Post on 09-Sep-2020
SYLLABUS
For
Swami Vivekanand University, Sironja Sagar2015-2016
SWAMI VIVEKANAND UNIVERSITY, SIRONJA,SAGAR (M.P.)
L T P CTheory
(I)MST(II)
Total(I)+(II)
Practical (III)
TW(IV)
Total(III)+(IV
)
1 PC-801 Total Quality Management 3 1 4 80 20 100 - - - 100
2 PC-802 Safety and Risk Management 3 1 2 6 80 20 100 100 100 200
3 PC-803 E2 Elective -II 3 1 2 6 80 20 100 100 100 200
4 PC-804 Major Project Work 3 1 2 6 200 200 400 400Total 12 4 8 24 240 60 300 200 400 600 900
B.Tech. PetroChemical Engineering Sem. - VIII Scheme of Examination
GrandTotal
(I+II+III+IV)
Sno.Coursecode
Subject
Periods Per week Distribution of Marks
B.TECH. PETROCHEMICAL ENGINEERING
SEMSTER-VIII
THEORY PAPER:
1 Total Quality Management
2 Safety and Risk Management
3 E2 Elective -II
PRACTICAL:
4 Project Work
PC-801 TOTAL QUALITY MANAGEMENT
UNIT I: INTRODUCTION
Introduction - Need for quality - Evolution of quality - Definitionof quality - Basic concepts of TQM - Definition of TQM – TQMFramework - Contributions of Deming,
UNIT II: TQM PRINCIPLES
Leadership – Strategic quality planning, Quality statements -Customer focus – Customer orientation, Customer satisfaction,Customer complaints, Customer retention - Employee involvem ent– Motivation, Empowerment, Team and Teamwork, Recognitionand Reward, Supplier partnership – Partnering, Supplier selection,Supplier Rating.
UNIT III: TQM TOOLS & TECHNIQUES
The seven traditional tools of quality – New management tools –Six-sigma: Concepts, methodology, applications to manufacturing,service sector including IT – Bench marking – Reason to benchmark, Bench marking process – FMEA – Stages, Types.
UNIT IV: TQM TOOLS & TECHNIQUES II
Quality circles – Quality Function Deployment (QFD) – Taguchiquality loss function – TPM – Concepts, improvement needs – Costof Quality – Performance measures.
UNIT V: QUALITY SYSTEMS
Need for ISO 9000- ISO 9000-2000 Quality System – Elements,Documentation, Quality auditingQS 9000 – ISO 14000 – Concepts,Requirements and Benefits – Case studies of TQM
TEXT BOOK:
1. Dale H.Besterfiled, et at., “Total Quality Management”, PearsonEducation Asia, Third Edition, Indian Reprint (2006).
REFERENCES:
1. James R. Evans and William M. Lindsay, “The Management andControl of Quality”, 6thEdition, South- Western (Thomson Learning),2005.
2. Oakland, J.S. “TQM – Text with Cases”, Butterworth – HeinemannLtd., Oxford, 3rd Edition, 2003.
3. Suganthi,L and Anand Samuel, “Total Quality Management”,Prentice Hall (India) Pvt. Ltd.,2006.
4. Janakiraman,B and Gopal, R.K, “Total Quality Management – Textand Cases”, Prentice Hall (India) Pvt. Ltd., 2006.
PC-802 SAFETY AND RISK MANAGEMENT
UNIT I: RISK MANAGEMENT
Overall risk analysis – Chapains model, E and FI model– Methods fordetermining consequences effects: Effect of fire, Effect of explosionand toxic effect – Disaster management plan – Emergencyplanning – Onsite and offsite emergency planning – Riskmanagement.
UNIT II: HAZARD IDENTIFICATION AND CONTROL
HAZOP, job safety analysis – Fault tree analysis – Event tree analysis– Failure modes and effect analysis and relative ranking techniques –Safety audit – Plant inspection – Past accident analysis.
UNIT III: INDUSTRIAL SAFETY
Concepts of safety – Hazard classification chemical, physical,mechanical, ergonomics, biological and noise hazards – Hazards fromutilities like air, water, steam.
UNIT IV: SAFETY IN HANDLING AND STORAGE OF CHEMICALS
Safety measures in handling and storage of chemicals – Firechemistry and its control –Personnel protection – Safety color codesof chemicals.
UNIT V: SAFETY PROCEDURES
Safety in plant design and layout – Safety provisions in the factory act1948 – Indian explosive act 1884 – ESI act 1948 – Advantages ofadopting safety laws.
TEXT BOOKS:
1. Blake, R.P., “Industrial Safety”, Prentice Hall, 1953.
2. Lees, F.P., “Loss Prevention in Process Industries”, 2nd Edition,Butterworth Heinemann, 1996.
REFERENCES:
1. Geoff Wells, “Hazard Identification and Risk Assessment”, I.ChE.
2. John Ridley and John Channing, “Safety at Work”, 6thEdition.Butterworth-Heinemann, 2003.
ELECTIVE II
PC-803(A) ENERGY MANAGEMENT IN CHEMICAL INDUSTRIES
UNIT I: ENERGY RESOURCES
Energy sources – Coal oil, natural gas – Nuclear energy – Hydroelectricity – Other fossil fuels – Geothermal – Supply and demand –Depletion of resources of resources – conservation Technology
UNIT II: ENERGY AND ENVIRONMENT
Energy – Various forms – Energy storage – Structural properties ofenvironment – Bio-geo – chemical cycles – Society and environmentpopulation and technology.
UNIT III: ENERGY ALTERNATIVES
Sources of continuous power – Wind and water – Geothermal – Tidaland solar power – MHD, fuel cells – Hydrogen as fuel
UNIT IV: MANAGEMENT OF ENERGY CONSERVATION
Chemical industries – Classification – Conservation in unitoperation such as separation –Cooling tower – Drying –Conservationapplied to refineries, petrochemical, fertilizers, cement, pulp andpaper, food industries.
UNIT V: ECONOMIC BALANCE IN ENERGY CONSUMPTION
Cost analysis – Capacity – Production rate – System rate – System costanalysis – Corporate models – Production analysis and productionusing fuel inventories – Input-output analysis –Economics – Tariffs.
TEXT BOOKS:
1. Krentz, J. H., “Energy Conservation and Utilisation”, Allyn and BacurInc., 1976.
2. Gramlay, G. M., “Energy”, Macmillon Publishing Co., 1975.
REFERENCES:
1. Rused C.K., “Elements of Energy Conservation”, McGraw – Hill BookCo., 1985.
2. Judson King; “Separation Processes”, McGraw – Hill Book Co., 1985.
3. Samir Sarkar, “Fuels and Combustion”, 2nd Edition, Orient LongmanPublication, 1988.
PC-803(B) NOVEL SEPARATION PROCESS
UNIT I: MEMBRANE SEPARATIONS
Types and choice of membranes – Plate and frame membranes, tubularmembranes, spiral wound membranes, hollow fibre membrane andtheir relative merits, membrane reactors, membrane permeatorsinvolving Dialysis – Reverse osmosis – Ultrafiltration –
UNIT II: CHROMATOGRAPHY TECHNIQUES
Affinity chromatography, immuno chromatography and Ion exchangechromatography –Introduction – Principles – Types of equipment –Commercial processes – Applications.
UNIT III: SEPARATIONS BY ADSORPTION TECHNIQUES 9
Types of adsorption – Nature of adsorbents – Adsorption equilibria– Adsorption hysterisis adsorption isotherms – Effect oftemperature and pressure – Freundlich equation – Stagewise
adsorption – Single and multistage crosscurrent adsorption – Breakthrough curves and rates of adsorption.
UNIT IV: IONIC SEPARATIONS
Electrophoresis – Introduction – Electrokinetics – The electrical doublelayer – Zeta potential and electrophoresis – Laboratory methods –Analytical and Preparative methods – Applications.
UNIT V: ZONE MELTING
Zone melting – Introduction – Equilibrium Diagram – Apparatus andApplications – Large scale and continuous operations – Limitations.
TEXT BOOKS:
1. Schoen, H.M., “New Chemical Engineering Separation Techniques”,Interscience Publishers, 1972.
2. Treybal, R.E., “Mass Transfer Operations”, 3rd Edition, McGraw HillBook Co., 1980.
REFERENCES:
1. Geankoplis, C.J. “Transport Processes and Unit Operations”, 3rdEdition, Prentice Hall of India Pvt. Ltd, 2000.
2. Sivasankar, B., “Bioseparations Principles and Techniques”, PrenticeHall India Pvt. Ltd, 2006.
3. Seader, J.D. and Henley, E.J., “Separation Process Principles”, 2ndEdition, John Wiley and Sons,Inc, 2006.
PC-803(C) MULTICOMPONENT DISTILLATION
UNIT I: THERMODYNAMIC PRINCIPLES
General considerations in the design of columns – Column sequencing –Heuristics for column sequencing – Key components – Distributedcomponents – Non-Distributed components – Adjacent keys.
Estimation of the fugacity coefficients for the vapor phase of polargas mixtures.
UNIT II: THERMODYNAMIC PROPERTY EVALUATION
Fundamental principles involved in the separation of multi componentmixtures – Determination of bubble-point and Dew PointTemperatures for multi component mixtures – equilibrium flash
distillation calculations for multi component mixtures – separation ofmulti component mixtures at total reflux.
UNIT III: VARIOUS METHODS OF MCD COLUMN DESIGN
Theta method of convergence – Kb method and the constantcomposition method – Application of the Theta method to complexcolumns and to system of columns – Lewis Matheson method –
UNIT IV: VARIOUS TYPES OF MCD COLUMNS
Design of sieve, bubble cap, valve trays and structured packingcolumns for multi component distillation – computation of plateefficiencies.
UNIT V: MINIMUM REFLUX RATIO FOR MCD SYSTEM
Definition of minimum reflux ratio – calculation of Rm for multicomponent distillation – Underwood
method – Colburn method.
TOTAL: 60 PERIODS
TEXT BOOKS:
1. Holland, C.D., “Fundamentals of Multi Component Distillation”,McGraw Hill Book Company,1981
2. Van Winkle, “Distillation Operations”, McGraw Hill Publications,1987.
REFERENCES:
1. King, C.J., “Separation Process Principles”, Mc Graw Publications,1986.
2. Treybal, R.E., “Mass Ttransfer Operations”, 5th Edition, Mc Graw Hillpublications. 1996.
3. Mc Cabe and Smith, J.C., Harriot, “Unit Operation of ChemicalEngineering”, 6th Edition,
McGraw Hill, 2001.
PC-803(D) POLYMER TECHNOLOGY
UNIT I: CHARACTERISTICS OF POLYMERS
The science of large molecules – Theory of polymer solutions –Measurement of molecular weight and size – Analysis and testing ofpolymers.
UNIT II: STRUCTURE AND PROPERTIES OF POLYMER MATERIAL
Deformation, flow and melt characteristics – Morphology and order incrystalline polymers – Rheology and the mechanical properties ofpolymers – Polymer structure and physical properties.
UNIT III: POLYMER SYNTHESIS
Condensation polymerization – Addition polymerization – Ionic andcoordination polymerization – Copolymerisation – Polymerizationconditions and polymer reactions.
UNIT IV: INDUSTRIAL POLYMERS
Hydrocarbon plastics and elastomers – Other carbon chainpolymers – Heterochain thermoplastics, thermosetting resins
UNIT V: PROCESSING OF POLYMERS
Polymers developed for synthetic plastics, fibres and elastomerapplications – Plastics technology Fiber technology – Elastomertechnology.
PC-804 PROJECT WORK
The project may be considered as the ultimate exercise presentedto the final semester student before graduation to measureaccumulated engineering knowledge and experience. At the same
time, the project itself should provide the students with some newskills, innovation and information, and strengthen the acquired ones.
The project programme consists of different assignment, allotted time,submission of report under internal faculty guidance and evaluation byexternal member along with internal faculty. The activities performedduring a project may cover one or more of the following;
Data collection Critical literature review Laboratory experienceand tests Mathematical modeling Software application Industrialvisits Design and/or assembly Process analysis The major project maybe assigned to a group of two students. The project topic allotted maybe of theoretical, experimental or industrial projects to be carried outunder the supervision of internalguide and external guide (in case ofindustrial projects).
Major projects are to be executed strictly as per the project scheduleprepared during VIII semester.
A committee of departmental faculty members comprising the projectguide, one more faculty member and the head of department willmonitor and review the progress achieved by the student at various
stages. The internal assessment will be done by the committee basedon the progress achieved on completion of the project work.
On completion of the project work, each student has to prepare aproject report and submit the same in triplicate to the department.The project work and the report will be evaluated by the internal
assessment committee for a total of 100 marks. The external universityexamination, which carries a total of 100 marks, will have reportevaluation and viva voce examination conducted by a committee of
one external examiner and one internal examiner appointed by theuniversity.