 1.52E-02

8 295.46 2.16E+02 40.73 1. 4 6E-02

9 302.20 2.86E+0l 29.65 1.43E-02

10 338.95 1.09E+02 52.38 l.32E-02

11 352.20 3.47E+02 55.79 1.28E-02

12 408.80 2.60E+01 28.18 1.14E-02

13 463.05 3.59E+0l 29.62 l.03E-02

14 477.97 3.32E+0l 29.42 1.00E-02

Page 8 of29

Continuum Tentative Counts Nuclide

2.95E+0l 2.34E+0l K-40 2.38E+0l 1.89E+0l 4. llE+00 7.00E+00 0.00E+00 9.00E+00 5.75E+00 1.80E+0l BI-214 0.00E+00 4.56E+00 0.00E+00 3.00E+00 0.00E+00 BI-214 0.00E+00 TL-208

Efficiency Uncertainty

1.53E-03 1.88E-03 2.09E-03 2.07E-03 2.44E-03 2.41E-03 2.39E-03 2.38E-03 2.38E-03 2.36E-03 2.35E-03 2.23E-03 1.91E-03 1.83E-03

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Analysis Report for 1803111-03

AC-SED-11

Peak Energy Net Peak Net Area Peak Efficiency

No. (keV) Area Uncertainty Efficiency Uncertainty

15 511.42 l.28E+02 41. 25 9.SlE-03 l.63E-03

16 563.56 2.09E+Ol 23.54 8. 77E-03 1.33E-03

17 583.18 1.66E+02 43.91 8.53E-03 1.22E-03

18 609.34 2.78E+02 46.89 8.22E-03 1.07E-03

19 663.21 7.14E+Ol 37.20 7.66E-03 7.70E-04

20 750.47 2.52E+Ol 28.35 6.91E-03 9.36E-04

M 21 766.58 2.24E+Ol 17.27 6.79E-03 9.67E-04

m 22 771.59 1.63E+Ol 19.03 6.7SE-03 9. 77E-04

23 795.62 3.24E+Ol 22 .11 6.59E-03 1.02E-03

24 860.86 2.0SE+Ol 17.55 6.17E-03 1.lSE-03

25 911. 33 9.16E+Ol 27.74 S.89E-03 1.18E-03

26 932.18 3.28E+Ol 27.57 S.79E-03 l.12E-03

27 950.24 l.23E+Ol 13.67 S.70E-03 1.07E-03

28 969.18 4.36E+Ol 25.73 S.61E-03 1.0lE-03

29 1003.27 4.3SE+Ol 32.37 S.46E-03 9.14E-04

30 1098.74 1.66E+Ol 21.24 S.09E-03 6.39E-04

31 1120.52 3.29E+Ol 28.77 S.OlE-03 S.76E-04

32 1237.76 2.39E+Ol 23.41 4.66E-03 4.00E-04

33 1327.57 7.SOE+OO 8.66 4.43E-03 3.67E-04

34 1335.60 2.87E+Ol 17.87 4.41E-03 3.65E-04

35 1352.42 1.30E+Ol 14.04 4.38E-03 3.67E-04

36 1377.95 2.SOE+Ol 20.32 4.32E-03 3.70E-04

M 37 1457.14 l.23E+Ol 18.22 4.17E-03 3.80E-04

m 38 1460.90 4.57E+02 45.12 4.16E-03 3.80E-04

39 1510.18 1.31E+Ol 14.00 4.08E-03 3.86E-04

40 1589.70 1.3SE+Ol 14.73 3.9SE-03 3. 96E-04

41 1597.80 6.94E+OO 6.95 3.94E-03 3.97E-04

42 1639.41 7.SOE+OO 8.28 3.89E-03 4.02E-04

43 1662.23 1.lOE+Ol 6.63 3.86E-03 4.04E-04

44 1729.66 9.SOE+OO 9.82 3.78E-03 4.12E-04

45 1739.41 S. 13E+OO 7.07 3.77E-03 4.13E-04

46 1764.67 3.SOE+Ol 16.03 3.74E-03 4.16E-04

47 1832.00 8.00E+OO 5.66 3.67E-03 4.24E-04

48 1887.19 6.72E+OO 7.50 3.63E-03 4.2SE-04

49 1894.20 1.00E+Ol 6.32 3.62E-03 4.2SE-04

so 2027.45 4.SOE+OO 5.74 3.53E-03 4.2SE-04

51 2203. 96 2.SOE+Ol 10.00 3.44E-03 4.2SE-04

52 2614.32 S.SOE+Ol 14.83 3.36E-03 4.2SE-04

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet

Errors quoted at 2.000 sigma

BACKGROUND SUBTRACT REPORT

Peak Analysis Performed on : 4/17/2018 6:43:01AM

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Analysis Report for 1803111-03

AC-SED-11

Env. Background File : \\OR-GAMMA 1\ApexRoot\Countroom\Data\0000063825.CNF

Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted

No. (keV) Area Uncertainty Background Uncert. Area Uncert.

1 47.14 1.21E+02 58.34 2.91E+0l 5.55E+00 9.19E+0l 5.86E+0l

2 76.59 6.37E+02 116.04 6.37E+02 1.16E+02

3 93.65 1.40E+02 70.29 5.03E+0l 8.08E+00 8.99E+0l 7.07E+0l

4 99.87 8.19E+0l 70.54 8.19E+0l 7.05E+0l

5 185.97 1.64E+02 79.46 4.04E+0l 9.60E+00 1.23E+02 8.00E+0l

6 239.38 7.01E+02 83.70 1.86E+0l 1.03E+0l 6.82E+02 8.43E+0l

7 277.51 5.27E+0l 46.35 5.27E+0l 4.63E+01

M 8 295.46 2.16E+02 40.73 8.49E+00 5.60E+00 2.07E+02 4. llE+0l

m 9 302.20 2.86E+0l 29.65 2.86E+0l 2.97E+0l

10 338.95 1.09E+02 52.38 1.09E+02 5.24E+0l

11 352.20 3.47E+02 55.79 1.76E+0l 5.14E+00 3.29E+02 5.60E+0l

12 408.80 2.60E+0l 28.18 2.60E+0l 2.82E+0l

13 463.05 3.59E+0l 29.62 3.59E+0l 2. 96E+01

14 477.97 3.32E+0l 29.42 3.32E+0l 2.94E+0l

15 511. 42 l.28E+02 41.25 7.91E+0l 5.07E+00 4.87E+0l 4.16E+0l

16 563.56 2.09E+0l 23.54 2.09E+0l 2.35E+0l

17 583.18 1.66E+02 43.91 6.66E+00 3.73E+00 1.59E+02 4.41E+0l

18 609.34 2.78E+02 46.89 l.26E+0l 6.94E+00 2.66E+02 4.74E+0l

19 663.21 7.14E+0l 37.20 7.14E+0l 3.72E+0l

20 750.47 2.52E+0l 28.35 2.52E+0l 2.84E+0l

M 21 766.58 2.24E+0l 17.27 2.24E+0l 1.73E+0l

m 22 771.59 1.63E+0l 19.03 1.63E+0l 1.90E+0l

23 795.62 3.24E+0l 22 .11 3.24E+0l 2.21E+0l

24 860.86 2.05E+0l 17.55 2.05E+0l 1.75E+0l

25 911. 33 9.16E+0l 27.74 2.63E+00 2.68E+00 8.90E+0l 2.79E+0l

26 932.18 3.28E+0l 27.57 3.28E+0l 2.76E+01

27 950.24 1.23E+0l 13.67 1.23E+0l 1.37E+0l

28 969.18 4.36E+0l 25.73 4.36E+0l 2.57E+0l

29 1003.27 4.35E+0l 32.37 4.35E+0l 3.24E+0l

30 1098.74 1.66E+0l 21.24 1.66E+0l 2.12E+0l

31 1120.52 3.29E+0l 28.77 1.l0E+00 2.71E+00 3.18E+0l 2.89E+0l

32 1237.76 2.39E+0l 23.41 2.39E+0l 2.34E+01

33 1327.57 7.50E+00 8.66 7.50E+00 8.66E+00

34 1335. 60 2.87E+0l 17.87 2.87E+0l 1.79E+0l

35 1352.42 1.30E+0l 14.04 1.30E+0l 1.40E+0l

36 1377.95 2.50E+0l 20.32 2.07E+00 2.17E+00 2.29E+0l 2.04E+0l

M 37 1457.14 l.23E+0l 18.22 l.23E+0l l.82E+0l

m 38 1460.90 4.57E+02 45.12 7.43E+00 2.27E+00 4.50E+02 4.52E+01

39 1510.18 1.31E+0l 14.00 1.31E+0l 1.40E+0l

40 1589.70 1.35E+0l 14.73 1.35E+0l 1.47E+0l

41 1597.80 6.94E+00 6.95 6.94E+00 6.95E+00

42 1639.41 7.50E+00 8.28 7.50E+00 8.28E+00

43 1662.23 l.l0E+0l 6.63 1.l0E+0l 6.63E+00

44 1729.66 9.50E+00 9.82 9.50E+00 9.82E+00

45 1739.41 5.13E+00 7.07 5.13E+00 7.07E+00

46 1764.67 3.50E+0l 16.03 2.32E+00 1.91E+00 3.27E+0l 1.61E+0l

47 1832.00 8.00E+00 5.66 8.00E+00 5.66E+00

48 1887.19 6. 72E+00 7.50 6.72E+00 7.50E+00

49 1894.20 1.00E+0l 6.32 1.00E+0l 6.32E+00

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Analysis Report for 1803111-03

AC-SED-11

Peak Energy No. (keV)

50 2027.45 51 2203.96 52 2614.32

Original Area

4.50E+00 2.50E+0l 5.50E+0l

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet

Errors quoted at 2.000sigma

Orig. Area Uncertainty

5.74 10.00 14.83

Ambient Background

4.72E+00

Backgr. Uncert.

1.41E+00

AREA CORRECTION REPORT

Subtracted Area

4.50E+00 2.50E+0l 5.03E+0l

REFERENCEPEAKIBKG.SUBTRACT

Peak Analysis Performed on : 4/17/2018 6:43:01AM

Ref. Peak Energy : 0.00 Reference Date

Peak Ratio : 0.00 Uncertainty : 0.00

Background File : \\OR-GAMMA 1\ApexRoot\Countroom\Data\0000063825.CNF

Corrected Area is: Original* Peak Ratio - Background

Peak Energy Original Orig. Area Ambient Backgr. Corrected

No. (keV) Area Uncertainty Background Uncert. Area

1 47.14 l.21E+02 58.34 2.91E+0l 5.55E+00 9.19E+0l

2 76.59 6.37E+02 116.04 6.37E+02

3 93.65 1.40E+02 70.29 5.03E+0l 8.08E+00 8.99E+0l

4 99.87 8.19E+0l 70.54 8.19E+0l

5 185.97 l.64E+02 79.46 4.04E+0l 9.60E+00 l.23E+02

6 239.38 7.01E+02 83.70 1.86E+0l 1.03E+0l 6.82E+02

7 277.51 5.27E+0l 46.35 5.27E+0l

M 8 295.46 2.16E+02 40.73 8.49E+00 5.60E+00 2.07E+02

m 9 302.20 2.86E+0l 29.65 2.86E+0l

10 338.95 1.09E+02 52.38 l.09E+02

11 352.20 3.47E+02 55.79 1.76E+0l 5.14E+00 3.29E+02

12 408.80 2.60E+0l 28.18 2.60E+0l

13 463.05 3.59E+0l 29.62 3.59E+0l

14 477.97 3.32E+0l 29.42 3.32E+0l

15 511.42 1.28E+02 41.25 7.91E+0l 5.07E+00 4.87E+0l

16 563.56 2.09E+0l 23.54 2.09E+0l

17 583.18 l.66E+02 43.91 6.66E+00 3.73E+00 1.59E+02

18 609.34 2.78E+02 46.89 1.26E+0l 6.94E+00 2.66E+02

19 663.21 7.14E+0l 37.20 7.14E+0l

20 750.47 2.52E+0l 28.35 2.52E+0l

M 21 766.58 2.24E+0l 17.27 2.24E+0l

m 22 771.59 1.63E+0l 19.03 1.63E+0l

23 795.62 3.24E+0l 22 .11 3.24E+0l

24 860.86 2.05E+0l 17.55 2.05E+0l

25 911. 33 9.16E+0l 27.74 2.63E+00 2.68E+00 8.90E+0l

Subtracted Uncert.

5.74E+00 1.00E+0l l.49E+0l

Corrected Uncert.

5.86E+0l l.16E+02 7.07E+0l 7.05E+0l 8.00E+0l 8.43E+0l 4.63E+0l 4.llE+0l 2.97E+0l 5.24E+0l 5.60E+0l 2.82E+0l 2.96E+0l 2.94E+0l 4.16E+0l 2.35E+0l 4.41E+0l 4.74E+0l 3.72E+0l 2.84E+0l 1.73E+0l 1.90E+0l 2.21E+0l 1.75E+0l 2.79E+0l

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Analysis Report for 1803111-03

AC-SED-11

Peak Energy Original Orig. Area Ambient Backgr. Corrected Corrected

No. (keV) Area Uncertainty Background Uncert. Area Uncert.

26 932.18 3.28E+01 27. 57 3.28E+01 2.76E+Ol

27 950.24 1.23E+Ol 13.67 l.23E+Ol 1.37E+Ol

28 969.18 4.36E+Ol 25.73 4.36E+Ol 2.57E+Ol

29 1003.27 4.3SE+Ol 32.37 4.35E+Ol 3.24E+Ol

30 1098.74 1.66E+Ol 21. 24 1.66E+Ol 2.12E+Ol

31 1120.52 3.29E+Ol 28.77 l.lOE+OO 2.71E+OO 3.18E+Ol 2.89E+Ol

32 1237.76 2.39E+Ol 23.41 2.39E+Ol 2.34E+Ol

33 1327.57 7.SOE+OO 8.66 7.SOE+OO 8.66E+OO

34 1335.60 2.87E+Ol 17.87 2.87E+Ol 1.79E+Ol

35 1352.42 1.30E+01 14.04 1.30E+Ol 1.40E+Ol

36 1377.95 2.SOE+Ol 20.32 2.07E+OO 2.17E+OO 2.29E+Ol 2.04E+Ol

M 37 1457.14 1.23E+01 18.22 1.23E+Ol 1.82E+Ol

m 38 1460.90 4.57E+02 45.12 7.43E+OO 2. 27E+OO 4.SOE+02 4.52E+Ol

39 1510.18 1.31E+Ol 14.00 1.31E+Ol 1.40E+Ol

40 1589.70 1.3SE+Ol 14.73 1.3SE+Ol 1.47E+Ol

41 1597.80 6.94E+OO 6.95 6.94E+OO 6.9SE+OO

42 1639.41 7.SOE+OO 8.28 7.SOE+OO 8.28E+OO

43 1662.23 1.lOE+Ol 6.63 1.lOE+Ol 6.63E+OO

44 1729.66 9.SOE+OO 9.82 9.SOE+OO 9.82E+OO

45 1739.41 S.13E+OO 7.07 S.13E+OO 7.07E+OO

46 1764.67 3.SOE+Ol 16.03 2.32E+OO 1.91E+00 3.27E+Ol 1.61E+Ol

47 1832.00 8.00E+OO 5.66 8.00E+OO S.66E+OO

48 1887.19 6.72E+OO 7.50 6.72E+OO 7.SOE+OO

49 1894.20 1.00E+Ol 6.32 1.00E+Ol 6.32E+OO

so 2027.45 4.50E+OO 5.74 4.SOE+OO S.74E+00

51 2203. 96 2.SOE+Ol 10.00 2.50E+Ol 1.00E+Ol

52 2614.32 S.50E+Ol 14.83 4. 72E+00 1.41E+OO S.03E+Ol 1.49E+Ol

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet

Errors quoted at 2.000sigma

NUCLIDE IDENTIFICATION REPORT

Nuclide Library Used : \\OR-GAMMA 1 \ApexRoot\Countroom\Library\TMA2.NLB

IDENTIFIED NUCLIDES

Nuclide Name Id Confidence Energy (keV) Yield(%) Activity Activity

(pCi/grams) Uncertainty

BE-7 0.976 477.59 * 10.42 7.08E-01 6.41E-01

K-40 0.999 1460.81 * 10.67 1.60E+Ol 2.17E+OO

FE-59 0.308 1099.22 * 56.50 1.38E-01 1.78E-01

1291.56 43.20

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Analysis Report for 1803111-03

AC-SED-11

Nuclide Name Id Confidence Energy (keV) Yield(%) Activity

(pCi/grams)

GA-67 0.377 93.31 * 35.70 5.00E+0l

208.95 2.24 300.22 16.00

NB-95 0.901 765.79 * 99.81 8.86E-02

TL-208 0.988 583.14 * 30.22 9.75E-01

860.37 * 4.48 l.17E+00

2614.66 * 35.85 6.58E-01

PB-210 0.936 46.50 * 4.25 2.l0E+00

PB-212 0.815 238.63 * 44.60 l.44E+00 300.09 3.41

BI-214 0.997 609.31 * 46.30 l.l0E+00

1120.29 * 15.10 6.62E-01

1764.49 * 15.80 8. 72E-01

2204.22 * 4.98 2.30E+00

PB-214 0.989 295.21 * 19.19 l.17E+00

351.92 * 37.19 l.09E+00

RA-226 0.991 186.21 * 3.28 3.03E+00

AC-228 0.982 338.32 * 11. 40 l.15E+00 911. 07 * 27.70 8.60E-01 969 .11 * 16.60 7.38E-01

PA-231 0.314 283.67 1. 60 302.67 * 2.30 l.37E+00

* = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

Energy Tolerance : 1.000 keV

Nuclide confidence index threshold = 0.30

Errors quoted at 2.000sigma

UNIDENTIFIED PEAKS

Peak Locate Performed on

Peak Locate From Channel

Peak Locate To Channel

Peak No. Energy (keV)

2 76.59 4 99.87 7 277.51

12 408.80 13 463.05 15 511. 42

: 4/17/2018 6:43:01AM

: 1 : 4096

Peak Size (CPS)

1. 76911E-01 2.27560E-02 l.46292E-02

7.22222E-03 9. 98112E-03 l.35394E-02

Peak CPS(%} Peak

Uncertainty Type

9 .11 D-Esc 43.05 Tol. 44.00 Tol.

54.19 41.22 Tol. 42.63

Page 13 of29

Activity

Uncertainty

3.96E+0l

6.95E-02 3.03E-01 l.02E+00 2.12E-01 l.36E+00 2. 72E-01

2.43E-01 6.07E-01 4. 41E-01 9.64E-01 3. 0lE-01 2.73E-01 2.0lE+00 5.87E-01 3.19E-01 4.56E-01

l.44E+00

Tolerance

Nuclide

LU-173 NP-239 CM-243

SB-125

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0231

Analysis Report for 1803111-03

m

M

AC-SED-11

Peak No. Energy (keV)

16 563.56 19 663.21 20 750.47 22 771.59 23 795.62 26 932.18 27 950.24 29 1003.27 32 1237.76 33 1327.57 34 1335.60 35 1352.42 36 1377.95 37 1457.14 39 1510.18 40 1589.70 41 1597.80 42 1639.41 43 1662.23 44 1729.66 45 1739.41 47 1832.00 48 1887.19 49 1894.20 50 2027.45

M ::: First peak in a multiplet region

m == Other peak in a multiplet region

F ::: Fitted singlet

Errors quoted at 2.000sigma

4/17/2018 6:43:09AM

Peak Size (CPS) Peak CPS(%) Peak

Uncertainty Type

5.79914E-03 56.37 Tol.

1. 98391E-02 26.04 Sum

6.99561E-03 56.29 4. 52116E-03 58.47 8.99740E-03 34.13 Sum

9.10769E-03 42.04 3. 40278E-03 55.82 S-Esc

1.20946E-02 37.18 6.63479E-03 49.00 Tol.

2.08333E-03 57.74 7. 96627E-03 31.15 3.60532E-03 54.10 6.36076E-03 44.63 3.40748E-03 74.27 3.64444E-03 53.35 3.76208E-03 54.38 1.92901E-03 50.01 Sum

2.08333E-03 55.18 3.05556E-03 30.15 2.63889E-03 51.70 Sum

1. 42361E-03 68.99 2.22222E-03 35.36 1.86728E-03 55.79 Sum

2.77778E-03 31.62 1.25000E-03 63.83

NUCLIDE IDENTIFICATION REPORT

Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\TMA2.NLB

IDENTIFIED NUCLIDES

Nuclide Id Energy Yield(%) Activity

Page 14 of29

Tolerance Nuclide

CS-134

CO-56

Activity

Name Confidence (keV) (pCi/grams) Uncertainty

BE-7 0.97 477.59 * 10.42 7.08E-01 6.41E-01

K-40 0.99 1460.81 * 10.67 1.60E+0l 2.17E+00

FE-59 0.30 1099.22 * 56.50 1.38E-01 1.78E-01

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Analysis Report for 1803111-03

AC-SED-11

Nuclide Id Energy Yield(%) Activity Activity

Name Confidence (keV) (pCi/grams) Uncertainty

FE-59 0.30 1291.56 43.20

GA-67 0.37 93.31 * 35.70 5.00E+0l 3. 96E+0l

208.95 2.24 300.22 16.00

NB-95 0.90 765.79 * 99.81 8.86E-02 6.95E-02

TL-208 0.98 583.14 * 30.22 9.75E-01 3.03E-01

860.37 * 4.48 l.17E+00 1.02E+00

2614.66 * 35.85 6.58E-01 2.12E-01

PB-210 0.93 46.50 * 4.25 2.l0E+00 1.36E+00

PB-212 0.81 238.63 * 44.60 1.44E+00 2.72E-0l

300.09 3.41

BI-214 0.99 609.31 * 46.30 1.l0E+00 2.43E-01

1120.29 * 15.10 6.62E-01 6.07E-01

1764.49 * 15.80 8. 72E-01 4.41E-01

2204.22 * 4.98 2.30E+00 9.64E-01

PB-214 0.98 295.21 * 19.19 l.17E+00 3.0lE-01

351.92 * 37.19 1.09E+00 2.73E-0l

RA-226 0.99 186.21 * 3.28 3.03E+00 2.0lE+00

AC-228 0.98 338.32 * 11. 40 l.15E+00 5.87E-01

911.07 * 27.70 8.60E-01 3.19E-01

969. 11 * 16.60 7.38E-01 4.56E-01

PA-231 0.31 283.67 1. 60 302.67 * 2.30 1.37E+00 1.44E+00

* = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity

Energy Tolerance : 1.000 keV

Nuclide confidence index threshold = 0.30

Errors quoted at 2.000sigma

INTERFERENCE CORRECTED REPORT

Nuclide Nuclide Wt mean Wt mean Comments

Name Id Activity Activity

Confidence (pCilgrams) Uncertainty

BE-7 0.976 7.08E-01 6.41E-01

K-40 0.999 1.60E+0l 2.17E+00

FE-59 0.308 1.38E-01 1.78E-01

GA-67 0. 377 5.00E+0l 3.96E+0l

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0233

Analysis Report for 1803111-03

? = X =

AC-SED-11

Nuclide Name

NB-95 TL-208 PB-210 PB-212 BI-214 PB-214 RA-226 AC-228 PA-231

Nuclide Id

Confidence

0.901 0.988 0.936 0.815 0.997 0.989 0.991 0.982 0.314

nuclide is part of an undetermined solution

nuclide rejected by the interference analysis

4/17/2018 6:43:09AM

Wt mean Wt mean

Activity Activity

(pCilgrams) Uncertainty

8.86E-02 6.95E-02 7.74E-01 1.71E-01 2.l0E+00 1.36E+00 1.44E+00 2. 72E-01 1.06E+00 1.97E-0l 1.13E+00 2.02E-01 3.03E+00 2.0lE+00 8.74E-01 2.39E-01 1.37E+00 1.44E+00

@ = nuclide contains energy lines not used in Weighted Mean Activity

Errors quoted at 2.000sigrna

Page 16 of29

Comments

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0234

Analysis Report for 1803111-03

m

M

AC-SED-11

Peak Locate Performed on

Peak Locate From Channel

Peak Locate To Channel

Peak No. Energy (ke VJ

2 76.59

4 99.87

7 277.51

12 408.80

13 463.05

15 511.42

16 563.56

19 663.21

20 750.47

22 771.59

23 795.62

26 932.18

27 950.24

29 1003.27

32 1237.76

33 1327.57

34 1335.60

35 1352.42

36 1377. 95

37 1457.14

39 1510.18

40 1589.70

41 1597.80

42 1639.41

43 1662.23

44 1729.66

45 1739.41

47 1832.00

48 1887.19

49 1894.20

50 2027.45

4/17/2018 6:43:09AM

UNIDENTIFIED PEAKS

: 4/17/2018 6:43:01AM

: 1 : 4096

Peak Size (CPS)

1. 76911E-01

2.27560E-02

l.46292E-02

7.22222E-03

9. 98112E-03

1.35394E-02

5.79914E-03

1. 98391E-02

6.99561E-03

4. 52116E-03

8.99740E-03

9.10769E-03

3.40278E-03

1.20946E-02

6.63479E-03

2.08333E-03

7. 96627E-03

3.60532E-03

6.36076E-03

3.40748E-03

3.64444E-03

3.76208E-03

1.92901E-03

2.08333E-03

3.05556E-03

2.63889E-03

l.42361E-03

2.22222E-03

1. 86728E-03

2.77778E-03

1.25000E-03

Peak CPS(%) Peak

Uncertainty Type

9 .11 D-Esc

43.05 Tol.

44.00 Tol.

54.19 41. 22 Tol.

42.63

56.37 Tol.

26.04 Sum

56.29

58.47

34. 13 Sum

42.04 55.82 S-Esc

37.18

49.00 Tol.

57.74 31.15

54.10 44.63 74.27 53.35

54.38 50.01 Sum

55.18

30.15

51.70 Sum

68.99 35.36

55.79 Sum

31.62

63.83

Page 17 of29

Tolerance Nuclide

LU-173 NP-239 CM-243

SB-125

CS-134

CO-56

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0235

Analysis Report for 1803111-03

AC-SED-11

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet

Errors quoted at 2.000sigma

4/17/2018 6:43:09AM

NUCLIDE MDA REPORT

Nuclide Library Used : \ \0 R-GAM MA 1 \ApexRoot\Countroom\Library\ TMA2. N LB

Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA

Name (keV) (pCilgrams) (pCilgrams) (pCi/grams)

+ BE-7 477.59 * 10.42 7.08E-01 1.0lE+00 1.0lE+00

+ NA-22 1274.54 99.94 -1.57E-02 8.99E-02 8.99E-02

+ NA-24 1368.53 99.99 2.00E-02 4.36E-02 8.15E-02

2754.09 99.86 7.04E-03 4.36E-02

+ AL-26 1808.65 99.76 -4. 27E-03 6.78E-02 6.78E-02

+ K-40 1460.81 * 10.67 1.60E+0l 1.15E+00 1.15E+00

+ @ AR-41 1293.64 99.16 1.00E+26 1.00E+26 l.00E+26

+ TI-44 67.88 94.40 -4.38E-02 7.21E-02 7.21E-02

78.34 96.00 1.63E-01 9.39E-02

+ SC-46 889.25 98.98 -4.30E-02 1.0lE-01 1.0lE-01

1120. 51 99.90 1.41E-01 l.64E-01

+ V-48 983.52 99.98 9.00E-02 2.76E-01 2.76E-01

1312.10 97.50 4.41E-02 3.02E-01

+ CR-51 320.08 9.83 -7.47E-01 1.07E+00 1.07E+00

+ MN-54 834.83 99.97 1.00E-02 9.59E-02 9.59E-02

+ CO-56 846.75 99. 96 -8.84E-04 1.04E-01 1.04E-01

1037.75 14.03 l.l0E-01 8.75E-01

1238.25 67.00 1. 58E-01 2.47E-01

1771.40 15.51 6.59E-02 5.91E-01

2587.48 16.90 3.62E-02 3.36E-01

+ CO-57 122.06 85.51 4.55E-02 6.50E-02 6.50E-02

136.48 10.60 1.05E-01 5.53E-01

+ CO-58 810.76 99.40 1.04E-02 9.87E-02 9.87E-02

+ FE-59 1099.22 * 56.50 1.38E-01 2.88E-01 2.91E-01

1291.56 43.20 -7.54E-02 2.88E-01

+ CO-60 1173.22 100.00 3.08E-02 9.84E-02 1.07E-01

1332.49 100.00 1.95E-02 9.84E-02

+ ZN-65 1115.52 50.75 5.57E-02 2.14E-01 2.14E-01

+ GA-67 93.31 * 35.70 5.00E+0l 6.38E+0l 6.38E+0l

208.95 2.24 1.77E+02 7. 85E+02

300.22 16.00 2.35E+0l 1.09E+02

+ SE-75 121.11 16.70 5.81E-02 1.07E-01 3.55E-01

Page 18 of29

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Analysis Report for 1803111-03

AC-SED-11

Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA

Name (keV) (pCi/grams) (pCilgrams) (pCilgrams)

SE-75 136.00 59.50 2.04E-02 1.07E-01 1.07E-01

264.65 59.80 -2.40E-03 1.l0E-01

279.53 25.20 9.12E-02 2.65E-01

400.65 11. 40 -4.93E-02 5.73E-01

+ RB-82 776.52 13.00 -4.35E-01 1.22E+00 1.22E+00

+ RB-83 520.41 46.00 5.20E-02 1.69E-01 1.69E-01

529.64 30.30 -1.17E-01 2.19E-01

552.65 16.40 -4. llE-02 4.72E-01

+ KR-85 513.99 0.43 -1.llE+0l 1.58E+0l 1.58E+0l

+ SR-85 513.99 99. 27 -6.41E-02 9.18E-02 9.18E-02

+ Y-88 898.02 93.40 2.36E-02 7.26E-02 1.02E-01

1836.01 99.38 1.03E-02 7.26E-02

+ MO-93 263.06 56.72 8.85E-03 6.44E-02 9.83E-02

684.67 99.68 -1.62E-02 7.07E-02

1477.11 99.08 -9.45E-03 6.44E-02

+ NB-93M 16.57 9.43 0.00E+00 l.28E+00 1.28E+00

+ NB-94 702.63 100.00 -3.69E-03 8.49E-02 8.49E-02

871.10 100.00 1.32E-03 9.0lE-02

+ NB-95 765.79 * 99.81 8.86E-02 1.82E-01 1.82E-01

+ NB-95M 235.69 25.00 -3.76E+02 4.04E+0l 4.04E+0l

+ ZR-95 724.18 43.70 8.37E-02 1.98E-01 2.73E-01

756.72 55.30 -2.62E-02 1.98E-01

+ MO-99 181.06 6.20 -1.20E+0l 5.41E+02 8.06E+02

739.58 12.80 1.88E+02 5.41E+02

778.00 4.50 -l.09E+02 1.53E+03

+ TC-99M 140.51 89.00 1.86E-02 6.00E-02 6.00E-02

+ RU-103 497.08 89.00 8.llE-03 1.0lE-01 1.0lE-01

+ RU-106 621.84 9.80 3.58E-01 8.42E-01 8.42E-01

+ AG-108M 433.93 89.90 -2.42E-03 6.31E-02 6.31E-02

614.37 90.40 -1.17E-02 8.34E-02

722.95 90.50 -5.66E-02 8.78E-02

+ CD-109 88.03 3. 72 3.08E+00 2.02E+00 2.02E+00

+ AG-ll0M 657.75 93.14 -l.12E-02 8.34E-02 8.34E-02

677.61 10.53 2.90E-01 7.97E-01

706.67 16.46 -1.58E-03 5.24E-01

763.93 21.98 1.91E-02 4.40E-01

884.67 21.98 4.48E-02 4.21E-01

1384.27 23.94 6.13E-02 3.51E-01

+ CD-113M 263.70 0.02 2.18E+0l 2.42E+02 2.42E+02

+ SN-113 255.12 1. 93 -9.36E-02 9.68E-02 3.27E+00

391.69 64.90 -3.95E-02 9.68E-02

+ TE-123M 159.00 84.10 -2.95E-02 6.83E-02 6.83E-02

+ SB-124 602.71 97.87 -9.49E-03 8.97E-02 8.97E-02

645.85 7.26 4.18E-0l 1.56E+00

722.78 11.10 -6.29E-01 9.75E-01

1691.02 49.00 4.95E-02 2.08E-01

+ I-125 35.49 6.49 -2.29E-01 1.86E+00 1.86E+00

+ SB-125 176.33 6.89 1.12E-01 1.98E-01 8.38E-01

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Analysis Report for 1803111-03

AC-SED-11

Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA

Name (keV) (pCilgrams) (pCi/grams) (pCilgrams)

SB-125 427.89 29.33 -1.90E-03 1.98E-01 1.98E-01

463.38 10.35 S.24E-01 6.79E-01

600.56 17.80 1.66E-01 3.96E-01

635.90 11. 32 2.84E-01 6.30E-01

+ SB-126 414.70 83.30 1.lSE-02 7.40E-02 7.40E-02

666.33 99.60 -9.37E-02 8.lOE-02

695.00 99.60 4.18E-03 8.06E-02

720.50 53.80 1.34E-02 1.46E-01

+ SN-126 87.57 37.00 -3.56E-01 1.83E-01 1.83E-01

+ SB-127 473.00 25.00 -1.97E+OO 2.48E+Ol 2.67E+Ol

685.00 35.70 -S.68E+00 2.48E+Ol

783.80 14.70 3.0SE+Ol 7.81E+Ol

+ I-129 29.78 57.00 -7. llE-03 2.27E-01 2.27E-01

33.60 13.20 1.63E-01 7.98E-01

39.58 7.52 -3.57E-03 9.83E-01

+ I-131 284.30 6.05 2.62E+OO 6.63E-01 9.14E+OO

364.48 81.20 -4.12E-01 6.63E-01

636.97 7.26 2.7SE+OO 9.80E+OO

722.89 1. 80 -2.89E+Ol 4.48E+Ol

+ TE-132 49. 72 13.10 -1.80E+02 1.8SE+Ol 1.26E+02

228.16 88.00 -9.26E-01 1.8SE+Ol

+ BA-133 81.00 33.00 -1.20E-01 9.70E-02 1.79E-Ol

302.84 17.80 1.25E-01 3.23E-01

356.01 60.00 3.53E-02 9.70E-02

+ I-133 529.87 86.30 -7.12E+07 1.34E+08 1.34E+08

+ XE-133 81.00 38.00 -3.62E+OO S.41E+OO S.41E+OO

+ CS-134 563.23 8.38 3.62E-01 6.92E-02 7.7SE-Ol

569.32 15.43 7.SOE-02 4.08E-01

604.70 97.60 -1.91E-02 6.92E-02

795.84 85.40 7.89E-02 1.lSE-01

801.93 8.73 -6.06E-03 9.59E-01

+ CS-135 268.24 16.00 4.80E-02 3.7SE-01 3.75E-01

+ @ I-135 1131. 51 22. so 1.00E+26 1.00E+26 1.00E+26

@ 1260.41 28.60 1.00E+26 1.00E+26

@ 1678.03 9.54 1.00E+26 1.00E+26

+ CS-136 153.22 7.46 4.94E-01 3.02E-01 3.04E+OO

163.89 4.61 2.14E+OO 4.80E+OO

176.55 13.56 2.30E-01 1. 72E+OO

273.65 12.66 -4.22E-01 1.89E+OO

340.57 48.50 1.28E+OO 7.03E-01

818.50 99.70 -4.12E-02 3.02E-01

1048.07 79.60 -1.72E-01 4.68E-01

1235.34 19.70 1.63E-01 2.6SE+OO

+ CS-137 661.65 85.12 4.18E-02 1.16E-01 1.16E-01

+ LA-138 788.74 34.00 8.54E-02 1.36E-01 2.62E-01

1435.80 66.00 3.22E-02 1.36E-01

+ CE-139 165.85 80.35 -3.71E-02 7.43E-02 7.43E-02

+ BA-140 162.64 6.70 -8. 72E-01 1.09E+OO 3.29E+OO

304.84 4.50 3.3SE-01 S.13E+OO

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Analysis Report for 1803111-03

AC-SED-11

Nuclide Energy Yield(¾) Activity Nuclide MDA Line MDA

Name (keV) (pCi/grams) (pCi/grams) (pCilgrams)

BA-140 423.70 3.20 -l.03E+00 l.09E+00 7.16E+00

437.55 2.00 -3.80E-01 1. 27E+0l

537.32 25.00 4.73E-01 l.09E+00

+ LA-140 328. 77 20.50 8.69E-01 2.99E-01 l.29E+00

487.03 45.50 -7.75E-03 5.91E-01

815.85 23.50 -1.0lE+00 l.16E+00

1596.49 95.49 -l.20E-02 2.99E-0l

+ CE-141 145.44 48.40 -2. 21E-02 l.98E-0l l.98E-0l

+ CE-143 57.36 11. 80 -2.92E+05 l.54E+05 4.61E+05

293.26 42.00 l.62E+05 l.54E+05

664.55 5.20 2.05E+06 l.53E+06

+ CE-144 133.54 10.80 -2.83E-01 5.14E-01 5.14E-01

+ PM-144 476.78 42.00 9.66E-02 8.21E-02 l.71E-0l

618.01 98.60 7.25E-03 8. 21E-02

696. 4 9 99.49 -2.87E-02 8.51E-02

+ PM-145 36.85 21.70 l. l3E-01 2.08E-0l 3.91E-0l

37.36 39.70 5.98E-02 2.08E-0l

42.30 15.10 8.42E-02 4.66E-0l

72. 40 2.31 3.09E-0l 3.15E+00

+ PM-146 453.90 39.94 -8.38E-02 l.52E-0l l.52E-0l

735.90 14.01 -5.15E-02 5.37E-0l

747.13 13.10 -4.77E-03 6.29E-0l

+ ND-147 91.11 28.90 6.93E-01 l.39E+00 l.39E+00

531.02 13 .10 -5.86E-01 2.37E+00

+ PM-149 285.90 3.10 -l.68E+03 8.26E+03 8.26E+03

+ EU-152 121.78 20.50 l.78E-01 2.54E-01 2.54E-01

244.69 5.40 l.22E-01 l.19E+00

344.27 19 .13 -4.21E-02 2.92E-01

778.89 9.10 l.56E-0l 9.07E-01

964.01 10.40 l.58E-0l l.0lE+00

1085.78 7.22 2.67E-03 l.24E+00

1112.02 9.60 l. llE-01 l.00E+00

1407.95 14.94 9.l9E-02 5.84E-0l

+ GD-153 97.43 31.30 -2. 96E-0l l.92E-0l l.92E-0l

103.18 22.20 -2. 72E-0l 2.52E-0l

+ EU-154 123.07 40.50 -6. 72E-02 l.27E-0l l.27E-01

723.30 19.70 -l.84E-01 4.20E-01

873.19 11. 50 5.57E-0l 7.74E-0l

996. 32 10.30 -3.23E-01 8.26E-0l

1004.76 17.90 l.23E-01 5.40E-0l

1274.45 35.50 -4.37E-02 2.50E-0l

+ EU-155 86.50 30.90 3.54E-01 2.30E-0l 2.30E-01

105.30 20.70 l.98E-01 2.57E-0l

+ EU-156 811. 77 10.40 3.31E-0l 2.35E+00 2.35E+00

1153.47 7.20 l.22E+00 4.66E+00

1230.71 8.90 5.79E-01 4.l0E+00

+ HO-166M 184.41 72. 60 8.03E-02 9.85E-02 9.85E-02

280.45 29.60 -l.23E-01 l.79E-0l

410.94 11.10 -l.0lE-01 5.21E-0l

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Analysis Report for 1803111-03

AC-SED-11

Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA

Name (keV) (pCi/grams) (pCi/grams) (pCi/grams)

HO-166M 711.69 54.10 3.09E-02 9.85E-02 1.48E-01

+ TM-171 66. 72 0.14 -2.29E+0l 5.30E+0l 5.30E+0l

+ HF-172 67.35 5.31 -8.30E-01 4.81E-01 1.33E+00

125.82 11. 30 -3.81E-01 4.81E-01

+ LU-1 72 181.53 20.60 -6.68E-02 2.14E+00 4.49E+00

900.72 29.81 -2.46E+00 4.16E+00

1093.66 62.50 -4.43E-01 2.14E+00

+ LU-173 100.72 5.24 l.04E+00 2.97E-01 1.15E+00

272.11 21.20 5. 27E-02 2.97E-01

+ HF-175 343.40 84.00 5.19E-03 8.76E-02 8.76E-02

+ LU-176 88.34 13.30 8.27E-01 5.49E-02 5.42E-01

201.83 86.00 5.25E-03 6.73E-02

306.78 94.00 1.71E-02 5.49E-02

+ HF-181 133. 02 41.70 -1.06E-01 1.14E-01 1.93E-01

345.85 17.20 3. llE-01 5.30E-01

482.03 82.80 1.42E-02 1.14E-01

+ TA-182 67.75 41.20 -1.18E-01 1.94E-01 1.94E-01

1121.30 34.90 4.l0E-01 4.39E-01

1189.05 16.23 4.02E-02 7.66E-01

1221.41 26.98 -3.66E-02 4.86E-01

1231.02 11. 44 l.56E-01 1.l0E+00

+ IR-192 308.46 29.68 4.63E-02 1.44E-01 2.21E-01

468.07 48.10 -6.36E-03 1.44E-01

+ HG-203 279.19 77.30 3.79E-02 1.l0E-01 1.l0E-01

+ TL-204 374.74 94 .11 -1. 96E-02 5.68E-02 5.68E-02

899.15 99.16 -3.74E-02 7.74E-02

911.74 91.10 2.78E-01 1.65E-01

+ BI-207 569.67 97. 72 l.16E-02 6.30E-02 6.30E-02

1063.62 74.90 -1.44E-02 l.24E-01

+ TL-208 583.14 * 30.22 9.75E-01 l.34E-01 3.80E-01

860.37 * 4.48 1.17E+00 1.56E+00

2614.66 * 35.85 6.58E-01 1.34E-01

+ BI-210M 262.00 45.00 -5.81E-02 1.24E-01 1.24E-01

300.00 23.00 5.41E-02 2.50E-01

+ PB-210 46.50 * 4.25 2.l0E+00 2.15E+00 2.15E+00

+ PB-211 404.84 2.90 3.30E-01 1.86E+00 1.86E+00

831.96 2.90 -1.16E+00 2.78E+00

+ BI-212 727.17 11. 80 2.14E-01 7.73E-01 7.73E-01

1620.62 2.75 1.39E+00 2.85E+00

+ PB-212 238.63 * 44.60 1.44E+00 2.35E-0l 2.35E-01

300.09 3.41 3.65E-01 1.69E+00

+ BI-214 609.31 * 46.30 1.l0E+00 2.46E-0l 2.46E-01

1120.29 * 15.10 6.62E-01 9.68E-01

1764.49 * 15.80 8. 72E-01 5. 72E-01

2204.22 * 4.98 2.30E+00 2.49E-01

+ PB-214 295.21 * 19.19 1.17E+00 2.42E-01 6.61E-01

351.92 * 37.19 1.09E+00 2.42E-01

+ RN-219 401.80 6.50 3.65E-01 8.80E-01 8.80E-0l

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Nuclide Energy Yield(%} Activity Nuclide MDA Line MDA

Name (keV) (pCi/grams) (pCi/grams) (pCilgrams)

+ RA-223 323.87 3.88 -4.64E-01 1.38E+00 1.38E+00

+ RA-224 240.98 3.95 4.72E+00 2.70E+00 2.70E+00

+ RA-225 40.00 31.00 -3.54E-01 8.l0E-01 8.l0E-01

+ RA-226 186.21 * 3.28 3.03E+00 3.18E+00 3.18E+00

+ TH-227 50.10 8.40 7.63E-02 6.33E-01 6.33E-01

236.00 11. 50 -l.86E+00 7.66E-01

256.20 6.30 -3.36E-01 8.99E-01

+ AC-228 338.32 * 11. 40 1.15E+00 3.52E-01 8.59E-01

911.07 * 27.70 8.60E-01 3.52E-0l

969 .11 * 16.60 7.38E-01 6.61E-01

+ TH-230 48.43 16.90 4. llE-01 4.07E-01 4.07E-01

62.85 4.60 l.42E+00 1.70E+00

67.67 0.37 -1.16E+0l 1.85E+0l

+ PA-231 283.67 1. 60 1.61E+00 3.33E+00 3.33E+00

302.67 * 2.30 1.37E+00 5.53E+00

+ TH-231 25.64 14.70 0.00E+00 7.27E-02 7. 27E-02

84.21 6.40 -9.35E-01 9.87E-01

+ PA-233 311.98 38.60 3.67E-02 2.81E-01 2.81E-01

+ PA-234 131.20 20.40 9.15E-03 2.62E-01 2.62E-01

733.99 8.80 -2.88E-01 8.54E-01

946.00 12.00 5.54E-03 6.76E-01

+ PA-234M 1001.03 0.92 3.68E+00 1.08E+0l 1.08E+0l

+ TH-234 63.29 3.80 1. 72E+00 2.05E+00 2.05E+00

+ U-235 143.76 10.50 4.80E-02 5.06E-01 5.06E-01

163.35 4.70 4.91E-01 1.13E+00

205.31 4.70 -5.06E-01 1.17E+00

+ NP-237 86.50 12.60 8.60E-01 5.58E-01 5.58E-01

+ NP-239 106.10 22.70 2.97E+02 6.19E+02 6.19E+02

228.18 10.70 -6.81E+0l 1.36E+03

277.60 14.10 4.66E+02 1.17E+03

+ AM-241 59.54 35.90 1.49E-01 2.05E-01 2.05E-01

+ AM-243 74.67 66.00 -4.57E-0l 1. 2 9E-01 1.29E-01

+ CM-243 209.75 3.29 3.99E-01 4.36E-01 1.78E+00

228.14 10.60 -2.53E-02 5.07E-01

277.60 14.00 1.73E-01 4.36E-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

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NUCLIDE MDA REPORT

Nuclide Library Used : \\OR-GAMMA 1\ApexRoot\Countroom\Library\TMA2.NLB

Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level

Name (keV) (pCilgrams) (pCi/grams) (pCilgrams) (pCilgrams)

+ BE-7 47'7.59 * 10.42 1.0lE+00 1.0lE+00 7.08E-01 4.75E-01

NA-22 1274.54 99.94 8.99E-02 8.99E-02 -1.57E-02 4.02E-02

NA-24 1368.53 99.99 8.15E-02 4.36E-02 2.00E-02 3.58E-02

2754.09 99.86 4.36E-02 7.04E-03 1.54E-02

AL-26 1808.65 99.76 6. 78E-02 6.78E-02 -4. 27E-03 2.81E-02

+ K-40 1460.81 * 10.67 1.15E+00 1.15E+00 l.60E+0l 5.25E-01

@ AR-41 1293.64 99.16 1.00E+26 1.00E+26 l.00E+26 1.00E+20

TI-44 67.88 94.40 7.21E-02 7.21E-02 -4.38E-02 3.50E-02

78. 34 96. 00 9.39E-02 1.63E-01 4.60E-02

SC-46 889.25 98.98 1.0lE-01 1.0lE-01 -4.30E-02 4.62E-02

1120. 51 99.90 1.64E-01 1.41E-01 7.65E-02

V-48 983.52 99.98 2.76E-01 2.76E-01 9.00E-02 l.26E-01

1312.10 97.50 3.02E-01 4.41E-02 1.35E-01

CR-51 320.08 9.83 1.07E+00 1.07E+00 -7.47E-01 5.05E-01

MN-54 834.83 99.97 9.59E-02 9.59E-02 1.00E-02 4.44E-02

CO-56 846.75 99. 96 1.04E-01 1.04E-01 -8.84E-04 4.77E-02

1037.75 14.03 8.75E-01 1.l0E-01 4.00E-01

1238.25 67.00 2.47E-01 1.58E-0l l.15E-01

1771.40 15.51 5.91E-01 6.59E-02 2.48E-01

2587.48 16.90 3.36E-01 3.62E-02 l.19E-01

CO-57 122.06 85.51 6.50E-02 6.50E-02 4.55E-02 3.14E-02

136.48 10.60 5.53E-01 1.05E-01 2.67E-01

CO-58 810.76 99.40 9.87E-02 9.87E-02 1.04E-02 4.50E-02

+ FE-59 1099.22 * 56.50 2.91E-01 2.88E-01 1.38E-01 l.34E-01

1291.56 43.20 2.88E-01 -7.54E-02 1.28E-01

CO-60 1173.22 100.00 1.07E-01 9.84E-02 3.08E-02 4.90E-02

1332.49 100.00 9.84E-02 l.95E-02 4.43E-02

ZN-65 1115.52 50.75 2.14E-01 2.14E-01 5.57E-02 9.81E-02

+ GA-67 93.31 * 35.70 6.38E+0l 6.38E+0l 5.00E+0l 3.12E+0l

208.95 2.24 7.85E+02 1.77E+02 3.77E+02

300.22 16.00 1.09E+02 2.35E+0l 5.16E+0l

SE-75 121.11 16.70 3.55E-0l 1.07E-01 5.81E-02 1.71E-01

136.00 59.50 1.07E-01 2.04E-02 5.18E-02

264.65 59.80 1.l0E-01 -2.40E-03 5.24E-02

279.53 25.20 2.65E-01 9.12E-02 1.26E-01

400.65 11. 40 5.73E-01 -4.93E-02 2.68E-01

RB-82 776.52 13.00 1.22E+00 1.22E+00 -4.35E-01 5.57E-01

RB-83 520.41 46.00 l.69E-01 1.69E-01 5.20E-02 7.83E-02

529.64 30.30 2.19E-01 -l.17E-0l l.00E-01

552.65 16.40 4. 72E-01 -4. llE-02 2.18E-01

KR-85 513.99 0.43 1.58E+0l 1.58E+0l -1.llE+0l 7.39E+00

SR-85 513.99 99. 27 9.18E-02 9.18E-02 -6.41E-02 4.29E-02

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Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level

Name (keV) (pCilgrams) (pCi/grams) (pCilgrams) (pCi/grams)

Y-88 898.02 93.40 1.02E-0l 7.26E-02 2.36E-02 4.64E-02

1836.01 99.38 7.26E-02 1.03E-02 2.93E-02

MO-93 263.06 56. 72 9.83E-02 6.44E-02 8.85E-03 4.67E-02

684.67 99.68 7.07E-02 -1.62E-02 3.25E-02

1477.11 99.08 6.44E-02 -9.45E-03 2.70E-02

NB-93M 16.57 9.43 1.28E+00 l.28E+00 0.00E+00 0.00E+00

NB-94 702.63 100.00 8.49E-02 8.49E-02 -3.69E-03 3.95E-02

871.10 100.00 9.0lE-02 l.32E-03 4.16E-02

+ NB-95 765.79 * 99.81 1.82E-01 l.82E-01 8.86E-02 8.57E-02

NB-95M 235.69 25.00 4.04E+0l 4.04E+0l -3.76E+02 1.93E+0l

ZR-95 724.18 43.70 2.73E-01 l.98E-01 8.37E-02 l.27E-01

756.72 55.30 l.98E-01 -2.62E-02 9.14E-02

MO-99 181.06 6.20 8.06E+02 5.41E+02 -1.20E+0l 3.88E+02

739.58 12.80 5. 41E+02 1.88E+02 2.50E+02

778.00 4.50 1.53E+03 -l.09E+02 7.02E+02

TC-99M 140.51 89.00 6.00E-02 6.00E-02 1.86E-02 2.89E-02

RU-103 497.08 89.00 1.0lE-01 1.0lE-01 8.llE-03 4.66E-02

RU-106 621. 8 4 9.80 8.42E-01 8.42E-01 3.58E-01 3.92E-01

AG-108M 433.93 89.90 6.31E-02 6.31E-02 -2.42E-03 2.93E-02

614.37 90.40 8.34E-02 -l.17E-02 3.88E-02

722.95 90.50 8.78E-02 -5.66E-02 4.06E-02

CD-109 88.03 3.72 2.02E+00 2.02E+00 3.08E+00 9.85E-01

AG-ll0M 657.75 93.14 8.34E-02 8.34E-02 -l.12E-02 3.85E-02

677.61 10.53 7.97E-01 2.90E-01 3.70E-01

706.67 16.46 5.24E-01 -l.58E-03 2.43E-01

763.93 21.98 4.40E-01 l.91E-02 2.04E-01

884.67 21.98 4.21E-01 4.48E-02 1.93E-01

1384.27 23.94 3.51E-01 6.13E-02 l.53E-01

CD-113M 263.70 0.02 2.42E+02 2.42E+02 2.18E+0l l.15E+02

SN-113 255.12 1. 93 3.27E+00 9.68E-02 -9.36E-02 1.56E+00

391.69 64.90 9.68E-02 -3.95E-02 4.51E-02

TE-123M 159.00 84.10 6.83E-02 6.83E-02 -2.95E-02 3. 27E-02

SB-124 602.71 97.87 8.97E-02 8.97E-02 -9.49E-03 4.13E-02

645.85 7.26 1.56E+00 4.18E-01 7.30E-01

722.78 11.10 9.75E-01 -6.29E-01 4.51E-01

1691.02 49.00 2.08E-01 4.95E-02 8.85E-02

I-125 35.49 6.49 1.86E+00 1.86E+00 -2.29E-0l 8.86E-01

SB-125 176.33 6.89 8.38E-01 1.98E-01 1.12E-01 4.03E-0l

427.89 29.33 l.98E-01 -1.90E-03 9.20E-02

463.38 10.35 6.79E-01 5.24E-0l 3.19E-01

600.56 17.80 3.96E-01 1.66E-0l l.84E-01

635.90 11. 32 6.30E-01 2.84E-01 2.91E-0l

SB-126 414.70 83.30 7.40E-02 7.40E-02 1.15E-02 3.47E-02

666.33 99.60 8.l0E-02 -9.37E-02 3.77E-02

695.00 99.60 8.06E-02 4.18E-03 3.74E-02

720.50 53.80 l.46E-01 1.34E-02 6.74E-02

SN-126 87.57 37.00 1.83E-01 l.83E-01 -3.56E-01 8.89E-02

SB-127 473.00 25.00 2.67E+0l 2.48E+0l -1.97E+00 1.23E+0l

685.00 35.70 2.48E+0l -5.68E+00 l.14E+0l

783.80 14.70 7.81E+0l 3.05E+0l 3.63E+0l

I-129 29.78 57.00 2.27E-01 2.27E-01 -7. llE-03 l.08E-01

33.60 13.20 7.98E-01 l.63E-01 3.81E-01

39.58 7.52 9.83E-01 -3.57E-03 4.69E-01

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Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level

Name (keV) (pCilgrams) (pCi!grams) (pCi!grams) (pCi!grams)

I-131 284.30 6.05 9.14E+00 6.63E-01 2.62E+00 4.33E+00

364.48 81.20 6.63E-01 -4.12E-01 3.l0E-01

636.97 7.26 9.80E+00 2.75E+00 4.52E+00

722.89 1. 80 4.48E+0l -2.89E+0l 2.07E+0l

TE-132 49.72 13. 10 1.26E+02 1.85E+0l -l.80E+02 6.02E+0l

228.16 88.00 1.85E+0l -9.26E-01 8.84E+00

BA-133 81.00 33.00 l.79E-01 9.70E-02 -l.20E-01 8.69E-02

302.84 17.80 3.23E-01 l.25E-01 l.53E-01

356.01 60.00 9.70E-02 3.53E-02 4.57E-02

I-133 529.87 86.30 1.34E+08 1.34E+08 -7.12E+07 6.12E+07

XE-133 81.00 38.00 5.41E+00 5.41E+00 -3.62E+00 2.62E+00

CS-134 563.23 8.38 7.75E-01 6.92E-02 3.62E-01 3.58E-01

569.32 15.43 4.08E-01 7.50E-02 l.88E-01

604.70 97.60 6.92E-02 -1.91E-02 3.19E-02

795.84 85.40 l.15E-01 7.89E-02 5.35E-02

801.93 8.73 9.59E-01 -6.06E-03 4.41E-01

CS-135 268.24 16.00 3.75E-01 3.75E-01 4.80E-02 l.79E-01

@ I-135 1131.51 22.50 1.00E+26 1.00E+26 l.00E+26 l.00E+20

@ 1260.41 28.60 1.00E+26 l.00E+26 1.00E+20

@ 1678.03 9.54 1.00E+26 1.00E+26 1.00E+20

CS-136 153.22 7.46 3.04E+00 3.02E-01 4.94E-01 1.47E+00

163.89 4.61 4.80E+00 2.14E+00 2.31E+00

176.55 13.56 1.72E+00 2.30E-01 8.29E-01

27 3. 65 12.66 1.89E+00 -4.22E-01 9.02E-01

340.57 48.50 7.03E-01 1.28E+00 3.38E-01

818.50 99.70 3.02E-01 -4.12E-02 1.37E-01

1048.07 79.60 4.68E-01 -1. 72E-01 2.13E-01

1235.34 19.70 2.65E+00 1.63E-01 1.23E+00

CS-137 661.65 85.12 l.16E-01 1.16E-01 4.18E-02 5.45E-02

LA-138 788.74 34.00 2.62E-01 l.36E-01 8.54E-02 l.22E-01

1435.80 66.00 1.36E-01 3.22E-02 6.05E-02

CE-139 165.85 80.35 7.43E-02 7.43E-02 -3. 71E-02 3.57E-02

BA-140 162.64 6.70 3.29E+00 1.09E+00 -8. 72E-01 1.58E+00

304.84 4.50 5.13E+00 3.35E-01 2.42E+00

423.70 3.20 7.16E+00 -1.03E+00 3.32E+00

437.55 2.00 1.27E+0l -3.80E-01 5.92E+00

537.32 25.00 1.09E+00 4.73E-01 5.07E-01

LA-140 328.77 20.50 1.29E+00 2.99E-01 8.69E-01 6.llE-01

487.03 45.50 5.91E-01 -7.75E-03 2.75E-01

815.85 23.50 1.16E+00 -1.0lE+00 5.19E-01

1596.49 95.49 2.99E-01 -1.20E-02 1.25E-01

CE-141 145.44 48.40 1.98E-01 1.98E-01 -2.21E-02 9.56E-02

CE-143 57.36 11. 80 4.61E+05 l.54E+05 -2.92E+05 2.24E+05

293.26 42.00 1.54E+05 1.62E+05 7.45E+04

664.55 5.20 l.53E+06 2.05E+06 7.26E+05

CE-144 133.54 10.80 5.14E-01 5.14E-01 -2.83E-01 2.47E-01

PM-144 476.78 42.00 l.71E-01 8.21E-02 9.66E-02 8.0lE-02

618.01 98.60 8.21E-02 7.25E-03 3.82E-02

696.49 99.49 8. 51E-02 -2.87E-02 3.95E-02

PM-145 36.85 21.70 3.91E-01 2.08E-01 l.13E-01 1.86E-01

37.36 39.70 2.08E-01 5.98E-02 9.90E-02

42.30 15.10 4.66E-01 8.42E-02 2.23E-01

72. 40 2.31 3.15E+00 3.09E-01 1.53E+00

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Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level

Name (keV) (pCilgrams) (pCi/grams) (pCilgrams) (pCi/grams)

PM-146 453.90 39.94 l.52E-01 1.52E-01 -8.38E-02 7.08E-02

735.90 14.01 5.37E-01 -5.15E-02 2.47E-01

747.13 13.10 6.29E-01 -4.77E-03 2.91E-01

ND-147 91.11 28.90 1.39E+00 1.39E+00 6.93E-01 6.77E-01

531.02 13.10 2.37E+00 -5.86E-01 1.09E+00

PM-149 285.90 3.10 8.26E+03 8.26E+03 -1.68E+03 3.92E+03

EU-152 121.78 20.50 2.54E-01 2.54E-01 1.78E-0l 1.22E-01

244.69 5.40 1.19E+00 1.22E-0l 5.70E-01

34 4. 27 19.13 2.92E-01 -4. 21E-02 1.37E-01

778.89 9.10 9.07E-01 1.56E-01 4.18E-01

964.01 10.40 1.0lE+00 1.58E-01 4.66E-01

1085.78 7.22 1.24E+00 2.67E-03 5.62E-01

1112.02 9.60 1.00E+00 1. llE-01 4.56E-01

1407.95 14.94 5.84E-01 9.19E-02 2.59E-01

GD-153 97.43 31.30 1.92E-01 1.92E-01 -2. 96E-01 9.32E-02

103.18 22.20 2.52E-01 -2.72E-01 1.21E-01

EU-154 123.07 40.50 1.27E-01 1.27E-0l -6.72E-02 6. llE-02

723.30 19.70 4.20E-01 -1.84E-01 1.95E-01

873.19 11. 50 7.74E-01 5.57E-01 3.57E-01

996. 32 10.30 8.26E-01 -3.23E-01 3.75E-01

1004.76 17.90 5.40E-01 1.23E-01 2.48E-01

1274.45 35.50 2.50E-01 -4.37E-02 1.12E-01

EU-155 86.50 30.90 2.30E-01 2.30E-01 3.54E-01 1.12E-01

105.30 20.70 2.57E-01 1.98E-01 1.24E-01

EU-156 811.77 10.40 2.35E+00 2.35E+00 3.31E-01 1.07E+00

1153.47 7.20 4.66E+00 1.22E+00 2.13E+00

1230.71 8.90 4.l0E+00 5.79E-01 1.88E+00

HO-166M 184.41 72. 60 9.85E-02 9.85E-02 8.03E-02 4.78E-02

280.45 29.60 1.79E-01 -1.23E-0l 8.49E-02

410.94 11.10 5.21E-01 -1. 0lE-01 2.44E-01

711.69 54.10 1.48E-01 3.09E-02 6.83E-02

TM-171 66. 72 0.14 5.30E+0l 5.30E+0l -2.29E+0l 2.58E+0l

HF-1 72 67.35 5.31 1.33E+00 4.81E-0l -8.30E-01 6.47E-01

125.82 11.30 4.81E-01 -3.81E-01 2.32E-01

LU-1 72 181.53 20.60 4.49E+00 2.14E+00 -6.68E-02 2.16E+00

900. 72 29.81 4.16E+00 -2.46E+00 1.89E+00

1093.66 62.50 2.14E+00 -4.43E-01 9.63E-01

LU-173 100.72 5.24 1.15E+00 2.97E-01 1.04E+00 5.55E-01

272.11 21. 20 2.97E-01 5.27E-02 l.42E-01

HF-175 343.40 84.00 8. 76E-02 8.76E-02 5.19E-03 4.12E-02

LU-176 88.34 13.30 5.42E-01 5.49E-02 8.27E-01 2.65E-01

201.83 86.00 6.73E-02 5.25E-03 3.23E-02

306.78 94.00 5.49E-02 1.71E-02 2.58E-02

HF-181 133.02 41.70 1.93E-01 l.14E-01 -1.06E-01 9.30E-02

345.85 17.20 5.30E-01 3.llE-01 2.50E-01

482.03 82.80 1.14E-01 1.42E-02 5.29E-02

TA-182 67.75 41.20 1.94E-01 1.94E-01 -1.18E-0l 9.44E-02

1121.30 34.90 4.39E-01 4.l0E-01 2.05E-01

1189.05 16.23 7.66E-01 4.02E-02 3.51E-01

1221.41 26.98 4.86E-01 -3.66E-02 2.23E-01

1231.02 11. 44 1.l0E+00 1.56E-01 5.04E-01

IR-192 308.46 29.68 2.21E-01 1.44E-01 4.63E-02 1.04E-01

468.07 48.10 1.44E-01 -6.36E-03 6.65E-02

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Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level

Name (keV) (pCi!grams) (pCi!grams) (pCi/grams) (pCi/grams)

HG-203 279.19 77.30 1.l0E-01 1.l0E-01 3.79E-02 5.24E-02

TL-204 374.74 94.11 5.68E-02 5.68E-02 -1.96E-02 2.65E-02

899.15 99.16 7.74E-02 -3.74E-02 3.50E-02

911.74 91.10 1.65E-01 2.78E-01 7.84E-02

BI-207 569.67 97. 72 6.30E-02 6.30E-02 1.16E-02 2.90E-02

1063.62 74.90 1.24E-01 -1.44E-02 5.64E-02

+ TL-208 583.14 * 30.22 3.80E-01 l.34E-01 9.75E-01 1.82E-01

860.37 * 4.48 1.56E+00 1.17E+00 7.05E-01

2614.66 * 35.85 1.34E-01 6.58E-01 4.92E-02

BI-210M 262.00 45.00 l.24E-01 1.24E-01 -5.81E-02 5.92E-02

300.00 23.00 2.50E-01 5.41E-02 1.19E-01

+ PB-210 46.50 * 4.25 2.15E+00 2.15E+00 2.l0E+00 1.04E+00

PB-211 404.84 2.90 1.86E+00 1.86E+00 3.30E-01 8.68E-01

831.96 2.90 2.78E+00 -1.16E+00 l.28E-t-00

BI-212 727.17 11. 80 7.73E-01 7.73E-01 2.14E-01 3.61E-01

1620.62 2.75 2.85E+00 1.39E+00 1.23E+00

+ PB-212 238.63 * 44.60 2.35E-01 2.35E-01 1.44E+00 1.15E-01

300.09 3.41 1.69E+00 3.65E-01 8.0lE-01

+ BI-214 609.31 * 46.30 2.46E-01 2.46E-01 1.l0E+00 l.17E-01

1120.29 * 15.10 9.68E-01 6.62E-01 4.56E-01

1764.49 * 15.80 5.72E-01 8. 72E-01 2.50E-01

2204.22 * 4.98 2.49E-01 2.30E+00 0.00E+00

+ PB-214 295.21 * 19.19 6.61E-01 2.42E-01 1.17E+00 3.23E-01

351.92 * 37.19 2.42E-01 1.09E+00 1.16E-01

RN-219 401.80 6.50 8.80E-01 8.80E-01 3.65E-01 4.12E-01

RA-223 323.87 3.88 1.38E+00 l.38E+00 -4.64E-01 6.51E-01

RA-224 240.98 3.95 2.70E+00 2.70E+00 4. 72E+00 l.32E+00

RA-225 40.00 31.00 8.l0E-01 8.l0E-01 -3.54E-01 3.86E-01

+ RA-226 186.21 * 3.28 3.18E+00 3.18E+00 3.03E+00 1.56E+00

TH-227 50.10 8.40 6.33E-01 6.33E-01 7.63E-02 3.02E-01

236.00 11. 50 7.66E-01 -1.86E+00 3. 72E-01

256.20 6 •' 30 8.99E-01 -3.36E-01 4.29E-01

+ AC-228 338.32 * 11. 40 8.59E-01 3.52E-01 1.15E+00 4.15E-01

911.07 * 27.70 3.52E-01 8.60E-01 1.63E-01

969 .11 * 16.60 6.61E-01 7.38E-01 3.07E-01

TH-230 48.43 16.90 4.07E-01 4.07E-01 4.llE-01 1.96E-01

62.85 4.60 1.70E+00 1.42E+00 8.30E-01

67. 67 0.37 1.85E+0l -1.16E+0l 9.0lE+00

+ PA-231 283.67 1. 60 3.33E+00 3.33E+00 1.61E+00 1.58E+00

302. 67 * 2.30 5.53E+00 1.37E+00 2.70E+00

TH-231 25.64 14.70 7.27E-02 7. 27E-02 0.00E+00 0.00E+00

84.21 6.40 9.87E-01 -9.35E-01 4.79E-01

PA-233 311.98 38.60 2.81E-01 2.81E-01 3.67E-02 1.33E-01

PA-234 131.20 20.40 2.62E-01 2.62E-01 9.15E-03 1.27E-01

733.99 8.80 8.54E-01 -2.88E-01 3.93E-01

946.00 12.00 6.76E-01 5.54E-03 3.07E-01

PA-234M 1001.03 0.92 1.08E+0l 1.08E+0l 3.68E+00 5.00E+00

TH-234 63.29 3.80 2.05E+00 2.05E+00 1.72E+00 1.00E+00

U-235 143.76 10.50 5.06E-01 5.06E-01 4.80E-02 2.44E-01

163.35 4.70 1.13E+00 4.91E-01 5.42E-01

205.31 4.70 1.17E+00 -5.06E-01 5.60E-01

NP-237 86.50 12.60 5.58E-01 5.58E-01 8.60E-01 2. 72E-01

NP-239 106.10 22.70 6.19E+02 6.19E+02 2.97E+02 2.99E+02

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4/17/2018 6:43:09AM Page 29 of29

Analysis Report for 1803111-03

AC-SED-11

Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level

Name (keV) (pCilgrams) (pCi/grams) (pCilgrams) (pCi/grams)

NP-239 228.18 10.70 1.36E+03 6.19E+02 -6.81E+0l 6.50E+02

277.60 14.10 1.17E+03 4.66E+02 5.60E+02

AM-241 59.54 35.90 2.05E-01 2.05E-01 1.49E-01 9.97E-02

AM-243 74.67 66.00 1.29E-01 1.29E-01 -4.57E-01 6.30E-02

CM-243 209.75 3.29 1.78E+00 4.36E-01 3.99E-01 8.53E-01

228.14 10.60 5.07E-0l -2.53E-02 2.42E-01

277.60 14.00 4.36E-0l l.73E-0l 2.08E-01

+ = Nuclide identified during the nuclide identification

* = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

No Action Level results available for reporting purposes.

DATA REVIEW COMMENTS REPORT

Creation Date Comment User

No Data Review Comments Entered.

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Channel Data Report 4/17/2018 6: 43: 33 AM Page 1

*******************************************************

***** S P E C T R A L D A T A R E P O R T *****

*******************************************************

Sample Title: AC-SED-11

Elapsed Live time: 3600 Elapsed Real Time: 3601

Channell------1-------l-------l-------1-------1-------1-------1-------I

1: 0 0 0 0 0 0 0 0

9: 0 0 0 0 0 0 0 0

17: 0 0 0 0 0 0 0 0

25: 0 0 0 22 28 42 46 50

33: 51 45 44 43 44 54 40 48

41: 49 54 58 51 51 78 125 63

49: 42 45 59 51 66 79 63 57

57: 61 90 81 84 85 73 132 117

65: 84 78 85 82 78 78 97 84

7 3: 96 129 241 136 341 175 76 68

81: 58 75 61 109 81 70 124 114

89: 71 148 65 107 159 104 73 43

97: 48 65 83 77 44 66 53 36

105: 66 65 53 43 53 46 58 45

113: 61 55 41 49 51 34 43 47

121: 40 60 50 54 37 62 54 50

129: 73 48 56 43 36 51 52 61

137: 42 55 58 52 42 36 45 64

145: 49 41 44 59 40 47 49 51

153: 55 44 42 45 48 31 39 33

161: 33 41 54 36 46 38 39 41

169: 42 41 43 39 45 40 36 57

177: 44 46 41 44 42 44 51 49

185: 74 126 67 36 39 38 38 44

193: 44 41 36 41 44 39 37 44

201: 45 49 35 27 40 40 34 35

209: 58 36 31 33 35 38 36 37

217: 34 45 36 30 33 37 28 39

225: 23 28 25 27 26 40 35 28

233: 23 31 29 43 39 250 296 62

241: 90 92 24 24 24 28 22 26

249: 20 27 34 19 17 27 19 29

257: 34 31 44 26 21 33 23 29

265: 23 24 30 29 26 39 32 27

273: 22 28 26 29 37 32 21 22

281: 14 18 24 18 32 19 23 26

289: 27 22 20 26 22 40 159 61

2 97: 25 18 19 19 25 34 17 17

305: 18 11 16 26 15 17 19 20

313: 21 19 20 11 22 21 20 18

321: 15 16 26 18 13 15 24 34

329: 19 23 18 21 23 25 24 21

337: 20 80 65 20 22 15 14 17

345: 21 19 25 13 15 23 109 246

353: 53 18 13 21 18 19 14 32

361: 23 11 13 22 14 11 17 24

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Channel Data Report 4/17/2018 6:43:33 AM Page 2

369: 12 11 18 15 15 11 6 20

Sample Title: AC-SED-11

Channell------l-------l-------1-------1-------1-------I-------I-------I

377: 15 14 16 20 20 14 10 23

385: 22 9 14 19 9 14 14 18

393: 9 14 15 10 12 13 10 15

401: 16 14 16 9 14 9 19 23

409: 14 16 14 9 17 24 12 17

417: 16 12 8 18 6 5 14 12

425: 19 10 13 9 12 11 14 10

433: 15 13 13 10 11 14 18 14

441: 12 8 11 11 13 18 16 15

449: 17 21 14 11 12 14 13 16

457: 16 12 10 8 9 32 22 9

465: 11 12 8 9 9 10 7 9

473: 10 8 11 10 26 22 16 7

481: 13 9 15 15 8 16 9 12

489: 17 7 14 11 15 8 17 8

497: 5 7 10 10 5 10 15 6

505: 11 6 10 7 20 50 45 23

513: 19 14 7 5 7 12 7 5

521: 15 16 10 12 4 12 9 11

529: 4 9 5 10 15 10 11 17

537: 9 9 8 5 5 12 10 10

545: 11 11 9 14 11 13 6 9

553: 9 12 8 10 10 16 8 1

561: 7 8 14 11 9 8 8 8

569: 9 12 8 5 10 12 7 9

577: 10 5 10 12 14 53 107 33

585: 5 7 11 10 8 7 8 10

593: 6 12 9 12 5 10 12 14

601: 12 5 8 6 15 13 9 64

609: 164 53 13 8 11 6 7 7

617: 9 10 6 11 13 8 9 8

625: 5 7 8 13 7 4 3 3

633: 7 7 7 5 8 12 3 9

641: 6 6 10 9 6 14 13 11

649: 10 8 8 7 13 3 9 8

657: 6 8 4 11 24 30 9 8

665: 15 14 6 4 5 7 10 4

67 3: 9 6 10 8 11 5 6 9

681: 5 6 7 4 6 9 6 9

689: 5 7 10 8 6 4 12 9

697: 7 10 8 12 9 10 9 7

705: 7 9 10 5 7 7 6 7

713: 9 12 5 2 7 10 5 6

721: 7 8 7 10 8 9 16 9

729: 10 6 9 8 7 9 1 4

737: 8 6 5 7 5 14 5 6

745: 5 3 6 10 11 10 9 6

753: 6 8 7 5 9 10 5 8

7 61: 10 4 4 9 9 16 10 17

769: 19 5 13 10 8 4 5 7

777: 5 8 4 11 8 8 4 6

785: 13 9 7 6 7 7 7 5

793: 9 13 15 11 8 3 4 4

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Channel Data Report 4/17/2018 6:43:33 AM Page 3

801: 11 5 8 10 9 8 5 6

Sample Title: AC-SED-11

Channell------1-------1-------1-------1-------I-------I-------I-------I

809: 5 8 7 4 2 1 4 2

817: 3 9 6 6 4 9 9 6

825: 10 8 3 3 6 5 9 2

833: 6 10 12 8 5 9 7 9

841: 6 7 9 3 5 3 9 7

849: 3 4 6 2 7 4 9 6

857: 8 4 9 13 10 3 2 2

865: 7 6 8 6 5 8 6 9

873: 6 5 9 3 2 1 7 4

881: 6 5 3 7 7 9 5 4

889: 7 3 6 2 6 8 5 6

897: 2 5 6 3 4 4 8 10

905: 7 7 6 8 9 35 55 13

913: 2 6 3 5 7 4 2 5

921: 7 8 5 8 4 2 3 4

92 9: 6 8 12 10 9 5 4 3

937: 6 3 5 2 4 4 5 3

945: 10 6 1 4 8 9 5 2

953: 5 4 5 7 5 1 3 1

961: 4 6 7 13 14 10 16 25

969: 25 10 3 7 7 3 8 3

977: 6 2 4 5 6 6 5 4

985: 3 6 6 2 7 3 6 2

993: 5 3 4 5 4 4 8 9

1001: 8 10 4 3 8 6 4 5

1009: 1 2 2 5 2 6 5 5

1017: 4 3 3 3 12 3 7 7

1025: 8 6 2 5 6 3 8 5

1033: 5 5 7 5 7 6 6 3

1041: 6 4 6 3 5 5 4 6

1049: 8 4 8 8 5 2 5 7

1057: 8 5 2 3 7 8 5 8

1065: 3 2 7 7 5 3 4 6

1073: 3 4 1 3 2 4 3 5

1081: 8 4 4 4 4 6 8 2

1089: 4 2 2 4 4 4 1 10

1097: 3 10 6 7 2 5 3 5

1105: 3 4 3 4 6 3 6 10

1113: 6 1 8 3 5 7 19 23

1121: 8 3 5 4 5 4 6 2

1129: 6 4 4 5 5 4 4 4

1137: 6 4 6 5 5 3 4 7

1145: 8 4 7 3 5 5 2 4

1153: 5 5 5 10 5 3 2 7

1161: 5 5 10 7 4 6 5 5

1169: 3 2 6 9 6 6 9 3

1177: 5 5 6 3 6 4 4 4

1185: 6 8 4 3 10 4 5 6

1193: 7 10 3 5 6 9 2 5

1201: 6 9 5 4 4 3 6 4

1209: 6 4 5 10 7 9 3 5

1217: 8 6 4 8 7 4 4 10

1225: 6 7 6 11 3 4 4 6

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Channel Data Report 4/17/2018 6:43:33 AM Page 4

1233: 5 3 8 10 20 12 2 1

Sample Title: AC-SED-11

Channell------l-------1-------1-------1-------I-------I-------I-------I

1241: 7 1 1 9 7 8 5 3

1249: 3 7 2 3 2 5 4 2

1257: 10 6 3 10 2 3 3 3

1265: 4 2 2 3 3 4 3 4

1273: 4 2 3 5 3 5 4 8

1281: 6 3 7 2 6 5 2 1

1289: 2 2 3 3 7 2 5 3

1297: 2 5 4 1 1 5 1 4

1305: 6 2 1 4 4 6 3 0

1313: 5 3 6 2 1 0 5 3

1321: 1 2 0 0 0 5 3 3

1329: 1 2 3 4 8 4 6 4

1337: 3 4 3 1 1 1 4 5

1345: 1 1 2 1 4 1 6 2

1353: 5 3 0 2 1 4 1 3

1361: 3 1 1 1 1 4 2 2

1369: 3 2 4 4 1 3 6 7

1377: 16 3 4 5 1 1 3 2

1385: 1 3 2 1 4 2 3 1

1393: 1 2 2 0 1 1 6 3

1401: 4 5 3 4 0 2 6 3

1409: 2 3 1 1 0 2 3 2

1417: 0 4 1 3 2 1 2 1

1425: 2 1 2 4 2 2 3 4

1433: 3 4 3 3 0 4 2 2

1441: 3 0 0 2 1 1 0 2

1449: 3 1 5 3 2 3 2 8

1457: 6 44 127 201 102 11 0 3

1465: 3 0 1 2 3 3 0 2

1473: 1 2 2 2 0 1 1 0

1481: 4 1 1 1 3 3 2 2

1489: 0 1 1 5 1 3 4 0

1497: 0 2 1 0 2 1 2 1

1505: 1 1 1 8 4 3 4 3

1513: 1 0 1 2 1 0 3 1

1521: 1 1 1 0 0 1 1 0

152 9: 0 2 2 1 4 1 3 1

1537: 2 1 5 2 1 2 2 0

1545: 1 3 2 1 1 0 0 3

1553: 1 1 1 0 2 0 1 2

1561: 1 1 0 2 0 0 0 1

1569: 0 1 2 0 1 2 1 3

1577: 0 1 3 2 3 1 3 2

1585: 1 3 6 3 3 1 3 1

1593: 0 0 1 2 4 1 1 0

1601: 1 0 1 1 0 0 2 2

1609: 0 0 1 0 2 1 0 1

1617: 1 2 3 3 2 1 1 1

1625: 0 3 0 2 2 2 2 1

1633: 0 0 1 0 2 2 5 1

1641: 0 1 2 0 2 0 1 0

164 9: 0 2 2 0 0 2 0 0

1657: 0 1 1 2 2 3 1 1

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Channel Data Report 4/17/2018 6:43:33 AM Page 5

1665: 0 0 0 2 0 2 0 0

Sample Title: AC-SED-11

Channell------l-------1-------1-------1-------I-------I-------I-------I

1673: 0 0 0 0 1 1 2 1

1681: 0 1 2 1 1 2 2 1

1689: 2 0 1 4 1 0 1 1

1697: 2 0 2 1 1 1 0 1

1705: 0 1 2 0 2 0 1 0

1713: 0 1 1 2 0 0 3 1

1721: 0 0 1 0 1 1 1 4

1729: 5 0 1 1 0 2 0 1

1737: 2 2 3 0 0 1 1 0

1745: 2 1 0 0 0 2 0 0

1753: 0 0 1 3 3 2 2 0

1761: 3 6 11 15 7 1 1 0

1769: 2 2 1 1 0 1 1 1

1777: 1 0 0 1 1 0 0 0

1785: 0 2 1 2 3 0 3 1

1793: 0 0 1 0 0 0 1 4

1801: 1 1 1 2 1 1 1 0

1809: 0 0 2 1 1 0 1 1

1817: 0 0 1 0 1 0 1 1

1825: 1 0 0 0 1 4 0 2

1833: 1 0 0 1 1 1 0 0

1841: 0 0 0 0 0 1 4 1

1849: 1 2 2 0 0 0 0 1

1857: 1 2 0 1 0 0 0 0

1865: 1 0 0 0 1 1 0 0

1873: 0 1 2 0 0 1 1 0

1881: 1 0 0 1 2 1 3 1

1889: 0 0 3 0 2 5 0 0

1897: 1 0 0 1 1 1 2 1

1905: 1 1 3 1 1 1 2 1

1913: 0 1 1 1 0 2 0 2

1921: 2 1 0 0 0 0 0 2

1929: 1 2 3 0 0 1 1 0

1937: 0 0 1 0 2 0 0 0

1945: 0 0 1 0 0 0 0 3

1953: 1 0 0 3 0 0 1 0

1961: 2 3 0 0 1 1 1 2

1969: 0 1 1 0 1 0 1 1

1977: 0 1 1 1 1 0 0 0

1985: 0 0 1 2 0 1 1 0

1993: 0 1 0 0 1 0 0 0

2001: 2 0 0 0 1 1 0 0

2009: 0 2 1 0 0 0 1 2

2017: 0 0 1 0 1 1 0 0

2025: 2 2 2 0 0 0 1 1

2033: 1 0 1 0 1 1 0 1

2041: 0 2 0 2 1 0 0 3

2049: 0 0 1 0 1 1 0 0

2057: 0 0 3 1 1 0 0 1

2065: 1 0 1 1 0 0 0 0

2073: 0 1 0 2 0 0 0 0

2081: 1 0 1 2 0 0 0 2

2089: 1 2 0 1 0 0 0 3

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Channel Data Report 4/17/2018 6:43:33 AM Page 6

2097: 1 1 2 3 0 2 3 1

Sample Title: AC-SED-11

Channell------l-------l-------1-------1-------1-------I-------I-------I

2105: 1 1 2 1 1 2 0 2

2113: 0 1 1 4 2 1 0 1

2121: 1 0 0 1 0 2 1 0

212 9: 0 0 1 0 2 0 0 0

2137: 0 2 1 1 1 0 0 1

2145: 0 0 1 1 1 1 1 0

2153: 0 0 1 3 2 1 1 1

2161: 0 0 0 2 2 0 1 1

2169: 2 0 1 0 0 0 1 1

2177: 1 1 1 0 2 0 0 2

2185: 1 0 0 0 0 2 0 0

2193: 0 1 0 0 0 0 0 4

2201: 3 5 7 4 1 1 0 0

2209: 0 1 0 0 1 1 0 0

2217: 2 0 0 1 2 0 2 1

2225: 0 1 1 0 0 0 2 1

2233: 1 0 0 1 1 2 0 0

2241: 0 3 2 2 1 1 1 0

2249: 0 1 2 1 1 1 1 1

2257: 0 0 2 0 1 0 0 1

2265: 0 1 0 0 1 0 0 1

2273: 0 0 1 0 1 0 0 1

2281: 0 2 1 1 3 0 0 0

2289: 1 0 0 0 0 2 2 1

2297: 0 1 0 2 2 0 0 1

2305: 0 1 1 0 0 0 1 2

2313: 2 0 1 1 3 0 1 2

2321: 0 0 0 2 1 1 1 0

2329: 0 1 0 0 1 2 0 1

2337: 1 1 1 0 0 0 1 1

2345: 2 2 0 1 0 1 0 0

2353: 1 1 0 0 0 0 0 0

2361: 0 1 2 3 0 3 1 1

2369: 0 1 1 1 0 1 2 1

2377: 0 1 1 0 0 0 1 0

2385: 0 0 0 1 0 0 1 1

2393: 1 1 2 0 0 0 3 0

2401: 0 0 0 0 0 0 0 0

2409: 0 0 0 1 0 0 0 2

2417: 0 0 1 1 0 0 0 0

2425: 2 0 1 0 0 0 3 3

2433: 0 2 1 0 0 0 1 1

2441: 1 0 2 0 2 0 0 1

2449: 0 1 0 0 0 0 1 0

2457: 0 1 0 0 1 1 1 0

2465: 1 0 1 1 0 0 0 0

2473: 0 0 0 3 0 0 0 1

2481: 1 0 0 0 0 1 0 0

2489: 1 0 0 0 1 1 2 0

2497: 1 1 2 1 0 0 0 0

2505: 0 0 0 0 0 0 0 1

2513: 1 0 2 1 0 1 0 0

2521: 0 0 0 0 0 1 0 0

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Channel Data Report 4/17/2018 6:43:33 AM Page 7

2529: 0 1 0 2 0 1 0 0

Sample Title: AC-SED-11

Channell------l-------l-------l-------1-------1-------l-------1-------I

2537: 0 0 1 0 1 0 0 0

2545: 0 0 0 1 0 1 0 2

2553: 0 0 0 1 1 0 0 0

2561: 0 0 0 0 1 1 0 2

2569: 0 0 1 0 1 1 1 1

2577: 0 2 0 0 0 0 0 0

2585: 0 1 0 0 0 1 0 1

2593: 0 1 0 1 0 0 1 0

2601: 1 1 1 0 0 0 0 1

2609: 2 5 6 11 17 6 5 2

2617: 0 0 1 0 2 0 0 1

2625: 0 0 0 1 1 1 0 0

2633: 0 0 0 0 0 0 0 0

2641: 1 1 0 0 0 0 0 1

2649: 0 0 0 0 0 0 1 0

2657: 0 0 0 0 0 0 0 0

2665: 0 0 0 0 0 0 0 0

2673: 3 0 0 0 1 0 1 0

2681: 1 0 0 1 0 2 0 0

2 68 9: 1 0 0 0 0 1 0 0

2697: 1 0 0 0 0 0 0 1

2705: 0 0 0 1 0 1 0 0

2713: 0 0 0 1 1 1 0 1

2721: 0 0 0 0 0 0 0 0

2729: 0 0 1 0 0 0 0 0

2737: 0 0 0 0 0 0 0 1

2745: 0 0 0 0 0 0 0 0

2753: 0 0 1 1 0 0 1 0

2761: 0 0 0 0 0 0 0 0

2769: 0 0 0 0 2 0 0 0

2777: 0 0 0 0 1 0 0 1

2785: 1 1 0 0 0 1 0 0

2793: 0 1 2 1 1 1 0 1

2801: 0 0 0 0 0 0 1 0

2809: 0 0 1 0 0 0 0 0

2817: 0 0 0 0 1 0 1 0

2825: 0 0 0 0 0 0 0 0

2833: 0 0 2 0 0 0 0 0

2841: 0 0 0 0 0 0 0 0

2849: 0 0 0 0 0 1 0 0

2857: 0 0 0 0 0 0 1 1

2865: 0 0 1 1 0 0 0 0

2873: 0 0 0 0 0 0 0 0

2881: 1 1 0 2 0 0 0 1

2889: 0 0 0 0 0 0 0 0

2897: 0 0 0 1 0 0 0 0

2905: 0 0 0 0 0 0 2 0

2913: 0 0 0 0 0 2 0 0

2921: 1 1 0 0 0 0 0 0

2929: 0 0 0 0 1 1 0 0

2937: 0 0 0 0 0 0 0 0

2945: 1 0 1 0 0 0 0 0

2953: 0 0 1 0 1 0 0 1

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2961: 0 0 0 0 0 0 0 1

Sample Title: AC-SED-11

Channell------l-------l-------l-------1-------1-------1-------I-------I

2969: 0 0 0 1 0 0 0 0

2977: 0 0 1 1 1 0 0 0

2985: 0 0 0 0 0 0 0 0

2993: 1 0 0 0 0 0 1 0

3001: 0 0 0 0 0 0 1 1

3009: 0 0 0 0 0 1 0 0

3017: 0 0 0 0 0 0 0 1

3025: 0 0 0 0 0 0 0 2

3033: 0 0 0 0 1 2 0 0

3041: 1 1 0 1 0 0 0 0

3049: 0 0 0 0 0 0 0 0

3057: 0 0 1 0 0 0 0 0

3065: 0 0 0 0 1 0 0 0

3073: 0 0 0 0 1 0 0 0

3081: 0 0 0 0 0 0 0 1

3089: 0 0 0 0 0 0 1 0

3097: 0 0 0 0 0 1 0 0

3105: 1 0 0 0 0 0 1 0

3113: 0 0 0 0 0 2 0 0

3121: 0 0 0 1 0 0 0 0

3129: 1 0 0 0 0 0 1 0

3137: 0 0 0 1 0 0 0 0

3145: 0 0 0 0 0 0 0 1

3153: 0 1 0 1 0 0 1 0

3161: 0 0 0 0 0 0 2 0

3169: 0 0 1 0 0 0 0 0

3177: 0 0 0 0 0 0 0 0

3185: 0 0 0 0 0 1 1 0

3193: 0 0 0 0 0 3 0 0

3201: 0 0 0 0 0 0 0 0

3209: 0 0 1 0 0 0 1 0

3217: 0 0 0 0 0 0 0 2

3225: 0 0 0 0 1 0 0 0

3233: 0 0 0 0 0 0 0 0

3241: 0 0 1 0 0 0 2 0

3249: 0 1 0 1 0 0 0 0

3257: 0 0 0 0 0 0 0 0

32 65: 0 0 0 0 1 0 0 0

3273: 0 0 0 0 1 0 1 0

3281: 0 0 0 0 0 1 0 0

3289: 0 0 1 0 0 0 0 0

3297: 0 0 0 0 0 0 0 0

3305: 0 0 1 0 0 3 0 0

3313: 0 0 1 1 0 0 0 0

3321: 0 0 1 0 0 0 0 0

3329: 0 0 0 0 1 0 0 0

3337: 0 0 0 0 0 0 0 1

3345: 0 0 0 0 0 0 0 1

3353: 0 0 1 0 1 0 0 0

3361: 0 0 0 0 0 1 0 0

3369: 0 0 0 0 1 0 0 0

3377: 0 0 0 0 0 1 0 1

3385: 0 0 0 0 0 0 0 0

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0255

Channel Data Report 4/17/2018 6:43:33 AM Page 9

3393: 0 0 0 1 0 1 0 0

Sample Title: AC-SED-11

Channell------l-------1-------1-------1-------I-------I-------I-------I

3401: 0 0 0 0 0 0 1 0

3409: 1 0 0 0 0 0 1 1

3417: 0 0 1 0 0 0 0 0

3425: 0 0 0 0 0 1 0 0

3433: 1 0 0 0 0 0 0 0

3441: 0 0 0 0 0 0 0 0

3449: 0 0 0 0 0 0 0 0

3457: 1 0 0 0 0 0 0 0

3465: 0 0 0 1 0 1 0 0

3473: 0 0 0 0 0 0 0 0

3481: 0 0 0 0 0 0 0 1

3489: 0 0 0 0 1 0 1 1

3497: 0 0 0 0 0 0 1 0

3505: 0 0 0 0 0 0 0 0

3513: 0 0 0 1 0 0 1 1

3521: 0 0 0 0 1 0 0 0

3529: 0 1 0 0 1 0 0 0

3537: 0 0 0 0 0 0 0 0

3545: 0 0 0 0 0 0 0 0

3553: 0 0 0 0 0 0 0 0

3561: 0 0 0 1 0 1 0 0

3569: 0 0 0 0 1 0 1 0

3577: 1 0 0 0 0 0 0 0

3585: 0 0 0 0 0 0 0 0

3593: 0 0 0 0 0 0 0 0

3601: 0 0 0 0 0 0 0 0

3609: 0 0 2 0 0 0 0 0

3617: 0 0 0 1 0 0 1 0

3625: 0 0 0 0 0 1 0 0

3633: 0 0 0 0 1 0 0 0

3641: 1 0 0 0 0 0 1 1

3649: 0 0 0 0 0 1 0 1

3657: 0 0 0 0 0 1 0 0

3665: 0 0 0 0 0 0 0 0

3673: 0 0 0 0 0 0 1 0

3681: 0 1 0 0 1 0 0 0

3689: 0 0 0 1 0 0 0 0

3697: 0 0 0 1 0 0 0 0

3705: 1 0 1 0 1 0 0 0

3713: 0 0 0 0 0 0 1 0

3721: 0 0 0 0 1 1 0 0

372 9: 0 0 0 0 0 0 0 0

3737: 1 0 0 0 0 1 0 0

3745: 0 0 0 0 0 0 0 0

3753: 1 0 0 0 0 0 0 0

3761: 0 0 0 0 0 0 0 0

3769: 0 0 0 0 0 0 0 0

3777: 0 0 0 0 0 0 1 0

3785: 0 0 0 0 0 0 0 0

3793: 0 0 0 0 0 0 0 1

3801: 0 0 0 0 1 0 0 0

3809: 0 0 0 1 0 0 0 1

3817: 0 0 0 0 0 0 0 0

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0256

Channel Data Report 4/17/2018 6:43:33 AM Page 10

3825: 0 0 0 0 0 0 0 1

Sample Title: AC-SED-11

Channell------l-------l-------l-------l-------1-------1-------1-------I

3833: 0 0 0 0 0 0 1 0

3841: 0 0 0 1 0 0 0 0

3849: 0 0 0 0 0 0 0 0

3857: 0 0 0 0 0 0 0 0

3865: 0 0 0 0 0 0 0 0

3873: 0 0 0 0 0 0 0 0

3881: 0 1 0 0 0 0 0 0

3889: 1 0 0 0 0 1 0 0

3897: 0 0 0 0 0 0 0 0

3905: 0 0 0 0 0 0 0 0

3913: 0 0 0 0 0 0 1 0

3921: 0 1 0 1 0 0 0 0

3929: 0 0 0 0 1 0 0 0

3937: 0 0 0 0 0 0 0 0

3945: 0 0 0 0 1 0 0 0

3953: 1 0 0 0 0 0 0 1

3961: 0 0 0 0 0 0 0 0

3969: 0 0 0 0 0 0 0 0

3977: 0 0 1 0 0 0 0 0

3985: 0 0 0 1 0 0 0 1

3993: 0 1 0 0 0 0 0 0

4001: 0 0 0 0 0 0 0 0

4009: 0 0 0 0 1 0 0 0

4017: 0 0 0 1 0 1 0 0

4025: 0 0 0 0 1 0 1 0

4033: 0 0 0 0 0 0 0 2

4041: 0 0 1 0 0 0 0 0

4049: 2 0 0 0 0 0 0 0

4057: 0 0 0 0 0 0 1 0

4065: 0 0 0 0 0 0 0 0

4073: 0 0 0 0 0 0 0 0

4081: 0 0 0 0 0 0 0 0

4089: 1 0 0 0 0 0 0 0

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0257

lQS

104

aJ 103 ,-

"" ro .--< u ~ ' V) = ~ o,_

.--< O'I ' 0 =

I o,_

~ r ~ .J-' C> I ~ ci:l i

~ 1Q2 fu r ¥~ 11

101

"" .--<

~

=

00

~ f-

00

' ~

00

~ ~

"" .--< ~ ' ~ =

!

0000064639.CNF

"" .--< ~ t

""

r

00 G>

1

Live Time :3600.000 sec Real Ti me : 3600. 820 sec Start: 1: l.2(kev) Stop : 4096: 4099. 2 (kev) Acq. Start :Tue Apr 17 05 :42: 57 2018

lQ0111u11 ' 1 ' 11 F 111 1' P! 11 '11 ""! 1• II lrnjll,ll'""'""''''l!ll"'j,lllffi111illllll'ftl111Mllllllllillll/llll/llrnllllllllllqrn11n111m1 !//111/W 111,111rn111 I I ii I I I 1111

500 1000 1500 2000 channel

2500 3000 3500 4000

~ ROI Type: 1 ROI Type: 2

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0258

4/17/2018 7:44:46AM

Analysis Report for 1803111-04

AC-SED-11

GAMMA SPECTRUM ANALYSIS

Sample Identification

Sample Description

Sample Type

Sample Size

Facility

Sample Taken On

Acquisition Started

Procedure

Operator Detector Name

Geometry Live Time

Real Time

Dead Time

Peak Locate Threshold

Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance

Energy Calibration Used Done On

Efficiency Calibration Used Done On

Efficiency Calibration Description

Sample Number

: 1803111-04

: AC-SED-11

: SOIL

: 4.763E+02 grams

: Countroom

: 3/21/2018 9:15:45AM

: 4/17/2018 6:44:34AM

: GAS-1602 pCi

: Administrator

: GE2 : GAS-1602

: 3600.0 seconds

: 3600.8 seconds

: 0.02 %

: 2.50

: 1 - 4096

: 28 - 4096

: 1.000 keV

: 2/17/2018 : 2/17/2018

: 64641

PEAK-TO-TOTAL CALIBRATION REPORT

Peak-to-Total Efficiency Calibration Equation

Page 1 of29

v{P l//l 7/Jf3

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0259

4/17/2018 7 :44 :46AM

Analysis Report for 1803111-04

AC-SED-11

PEAK LOCATE REPORT

Peak No.

1 2 3 4 5 6 7 8 9

10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42

Peak Locate Performed on

Peak Locate From Channel

Peak Locate To Channel

Peak Search Sensitivity

Energy (keV)

47.12 63.71 76.81 87.06 92.98

186.24 239.51 269.77 295.30 300.11 328.20 339.04 352.16 384.90 427.01 462.09 477.47 480.28 511.37 583.48 609.42 661.89 665.38 727.24 767.85 794.18 860.05 883.58 911.18 925.35 965. 2 9 969. 0 9

1078.18 1082.18 1120.57 1238.93 1262.15 1334. 92 1460.72 1560.68 1582.32 1587.31

: 4/17/2018 7:44:38AM

: 1 : 4096 : 2.50

Centroid Channel

46.90 63.48 76.58 86.82 92.74

185.95 239.19 269.45 294.97 299.76 327.85 338.68 351.79 384.51 426.60 461.67 477.04 479.84 510.92 582.99 608.92 661.36 664.85 726.68 767.27 793.58 859.41 882.93 910.51 924.67 964.60 968.39

1077.42 1081.42 1119.78 1238.07 1261.28 1334.00 1459. 72 1559.61 1581.24 1586.22

Centroid Uncertainty

0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000

Page 2 of29

Peak Significance

0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00

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0260

Analysis Report for 1803111-04

AC-SED-11

Peak No. Energy (keV)

43 1590.31 44 1593.00 45 1764.32 46 1848.86 47 1873.12 48 1939.70 49 2086.60 50 2146.73 51 2614.03

? = Adjacent peak noted

Errors quoted at 2.000sigma

Centroid Channel

1589.23 1591.91 1763.11 1847.60 1871.84 1938.38 2085.17 2145.25 2612.18

4/17/2018 7:44:46AM

Centroid Uncertainty

0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000

Page 3 of 29

Peak Significance

0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00

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0261

4/17/2018 7:44:46AM Page 4 of29

Analysis Report for 1803111-04

AC-SED-11

PEAK ANALYSIS REPORT

Peak Analysis Performed on : 4/17/2018 7:44:38AM

Peak Analysis From Channel : 1

Peak Analysis To Channel : 4096

Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM

No. (keV) start end Centroid Area Uncertainty Counts (keV)

1 47.12 43 - 50 46.90 1.17E+02 73.24 8.16E+02 1. 21

2 63.71 61 - 65 63.48 7.41E+0l 59.28 7.12E+02 1. 51

3 76.81 72 - 82 76.58 7.49E+02 125.00 1.66E+03 3.49

4 87.06 83 - 89 86.82 1.33E+02 81.26 1.11E+03 1. 69

5 92.98 90 - 96 92.74 2.12E+02 79.17 9.46E+02 1. 68

6 186.24 183 - 189 185.95 1.41E+02 59.66 5.43E+02 1.17

7 239.51 234 - 243 239.19 6.69E+02 85.20 6.54E+02 1. 76

8 269.77 266 - 273 269.45 5.70E+0l 50.83 3.94E+02 1. 89

M 9 295.30 2 91 - 303 294.97 2.54E+02 44.30 1.99E+02 1. 73

m 10 300.11 2 91 - 303 299.76 3.17E+0l 37.03 2. 72E+02 1. 85

11 328.20 326 - 331 327.85 3.79E+0l 34.66 2.14E+02 1. 81

12 339.04 334 - 343 338.68 1.14E+02 54.03 3.43E+02 1. 59

13 352.16 348 - 354 351.79 3.05E+02 50.69 2.45E+02 1. 46

14 384.90 382 - 388 384.51 2.72E+0l 32.50 1.74E+02 3.87

15 427.01 424 - 430 426.60 2.32E+0l 27.58 1.20E+02 2.20

16 462.09 457 - 4 67 461.67 7.30E+0l 42.15 1.98E+02 1.85

M 17 477.47 4 72 - 483 477.04 3.89E+0l 23.63 8.66E+0l 1. 72

m 18 480.28 472 - 483 479.84 1.62E+0l 24.05 7.50E+0l 1. 72

19 511.37 506 - 517 510.92 1.42E+02 49.36 2.31E+02 2.73

20 583.48 57 8 - 587 582.99 1.71E+02 42.43 1.58E+02 1. 50

21 609.42 605 - 611 608.92 2.79E+02 43.47 1.42E+02 1. 50

M 22 661.89 657 - 667 661.36 2.92E+0l 21.21 5.56E+0l 2.07

m 23 665.38 657 - 667 664.85 2.16E+0l 20.64 5.03E+0l 2.07

24 727.24 7 24 - 730 72 6. 68 3.41E+0l 24.70 8.38E+0l 3.03

25 767.85 7 64 - 770 767.27 2.81E+01 26.30 1.06E+02 1. 21

26 794.18 7 91 - 798 793.58 2.60E+0l 26.23 1.00E+02 3.56

27 860.05 85 6 - 863 859.41 l.84E+0l 23.58 8.12E+0l 1. 94

28 883.58 87 9 - 886 882.93 1.68E+0l 21.73 6.65E+0l 3.40

29 911.18 90 6 - 915 910.51 1. 11E+02 31.10 7.32E+0l 2.06

30 925.35 919 - 930 924.67 2.97E+0l 28.14 8.45E+0l 7.97

M 31 965. 2 9 962 - 974 964. 60 1.46E+0l 17.18 5.76E+0l 2.32

m 32 969.09 962 - 974 968.39 6.48E+0l 26.86 7.19E+0l 2.32

M 33 1078.18 107 6 - 1089 1077.42 1.15E+0l 6.93 1.02E+0l 1. 96

m 34 1082.18 107 6 - 1089 1081.42 1.54E+0l 17.52 4.09E+0l 2.40

35 1120.57 1115 - 1124 1119.78 5.27E+0l 29.58 9.47E+0l 1. 88

36 1238.93 1232 - 1244 1238.07 4.85E+0l 30.15 8.31E+0l 3.08

37 1262.15 1259 - 1263 1261.28 1.06E+0l 9. 96 1.28E+0l 1. 77

38 1334.92 1328 - 1343 1334.00 3.70E+0l 21.63 3.20E+0l 5.00

39 1460.72 1453 - 1464 1459.72 4.82E+02 48.58 5.46E+0l 2.75

40 1560.68 1555 - 1563 1559.61 8.50E+00 9.62 9.00E+00 2.78

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0262

M m m

Analysis Report for 1803111-04

AC-SED-11

Peak Energy ROI

No. (keV) start

41 1582.32 157 9 -42 1587.31 1584 -43 1590.31 1584 -44 1593.00 1584 -45 1764.32 1758 -46 1848.86 184 4 -47 1873.12 1868 -48 1939.70 1934 -49 2086.60 2083 -so 2146.73 2142 -51 2614.03 2 607 -

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet

Errors quoted at 2.000sigma

ROI Peak

end Centroid

1584 1581.24 1595 1586.22 1595 1589.23 1595 1591.91 1768 1763.11 1852 1847.60 1875 1871.84 1941 1938.38 2087 2085.17 2147 2145.25 2 616 2612.18

4/17/2018 7:44:46AM Page 5 of29

Net Peak Net Area Continuum FWHM Area Uncertainty Counts (keV)

9.00E+OO 7.87 4.00E+OO 1. so 1.31E+Ol 7.37 4.lSE+OO 2.48

1.lOE+Ol 11. so 3.39E+OO 2.48

1.40E+Ol 10.21 1.91E+OO 2.48

4.56E+Ol 17.51 1.68E+Ol 2.29

1.32E+Ol 8. 96 3.53E+OO 3.46

9.18E+OO 7.75 3.64E+OO 3.10

8.00E+OO 5.66 O.OOE+OO 1. 98

6.00E+OO 4.90 O.OOE+OO 2.74

4.42E+OO 5.74 3.17E+OO 2.57

7.60E+Ol 17.44 O.OOE+OO 3.20

PEAK ANALYSIS REPORT

Peak Analysis Performed on : 4/17/2018 7:44:38AM

Peak Analysis From Channel : 1

Peak Analysis To Channel : 4096

Peak Energy ROI ROI Net Peak Net Area Continuum Critical

No. (keV) start end Area Uncertainty Counts Level

1 47.12 43 - so 1.17E+02 73.24 8.16E+02 S.7SE+Ol

2 63.71 61 - 65 7.41E+Ol 59.28 7.12E+02 4.66E+Ol

3 76.81 72 - 82 7.49E+02 125.00 1.66E+03 9.24E+Ol

4 87.06 83 - 89 1.33E+02 81.26 1.11E+03 6.40E+Ol

s 92.98 90 - 96 2.12E+02 79.17 9.46E+02 6.0SE+Ol

6 186.24 183 - 189 1.41E+02 59.66 S.43E+02 4.SOE+Ol

7 239.51 234 - 243 6.69E+02 85.20 6.54E+02 S.56E+Ol

8 269.77 266 - 273 S.70E+Ol 50.83 3.94E+02 3.99E+Ol

M 9 295.30 291 - 303 2.54E+02 44.30 1.99E+02 2.32E+Ol

m 10 300.11 291 - 303 3.17E+Ol 37.03 2. 72E+02 2.71E+Ol

11 328.20 326 - 331 3.79E+Ol 34.66 2. 14E+02 2.66E+Ol

12 339.04 334 - 343 1. 14E+02 54.03 3.43E+02 4.08E+Ol

13 352.16 34 8 - 354 3.0SE+02 50.69 2.4SE+02 3.02E+Ol

14 384.90 382 - 388 2. 72E+Ol 32.50 1.74E+02 2.53E+Ol

15 427.01 424 - 430 2.32E+Ol 27.58 1.20E+02 2.12E+Ol

16 462.09 457 - 467 7. 30E+Ol 42.15 1. 98E+02 3.17E+Ol

M 17 477.47 4 7 2 - 483 3.89E+Ol 23.63 8.66E+Ol 1.53E+Ol

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0263

Analysis Report for 1803111-04

m

M m

M

m M

m

M

m m

AC-SED-11

Peak Energy ROI

No. (keV) start

18 480.28 472 -

19 511.37 506 -

20 583.48 57 8 -

21 609.42 605 -

22 661.89 657 -

23 665.38 657 -

24 727.24 724 -

25 767.85 7 64 -

26 794.18 7 91 -

27 860.05 856 -

28 883.58 87 9 -

29 911.18 906 -

30 925.35 919 -

31 965. 29 962 -

32 969.09 962 -

33 1078.18 107 6 -

34 1082.18 107 6 -

35 1120.57 1115 -

36 1238.93 1232 -

37 1262.15 1259 -

38 1334.92 1328 -

39 1460.72 1453 -

40 1560.68 1555 -

41 1582.32 157 9 -

42 1587.31 1584 -

43 1590.31 1584 -

44 1593.00 1584 -

45 1764.32 1758 -

46 1848.86 1844 -

47 1873.12 18 68 -

48 1939.70 1934 -

49 2086.60 2083 -

50 2146.73 2142 -

51 2614.03 2 607 -

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet

Errors quoted at 2.000sigma

4/17/2018 7:44:46AM Page 6 of 29

ROI Net Peak Net Area Continuum Critical

end Area Uncertainty Counts Level

483 1.62E+0l 24.05 7.50E+0l 1.42E+0l

517 1.42E+02 49.36 2.31E+02 1.93E+0l

587 1.71E+02 42.43 1.58E+02 2.75E+0l

611 2.79E+02 43.47 1.42E+02 2.29E+0l

667 2.92E+0l 21. 21 5.56E+0l 1.23E+0l

667 2.16E+0l 20.64 5.03E+0l 1.17E+0l

730 3.41E+0l 24.70 8.38E+0l 1.79E+0l

770 2.81E+0l 26.30 1.06E+02 1.98E+0l

798 2.60E+0l 26.23 1.00E+02 1.99E+0l

863 1.84E+0l 23.58 8.12E+0l 1.81E+0l

886 1.68E+0l 21.73 6.65E+0l 1.65E+0l

915 1. 11E+02 31.10 7.32E+0l 1.88E+0l

930 2.97E+0l 28.14 8.45E+0l 2. 13E+0l

974 l.46E+0l 17.18 5.76E+0l 1.25E+0l

97 4 6.48E+0l 26.86 7.19E+0l 1.39E+0l

1089 1.15E+0l 6.93 1.02E+0l 5.26E+00

1089 1.54E+0l 17.52 4.09E+0l 1.05E+0l

1124 5.27E+0l 29.58 9.47E+0l 2.12E+0l

1244 4.85E+0l 30.15 8.31E+0l 2.20E+0l

1263 1.06E+0l 9. 96 1.28E+0l 6.19E+00

1343 3.70E+0l 21.63 3.20E+0l 1.47E+0l

1464 4.82E+02 48.58 5.46E+0l 1.71E+0l

1563 8.50E+00 9.62 9.00E+00 6.29E+00

1584 9.00E+00 7.87 4.00E+00 4.19E+00

1595 1.31E+0l 7.37 4.15E+00 3.35E+00

1595 1.l0E+0l 11. 50 3.39E+00 3.03E+00

1595 1.40E+0l 10.21 1.91E+00 2.27E+00

1768 4.56E+0l 17.51 1.68E+0l 9.16E+00

1852 1.32E+0l 8. 96 3.53E+00 4.30E+00

1875 9.18E+00 7.75 3.64E+00 3.97E+00

1941 8.00E+00 5.66 0.00E+00 0.00E+00

2087 6.00E+00 4.90 0.00E+00 0.00E+00

2147 4.42E+00 5.74 3.17E+00 3.22E+00

2616 7.60E+0l 17.44 0.00E+00 0.00E+00

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0264

4/17/2018 7:44:46AM

Analysis Report for 1803111-04

M m

M

m

M m

M m

AC-SED-11

PEAK WITH N/0 REPORT

Peak Analysis Performed on : 4/17/2018 7:44:38AM

Peak Analysis From Channel : 1

Peak Analysis To Channel : 4096

Tentative NID Library

Peak Match Tolerance

Peak Energy

No. (keV)

1 47.12 2 63.71

3 76.81 4 87.06

5 92.98 6 186.24 7 239.51 8 269.77 9 295.30

10 300.11

11 328.20 12 339.04 13 352.16 14 384.90 15 427.01 16 462.09 17 477.47

18 480.28 19 511.37 20 583.48 21 609.42 22 661.89 23 665.38

24 727.24 25 767.85 26 794.18 27 860.05 28 883.58 29 911.18

30 925.35 31 965. 2 9 32 969.09

: \\OR-GAMMA1\ApexRoot\Countroom\Library\TMA2.NLB

: 1.000 keV

ROI ROI Peak Net Peak

start end Centroid Area

43 - 50 46.90 1.17E+02 61 - 65 63.48 7.41E+0l

72 - 82 76.58 7.49E+02 83 - 89 86.82 1.33E+02

90 - 96 92.74 2.12E+02

183 - 189 185.95 1.41E+02

234 - 243 239.19 6.69E+02 266 - 273 269.45 5.70E+0l

291 - 303 294.97 2.54E+02

2 91 - 303 299.76 3.17E+0l

326 - 331 327.85 3.79E+0l

334 - 343 338.68 1.14E+02 348 - 354 351.79 3.05E+02 382 - 388 384.51 2.72E+0l 424 - 430 426.60 2.32E+0l

457 - 4 67 461.67 7.30E+0l 4 72 - 483 477.04 3.89E+0l

4 72 - 483 479.84 l.62E+0l

50 6 - 517 510.92 1.42E+02

578 - 587 582.99 1.71E+02

605 - 611 608.92 2.79E+02

657 - 667 661.36 2.92E+0l

657 - 667 664.85 2.16E+0l

724 - 730 726.68 3.41E+0l

7 64 - 770 767.27 2.81E+0l

791 - 798 793.58 2.60E+0l

856 - 863 859.41 1.84E+0l

87 9 - 886 882.93 1.68E+0l

906 - 915 910.51 1. 11E+02

919 - 930 924.67 2.97E+0l

962 - 974 964. 60 1.46E+0l

962 - 974 968.39 6.48E+0l

Net Area Uncertainty

73.24 59.28

125.00 81.26

79.17 59.66 85.20 50.83 44.30 37.03

34.66 54.03 50.69 32.50 27.58 42.15 23.63

24.05 49.36 42.43 43.47 21. 21 20.64

24.70 26.30 26.23 23.58 21. 73 31.10

28.14 17.18 26.86

Page 7 of29

Continuum Tentative Counts Nuclide

8.16E+02 PB-210 7.12E+02 TH-234

TH-230 1.66E+03 1. 11E+03 SN-126

NP-237 EU-155 CD-109

9.46E+02 GA-67 5.43E+02 RA-226 6.54E+02 PB-212 3.94E+02 l.99E+02 PB-214 2. 72E+02 PB-212

BI-210M GA-67

2.14E+02 LA-140 3.43E+02 AC-228 2.45E+02 PB-214 1.74E+02 1.20E+02 SB-125 1.98E+02 8.66E+0l BE-7

PM-144 7.50E+0l 2.31E+02 1.58E+02 TL-208 1.42E+02 BI-214 5.56E+0l CS-137 5.03E+0l CE-143

SB-126 8.38E+0l BI-212 1.06E+02 1.00E+02 ..... '

8.12E+0l TL-208 6.65E+0l 7.32E+0l AC-228

TL-204 8.45E+0l 5.76E+0l 7.19E+0l AC-228

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Analysis Report for 1803111-04

M m

M m m

M

AC-SED-11

Peak Energy ROI

No. (keV) start

33 1078.18 107 6 -34 1082.18 1076 -35 1120.57 1115 -

36 1238.93 1232 -37 1262.15 1259 -38 1334.92 1328 -39 1460.72 1453 -40 1560.68 1555 -41 1582.32 157 9 -42 1587.31 1584 -43 1590.31 1584 -44 1593.00 1584 -45 1764.32 1758 -46 1848.86 184 4 -47 1873.12 18 68 -48 1939.70 1934 -49 2086.60 2083 -50 2146.73 2142 -51 2614.03 2607 -

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet

Errors quoted at 2.000sigma

ROI Peak Net Peak Net Area

end Centroid Area Uncertainty

1089 1077,42 1.15E+0l 6.93

1089 1081.42 1.54E+0l 17.52

1124 1119.78 5.27E+0l 29.58

1244 1238.07 4.85E+0l 30.15

1263 1261.28 1.06E+0l 9. 96

1343 1334.00 3.70E+0l 21.63

14 64 1459.72 4.82E+02 48.58

1563 1559.61 8.50E+00 9.62

1584 1581.24 9.00E+00 7.87

1595 1586.22 1.31E+0l 7.37

1595 1589.23 1.l0E+0l 11. 50

1595 1591.91 1.40E+0l 10.21

1768 1763.11 4.56E+0l 17.51

1852 1847.60 1.32E+0l 8. 96

1875 1871.84 9.18E+00 7.75

1941 1938.38 8.00E+00 5.66

2087 2085.17 6.00E+00 4.90

2147 2145.25 4.42E+00 5.74

2616 2612.18 7.60E+0l 17.44

PEAK EFFICIENCY REPORT

Peak Analysis Performed on : 4/17/2018 7:44:38AM

Peak Energy Net Peak Net Area Peak

No. (keV) Area Uncertainty Efficiency

1 47.12 l.17E+02 73.24 1.62E-02

2 63. 71 7.41E+0l 59.28 2.15E-02

3 76.81 7.49E+02 125.00 2.33E-02

4 87.06 1.33E+02 81.26 2.39E-02

5 92.98 2.12E+02 79 .17 2.40E-02

6 186.24 1.41E+02 59.66 1.95E-02

7 239.51 6.69E+02 85.20 1.68E-02

8 269.77 5.70E+0l 50.83 1.55E-02

9 295.30 2.54E+02 44.30 l,46E-02

Page 8 of29

Continuum Tentative Counts Nuclide

1.02E+0l 4.09E+0l 9.47E+0l SC-46

BI-214 TA-182

8.31E+0l CO-56 l.28E+0l 3.20E+0l 5.46E+0l K-40 9.00E+00 4.00E+00 4.15E+00 3.39E+00 1.91E+00 1.68E+0l BI-214 3.53E+00 3.64E+00 0.00E+00 0.00E+00 3.17E+00 0.00E+00 TL-208

Efficiency Uncertainty

1.53E-03 1.62E-03 1.89E-03 2.l0E-03 2.l0E-03 2.44E-03 2.41E-03 2.40E-03 2.38E-03

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Analysis Report for 1803111-04

AC-SED-11

Peak Energy Net Peak Net Area Peak Efficiency

No. (keV) Area Uncertainty Efficiency Uncertainty

m 10 300. 11 3.17E+01 37.03 1.44E-02 2.38E-03

11 328.20 3.79E+0l 34.66 l.35E-02 2.36E-03

12 339.04 l.14E+02 54.03 1.32E-02 2.36E-03

13 352.16 3.05E+02 50.69 1.28E-02 2.35E-03

14 384.90 2. 72E+0l 32.50 1.19E-02 2.33E-03

15 427.01 2.32E+0l 27.58 1.l0E-02 2.12E-03

16 462.09 7.30E+0l 42.15 1.03E-02 1.92E-03

M 17 477.47 3.89E+0l 23.63 1.0lE-02 1.83E-03

m 18 480.28 1.62E+0l 24.05 l.00E-02 1.81E-03

19 511. 37 1.42E+02 49.36 9.51E-03 1.63E-03

20 583.48 1.71E+02 42.43 8.53E-03 1. 22E-03

21 609.42 2.79E+02 43.47 8.22E-03 1.07E-03

M 22 661.89 2.92E+0l 21. 21 7.68E-03 7.67E-04

m 23 665.38 2.16E+0l 20.64 7.64E-03 7.74E-04

24 727.24 3.41E+0l 24.70 7.l0E-03 8.92E-04

25 767.85 2.81E+0l 26.30 6.78E-03 9.70E-04

26 794.18 2.60E+0l 26.23 6.60E-03 l.02E-03

27 860.05 1.84E+0l 23.58 6.18E-03 l.15E-03

28 883.58 1.68E+0l 21.73 6.04E-03 1.19E-03

29 911.18 1.11E+02 31.10 5.89E-03 l.18E-03

30 925.35 2.97E+0l 28.14 5.82E-03 1.14E-03

M 31 965. 2 9 1.46E+0l 17.18 5.63E-03 l.02E-03

m 32 969.09 6.48E+0l 26.86 5.61E-03 1.0lE-03

M 33 1078.18 l.15E+0l 6.93 5.16E-03 6.98E-04

m 34 1082.18 1.54E+0l 17.52 5.14E-03 6.87E-04

35 1120.57 5.27E+0l 29.58 5.0lE-03 5.76E-04

36 1238.93 4.85E+0l 30.15 4.65E-03 4.00E-04

37 1262.15 l.06E+0l 9. 96 4.59E-03 3.91E-04

38 1334. 92 3.70E+0l 21.63 4.42E-03 3.65E-04

39 1460.72 4.82E+02 48.58 4.16E-03 3.80E-04

40 1560.68 8.50E+00 9.62 4.00E-03 3.92E-04

41 1582.32 9.00E+00 7.87 3.97E-03 3.95E-04

M 42 1587.31 1.31E+0l 7.37 3.96E-03 3.95E-04

m 43 1590.31 l.l0E+0l 11. 50 3.95E-03 3.96E-04

m 44 1593.00 1.40E+0l 10. 21 3.95E-03 3. 96E-04

45 1764.32 4.56E+0l 17.51 3.74E-03 4.16E-04

46 1848.86 1.32E+0l 8. 96 3.66E-03 4.25E-04

47 1873.12 9.18E+00 7.75 3.64E-03 4.25E-04

48 1939.70 8.00E+00 5.66 3.59E-03 4.25E-04

49 2086.60 6.00E+00 4.90 3.49E-03 4.25E-04

50 2146.73 4.42E+00 5.74 3.46E-03 4.25E-04

51 2614.03 7.60E+0l 17.44 3.36E-03 4.25E-04

M = First peak in a multiplet region

m = other peak in a multiplet region

F = Fitted singlet

Errors quoted at 2.000 sigma

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Analysis Report for 1803111-04

AC-SED-11

BACKGROUND SUBTRACT REPORT

Peak Analysis Performed on : 4/17/2018 7:44:38AM

Env. Background File : \\OR-GAMMA 1 \ApexRoot\Countroom\Data\0000063825.CN F

Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted

No. (keV) Area Uncertainty Background Uncert. Area Uncert.

1 47.12 l.17E+02 73.24 2.91E+0l 5.55E+00 8.79E+0l 7.34E+0l

2 63.71 7.41E+0l 59.28 2.20E+0l 9.99E+00 5.20E+0l 6.0lE+0l

3 76.81 7.49E+02 125.00 7.49E+02 l.25E+02

4 87.06 l.33E+02 81. 26 l.33E+02 8.13E+0l

5 92.98 2.12E+02 79.17 5.03E+0l 8.08E+00 l.62E+02 7. 96E+0l

6 186.24 l.41E+02 59.66 4.04E+0l 9.60E+00 l.00E+02 6.04E+0l

7 239.51 6.69E+02 85.20 l.86E+0l l.03E+0l 6.50E+02 8.58E+0l

8 269.77 5.70E+0l 50.83 5.70E+0l 5.08E+01

M 9 295.30 2.54E+02 44.30 8.49E+00 5.60E+00 2.46E+02 4.47E+01

m 10 300.11 3.17E+0l 37.03 3.17E+0l 3.70E+0l

11 328.20 3.79E+0l 34.66 3.79E+0l 3.47E+0l

12 339.04 l.14E+02 54.03 l.14E+02 5.40E+0l

13 352.16 3.05E+02 50.69 l.76E+0l 5.14E+00 2.88E+02 5.l0E+0l

14 384.90 2. 72E+0l 32.50 2.72E+0l 3.25E+01

15 427. 01 2.32E+0l 27. 58 2.32E+0l 2.76E+0l

16 462.09 7.30E+0l 42.15 7.30E+0l 4.22E+0l

M 17 477.47 3.89E+0l 23.63 3.89E+0l 2.36E+0l

m 18 480.28 l.62E+0l 24.05 l.62E+0l 2.40E+0l

19 511.37 l.42E+02 49.36 7.91E+0l 5.07E+00 6.33E+0l 4.96E+01

20 583.48 l.71E+02 42.43 6.66E+00 3.73E+00 l.64E+02 4.26E+0l

21 609.42 2.79E+02 43.47 l.26E+0l 6.94E+00 2.67E+02 4.40E+0l

M 22 661.89 2.92E+0l 21. 21 3.98E+00 2.76E+00 2.52E+0l 2.14E+0l

m 23 665.38 2.16E+0l 20.64 2.16E+0l 2.06E+0l

24 727. 24 3.41E+0l 24.70 3.41E+0l 2.47E+0l

25 767.85 2.81E+0l 26.30 2.81E+0l 2.63E+0l

26 794.18 2.60E+0l 26.23 2.60E+0l 2.62E+0l

27 860.05 l.84E+0l 23.58 l.84E+0l 2.36E+0l

28 883.58 l.68E+0l 21. 73 l.68E+0l 2.17E+0l

29 911.18 l.11E+02 31.10 2.63E+00 2.68E+00 l.09E+02 3.12E+0l

30 925.35 2.97E+0l 28.14 2.97E+0l 2.81E+0l

M 31 965. 2 9 l.46E+0l 17.18 l.46E+0l l.72E+0l

m 32 969.09 6.48E+0l 26.86 6.48E+0l 2.69E+0l

M 33 1078.18 l.15E+0l 6.93 l.15E+0l 6.93E+00

m 34 1082.18 l.54E+0l 17.52 l.54E+0l l.75E+0l

35 1120.57 5.27E+0l 29.58 l.l0E+00 2.71E+00 5.16E+0l 2.97E+0l

36 1238.93 4.85E+0l 30.15 4.85E+0l 3.02E+0l

37 1262.15 l.06E+0l 9. 96 l.06E+0l 9. 96E+00

38 1334. 92 3.70E+0l 21.63 3.70E+0l 2.16E+0l

39 1460.72 4.82E+02 48.58 7.43E+00 2.27E+00 4.74E+02 4.86E+0l

40 1560.68 8.50E+00 9.62 8.50E+00 9.62E+00

41 1582.32 9.00E+00 7.87 9.00E+00 7.87E+00

M 42 1587.31 l.31E+0l 7.37 l.31E+0l 7.37E+00

m 43 1590.31 l.l0E+0l 11. 50 l.l0E+0l l.15E+0l

m 44 1593.00 l.40E+0l 10.21 l.40E+0l l.02E+0l

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Analysis Report for 1803111-04

AC-SED-11

Peak Energy No. (keV)

45 1764.32 46 1848.86 47 1873.12 48 1939.70 49 2086.60 so 2146.73 51 2614.03

Original Area

4.56E+Ol 1.32E+01 9.18E+OO 8.00E+OO 6.00E+OO 4.42E+00 7.60E+Ol

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet

Errors quoted at 2.000sigma

Orig. Area Uncertainty

17.51 8. 96 7.75 5.66 4.90 5.74

17.44

Ambient Background

2.32E+OO

4.72E+OO

Backgr. Uncert.

1.91E+OO

1.41E+OO

AREA CORRECTION REPORT

Subtracted Area

4.33E+Ol 1.32E+Ol 9.18E+OO 8.00E+OO 6.00E+OO 4.42E+OO 7.13E+Ol

REFERENCE PEAK I 8KG. SUBTRACT

Peak Analysis Performed on : 4/17/2018 7:44:38AM

Ref. Peak Energy : 0.00 Reference Date

Peak Ratio : 0.00 Uncertainty : 0,00

Background File : \\OR-GAMMA 1 \ApexRoot\Countroom\Data\0000063825.CNF

Corrected Area is: Original * Peak Ratio - Background

Peak Energy Original Orig. Area Ambient Backgr. Corrected

No. (keV) Area Uncertainty Background Uncert. Area

1 47.12 1.17E+02 73.24 2.91E+Ol S.SSE+OO 8.79E+Ol

2 63.71 7.41E+Ol 59.28 2.20E+Ol 9.99E+OO S.20E+Ol

3 76.81 7.49E+02 125.00 7.49E+02

4 87.06 1.33E+02 81. 26 1.33E+02

s 92.98 2.12E+02 79.17 S.03E+Ol 8.08E+OO 1.62E+02

6 186.24 1.41E+02 59.66 4.04E+Ol 9.60E+OO 1.00E+02

7 239.51 6.69E+02 85.20 1.86E+Ol 1.03E+Ol 6.SOE+02

8 269.77 S.70E+Ol 50.83 S.70E+Ol

M 9 295.30 2.54E+02 44.30 8.49E+OO S.60E+OO 2.46E+02

m 10 300.11 3.17E+Ol 37.03 3.17E+Ol

11 328.20 3.79E+Ol 34.66 3.79E+Ol

12 339.04 1.14E+02 54.03 l.14E+02

13 352.16 3.0SE+02 50.69 1.76E+Ol S.14E+OO 2.88E+02

14 384.90 2. 72E+Ol 32.50 2.72E+Ol

15 427.01 2.32E+Ol 27.58 2.32E+Ol

16 462.09 7.30E+Ol 42.15 7.30E+Ol

M 17 477.47 3.89E+Ol 23.63 3.89E+Ol

m 18 480.28 1.62E+Ol 24.05 1.62E+Ol

19 511.37 1.42E+02 49.36 7.91E+Ol S.07E+OO 6.33E+Ol

20 583.48 1.71E+02 42.43 6.66E+OO 3.73E+OO 1.64E+02

21 609.42 2.79E+02 43.47 1.26E+Ol 6.94E+OO 2.67E+02

Subtracted Uncert.

1.76E+Ol 8. 96E-1-00 7.7SE+OO S.66E+OO 4.90E+OO S.74E+OO 1.7SE+Ol

Corrected Uncert.

7.34E+Ol 6.0lE+Ol 1.2SE+02 8.13E+Ol 7. 96E+Ol 6.04E+Ol 8.58E+Ol S.08E+Ol 4.47E+Ol 3.70E+Ol 3.47E+Ol S.40E+Ol S.lOE+Ol 3.2SE+Ol 2.76E+Ol 4.22E+Ol 2.36E+Ol 2.40E+Ol 4.96E+Ol 4.26E+Ol 4.40E+Ol

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Analysis Report for 1803111-04

AC-SED-11

Peak Energy Original Orig. Area Ambient Backgr. Corrected

No. (keV) Area Uncertainty Background Uncert. Area

M 22 661.89 2.92E+Ol 21. 21 3.98E+OO 2.76E+OO 2.52E+Ol

m 23 665.38 2.16E+Ol 20.64 2.16E+Ol

24 727.24 3.41E+Ol 24.70 3.41E+Ol

25 767.85 2.81E+Ol 26.30 2.81E+Ol

26 794.18 2.60E+Ol 26.23 2.60E+Ol

27 860.05 l.84E+Ol 23.58 l.84E+Ol

28 883.58 l.68E+Ol 21.73 l.68E+Ol

29 911.18 1. 11E+02 31.10 2.63E+OO 2.68E+OO l.09E+02

30 925.35 2.97E+Ol 28.14 2.97E+Ol

M 31 965. 2 9 l.46E+Ol 17.18 l.46E+Ol

m 32 969.09 6.48E+Ol 26.86 6.48E+Ol

M 33 1078.18 l.15E+Ol 6.93 l.15E+Ol

m 34 1082.18 l.54E+Ol 17.52 l.54E+Ol

35 1120.57 5.27E+Ol 29.58 l.lOE+OO 2.71E+OO 5.16E+Ol

36 1238.93 4.85E+Ol 30.15 4.85E+Ol

37 1262.15 l.06E+Ol 9. 96 l.06E+Ol

38 1334. 92 3.70E+Ol 21.63 3.70E+Ol

39 1460.72 4.82E+02 48.58 7.43E+OO 2.27E+OO 4.74E+02

40 1560.68 8.50E+OO 9.62 8.50E+OO

41 1582.32 9.00E+OO 7.87 9.00E+OO

M 42 1587.31 l.31E+Ol 7.37 l.31E+Ol

m 43 1590.31 l.lOE+Ol 11. 50 l.lOE+Ol

m 44 1593.00 l.40E+Ol 10.21 l.40E+Ol

45 1764.32 4.56E+Ol 17.51 2.32E+OO l.91E+OO 4.33E+Ol

46 1848.86 l.32E+Ol 8. 96 l.32E+Ol

47 1873.12 9.18E+OO 7.75 9.18E+OO

48 1939.70 8.00E+OO 5.66 8.00E+OO

49 2086.60 6.00E+OO 4.90 6.00E+OO

50 2146.73 4.42E+OO 5.74 4.42E+OO

51 2614.03 7.60E+Ol 17.44 4.72E+OO l.41E+OO 7.13E+Ol

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet

Errors quoted at 2.000sigma

NUCLIDE IDENTIFICATION REPORT

Nuclide Library Used

Nuclide Name

BE-7

: \\OR-GAMMA 1 \ApexRoot\Countroom\Library\TMA2.NLB

IDENTIFIED NUCLIDES

Id Confidence Energy (keV) Yield(%)

0.997 477.59 * 10.42

Activity

(pCi/grams)

8.30E-Ol

Corrected Uncert.

2.14E+Ol 2.06E+Ol 2.47E+Ol 2.63E+Ol 2.62E+Ol 2.36E+Ol 2.17E+Ol 3.12E+Ol 2.81E+Ol 1. 72E+Ol 2.69E+Ol 6.93E+OO l.75E+Ol 2.97E+Ol 3.02E+Ol 9.96E+OO 2.16E+Ol 4.86E+Ol 9.62E+OO 7.87E+OO 7.37E+OO l.15E+Ol l.02E+Ol l.76E+Ol 8.96E+OO 7.75E+OO 5.66E+OO 4.90E+OO 5.74E+00 l.75E+Ol

Activity

Uncertainty

5.26E-01

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Analysis Report for 1803111-04

AC-SED-11

Nuclide Name Id Confidence Energy (keV) Yield(%) Activity

(pCilgrams)

K-40 0.999 1460.81 * 10.67 l.68E+0l

GA-67 0.659 93.31 * 35.70 9.08E+0l

208.95 2.24 300.22 * 16.00 6.61E+0l

CD-109 0.860 88.03 * 3.72 2.46E+00

SN-126 0. 960 87.57 * 37.00 2.38E-01

CS-137 0.991 661.65 * 85.12 6.08E-02

EU-155 0.329 86.50 * 30.90 2.88E-01

105.30 20.70

TL-208 0. 960 583.14 * 30.22 l.00E+00

860.37 * 4.48 l.05E+00

2614.66 * 35.85 9.33E-01

PB-210 0.940 46.50 * 4.25 2.0lE+00

BI-212 0.763 727. 17 * 11.80 6.42E-01

1620.62 2.75

PB-212 0.892 238.63 * 44.60 l.37E+00

300.09 * 3.41 l.02E+00

BI-214 0.924 609.31 * 46.30 l.l0E+00

1120.29 * 15.10 l.07E+00

1764.49 * 15.80 l.15E+00

2204.22 4.98

PB-214 0.994 295.21 * 19.19 l.39E+00

351.92 * 37.19 9.54E-0l

RA-226 1.000 186.21 * 3.28 2.47E+00

AC-228 0.982 338.32 * 11. 40 l.20E+00

911. 07 * 27.70 l.05E+00

969. 11 * 16.60 l.l0E+00

TH-234 0. 972 63.29 * 3.80 l.0lE+00

NP-237 0.951 86.50 * 12.60 6.98E-01

* = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

Energy Tolerance : 1.000 keV

Nuclide confidence index threshold = 0.30

Errors quoted at 2.000sigma

UNIDENTIFIED PEAKS

Peak Locate Performed on

Peak Locate From Channel

Peak Locate To Channel

Peak No. Energy (ke V)

: 4/17/2018 7:44:38AM

: 1 : 4096

Peak Size (CPS) Peak CPS(%)

Uncertainty

Peak Type

Page 13 of29

Activity

Uncertainty

2.31E+00 4.54E+0l

7.81E+0l l.52E+00 l.46E-01 5. 21E-02 1. 77E-01

2.97E-01 l.36E+00 2.58E-01 l.69E+00 4.72E-01

2.67E-0l l.20E+00 2.32E-01 6. 31E-01 4.87E-0l

3.39E-0l 2.43E-01 l.52E+00 6.07E-01 3.67E-01 4. 96E-01 l.16E+00 4.30E-01

Tolerance

Nuclide

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0271

Analysis Report for 1803111-04

m

m

M M m

M m m

AC-SED-11

Peak No. Energy (keV)

3 76.81 8 269.77

11 328.20 14 384.90 15 427.01 16 462.09 18 480.28 19 511.37 23 665.38

25 767.85 26 794.18 28 883.58 30 925.35 31 965. 2 9 33 1078.18 34 1082.18 36 1238.93 37 1262.15 38 1334.92 40 1560.68 41 1582.32 42 1587.31 43 1590.31 44 1593.00 46 1848.86 47 1873.12 48 1939.70 49 2086.60 50 2146.73

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet

Errors quoted at 2.000sigma

4/17/2018 7:44:46AM

Peak Size (CPS) Peak CPS(%) Peak

Uncertainty Type

2.08073E-01 8.34 l.58224E-02 44.62

l.05364E-02 45.68 Tol.

7.56944E-03 59.63 6.43072E-03 59.57 Sum

2. 02778E-02 28.87

4. 50231E-03 74.18

l.75959E-02 39.16

6.00885E-03 47.71 Tol.

7.81893E-03 46.71 7.22222E-03 50.44 4.65278E-03 64.85 Sum

8.26389E-03 47.30

4.04624E-03 58.98

3.19991E-03 30.07

4.28806E-03 56.75 l.34583E-02 31.12 2.94935E-03 46.91 1. 027 78E-02 29.23 2.36111E-03 56.57

2.50000E-03 43.74

3.64469E-03 28.07 Sum

3.06760E-03 52.07

3.88818E-03 36.47 D-Esc

3.67593E-03 33.85

2.55051E-03 42.18

2.22222E-03 35.36

l.66667E-03 40.82 l.22685E-03 65.03

NUCLIDE IDENTIFICATION REPORT

Nuclide Library Used : \\OR-GAMMA 1\ApexRoot\Countroom\Library\TMA2.NLB

IDENTIFIED NUCLIDES

Page 14 of 29

Tolerance

Nuclide

LA-140

SB-126 CE-143

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0272

4/17/2018 7:44:46AM Page 15 of29

Analysis Report for 1803111-04

AC-SED-11

Nuclide Id Energy Yield(%) Activity Activity

Name Confidence (keV) (pCi/grams) Uncertainty

BE-7 0.99 477.59 * 10.42 8.30E-01 5.26E-01

K-40 0.99 1460.81 * 10.67 1.68E+0l 2.31E+00

GA-67 0.65 93.31 * 35.70 9.08E+0l 4.54E+0l

208.95 2.24 300.22 * 16.00 6.61E+0l 7. 81E+0l

CD-109 0.86 88.03 * 3.72 2.46E+00 1.52E+00

SN-126 0. 96 87.57 * 37.00 2.38E-01 1.46E-01

CS-137 0.99 661.65 * 85.12 6.08E-02 5.21E-02

EU-155 0.32 86.50 * 30.90 2.88E-01 1.77E-01

105.30 20.70

TL-208 0. 96 583.14 * 30.22 1.00E+00 2.97E-01

860.37 * 4.48 1.05E+00 1.36E+00

2614.66 * 35.85 9.33E-01 2.58E-01

PB-210 0.94 46.50 * 4.25 2.0lE+00 1.69E+00

BI-212 0.76 727.17 * 11. 80 6.42E-01 4. 72E-01

1620.62 2.75

PB-212 0.89 238.63 * 44.60 1.37E+00 2.67E-01

300.09 * 3.41 1.02E+00 1.20E+00

BI-214 0.92 609.31 * 46.30 l.l0E+00 2.32E-01

1120.29 * 15.10 1.07E+00 6.31E-01

1764.49 * 15.80 1.15E+00 4.87E-01

2204.22 4.98

PB-214 0.99 295.21 * 19.19 1.39E+00 3.39E-01

351.92 * 37.19 9.54E-01 2.43E-01

RA-226 1. 00 186.21 * 3.28 2.47E+00 1.52E+00

AC-228 0.98 338.32 * 11. 40 l.20E+00 6.07E-01

911. 07 * 27.70 1.05E+00 3.67E-01

969.11 * 16.60 1.l0E+00 4.96E-01

TH-234 0.97 63.29 * 3.80 1.0lE+00 1.16E+00

NP-237 0.95 86.50 * 12.60 6.98E-01 4.30E-01

* = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity

Energy Tolerance : 1.000 keV

Nuclide confidence index threshold = 0.30

Errors quoted at 2.000sigma

INTERFERENCE CORRECTED REPORT

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0273

Analysis Report for 1803111-04

AC-SED-11

Nuclide Name

BE-7 K-40 GA-67

? CD-109 ? SN-126

CS-137 ? EU-155

TL-208 PB-210 BI-212 PB-212 BI-214 PB-214 RA-226 AC-228 TH-234

? NP-237

Nuclide Id

Confidence

0.997 0.999 0.659 0.860 0. 960 0.991 0.329 0. 960 0.940 0.763 0.892 0.924 0.994 1.000 0.982 0. 972 0.951

? nuclide is part of an undetermined solution

X = nuclide rejected by the interference analysis

4/17/2018 7:44:46AM

Wt mean Wt mean

Activity Activity

(pCi/grams) Uncertainty

8.30E-01 5.26E-01 1.68E+0l 2.31E+00 6.31E+0l 3.94E+0l 2.46E+00 1.52E+00 2.38E-01 1.46E-01 6.08E-02 5.21E-02 2.88E-01 1.77E-01 9.65E-01 1.93E-01 2. 0lE+00 1.69E+00 6.42E-01 4. 72E-01 1.31E+00 2.62E-01 1. llE+00 1.99E-01 1.l0E+00 1.98E-01 2.47E+00 1.52E+00 1.09E+00 2.66E-01 1.0lE+00 1.16E+00 6.98E-01 4.30E-0l

@ = nuclide contains energy lines not used in Weighted Mean Activity

Errors quoted at 2.000sigma

Page 16 of29

Comments

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0274

Analysis Report for 1803111-04

m

m

M

M

m

M

m m

AC-SED-11

Peak Locate Performed on

Peak Locate From Channel

Peak Locate To Channel

Peak No. Energy (ke V)

3 76.81

8 269.77

11 328.20

14 384.90

15 427.01

16 462.09

18 480.28

19 511.37

23 665.38

25 767.85

26 794.18

28 883.58

30 925.35

31 965. 2 9

33 1078.18

34 1082.18

36 1238.93

37 1262.15

38 1334.92

40 1560.68

41 1582.32

42 1587.31

43 1590.31

44 1593.00

46 1848.86

47 1873.12

48 1939.70

49 2086.60

so 2146.73

4/17/2018 7:44:46AM

UNIDENTIFIED PEAKS

: 4/17/2018 7:44:38AM

: 1 : 4096

Peak Size (CPS)

2.08073E-01

1.58224E-02

1.05364E-02

7.56944E-03

6. 43072E-03

2.02778E-02

4.50231E-03

1.75959E-02

6.00885E-03

7.81893E-03

7.22222E-03

4.65278E-03

8.26389E-03

4.04624E-03

3 .19991E-03

4.28806E-03

1.34583E-02

2.94935E-03

1. 027 7 8E-02

2. 36111E-03

2.SOOOOE-03

3.64469E-03

3.06760E-03

3.88818E-03

3.67593E-03

2.SSOSlE-03

2.22222E-03

1.66667E-03

1.22685E-03

Peak CPS(%) Peak

Uncertainty Type

8.34 44.62

45.68 Tol.

59.63 59.57 Sum

28.87 74.18

39.16

47.71 Tol.

46.71

50.44

64.85 Sum

47.30

58.98

30.07 56.75

31.12 46.91

29.23 56.57 43.74

28.07 Sum

52.07

36.47 D-Esc

33.85 42.18

35.36

40.82

65.03

Page 17 of29

Tolerance Nuclide

LA-140

SB-126

CE-143

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Analysis Report for 1803111-04

AC-SED-11

M = First peak in a multiplet region

m = Other peak in a multiplet region

F = Fitted singlet

Errors quoted at 2.000sigma

4/17/2018 7:44:46AM

NUCLIDE MDA REPORT

Nuclide Library Used : \\OR-GAMMA 1 \ApexRoot\Countroom\Library\TMA2.NLB

Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA

Name (keV) (pCi/grams) (pCi!grams) (pCi/grams)

+ BE-7 477.59 * 10.42 8.30E-01 1.35E+00 1.35E+00

+ NA-22 1274.54 99.94 1.23E-02 9.64E-02 9.64E-02

+ NA-24 1368.53 99.99 3.74E-02 3.45E-02 8.54E-02

2754.09 99.86 -1. 72E-02 3.45E-02

+ AL-26 1808.65 99.76 -4.57E-02 5.60E-02 5.60E-02

+ K-40 1460.81 * 10.67 1.68E+0l 1.36E+00 1.36E+00

+ @ AR-41 1293.64 99.16 1.00E+26 1.00E+26 1.00E+26

+ TI-44 67.88 94.40 -1.46E-02 7.14E-02 7.14E-02

78.34 96. 00 9.77E-02 9.80E-02

+ SC-46 889.25 98.98 -1.83E-02 9.87E-02 9.87E-02

1120.51 99.90 2.36E-01 1.84E-01

+ V-48 983.52 99.98 l.29E-01 2.80E-01 2.87E-01

1312.10 97.50 4.76E-02 2.80E-01

+ CR-51 320.08 9.83 -2.07E-01 1.14E+00 l.14E+00

+ MN-54 834.83 99.97 1.54E-02 1.0lE-01 1.0lE-01

+ CO-56 846.75 99. 96 1.64E-03 1.0lE-01 1.0lE-01

1037.75 14.03 -8.16E-02 7.16E-01

1238.25 67.00 1.84E-01 2.59E-01

1771.40 15.51 -2. 96E-02 5.00E-01

2587.48 16.90 -3.62E-02 3.36E-01

+ CO-57 122.06 85.51 1.59E-02 6.68E-02 6.68E-02

136.48 10.60 -6.16E-02 5.68E-01

+ CO-58 810.76 99.40 -2. 96E-02 9.24E-02 9.24E-02

+ FE-59 1099.22 56.50 -5.62E-02 2.31E-01 2.31E-01

1291.56 43.20 5. llE-02 3.30E-01

+ CO-60 1173.22 100.00 -4.98E-02 9.54E-02 9.54E-02

1332.49 100.00 6.57E-02 1.06E-01

+ ZN-65 1115.52 50.75 1.37E-02 2.14E-01 2.14E-01

+ GA-67 93.31 * 35.70 9.08E+0l 7. llE+0l 7. llE+0l

208.95 2.24 3.74E+02 8.08E+02

300.22 * 16.00 6.61E+0l 2.24E+02

+ SE-75 121.11 16.70 -1.23E-01 1.l0E-01 3.68E-01

Page 18 of29

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4/17/2018 7:44:46AM Page 19 of29

Analysis Report for 1803111-04

AC-SED-11

Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA

Name (keV) (pCi/grams) (pCilgrams) (pCi/grams)

SE-75 136.00 59.50 -1.20E-02 1.l0E-01 1.l0E-01

264.65 59.80 1.75E-02 1.l0E-01

279.53 25.20 -2.90E-02 2.53E-01

400.65 11. 40 5.03E-02 6.30E-01

+ RB-82 776.52 13.00 -2.60E-01 1.27E+00 1.27E+00

+ RB-83 520.41 46.00 1.12E-02 1.66E-01 1.66E-01

529.64 30.30 -7.69E-02 2.40E-01

552.65 16.40 3.0lE-01 5.06E-01

+ KR-85 513.99 0.43 -8.18E+00 1.74E+0l 1.74E+0l

+ SR-85 513.99 99.27 -4.75E-02 1.0lE-01 1.0lE-01

+ Y-88 898.02 93.40 -5. llE-02 8.58E-02 1.07E-01

1836.01 99.38 2.32E-02 8.58E-02

+ MO-93 263.06 56. 72 2.16E-02 6.14E-02 1.0lE-01

684.67 99.68 -1.59E-02 7.15E-02

1477.11 99.08 -1.84E-02 6.14E-02

+ NB-93M 16.57 9.43 0.00E+00 1.28E+00 1.28E+00

+ NB-94 702.63 100.00 2.25E-03 7.38E-02 8.93E-02

871.10 100.00 -3.21E-02 7.38E-02

+ NB-95 765.79 99.81 -7.35E-03 1.72E-01 1. 72E-01

+ NB-95M 235.69 25.00 -4.02E+02 4.25E+0l 4.25E+0l

+ ZR-95 724.18 43.70 3.04E-02 l.96E-01 3.04E-01

756.72 55.30 -l.09E-02 1.96E-01

+ MO-99 181.06 6.20 -1.63E+02 5.21E+02 7.93E+02

739.58 12.80 3.l0E+0l 5.21E+02

778.00 4.50 -4.80E+0l 1.58E+03

+ TC-99M 140.51 89.00 -1.39E-02 5.89E-02 5.89E-02

+ RU-103 497.08 89.00 -5.85E-02 9.92E-02 9.92E-02

+ RU-106 621.84 9.80 4.98E-0l 8.65E-01 8.65E-01

+ AG-108M 433.93 89.90 3.52E-02 6.54E-02 6.54E-02

614.37 90.40 -1.22E-01 7.53E-02

722.95 90.50 2.23E-02 9.61E-02

+ CD-109 88.03 * 3. 72 2.46E+00 2.42E+00 2.42E+00

+ AG-ll0M 657.75 93.14 2.62E-03 8.42E-02 8.42E-02

677.61 10.53 2.43E-02 7.84E-01

706.67 16.46 9.70E-02 5.87E-01

763.93 21.98 -2.74E-03 4.33E-01

884.67 21.98 1.13E-01 4.25E-01

1384.27 23.94 9.70E-02 4.12E-01

+ CD-113M 263.70 0.02 5.34E+0l 2.49E+02 2.49E+02

+ SN-113 255.12 1. 93 -4.19E-01 1.07E-01 3.35E+00

391.69 64.90 5.l0E-03 l.07E-01

+ TE-123M 159.00 84.10 2.97E-02 7.39E-02 7.39E-02

+ SB-124 602.71 97.8'7 -1.05E-02 9.33E-02 9.33E-02

645.85 7.26 2.61E-03 1.44E+00

722.78 11.10 2.48E-01 1.07E+00

1691.02 49.00 5.21E-02 2.24E-01

+ I-125 35.49 6.49 2.62E-01 1.93E+00 1.93E+00

+ SB-125 176.33 6.89 1.33E-01 2.05E-01 7.95E-01

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4/17/2018 7:44:46AM Pago 20 of29

Analysis Report for 1803111-04

AC-SED-11

Nuclide Energy Yield(¾) Activity Nuclide MDA Line MDA

Name (keV) (pCi!grams) (pCi!grams) (pCilgrams)

SB-125 427.89 29.33 1.25E-01 2.05E-01 2.05E-01

463.38 10.35 3.95E-01 7.05E-01

600.56 17.80 -1.29E-01 3.48E-01

635.90 11. 32 2.41E-01 7.24E-01

+ SB-126 414.70 83.30 -2.23E-02 6.41E-02 6.41E-02

666.33 99.60 -l.31E-02 8.03E-02

695.00 99.60 2.42E-02 9.00E-02

720.50 53.80 2.59E-02 1.58E-01

+ SN-126 87.57 * 37.00 2.38E-01 2.33E-01 2.33E-0l

+ SB-127 473.00 25.00 -2.66E+0l 2.53E+0l 2.85E+0l

685.00 35.70 -5.63E+00 2.53E+0l

783.80 14.70 5.62E+0l 7.74E+0l

+ I-129 29.78 57.00 1.53E-01 2.41E-01 2.41E-01

33.60 13.20 7.87E-02 7.77E-01

39.58 7.52 9.99E-02 9.87E-01

+ I-131 284.30 6.05 1.24E+00 7.99E-01 9.21E+00

364.48 81.20 3.28E-02 7.99E-01

636.97 7.26 3.44E+00 1.14E+0l

722.89 1. 80 1.14E+0l 4.92E+0l

+ TE-132 49.72 13.10 -l.51E+02 2.05E+0l 1.34E+02

228.16 88.00 -3.l0E+00 2.05E+01

+ BA-133 81.00 33.00 -8.25E-01 1.00E-01 1.81E-01

302.84 17.80 5.22E-02 3.44E-01

356.01 60.00 3.59E-02 1.00E-01

+ I-133 529.87 86.30 -4.86E+07 1.51E+08 1.51E+08

+ XE-133 81.00 38.00 -2.50E+0l 5.50E+00 5.50E+00

+ CS-134 563.23 8.38 2.77E-02 7.81E-02 8.l0E-01

569.32 15.43 -3.0lE-02 4.48E-01

604.70 97.60 5.72E-03 7.81E-02

795.84 85.40 7.30E-02 l.22E-01

801.93 8.73 l.03E-01 1.07E+00

+ CS-135 268.24 16.00 6. llE-02 3.99E-01 3.99E-01

+ @ I-135 1131.51 22.50 1.00E+26 1. 00E+2 6 1.00E+26

@ 1260.41 28.60 l.00E+26 1.00E+26

@ 1678.03 9.54 1.00E+26 1.00E+26

+ CS-136 153.22 7.46 1.llE+00 3.26E-01 3.17E+00

163.89 4.61 -2.14E-01 4.73E+00

176.55 13.56 2.74E-01 1.64E+00

273. 65 12.66 3.00E-01 1.95E+00

340.57 48.50 1.06E+00 6.73E-01

818.50 99.70 1.83E-01 3.26E-01

1048.07 79.60 -2.42E-02 4.50E-01

1235.34 19.70 1.13E-01 2.55E+00

+ CS-137 661.65 * 85.12 6.08E-02 1.l0E-01 1.l0E-01

+ LA-138 788.74 34.00 -1.41E-01 1.07E-01 2.27E-01

1435.80 66.00 2.89E-02 l.07E-01

+ CE-139 165.85 80.35 6.51E-03 7.89E-02 7.89E-02

+ BA-140 162. 64 6.70 -3.46E+00 1.14E+00 3.21E+00

304.84 4.50 1.36E+00 5. llE+00

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4/17/2018 7:44:46AM Page 21 of29

Analysis Report for 1803111-04

AC-SED-11

Nuclide Energy Yield(¾) Activity Nuclide MDA Line MDA

Name (keV) (pCi/grams) (pCi/grams) (pCi!grams)

BA-140 423.70 3.20 -1.llE+00 1.14E+00 7.53E+00

437.55 2.00 -l.92E+00 1.18E+01

537.32 25.00 9.16E-02 1.14E+00

+ LA-140 328.77 20.50 7.77E-01 3.39E-01 1.34E+00

487.03 45.50 6.83E-02 5.74E-01

815.85 23.50 1.08E-01 1.42E+00

1596.49 95.49 2.70E-02 3.39E-01

+ CE-141 145.44 48.40 5.61E-02 2.05E-01 2.05E-01

+ CE-143 57.36 11. 80 -1.08E+05 1.67E+05 4.47E+05

293.26 42.00 2.02E+05 1.67E+05

664.55 5.20 1.32E+06 1.43E+06

+ CE-144 133.54 10.80 -1.36E-01 5.55E-01 5.55E-01

+ PM-144 476.78 42.00 1.14E-01 7.96E-02 1.82E-01

618.01 98.60 -1.55E-02 7. 96E-02

696. 4 9 99.49 l.93E-02 9.31E-02

+ PM-145 36.85 21. 70 1.09E-01 2.l0E-01 3.95E-01

37.36 39.70 5.80E-02 2.l0E-01

42.30 15.10 -5.19E-02 4.47E-01

72. 40 2.31 -1.34E-01 2.96E+00

+ PM-146 453.90 39.94 1.99E-02 1.56E-01 1.56E-01

735.90 14.01 -1.57E-01 5.07E-01

747.13 13.10 2.23E-02 5.88E-01

+ ND-147 91.11 28.90 -l.51E+00 1.37E+00 1.37E+00

531.02 13.10 -1.62E-01 2.57E+00

+ PM-149 285.90 3.10 -2.89E+03 7.99E+03 7.99E+03

+ EU-152 121.78 20.50 6.20E-02 2.61E-01 2.61E-01

244.69 5.40 -1. 96E-01 1.30E+00

344.27 19.13 -5.62E-02 2.68E-01

778.89 9.10 -1.32E-01 9.15E-01

964.01 10.40 -1.17E-01 9.79E-01

1085.78 7.22 2.60E-01 1.39E+00

1112.02 9.60 1.72E-01 1.06E+00

1407.95 14.94 1.62E-01 5.30E-01

+ GD-153 97.43 31.30 2.57E-03 1.86E-01 1.86E-01

103.18 22.20 -2. llE-01 2.49E-01

+ EU-154 123.07 40.50 6.24E-02 1.34E-01 1.34E-01

723.30 19.70 4.75E-02 4.70E-01

873.19 11. 50 -l.24E-01 6.65E-01

996.32 10.30 -8.68E-01 7.28E-01

1004.76 1 7. 90 -4.04E-02 5.l0E-01

1274.45 35.50 3.43E-02 2.68E-01

+ EU-155 86.50 * 30.90 2.88E-01 2.54E-01 2.82E-01

105.30 20.70 -7.34E-02 2.54E-01

+ EU-156 811.77 10.40 -2.85E-01 2.35E+00 2.35E+00

1153.47 7.20 2.34E+00 5.12E+00

1230.71 8.90 1.60E+00 4. llE+00

+ HO-166M 184.41 72. 60 6.24E-02 9.45E-02 9.45E-02

280.45 29.60 -8.49E-02 1.83E-01

410.94 11.10 2.18E-01 5.42E-01

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Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA

Name (keV) (pCi/grams) (pCi/grams) (pCi/grams)

HO-166M 711.69 54.10 -9 .16E-03 9.45E-02 1.55E-01

+ TM-171 66. 72 0.14 1.68E+0l 5.25E+0l 5.25E+0l

+ HF-172 67.35 5.31 9.16E-01 4.68E-01 1.31E+00

125.82 11. 30 -5.40E-01 4.68E-01

+ LU-1 72 181.53 20.60 -9.02E-01 2.39E+00 4.39E+00

900. 72 29.81 1.98E+00 5.08E+00

1093.66 62.50 3.77E-02 2.39E+00

+ LU-173 100.72 5.24 9.84E-01 3.12E-01 1.09E+00

272.11 21.20 9.55E-02 3.12E-01

+ HF-175 343.40 84.00 1.85E-02 8.53E-02 8.53E-02

+ LU-176 88.34 13. 30 5.59E-0l 5.99E-02 5.54E-01

201.83 86.00 -3.05E-02 6.47E-02

306.78 94.00 3.98E-02 5.99E-02

+ HF-181 133.02 41.70 -5.llE-02 1.06E-01 2.09E-01

345.85 17.20 1.45E-02 4.60E-01

482.03 82.80 -2.02E-02 1.06E-01

+ TA-182 67.75 41.20 -3.93E-02 1.93E-01 1.93E-0l

1121.30 34.90 5.llE-01 4.92E-01

1189.05 16.23 -2.86E-01 6.72E-01

1221.41 26.98 -1. 72E-01 4.42E-01

1231.02 11. 44 4.30E-01 1.l0E+00

+ IR-192 308.46 29.68 -9.27E-02 1.52E-01 2.25E-01

468.07 48.10 1.04E-02 1.52E-01

+ HG-203 279.19 77.30 -1.21E-02 1.05E-01 1.05E-01

+ TL-204 374.74 94 .11 -1.39E-03 5.95E-02 5.95E-02

899.15 99.16 -2.l0E-02 8.98E-02

911.74 91.10 3.27E-01 1.70E-01

+ BI-207 569.67 97. 72 -4.64E-03 6.91E-02 6.91E-02

1063.62 74.90 -1.03E-02 1.22E-01

+ TL-208 583.14 * 30.22 1.00E+00 1.34E-01 3.59E-01

860.37 * 4.48 1.05E+00 2.21E+00

2614.66 * 35.85 9.33E-01 1.34E-01

+ BI-210M 262.00 45.00 3.55E-02 1.27E-01 1.27E-01

300.00 23.00 2.57E-01 2.74E-01

+ PB-210 46.50 * 4.25 2.0lE+00 2.74E+00 2.74E+00

+ PB-211 404.84 2.90 1.08E+00 2.20E+00 2.20E+00

831.96 2.90 -8.08E-01 3.02E+00

+ BI-212 727.17 * 11.80 6.42E-01 7.25E-01 7.25E-01

1620.62 2.75 1.51E+00 3.21E+00

+ PB-212 238.63 * 44.60 1.37E+00 2.45E-01 2.45E-01

300.09 * 3.41 1.02E+00 3.45E+00

+ BI-214 609.31 * 46.30 1.l0E+00 2.12E-01 2.12E-01

1120.29 * 15.10 1.07E+00 9.48E-01

1764.49 * 15.80 1.15E+00 5.86E-01

2204.22 4.98 1.20E+00 2.12E+00

+ PB-214 295.21 * 19.19 1.39E+00 2.16E-01 6.00E-01

351.92 * 37.19 9.54E-01 2.16E-01

+ RN-219 401.80 6.50 -7.43E-02 9.63E-01 9.63E-01

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Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA

Name (keV) (pCilgrams) (pCilgrams) (pCilgrams)

+ RA-223 323.87 3.88 6.43E-01 1.43E+00 1.43E+00

+ RA-224 240.98 3.95 6.00E+00 2.80E+00 2.80E+00

+ RA-225 40.00 31.00 -3.61E-0l 7.94E-01 7.94E-01

+ RA-226 186.21 * 3.28 2.47E+00 2.38E+00 2.38E+00

+ TH-227 50.10 8.40 l.45E-01 6.87E-01 6.87E-01

236.00 11. 50 -3.0lE+00 7.63E-01

256.20 6.30 -l.12E-01 8.75E-01

+ AC-228 338.32 * 11. 40 l.20E+00 3.95E-01 8.86E-01

911.07 * 27.70 1.05E+00 3.95E-01

969 .11 * 16.60 1.l0E+00 9.40E-01

+ TH-230 48.43 16.90 4.75E-01 4.21E-01 4.21E-01

62.85 4.60 1.21E+00 1.60E+00

67.67 0.37 1.28E+0l 1.82E+0l

+ PA-231 283.67 1. 60 8. 72E-01 2.65E+00 3.46E+00

302.67 2.30 4.02E-01 2.65E+00

+ TH-231 25.64 14.70 0.00E+00 7.27E-02 7.27E-02

84.21 6.40 -1.99E+00 9.74E-01

+ PA-233 311.98 38.60 9.88E-03 2.76E-01 2.76E-01

+ PA-234 131. 20 20.40 1.llE-01 2.84E-01 2.84E-01

733.99 8.80 2.59E-01 8.08E-01

946.00 12.00 -l.44E-01 7.12E-01

+ PA-234M 1001.03 0.92 7.83E-0l 9.35E+00 9.35E+00

+ TH-234 63.29 * 3.80 1.0lE+00 l.91E+00 1.91E+00

+ U-235 143.76 10.50 -5.22E-01 4.93E-01 4.93E-01

163.35 4.70 -l.60E-01 1.09E+00

205.31 4.70 -2.36E-01 1.20E+00

+ NP-237 86.50 * 12.60 6.98E-01 6.85E-01 6.85E-01

+ NP-239 106.10 22.70 2.18E+02 6.52E+02 6.52E+02

228.18 10.70 -2.29E+02 1.51E+03

277.60 14.10 -l.84E+02 l.09E+03

+ AM-241 59.54 35.90 -2. 96E-03 l.93E-01 1.93E-01

+ AM-243 74.67 66.00 -4.79E-0l l.30E-01 1.30E-01

+ CM-243 209.75 3.29 8.38E-01 3.98E-01 1.81E+00

228.14 10.60 -8.40E-02 5.55E-01

277.60 14.00 -6.74E-02 3.98E-01

+ = Nuclide identified during the nuclide identification

* = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

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NUCLIDE MDA REPORT

Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\TMA2.NLB

Nuclide Energy Yield(¾) Line MDA Nuclide MDA Activity Dec. Level

Name (keV) (pCilgrams) (pCilgrams) (pCi!grams) (pCi/grams)

+ BE-7 477.59 * 10.42 1.35E+00 1.35E+00 8.30E-0l 6.47E-01

NA-22 1274.54 99.94 9.64E-02 9.64E-02 1.23E-02 4.34E-02

NA-24 1368.53 99.99 8.54E-02 3.45E-02 3.74E-02 3.78E-02

2754.09 99.86 3.45E-02 -1.72E-02 1.09E-02

AL-26 1808.65 99.76 5.60E-02 5.60E-02 -4.57E-02 2.22E-02

+ K-40 1460.81 * 10.67 1.36E+00 1.36E+00 1.68E+0l 6.32E-01

@ AR-41 1293.64 99.16 1.00E+26 1.00E+26 1.00E+26 1.00E+20

TI-44 67.88 94.40 7.14E-02 7.14E-02 -1.46E-02 3.47E-02

78.34 96. 00 9.80E-02 9.77E-02 4.80E-02

SC-46 889.25 98.98 9.87E-02 9.87E-02 -1.83E-02 4.49E-02

1120. 51 99.90 1.84E-01 2.36E-01 8.68E-02

V-48 983.52 99.98 2.87E-01 2.80E-01 1.29E-01 1.31E-01

1312.10 97.50 2.80E-01 4.76E-02 1.24E-01

CR-51 320.08 9.83 1.14E+00 1.14E+00 -2.07E-01 5.38E-01

MN-54 834.83 99.97 1.0lE-01 1.0lE-01 1.54E-02 4.68E-02

CO-56 846.75 99. 96 1.0lE-01 1.0lE-01 1.64E-03 4.59E-02

1037.75 14.03 7.16E-01 -8.16E-02 3.21E-01

1238.25 67.00 2.59E-01 1.84E-01 1.21E-01

1771.40 15.51 5.00E-01 -2. 96E-02 2.02E-01

2587.48 16.90 3.36E-01 -3.62E-02 1.19E-01

CO-57 122.06 85.51 6.68E-02 6.68E-02 1.59E-02 3.22E-02

136.48 10.60 5.68E-01 -6.16E-02 2.74E-01

CO-58 810.76 99.40 9.24E-02 9.24E-02 -2. 96E-02 4.19E-02

FE-59 1099.22 56.50 2.31E-01 2.31E-01 -5.62E-02 1.04E-01

1291.56 43.20 3.30E-01 5. llE-02 l.48E-01

CO-60 1173.22 100.00 9.54E-02 9.54E-02 -4.98E-02 4.33E-02

1332.49 100.00 1.06E-01 6.57E-02 4.81E-02

ZN-65 1115.52 50.75 2.14E-01 2.14E-01 l.37E-02 9.81E-02

+ GA-67 93.31 * 35.70 7.llE+0l 7.llE+0l 9.08E+0l 3.48E+0l

208.95 2.24 8.08E+02 3.74E+02 3.88E+02

300.22 * 16.00 2.24E+02 6.61E+0l 1.09E+02

SE-75 121.11 16.70 3.68E-01 1.l0E-01 -l.23E-01 1.78E-01

136.00 59.50 1.l0E-01 -l.20E-02 5.33E-02

264.65 59.80 1.l0E-01 1.75E-02 5.26E-02

279.53 25.20 2.53E-01 -2.90E-02 1. 20E-01

400.65 11.40 6.30E-01 5.03E-02 2. 96E-01

RB-82 776.52 13.00 1.27E+00 1. 27E+00 -2.60E-01 5.84E-01

RB-83 520.41 46.00 1.66E-01 1.66E-01 1.12E-02 7.69E-02

529.64 30.30 2.40E-01 -7.69E-02 1.l0E-01

552.65 16.40 5.06E-01 3.0lE-01 2.35E-01

KR-85 513.99 0.43 1.74E+0l 1.74E+0l -8.18E+00 8.17E+00

SR-85 513.99 99.27 1.0lE-01 1.0lE-01 -4.75E-02 4.74E-02

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Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level

Name (keV) (pCi/grams) (pCilgrams) (pCilgrams) (pCilgrams)

Y-88 898.02 93.40 l.07E-01 8.58E-02 -5. llE-02 4.90E-02

1836.01 99.38 8.58E-02 2.32E-02 3.59E-02

MO-93 263.06 56. 72 l.0lE-01 6.14E-02 2.16E-02 4.80E-02

684.67 99.68 7.15E-02 -l.59E-02 3.29E-02

14Tl.ll 99.08 6.14E-02 -l.84E-02 2.54E-02

NB-93M 16.57 9.43 l.28E+00 l.28E+00 0.00E+00 0.00E+00

NB-94 702.63 100.00 8.93E-02 7.38E-02 2.25E-03 4.17E-02

871.10 100.00 7.38E-02 -3.21E-02 3.34E-02

NB-95 765.79 99.81 1. 72E-01 l.72E-01 -7.35E-03 8.08E-02

NB-95M 235.69 25.00 4.25E+0l 4.25E+0l -4.02E+02 2.04E+0l

ZR-95 724.18 43.70 3.04E-01 l.96E-01 3.04E-02 l.43E-01

756.72 55.30 1. 96E-01 -l.09E-02 9.05E-02

MO-99 181.06 6.20 7.93E+02 5. 21E+02 -l.63E+02 3.81E+02

739.58 12.80 5. 21E+02 3.l0E+0l 2.39E+02

778.00 4.50 l.58E+03 -4.80E+0l 7.26E+02

TC-99M 140.51 89.00 5.89E-02 5.89E-02 -l.39E-02 2.84E-02

RU-103 497.08 89.00 9.92E-02 9.92E-02 -5.85E-02 4.56E-02

RU-106 621.84 9.80 8.65E-01 8.65E-01 4.98E-01 4.04E-01

AG-108M 433.93 89.90 6.54E-02 6.54E-02 3.52E-02 3.05E-02

614.37 90.40 7.53E-02 -l.22E-01 3.48E-02

722.95 90.50 9.61E-02 2.23E-02 4.48E-02

+ CD-109 88.03 * 3.72 2.42E+00 2.42E+00 2.46E+00 l.18E+00

AG-ll0M 657.75 93.14 8.42E-02 8.42E-02 2.62E-03 3.89E-02

677.61 10.53 7.84E-01 2.43E-02 3.63E-01

706.67 16.46 5.87E-01 9.70E-02 2.74E-01

763.93 21.98 4.33E-01 -2.74E-03 2.0lE-01

884.67 21. 98 4.25E-01 l.13E-01 l.95E-01

1384.27 23.94 4.12E-01 9.70E-02 l.84E-01

CD-113M 263.70 0.02 2.49E+02 2.49E+02 5.34E+0l l.18E+02

SN-113 255.12 1. 93 3.35E+00 l.07E-01 -4.19E-01 l.59E+00

391.69 64.90 l.07E-01 5.l0E-03 5.0lE-02

TE-123M 159.00 84.10 7.39E-02 7.39E-02 2.97E-02 3.56E-02

SB-124 602.71 97.87 9.33E-02 9.33E-02 -l.05E-02 4. 31E-02

645.85 7.26 l.44E+00 2.61E-03 6.69E-01

722. 7 8 11.10 l.07E+00 2.48E-01 4.97E-01

1691.02 49.00 2.24E-01 5.21E-02 9.62E-02

I-125 35.49 6.49 l.93E+00 l.93E+00 2.62E-01 9.20E-01

SB-125 176.33 6.89 7.95E-01 2.05E-01 l.33E-01 3.82E-01

427.89 29.33 2.05E-01 l.25E-01 9.56E-02

463.38 10.35 7.05E-01 3.95E-01 3.32E-01

600.56 17.80 3.48E-01 -l.29E-01 l.59E-01

635.90 11. 32 7.24E-01 2.41E-01 3.38E-01

SB-126 414.70 83.30 6.41E-02 6.41E-02 -2.23E-02 2.98E-02

666.33 99.60 8.03E-02 -l.31E-02 3.74E-02

695.00 99.60 9.00E-02 2.42E-02 4.21E-02

720.50 53.80 l.58E-01 2.59E-02 7.32E-02

+ SN-126 87.57 * 37.00 2.33E-01 2.33E-01 2.38E-01 l.14E-01

SB-127 473.00 25.00 2.85E+0l 2.53E+0l -2.66E+0l l.32E+0l

685.00 35.70 2.53E+0l -5.63E+00 l.16E+0l

783.80 14.70 7.74E+0l 5.62E+0l 3.60E+0l

I-129 29.78 57.00 2.41E-01 2.41E-0l l.53E-01 l.15E-01

33.60 13. 20 7.77E-01 7.87E-02 3.70E-01

39.58 7.52 9.87E-01 9.99E-02 4.70E-01

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Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level

Name (keV) (pCi!grams) (pCi!grams) (pCi/grams) (pCi/grams)

I-131 284.30 6.05 9.21E+00 7.99E-01 1.24E+00 4.37E+00

364.48 81.20 7.99E-01 3.28E-02 3. 78E-01

636.97 7.26 1.14E+0l 3.44E+00 5.31E+00

722.89 1. 80 4.92E+0l 1.14E+0l 2.29E+0l

TE-132 4 9. 72 13.10 1.34E+02 2.05E+0l -1. 51E+02 6.39E+0l

228.16 88.00 2.05E+0l -3.l0E+00 9.82E+00

BA-133 81.00 33.00 1.81E-01 1.00E-01 -8.25E-01 8.79E-02

302.84 17.80 3.44E-01 5.22E-02 1.64E-01

356.01 60.00 1.00E-01 3.59E-02 4. 72E-02

I-133 529.87 86.30 1.51E+08 1.51E+08 -4.86E+07 6.97E+07

XE-133 81.00 38.00 5.50E+00 5.50E+00 -2.50E+0l 2.67E+00

CS-134 563.23 8.38 8.l0E-01 7.81E-02 2.77E-02 3.75E-01

569.32 15.43 4.48E-01 -3.0lE-02 2.08E-01

604.70 97.60 7.81E-02 5. 72E-03 3.63E-02

795.84 85.40 l.22E-01 7.30E-02 5.71E-02

801.93 8.73 1.07E+00 1.03E-01 4.97E-01

CS-135 268.24 16.00 3.99E-01 3.99E-01 6. llE-02 1.91E-01

@ I-135 1131.51 22.50 1.00E+26 1.00E+26 1.00E+26 1.00E+20

@ 1260.41 28.60 1.00E+26 1.00E+26 1.00E+20

@ 1678.03 9.54 1.00E+26 1.00E+26 1.00E+20

CS-136 153.22 7.46 3.17E+00 3.26E-01 1. llE+00 1.53E+00

163.89 4.61 4.73E+00 -2.14E-01 2.28E+00

176.55 13.56 1.64E+00 2.74E-01 7.87E-01

273.65 12.66 1.95E+00 3.00E-01 9.27E-01

340.57 48.50 6.73E-01 l.06E+00 3.23E-01

818.50 99.70 3.26E-01 1.83E-01 1.49E-01

1048.07 79.60 4.50E-01 -2.42E-02 2.04E-01

1235.34 19.70 2.55E+00 1.13E-01 1.18E+00

+ CS-137 661.65 * 85.12 1.l0E-01 1.l0E-01 6.08E-02 5.18E-02

LA-138 788.74 34.00 2.27E-01 1.07E-01 -1.41E-01 1.04E-01

1435.80 66.00 1.07E-01 2.89E-02 4.57E-02

CE-139 165.85 80.35 7.89E-02 7.89E-02 6.51E-03 3.80E-02

BA-140 162.64 6.70 3.21E+00 1.14E+00 -3.46E+00 1.54E+00

304.84 4.50 5.llE+00 1.36E+00 2.41E+00

423.70 3.20 7.53E+00 -1. llE+00 3.51E+00

437.55 2.00 1.18E+0l -1.92E+00 5.47E+00

537.32 25.00 1.14E+00 9.16E-02 5.31E-01

LA-140 328.77 20.50 1.34E+00 3.39E-01 7.77E-01 6.36E-01

487.03 45.50 5.74E-01 6.83E-02 2.67E-01

815.85 23.50 1.42E+00 1.08E-01 6.50E-01

1596.49 95.49 3.39E-01 2.70E-02 l.45E-01

CE-141 145.44 48.40 2.05E-01 2.05E-01 5.61E-02 9.90E-02

CE-143 57.36 11. 80 4.47E+05 1.67E+05 -1.08E+05 2.16E+05

293.26 42.00 1.67E+05 2.02E+05 8.10E+04

664.55 5.20 l.43E+06 l.32E+06 6. 72E+05

CE-144 133.54 10.80 5.55E-01 5.55E-01 -1.36E-01 2.68E-01

PM-144 476.78 42.00 1.82E-01 7. 96E-02 1.14E-01 8.56E-02

618.01 98.60 7. 96E-02 -1.55E-02 3.70E-02

696.49 99.49 9.31E-02 l.93E-02 4.35E-02

PM-145 36.85 21.70 3.95E-01 2.l0E-01 1.09E-01 1.88E-01

37.36 39.70 2.l0E-01 5.80E-02 1.00E-01

42.30 15.10 4.47E-01 -5.19E-02 2.14E-01

72. 40 2.31 2.96E+00 -1.34E-01 1.44E+00

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Nuclide Energy Yield(¾) Line MDA Nuclide MDA Activity Dec. Level

Name (keV) (pCi!grams) (pCi!grams) (pCi!grams) (pCi/grams)

PM-146 453.90 39.94 1.56E-01 1.56E-01 1.99E-02 7.29E-02

735.90 14.01 5.07E-01 -1.57E-01 2.32E-01

747.13 13.10 5.88E-01 2.23E-02 2.70E-01

ND-147 91.11 28.90 1.37E+00 1.37E+00 -1.51E+00 6.67E-01

531.02 13.10 2.57E+00 -1.62E-01 1.19E+00

PM-149 285.90 3.10 7.99E+03 7.99E+03 -2.89E+03 3.78E+03

EU-152 121.78 20.50 2.61E-01 2.61E-01 6.20E-02 l.26E-01

244.69 5.40 1.30E+00 -1.96E-01 6.24E-01

344.27 19.13 2.68E-01 -5.62E-02 1.26E-01

778.89 9.10 9.15E-01 -1.32E-01 4.23E-01

964.01 10.40 9.79E-01 -1.17E-01 4.53E-01

1085.78 7.22 1.39E+00 2.60E-01 6.36E-01

1112.02 9.60 1.06E+00 1.72E-01 4.87E-01

1407.95 14.94 5.30E-01 1.62E-01 2.31E-01

GD-153 97.43 31.30 1.86E-01 1.86E-01 2.57E-03 9.00E-02

103.18 22.20 2.49E-01 -2.llE-01 1.20E-01

EU-154 123.07 40.50 1.34E-01 1.34E-01 6.24E-02 6.45E-02

723. 30 19.70 4.70E-01 4.75E-02 2.20E-01

873.19 11. 50 6.65E-01 -1.24E-01 3.02E-01

996.32 10.30 7.28E-01 -8.68E-01 3.26E-01

1004.76 17.90 5.l0E-01 -4.04E-02 2.33E-01

1274.45 35.50 2.68E-01 3.43E-02 1.21E-01

+ EU-155 86.50 * 30.90 2.82E-01 2.54E-01 2.88E-01 1.38E-01

105.30 20.70 2.54E-01 -7.34E-02 1.23E-01

EU-156 811.77 10.40 2.35E+00 2.35E+00 -2.85E-01 1.07E+00

1153.47 7.20 5.12E+00 2.34E+00 2.35E+00

1230.71 8.90 4.llE+00 1.60E+00 l.88E+00

HO-166M 184.41 72. 60 9.45E-02 9.45E-02 6.24E-02 4.58E-02

280.45 29.60 1.83E-01 -8.49E-02 8.68E-02

410.94 11.10 5.42E-01 2.18E-01 2.54E-01

711.69 54.10 1.55E-01 -9.16E-03 7.21E-02

TM-171 66. 72 0.14 5.25E+0l 5.25E+0l 1.68E+0l 2.55E+0l

HF-172 67.35 5.31 1.31E+00 4.68E-01 9.16E-01 6.36E-01

125.82 11. 30 4.68E-01 -5.40E-01 2.25E-01

LU-1 72 181.53 20.60 4.39E+00 2.39E+00 -9.02E-01 2. llE+00

900. 72 29.81 5.08E+00 1.98E+00 2.34E+00

1093.66 62.50 2.39E+00 3.77E-02 1.09E+00

LU-173 100.72 5.24 1.09E+00 3.12E-01 9.84E-01 5.25E-01

272.11 21.20 3.12E-01 9.55E-02 1.49E-01

HF-175 343.40 84.00 8.53E-02 8.53E-02 1.85E-02 4.0lE-02

LU-176 88.34 13.30 5.54E-01 5.99E-02 5.59E-01 2.70E-01

201.83 86.00 6.47E-02 -3.05E-02 3.l0E-02

306.78 94.00 5.99E-02 3.98E-02 2.84E-02

HF-181 133.02 41.70 2.09E-01 1.06E-01 -5. llE-02 1.0lE-01

345.85 17.20 4.60E-01 l.45E-02 2.15E-01

482.03 82.80 1.06E-01 -2.02E-02 4. 92E-02

TA-182 67.75 41.20 1.93E-01 1.93E-01 -3.93E-02 9.35E-02

1121.30 34.90 4. 92E-01 5.llE-01 2.32E-01

1189.05 16.23 6. 72E-01 -2.86E-01 3.04E-01

1221.41 26.98 4.42E-01 -1.72E-01 2.0lE-01

1231.02 11. 44 1.l0E+00 4.30E-01 5.04E-01

IR-192 308.46 29.68 2.25E-01 1.52E-01 -9.27E-02 1.06E-01

468.07 48.10 1.52E-01 l.04E-02 7.05E-02

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4/17/2018 7:44:46AM Page 28 of29

Analysis Report for 1803111-04

AC-SED-11

Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level

Name (keV) (pCilgrams) (pCilgrams) (pCilgrams) (pCi/grams)

HG-203 279.19 77.30 l.05E-01 l.05E-01 -l.21E-02 4.99E-02

TL-204 374.74 94 .11 5.95E-02 5.95E-02 -l.39E-03 2.79E-02

899.15 99.16 8.98E-02 -2.l0E-02 4.13E-02

911. 7 4 91.10 l.70E-01 3.27E-01 8.08E-02

BI-207 569.67 97.72 6.91E-02 6.91E-02 -4.64E-03 3.20E-02

1063.62 74.90 l.22E-01 -l.03E-02 5.56E-02

+ TL-208 583.14 * 30.22 3.59E-01 l.34E-01 l.00E+00 l.71E-01

860.37 * 4.48 2.21E+00 l.05E+00 l.03E+00

2614.66 * 35.85 l.34E-01 9.33E-01 4.92E-02

BI-210M 262.00 45.00 l.27E-01 l.27E-01 3.55E-02 6.07E-02

300.00 23.00 2.74E-01 2.57E-01 l.31E-01

+ PB-210 46.50 * 4.25 2.74E+00 2.74E+00 2.0lE+00 l.34E+00

PB-211 404.84 2.90 2.20E+00 2.20E+00 l.08E+00 l.03E+00

831. 96 2.90 3.02E+00 -8.08E-01 l.39E+00

+ BI-212 727.17 * 11. 80 7.25E-01 7.25E-01 6.42E-01 3.37E-01

1620.62 2.75 3.21E+00 l.51E+00 l.41E+00

+ PB-212 238.63 * 44.60 2.45E-01 2.45E-01 l.37E+00 l.19E-01

300.09 * 3.41 3.45E+00 l.02E+00 l.68E+00

+ BI-214 609.31 * 46.30 2.12E-01 2.12E-01 l.l0E+00 l.0lE-01

1120.29 * 15.10 9.48E-01 l.07E+00 4.46E-01

1764.49 * 15.80 5.86E-01 l.15E+00 2.57E-01

2204.22 4.98 2.12E+00 l.20E+00 9.34E-01

+ PB-214 295.21 * 19.19 6.00E-01 2.16E-01 l.39E+00 2.92E-01

351.92 * 37.19 2.16E-01 9.54E-01 l.04E-01

RN-219 401.80 6.50 9.63E-01 9.63E-01 -7.43E-02 4.53E-01

RA-223 323.87 3.88 l.43E+00 l.43E+00 6.43E-01 6.73E-01

RA-224 240.98 3.95 2.80E+00 2.80E+00 6.00E+00 l.37E+00

RA-225 40.00 31.00 7.94E-01 7.94E-01 -3.61E-01 3.78E-01

+ RA-226 186.21 * 3.28 2.38E+00 2.38E+00 2.47E+00 l.15E+00

TH-227 50.10 8.40 6.87E-01 6.87E-01 l.45E-01 3.29E-01

236.00 11. 50 7.63E-01 -3.0lE+00 3.70E-01

256.20 6.30 8.75E-01 -l.12E-01 4.16E-01

+ AC-228 338.32 * 11.40 8.86E-0l 3.95E-01 l.20E+00 4.29E-01

911.07 * 27. 70 3.95E-01 l.05E+00 l.84E-01

969 .11 * 16.60 9.40E-01 l.l0E+00 4.47E-01

TH-230 48.43 16.90 4.21E-01 4.21E-01 4.75E-01 2.03E-01

62.85 4.60 l.60E+00 l.21E+00 7.76E-01

67. 67 0.37 l.82E+0l l.28E+0l 8.86E+00

PA-231 283.67 1. 60 3.46E+00 2.65E+00 8. 72E-01 l.64E+00

302.67 2.30 2.65E+00 4.02E-01 l.26E+00

TH-231 25.64 14.70 7. 27E-02 7. 27E-02 0.00E+00 0.00E+00

84.21 6.40 9.74E-01 -l.99E+00 4.73E-01

PA-233 311.98 38.60 2.76E-01 2.76E-01 9.88E-03 1. 30E-01

PA-234 131.20 20.40 2.84E-01 2.84E-01 l. llE-01 l.37E-01

733.99 8.80 8.08E-01 2.59E-01 3.70E-01

946.00 12.00 7.12E-01 -l.44E-01 3.25E-01

PA-234M 1001.03 0.92 9.35E+00 9.35E+00 7.83E-01 4.25E+00

+ TH-234 63.29 * 3.80 l.91E+00 l.91E+00 l.0lE+00 9.27E-01

U-235 143.76 10.50 4.93E-01 4.93E-01 -5.22E-01 2.37E-01

163.35 4.70 l.09E+00 -l.60E-01 5.25E-01

205.31 4.70 l.20E+00 -2.36E-01 5.78E-01

+ NP-237 86.50 * 12.60 6.85E-01 6.85E-01 6.98E-01 3.35E-01

NP-239 106.10 22.70 6.52E+02 6.52E+02 2.18E+02 3.15E+02

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0286

Analysis Report for 1803111-04

AC-SED-11

Nuclide Energy Yield(%)

Name (keV)

NP-239 228.18 10.70 277. 60 14.10

AM-241 59.54 35.90

AM-243 74.67 66.00

CM-243 209.75 3.29 228.14 10.60 277.60 14.00

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

Line MDA

(pCi/grams)

1.51E+03 1.09E+03 1.93E-01 1.30E-01 1.81E+00 5.55E-01 3.98E-01

@ = Half-life too short to be able to perform the decay correction

No Action Level results available for reporting purposes.

4/17/2018 7:44:46AM

Nuclide MDA Activity

(pCi/grams) (pCi/grams)

6.52E+02 -2.29E+02 -1.84E+02

1.93E-01 -2. 96E-03 1.30E-01 -4.79E-01 3.98E-01 8.38E-01

-8.40E-02 -6.74E-02

DATA REVIEW COMMENTS REPORT

Creation Date Comment User

No Data Review Comments Entered.

Page 29 of 29

Dec. Level

(pCi/grams)

7.25E+02 5.16E+02 9.34E-02 6.34E-02 8.70E-01 2.66E-01 1.89E-01

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Channel Data Report 4/17/2018 7:45:09 AM Page 1

*******************************************************

***** S P E C T R A L D A T A R E P O R T *****

*******************************************************

Sample Title: AC-SED-11

Elapsed Live time: 3600 Elapsed Real Time: 3601

Channell------1-------1-------1-------I-------I-------I-------I-------I

1: 0 0 0 0 0 0 0 0

9: 0 0 0 0 0 0 0 0

17: 0 0 0 0 0 0 0 0

25: 0 0 0 15 47 46 39 40

33: 44 54 47 41 45 58 40 45

41: 46 49 53 58 47 75 126 49

49: 71 46 56 55 59 62 60 53

57: 59 62 81 71 79 66 99 120

65: 66 71 85 95 77 65 93 83

73: 83 103 300 127 364 241 66 70

81: 78 62 70 90 91 73 143 152

89: 70 112 85 98 167 112 59 52

97: 54 55 71 64 49 61 39 51

105: 60 66 52 56 60 59 55 59

113: 46 48 52 50 55 57 51 44

121: 57 45 62 57 48 48 43 46

129: 68 76 49 61 47 58 64 48

137: 61 45 63 47 40 39 44 50

145: 51 70 45 54 46 51 53 45

153: 47 56 61 44 50 39 57 38

161: 33 34 44 38 48 44 49 47

169: 44 47 54 35 34 49 45 28

177: 31 47 40 45 44 37 44 47

185: 46 142 61 39 33 42 40 35

193: 45 27 37 35 25 39 40 40

201: 34 35 37 38 45 45 22 43

209: 59 46 32 26 41 25 33 40

217: 38 40 26 43 38 38 33 31

225: 35 29 40 33 42 33 39 36

233: 34 37 39 33 37 242 337 51

241: 78 105 37 23 41 24 31 25

249: 27 28 24 26 29 24 21 35

257: 23 29 27 26 27 31 32 23

265: 23 24 34 28 33 49 39 25

273: 22 29 27 24 26 30 13 24

281: 21 24 28 23 19 18 21 26

289: 23 17 19 24 24 78 157 78

297: 17 25 33 40 28 13 17 30

305: 19 17 18 22 13 18 23 24

313: 10 17 21 16 16 17 20 18

321: 22 25 27 15 15 12 28 39

329: 25 20 21 21 25 19 17 22

337: 35 72 40 28 23 21 9 18

345: 13 11 20 19 13 22 105 214

353: 42 13 18 25 23 16 18 13

361: 16 20 22 12 26 25 24 15

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Channel Data Report 4/17/2018 7:45:09 AM Page 2

369: 12 17 15 11 13 20 18 12

Sample Title: AC-SED-11

Channel[------[-------[-------[-------[-------[-------[-------[-------[

377: 15 14 15 19 12 11 20 21

385: 18 22 13 9 17 18 18 15

393: 11 19 15 15 13 15 11 22

401: 19 16 18 20 16 18 9 17

409: 19 20 12 8 17 6 16 11

417: 10 16 13 20 13 17 6 13

425: 13 12 17 17 9 2 14 9

433: 14 18 6 19 11 8 12 8

441: 12 20 15 4 13 8 14 15

449: 15 19 11 14 12 11 20 6

457: 12 16 18 15 10 23 33 16

465: 8 14 7 11 12 10 10 10

473: 8 14 9 10 32 23 12 17

481: 9 12 8 5 6 12 9 16

489: 15 9 20 3 10 16 9 9

4 97: 8 13 6 13 13 14 14 11

505: 11 10 10 15 26 47 58 37

513: 11 16 6 13 9 9 14 9

521: 9 12 14 5 11 10 9 10

529: 7 12 8 16 8 10 13 15

537: 9 10 12 9 16 12 5 6

545: 9 7 14 4 6 13 13 11

553: 11 9 8 8 6 8 11 9

561: 7 8 15 12 12 11 11 14

569: 10 11 9 15 8 10 18 10

577: 10 9 10 9 20 38 97 37

585: 15 8 7 6 7 10 9 5

593: 8 13 9 8 7 7 9 6

601: 8 10 10 15 14 12 17 75

609: 175 53 4 7 11 8 9 6

617: 4 10 11 7 12 15 4 10

625: 9 6 13 6 15 5 7 8

633: 12 12 9 9 11 5 9 8

641: 8 9 6 8 7 8 13 7

649: 5 12 5 10 8 8 8 7

657: 3 10 7 7 21 18 9 10

665: 16 9 4 4 8 12 9 7

673: 9 8 10 6 8 8 4 9

681: 4 10 5 6 5 9 5 7

689: 9 12 12 5 11 12 11 9

697: 11 5 9 9 8 11 17 8

705: 7 9 13 7 8 10 7 11

713: 8 8 6 8 5 8 9 8

721: 11 6 12 3 13 17 20 15

729: 5 3 7 8 3 7 5 6

737: 5 4 13 3 10 3 7 5

745: 5 9 5 4 12 4 6 8

753: 6 3 13 7 8 4 8 7

761: 8 10 4 10 6 13 10 24

769: 11 7 9 7 7 3 8 7

777: 11 6 3 8 6 7 12 8

785: 9 7 5 3 9 5 3 16

793: 5 16 13 7 7 9 7 10

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Channel Data Report 4/17/2018 7:45:09 AM Page 3

801: 11 5 8 7 7 7 4 4

Sample Title: AC-SED-11

Channel[------[-------l-------l-------l-------[-------1-------1-------1

809: 3 6 5 7 3 5 5 5

817: 9 5 5 5 6 1 4 4

825: 6 5 9 5 6 6 11 5

833: 9 7 11 8 7 7 10 12

841: 11 4 4 6 5 2 7 6

84 9: 6 1 5 6 11 4 6 3

857: 9 8 8 12 13 2 4 7

865: 7 3 5 6 5 2 5 4

873: 4 6 8 4 6 5 5 6

881: 3 10 10 6 7 3 4 4

889: 5 8 3 7 9 5 3 6

897: 5 7 7 6 9 6 9 5

905: 6 3 7 8 9 47 50 13

913: 3 6 2 4 6 3 3 4

921: 4 12 7 8 6 4 4 4

92 9: 10 6 2 8 10 4 7 3

937: 4 4 11 4 5 3 7 4

945: 7 6 6 4 11 4 3 4

953: 7 2 2 5 4 6 10 4

961: 7 5 10 9 13 4 16 35

969: 31 10 7 7 5 3 6 6

977: 11 5 3 6 6 7 3 3

98 5: 7 6 2 4 7 5 8 6

993: 7 2 5 4 1 5 1 10

1001: 7 5 5 3 6 5 7 6

1009: 6 8 8 4 4 10 4 4

1017: 5 2 0 8 1 2 3 6

1025: 5 7 3 3 2 6 2 5

1033: 7 3 8 5 2 4 0 3

1041: 3 3 4 1 4 6 3 10

1049: 5 3 3 9 6 2 11 6

1057: 4 5 8 5 4 3 8 6

1065: 6 3 5 4 3 7 4 5

1073: 6 4 5 0 9 6 4 4

1081: 10 7 7 2 8 4 7 6

1089: 3 4 5 5 6 6 5 3

1097: 6 4 3 5 3 4 5 3

1105: 6 7 6 6 5 5 8 5

1113: 4 8 2 6 4 11 21 30

1121: 8 9 7 2 7 5 10 4

112 9: 7 6 10 5 4 6 5 4

1137: 2 1 3 9 3 7 4 5

1145: 2 10 6 2 8 9 3 10

1153: 4 7 6 5 3 4 8 4

1161: 3 6 4 6 7 6 6 7

1169: 1 4 4 5 5 7 6 9

1177: 5 1 4 3 1 3 5 7

1185: 0 6 6 5 5 3 5 2

1193: 10 2 7 6 4 9 7 3

1201: 4 6 4 5 3 2 11 6

1209: 3 2 10 5 6 2 8 5

1217: 6 6 3 9 5 2 4 6

1225: 6 9 9 9 3 5 8 0

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Channel Data Report 4/17/2018 7:45:09 AM Page 4

1233 :. 5 9 7 8 14 11 10 3

Sample Title: AC-SED-11

Channell------l-------l-------l-------l-------1-------1-------1-------I

1241: 6 7 7 3 2 6 6 7

1249: 3 3 7 5 6 4 6 6

1257: 4 2 0 4 5 8 0 3

1265: 2 4 7 9 5 2 5 5

1273: 2 8 3 3 2 4 3 2

1281: 10 5 5 2 6 3 6 6

1289: 2 5 4 3 6 1 0 5

1297: 1 5 2 5 2 3 0 4

1305: 4 2 4 4 3 2 3 4

1313: 1 4 2 2 2 2 1 4

1321: 4 3 2 3 5 2 1 1

1329: 3 4 5 8 5 3 5 4

1337: 2 3 3 2 2 2 1 1

1345: 1 2 2 5 3 4 3 3

1353: 1 1 1 1 2 5 2 0

1361: 0 3 2 2 4 2 2 5

1369: 3 3 1 2 0 2 2 4

1377: 3 3 4 0 4 4 5 4

1385: 3 3 1 2 3 0 0 2

1393: 1 0 1 3 4 4 4 3

1401: 6 3 2 0 2 5 5 1

1409: 1 2 1 0 2 3 1 1

1417: 0 3 3 1 2 3 3 1

1425: 0 3 2 1 0 1 2 1

1433: 0 3 2 2 3 1 1 0

1441: 0 1 2 3 2 3 1 2

1449: 1 3 3 3 2 3 4 10

1457: 10 35 143 175 115 11 1 0

1465: 4 2 3 1 2 2 4 1

1473: 1 2 3 0 0 2 0 3

1481: 0 2 2 0 2 0 2 2

1489: 1 0 3 0 2 1 2 1

1497: 2 2 1 1 3 0 2 1

1505: 1 3 6 2 3 3 0 5

1513: 3 0 1 2 2 0 0 1

1521: 1 1 3 1 0 2 1 2

1529: 1 0 2 0 3 3 0 0

1537: 2 1 4 1 0 3 1 1

1545: 0 0 0 1 0 0 0 1

1553: 4 0 1 0 1 1 3 3

1561: 2 1 1 0 0 1 1 0

1569: 0 0 2 0 1 2 1 0

1577: 1 0 2 2 2 4 1 0

1585: 0 6 4 2 5 3 4 6

1593: 2 1 0 0 2 1 1 0

1601: 2 0 3 0 0 0 3 1

1609: 1 1 1 1 2 0 2 1

1617: 0 3 3 4 3 3 1 1

1625: 0 2 0 0 3 2 0 0

1633: 3 0 1 2 1 2 1 0

1641: 1 0 2 0 0 2 1 2

1649: 1 2 1 0 0 2 0 1

1657: 2 2 0 3 1 2 1 1

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0291

Channel Data Report 4/17/2018 7:45:09 AM Page 5

1665: 2 1 1 0 1 0 1 0

Sample Title: AC-SED-11

Channel[------[-------[-------[-------[-------[-------[-------1-------1

1673: 2 2 2 2 0 1 1 1

1681: 1 0 2 1 0 3 1 1

1689: 4 3 1 2 1 2 0 0

1697: 1 2 1 3 2 0 0 0

1705: 0 0 0 1 1 3 0 1

1713: 1 2 1 0 1 1 1 1

1721: 2 0 0 1 0 0 2 1

1729: 2 2 0 2 2 0 2 1

1737: 3 1 1 0 1 2 0 0

1745: 0 0 2 1 1 2 1 0

1753: 1 2 2 1 0 1 1 2

1761: 3 6 16 17 5 1 1 1

1769: 1 0 1 1 0 0 0 1

1777: 0 1 0 1 4 0 0 0

1785: 0 0 1 1 0 1 1 1

1793: 0 0 2 2 0 1 1 0

1801: 1 0 1 1 1 0 0 0

1809: 1 0 1 3 2 1 0 1

1817: 0 0 0 1 0 0 1 1

1825: 0 1 1 0 1 0 2 1

1833: 0 0 2 1 1 0 2 0

1841: 1 0 1 0 3 0 5 3

1849: 2 1 1 0 0 0 0 0

1857: 2 1 1 1 1 0 1 0

1865: 1 0 1 0 1 1 3 3

1873: 2 1 0 0 1 0 1 1

1881: 2 2 0 2 1 1 2 3

1889: 3 2 1 0 3 0 1 1

1897: 2 1 0 0 2 0 0 1

1905: 1 0 1 3 1 0 1 2

1913: 0 0 1 3 1 0 0 1

1921: 2 0 0 2 1 0 0 0

192 9: 1 0 1 0 0 0 1 0

1937: 1 1 3 2 0 0 0 1

1945: 2 0 1 0 1 1 0 0

1953: 3 1 0 0 1 1 0 2

1961: 2 2 1 0 0 1 0 0

1969: 0 0 0 0 0 1 1 0

1977: 2 0 1 0 1 0 1 0

1985: 0 2 2 1 1 0 0 1

1993: 0 1 2 0 2 0 1 0

2001: 1 1 1 0 2 0 2 1

2009: 1 1 0 0 1 1 2 1

2017: 3 1 1 0 1 1 1 0

2025: 1 1 1 0 1 0 0 0

2033: 3 2 2 1 0 2 0 1

2041: 0 0 1 0 0 0 2 0

204 9: 0 2 0 0 1 1 1 1

2057: 1 0 0 0 0 0 3 1

2065: 2 0 2 0 0 0 0 0

2073: 0 1 0 1 1 0 2 3

2081: 0 0 0 2 1 3 0 0

2089: 1 2 2 0 0 2 0 0

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Channel Data Report 4/17/2018 7:45:09 AM Page 6

2097: 0 1 4 3 4 1 2 2

Sample Title: AC-SED-11

Channell------1-------1-------1-------I-------I-------I-------I-------I

2105: 3 0 2 1 1 1 0 0

2113: 1 2 2 1 0 1 1 0

2121: 1 1 1 2 0 1 0 2

2129: 1 1 0 0 2 1 2 0

2137: 2 0 0 0 1 0 0 2

2145: 1 3 0 0 0 1 0 2

2153: 0 1 0 1 1 1 2 1

2161: 0 1 2 0 1 2 0 0

2169: 1 0 1 0 0 1 2 0

2177: 1 0 1 1 3 1 0 1

2185: 0 1 0 1 0 0 1 2

2193: 0 0 1 1 0 1 2 2

2201: 5 1 2 4 0 2 1 1

2209: 0 1 0 1 0 1 0 1

2217: 0 1 0 0 0 0 1 2

2225: 0 0 1 0 0 0 2 0

2233: 0 0 3 1 0 0 1 3

2241: 0 0 1 0 0 1 0 0

2249: 0 0 0 0 0 0 1 0

2257: 0 2 2 1 1 1 0 0

2265: 1 0 0 1 1 0 1 0

2273: 1 0 1 1 1 1 0 2

2281: 0 1 0 0 1 1 0 1

2289: 1 1 0 1 2 0 2 0

2297: 0 1 0 1 0 0 1 1

2305: 1 2 0 0 2 0 1 1

2313: 1 2 1 0 0 0 1 2

2321: 0 0 0 1 1 1 2 1

2329: 1 2 0 0 1 1 1 0

2337: 1 1 1 1 3 0 2 0

2345: 2 1 2 1 1 0 0 2

2353: 1 1 0 2 0 1 0 1

2361: 0 4 1 2 0 2 1 2

2369: 0 1 0 0 2 2 0 1

2377: 1 1 0 2 0 0 1 0

2385: 0 2 1 0 0 1 0 0

2393: 0 1 0 0 0 0 0 0

2401: 2 0 0 0 0 0 1 0

2409: 1 0 0 0 0 1 1 1

2417: 1 1 1 0 1 1 0 2

2425: 0 0 0 0 1 1 0 0

2433: 0 0 0 1 0 1 1 0

2441: 1 0 1 0 1 3 1 0

2449: 1 0 0 0 0 2 0 1

2457: 1 0 1 0 0 0 0 0

2465: 0 0 0 1 1 1 0 0

2473: 2 0 1 0 0 0 0 0

2481: 0 1 1 1 0 0 0 1

2489: 0 0 0 0 0 0 0 0

2497: 0 1 0 0 1 0 0 0

2505: 0 0 0 0 0 0 0 1

2513: 0 0 0 0 1 0 1 0

2521: 0 0 1 0 1 0 1 1

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0293

Channel Data Report 4/17/2018 7:45:09 AM Page 7

2529: 0 1 0 0 1 0 1 0

Sample Title: AC-SED-11

Channell------l-------1-------1-------1-------I-------I-------I-------I

2537: 1 0 0 1 0 0 0 1

2545: 3 1 1 0 0 0 0 0

2553: 0 0 0 0 0 0 0 0

2561: 0 1 2 0 0 0 1 0

2569: 1 1 0 0 0 0 1 0

2577: 1 0 0 0 1 1 0 0

2585: 0 0 0 1 0 0 0 1

2593: 0 1 0 0 1 1 1 0

2601: 1 0 1 0 0 0 0 1

2609: 6 6 9 19 18 12 5 0

2617: 0 2 0 1 0 1 0 1

262 5: 0 0 0 1 1 0 0 1

2633: 1 0 0 0 1 1 0 0

2641: 1 0 3 0 0 1 0 2

2649: 0 0 0 0 1 0 0 0

2657: 0 1 0 0 0 0 0 0

2665: 0 0 3 0 0 1 0 0

2 67 3: 0 0 0 2 0 0 0 0

2681: 0 0 0 2 0 1 0 0

2689: 0 0 0 0 1 0 0 0

2697: 0 0 0 0 0 0 0 0

2705: 0 0 1 0 0 0 0 0

2713: 0 0 0 0 0 0 0 0

2721: 0 0 1 0 0 0 0 1

2729: 0 1 0 1 1 0 0 0

2737: 0 2 2 0 0 2 0 0

2745: 0 0 0 0 0 1 0 0

2753: 0 0 0 0 1 1 0 0

27 61: 0 0 0 0 0 0 1 0

2769: 0 0 0 0 0 0 0 1

2777: 2 0 1 0 0 0 1 0

2785: 0 0 0 0 0 0 1 0

2793: 1 1 0 0 0 0 1 0

2801: 1 0 1 0 0 0 0 0

2809: 0 0 0 0 0 0 0 0

2817: 0 0 1 0 2 0 0 0

2825: 0 0 0 1 0 0 0 0

2833: 0 0 1 2 0 0 1 0

2841: 0 0 1 0 0 0 0 0

2849: 0 0 0 0 2 0 0 0

2857: 0 0 1 0 0 0 0 0

2865: 0 0 0 0 0 0 0 0

2873: 1 0 0 0 0 0 0 0

2881: 1 1 1 0 0 0 1 0

2889: 0 0 2 0 0 0 0 0

2897: 0 0 0 0 1 1 1 0

2905: 0 0 0 0 0 0 0 0

2913: 0 0 0 0 0 0 1 0

2921: 1 0 1 0 0 0 1 1

2929: 0 0 0 0 0 0 0 0

2937: 0 0 0 0 0 0 0 0

2945: 0 0 0 0 0 2 1 0

2953: 0 0 1 0 0 0 0 0

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0294

Channel Data Report 4/17/2018 7:45:09 AM Page 8

2961: 0 0 0 0 0 0 0 0

Sample Title: AC-SED-11

Channell------l-------1-------1-------1-------I-------I-------I-------I

2969: 2 0 0 0 1 1 0 1

2977: 0 0 0 0 0 0 0 0

2985: 0 1 0 0 0 0 0 0

2993: 0 0 0 0 0 0 1 0

3001: 1 0 0 0 0 0 0 0

3009: 0 0 0 1 0 0 0 0

3017: 0 0 0 0 0 0 0 0

3025: 0 0 0 0 2 0 0 0

3033: 0 0 0 0 0 3 0 0

3041: 0 0 1 0 0 0 0 0

3049: 0 0 0 0 0 1 1 0

3057: 0 0 0 0 0 0 0 0

3065: 0 0 0 0 0 0 0 0

3073: 1 1 0 0 0 0 0 0

3081: 0 0 0 1 0 0 0 0

3089: 0 0 0 1 0 1 0 0

3097: 0 0 0 0 1 0 0 0

3105: 0 0 0 0 0 1 0 0

3113: 0 0 0 0 1 0 0 1

3121: 0 0 0 0 0 0 0 0

3129: 0 0 0 0 0 0 0 0

3137: 0 0 0 0 0 0 0 1

3145: 0 0 0 0 0 0 0 0

3153: 0 0 0 0 0 0 0 0

3161: 0 0 0 0 0 0 0 0

3169: 0 0 0 0 0 0 0 0

3177: 1 1 0 0 0 0 0 0

3185: 2 0 0 1 0 0 0 0

3193: 0 0 1 0 1 0 0 0

3201: 0 0 0 0 0 0 0 1

3209: 1 0 0 0 0 0 1 0

3217: 0 0 0 1 1 0 0 0

3225: 0 0 0 1 1 0 1 0

3233: 0 0 0 1 0 0 0 1

3241: 0 0 0 0 0 0 0 0

3249: 0 0 0 0 0 0 0 0

3257: 0 0 0 1 0 0 0 0

3265: 0 0 1 1 1 0 0 0

3273: 0 0 0 1 0 0 0 0

3281: 0 0 0 2 0 0 0 0

3289: 0 0 0 0 0 0 0 1

3297: 0 0 0 0 0 0 0 1

3305: 0 1 0 2 0 0 0 0

3313: 0 1 0 0 0 0 0 0

3321: 0 0 0 1 0 0 0 0

3329: 0 0 0 0 0 1 0 0

3337: 0 0 1 0 0 0 0 0

3345: 0 0 0 1 0 0 0 1

3353: 0 0 0 0 0 0 0 0

3361: 0 0 0 0 0 0 0 0

3369: 0 0 0 0 1 0 0 0

3377: 0 0 0 0 0 0 0 0

3385: 0 0 1 0 0 0 0 2

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0295

Channel Data Report 4/17/2018 7:45:09 AM Page 9

3393: 0 0 1 0 0 0 0 0

Sample Title: AC-SED-11

Channell------l-------l-------l-------1-------1-------1-------I-------I

3401: 0 0 0 0 1 0 0 1

3409: 0 0 0 0 0 1 0 0

3417: 0 0 0 0 0 0 1 0

3425: 0 0 0 0 1 0 0 0

3433: 0 0 0 0 0 1 1 0

3441: 0 0 1 0 0 0 1 0

3449: 0 0 2 0 0 0 0 0

3457: 0 0 0 0 1 0 0 1

3465: 0 0 0 0 1 0 0 0

3473: 1 0 0 0 0 0 0 1

3481: 0 0 0 0 0 0 0 0

3489: 0 0 1 0 0 0 0 0

3497: 1 0 0 0 0 0 0 0

3505: 1 0 0 0 0 0 0 0

3513: 0 0 0 0 0 0 0 0

3521: 0 1 1 0 1 0 0 0

352 9: 0 0 0 1 0 0 0 0

3537: 0 0 0 0 0 0 0 0

3545: 0 0 0 1 0 0 1 0

3553: 0 0 0 0 0 0 0 0

3561: 0 0 0 0 0 0 0 0

3569: 0 0 0 0 1 0 0 0

3577: 1 0 0 0 0 0 0 1

3585: 0 0 0 0 0 0 0 0

3593: 0 0 0 0 1 0 0 0

3601: 0 0 1 0 0 1 0 0

3609: 0 0 0 0 0 1 0 0

3617: 0 1 0 0 0 0 0 1

3625: 0 0 0 1 0 0 1 0

3633: 1 0 0 0 0 0 0 0

3641: 0 0 0 0 0 0 0 0

3649: 0 1 0 0 0 0 0 0

3657: 0 1 0 0 0 0 0 0

3665: 0 0 0 0 0 0 0 0

3673: 0 0 0 0 0 1 0 1

3681: 0 0 0 0 1 1 0 0

368 9: 0 0 0 0 0 1 0 0

3697: 0 0 0 0 0 0 1 0

3705: 0 0 0 0 0 0 0 0

3713: 0 0 0 0 0 0 0 0

3721: 0 0 1 0 0 0 0 0

3729: 0 0 0 0 0 0 0 0

3737: 0 0 0 0 1 0 0 0

3745: 0 0 0 0 1 1 1 0

3753: 0 0 0 0 1 0 0 0

3761: 0 0 0 0 0 0 0 0

3769: 0 0 1 0 0 0 0 0

3777: 1 0 0 1 0 0 0 0

3785: 0 0 0 0 0 0 0 1

3793: 0 0 0 0 0 0 0 0

3801: 0 1 1 0 1 0 0 0

3809: 0 0 1 0 0 0 1 0

3817: 0 0 0 0 0 0 1 1

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0296

Channel Data Report 4/17/2018 7:45:09 AM Page 10

3825: 0 0 0 0 0 1 0 0

Sample Title: AC-SED-11

Channell------l-------1-------1-------1-------I-------I-------I-------I

3833: 0 0 0 0 0 0 0 0

3841: 0 0 0 0 0 1 0 0

3849: 0 0 0 0 0 0 0 0

3857: 0 0 0 0 0 0 2 0

3865: 0 0 1 0 0 0 0 0

3873: 0 0 0 0 0 0 0 0

3881: 0 0 0 0 0 0 1 0

3889: 0 1 0 0 0 0 0 0

3897: 0 0 1 0 0 1 0 1

3905: 0 0 1 0 0 0 1 0

3913: 0 0 0 0 0 0 0 0

3921: 0 0 0 0 0 1 0 0

3929: 0 0 0 0 0 0 1 0

3937: 0 0 0 0 0 0 0 0

3945: 1 0 1 0 0 0 1 0

3953: 0 0 0 0 0 0 0 0

3961: 0 0 0 0 0 0 1 1

3969: 1 0 0 0 1 0 1 1

3977: 0 0 0 0 0 0 0 0

3985: 0 0 0 0 1 1 0 0

3993: 0 0 0 0 0 0 0 0

4001: 0 1 0 0 0 1 0 0

4009: 0 0 0 1 0 0 0 0

4017: 0 0 0 0 0 0 1 0

4025: 0 0 0 0 0 1 0 0

4033: 0 0 0 0 0 0 0 0

4041: 0 0 0 0 0 0 0 0

4049: 0 0 0 1 0 0 0 0

4057: 0 1 0 0 1 1 0 1

4065: 0 1 0 0 0 1 0 0

4073: 0 0 0 0 0 0 0 0

4081: 0 0 0 0 0 0 0 1

4089: 0 0 0 0 0 0 0 0

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0297

105

104

~ 103 ro u V)

O'l 0

r--1

V) .µ s::: ~ 0 u

102

101

-= '3

';" EB a,

= ';" C, u -= ' o._

z

= _, ' z

V,

.._,_ = ~

~

.._,_

~ ~ ' "' ~ o._

lQO n ""

500

.._,_ _,

' ~ "'

co = ---' f-

co ~ ' Uco « ~

~

1000

~

.._,_ _,

' ~ "'

ROI Type: 1

!

1500

0000064641. CNF

.._,_

~

2000 channel

2500

co = ' ---' f-

Live Time :3600.000 sec Real Time :3600.830 sec Start: 1: 1. 2 (kev) stop : 4096: 4099. 2 (kev) Acq. Start :Tue Apr 17 06:44:34 2018

3000

!Im ROI Type: 2

3500 4000

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0298

Last Measurement Q.A. Report 4/17/18 5:24:37 AM Page 1

**************************************************************************

***** G E N I E Q U A L I T Y A S S U R A N C E *****

**************************************************************************

Last Results Report 4/17/18 5:24:37 AM

QA File:

Detector:

\\OR-GAMMAl\ApexRoot\Countroom\QA\D000000000lB.QCK

GEl Geometry: <None> Certificate: <None> Sample ID: Sample Desc: Sample Quantity: Sample Date: Measurement Date: Elapsed Live Time:

QA Background Ch QA Count

1.0000E+000 4/17/18 5:09:22 4/17/18 5:09:24

900.0 seconds Elapsed Real Time:

Parameter Description [Mean+/- Std. Dev.]

900.1 seconds

Value

AM AM

DAILY BKG CT RATE GEl 2.3622E+000

[SD: 2.2718E+000+/- 1.162]

Deviation/Flags <LU: SD: UD: BS>

7.7782E-002 < >

fq) lf/(l/18

Flags Key: LU Lower/Upper Bounds Test SD Sample Driven N-Sigma Test UD = User Driven N-Sigma Test BS Measurement Bias Test

(Ab (In (In (In

Above, Be= Below) Investigate, Ac Action) Investigate, Ac Action) Investigate, Ac Action)

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0299

Last Measurement Q.A. Report 4/17/18 5:24:46 AM Page 1

**************************************************************************

***** G E N I E Q U A L I T Y A S S U R A N C E *****

**************************************************************************

Last Results Report 4/17/18 5:24:46 AM

QA File:

Detector:

\\OR-GAMMAl\ApexRoot\Countroom\QA\D0000000002B.QCK

GE2 Geometry: <None> Certificate: <None> Sample ID: Sample Desc: Sample Quantity: Sample Date: Measurement Date: Elapsed Live Time:

QA Background Ch QA Count

l.0000E+000 4/17/18 5:09:28 4/17/18 5:09:31

900.0 seconds Elapsed Real Time:

Parameter Description [Mean+/- Std. Dev.]

900.1 seconds

Value

AM AM

Deviation/Flags < LU : SD: UD: BS>

DAILY BKG CT RATE GE2 l.8489E+000 2.9374E-002

[SD:-l.4680E+035+/-******] < >

Trend Test: The last 9 samples exhibit a bias trend.

KP cr(t,-/tB

Flags Key: LU SD UD BS

Lower/Upper Bounds Test Sample Driven N-Sigma Test User Driven N-Sigma Test Measurement Bias Test

(Ab (In = (In = (In =

Above, Be= Below) Investigate, Ac Action) Investigate, Ac Action) Investigate, Ac Action)

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0300

Last Measurement Q.A. Report 4/17/18 5:41:05 AM /l f:::, Page 1 l/ Ii 1/18

**************************************************************************

***** G E N I E Q O A L I T Y A S S O R A N C E *****

**************************************************************************

Last Results Report 4/17/18 5:41:05 AM

QA File:

Detector:

\\OR-GAMMA1\ApexRoot\Countroom\QA\D0000000001GAF-16C.QCK

GEl Geometry: Certificate: Sample ID: Sample Desc: Sample Quantity: Sample Date: Measurement Date:

<None> GAF-16

Elapsed Live Time:

QA Calibration C QA Count

1.0000E+000 10/1/16 12:00:00 4/17/18 5:25:30

900.0 seconds Elapsed Real Time: 919.7 seconds

Value

PM AM

Deviation/Flags Parameter Description [Mean+/- Std. Dev.] < LU : SD: UD: BS>

Peak centroid 59.54 kev 5.9999E+001 Boundary Limits: [ 5.800E+001, 6.l00E+00l] < > Trend Test: The last 9 samples exhibit a bias trend.

Peak centroid 661.65 kev 6.6181E+002 Boundary Limits: [ 6. 600E+002, 6. 630E+002] < > Trend Test: The last 9 samples exhibit a bias trend.

Peak centroid 1332.49 ke 1.3324E+003 Boundary Limits: [ 1.331E+003, 1.334E+003] < >

Peak centroid 1836.01 ke 1.8358E+003 Boundary Limits: [ 1.834E+003, 1.838E+003] < >

Peak FWHM Am-241 1.5083E+000 Boundary Limits: [ 5.000E-001, 3.000E+000] < > Trend Test: The last 9 samples exhibit a bias trend.

Peak FWHM Cs-137 l.8998E+000 Boundary Limits: 5.000E-001, 3.000E+000] < >

Peak FWHM Co-60 2.3028E+000 Boundary Limits: 5.000E-001, 3.000E+000] < >

Peak FWHM Y-88 2.7380E+000 Boundary Limits: 5.000E-001, 3.000E+000] < >

Decay corrected activity 1.5191E+004 Boundary Limits: [ 1.254E-002, 1.881E-002] < > Trend Test: The last 9 samples exhibit a bias trend.

Decay corrected activity 6.4156E+003

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0301

Last Measurement Q.A. Report 4/17/18 5:41:05 AM Page 2

Boundary Limits: [ 5.134E-003, 7.700E-003]

Decay corrected activity 1.0396E+004 Boundary Limits: [ 8.130E-003, 1.220E-002]

Parameter Description [Mean+/- Std. Dev.]

Value

Decay corrected activity 1.8411E+004 Boundary Limits: [ l.690E-002, 2.534E-002]

Flags Key: LU Lower/Upper Bounds Test (Ab SD Sample Driven N-Sigma Test (In UD = User Driven N-Sigma Test (In BS Measurement Bias Test (In

< >

< >

Deviation/Flags < LU : SD: UD : BS>

< >

Above, Be= Below) Investigate, Ac Action) Investigate, Ac= Action) Investigate, Ac= Action)

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0302

Last Measurement Q.A. Report 4/17/18 5:41:16 AM Page 1

**************************************************************************

***** G E N I E Q U A L I T Y A S S U R A N C E *****

**************************************************************************

Last Results Report 4/17/18 5:41:16 AM

t'P t.r/11/18

QA File:

Detector:

\\OR-GAMMAl\ApexRoot\Countroom\QA\D0000000002GAS-1601C.QC

GE2 Geometry: Certificate: Sample ID: Sample Desc: Sample Quantity: Sample Date: Measurement Date:

<None> GAS-1601

Elapsed Live Time:

QA Calibration C QA Count

1.0000E+000 10/1/16 12:00:00 4/17/18 5:25:38

900.0 seconds Elapsed Real Time: 918.3 seconds

Value

PM AM

Deviation/Flags Parameter Description [Mean+/- Std. Dev.] < LU : SD: UD: BS>

Peak centroid 59.54 kev 6.0000E+00l Boundary Limits: [ 5.800E+001, 6. l00E+00l] < Trend Test: The last 9 samples exhibit a bias trend.

Peak centroid 661.65 kev 6.6128E+002 Boundary Limits: [ 6.600E+002, 6.630E+002] < Trend Test: The last 9 samples exhibit a bias trend.

Peak centroid 1332.49 ke 1.3316E+003 Boundary Limits: [ 1.331E+003, 1.334E+003] < Trend Test: The last 9 samples exhibit a bias trend.

Peak centroid 1836.01 ke 1.8349E+003 Boundary Limits: [ 1.833E+003, 1.838E+003] < Trend Test: The last 9 samples exhibit a bias trend.

Peak FWHM Am-241 1.3606E+000 Boundary Limits: 5.000E-001, 3.000E+000] < Trend Test: The last 9 samples exhibit a bias trend.

Peak FWHM Cs-137 l.9175E+000 Boundary Limits: 5.000E-001, 3.000E+000] < Trend Test: The last 9 samples exhibit a bias trend.

Peak FWHM Co-60 2.3921E+000 Boundary Limits: 5.000E-001, 3.000E+000] < Trend Test: The last 9 samples exhibit a bias trend.

Peak FWHM Y-88 Boundary Limits:

2.4231E+000 5.000E-001, 3.000E+000]

Decay corrected activity 1.4734E+005

<

>

>

>

>

>

>

>

>

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0303

Last Measurement Q.A. Report 4/17/18 5:41:16 AM Page 2

Boundary Limits: [ l.190E-001, 1. 785E-001] < > Trend Test: The last 9 samples exhibit a bias trend.

Parameter Oescriptinn [Mean+/- Std. Dev.]

Vri l \JP

Decay corrected activity 6.7614E+004

Deviation/Flags < LU : SD: UD : BS>

Boundary Limits: [ 5.718E-002, 8.577E-002] < > Trend Test: The last 9 samples exhibit a bias trend.

Decay corrected activity 9.5589E+004 Boundary Limits: [ 7.706E-002, l.156E-001]

Decay corrected activity 2.1048E+005 Boundary Limits: [ l.602E-001, 2.403E-001]

Flags Key: LU= Lower/Upper Bounds Test SD= Sample Driven N-Sigma Test UD User Driven N-Sigma Test BS Measurement Bias Test

< >

< >

(Ab= Above, Be= Below) (In= Investigate, Ac Action) (In= Investigate, Ac Action) (In= Investigate, Ac Action)