Chapter Twelve Quality Control and Initial Analysis of Data.
Deep Sea Drilling Project Initial Reports Volume 33MINERAL NOTES Twelve
Transcript of Deep Sea Drilling Project Initial Reports Volume 33MINERAL NOTES Twelve
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17. X-RAY MINERALOGY DATA FROM THE CENTRAL PACIFIC,LEG 33 DEEP SEA DRILLING PROJECT1
H.E. Cook and I. Zemmels, University of California, Riverside, California
METHODS
Semiquantitative determinations of the mineral com-position of bulk samples, 2-20 µm, and
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H. E. COOK, I. ZEMMELS
TABLE 1Summary of X-Ray Mineralogy Samples, Sample Depths,Lithology, Age, and X-Ray Diffraction Results, Site 314
SampleDepth Below
Sea Floor(m)
0.0045 a
(M5a
Lithology
Brownzeolitic
clay
Age
Quat.?
Bulk SampleMajor Constituent
1 2 3
Clin. Magn. Goet.Phil. Mica Quar.Phil. Mica Quar.
2-20 µm FractionMajor Constituent
1 2 3
Clin. Magn. Goet.Phil. Mica Clin.Phil. Mica Quar.
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X-RAY MINERALOGY DATA
TABLE 3Summary of X-Ray Mineralogy Samples, Sample Depths,
Lithology, Age, and X-Ray Diffraction Results, Hole 315A
SampleDepth Below
Sea Floor(m)
76.682.9
124.9142.6148.9260.0372.1465.9513.5591.0703.6
731.3739.3741.4779.2779.6788.5797.1799.2808.6818.7826.9830.0836.8837.0
850.5856.0858.3875.9893.4
911.3932.7952.8952.9970.9990.0
Lithology
Unit 2:Variegated
nanno-foramand
nanno-radoozes
Unit 3:Claystone,
chert,and
limestone
Unit 4:Volcanic sand-stone and clay-stone interbed.With clayey
limestone
Unit 5:Red-brown
and blue-greenferr. claystonesinterbed. Withgraded volcanic
sands
Age
o
c c« ao o.SP§
?ö
a
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H. E. COOK, I. ZEMMELS
TABLE 4Summary of X-Ray Mineralogy Samples, Sample Depth,Lithology, Age, and X-Ray Diffraction Results, Site 316
SampleDepth Below
Sea Floor(m)
0.8
2.7155.3268.3
391.8448.6469.3486.5495.9515.4524.7533.6553.3562.9571.8573.6
583.1584.4587.4609.8610.5613.6630.6638.4641.8642.1667.1668.1686.7704.5705.7727.0744.8771.2830.3
Lithology
U n i t l : a
Unit 2:calc. and
siliceous oozesand chalk
Unit 3:Siliceous chalk,limestone, and
dolomite
Unit 4:Volcaniclastic
brecciaand gradedsandstone,chalk, andlimestone
Age
a
o 0
s «d>
1o
1ou
Io
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X-RAY MINERALOGY DATA
TABLE 5Summary of X-Ray Mineralogy Samples, Sample Depths,
Lithology, Age, and X-Ray Diffraction Results Hole 317A
SampleDepth Below
Sea Floor(m)
554.2564.5576.9585.0602.4623.3644.1
651.0670.0698.6727.7755.9756.7757.4759.4777.7778.1779.6821.1849.9887.4887.4
927.5
Lithology
Unit 2:Foram-nanno
oozes andchalk withblack chert
Unit 3:Volcaniclastic
sandstones andsiltstones
Basalts withsiltstones
Age
u
β S° 8If
u
so
Mp
£ o
Bulk SampleMajor Constituent
1
Calc.Calc.Calc.Paly.Calc.Cris.Calc.
Mont.Mont.Mont.Mont.Mont.Mont.Mont.Mont.Mont.Mont.Mont.Mont.Mont.Mont.Mont.
Plag.
2
Clin.Quar.Quar.K-Fe.Cris.Calc.Mont.
Plag.Anal.Sani.K-Fe.Hema.Sani.Sani.Anal.Sani.Sani.Sani.Anal.Anal.Anal.Anal.
Mont.
3
Mica
K-Fe.Quar.Quar.Trid.K-Fe.
Clin.
Anal.Plag.Quar.Anal.
Sani.Anal.Calc.Anal.Sani.Sani.
Hema.
2-20 µm FractionMajor Constituent
1
Clin.K-Fe.K-Fe.K-Fe.Cris.Cris.Clin.
Plag.Mont.Mont.K-Fe.Mont.Mont.Mont.Mont.Mont.Mont.Mont.Mont.Mont.Anal.Mont.
Plag.
2
Quar.Quar.Quar.MicaQuar.K-Fe.K-Fe.
Mont.Anal.Anal.Mont.Feld.Sani.Sani.Sani.Sani.Sani.Sani.Sani.Sani.Mont.Sani.
Quar.
3
K-Fe.MicaMicaQuar.Bari.Trid.Plag.
Quar.
Sani.Plag.Hema.Hema.Anal.
Anal.Anal.Anal.Anal.Anal.Sani.Anal.
Hema.
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H. E. COOK, I. ZEMMELS
TABLE 7Summary of X-Ray Mineralogy Samples, Sample Depths,Lithology, Age, and X-Ray Diffraction Results, Site 318
SampleDepth Below
Sea Floor(m)
1.393.7
122.5179.7
266.5350.8
407.5492.7
578.5581.1615.8630.7665.6703.8734.5
Lithology
Unit l:a
Unit 2:Foram-nanno
ooze
Unit 3:Foram-nanno
chalkUnit 4 :
Nanno-foramlimestoneUnit 5:
Limestone,siltstone,
and gradedsandstone
Age
a
•2 °
à, dD Oo o
O Q. .
• o O
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TABLE 9Results of X-Ray Diffraction Analysis, Hole 315
SampleDepth Below
Sea Floor(m)
Bulk Sample
1.303.90
57.9059.2061.9065.50
Amor.
20.424.747.626.826.919.0
2-20 µm Fraction
1.303.90
57.9059.2061.9065.50
87.686.789.886.783.891.6
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TABLE 10Results of X-Ray Diffraction Analysis, Hole 3ISA
Arag. Feld.a Quar. Cris. K-Fe. Plag. Kaol. Mica Chlo. Goet. Paly. Mont. Trid. Clin. Phil. Pyri. Hema. Gyps. Bari. Amph. Gibb. Magn.
SampleDepth Below
Sea Floor(m)
Bulk Samples
76.682.90
124.90142.60148.90260.00372.10465.90513.50591.00703.60731.30739.30741.40779.20779.60788.50797.10799.20808.60875.90893.40911.30932.70952.80952.90970.90990.00
Amor.
20.517.319.219.720.818.718.717.112.110.218.210.088.313.774.873.366.048.134.244.732.847.256.445.751.844.545.370.8
2-20 µm Fraction
82.90124.90142.60148.90260.00372.10465.90513.50591.00703.60731.30739.30741.40779.20779.60788.50797.10799.20808.60818.70826.90836.80837.00850.50856.00858.30875.90893.40
86.196.190.897.476.995.594.691.595.288.537.690.313.559.648.747.337.353.236.847.649.244.641.134.523.838.248.044.6
Calc. Dolo
100.099.7
100.099.499.2
100.098.6
100.0100.0100.0100.098.461.726.714.6_ __ __ _
88.376.677.250.417.1- __ _
93.6_ _-
8.0
15.2
0.3
0.20.2
0.1
0.23.9
48.123.625.926.628.84.68.78.9
36.848.2
0.675.8
19.953.9
7.95.72.48.42.16.14.4
5.91.01.96.9
35.628.625.126.725.140.828.623.636.525.69.7
1.153.269.5
22.3
12.1
56.7
15.5
8.75.03.87.20.61.21.21.66.4
43.9
2.94.1
19.610.4
_15.714.322.9
13.88.2
13.2
8.711.95.19.29.5
12.717.019.731.0
9.87.1
66.536.810.16.4
6.66.13.24.70.40.80.71.64.24.1
1.41.9
10.113.46.8
40.413.612.44.7
13.85.4
10.3
9.58.33.66.05.46.65.92.3
10.26.4
37.311.75.83.83.9
2.3
12.422.816.017.03.15.74.02.2
12.30.9
14.82.3
36.02.5
9.19.6
16.23.5
6.13.4
12.413.34.4
11.218.57.46.8
23.49.95.71.21.01.6
15.35.9
20.0
2.2
0.7
0.7
12.5
0.8
14.4
9.0
0.9
0.5
2.914.916.914.011.3
1.52.97.43.46.9
32.49.41.2
31.324.2
13.821.124.327.0
1.54.10.64.22.9
16.9_-0.4_
0.50.4
1.5
0.40.6
0.3
0.917.7
5.11.8
2.4
4.113.643.2
8.7
6.75.7
18.5_8.15.16.34.06.1_4.35.00.75.5
47.612.249.016.73.9
—--7.6_-__—__—__-____
7,57.5- -_ _
24.336.325.743.819.744.742.413.214.355.6
2.33.95.6— —9.4
1.91.2
2.9_
13.4
__-__
_____
—-
_0.1—
-_-_-_
-0.1__
—-
_-—
11.251.776.341.8
1.855.968.872.478.948.717.851.0
61.7
8.4
7.4 0.37.33.84.7
0.91.0
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911.30932.70952.80952.90970.90990.00
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TABLE 11Results of X-Ray Diffraction Analysis, Site 316
Sample DepthBelow SeaFloor (m) Amor. Calc. Dolo. Feld.a Quar. Cris. K-Fe. Plag. Kaol. Mica Chlo. Goet. Paly. Mont. Trid. Clin. Phil. Anal. Hema. Pyri. Gibb. Gyps. Bari. Augi. Magn. U-2b
Bulk Sample
0.802.70
155.30268.30391.80448.60469.30486.50495.90515.40524.70533.60553.30562.90571.80573.60583.10584.40587.40609.80610.50613.60630.60638.40641.80642.10667.10668.10686.70704.50705.70727.00744.80771.20830.30
31.815.820.821.629.820.555.222.5-7.311.510.013.129.020.321.4
8.720.674.610.624.852.1
9.016.013.420.435.316.418.87.7
25.944.338.944.738.715.5
2-20 µm Fraction
0.802.70
155.30268.30391.80448.60469.30486.50495.90515.40524.70533.60553.30562.90571.80573.60583.10584.40587.40609.80610.50613.60630.60638.40641.80
86.992.296.395.295.295.832.932.4
-19.866.157.640.149.649.950.045.838.743.644.645.439.643.742.235.634.7
97.699.8
100.094.599.1
100.083.4
97.4 0.534.698.1 0.399.898.996.298.596.398.878.416.395.281.752.097.191.396.080.566.298.295.598.078.577.6 0.158.473.141.895.1
0.3
0.3
0.40.2
0.20.2
0.80.35.31.70.20.71.60.81.01.2
19.236.1
3.215.10.32.22.32.70.10.80.70.71.40.69.30.91.02.51.5
22.327.913.310.313.116.013.49.3
14.730.530.340.241.233.632.438.073.046.857.643.8
1.758.127.039.8
3.3
47.1
80.0
5.3
3.5 1.1
1.3 0.9
0.8 0.5
5.4 5.2
7.47.8
6.22.0
20.013.112.7
2.2
5.713.54.6
17.831.928.014.8
7.6
14.415.713.723.124.619.69.2
12.912.814.9
2.615.0
7.616.044.3
4.84.2
1.81.66.22.90.7-
20.420.3
7.017.420.818.29.85.7
6.32.36.37.77.16.66.0
8.48.37.21.25.93.36.26.4
5.1
1.0
0.9
0.5
1.4
3.3
1.0
1.0
17.51.61.4
1.11.3
0.95.91.3
0.9
11.912.4
-
13.514.15.22.3
21.623.118.716.516.517.017.73.6
11.317.813.63.6
11.48.88.15.9
1.64.44.4
__
-
1.61.21.01.91.2
-0.9
__
1.51.0
_____
3.0
0.9
10.0
1.546.7
0.76.20.64.3
13.61.13.50.6
11.63.46.76.1
30.70.4
6.0
8.1
12.018.1-
I3.3-
__
-
_-1.0
2.51.40.9
2.12.14.0
0.61.32.4
81.0
44.21.14.2
0.7
5.61.8
11.9
5.4
2.49.3
0.41.0
0.20.40.42.2
0.5
1.42.8
42.064.9
0.5
23.419.90.7
13.36.2
8.221.011.6
0.6
0.7
1.7
0.4
0.71.8
0.2
0.49.6
1.23.4
0.4
4.9
1.3
0.5
2.3
0.9
0.1
0.1
1.10.9
0.7
15.3
9.5
0.10.80.20.30.8
0.2
5.2
6.117.3
31.120.044.554.515.714.114.810.2
11.08.0
13.80.8
14.117.623.3
4.0
3.50.91.4
7.9
3.7
6.0
PTR
aw
§
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642.10667.10668.10686.70704.50727.00744.80771.20830.30
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TABLE 12Results of X-Ray Diffraction Analysis, Hole 317A
Calc. Dolo. Quar. Cris. K-Fe. Plag. Kaol. Mica Chlo. Paly. Mont. Trid. Clin. Phil. Anal. Hema. Pyri. Gibb. Gyps. Apat. Bari. Amph. Magn. Sani.
SampleDepth Below
Sea Floor(m)
Bulk Sample
554.20564.50576.90585.00602.40623.30644.10651.00670.00698.60727.70755.90756.70757.40759.40777.70778.10779.60821.10849.90887.40887.40927.50
Amor.
41.27.4
52.556.9
7.1-6.228.744.213.252.548.352.758.251.062.843.058.848.549.144.825.139.447.9
2-20 µm Fraction
554.20564.50576.90585.00602.40623.30644.10651.00670.00698.60727.00755.90756.70757.40759.40777.70778.10c
779.60821.10849.90887.40887.40927.50
30.124.031.449.7
-12.9-33.421.249.1
3.045.663.759.164.666.662.064.858.062.458.556.635.260.939.1
Feld.a
_—_____-___
6.5__-________
Calc
82.997.878.2
-43.734.37,8.7
_—-___-__4.5_-1.40.4_
-
0.3
2.52.28.39.75.90.60.62.10.2
2.32.8
—___
42.255.5
__
-
_
1.5_7.3
10.8-0.94.8_
-
17.1_
0.8_--.-0.43.3
16.0-
11.1_
—__
___
0.6-
_
3.0_5.9----_
-
_
8.1
0.9 63.3
2.3
8.7 36.1 10.5
16.643.034.620.725.1
2.33.15.70.3
3.74.4
—_--
56.675.8
__
-
_
9.647.842.623.7
1.16.1
23.3_1.7-
46.2_
5.94.01.12.80.72.1
15.254.8
-
20.9_
9.05.2
20.021.0
—_
0.81.7 4.1
0.5
8.1
13.4
0.7
2.91.2
10.0 45.3
1.8 1.0
1.1
7.8
5.6
1.0
10.5
0.93.3
37.052.156.129.183.687.376.591.566.681.664.173.840.230.176.64.3
7.8
1.4—1.56.0
71.876.358.669.590.491.795.680.192.884.588.388.868.792.394.813.4
5.54.3----_---_---
—1.23.29.5------__-
-10.0
5.48.6
45.0 3.8
6.9
0.733.8
2.0
23.412.4
2.40.5
11.12.52.84.16.4
25.75.73.8
0.8
1.5
0.1
0.4_
0.2__
—6.0__
0.3
—_2.00.51.5
—__0.71.5
4.60.6
29.1
5.23.88.94.78.37.64.84.21.5
1.413.2
8.3
0.98.6—
0.71.6
11.11.59.5
—1.3
10.2
10.3
45.922.9
I3.7
7.63.04.86.9
17.454.3
8.7_
—-
5.55.5-
_-----0.6
10.6
0.7
0.4
0.9
20.9
7.119.38.5
25.87.3
30.316.537.914.513.0
O
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TABLE 13Results of X-Ray Diffraction Analysis, Hole 317B
Dolo. Arag. Feld. Cris. K-Fe. Plag. Kaol. Mica Chlo. Mont. Trid. Clin. Gibb. Quar. Gyps. Apat. Bari. Psü.a Magn.
SampleDepth Below
Sea Floor(m)
Bulk Sample
0.3027.4065.70
102.20141.20179.50220.70227.10266.80312.40352.30389.40
Amor.
23.421.126.520.317.323.735.721.829.529.517.428.9
2-20 µm Fraction
0.3027.4065.70
102.20141.20179.50220.70227.10266.80352.30389.40
31.010.532.580.889.491.9
_94.8
2.632.341.8
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TABLE 14Results of X-Ray Diffraction Analysis, Site 318
SampleDepth Below
Sea Floor(m)
Bulk Sample1.30
93.70122.50179.80266.50350.80407.50492.70578.50581.10615.80630.70665.60703.80743.50
Amor.
39.427.031.025.230.330.825.029.727.234.710.245.769.458.341.2
2-20 µm Fraction
1.30179.80266.50350.80407.50492.70578.50581.10615.80630.70665.60703.80743.50
48.791.394.795.150.156.756.933.738.172.943.446.437.1
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H. E. COOK, I. ZEMMELS
TABLE 15Samples Used in X-Ray Diffraction
Analysis, Leg 33 (Compositedsamples are bracketed)
TABLE 15 - Continued
Sample(Interval in cm)
Site 314
3,CCXX
Hole 315
1-1, 130-1321-1, 135-1371-2, 20-221-2, 88-901-3, 85-874-1,143-1454-2,121-1234-2,135-1374-3, 56-584-3, 85-8744, 87-894-4, 116-1184-5, 7-94-5,130-1324-6, 148-150
Hole 315 A
1-1,108-1101-5,90-921-5,95-971-6,136-1381-6,142-1442-1, 140-1422-1,145-1473-1,40423-1,68-703-3, 70-723-3, 74-763-5, 70-723-5,138-1404-3,103-1054-3,117-1195-2, 59-615-2,144-1466-1,87-896-1,92-946-2,128-1306-2,140-1427-1,94-967-1,100-1027-2, 69-717-2, 98-1008-2, 97-998-2,101-1039-1, 108-1109-1,120-12210-1,52-5410-1,70-7210-1,115-11710-6, 100-10210-6,102-10411-1,134-13611-1,146-15015-1,114-11615-2, 82-8416-1, 101-10317-1,7-9
Depth BelowSea Floor (m)
0 4 50 4 5
1.3'1.41.72.43.9
57.959.259.460.160.461.9'62.262.663.865.5
76.682.983.084.984.9,
124.9125.0142.6'142.9145.9146.0148.9'149.6.260.0260.2372.1373.0465.9'465.9467.8467.9513.5"513.5514.7515.0,591.0'591.0 J703.6'703.7731.3 ^731.4732.0
•
739.3739.3741.4 1741.5 J779.2779.6788.5797.1
Sample(Interval in cm)
19-2,118-12019-3,52-5320-1,143-14420-2, 96-97204, 0-15021-2, 32-3421-2, 32-3421-2,4647224,145-14623-2,49-5123-3,130-13124-2, 136-13725-1,138-13925-2, 72-7425-3,48-5026-1,26-2826-1,130-13227-2,119-12028-3, 75-7728-3, 85-8729-2, 136-13830-2,148-150
Site 316
1-1,83-851-1,85-881-2,116-1181-2,118-1202-2, 80-82.52-2, 82.5-853-1,126-1283-2, 72-744-1,124-1284-1, 128-1315-1,110-1155-2, 101-1047-2,133-1359-1,100-10210-1,91-9311-1,135-13812-1,123-12612-2,15-1713-1,56-5915-1,101-10316-1,137-14017-1,77-8017-2, 104-10618-2,109-11118-3, 96-9918-5, 84-8619-1,83-8519-1,146-150194, 10-1420-2,112-11421-1,92-9621-3, 25-2921-3,126-128214,8-1123-1,104-10723-1,54-5624-2, 20-2324-3, 63-6625-1,454725-2, 20-2226-3, 95-9727-2,141-14628-1,64-66
Depth BelowSea Floor (m)
818.71819.5 J826.91828.0]830.0836.81836.8]837.0850.5856.0858.3875.9893.4]894.2 \895.5 J911.31912.3J932.7952.8952.9970.9990.0
0.80.92.72.7
155.3155.3268.31269.2J391.81393.3J448.6\450.0J469.3486.5495.9515.4524.71525.2]533.6553.3562.9571.8573.6583.1584.4587.4609.8610.5613.6630.6638.41640.8]641.8642.1667.1668.1686.7*1688.6]704.5705.7727.0744.8771.2
554
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X-RAY MINERALOGY DATA
TABLE 15 - Continued TABLE 15 - Continued
Sample(Interval in cm)
30-2, 132-134
Hole 317A
2-1,22-242-1,41-433-1,103-1053-1,128-1303-2, 25-273-2, 28-305-1,93-956-2, 103-1058-1,90-9210-2,128-13010-2,130-13212-4, 5-713-2,49-5115-2, 53-55154,102-10418-2,60-6218-2, 72-7420-3, 50-5222-2, 84-8622-3,18-2022-3, 86-88224,139-141244, 70-72244,107-10924-5,113-11526-1,107-10926-2, 25-2728-1,134-13830-1,88-9233-3, 0 4
Hole 317B
1-1,20-221-1,22-241-1,101-1021-2,102-1041-2, 29-311-6, 100-1021-6, 102-1044-2, 40424-2, 43454-3, 82-844-3, 85-878-2, 70-728-2, 73-7584, 60-6284, 63-6512-1,70-7212-1,73-7512-3,404212-3,434512-5, 60-6212-5,63-6516-1,134-13616-1,136-13816-2, 60-6216-2, 62-64164,100-102164,103-10516-6, 60-6216-6, 62-6420-2,53-5520-2, 98-100204, 58-60204, 60-6220-6, 78-8020-6,81-83
Depth BelowSea Floor (m)
830.3
554.2'554.4564.5'564.8565.3565.3576.9585.0602.4623.3)623.3 J644.1651.0670.0 1673.5 J698.6 \698.7 J727.0755.9756.7757.4759.4777.7778.1779.6821.1821.8849.9887.4927.5
0.3'0.31.11.11.98.68.6.
27.4'27.429.329.465.765.768.668.6
102.2'102.2104.9104.9108.1108.1 ,141.2'141.2141.9141.9145.3145.3147.9147.9.179.5'180.0182.6182.6185.8185.8.
Sample(Interval in cm)
244, 70-9025-2, 54-5625-2, 56-58254, 3840254,52-5425-6, 30-3225-6,48-5029-3, 80-8229-3, 82-8429-5,5-729-5,13-1534-2,404234-2, 434534-5, 76-7834-5, 86-8838-3,79-8138-3, 82-84384, 90-92384, 93-9542-2,140-142
Site 318
1-1,129-1321-2, 82-851-3,65-701-3, 72-7814,65-7214, 72-761-5,94-1034-1,41434-1,45474-2, 71-734-2, 74-764-3, 72-744-3, 74-7644 , 70-7244, 74 764-5,52-544-5, 56-584-6, 79-824-6, 83-825-1,75-785-1,78-807-1,75-777-1,78-807-2, 75-777-2, 80-827-3,120-1227-3, 123-12574, 70-7274, 72-7410-2,100-10210-2,106-10810-3,70-7210-3, 72-7513-1,124-12713-2, 33-3515-1,95-9815-2,126-12918-1,71-7318-2,137-13921-1,94-9721-2,18-2021-3,62-6424-1,25-29254,120-12228-2,106-11030-2, 128-132324, 0-3
Depth BelowSea Floor (m)
220.7227.l'227.1229.9230.0232.8233.0266.8266.8269.1269.1312.4312.4317.3317.4352.3352.3353.9353.9'389.4
1.32.33.73.75.25.27.0
93.7'93.895.595.697.097.198.598.699.899.9
101.6101.6.122.5123.9 .179.8'179.8181.3181.3183.2183.2184.2184.2,266.5266.6267.7267.7350.8 '351.3407.5 '409.3 .492.7494.9578.5 '579.2581.1615.8630.7665.6703.8743.5
555