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SFUND RECORDS CTR
0222-00455
SFUND RECORDS CTR
88015017
Ouly 29, 1991
AR0759
I I
SUPPLEMENTAL DATA SUBMITTAL FOR SOIL BORINGS
FOR HAZARDOUS WASTE AREA HASSAYAMPA LANDFILL
MARICOPA COUNTY, ARIZONA
I I I
I I I I I I I
ERROL L. MONTGOMERY & ASSOCIATES, INC. CONSULTANTS IN HYDROGEOIOGY
1075 EAST FORT LOWELL ROAD, SUITE B TUCSON, ARIZONA 85719 (602)881.4912 TELEX: 165597 MONTE TUC
CRA Consulting Engineers
CONESTOGA-ROVERS & ASSOCIATES 382 WEST COUNTY ROAD D
ST. PAUL, MINNESOTA 55112
TELEPHONE (6)2)639-0913
ERROL L. MONTGOMERY & ASSOCIATES, INC. CONSULTANTS IN HYDROGEOLOGY
1075 EAST FORT LOWELL ROAD. SUITE B
TUCSON, ARIZONA 85719 (602)881-4912
TELEX: 165597 MONTE TUC
FAX: (602)8811609
ERROL L. MONrGOMERY J W. HARSHBARGER. P.G
OONAID K GREEN WILIIA.M R. VICTOR
EDWARD W. PEACOCK, RONAID H. DEWI7T,
MARK .'/ CROSS, DENNISG. HALL
ANDREW A. MESSER IODD KEAY,
JAMESS. DAVIS, MICHAEL J. ROSKO, LAURA J. SIRAUSS,
. P G .
.. PE. P.E.
. PG. ,P.G. . PG.
I, P.G. .P.G. . PG , P.G
i, P.G. . P.G. . P.O.
July 29, 1991
Thomas J. Dunkelman (H-7-2) Remedial Project Manager U. S. ENVIRONMENTAL PROTECTION AGENCY 75 Hawthorne Street San Francisco, California 94105
RE: SUPPLEMENTAL DATA SUBMITTAL FOR SOIL BORINGS
Dear Mr. Dunkelman:
In accordance with Section XII.A of the Administrative Consent Order dated February 19, 1988, for the Hassayampa Landfill Remedial Investigation / Feasibility Study (RI/FS), this data submittal has been prepared for final laboratory chemical data obtained or received during July 1991 for the recent soil boring program at Pits 1, 3b, and 3c.
Preliminary laboratory chemical data for soil borings SB-17, SB-18, and SB-19 were intended to be included in the data submittal for May 1991, which was dated June 28. However, chemical laboratory reports received in late June contained data that were substantially different from the preliminary data and, due to timing, these new data could not be included in the data submittal for May. Chemical laboratory reports for these soil borings were finalized in July and are not due for submittal to the U.S. Environmental Protection Agency (EPA) until the end of August. However, this supplemental data submittal was prepared to provide the data in advance to accommodate requests by EPA. Data given in this data submittal that were not given in previous data submittals include:
• results of laboratory chemical analyses for samples of soil and residual waste obtained from soil borings SB-17, SB-18, and SB-19; and
• field notes specifically requested by EPA for sampling operations at soil borings SB-17, SB-18, and SB-19.
In addition, EPA requested that photographs taken during the soil boring sampling operations be provided. These photographs are included under separate cover solely to EPA in a letter dated July 30, 1991.
ERROL L. MONTGOMERY & ASSOCIATES, INC.
In accordance with the distribution procedures for this project, two additional copies of this data submittal are enclosed herewith. If you have questions or require further discussion, please contact us.
Very truly yours,
ERROL L. MONTGOMERY & ASSOCIATES, INC.
^MiMuky^ /?. U L C ^ ^ 6y ( j ^ ) William R. Vic tor
SENT VIA FEDERAL EXPRESS Enclosures cc: Jackie Maye (3)
Grant J. Gibson (3) James G. Derouin (2) David Machlowitz (2) David P. Kimball (2) Kim E. Williamson (2) Charles A. Bischoff (1) Errol L. Montgomery (1) Terry A. Thompson (1)
Lt. Col. Ray Swensen (1) William J. Cheeseman (1) Roger K. Ferland (1) Robert W. Hacker (1) Alan Abbott (1) G. Van Velsor Wolf (1) Richard C. Keiffer (1) Robert H. Brauer (1) E. Powell / C. Case (1)
Carl C. Meier (1) Charles 0. Geadelmann (1 G. S. Hagy (1) Cindy Lewis (1) G. Eugene Neil (1) Stephen M. Quigley (1) Rod Whitten (1) Louis C. Thanukos (1)
July 29, 1991
SUPPLEMENTAL DATA SUBMITTAL FOR SOIL BORINGS
FOR HAZARDOUS WASTE AREA HASSAYAMPA LANDFILL
MARICOPA COUNTY, ARIZONA
CONTENTS
Page
INTRODUCTION 1
DATA FOR SOIL BORING PROGRAM 3 SOIL BORING SB-17 AT PIT 3c 3 SOIL BORING SB-18 AT PIT 3b 3 SOIL BORING SB-19 AT PIT 1 4 RESULTS OF LABORATORY CHEMICAL ANALYSES 4 DATA VALIDATION FOR LABORATORY CHEMICAL RESULTS 5
EPA Method 8240 for Samples of Soil 5 EPA Method 8240 for Samples of Residual Waste 6 EPA Method 8270 for Samples of Soil 7 EPA Method 8270 for Samples of Residual Waste 7 EPA Method 8080 for Samples of Soil 8 EPA Method 8080 for Samples of Residual Waste 8
Table
TABLES
SUMMARY OF LABORATORY CHEMICAL RESULTS FOR TOXICITY CHARACTERISTIC LEACHING PROCEDURE (TCLP) FOR METALS IN SAMPLES OF SOIL AND RESIDUAL WASTE FROM SOIL BORINGS, HASSAYAMPA LANDFILL, MARICOPA COUNTY, ARIZONA
SUMMARY OF LABORATORY CHEMICAL RESULTS FOR EPA METHOD 8240 FOR VOLATILE ORGANIC COMPOUNDS IN SAMPLES OF SOIL FROM SOIL BORINGS, HASSAYAMPA LANDFILL, MARICOPA COUNTY, ARIZONA
SUMMARY OF LABORATORY CHEMICAL RESULTS FOR TOXICITY CHARACTERISTIC LEACHING PROCEDURE (TCLP) FOR VOLATILE ORGANIC COMPOUNDS IN SAMPLES OF RESIDUAL WASTE FROM SOIL BORINGS, HASSAYAMPA LANDFILL, MARICOPA COUNTY, ARIZONA
SUMMARY OF LABORATORY CHEMICAL RESULTS FOR EPA METHOD 8270 FOR SEMI-VOLATILE ORGANIC COMPOUNDS IN SAMPLES OF SOIL FROM SOIL BORINGS, HASSAYAMPA LANDFILL, MARICOPA COUNTY, ARIZONA
SUMMARY OF LABORATORY CHEMICAL RESULTS FOR TOXICITY CHARACTERISTIC LEACHING PROCEDURE (TCLP) FOR SEMI-VOLATILE ORGANIC COMPOUNDS IN SAMPLES OF RESIDUAL WASTE FROM SOIL BORINGS, HASSAYAMPA LANDFILL, MARICOPA COUNTY, ARIZONA
TABLES - continued
SUMMARY OF LABORATORY CHEMICAL RESULTS FOR TOXICITY CHARACTERISTIC LEACHING PROCEDURE (TCLP) FOR ORGANOCHLORINE PESTICIDES AND POLYCHLORINATED BIPHENYLS (PCBs) IN SAMPLES OF RESIDUAL WASTE FROM SOIL BORINGS, HASSAYAMPA LANDFILL, MARICOPA COUNTY, ARIZONA
SUMMARY OF LABORATORY CHEMICAL RESULTS FOR EPA METHOD 8080 FOR ORGANOCHLORINE PESTICIDES AND POLYCHLORINATED BIPHENYLS (PCBs) IN SOIL SAMPLES FROM SOIL BORINGS, HASSAYAMPA LANDFILL, MARICOPA COUNTY, ARIZONA
SUMMARY OF LABORATORY CHEMICAL RESULTS FOR ADDITIONAL ANALYSES OF SAMPLES OF RESIDUAL WASTE FROM SOIL BORINGS, HASSAYAMPA LANDFILL, MARICOPA COUNTY, ARIZONA
APPENDICES
Appendix
A LABORATORY CHEMICAL RESULTS
B FIELD NOTES FOR SOIL BORINGS
July 29, 1991
SUPPLEMENTAL DATA SUBMITTAL FOR SOIL BORINGS
FOR HAZARDOUS WASTE AREA HASSAYAMPA LANDFILL
MARICOPA COUNTY, ARIZONA
INTRODUCTION
In accordance with Section XII.A of the Administrative Consent Order
dated February 19, 1988, for the Hassayampa Landfill Remedial Investigation
/ Feasibility Study (RI/FS), this data submittal has been prepared for final
laboratory chemical data obtained or received during July 1991 for the recent
soil boring program at Pits 1, 3b, and 3c.
Preliminary laboratory chemical data for soil borings SB-17, SB-18, and
SB-19 were intended to be included in the data submittal for May 1991, which
was dated June 28. However, chemical laboratory reports received in late
June contained data that were substantially different from the preliminary
data and, due to timing, these new data could not be included in the data
submittal for May. Chemical laboratory reports for these soil borings were
finalized in July and are not be due for submittal to the U.S. Environmental
Protection Agency (EPA) until the end of August. However, this supplemental
data submittal was prepared to provide the data in advance to accommodate
requests by EPA. Data given in this data submittal that were not given in
previous data submittals include:
Results of laboratory chemical analyses for samples of soil and residual waste obtained from soil borings SB-17, SB-18, and SB-19 are given in Appendix A.
Field notes specifically requested by EPA for sampling operations at soil borings SB-17, SB-18, and SB-19 are given in Appendix B.
In addition, EPA requested that photographs taken during the soil boring
sampling operations be provided. These photographs are included under
separate cover solely to EPA in a letter dated July 30, 1991.
DATA FOR SOIL BORING PROGRAM
Soil borings SB-17, SB-18, and SB-19 were drilled and sampled during the
period from April 30 through May 2, 1991. These soil borings were drilled
and sampled in accordance with the scope of work dated April 22, 1991, which
was requested and formally approved by EPA. These additional soil borings
were requested by EPA to provide data for the depth of former disposal Pits
1, 3b, and 3c, and data for chemical quality of residual wastes and
underlying soils at the pits. The new soil borings were located based on
results from the RI. Soil borings SB-17 and SB-19 were drilled to auger
refusal at the top of the basaltic lava-flow unit.
SOIL BORING SB-17 AT PIT 3c
Soil boring SB-17 was drilled through Pit 3c on April 30 and May 1, and
samples of the pit contents and underlying soils were obtained for laboratory
chemical analyses. Based on inspection of soil samples and action of the
drilling rig, depth to the bottom of Pit 3c was judged to be about nine feet
below land surface. Native soils were encountered below nine feet. Soil
boring SB-17 was drilled to a total depth of 55 feet.
SOIL BORING SB-18 AT PIT 3b
Soil boring SB-18 was drilled through Pit 3b on May 1, and samples of
the pit contents and underlying soils were obtained for laboratory chemical
analyses. Based on inspection of soil samples and action of the drilling
rig, depth to the bottom of the Pit 3b was judged to be about six feet below
land surface. Native soils were encountered below six feet. Soil boring SB-
18 was drilled to a total depth of 20 feet.
SOIL BORING SB-19 AT PIT I
Soil boring SB-19 was drilled through Pit 1 on May 2, and samples of the
pit contents and underlying soils were obtained for laboratory chemical
analyses. Based on inspection of soil samples and action of the drilling
rig, depth to the bottom of Pit 1 was judged to be no more than 15 feet below
land surface. Native soils were encountered below 15 feet. Soil boring SB-
19 was drilled to a total depth of 60 feet.
RESULTS OF LABORATORY CHEMICAL ANALYSES
Laboratory chemical analyses conducted for samples of residual waste
included:
Toxicity Characteristic Leaching Procedure (TCLP) using EPA method 1311. Analyses conducted for the extracted leachate from the TCLP included:
• volatile organic compounds using EPA method 8240;
• semi-volatile organic compounds using EPA method 8270;
• organochlorine pesticides and polychlorinated biphenyls (PCBs) using EPA method 8080; and
• TCLP metals, including arsenic, barium, cadmium, chromium, copper, lead, selenium, silver, nickel, and mercury.
pH using EPA method 9040/9045
cyanide using EPA method 9012
sulfide using EPA method 9030
ignitability using EPA method 1010
Laboratory chemical analyses conducted for samples of soil included:
• TCLP using EPA method 1311. Analyses conducted for the extracted leachate from the TCLP included:
• volatile organic compounds using EPA method 8240;
• semi-volatile organic compounds using EPA method 8270;
• organochlorine pesticides and PCBs using EPA method 8080; and
• TCLP metals, including arsenic, barium, cadmium, chromium, copper, lead, selenium, silver, nickel, and mercury.
Results from these laboratory chemical analyses are summarized in Tables
1 through 8. Chemical laboratory reports are given in Appendix A.
DATA VALIDATION FOR LABORATORY CHEMICAL RESULTS
Laboratory chemical results were evaluated in accordance with the
Quality Assurance Project Plan (QAPP), dated January 29, 1988, and in
accordance with the Montgomery & Associates Quality Assurance/Quality Control
(QA/QC) procedures. Samples were submitted to Analytical Technologies, Inc.
(ATI), Tempe, Arizona, for chemical analyses.
With the following exceptions, the data validation for samples of soil
and residual waste obtained during the period from April 30 to May 2, 1991,
indicated that sampling procedures, sample chain-of-custody, laboratory
methods, and representativeness of results met criteria given in the QAPP.
EPA Method 8240 for Samples of Soil
Concentrations of dichloromethane (DCM) were detected in several soil
samples (Table 2). Results of QA/QC documentation indicate that, with one
exception, it is likely that DCM was present in all of the soil samples for
which it was detected. For the soil sample obtained from soil boring SB-19
at a depth of 24.5 feet (field identifier 004451), the concentration reported
for DCM is less than 10 times the concentration of DCM detected in the
reagent blank, when dilution factors are considered, and is attributable to
laboratory contamination. Please note that, although all soil samples were
analyzed on May 11, several of these analyses were conducted before the
reagent blank for those samples was analyzed. The appropriate reagent blank
for these soil samples was analyzed on May 10.
EPA Method 8240 for Samoles of Residual Waste
Concentrations of DCM were detected in all of the samples of residual
waste (Table 3), which were extracted using the TCLP. In addition, DCM was
detected at a concentration of 50 jig/l in the zero headspace extraction blank
(ZHE reagent blank). Because the TCLP extraction requires acetic acid to be
added to samples, it was standard method procedure to use a minimum dilution
faction of 10 for all samples and the ZHE reagent blank.
The concentrations of DCM detected in samples of residual waste obtained
from soil boring SB-19 at depths of eight feet (field identifier 004449) and
11.5 feet (field identifier 004450) are less than 10 times the concentration
of DCM detected in the ZHE reagent blank, when dilution factors are
considered, and are attributable to laboratory contamination.
The concentration of DCM detected in the sample of residual waste
obtained from soil boring SB-17 at a depth of eight feet (field identifier
004442) is more than 10 times the concentration of DCM detected in the ZHE
reagent blank, and is not attributed to laboratory contamination.
The concentration of DCM detected in the sample of residual waste
obtained from soil boring SB-18 at a depth of five feet (field identifier
004447) is less than 10 times the concentration of DCM detected in the ZHE
reagent blank, and is attributable to laboratory contamination. The
concentration of DCM detected in the split of this sample is nearly 10 times
the concentration of DCM detected in the ZHE reagent blank. The data for
these two samples are considered to be inconclusive regarding the presence
of DCM in the samples.
EPA Method 8270 for Samples of Soil
The matrix spike/matrix spike duplicate (MS/MSD) analyses for the soil
sample obtained from soil boring SB-17 at a depth of 19.5 feet (field
identifier 004443) exceeded the 40-day holding time by five days. Due to the
dark color of the extract, the spiked sample was not analyzed with the sample
batch on May 17; the spiked sample was analyzed on June 21. Another MS/MSD
analyzed on May 17 was provided in addition to the June 21 MS/MSD.
The cover letter of the laboratory report for accession number 105574
(Appendix A) erroneously identified the field identifier for the sample used
for the MS/MSD analyses as 004442. The correct field identifier was 004443.
EPA Method 8270 for Samples of Residual Waste
The extraction holding time was exceeded for the sample of residual
waste obtained from soil boring SB-17 at a depth of eight feet (field
identifier 004442). The sample was first extracted on May 6 and analyzed on
May 17. Surrogate compound recovery was not within laboratory limits and the
same extract was reanalyzed on May 21, again with unacceptable surrogate
recovery. The sample was re-extracted on May 21 and analyzed on May 30.
Although the holding time for extraction of the soil sample was exceeded by
one week, the extract obtained on May 21 met surrogate recovery criteria and
results of May 30 analysis are consistent with results using other methods
for this sample.
EPA Method 8080 for Samples of Soil
For several soil samples, the percent recovery of the surrogate compound
was not attainable due to requisite dilution of the sample. Dilution was
necessary to avoid matrix interference from concentrations of volatile and
semi-volatile organic compounds. No target compounds were detected in any
of the soil samples.
EPA Method 8080 for Samples of Residual Waste
For several samples of residual waste, the percent recovery of the
surrogate compound was not attainable due to requisite dilution of the
sample. Dilution was necessary to avoid matrix interference from concentra
tions of volatile and semi-volatile organic compounds. No target compounds
were detected in any of the soil samples.
TABLE 1. SUMMARY OF LABORATORY CHEMICAL RESULTS FOR TOXICITY CHARACTERISTIC LEACHING PROCEDURE (TCLP) FOR METALS IN SAMPLES OF SOIL AND RESIDUAL WASTE FROH SOIL BORINGS
HASSAYAMPA LANDFILL, MARICOPA COINTY, ARIZONA
INORGANIC CONSTITUENTS'-
SAMPLE LOCATION IDENTIFIER^
SB-17(Pit 3c)
SB-1B(Pit 3b)
SB-19(Pit 1)
19 29, 39. 50
11. 24, 35 45. 45. 55. 56.
DEPTH^
_L! 8-.5 .5 .5
5-5-
8-.5-.5
.5
.5 ,5 .5
feel
•9^
< •6"^
• 9 ^ •13.
• r
dup split
.5 ^
dup split
SAMPLE FIELD
004442 004443 004444 004445 004446
004448 004448
004449 004450 004451 004452 004454 004454 004455 004456
IDENTIFIER LAB
105574-01 105574-09 105574-08 105574-10 105574-11
105574-04 105574-05
105574-06 105574-07 105574-12 105574-13 105574-16 105574-17 105574-18 105574-19
DATE SAMPLED
04-30-91 04-30-91 04-30-91 04-30-91 05-01-91
05-01-91 05-01-91
05-02-91 05-02-91 05-02-91 05-02-91 05-02-91 05-02-91 05-02-91 05-02-91
As
ND ND NO ND ND
ND ND
ND ND ND ND NO ND ND ND
Ba
0.235 0.680 0.298 0.152 0.062
0.232 0.300
3.30 0.052 0.425 0.263 0.204 0.296 0.253 0.228
Cd
0.012 ND ND ND ND
0.013 0.021
0.146 ND ND ND ND ND ND ND
(milllgrams per
Cr
ND ND NO ND 0.012
0.013 0.034
0.035 ND ND ND NO ND ND ND
Pb
ND ND ND ND ND
0.14 0.21
0.32 ND ND ND ND ND ND ND
liter l<
Ni
0.596 ND ND ND ND
0.697 0.962
0.468 0.034 0.023 ND ND ND ND ND
'achate
Se
ND ND NO ND ND
ND ND
ND ND ND ND NO ND ND ND
)
Af)
ND ND NO ND ND
ND ND
ND ND ND ND ND ND ND ND
Cu
27.2 ND NO ND 0.015
40.8 88.7
25.4 0.031 0.023 0.022 0.010 0.014 0.013 0.023
H3
0.0010 ND ND ND ND
ND ND
0.0010 ND ND ND ND ND ND ND
SB = Vertical soil boring Depth interval of residual waste composited for samples
Feet below land surface dup = Duplicate sample
split = Split of preceding sample
Samples extracted by EPA method 1311 (TCLP) Leachate analyzed by EPA method 6010, except Mercury, which was analyzed by EPA method 7470
As = Arsenic Ni = Nickel Ba = Barium Se = Selenium Cd = Cadmium Ag = Silver Cr = Chromium Cu = Copper Pb = Lead Hg = Mercury
NOTE: Samples analyzed by Analytical Technologies, Inc., Phoenix, Arizona
ND Not detected
TABLE 2. SUHMARY OF LABOftATORT CHEHICAL RESULTS FOR EPA METHOD 82^0 FOR VOLATILE ORGANIC COHPOUMOS IN SAMPLES OF SOIL FROH SOIL BORINGS
HASSAYAMPA LANOFILL, MARICOPA COUNTY, ARIZONA
VOLATILE ORGANIC COHPOJNOS SAMPLE LOCAIION lOENTIFIER*
Sfl-17(Pit 3c)
SB-19(Pit 1>
OEPIH, (feet)"
19.5 29.5 39.5 50
2;.5 35 «.5 45.5 $p(it 55.5 54.5
QUALITY CONTROL BLAN*:S:
REAGENT BLANK REACENT BLANK
--* ...
SAHPLE FIELO
0O4A43 004444 004445 004446
004451 004452 004453 004453 004455 004456
...
...
lOENTIFIER LAB
105574-09 105574-OS 105574-10 105574-11
105574-12 105574-13 105574-14 105574-.1f 10557*-ia 105J74-19
105574 105574
DATE SAMPLED
04-30-91 04-30-w'. •"*
C;
Ji-CIS . , \ C.-d2-91 05-02-91 05-02-91 05-02-91
...
DATE ANALTTfO
O'-.- M ••?1
•1-91 .5-11-91
05-11-91 05-11-91 05-11-91 05-11-91 05-11-91 05-11-91
05-10-91 05-11-91
DILUTION
1 1 1 1
4 4 20 20 20 20
1 1
ACTOR
(200) (2,000) (200) (200) (2,000) (2.000)
DCH
ND ND ND ND
4.5 R 70 R 32 27 990 840
0.4 ND
OMK
ND ND 5.3 ND
(2,030) (2,540)
184 200
ND 30
ND NO
1,
NO NO ND ND
(1
ND ND
-DCE
5.8 80 40 42
630) 660
I,'
ND NO NO NO
2. 10. ND ND 45 47
ND NO
-OCA
2 7
MEK
ND NO NO NO
30 76 NO ND 405 292
ND ND
1,1.1-TCA
ND NO NO ND
(1,210) (3,100) (1,000) (820)
(23,000) (18,300)
NO ND
',?-
NO NO ND ND
10 25 12 21 207 160
NO NO
DCP
2
TCE
NO NO ND ND
20.9 113 54 51 590 440
ND NO
1.1.2-
ND ND ND ND
1.4 1 ND ND 12 20
NO NO
TCA MBK
NO ND ND ND
2.1 5 ND ND 23 HD
ND ND
MIBK
NO NO NO NO
9.2 16 Tr 11 48 43
NO NO
PCE
NO ND ND ND
(290) (600) 92 94 560 480
ND ND
MB
NO NO ND NO
44.8 164 64 71 510 400
NO NO
EB
NO NO NO NO
3.5 9 3 3 57 49
NO NO
DHB
ND ND ND ND
25.1 61 26 17 320 350
ND ND
TCIFA
NO ND ND NO
(12 (10
NO ND
6.1 (610) 117 106 ,000) ,500)
OTHERS
NO ND NO ND
0{P)-OCB=2.3 O(P)-0C8=22 ND o(P)-oca=9 BENZENE^l ND
ND ND
' sa > Vertical soil boring
Feet below land surface split : Split of preceding sanfile
DCM > Dichloronwthane (Hethylene Chloride) OMK ' Dimethylketone (Acetone)
1,1-DCE 3 l.l-oichloroethene 1,1-OCA « 1,1-Oichloroethane
MEK • Methylethylketone (2-Butanon«) 1,1,1-TCA s 1,1,1-Trichloroethane 1,2-OCP » 1,2-Oichloropropane
TCE » Trichloroethene 1,1,2-rCA a 1,1,2-Trichloroethane
MBK - 2-Hexanone MIBK = Hethyl isobutyl ketone (4-Hethyl-2-Pentanone)
PCE « Tetrachloroethene HB • Hethylbenzene (Toluene) EB * Ethylbenzene
DHB • Total dimethylbenzenes (xylenes) TCTFA • Trichlorotrifluoroethane (Freon 113)
0(P)-OCa • 0(P)-Dichlorobenzene ND • Not detected — " Not applicable Tr « Trace concentration; positively identified using mass spectrometer,
but detected below limit of quantitation for EPA method 8240 R > Also detected in reagent blank Results given in parentheses are for dilution factors listed in parentheses
NOTE; Samples analyzed by Analytical Technologies, Inc., Phoenix, Arizona
TABLE 3. SUHMARY OF LABORATORY CHEMICAL RESULTS FOR TOXICITY CHARACTERISTIC LEACHING PROCEDURE (TCLP) FOR VOLATILE ORGANIC COHPOUNDS IN SAMPLES OF RESIDUAL UASTE FRCH SOIL BORINGS
HASSAVAMPA LANOFILL, HARICOPA COUNTY, ARIZONA
VOLATILE ORGANIC COMPOUNDS SAMPIE
LOCATION lOENTIFIER
$8-17(Pit 3c)
58-18(Pit 3b)
58-19(P(t I)
DUALITY CONTROL
11
BLANKS
ZKE^ REAGENT SLANK REAGENT BLANK REAGEHT BLANK
DEPTH. (feet)"
8-9
5-6 5-6 spUt
8-9
.5-13.5
...
SAMPLE FIELP,
004442
004447 004447
004449
004450
...
lOENTIFIER LAB
105574-01
105574-02 105574-03
105574-06
105574-07
105574 105574 105574
OATE SAMPLED
04-30-91
05-01-91 05-01-91
05-02-91
05-02-91
...
OATE EXTRACTED
05-08-91
05-08-91 05-08-91
05-08-91
05-08-91
05-08-91 05-16-91 05-17-91
OATE ANALYZED
05-17-91
05-17-91 05-18-91
05-17-91
05-18-91
05-17-91 05-16-91 05-17-91
DILUTION FACTOR
10
10 10
1,000
50
10 1 1
pCH
790
60 470
20,000
880
50 Tr NO
R
R R
R
R
OMK
Tr
Tr Tr
32,000
1,800
ND ND KO
1,1-0C5
Tr
60 60
3,000
ND
NO NO NO
1.1-DCA
60
710 690
8,000
ND
NO NO NO
IA
1 1
220
ND ND NO
...(mic
,1-TCA
30
,300 ,200
,000
800
rograms
1.?-0CP
NO
60 50
4,000
ND
NO NO NO
per liter
TCE .
NO
70 60
10,000
200
ND ND NO
leacha
PCE
100
540 500
9,000
1,500
HD NO NO
te)
MB
ND
ND NO
13,000
790
ND ND ND
DHB
30
20 40
3,000
1,000
NO ND NO
TCTFA .
ND
13,
ND
NO ND ND
90 90
000
OTHERS
0(P)-OCB=10
0(P)-DCB»20 0(P)-OCB»30
MEK=rr; HIBK'Tr; l,1,2-TCA=Tr 0(P)-DCB»IOO; EB=200
HD HO NO
' SB » Vertical soil boring
Feet below land surface dup = Duplicate sarrple
split a Split of preceding sarrple
" Sanples extracted using EPA method 1311 (TCLP) Leachate analyzed using EPA method 8240
DCH =• Dichloromethane (Methylene Chloride) DMK = Dimethylketone (Acetone)
1,1-DCE = 1,1-Oichloroethene 1,1-OCA a 1,1-Dichloroethane
1,1,1-TCA = 1,1,1-Trichloroethane 1,2-DCP • 1,2-Dichloropropane
TCE a Trichloroethene PCE • Tetrachloroethene HB » Hethylbenzene (Toluene)
OMB » Total dimethylbenzenes (xylenes)
ZHE • Zero headspace extraction
TCTFA • Trichlorotrifluoroethane (Freon 113) 0(P)-OCB a 0(P)-dichlorobenzene
HEK " Methylethylketone (2-Butanone) MIBK » 4-Hethyl-2-Pentanone
1,1,2-rcA ' 1,1,2-Trichloroethane EB » Ethylbenzene — • Not applicable Tr • Trace concentration; positively identified using mass spectrometer,
but detected below limit of quantitation for EPA method 8240 ND > Not detected R * Also detected in reagent blank or zero headspace extraction reagent blank
NOIE: Samples analyzed by AnalyticaL Technologies, Inc., Phoenix, Arizona
TABLE 4. SUMMARY OF LABORATORY CHEMICAL RESULTS FOR EPA METHOD 8270 FOR SEMI-VOLATILE ORGANIC COMPOUNDS IN SAMPLES OF SOIL FROM SOIL BORINGS
HASSAYAMPA LANDFILL, MARICOPA COUNTY, ARIZONA
SAMPLE LOCATION IDENTIFIER^
SB-17(Pit 3c)
SB-19(P)t 1)
DEPTH, (feet)"
19.5 29.5 39.5 50
24.5 35 45.5 45.5 split 55.5 56.5
QUALITY CONTROL BLANKS:
SAMPLE FIELD
004443 004444 004445 004446
004451 004452 004453 004453 004455 004456
IDENTIFIER LAB
105574-09 105574-08 105574-10 105574-11
105574-12 105574-13 105574-14 105574-15 105574-18 105574-19
DATE SAMPLED
04-30-91 04-30-91 04-30-91 05-01-91
05-02-91 05-02-91 05-02-91 05-02-91 05-02-91 05-02-91
DATE EXTRACTED
05-07-91 05-07-91 05-07-91 05-07-91
05-07-91 05-07-91 05-07-91 05-07-91 05-07-91 05-07-91
DATE ANALYZED
05-17-91 05-17-91 05-17-91 05-17-91
05-17-91 05-17-91 05-17-91 05-17-91 05-17-91 05-17-91
DILUTION FACTOR
1 1 1 1
20 20 20 20 20 20
PH
ND ND 0.7 ND
17 26 10 8 4 5
2MPH
ND ND ND ND
ND 4 Tr ND ND ND
TARGETED SEMI-VOLATILE ORGANIC COMPOUNDS'^
(mi 11ig
4MPH
ND ND ND ND
ND 4 ND ND ND ND
1.2
ND ND ND ND
ND ND 4 4 Tr 4
per k
-DCB NPH
ND ND ND ND
ND ND ND ND ND 6
2MNPH
ND ND ND ND
ND ND ND ND 9 11
B2EHP
ND ND ND ND
ND ND ND ND ND 6
NON-TARGETEO SEMI-VOLATILE ^
ORGANIC COMPOUNDS"
0HC7
ND ND ND ND
200 200 200 200 100 100
(milligrams per ki logram)
TOA
ND ND ND ND
300 500 200 200
5,000 6,000
TEHC8-C20
ND ND ND ND
200 700 200 200
1,000 2,000
REAGENT BLANK 105574 05-07-91 05-17-91 ND ND ND ND ND ND ND ND ND ND
NOTE:
SB = Vertical soil boring
Feet below land surface split = Split of preceding sample
PH = Phenol 2MPH = 2-Methylphenol 4MPH = 4-Methylphenol
1,2-DCB = 1,2-Dichlorobenzene NPH = Naphthalene
2MNPH = 2-Methylnaphtalene B2EHP = Bis(2-Ethylhexyl)phthalate
Non-targeted compounds are semi-quantitated 0HC7 = Oxygenated hydrocarbons C7 TOA = Total Organic Acids
TEHC8-C20 = Total Extractable Hydrocarbons C8-C20
--- = Not applicable Tr = Trace concentration; positively identified using mass spectrometer,
but detected below limit of quantitation for EPA method 8270 ND = Not detected
Samples analyzed by Analytical Technologies, Inc., Phoenix, Arizona
TABLE 5. SUMMARY OF LABORATORY CHEMICAL RESULTS FOR TOXICITY CHARACTERISTIC LEACHING PROCEDURE (TCLP) FOR SEMI-VOLATILE ORGANIC COMPOUNDS IN SAMPLES OF RESIDUAL WASTE FROM SOIL BORINGS
HASSAYAMPA LANDFILL, MARICOPA COUNTY, ARIZONA
SAMPLE LOCATION IDENTIFIER^
SB-17(Pit 3c)
SB-18(Pit 3b)
SB-19(Pit 1)
DEPTH (feet)*^
8-9
5-6
SAMPLE IDENTIFIER DATE FIELD LAB SAMPLED
DATE DATE EXTRACTED ANALYZED
004442 105574-01 04-30-91 05-21-91 05-30-91
004447 105574-02 05-01-91 05-06-91 05-17-91 5-6 split 004447 105574-03 05-01-91 05-06-91 05-17-91
8-9 11.5-13.5
004449 105574-06 05-02-91 05-06-91 05-17-91 004450 105574-07 05-02-91 05-06-91 05-17-91
DILUTION FACTOR
20 20
TARGETED SEMI-VOLATILE ORGANIC COMPOUNDS'^
.(micrograms per liter leachate)...
PH
ND
ND ND
4MPH
ND
ND ND
BA
ND
ND ND
1.2-DCB OTHERS
ND
Tr Tr
9,400 2,800 1,200 ND 1,400 970 ND ND
ND
ND ND
ND ND
NON-TARGETED SEMI-VOLATILE ORGANIC COMPOUNDS*^'°
(micrograms per liter
BP
ND
200 200
ND ND
0CH7
ND
ND ND
70 20
000 000
OTHERS
B2EHP=e6; TOA=300; TEHC8-C20=60
ND ND
ND ND
QUALITY CONTROL BLANKS:
REAGENT BLANK REAGENT BLANK
105574 105574
05-06-91 05-20-91
05-17-91 05-29-91
1 1
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
SB Vertical soil boring
Feet below land surface split = Split of preceding sample
Samples extracted using EPA method 1311 (TCLP) Leachate analyzed using EPA method 8270
PH = Phenol 4MPH = 4-Methylphenol
BA = Benzoic Acid 1,2-DCB = 1,2-Dichlorobenzene
Tr
Non-targeted compounds are semi-quantitated BP = Benzophenone
0CHC7 = Oxygenated Hydrocarbons C7 TEHC8-C20 = Total Extractable Hydrocarbons C8-C20
— = Not applicable Trace concentration; positively identified using mass spectrometer,
but detected below limit of quantitation for EPA method 8270 ND = Not detected
NOTE: Samples analyzed by Analytical Technologies, Inc., Phoenix, Arizona
TABLE 6. SUMMARY OF LABORATORY CHEMICAL RESULTS FOR TOXICITY CHARACTERISTIC LEACHING PROCEDURE (TCLP) FOR ORGANOCHLORINE PESTICIDES AND POLYCHLORINATED BIPHENYLS (PCBs) IN SAMPLES OF RESIDUAL UASTE FROM SOIL BORINGS
HASSAYAMPA LANDFILL, MARICOPA COUNTY, ARIZONA
SAMPLE LOCATION lOENTIFIER*
SB-17(Pit 3c)
SB-18(Pit 3b)
SB-19(Pit 1)
OUALITY CONTROL
11
DEPTH, (feet)''
8-9
5-6 5-6 split
8-9 .5-13.5
BLANKS:
SAMPLE FIELD
004442
004447 004447
004449 004450
IDENTIFIER LAB
105574-01
105574-02 105574-03
105574-06 105574-07
DATE SAMPLED
04-30-91
05-01-91 05-01-91
05-02-91 05-02-91
DATE EXTRACTED
05-06-91
05-06-91 05-06-91
05-06-91 05-06-91
DATE ANALYZED
05-16-91
05-16-91 05-16-91
05-16-91 05-16-91
OR
ND
ND ND
ND ND
ORGANOCHLORINE PESTICIDES AND PCBs'' (micrograms per liter leachate)
REAGENT BLANK 105574 05-06-91 05-16-91 ND
SB Vertical soil boring
Feet below land surface split = Split of preceding sample
Samples extracted using EPA method 1311 (TCLP) Leachate analyzed using EPA method 8080
ND = Not detected — = Not applicable
NOTE: Samples analyzed by Analytical Technologies, Inc., Phoenix, Arizona
TABLE 7. SUMMARY OF LABORATORY CHEMICAL RESULTS FOR EPA METHOD 8080 FOR ORGANOCHLORINE PESTICIDES AND POLYCHLORINATED BIPHENYLS (PCBs) IN SOIL SAMPLES FROM SOIL BORINGS
HASSAYAMPA LANDFILL, MARICOPA COUNTY, ARIZONA
SAMPLE LOCATION IDENTIFIER a
DEPTH (feet)'^
SAHPLE IDENTIFIER FIELD LAB
DATE SAMPLED
DATE EXTRACTED
DATE ANALYZED
ORGANOCHLORINE PESTICIDES ANO PCBs^ (milligrams per kilogram)
SB-17(Pit 3c) 19.5 29.5 39.5 50
004443 004444 004445 004446
105574-09 105574-08 105574-10 105574-11
04-30-91 04-30-91 04-30-91 05-01-91
05-07-91 05-07-91 05-07-91 05-07-91
OS-OS-OS-OS-
18-91 18-91 18-91 18-91
ND ND ND ND
SB-19(Pit 1) 24.5 35 45.5 45.5 split 55.5 56.5
004451 004452 004453 004453 004455 004456
105574-12 105574-13 105574-14 105574-15 105574-18 105574-19
05-02-91 05-02-91 05-02-91 05-02-91 05-02-91 05-02-91
05-07-91 05-07-91 05-07-91 05-07-91 05-07-91 05-07-91
05-19-91 05-19-91 05-19-91 05-19-91 05-19-91 05-19-91
ND ND ND ND ND ND
QUALITY CONTROL BLANKS:
REAGENT BLANK 105574 05-07-91 05-17-91 ND
SB = Vertical soil boring
Feet below land surface split = Split of preceding sample
ND = Not detected — = Not applicable
NOTE: Samples analyzed by Analytical Technologies, Inc., Phoenix, Arizona Samples were not obtained from SB-18 from below the level of the residual waste for laboratory chemical analyses.
TABLE 8. SUMMARY OF LABORATORY CHEMICAL RESULTS FOR ADDITIONAL ANALYSES OF SAMPLES OF RESIDUAL WASTE FROM SOIL BORINGS
HASSAYAMPA LANDFILL, MARICOPA COUNTY, ARIZONA
SAMPLE LOCATION IDENTIFIER*
SB-17(Pit 3c)
SB-18(Pit 3b)
SB-19(Pit 1)
DEPTH, (feet)"
8-9
5-6 5-6 split 5-6 dup 5-6 split
8-9 11.5-13.5
SAMPLE FIELD
004442
004447 004447 004448 004448
004449 004450
IDENTIFIER LAB
105574-01
105574-02 105574-03 105574-04 105574-05
105574-06 105574-07
DATE SAMPLED
04-30-91
05-01-91 05-01-91 05-01-91 05-01-91
05-02-91 05-02-91
TOTAL CYANIDE'
12.3
12.8 9.3 — —
3.3 0.6
ADDITIONAL TOTAL
SULFIDE*^
ND
... ND ND
ND ND
ANALYSES
pH«
8.5
8.7 8.8 — —
5.7 7.0
IGNITABILITY^
Negligible
Negligible Negligible — —
Negligible Negligible
SB = Vertical soil boring
Feet below land surface dup = Duplicate sample
split = Split of preceding sample
Analyzed using EPA method 9012; mg/kg = Milligrams per kilogram
Analyzed using EPA method 9030; mg/kg = Milligrams per kilogram
Analyzed using EPA method 9040/9045
Analyzed using EPA method 1010
NOTE: Samples analyzed by Analytical Technologies, Inc., Phoenix, Arizona
ND = Not detected — = Not analyzed
I I I
I
I I I
I I
I I
A j X A n a l y t i c a l T e c h n o l o g i e s , Inc. 9330 s. sist street suae B-I 13 pnoemx. AZ 35044 (602)496-4400
ATI I.D. 105574
June 24, 1991
..tj
^•'iOl',:Z'J',"~V P. Afcri;-' IVC
Errol L. Montgomery & Associates JUM'???1GGi 1075 E. Fort Lowell Road ~^ '•-' Suite B Tucson, AZ 85719
Project Name/Nuiaber: Hassayampa/662-A
Attention: Bill Victor
On 05/02/91, Analytical Technologies, Inc. received a request to analyze non-aqueous sample(s). The sample(s) were analyzed with EPA methodology or equivalent methods. The results of these analyses and the quality control data, which follow each set of analyses, are enclosed.
B indicates compound also found in the reagent blank. TR indicates compound found at an unquantifiable trace level. D indicates compound analyzed at a greater dilution. Sulfide analyses were performed by ATI, San Diego. Zero Headspace Extraction (Method 1311) analyses were performed by ATI, Fort Collins.
Dates for inorganic analyses are given on the cjuality control report form.
The results reported for TCLP analyses are the actual measured values, and are not corrected for matrix spike recovery bias. The matrix spike recovery results for TCLP analyses are included in this report.
Method 8080 (TCLP) leachate procedure performed on 05/06/91, and leachate extraction on 05/08/91.
The first extraction on 05/06/91 for Method 8270 (TCLP) sample 03-004442 did not meet ATI criteria for surrogate percent recovery. Re-extraction on 05/21/91 met surrogate criteria and produced results that trend with the results of the other methods on this sample.
Corporc3Te Offices: 5550 Morehouse Drive San Diego. CA 92121 (619) 458-9M1
A - 1
I Montgomery & Associates _ Hassayampa/662-A H Paae 2 H Page 2
Since extraction holding time was exceeded by seven days, the charge for this sample has been dropped. We apologize for any inconvenience this may cause.
Due to the dark color of the Method 8270 matrix spike extract for sample 004442, it was not initially analyzed with the extraction sample batch. The analysis was performed on 06/21/91, five days after the 40 day holding time.
If you have any cjuestions or comments, please do not hesitate to contact us at (602) 496-4400.
n
I
Michael G. Barry Robert V. Woods Project Manager Laboratory Manager
RVW:jat Enclosure
0 I I I I I
f f -•'^.^ f » • «
A-2
^ J ^ AnalyticalTechnologies, Inc. 9830 S. 51st Street Suite B-113 Phoenix, AZ 85044 (602) 496-4400
ATI I.D. 105574
July 12, 1991
Errol L. Montgomery & Associates 1075 E. Fort Lowell Road Suite B Tucson, AZ 8 5719
Project Name/Number: Hassayampa/662-A
Attention: Bill Victor
JUL 15 n-l
:c;.:;::v i , A C S C C , I':C.
On 05/02/91, Analytical Technologies, Inc. received a request to analyze non-acjueous sample(s). The sample(s) were analyzed with EPA methodology or ecjuivalent methods. The results of these analyses and the cjuality control data, which follow each set of analyses, are enclosed.
Enclosed is an amended report for method 8240 any inconvenience this may have caused.
We apologize for
B indicates compound also found in the reagent blank. TR indicates compound found at an uncjuant if iable trace level. D inciicates compound analyzed at a greater dilution. Sulfide analyses were perfonned by ATI, San Diego. Zero Headspace Extraction (Method 1311) analyses were performed by ATI, Fort Collins.
Dates for inorganic analyses are given on the quality control report form.
The results reported for TCLP analyses are the actual measured values, and are not corrected for matrix spike recovery bias. The matrix spike recovery results for TCLP analyses are included in this report.
Method 8080 (TCLP) leachate procedure performed on 05/06/91, and leachate extraction on 05/08/91.
The first extraction on 05/06/91 for Method 8270 (TCLP) sample 03-004442 did not meet ATI criteria for surrogate percent
Corpa(3te Offices: 5550 Morehouse Drive San Diego. CA 92121 (619) 458-9141
A-3
Montgomery & A s s o c i a t e s Hassfift^ampa/662-A ssM^a
/ j [ \ A n a l y t i c a l T e c h n o l o g i e s , Inc. gases, sist street suite B-H 3 Phoenix, AZ 35044 (602)496-4400
recovery. Re-extraction on 05/21/91 met surrogate criteria and produced results that trend with the results of the other methods on this sample.
Since extraction holding time was exceeded by seven days, the charge for this sample has been dropped. We apologize for any inconvenience this may cause.
Due to the dark color of the Method 8270 matrix spike extract for sample 004442, it was not initially analyzed with the extraction sample batch. The analysis was performed on 06/21/91, five days after the 40 day holding time.
If you have any cjuestions or comments, please do not hesitate to contact us at (602) 496-4400.
ti^ {^Lr.^Ji Michael G. Barry Robert V. Woods Project Manager Laboratory Manager
RVW:jat Enclosure
Corporate Offices; 5550 Morehouse Drive San Diego. CA 92121 (619) 458-9141
A-4
/l\ 9830 8. 51st Street Suite B-113 Phoenix. AZ 85044 (602) 496-4400 yjjbjw AnalyticalTechnologies,Inc.
ATI I.D. 105574
July 12, 1991
Errol L. Montgomery & Associates 1075 E. Fort Lowell Road Suite B Tucson, AZ 85719 PaX/vfo
Project Name/Number: Hassayampa/662-A
Attention: Bill Victor
JUL 16 in-
' ' ^ ' ' ^ o ^ : r f a ASSOC, i::c.
On 05/02/91, Analytical Technologies, Inc. received a request to analyze non-acjueous sample(s). The sample(s) were analyzed with EPA methodology or ecjuivalent methods. The results of these analyses and the cjuality control data, which follow each set of analyses, are enclosed.
Enclosed is an amended report for method 8240. We apologize for any inconvenience this may have caused.
B indicates compound also found in the reagent blank. TR indicates compound found at an uncjuant if iable trace level. D indicates compound analyzed at a greater dilution. Sulfide analyses were performed by ATI, San Diego. Zero Headspace Extraction (Method 1311) analyses were performed by ATI, Fort Collins.
Dates for inorganic analyses are given on the quality control report form.
The results reported for TCLP analyses are' the actual measured values, and are not corrected for matrix spike recovery bias. The matrix spike recovery results for TCLP analyses are included in this report.
Method 8080 (TCLP) leachate procedure performed on 05/06/91, and leachate extraction on 05/08/91.
The first extraction on 05/06/91 for Method 8270 (TCLP) sample 03-004442 did not meet ATI criteria for surrogate percent
Corporate Offices: 5550 Morehouse Drive San Diego. CA 92121 (619) 458-9141
A-5
Montgomery & Associates Hassayampa/662-A Page 2
recovery. Re-extraction on 05/21/91 met surrogate criteria and produced results that trend with the results of the other methods on this sample.
Since extraction holding time was exceeded by seven days, the charge for this sample has been dropped. We apologize for any inconvenience this may cause.
Due to the dark color of the Method 8270 matrix spike extract for sample 004442, it was not initially analyzed with the extraction sample batch. The analysis was performed on 06/21/91, five days after the 4 0 day holding time.
If you have any questions or comments, please do not hesitate to contact us at (602) 496-4400.
Michael G. Barry Project Manager
Robert V. Woods Laboratory Manager
RVW:jat Enclosure
A-6
^ j ^ AnalyticalTechnologies
CLIENT PROJECT # PROJECT NAME
, Inc.
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA
ATI I.D. : 105574
DATE RECEIVED : 05/02/91
REPORT DATE : 06/22/91
ATI # CLIENT DESCRIPTION MATRIX DATE COLLECTED
01 02 03 04 05 06 07 08 09 10 11 12 13 14 15 16 17 18 19 20
03-004442 03-004447 03-004447 03-004448 03-004448 03-004449 03-004450 03-004444 03-004443 03-004445 03-004446 03-004451 03-004452 03-004453 03-004453 03-004454 03-004454 03-004455 03-004456
DUPLICATE
DUPLICATE
DUPLICATE
DUPLICATE
ZHE REAGENT BLANK
NON-AQUEOUS NON-AQUEOUS NON-AQUEOUS NON-AQUEOUS NON-AQUEOUS NON-AQUEOUS NON-AQUEOUS NON-AQUEOUS NON-AQUEOUS NON-AQUEOUS NON-AQUEOUS NON-AQUEOUS NON-AQUEOUS NON-AQUEOUS NON-AQUEOUS NON-AQUEOUS NON-AQUEOUS NON-AQUEOUS NON-AQUEOUS NON-AQUEOUS
04/30/91 05/01/91 05/01/91 05/01/91 05/01/91 05/02/91 05/02/91 04/30/91 04/30/91 04/30/91 05/01/91 05/02/91 05/02/91 05/02/91 05/02/91 05/02/91 05/02/91 05/02/91 05/02/91 05/08/91
TOTALS
MATRIX
NON-AQUEOUS
# SAMPLES
20
ATI STANDARD DISPOSAL PRACTICE
The samples from this project will be disposed of in thirty (30) days from th date of this report. If an extended storage period is required, please contac our sample control department before the scheduled disposal date.
A-7
A j S AnalyticalTechnologies ,lnc.
i , ?,-t 2 c s-B-n s - ^ ' c j ^ f i t 3to i-B-i? T-i'
GENERAL CHEMISTRY RESULTS
CLIENT : MONTGOMERY & ASSOCIATES PROJECT # : 66 2-A PROJECT NAME : HASSAYAMPA
ATI I.D. : 105574
DATE RECEIVED : 05/02/91
REPORT DATE ; 06/22/91
PARAMETER UNITS
MG/KG
UNITS MG/KG
01 02 03 04 05
CYANIDE, TOTAL IGNITABILITY PH SULFIDE, TOTAL
12.3 NEG 8.5 <0.5
12.8 NEG 8.7
9.3 NEG 8.8
<0.5 <2.5
A-8
/jj Vk AnalyticalTechnologies,I
o r T ' b ) i"?>-i'i )(?-l5-'
GENERAL CHEMISTRY RESULTS
CLIENT : MONTGOMERY & ASSOCIATES PROJECT # : 6 62-A PROJECT NAME : HASSAYAMPA
ATI I.D. : 105574
DATE RECEIVED : 05/02/91
REPORT DATE : 06/22/91
PARAMETER UNITS
MG/KG
UNITS MG/KG
06 07
CYANIDE, TOTAL IGNITABILITY PH SULFIDE, TOTAL
3.3 NEG 5.7 <2.5
0.6 NEG 7.0 <0.5
A-9
A T,r t ^'&-)'=) 10-/5"' / j \ AnalyticalTechnologies, Inc.
GENERAL CHEMISTRY - QUALITY CONTROL
CLIENT : MONTGOMERY & ASSOCIATES PROJECT # : 66 2-A PROJECT NAME : HASSAYAMPA ATI I.D, 105574
SAMPLE DUP. SPIKED SPIKE % UNITS ATI I.D. RESULT RESULT RPD SAMPLE CONC REC PARAMETER
CYANIDE, TOTAL IGNITABILITY PH SULFIDE, TOTAL
MG/KG
UNITS MG/KG
10557401 10557407 10557407 10599918
12.3 NEG 7.0 <0.5
10.8 NEG 7.0 <0.5
13 NA 0
NA
38.7 NA NA 0.41
25.0 NA NA 0.40
106 NA NA 103
X 100 % Recovery = (Spike Sample Result - Sample Result)
Spike Concentration
RPD (Relative Percent Difference) = (Sample Result - Duplicate Result)
Average Result X IOC
A-10
A j S AnalyticalTechnologies,Inc
CLIENT PROJECT # PROJECT NAME
MONTGOMERY 662-A HASSAYAMPA
METALS RESULTS
& ASSOCIATES
O l
o ^
r ' T
OL.
on
?.t 3c
?,t 3b 7. t 3& P . t 1
7 , IT)
tn,-n 4 B - ) t s^- lz sB-n -J-B-i' l
S-7'
5"- .' 'i^*/'
/o-/i"'
ATI I.D. : 105574
DATE RECEIVED : 05/0 2/91
REPORT DATE : 06/22/91
05 06 07 PARAMETER UNITS 01 04
SILVER (IN TCLP) ARSENIC (IN TCLP) BARIUM (IN TCLP) CADMIUM (IN TCLP) CHROMIUM (IN TCLP) COPPER (IN TLCP) MERCURY (IN TCLP) NICKEL (IN TCLP) LEAD (IN TCLP) SELENIUM (IN TCLP)
MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L
< 0 . 0 1 0 < 0 . 1 0 . 2 3 5 0 . 0 1 2 < 0 . 0 1 0 2 7 . 2 0 . 0 0 1 0 0 . 5 9 6 < 0 . 1 0 < 0 . 1
< 0 . 0 1 0 < 0 . 1 0 . 2 3 2 0 . 0 1 3 0 . 0 1 3 4 0 . 8 < 0 , 0 0 0 2 0 . 6 9 7 0 . 1 4 < 0 . 1
< 0 . 0 1 0 < 0 . 1 0 . 3 0 0 0 . 0 2 1 0 . 0 3 4 8 8 . 7 < 0 . 0 0 0 2 0 . 9 5 2 0 . 2 1 < 0 . 1
< 0 . 0 1 0 < 0 . 1 3 . 3 0 0 . 1 4 6 0 . 0 3 5 2 5 . 4 0 . 0 0 1 0 0 . 4 6 8 0 . 3 2 < 0 . 1
< 0 . 0 1 0 < 0 . 1 0 . 0 5 2 < 0 . 0 0 5 < 0 . 0 1 0 0 . 0 3 1 < 0 . 0 0 0 2 0 . 0 3 4 < 0 . 1 0 < 0 . 1
A-11
^ jS^ AnalyticalTechnologies, Inc.
METALS RESULTS
i'i Vit it: S'S-!? X'i.iT-ao' O P;t- 3^ •i'd-n l^,:>'-ZC'
/, ? . t 3 i i b - i ? 4'7.5--5T)' /X. P i t I . iB-i<^ 2«i.y - a s '
ATI I . D . : 105574
CLIENT PROJECT # PROJECT NAME
MONTGOMERY & ASSOCIATES 652-A HASSAYAMPA
DATE RECEIVED
REPORT DATE
05/02/91
06/22/91
PARAMETER UNITS 08 09 10 11 12
SILVER ( ARSENIC BARIUM ( CADMIUM CHROMIUM COPPER ( MERCURY NICKEL ( LEAD (IN SELENIUM
IN TCLP) (IN TCLP) IN TCLP) (IN TCLP) (IN TCLP)
IN TLCP) (IN TCLP) IN TCLP) TCLP) (IN TCLP)
MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L
<0.010 <0.1 0.298 <0.005 <0.010 <0.010 <0.0002 <0.020 <0.10 <0.1
<0.010 <0.1 0.680 <0.005 <0.010 <0.010 <0.0002 <0.020 <0.10 <0.1
<0.010 <0.1 0.152 <0.005 <0.010 <0.010 <0.0002 <0.020 <0.10 <0.1
<0.010 <0.1 0.062 <0.005 0.012 0.015 <0.0002 <0.020 <0.10 <0.1
<0.010 <0.1 0.425 <0.005 <0.010 0.023 <0.0002 0.023 <0.10 <0.1
A-12
A j S AnalyticalTechnologies,lr
METALS RESULTS
l-J 'fc. n iS
'1
p.r 1
?.v :
?.tl
ia-i? 3.5--3i-. 5-'
CLIENT PROJECT # PROJECT NAME
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA
ATI I.D, 105574
DATE RECEIVED : 05/0 2/91
REPORT DATE : 06/22/91
PARAMETER UNITS 13 16 17 18 19
SILVER ( ARSENIC BARIUM ( CADMIUM CHROMIUM COPPER ( MERCURY NICKEL ( LEAD (IN SELENIUM
IN TCLP) (IN TCLP) IN TCLP) (IN TCLP) (IN TCLP)
IN TLCP) (IN TCLP) IN TCLP) TCLP) (IN TCLP)
MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L
<0.010 <0.1 0.263 <0.005 <0.010 0.022 <0.0002 <0.020 <0.10 <0.1
<0.010 <0.1 0.204 0.005 <0.010 0.010 <0.0002 <0.020 <0.10 <0.1
<0.010 <0.1 0.296 <0.005 <0.010 0.014 <0.0002 <0.020 <0.10 <0.1
<0.010 <0.1 0.253 <0.005 <0.010 0.013 <0.0002 <0.020 <0.10 <0.1
<0.010 <0.1 0.228 <0.005 <0.010 0.023 <0.0002 <0.020 <0.10 <0.1
A-13
/ j S AnalyticalTechnologies,Inc.
METALS - QUALITY CONTROL
CLIENT PROJECT # PROJECT NAME
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA
t.B-17
ATI I.D, 105574
PARAMETER UNITS ATI I.D. SAMPLE RESULT
DUP. RESULT RPD
SPIKED SPIKE % SAMPLE CONC REC
SILVER (IN TCLP) MG/L 10557407 SILVER (IN TCLP) MG/L 10557417 ARSENIC (IN TCLP) MG/L 10557407 ARSENIC (IN TCLP) MG/L 10557417 BARIUM (IN TCLP) MG/L 10557407 BARIUM (IN TCLP) MG/L 10557417 CADMIUM (IN TCLP) MG/L 10557407 CADMIUM (IN TCLP) MG/L 10557417 CHROMIUM (IN TCLP) MG/L 10557407 CHROMIUM (IN TCLP) MG/L 10557416 COPPER (IN TLCP) MG/L 10557407 COPPER (IN TLCP) MG/L 10557417 MERCURY (IN TCLP) MG/L 10557406 MERCURY (IN TCLP) MG/L 10557407 MERCURY (IN TCLP) MG/L 10558213 NICKEL (IN LEACHATE) MG/L 10557407 NICKEL (IN LEACHATE) MG/L 10557417 LEAD (IN TCLP) MG/L 10557407 LEAD (IN TCLP) MG/L 10557417 SELENIUM (IN TCLP) MG/L 10557407 SELENIUM (IN TCLP) MG/L 10557417
<0.010 <0.010 <0.1 <0.1 0.052 0.296 <0.005 <0.005 <0.010 <0.010 0.031 0.014 0.0010 <0.0002 <0.0002 0.034 <0.020
10 10 1 1
<0, <0. <0 <0
<0.010 <0.010 <0.1 <0.1 0.049 0.296 <0.005 0.006 <0.010 <0.010 0.027 0.014 0.0009 <0.000 <0.000 0.033 <0.020 <0 <0 <0 <0
10 10 1 1
NA NA NA NA 6 0
NA NA NA NA 14 0
10 NA NA 3
NA NA NA NA NA
0. 0. 1. 1. 0. 1. 1. 0. 1. 0. 0. 0. 0. 0. 0. 0. 0. 0. 1. 1. 10
806 874 0 1 916 24 26 932 70 951 456 964 0049 0041 0043 832 929 86 02 0 .6
1 1 1 1 1 1 1 1 2. 1. 0. 1. 0. 0. 0. 1. 1. 1. 1. 1. 10
00 00 0 0 00 00 50 00 00 00 500 00 0050 0050 0050 00 00 00 00 0 0
81 8 7 100 110 86 94 84 93 85 95 8 7 95 78 82 86 80 93 86 102 100 106
% Recovery = (Spike Sample Result - Sample Result) X 100
Spike Concentration
RPD (Relative Percent Difference) = (Sample Result - Duplicate Result)
Average Result
* Result out of limits due to sample matrix interference
X 10-
A-14
AjS AnalyticalTechnologies, Inc.
S^-17
Page No. 0 6 / 2 4 / 9 1
ANALYTE
QUALITY CONTROL REPORT
IN-IT DATE OF CORR. QC
ANALYSIS COEFF. NAME
VALUE TRUE LOWER UPPER UNIT FOUND VALUE CONTROL CONTROL
LIMIT LIMIT
** ACCESSION Nl
METHOD 33 5.2
CYANIDE
METHOD 1010
IGNITABILITY
METHOD 9045
pH
METHOD 9030
SULFIDE
METHOD 200.7
SILVER ARSENIC BARIUM CADMIUM CHROMIUM COPPER NICKEL LEAD SELENIUM
JMBER:
NM
SH
IKW
SM
JJH JJH JJH JJH JJH JJH JJH JJH JJH
105574
05/16/91
05/10/91
05/13/91
05/09/91
05/17/91 05/17/91 05/17/91 05/17/91 05/20/91 05/17/91 05/17/91 05/17/91 05/17/91
0.999
NA
NA
NA
NA NA NA NA NA NA NA NA NA
LCS051
NA
FISHER
LCS
ICAP2 ICAP3 ICAP3 ICAP3 ICAP3 ICAP3 ICAP3 I CAP 3 I CAP 3
0.23
NA
6.87
0.40
0.988 1.0 1.02 1.02 1.00 1.02 1.01 1.06 10.1
0.25
NA
6.86
0.40
1.00 1.0 1.00 1.00 1.00 1.00 1.00 1.00 10.0
0.21
NA
5.83
0.36
0.850 0.8 0.850 0.850 0.850 0.850 0.850 0.85 8.5
0.29
NA
7.89
0.44
1.15 1.2 1.15 1.15 1.15 1.15 1.15 1.15 11.5
MG/L
NA
pH
MG/K(
MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L
METHOD 245.1
MERCURY MERCURY
JJH JJH
05/14/91 0.999 05/22/91 0.999
WP1085 2.23 WP989 1.99
2.03 2.02
1.83 1.46
2.23 2.58
UG/L UG/L
A-15 ^
AjS AnalyticalTechnologies,Inc.
51^1-7 :i i . ' T - - 50
GCMS - RESULTS
ATI I.D. : 10557408
TEST : VOLATILE ORGANICS (EPA 8240)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA 03-004444 NON-AQUEOUS
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
04/30/91 05/02/91 05/06/91 05/11/91 MG/KG
1
COMPOUNDS RESULTS
CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1, 2-DICHLOROETHANE 2-BUTANONE (MEK) 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE VINYL ACETATE BROMODICHLOROMETHANE 1,1,2,2-TETRACHLOROETHANE 1, 2-DICHLOROPROPANE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE CIS-1,3-DICHLOROPROPENE 2-CHLOROETHYLVINYLETHER BROMOFORM 2-HEXANONE (MBK) 4-METHYL-2-PENTANONE (MIBK) TETRACHLOROETHENE TOLUENE CHLOROBENZENE ETHYLBENZENE STYRENE TOTAL XYLENES
<0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0
.50
.50
.05
.05
.3
.50
.05
.05
.05
.05
.05
.05
.50
.05
.05
.50
.05
.05
.05
.05
.05
.05
.05
.05
.05
.50
.3
.50
.50
.05
.05
.05
.05
.05
.05
SURROGATE PERCENT RECOVERIES
l,2-DICHLOROETHANE-D4 (%) BROMOFLUOROBENZENE (%) T0LUENE-D8 (%)
A-16
105 107 104
X ^ AnalyticalTechnologies, Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED)
/ N Analyti(
TEST : VOLATILE ORGANICS (EPA 8240)
ATI I . D . : 10557408
COMPOUNDS
NO ADDITIONAL COMPOUNDS
RESULTS
<0.3
A-17
AjS Analytical Technologies, lr
6B-I1 \ ' I - 5 - - 2 J Z ' '
GCMS - RESULTS
TEST : VOLATILE ORGANICS (EPA 8240)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX : NON-AQUEOUS
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA 03-004443
ATI I.D. : 10557409
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
04/30/91 05/02/91 05/05/91 05/11/91 MG/KG
1
COMPOUNDS RESULTS
CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1, 1-DICHLOROETHENE 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1, 2-DICHLOROETHANE 2-BUTANONE (MEK) 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE VINYL ACETATE BROMODICHLOROMETHANE 1,1,2,2-TETRACHLOROETHANE 1,2-DICHLOROPROPANE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE CIS-1,3-DICHLOROPROPENE 2-CHLOROETHYLVINYLETHER BROMOFORM 2-HEXANONE (MBK) 4-METHYL-2-PENTANONE (MIBK) TETRACHLOROETHENE TOLUENE CHLOROBENZENE ETHYLBENZENE STYRENE TOTAL XYLENES
SURROGATE PERCENT RECOVERIES
< 0 . 5 0 < 0 . 5 0 < 0 . 0 5 < 0 . 0 5 < 0 . 3 < 0 . 5 0 < 0 . 0 5 < 0 . 0 5 < 0 . 0 5 < 0 . 0 5 < 0 . 0 5 < 0 . 0 5 < 0 . 5 0 < 0 . 0 5 < 0 . 0 5 < 0 . 5 0 < 0 . 0 5 < 0 . 0 5 < 0 . 0 5 < 0 . 0 5 < 0 . 0 5 < 0 . 0 5 < 0 . 0 5 < 0 . 0 5 < 0 . 0 5 < 0 . 5 0 < 0 . 3 < 0 . 5 0 < 0 . 5 0 < 0 . 0 5 < 0 . 0 5 < 0 . 0 5 < 0 . 0 5 < 0 . 0 5 < 0 . 0 5
e i
l,2-DICHLOROETHANE-D4 (%) BROMOFLUOROBENZENE (%) T0LUENE-D8 (%)
A-18
106 109 110
i
/ j ^ AnalyticalTechnologies, Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED)
A
TEST : VOLATILE ORGANICS (EPA 8 240)
ATI I.D. : 10557409
COMPOUNDS
NO ADDITIONAL COMPOUNDS
RESULTS
<0.3
A-19
A i S AnalyticalTechnologies,Inc.
$B-' - .^
GCMS - RESULTS
ATI I.D. : 10557410
TEST : VOLATILE ORGANICS (EPA 8240)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX
MONTGOMERY & ASSOCIATES 552-A HASSAYAMPA 03-004445 NON-AQUEOUS
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
04/30/91 05/02/91 05/06/91 05/11/91 MG/KG
1
COMPOUNDS RESULTS
CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1, 2-DICHLOROETHANE 2-BUTANONE (MEK) 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE VINYL ACETATE BROMODICHLOROMETHANE 1,1,2,2-TETRACHLOROETHANE 1,2-DICHLOROPROPANE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE CIS-1, 3-DICHLOROPROPENE . 2-CHLOROETHYLVINYLETHER BROMOFORM 2-HEXANONE (MBK) 4-METHYL-2-PENTANONE (MIBK) TETRACHLOROETHENE TOLUENE CHLOROBENZENE ETHYLBENZENE STYRENE TOTAL XYLENES
<0. <0. <0, <0, <0. 5.3 <0, <0, <0, <0, <0, <0, <0 <0, <0. <0, <0. <0 <0 <0 <o. <o, <0, <0, <0. <0, <0. <0. <o, <o. <o. <0, <o. <0, <0.
50 50 05 05 3
05 05 05 05 05 05 50 05 05 50 05 05 05 05 05 05 05 05 05 50 3 50 50 05 05 05 05 05 05
SURROGATE PERCENT RECOVERIES
l,2-DICHLOROETHANE-D4 (%) BROMOFLUOROBENZENE (%) T0LUENE-D8 (%) A-20
103 105 102
/ J s AnalyticalTechnologies,Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED)
A
TEST : VOLATILE ORGANICS (EPA 8240)
ATI I.D. : 10557410
COMPOUNDS
NO ADDITIONAL COMPOUNDS
RESULTS
<0.3
A-21
A j S AnalyticalTechnologies
GCMS - RESULTS
^ i h - n ^ ,.5 - ^ O '
ATI I.D. : 10557411
TEST : VOLATILE ORGANICS (EPA 8240)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX : NON-AQUEOUS
MONTGOMERY 662-A HASSAYAMPA 03-004446
& ASSOCIATES DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/01/91 05/02/91 05/06/91 05/11/91 MG/KG
1
COMPOUNDS . .RESULTS
CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1, 2-DICHLOROETHANE 2-BUTANONE (MEK) 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE VINYL ACETATE BROMODICHLOROMETHANE 1,1,2,2-TETRACHLOROETHANE 1,2-DICHLOROPROPANE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE CIS-1,3-DICHLOROPROPENE 2-CHLOROETHYLVINYLETHER BROMOFORM 2-HEXANONE (MBK) 4-METHYL-2-PENTANONE (MIBK) TETRACHLOROETHENE TOLUENE CHLOROBENZENE ETHYLBENZENE STYRENE TOTAL XYLENES
SURROGATE PERCENT RECOVERIES
<0.50 <0.50 <0.05 <0.05 < Q . 3 <0.50 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.50 <0.05 <0.05 <0.50 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.50 <0.3 <0.50 <0.50 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05
1,2-DICHLOROETHANE-D4 (%) BROMOFLUOROBENZENE (%) T0LUENE-D8 (%)
A-22
97 111 103
A 5l3-n ^^.T-SZ''
A j S AnalyticalTechnologies,Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED)
TEST : VOLATILE ORGANICS (EPA 8240)
ATI I.D. : 10557411
COMPOUNDS
NO ADDITIONAL COMPOUNDS
RESULTS
<0.3
A-23
A i S AnalyticalTechnologies,
5'B-i'i 2M.5--25-'
GCMS - RESULTS
ATI I.D, 10557412
TEST : VOLATILE ORGANICS (EPA 8240)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX : NON-AQUEOUS
MONTGOMERY 652-A HASSAYAMPA 03-004451
& ASSOCIATES DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/02/91 05/02/91 05/06/91 05/11/91 MG/KG
4
COMPOUNDS RESULTS
CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE 2-BUTANONE (MEK) 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE VINYL ACETATE BROMODICHLOROMETHANE 1,1,2,2-TETRACHLOROETHANE 1,2-DICHLOROPROPANE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE CIS-1,3-DICHLOROPROPENE 2-CHLOROETHYLVINYLETHER BROMOFORM 2-HEXANONE (MBK) 4-METHYL-2-PENTANONE (MIBK) TETRACHLOROETHENE TOLUENE CHLOROBENZENE ETHYLBENZENE STYRENE TOTAL XYLENES
SURROGATE PERCENT RECOVERIES
l,2-DICHLOROETHANE-D4 (%) BROMOFLUOROBENZENE (%) T0LUENE-D8 (%)
<2.00 <2.00 <0.20 <0.20
4.5 B 2030 D <0.20
5.8 2.2 <0.20 <0.20 <0.20 30 1210 D <0.20 <2.00 <0.20 <0.20 10.2 <0.20 20.9 <0.20 1.4 <0.20 <0.20 <2.00 <1.2 2.1 9.2 290 D 44.8 <0.20 3.5 <0.20 25.1
103 114 101
D INDICATES COMPOUND ANALYZED AT A DILUTION OF 200 A-24
A 5^-)") 2 ^ 1 , 5 - ^ : i '
A j S AnalyticalTechnologies,Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED)
TEST : VOLATILE ORGANICS (EPA 824 0)
ATI I.D. : 10557412
COMPOUNDS RESULTS
0(P)-DICHLOROBENZENE TRICHLOROTRIFLUOROETHANE
2.3 5.1
A-25
^ j ^ AnalyticalTechnologies, Inc.
b^-1^ i ^ -sy -s '
GCMS - RESULTS
TEST : VOLATILE ORGANICS (EPA 824 0)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX : NON-AQUEOUS
MONTGOMERY 6 6 2-A HASSAYAMPA 03-004452
& ASSOCIATES
ATI I.D, 10557413
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/02/91 05/02/91 05/06/91 05/11/91 MG/KG
4
COMPOUNDS RESULTS
CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE 2-BUTANONE (MEK) 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE VINYL ACETATE BROMODICHLOROMETHANE 1,1,2,2-TETRACHLOROETHANE 1,2-DICHLOROPROPANE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE CIS-1, 3-DICHLOROPROPENE 2-CHLOROETHYLVINYLETHER BROMOFORM 2-HEXANONE (MBK) 4-METHYL-2-PENTANONE (MIBK) TETRACHLOROETHENE TOLUENE CHLOROBENZENE ETHYLBENZENE STYRENE TOTAL XYLENES
<2.00 <2.00 <0.20 <0.20
70 B 2540 D <0.20
80 1 0 . 7
< 0 . 2 0 < 0 . 2 0 < 0 . 2 0 75 3100 D <0.20 <2 <0 <0 25 <0 113 <0
1 <0 <0 <2 <1 5 15 600 164 <0 9 <0 61
00 20 20
20
20
20 20 00 2
20
20
SURROGATE PERCENT RECOVERIES
l,2-DICHLOROETHANE-D4 (%) BROMOFLUOROBENZENE (%) T0LUENE-D8 (%)
110 96 99
D INDICATES COMPOUND ANALYZED AT A DILUTION OF 2000X A-26
/ N . Anc
5 3 - " - , 3-7 ' 3 i ^ . 5 ' '
A j S AnalyticalTechnologies,Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED)
TEST : VOLATILE ORGANICS (EPA 8240)
ATI I.D. : 10557413
COMPOUNDS RESULTS
0 (P)-DICHLOROBENZENE TRICHLOROTRIFLUOROETHANE
22 510 D
D INDICATES COMPOUND ANALYZED AT A DILUTION OF 2000X
A-27
A j S AnalyticalTechnologies,Inc
GCMS - RESULTS
5B-iT 5-.5 - ^ C
ATI I.D. : 10557414
TEST : VOLATILE ORGANICS (EPA 8240)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX : NON-AQUEOUS
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA 03-004453
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/02/91 05/02/91 05/06/91 05/11/91 MG/KG
20
COMPOUNDS RESULTS
CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE 2-BUTANONE (MEK) 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE VINYL ACETATE BROMODICHLOROMETHANE 1,1,2,2-TETRACHLOROETHANE 1, 2-DICHLOROPROPANE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE CIS-1,3-DICHLOROPROPENE 2 -CHLOROETHYLVINYLETHER BROMOFORM 2-HEXANONE (MBK) 4-METHYL-2-PENTANONE (MIBK) TETRACHLOROETHENE TOLUENE CHLOROBENZENE ETHYLBENZENE STYRENE TOTAL XYLENES
<10.0 <10.0 <1.0
0 <1 32 184 <1
40 <1 <1 <1 <1
0 0 0 0
<10.0 1000 D <1.0 <10.0 <1.0 <1.0 12 <1.0
54 <1.0 <1.0 <1.0 <1.0 <10.0 <6.0 <10.0
TR 92 64 <1.0 3 <1.0 26
SURROGATE PERCENT RECOVERIES
l,2-DICHLOROETHANE-D4 (%) 9 2 BROMOFLUOROBENZENE (%) 85 T0LUENE-D8 (%) 99 D INDICATES COMPOUND ANALYZED AT A DILUTION OF 200 TR - Compound detected at an unquantifiable trace level
A-28
A ^Tb-i ' i ^S.S'-^l:^'
A i s AnalyticalTechnologies, Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED)
TEST : VOIATILE ORGANICS (EPA 8240)
ATI I.D. : 10557414
COMPOUNDS
TRICHLOROTRIFLUOROETHANE
RESULTS
117
A-29
/ K AnalyticalTechnologies, ,nc.
GCMS - RESULTS
ATI I.D. : 10557415
TEST : VOLATILE ORGANICS (EPA 8 240)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX
MONTGOMERY 5. ASSOCIATES 662-A HASSAYAMPA 03-004453 DUPLICATE NON-AQUEOUS
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/02/91 05/02/91 05/06/91 05/11/91 MG/KG
20
COMPOUNDS RESULTS
CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE 2-BUTANONE (MEK) 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE VINYL ACETATE BROMODICHLOROMETHANE 1,1,2,2-TETRACHLOROETHANE 1, 2-DICHLOROPROPANE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE CIS-1 , 3-DICHLOROPROPENE 2-CHLOROETHYLVINYLETHER BROMOFORM 2-HEXANONE (MBK) 4-METHYL-2-PENTANONE (MIBK) TETRACHLOROETHENE TOLUENE CHLOROBENZENE ETHYLBENZENE STYRENE TOTAL XYLENES
SURROGATE PERCENT RECOVERIES
l,2-DICHLOROETHANE-D4 (%) BROMOFLUOROBENZENE (%) T0LUENE-D8 (%)
0
0 0 0 0
<10.0 <10.0 <1.0 <1.0 27 200 <1
42 <1 <1 <1 <1 <10.0 820 D <1.0 <10.0 <1.0 <1.0 21 <1 51 <1 <1 <1 <1 <10.0 <6.0 <10.0 11 94 71 <1.0 3 ' <1.0 17
86 96 101
0
0 0 0 0
A-30 D INDICATES COMPOUND ANALYZED AT A DILUTION OF 200
A j S AnalyticalTechnologies,Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED)
6P* 1T-
TEST : VOLATILE ORGANICS (EPA 8240)
ATI I.D. : 10557415
COMPOUNDS RESULTS
TRICHLOROTRIFLUOROETHANE 0(P)-dichlorobenzene
106 9
A-31
AjS AnalyticalTechnologies,Inc
So-)~\ S^S.s--^Sh'
GCMS - RESULTS
ATI I.D. : 10557418
TEST : VOLATILE ORGANICS (EPA 8240)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX : NON-AQUEOUS
MONTGOMERY 662-A HASSAYAMPA 03-004455
& ASSOCIATES DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/02/91 05/02/91 05/05/91 05/11/91 MG/KG
20
COMPOUNDS RESULTS
CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE 2-BUTANONE (MEK) 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE VINYL ACETATE BROMODICHLOROMETHANE 1,1,2,2-TETRACHLOROETHANE 1,2-DICHLOROPROPANE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE CIS-1, 3-DICHLOROPROPENE 2-CHLOROETHYLVINYLETHER BROMOFORM 2-HEXANONE (MBK) 4-METHYL-2-PENTANONE (MIBK) TETRACHLOROETHENE TOLUENE CHLOROBENZENE ETHYLBENZENE STYRENE TOTAL XYLENES
<I0.0 <10.0 <1.0 <1.0
990 <10 <1.0 1630 D 45
0 0 0
<1 <1 <1
405 23000 I <1.0 <10.0 <1.0 <1.0 207 <1.0 590 <1.0 12 1 <1.0 <10.0 <6.0 23 48 560 510 <1.0 57 <1.0 320
SURROGATE PERCENT RECOVERIES
l,2-DICHLOROETHANE-D4 (%) BROMOFLUOROBENZENE (%) T0LUENE-D8 (%)
104 101 91
D INDICATES COMPOUND ANALYZED AT A DILUTION OF2000X A-32
A j S AnalyticalTechnologies,Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED)
A
TEST : VOLATILE ORGANICS (EPA 8240)
ATI I.D. : 10557418
COMPOUNDS
TRICHLOROTRIFLUOROETHANE
RESULTS
12000 D
D INDICATES COMPOUND ANALYZED AT A DILUTION OF2000X
A-33
A K AnalyticalTechnologies,Inc.
GCMS - RESULTS
c,-3-)Cj ^^,5-'^7'
ATI I.D. : 10557419
TEST : VOLATILE ORGANICS (EPA 8 240)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX
MONTGOMERY & ASSOCIATES 562-A HASSAYAMPA 03-004455 NON-AQUEOUS
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/02/91 05/02/91 05/05/91 05/11/91 MG/KG
20
COMPOUNDS RESULTS
CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1, 2-DICHLOROETHANE 2-BUTANONE (MEK) 1 , 1,1-TRICHLOROETHANE CARBON TETRACHLORIDE VINYL ACETATE BROMODICHLOROMETHANE 1 ,1 ,2 ,2-TETRACHLOROETHANE 1 , 2-DICHLOROPROPANE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE DIBROMOCHLOROMETHANE 1,1 ,2-TRICHLOROETHANE BENZENE C I S - 1 , 3 - D I C H L O R O P R O P E N E 2-CHLOROETKYLVINYLETHER BROMOFORM 2-HEXANONE (MBK) 4-METHYL-2-PENTANONE (MIBK) TETRACHLOROETHENE TOLUENE CHLOROBENZENE ETHYLBENZENE STYRENE TOTAL XYLENES
0
0 0 0
<10.0 <10.0 <1.0 <1.0
840 30 <1 550 47 <1 <1 <1 292 18300 <1.0 <10.0 <1.0 <1 160 <1
440 <1 20 <1 <1 <10.0 <6.0 <10.0 43 480 400 <1.0 49 • <1.0 350
D
0
0
0
0 ,0
SURROGATE PERCENT RECOVERIES
l,2-DICHLOROETHANE-D4 (%) BROMOFLUOROBENZENE (%) T0LUENE-D8 (%)
101 109 103
D INDICATES COMPOUND ANALYZED AT A DILUTION OF2000X A-34
^ B - ) " ) S L - ^ - 5 1 >
A N AnalyticalTechnologies,Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED)
TEST : VOLATILE ORGANICS (EPA 824 0)
ATI I.D. : 10557419
COMPOUNDS
TRICHLOROTRIFLUOROETHANE
RESULTS
10500 D
D INDICATES COMPOUND ANALYZED AT A DILUTION OF 2000X
A-35
AjS AnalyticalTechnologies,Inc.
GCMS - RESULTS
^•g>-iT N'7.5--5-Z', 6-5,-,T 2.^i--2i,-
REAGENT BLANK
TEST : VOLATILE ORGANICS (EPA 8240)
CLIENT PROJECT # PROJECT NAME CLIENT I.D.
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA REAGENT BLANK
ATI I.D. DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
105574 05/06/91 05/10/91 MG/KG N/A
COMPOUNDS RESULTS
CHLOROMETKANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1, 2-DICHLOROETHANE 2-BUTANONE (MEK) 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE VINYL ACETATE BROMODICHLOROMETHANE 1,1,2,2-TETRACHLOROETHANE 1, 2-DICHLOROPROPANE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE CIS-1,3-DICHLOROPROPENE 2-CHLOROETHYLVINYLETHER BROMOFORM 2-HEXANONE (MBK) 4-METHYL-2-PENTANONE (MIBK) TETRACHLOROETHENE TOLUENE CHLOROBENZENE ETHYLBENZENE STYRENE TOTAL XYLENES
SURROGATE PERCENT RECOVERIES
l,2-DICHLOROETHANE-D4 (%) BROMOFLUOROBENZENE (%) T0LUENE-D8 (%)
<0 <0 <0 <0 0. <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0
50 50 05 05
50 05 05 05 05 05 05 50 05 05 50 05 05 05 05 05 05 05 05 05 50 3 50 50 05 05 05 05 05 05
103 114 110
A-36
^ X ^ AnalyticalTechnologies
GCMS - RESULTS
Xb.<;c s s-n '^T-^G'
REAGENT BLANK
TEST : VOLATILE ORGANICS (EPA 8240)
CLIENT PROJECT # PROJECT NAME CLIENT I.D.
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA REAGENT BLANK
ATI I.D. DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
105574 05/06/91 05/11/91 MG/KG N/A
COMPOUNDS RESULTS
CHLOROMETKANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE 2-BUTANONE (MEK) 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE VINYL ACETATE BROMODICHLOROMETHANE 1,1,2,2-TETRACHLOROETHANE 1,2-DICHLOROPROPANE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE CIS-1,3-DICHLOROPROPENE 2-CHLOROETHYLVINYLETHER BROMOFORM 2-HEXANONE (MBK) 4-METHYL-2-PENTANONE (MIBK) TETRACHLOROETHENE TOLUENE CHLOROBENZENE ETHYLBENZENE STYRENE TOTAL XYLENES
<0.50 <0.50 <0.05 <0.05 <0.3 <0.50 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.50 <0.05 <0.05 <0.50 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.50 <0.3 <0.50 <0.50 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05
SURROGATE PERCENT RECOVERIES
l,2-DICHLOROETHANE-D4 (%) BROMOFLUOROBENZENE (%) T0LUENE-D8 (%)
96 92 99
A-37
A j S AnalyticalTechnologies,!
6b-1^
QUALITY CONTROL DATA
TEST : VOLATILE ORGANICS (EPA 8240)
CLIENT PROJECT # PROJECT NAME REF I.D.
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA 10557408
ATI I.D.
DATE ANALYZED SAMPLE MATRIX UNITS
! 105574
05/11/91 NON-AQUEOUS MG/KG
COMPOUNDS
DUP. DUP SAMPLE CONC. SPIKED % SPIKED % RESULT SPIKED SAMPLE REC.SAMPLE REC RPD
1,1-DICHLOROETHENE TRICHLOROETHENE CHLOROBENZENE TOLUENE BENZENE
<0.05 <0.05 <0.05 <0.05 <0.05
2.5 2.5 2.5 2.5 2.5
3.0 2.5 2.6 2.5 2.1
120 2.9 104 2.5 104 2.7 100 2.5 84 2.3
115 100 108 100 92
3 4 4 0 9
% Recovery = (Spike Sample Result - Sample Result;
Spike Concentration X 100
RPD (Relative % Difference) = (Spiked Sample - Duplicate Spike) Result Sample Result
Average of Spiked Sample X 100
A-38
AjS AnalyticalTechnologies,Inc.
S>>~I7
ACCESSION: 105574
QUALITY CONTROL DATA; METHOD 824 0
589
CLIENT: MONTGOMERY AND ASSOCIATES UNITS: MG/KG ANALYSIS DATE: 05/10/91
1,1-DICHLOROETHENE CHLOROFORM 1,1,1-TRICHLOROETHANE BROMODICHLOROMETHANE TRICHLOROETHENE TETRACHLOROETHENE CHLOROBENZENE BENZENE TOLUENE
TRUE VALUE
2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5
FOUND
2.6 2.8 2.5 2.6 2.4 2.5 2.7 2.2 2.6
% R
104 112 100 104 96 100 108 88 104
% SURROGATE RECOVERY 112% 1,2-DICHLOROETHANE-D4 110% BROMOFLUOROBENZENE (BFB) 103% TOLUENE - D8
A-39
/f
A j S AnalyticalTechnologies,Inc. ACCESSION: 105574
QUALITY CONTROL DATA: METHOD 8240
589
CLIENT: MONTGOMERY AND ASSOCIATES UNITS: MG/KG ANALYSIS DATE: 05/11/91
1,1-DICHLOROETHENE CHLOROFORM 1,1,1-TRICHLOROETHANE BROMODICHLOROMETHANE TRICHLOROETHENE TETRACHLOROETHENE CHLOROBENZENE BENZENE TOLUENE
TRUE VALUE
2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5
FOUND
2.9 2.6 2.2 2.5 2.5 2.6 2.6 2.1 2.5
% R
116 104 88 100 100 104 104 84 100
% SURROGATE RECOVERY 98% l,2-DICHLOROETHANE-D4 90% BROMOFLUOROBENZENE (BFB) 96% TOLUENE - D8
A-40
I f
A j S AnalyticalTechnologies, Inc. ACCESSION:
5B- n
105574
QUALITY CONTROL DATA: METHOD 824 0
589
CLIENT: MONTGOMERY AND ASSOCIATES UNITS: MG/KG ANALYSIS DATE: 05/13/91
1,1-DICHLOROETHENE CHLOROFORM 1,1,1-TRICHLOROETHANE BROMODICHLOROMETHANE TRICHLOROETHENE TETRACHLOROETHENE CHLOROBENZENE BENZENE TOLUENE
TRUE VALUE
2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5
FOUND
2.7 2.4 2.6 2.7 2.4 2.7 2.6 2.5 2.6
% R
108 96 104 108 96 108 104 100 104
% SURROGATE RECOVERY 93% l,2-DICHLOROETHANE-D4
106% BROMOFLUOROBENZENE (BFB) 100% TOLUENE - D8
A-41
i
A j S AnalyticalTechnologies,Inc.
GCMS - RESULTS
5-b-)-? ^-//
ATI I.D. : 10557401
TEST : METHOD 824 0 (TCLP EXTRACT)
CLIENT PROJECT # PROJECT NAI-IE CLIENT I.D. SAMPLE MATRIX : NON-AQUEOUS
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA 03-004442
DATE SAMPLED DATE RECEIVED ZHE DATE DATE ANALYZED UNITS DILUTION FACTOR
04/30/91 05/02/91 05/08/91 05/17/91 UG/L
10
COMPOUNDS RESULTS
CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1, 2-DICHLOROETHANE 2-BUTANONE (MEK) 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE VINYL ACETATE BROMODICHLOROMETHANE 1,1,2,2-TETRACHLOROETHANE 1, 2-DICHLOROPROPANE TRANS-1,3-DICHLOROPROPENE TRICHLOROETKENE DIBROMOCHLOROMETHANE 1,1, 2-TRICKLOROETHANE BENZENE CIS-1,3-DICHLOROPROPENE 2-CHLOROETHYLVINYLETHER BROMOFORM 2-HEXANONE (MBK) 4-METHYL-2-PENTANONE (MIBK) TETRACHLOROETHENE TOLUENE CHLOROBENZENE ETHYLBENZENE STYRENE TOTAL XYLENES
<100 <100 <10 <10 790 B TR <10
TR 60 <10 <10 <10 <100 30 <10 <100 <10 <10 <10 <10 <i-o <10 <10 <10 <10 <100 <50 <100 <100 100 <10 <10 <10
. <10 30
SURROGATE PERCENT RECOVERIES
l,2-DICHLOROETHANE-D4 (%) BROMOFLUOROBENZENE (%) T0LUENE-D8 (%)
103 102 102
TR - Compound detected at an unquantifiable trace level A-42
s-&-n ?-^ '
A A j S AnalyticalTechnologies, Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED)
TEST : METHOD 824 0 (TCLP EXTRACT)
ATI I.D. : 10557401
COMPOUNDS
0(P)-DICHLOROBENZENE
RESULTS
10
A-43
7 K AnalyticalTechnologies,! nc.
GCMS - RESULTS
^B-JS- S'L
ATI I.D. : 10557402
TEST : METHOD 824 0 (TCLP EXTRACT)
CLIENT . PROJECT # PROJECT NAI4E CLIENT I.D. SAMPLE MATRIX : NON-AQUEOUS
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA 03-004447
DATE SAMPLED DATE RECEIVED ZHE DATE DATE ANALYZED UNITS DILUTION FACTOR
05/01/91 05/02/91 05/08/91 05/17/91 UG/L
10
COMPOUNDS RESULTS
CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1, 2-DICHLOROETHANE 2-BUTANONE (MEK) 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE VINYL ACETATE BROMODICHLOROMETHANE 1,1,2,2-TETRACHLOROETHANE 1,2-DICKLOROPROPANE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE CIS-1,3-DICHLOROPROPENE 2-CHLOROETHYLVINYLETHER BROMOFORM 2-HEXANONE (MBK) 4-METHYL-2-PENTANONE (MIBK) TETRACHLOROETHENE TOLUENE CHLOROBENZENE ETHYLBENZENE STYRENE TOTAL XYLENES
<100 <100 <10 <10
60 B TR <10 60 710 <10 <10 <10 <100 1300 <10 <100 <10 <10 60 <10 70 <10 <10 <10 <10 <100 <50 <100 <100 540 <10 <10 <10
• <10 20
SURROGATE PERCENT RECOVERIES
l,2-DICHLOROETHANE-D4 (%) BROMOFLUOROBENZENE (%) T0LUENE-D8 (%)
96 99 100
A-44 TR - Compound detected at an unquantifiable trace level
t>lb~rd S-L '
A / j \ AnalyticalTechnologies,Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED)
TEST : METHOD 8240 (TCLP EXTRACT)
ATI I.D. : 10557402
COMPOUNDS RESULTS
TRICHLOROTRIFLUOROETHANE 0 ( P)-DICHLOROBENZENE
90 20
A-45
AjS AnalyticalTechnologies,
GCMS - RESULTS
5"B-i§' 0 - 1 ^ ' 5Ptr\T
ATI I.D. 10557403
TEST : METHOD 8 24 0 (TCLP EXTRACT;
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX : NON-AQUEOUS
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA 03-004447 DUPLICATE
DATE SAMPLED DATE RECEIVED ZHE DATE DATE ANALYZED UNITS DILUTION FACTOR
05/01/91 05/02/91 05/08/91 05/18/91 UG/L
10
COMPOUNDS RESULTS
CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE 1,1-DICHLOROETHANE 1,2-DICKLOROETKENE (TOTAL) CHLOROFORM 1, 2-DICHLOROETHANE 2-BUTANONE (MEK) 1,1 ,1-TRICHLOROETHANE CARBON TETRACHLORIDE VINYL ACETATE BROMODICHLOROMETHANE 1,1 ,2 ,2-TETRACHLOROETHANE 1,2-DICHLOROPROPANE TRANS-1,3-DICKLOROPROPENE TRICHLOROETHENE DIBROMOCHLOROMETHANE 1 ,1 ,2-TRICHLOROETHANE BENZENE CIS-1, 3-DICHLOROPROPENE 2-CHLOROETHYLVINYLETHER BROMOFORM 2-HEXANONE (MBK) 4-METHYL-2-PENTANONE (MIBK) TETRACHLOROETHENE TOLUENE CHLOROBENZENE ETHYLBENZENE STYRENE TOTAL XYLENES
SURROGATE PERCENT RECOVERIES
l,2-DICHLOROETHANE-D4 (%) BROMOFLUOROBENZENE (%) T0LUENE-D8 (%)
<100 <100 <10 <10
470 B TR <10 60 690 <10 <10 <10 <100 1200 <10 <100 <10 <10 50 <10 60 <10 <10 <10 <10 <100 <50 <100 <100 500 <10 <10 <10
• <10 40
108 100 101
TR - Compound detected at an unquantifiable trace level A-46
^^-Zg" 5 - - ^ ' ^ P H )
A A j S AnalyticalTechnologies,Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED;
TEST : METHOD 8240 (TCLP EXTRACT)
ATI I.D. : 10557403
COMPOUNDS RESULTS
TRICHLOROTRIFLUOROETHANE 0( P)-DICHLOROBENZENE
90 30
A-47
^ X ^ AnalyticalTechnologies, Ir
^ - ) < i y - 5
GCMS - RESULTS
ATI I.D. : 10557406
TEST : METHOD 824 0 (TCLP EXTRACT)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA 03-004449 NON-AQUEOUS
DATE SAMPLED DATE RECEIVED ZHE DATE' DATE ANALYZED UNITS DILUTION FACTOR
05/02/91 05/02/91 05/08/91 05/17/91 UG/L 1000
COMPOUNDS RESULTS
CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE 1, 1-DICHLOROETHANE 1, 2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE 2-BUTANONE (MEK) 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE VINYL ACETATE BROMODICHLOROMETHANE 1,1,2,2-TETRACHLOROETHANE 1 , 2-DICHLOROPROPANE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE CIS-1,3-DICHLOROPROPENE 2-CHLOROETHYLVINYLETHER BROMOFORM 2-HEXANONE (MBK) 4-METHYL-2-PENTANONE (MIBK) TETRACHLOROETHENE TOLUENE CHLOROBENZENE ETHYLBENZENE STYRENE TOTAL XYLENES
SURROGATE PERCENT RECOVERIES-
l,2-DICHLOROETKANE-D4 (%) BROMOFLUOROBENZENE (%) T0LUENE-D8 (%)
<10000 <10000 <1000 <1000 20000 B 32000 <1000 3000 8000 <1000 <1000 <1000
TR 220000 <1000 <10000 <1000 <1000
4000 <1000 IOOOO <1000
TR <1000 <1000 <10000 <5000 <10000
TR 9000 13000 <1000 <1000 <1000 3000
114 85 98
A-48 TR - Compound detected at an unquantifiable trace level
5 ^ n S'" '
A AjS AnalyticalTechnologies,Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED)
TEST : METHOD 8240 (TCLP EXTRACT)
ATI I.D. : 10557406
COMPOUNDS
TRICHLOROTRIFLUOROETHANE
RESULTS
13000
A-49
A j S AnalyticalTechnologies, I
GCMS - RESULTS
^ ^ - ) i \ D - 1 5 '
ATI I.D, 10557407
TEST : METHOD 824 0 (TCLP EXTRACT)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX : NON-AQUEOUS
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA 03-004450
DATE SAMPLED DATE RECEIVED ZHE DATE DATE ANALYZED UNITS DILUTION FACTOR
05/02/91 05/02/91 05/08/91 05/18/91 UG/L
50
COMPOUNDS RESULTS
CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1, 2-DICHLOROETKANE 2-BUTANONE (MEK) 1,1 ,1-TRICHLOROETHANE CARBON TETRACHLORIDE VINYL ACETATE BROMODICHLOROMETHANE 1,1 ,2 ,2-TETRACHLOROETHANE 1 , 2-DICHLOROPROPANE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE DIBROMOCHLOROMETHANE 1,1 ,2-TRICHLOROETHANE BENZENE C I S - 1 , 3-DICHLOROPROPENE 2-CHLOROETKYLVINYLETHER BRO-MOFORM 2-HEXANONE (MBK) 4-METHYL-2-PENTANONE (MIBK) TETRACHLOROETHENE TOLUENE CHLOROBENZENE ETHYLBENZENE STYRENE TOTAL XYLENES
<500 <500 <50 <50 880 B 1800 <50 <50 <50 <50 <50 <50 <500 800 <50 <500 <50 <50 <50 <50 200 <50 <50 <50 <50 <500 <250 <500 <500 1500 790 <50 200 • <50 1000
SURROGATE PERCENT RECOVERIES
l,2-DICHLOROETHANE-D4 (%) BROMOFLUOROBENZENE (%) T0LUENE-D8 (%)
A-50
122 98 102
5-&-)^ ) b - ) S '
/ ^ AnalyticalTechnologies, Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED;
TEST : METHOD 8 24 0 (TCLP EXTRACT)
ATI I.D. : 10557407
COMPOUNDS RESULTS
0(P)-DICHLOROBENZENE 100
A-51
/ \ AnalyticalTechnologies, Inc
GCMS - RESULTS
i-Tb-n, ^fb-^t , s~&-n
ATI I . D . 1 0 5 5 7 4 2 0
TEST : METHOD 8 24 0 (TCLP EXTRACT)
CLIENT PROJECT # PROJECT NAME CLIENT I . D . SAMPLE MATRIX
MONTGOMERY & ASSOCIATES 6 6 2 - A HASSAYAMPA ZHE REAGENT BLANK NON-AQUEOUS
DATE SAMPLED DATE RECEIVED ZHE DATE DATE ANALYZED UNITS DILUTION FACTOR
05/08/91 05/02/91 05/08/91 05/17/91 UG/L
10
COMPOUNDS RESULTS
CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1, 2-DICHLOROETHANE 2-BUTANONE (MEK) 1,1 ,1-TRICHLOROETHANE CARBON TETRACHLORIDE VINYL ACETATE BROMODICHLOROMETHANE 1,1 ,2 ,2-TETRACHLOROETHANE 1 , 2-DICHLOROPROPANE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE DIBROMOCHLOROMETHANE 1,1 ,2-TRICKLOROETHANE BENZENE C I S - 1 , 3-DICHLOROPROPENE 2-CHLOROETKYLVINYLETHER BROMOFORJ-I 2-HEXANONE (MBK) 4-METHYL-2-PENTANONE (MIBK) TETRACHLOROETHENE TOLUENE CHLOROBENZENE ETHYLBENZENE STYRENE TOTAL XYLENES
SURROGATE PERCENT RECOVERIES
l,2-DICKLOROETHANE-D4 (%) BROMOFLUOROBENZENE (%) T0LUENE-D8 (%)
A-52
<100 <100 <10 <10 50 <100 <10 <10 <10 <10 <10 <10 <100 <10 <10 <100 <10 <10 <10 <10 <10 <10 <10 <10 <10 <100 <50 <100 <100 <10 <10 <10 <10
• <10 <10
109 84 99
A AjS AnalyticalTechnologies, Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED)
TEST : METHOD 824 0 (TCLP EXTRACT)
ATI I.D. : 10557420
^ • a , - i 5 ( , 5"?>-/<=t
COMPOUNDS
NO ADDITIONAL COMPOUNDS
RESULTS
<50
A-53
A j S AnalyticalTechnologies,Inc.
GCMS - RESULTS
REAGENT BLANK
TEST : METHOD 8 240 (TCLP EXTRACT)
CLIENT PROJECT # PROJECT NAME CLIENT I.D.
MONTGOMERY & ASSOCIATES 652-A HASSAYAMPA REAGENT BLANK
ATI I.D. DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
105574 05/16/91 05/15/91 UG/L N/A
COMPOUNDS RESULTS
CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE 2-BUTANONE (MEK) 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE VINYL ACETATE BROMODICHLOROMETHANE 1,1,2,2-TETRACHLOROETHANE 1,2-DICHLOROPROPANE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE CIS-1,3-DICHLOROPROPENE 2-CHLOROETHYLVINYLETHER BROMOFORM 2-HEXANONE (MBK) 4-METHYL-2-PENTANONE (MIBK) TETRACHLOROETHENE TOLUENE CHLOROBENZENE ETHYLBENZENE STYRENE TOTAL XYLENES
<10 <10 <1 <1 TR <10 <1 <1 <1 <1 <1 <1 <10 <1 <1 <10 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 <10 <5 <10 <10 <1 <1 <1 <1 <1 <1
SURROGATE PERCENT RECOVERIES
l,2-DICHLOROETHANE-D4 (%) BROMOFLUOROBENZENE (%) T0LUENE-D8 (%)
99 88 102
A-54
AjS AnalyticalTechnologies,!
•Si- I t ^ - < ^ ' , -Ti.,-^ ^ - -c - -irui-, ^-I'i ?-*?'_, 5B-/<; I O - I 5 '
GCMS - RESULTS
REAGENT BLANK
TEST : METHOD 8240 (TCLP EXTRACT)
CLIENT PROJECT # PROJECT NAME CLIENT I.D.
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA REAGENT BLANK
ATI I.D. DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
105574 05/17/91 05/17/91 UG/L N/A
COMPOUNDS RESULTS
CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE r,1-DICHLOROETHENE 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE 2-BUTANONE (MEK) 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE VINYL ACETATE ' BROMODICHLOROMETHANE 1,1,2,2-TETRACHLOROETHANE 1,2-DICHLOROPROPANE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE CIS-1,3-DICHLOROPROPENE 2-CHLOROETHYLVINYLETHER BROMOFORM 2-HEXANONE (MBK) 4-METHYL-2-PENTANONE (MIBK) TETRACHLOROETHENE TOLUENE CHLOROBENZENE ETHYLBENZENE STYRENE TOTAL XYLENES
SURROGATE PERCENT RECOVERIES
l,2-DICHLOROETHANE-D4 (%) BROMOFLUOROBENZENE (%) T0LUENE-D8 (%)
<10 <10 <1 <1 <5 <10 <1 <1 <1 <1 <1 <1 <10 < 1 <1 <10 < 1 < 1 < 1 < 1 < 1 < 1 <1 <1 <1 <10 <5 <10 <10 <1 <1 <1 < 1 < 1 < 1
102 98 102
A-55
A j S AnalyticalTechnologies,Inc.
QUALITY CONTROL DATA
TEST : METHOD 8240 (TCLP EXTRACT)
CLIENT PROJECT # PROJECT NAME REF I.D.
MONTGOMERY & ASSOCIATES 562-A HASSAYAMPA 10599923
ATI I.D, : 105574
DATE ANALYZED : 05/17/91 SAMPLE MATRIX : UNITS : UG/L
COMPOUNDS
DUP. DUP SAMPLE CONC. SPIKED % SPIKED % RESULT SPIKED SAMPLE REC.SAMPLE REC RPD
1,1-DICHLOROETHENE TRICHLOROETHENE CHLOROBENZENE TOLUENE BENZENE
<1 <1 <1 <1 <1
50 50 50 50 50
55 49 51 51 41
110 54 98 48 102 51 102 51 82 41
108 95 102 102 82
2 2 0 0 0
% Recovery = (Spike Sample Result - Sample Result)
Spike Concentration X 100
RPD (Relative % Difference) = (Spiked Sample - Duplicate Spike) Result Sample Result
Average of Spiked Sample
TR - Compound detected at an unquantifiable trace level
X 100
A-56
2 H e
AjS AnalyticalTechnologies,Inc. ACCESSION: 105574
QUALITY CONTROL DATA: METHOD 824 0
589
CLIENT: MONTGOMERY AND ASSOCIATES UNITS: UG/L ANALYSIS DATE: 05/16/91
1,1-DICHLOROETHENE CHLOROFORM 1,1,1-TRICHLOROETHANE BROMODICHLOROMETHANE TRICHLOROETHENE TETRACHLOROETHENE CHLOROBENZENE BENZENE TOLUENE
TRUE VALUE
50 50 50 50 50 50 50 50 50
FOUND
51 48 50 48 48 53 50 40 50
% R
102 96 100 96 96 106 100 80 100
% SURROGATE RECOVERY 100% l,2-DICHLOROETHANE-D4 93% BROMOFLUOROBENZENE (BFB) 101% TOLUENE - D8
A-57
#
A \ AnalyticalTechnologies, 1 ACCESSION: 105574
QUALITY CONTROL DATA: 589 METHOD 824 0
CLIENT: MONTGOMERY AND ASSOCIATES UNITS: UG/L ANALYSIS DATE: 05/17/91
1,1-DICHLOROETHENE CHLOROFORM 1,1,1-TRICHLOROETHANE BROMODICHLOROMETHANE TRICHLOROETHENE TETRACHLOROETHENE CHLOROBENZENE BENZENE TOLUENE
TRUE VALUE
50 50 50 50 50 50 50 50 50
FOUND
56 61 48 48 49 53 51 41 52
% R
112 122 96 96 98 106 102 82 104
% SURROGATE RECOVERY 116% l,2-DICHLOROETHANE-D4 101% BROMOFLUOROBENZENE (BFB) 100% TOLUENE - D8
A-58
- a
A j S AnalyticalTechnologies
sB-n zq.5-3o
GCMS - RESULTS
ATI I.D. 10557408
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
CLIENT PROJECT # PROJECT NAMS CLIENT I.D. SAMPLE MATRIX
MONTGOMERY & ASSOCIATES 552-A HASSAYAMPA 03-004444 NON-AQUEOUS
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
04/30/91 05/02/91 05/07/91 05/17/91 MG/KG
1
COMPOUNDS RESULTS
N-NITROSODIMETHYLAMINE PHENOL ANILINE BIS(2-CHLOROETHYL)ETHER 2-CHLOROPHENOL 1, 3-DICHLOROBENZENE 1, 4-DICHLOROBENZENE BENZYL ALCOHOL 1, 2-DICHLOROBENZENE 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL)ETHER 4-METHYLPHENOL N-NITROSO-DI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2 , 4-DIMETHYLPHENOL BENZOIC ACID BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOP ENTADIENE 2,4, 6-TRICHLOROPHENOL 2 , 4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYLPHTHALATE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE 2,5-DINITROTOLUENE
<0. <0. <0. <0. <0. <0. <0. <0. <0. <0. <0. <0. <0. <0. <0. <0 <0. <0. <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0
17 17 17 17 17 17 17 17 17 17 17 17 17 17 17 17 17 17 85 17 17 17 17 17 17 .17 .17 .17 .17 .85 .17 .85 .17 .17 .85 .17 .85 .85 .17 .17 .17
A-59 (CONTINUED NEXT PAGE)
A j S AnalyticalTechnologies,Inc.
GCMS - RESULTS ATI I.D.
s^~n z^.S'3o'
10557408
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
COMPOUNDS RESULTS
DIETHYLPHTHALATE 4-CHLOROPHENYL-PHENYLETHER FLUORENE 4-NITROANILINE 4,6-DINITRO-2-METHYLPHENOL N-NITROSODIPHENYLAMINE 4-BROMOPHENYL-PHENYLETHER HEXACHLOROBENZENE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE DI-N-BUTYLPHTHALATE FLUORANTHENE BENZIDINE PYRENE BUTYLBENZYLPHTHALATE 3,3-DICHLOROBENZIDINE BENZO(a)ANTHRACENE BIS(2-ETHYLHEXYL)PHTHALATE CHRYSENE DI-N-OCTYLPHTHALATE BENZO(b)FLUORANTHENE BENZO(k)FLUORANTHENE BEN20(a)PYRENE INDENO(1,2,3-cd)PYRENE DIBENZO(a,h)ANTHRACENE BENZO(g,h,i)PERYLENE
<0. <0. <0. <0. <0. <0. <0. <0. <0. <0. <0. <0, <0, <1, <0. <0, <0, <0, <0, <0, <0, <0, <0, <0, <0 <0 <o.
17 17 17 85 85 17 17 17 85 17 17 17 17 7 17 17 34 17 17 17 17 17 17 17 17 17 17
SURROGATE PERCENT RECOVERIES
NITROBENZENE-DS (%) 2-FLUOROBIPHENYL (%) TERPHENYL (%) PHEN0L-D6 (%) 2-FLUOROPHENOL (%) 2,4,6-TRIBROMOPHENOL (%)
56 57 77 42 51 39
A-60
5 i2,-]7 ^"^ '^ ' ^ '
AJS AnalyticalTechnologies,Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED)
A
TEST : SEMI-VOLATILE ORGANICS (EPA 8 270)
ATI I.D. : 10557408
COMPOUNDS
NO ADDITIONAL COMPOUNDS
RESULTS
<1
A-61
A j S AnalyticalTechnologies,I
613-n \<^.5'-20'
GCMS - RESULTS
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MJi TRIX : NON-AQUEOUS
MONTGOMERY & ASSOCIATES 552-A HASSAYAMPA 03-004443
ATI I.D. : 10557409
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
04/30/91 05/02/91 05/07/91 05/17/91 MG/KG
1
COMPOUNDS RESULTS
N-NITROSODIMETHYLAMINE PHENOL ANILINE BIS(2-CHLOROETHYL)ETHER 2-CHLOROPHENOL 1, 3-DICHLOROBENZENE 1,4-DICHLOROBENZENE BENZYL ALCOHOL 1, 2-DICHLOROBENZENE 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL)ETHER 4-METHYLPHENOL N-NITROSO-DI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BENZOIC ACID BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE 2,4,5-TRICHLOROPHENOL 2 , 4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYLPHTHALATE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE 2, 4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE 2,5-DINITROTOLUENE
<0. <0. <0. <0. <0. <0. <0, <0. <0. <0. <0. <0. <0. <0. <0. <0. <0. <0. <0. <0. <0. <0. <0. <0, <0, <0, <0, <0, <0. <0.
<o. <0, <0, <o. <o. <0 <0 <0 <0 <0
17 17 17 17 17 17 17 17 17 17 17 17 17 17 17 17 17 17 85 17 17 17 17 17 17 17 17 17 17 85 17 85 17 17 85 17 85 85 17 .17
<0.17 A-62
(CONTINUED NEXT PAGE)
A j S AnalyticalTechnologies,Inc.
GCMS - RESULTS ATI I.D,
5^-)-7 \ ^ i 5 ~ ' 2 6 '
10557409
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
COMPOUNDS RESULTS
DIETHYLPHTHALATE 4-CHLOROPHENYL-PHENYLETHER FLUORENE 4-NITROANILINE 4 , 6-DINITRO-2-METHYLPHENOL N-NITROSODIPHENYLAMINE 4-BROMOPHENYL-PHENYLETHER HEXACHLOROBENZENE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE DI-N-BUTYLPHTHALATE FLUORANTHENE BENZIDINE PYRENE BUTYLBENZYLPHTHALATE 3,3-DICHLOROBENZIDINE BENZO(a)ANTHRACENE BIS(2-ETHYLHEXYL)PHTHALATE CHRYSENE DI-N-OCTYLPHTHALATE BENZO(b)FLUORANTHENE BENZO(k)FLUORANTHENE BENZO(a)PYRENE INDENO(1,2,3-cd)PYRENE DIBENZO(a,h)ANTHRACENE BENZO(g,h,i)PERYLENE
<0.17 <0.17 <0.17 <0.85 <0.85 <0.17 <0.17 <0.17 <0. <0, <0, <0, <0, <1, <0, <0, <0. <0. <0, <0, <0 <0 <0 <0 <0 <0 <0
85 17 17 17 17 7 17 17 34 17 17 17 17 17 17 17 17 17 17
SURROGATE PERCENT RECOVERIES
NITROBENZENE-DS (%) 2-FLUOROBIPHENYL (%) TERPHENYL (%) PHEN0L-D6 (%) 2-FLUOROPHENOL (%) 2,4,6-TRIBROMOPHENOL (%)
75 66 80 48 59 36
A-63
AJS AnalyticalTechnologies, Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED) A
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
ATI I.D. : 10557409
COMPOUNDS
NO ADDITIONAL COMPOUNDS
RESULTS
<1
A-64
A j S AnalyticalTechnologies,
GCMS - RESULTS
6h-n Z^i-T-'iO .. I
ATI I.D. 10557410
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE M-ATRIX
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA 03-004445 NON-AQUEOUS
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
04/30/91 05/02/91 05/07/91 05/17/91 MG/KG
1
COMPOUNDS RESULTS
N-NITROSODIMETHYLAMINE PHENOL ANILINE BIS(2-CKLOROETHYL)ETHER 2-CKLOROPHENOL 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE BENZYL ALCOHOL 1,2-DICHLOROBENZENE 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL)ETHER 4-METHYLPHENOL N-NITROSO-DI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BENZOIC ACID BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYLPHTHALATE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE 2, 6-DINITROTOLUENE
<0.17 0.7 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.85 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.8S <0.17 <0.85 <0.17 <0.17 <0.85 <0.17 <0.85 <0.85 <0.17 <0.17 <0.17
(CONTINUED NEXT PAGE) A-65
A j S AnalyticalTechnologies, nc.
GCMS - RESULTS ATI I . D .
s i b - n 3^.X-^o'
1 0 5 5 7 4 1 0
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
COMPOUNDS RESULTS
DIETHYLPHTHALATE 4-CHLOROPHENYL-PHENYLETHER FLUORENE 4-NITROANILINE 4,6-DINITRO-2-METHYLPHENOL N-NITROSODIPHENYLAMINE 4-BROMOPHENYL-PHENYLETHER HEXACHLOROBENZENE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE DI-N-BUTYLPHTHALATE FLUORANTHENE BENZIDINE PYRENE BUTYLBENZYLPHTHALATE 3, 3-DICHLOROBENZIDINE BENZO(a)ANTHRACENE BIS(2-ETHYLHEXYL)PHTHALATE CHRYSENE DI -N-OCTYLPHTHALATE BENZO(b)FLUORANTHENE BENZO(k)FLUORANTHENE BENZO(a)PYRENE INDENO(1,2,3-cd)PYRENE DIBENZO(a,h)ANTHRACENE BENZO(g,h,i)PERYLENE
< 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 8 5 < 0 . 8 5 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 8 5 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 1 . 7 <0 . 17 < 0 . 1 7 < 0 . 3 4 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7
SURROGATE PERCENT RECOVERIES
NITROBENZENE-DS (%) 2-FLUOROBIPHENYL (%) TERPHENYL (%) PHEN0L-D6 (%) 2-FLUOROPHENOL (%) 2,4,6-TRIBROMOPHENOL %)
74 55 69 55 62 41
A-66
6 ^ - i l l > q . 5 " - v c '
AjS AnalyticalTechnologies,Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED)
A
TEST : SEMI-VOLATILE ORGANICS (EPA 8 270)
ATI I.D. : 10557410
COMPOUNDS
NO ADDITIONAL COMPOUNDS
RESULTS
<1
A-67
AjS AnalyticalTechnologies,lr 613-n s^-r-5z:'
GCMS - RESULTS
ATI I.D. 10557411
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX : NON-AQUEOUS
MONTGOMERY 662-A HASSAYAMPA 03-004446
& ASSOCIATES DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/01/91 05/02/91 05/07/91 05/17/91 MG/KG
1
COMPOUNDS RESULTS
N-NITROSODIMETHYLAMINE PHENOL ANILINE BIS(2-CHLOROETHYL)ETHER 2-CHLOROPHENOL 1, 3-DICHLOROBENZENE 1, 4-DICHLOROBENZENE BENZYL ALCOHOL 1,2-DICHLOROBENZENE 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL)ETHER 4-METHYLPHENOL N-NITROSO-DI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BENZOIC ACID BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL 1, 2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE 2,4,5-TRICHLOROPHENOL 2,4, 5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYLPHTHALATE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE 2,6-DINITROTOLUENE
<0. <0. <0. <0. <0. <0. <0. <0. <o. <0. <0. <0. <0. <0. <0. <0. <0. <0. <0, <0, <0. <0. <0, <0, <0, <0, <0. <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0
17 17 17 17 17 17 17 17 17 17 17 17 17 17 17 17 17 17 85 17 17 17 17 17 17 17 17 17 17 85 17 85 17 17 85 17 .85 ,85 .17 ,17 ,17
(CONTINUED NEXT PAGE) A-68
/ \ AnalyticalTechnologies,!
GCMS - RESULTS ATI I . D .
6 1 b - ) l H' i .3--ST-
1 0 5 5 7 4 1 1
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
COMPOUNDS RESULTS
DIETHYLPHTHALATE 4-CHLOROPHENYL-PHENYLETHER FLUORENE 4-NITROANILINE 4 , 6-DINITRO-2-METHYLPHENOL N-NITROSODIPHENYLAMINE 4-BROMOPHENYL-PHENYLETHER HEXACHLOROBENZENE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE DI-N-BUTYLPHTHALATE FLUORANTHENE BENZIDINE PYRENE BUTYLBENZYLPHTHALATE 3,3-DICHLOROBENZIDINE BENZO(a)ANTHRACENE BIS(2-ETHYLHEXYL)PHTHALATE CHRYSENE DI-N-OCTYLPHTHALATE BENZO(b)FLUORANTHENE BENZO(k)FLUORANTHENE BENZO(a)PYRENE INDENO(1,2,3-cd)PYRENE DIBENZO(a,h)ANTHRACENE BENZO(g,h,i)PERYLENE
SURROGATE PERCENT RECOVERIES
<0. <0. <0. <0. <0. <0. <0. <0. <0. <0. <0, <0, <0. < 1 , <0, <0, <0, <0, <0, <0. <0, <0 <o. <0 <0. <0 <0
17 17 17 85 85 17 17 17 85 17 17 17 17 7 17 17 34 17 17 17 17 17 17 17 17 17 17
NITROBENZENE-DS (%) 2-FLUOROBIPHENYL (%) TERPHENYL (%) PHEN0L-D6 (%) 2-FLUOROPHENOL (%) 2,4,6-TRIBROMOPHENOL (%)
56 50 71 37 45 31
A-69
A j S AnalyticalTechnologies, Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED)
A
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
ATI I.D. : 10557411
COMPOUNDS
NO ADDITIONAL COMPOUNDS
RESULTS
<1
A-70
A j S AnalyticalTechnologies,Inc
6 '^- l ' l 2^-5--25"
GCMS - RESULTS
ATI I.D. : 10557412
TEST : SEMI-VOLATILE ORGANICS (EPA 827 0)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA 03-004451 NON-AQUEOUS
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/02/91 05/02/91 05/07/91 05/17/91 MG/KG
20
COMPOUNDS RESULTS
N-NITROSODIMETHYLAMINE PHENOL ANILINE BIS(2-CHLOROETHYL)ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1,4-DICKLOROBENZENE BENZYL ALCOHOL 1,2-DICHLOROBENZENE 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL)ETHER 4-METHYLPHENOL N-NITROSO-DI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BENZOIC ACID BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE 2,4,5-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYLPHTHALATE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE 2,5-DINITROTOLUENE
<3.4 17 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3 <3 <3.4 <3.4 <17.0 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <17.0 <3.4 <17.0 <3.4 <3.4 <17.0 <3.4 <17.0 <17.0 <3.4 <3.4 <3.4
A-71 (CONTINUED NEXT PAGE)
A i S AnalyticalTechnologies,Inc.
GCMS - RESULTS ATI I . D ,
5^-'"i 2H-T-2S
1 0 5 5 7 4 1 2
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
COMPOUNDS RESULTS
DIETHYLPHTHALATE 4-CHLOROPHENYL-PHENYLETHER FLUORENE 4-NITROANILINE 4,5-DINITRO-2-METHYLPHENOL N-NITROSODIPHENYLAMINE 4-BROMOPHENYL-PHENYLETHER HEXACHLOROBENZENE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE DI-N-BUTYLPHTHALATE FLUORANTHENE BENZIDINE PYRENE BUTYLBENZYLPHTHALATE 3,3-DICHLOROBENZIDINE BENZO(a)ANTHRACENE BIS(2-ETHYLHEXYL)PHTHALATE CHRYSENE DI-N-OCTYLPHTHALATE BENZO(b)FLUORANTHENE BENZO(k)FLUORANTHENE BENZO(a)PYRENE INDENO(1,2,3-cd)PYRENE DIBENZO(a,h)ANTHRACENE BENZO(g,h,i)PERYLENE
<3.4 <3.4 <3.4 <17.0 <17.0 <3.4 <3.4 <3.4 <17.0 <3.4 <3.4 <3.4 <3.4 <34.0 <3.4 <3.4 <6.8 <3.4 <3.4 <3.4 <3 <3
4 4
<3.4 <3.4 <3 <3 <3
SURROGATE PERCENT RECOVERIES
NITROBENZENE-DS (%) 2-FLUOROBIPHENYL (%) TERPHENYL (%) PHEN0L-D6 (% ) 2-FLUOROPHENOL (%) 2,4,6-TRIBROMOPHENOL (%)
76 84 75 19 53 18
A-72
A j S AnalyticalTechnologies, Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED)
A
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
ATI I.D. : 10557412
COMPOUNDS RESULTS
OXYGENATED HYDROCARBON C7 TOTAL ORGANIC ACIDS TOTAL EXTRACTABLE HYDROCARBONS C8-C20
200 300
200
I I
I
A-73
A j S AnalyticalTechnologies
GCMS - RESULTS
6~b-\^ • 3 S , S '
ATI I.D. 10557413
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX : NON-AQUEOUS
MONTGOMERY 652-A HASSAYAMPA 03-004452
& ASSOCIATES DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/02/91 05/02/91 05/07/91 05/17/91 MG/KG
20
COMPOUNDS RESULTS
N-NITROSODIMETHYLAMINE PHENOL ANILINE BIS(2-CHLOROETHYL)ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE BENZYL ALCOHOL 1,2-DICHLOROBENZENE 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL)ETHER 4-METHYLPHENOL N-NITROSO-DI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BENZOIC ACID BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOP ENTADIENE 2,4,5-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYLPHTHALATE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE 2,5-DINITROTOLUENE
<3.4 25 <3.4 <3.4 <3 <3 <3 <3 <3 4 <3
4 <3 <3 <3 <3 <3 <3.4 <17.0 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <17.0 <3.4 <17.0 <3.4 <3.4 <17.0 <3.4 <17.0 <17.0 <3.4 <3.4 <3.4
0
(CONTINUED NEXT PAGE) A-74
I
AjS AnalyticalTechnologies,Inc.
GCMS - RESULTS ATI I.D,
6?>-'=i 35"-350
10557413
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
COMPOUNDS RESULTS
i
DIETHYLPHTHALATE 4-CHLOROPHENYL-PHENYLETHER FLUORENE 4-NITROANILINE 4,5-DINITRO-2-METHYLPHENOL N-NITROSODIPHENYLAMINE 4-BROMOPHENYL-PHENYLETHER HEXACHLOROBENZENE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE DI-N-BUTYLPHTHALATE FLUORANTHENE BENZIDINE PYRENE BUTYLBENZYLPHTHALATE 3,3-DICHLOROBENZIDINE BENZO(a)ANTHRACENE BIS(2-ETHYLHEXYL)PHTHALATE CHRYSENE DI-N-OCTYLPHTHALATE BENZO(b)FLUORANTHENE BENZO(k)FLUORANTHENE BENZO(a)PYRENE INDENO(1,2,3-cd)PYRENE DIBENZO(a,h)ANTHRACENE BENZO(g,h,i)PERYLENE
<3.4 <3.4 <3.4 <17.0 <17.0 <3.4 <3.4 <3.4 <17.0 <3.4 <3.4 <3.4 <3.4 <34.0 <3.4 <3.4 <5.8 <3.4 <3 <3 <3 <3 <3 <3 <3.4 <3.4 <3.4
SURROGATE PERCENT RECOVERIES
NITROBENZENE-DS (%) 2-FLUOROBIPHENYL (%) TERPHENYL (%) PHEN0L-D5 (%) 2-FLUOROPHENOL (%) 2,4,6-TRIBROMOPHENOL (%)
45 43 49 52 47 22
A-75
i / j j ^ AnalyticalTechnologies, Inc. IU
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
ATI I.D. : 10557413
COMPOUNDS RESULTS
OXYGENATED HYDROCARBON C7 200 TOTAL ORGANIC ACIDS 500 TOTAL EXTRACTABLE HYDROCARBONS C8-C20 700
0
n
I I B I I I
A-75
AjS AnalyticolTechnologies,Inc.
4"B-i^ l 5 - - ^ i
GCMS - RESULTS
ATI I.D. : 10557414
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA 03-004453 NON-AQUEOUS
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/02/91 05/02/91 05/07/91 05/17/91 MG/KG
20
COMPOUNDS RESULTS
N-NITROSODIMETHYLAMINE PHENOL ANILINE BIS(2-CHLOROETHYL)ETHER 2-CHLOROPHENOL 1, 3-DICHLOROBENZENE 1, 4-DICHLOROBENZENE BENZYL ALCOHOL 1, 2-DICHLOROBENZENE 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL)ETHER 4-METHYLPHENOL N-NITROSO-DI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BENZOIC ACID BIS(2-CHL0R0ETH0XY)METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOP ENTADIENE 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYLPHTHALATE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE 2,6-DINITROTOLUENE
<3.4 10 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 4 TR <3 <3 <3 <3 <3.4 <3.4 <3.4 <3.4 <17.0 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <17.0 <3.4 <17.0 <3.4 <3.4 <17.0 <3.4 <17.0 <17.0 <3.4 <3.4 <3.4
TR - Compound detected at an unquantifiable trace level (CONTINUED NEXT PAGE)
A-77
AjS AnalyticalTechnologies,lnc.
GCMS - RESULTS
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
ATI I.D.
^ I i> - l9 H6~-^6'
10557414
COMPOUNDS RESULTS
DIETHYLPHTFJ^iATE 4-CHLOROPHENYL-PHENYLETHER FLUORENE 4-NITROANILINE 4, 6-DINITRO-2-METHYLPHENOL N-NITROSODIPHENYLAMINE 4-BROMOPHENYL-PHENYLETHER HEXACHLOROBENZENE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE DI-N-BUTYLPHTHALATE FLUORANTHENE BENZIDINE PYRENE BUTYLBENZYLPHTHALATE 3,3-DICHLOROBENZIDINE BENZO(a)ANTHRACENE BIS(2-ETHYLHEXYL)PHTHALATE CHRYSENE DI-N-OCTYLPHTHALATE BENZO(b)FLUORANTHENE BENZO(k)FLUORANTHENE BENZO(a)PYRENE INDENO(1,2,3-cd)PYRENE DIBENZO(a,h)ANTHRACENE BENZO(g,h,i)PERYLENE
< 3 . 4 < 3 . 4 < 3 . 4 < 1 7 . 0 < 1 7 . 0 < 3 . 4 < 3 . 4 < 3 . 4 < 1 7 . 0 < 3 . 4 < 3 . 4 < 3 . 4 < 3 . 4 < 3 4 . 0 < 3 . 4 < 3 . 4 < 6 . 8 < 3 . 4 <3 <3 <3 <3 <3 <3 <3 <3 <3
SURROGATE PERCENT RECOVERIES
NITROBENZENE-DS (%) 2-FLUOROBIPHENYL (%) TERPHENYL (%) PHEN0L-D6 ( %) 2-FLUOROPHENOL (%) 2,4,6-TRIBROMOPHENOL (%)
85 94 59 111 58 24
A-78
A / J J I ^ AnalyticalTechnologies, Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED)
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
ATI I.D. : 10557414
COMPOUNDS RESULTS
OXYGENATED HYDROCARBON C7 TOTAL ORGANIC ACIDS TOTAL EXTRACTABLE HYDROCARBONS C8-C20
200 200
200
A-79
AjS Analytical Technologies, Inc
^ P L I T
GCMS - RESULTS
ATI I.D. : 10557415
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX
MONTGOMERY & ASSOCIATES 562-A HASSAYAMPA 03-004453 DUPLICATE NON-AQUEOUS
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/02/91 05/02/91 05/07/91 05/17/91 MG/KG
20
COMPOUNDS RESULTS
N-NITROSODIMETHYLAMINE PHENOL ANILINE BIS(2-CHLOROETHYL)ETHER 2-CHLOROPHENOL 1, 3-DICHLOROBENZENE 1,4-DICHLOROBENZENE BENZYL ALCOHOL 1, 2-DICHLOROBENZENE 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL)ETHER 4-METHYLPHENOL N-NITROSO-DI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BENZOIC ACID BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL 1, 2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYLPHTHALATE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE 2,6-DINITROTOLUENE
<3.4 8
4
<3.4 <3.4 <3.4 <3.4 <3.4 <3.4 [
<3.4 <3.4 <3.4 <3.4 <3 <3 <3 <3 <3.4 <17.0 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <17.0 <3.4 <17.0 <3.4 <3.4 <17.0 <3.4 <17.0 <17.0 <3.4 <3.4 <3.4
(CONTINUED NEXT PAGE) A-80
AjS AnalyticalTechnologies,
GCMS - RESULTS ATI I.D, 10557415
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
COMPOUNDS RESULTS
DIETHYLPHTHALATE 4-CHLOROPHENYL-PHENYLETHER FLUORENE 4-NITROANILINE 4,6-DINITRO-2-METHYLPHENOL N-NITROSODIPHENYLAMINE 4-BROMOPHENYL-PHENYLETHER HEXACHLOROBENZ ENE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE DI-N-BUTYLPHTHALATE FLUORANTHENE BENZIDINE PYRENE BUTYLBENZYLPHTHALATE 3,3-DICHLOROBENZIDINE BENZO(a)ANTHRACENE BIS(2-ETHYLHEXYL)PHTHALATE CHRYSENE DI-N-OCTYLPHTHALATE BENZO(b)FLUORANTHENE BENZO(k)FLUORANTHENE BENZO(a)PYRENE INDENO(1,2,3-cd)PYRENE DIBENZO(a,h)ANTHRACENE BENZO(g,h,i)PERYLENE
SURROGATE PERCENT RECOVERIES
NITROBENZENE-DS (%) 2-FLUOROBIPHENYL (%) TERPHENYL (%) PHEN0L-D6 (%) 2-FLUOROPHENOL (%) 2,4,6-TRIBROMOPHENOL M
<3.4 <3.4 <3.4 <17.0 <17.0 <3.4 <3.4 <3.4 <17.0 <3.4 <3.4 <3.4 <3.4 <34.0 <3.4 <3.4 <6.8 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4 <3.4
51 56 63 101 63 33
A-81
A ^ AnalyticalTechnologies, Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED)
A
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
ATI I.D. : 10557415
COMPOUNDS RESULTS
OXYGENATED HYDROCARBON C7 TOTAL ORGANIC ACIDS TOTAL EXTRACTABLE HYDROCARBONS C8-C20
200 200
200
A-82
AjS AnalyticalTechnologies,Inc.
GCMS - RESULTS
^"B-i^ 55,5--5Z.'
ATI I.D. : 10557418
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX
MONTGOMERY & ASSOCIATES 652-A HASSAYAMPA 03-004455 NON-AQUEOUS
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/02/91 05/02/91 05/07/91 05/17/91 MG/KG
20
COMPOUNDS RESULTS
I
I
I
N-NITROSODIMETHYLAMINE PHENOL ANILINE BIS(2-CHLOROETHYL)ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1, 4-DICHLOROBENZENE BENZYL ALCOHOL 1, 2-DICHLOROBENZENE 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL)ETHER 4-METHYLPHENOL N-NITROSO-DI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2 , 4-DIMETHYLPHENOL BENZOIC ACID BIS(2-CHLOROETHOXY)METHANE 2, 4-DICHLOROPHENOL 1, 2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYLPHTHALATE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE 2,6-DINITROTOLUENE
TR - Compound detected at an unquantifiable (CONTINUED NEXT PAGE)
<3.4
<3. <3. <3. <3. <3. <3.
TR <3. <3. <3. <3. <3. <3. <3. <3. <3. <1' <3 <3 <3 <3 <3 <3 <3 9 <3 <3
4 4 4 4 4 4
4 4 4 4 4 4 4 4 4 '.0 4 4 4 4 4 .4 .4
.4
.4 <17.0 <3 .4 <17.0 <3 <3
.4
.4 <17.0 <3 .4 <17.0 <17.0 <3 <3 <3
trace
.4
.4
.4
level A-83
/ \ AnalyticalTechnologies,Inc.
GCMS - RESULTS
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
61^-1'=' ^ ^ • ^ ~ ' S Z J '
ATI I.D. : 10557418
COMPOUNDS RESULTS
DIETHYLPHTHALATE 4-CHLOROPHENYL-PHENYLETHER FLUORENE 4-NITROANILINE 4,5-DINITRO-2-METHYLPHENOL N-NITROSODIPHENYLAMINE 4-BROMOPHENYL-PHENYLETHER HEXACHLOROBENZENE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE DI-N-BUTYLPHTHALATE FLUORANTHENE BENZIDINE PYRENE BUTYLB EN ZYLPHTHALATE 3,3-DICHLOROBENZIDINE BENZO(a)ANTHRACENE BIS(2-ETHYLHEXYL)PHTHALATE CHRYSENE DI-N-OCTYLPHTHALATE BENZO(b)FLUORANTHENE BENZO(k)FLUORANTHENE BENZO(a)PYRENE INDENO(1,2,3-cd)PYRENE DIBENZO(a,h)ANTHRACENE BENZO(g,h,i)PERYLENE
<3.4 <3.4 <3.4 <17.0 <17.0 <3.4 <3.4 <3.4 <17.0 <3.4 <3.4 <3.4 <3.4 <34.0 <3.4 <3.4 <5.8 <3.4 <3.4 <3.4 <3.4 <3,4 <3.4 <3.4 <3.4 <3.4 <3.4
I
SURROGATE PERCENT RECOVERIES
NITROBENZENE-DS (%) 2-FLUOROBIPHENYL (%) TERPHENYL (%) PHENOL-D6 (%) 2-FLUOROPHENOL (%) 2,4,5-TRIBROMOPHENOL (%)
64 52 90 78 21 24
A-84 H
/ ^ AnalyticalTechnologies, Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED)
X j \ Analytii
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
ATI I.D. : 10557418
COMPOUNDS RESULTS
OXYGENATED HYDROCARBON C7 TOTAL ORGANIC ACIDS TOTAL EXTRACTABLE HYDROCARBONS C8-C20
100 5000
1000
A-85
AjS AnalyticalTechnologies, , Inc. 6'lb-\<^ 5 Z . S - S 1 '
GCMS - RESULTS
ATI I.D. 10557419
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX
MONTGOMERY & ASSOCIATES 552-A HASSAYAMPA 03-004455 NON-AQUEOUS
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/02/91 05/02/91 05/07/91 05/17/91 MG/KG
20
COMPOUNDS RESULTS
N-NITROSODIMETHYLAMINE PHENOL ANILINE BIS(2-CHLOROETHYL)ETHER 2-CHLOROPHENOL 1, 3-DICHLOROBENZENE 1, 4-DICHLOROBENZENE BENZYL ALCOHOL 1, 2-DICHLOROBENZENE 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL)ETHER 4-METHYLPHENOL N-NITROSO-DI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2, 4-DIMETHYLPHENOL BENZOIC ACID BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL 1, 2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYLPHTHALATE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE 2, 6-DINITROTOLUENE
<3.4
<3.4 <3.4 <3 <3 <3 <3
4 4 4 4
4 <3 <3 <3 <3 <3 <3 <3.4 <3.4 <3.4 <17.0 <3.4 <3.4 <3.4 6 <3.4 <3.4 <3.4 11 <3.4 <3.4 <17.0 <3.4 <17.0 <3.4 <3.4 <17.0 <3.4 <17.0 <17.0 <3.4 <3.4 <3.4
A-86
(CONTINUED NEXT PAGE)
/ \ AnalyticalTechnologies,Inc.
GCMS - RESULTS ATI I.D.
SB'/'? 5^4.5--57'
10557419
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
COMPOUNDS RESULTS
DIETHYLPHTHALATE 4-CHLOROPHENYL-PHENYLETHER FLUORENE 4-NITROANILINE 4,6-DINITRO-2-METHYLPHENOL N-NITROSODIPHENYLAMINE 4-BROMOPHENYL-PHENYLETHER HEXACHLOROBENZENE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE DI-N-BUTYLPHTHALATE FLUORANTHENE BENZIDINE PYRENE BUTYLBENZYLPHTHALATE 3,3-DICHLOROBENZIDINE BENZO(a)ANTHRACENE BIS(2-ETHYLHEXYL)PHTHALATE CHRYSENE DI-N-OCTYLPHTHALATE BENZO(b)FLUORANTHENE BENZO(k)FLUORANTHENE BENZO(a)PYRENE INDENO(1,2,3-cd)PYRENE DIBENZO(a,h)ANTHRACENE BENZO(g,h,i)PERYLENE
SURROGATE PERCENT RECOVERIES
<3.4 <3.4 <3.4 <17.0 <17.0 <3.4 <3.4 <3.4 <17.0 <3.4 <3 <3 <3 <34.0 <3.4
4 4 .4
<3 <6 <3
<3 <3 <3 <3 <3 <3 <3. <3.
NITROBENZENE-DS (%) 2-FLUOROBIPHENYL (%) TERPHENYL (%) PHEN0L-D5 (%) 2-FLUOROPHENOL (%) 2,4,6-TRIBROMOPHENOL (%)
44 87 115 18 46 26
A-87
6 B - / 1 5 i . t r - 5 - 7 '
AJS AnalyticalTechnologies,Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED)
A
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
ATI I.D. 10557419
COMPOUNDS RESULTS
OXYGENATED HYDROCARBON C7 TOTAL ORGANIC ACIDS TOTAL EXTRACTABLE HYDROCARBONS C8-C20
100 6000
2000
A-88
AjS AnalyticalTechnologies,!
7,-^. for-.
GCMS - RESULTS
REAGENT BLANK
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
CLIENT PROJECT # PROJECT NAME CLIENT I.D.
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA REAGENT BLANK
ATI I.D. DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
105574 05/07/91 05/17/91 MG/KG N/A
COMPOUNDS RESULTS
N-NITROSODIMETHYLAMINE PHENOL ANILINE BIS(2-CHLOROETHYL)ETHER 2-CHLOROPHENOL 1, 3-DICHLOROBENZENE 1, 4-DICHLOROBENZENE BENZYL ALCOHOL 1,2-DICHLOROBENZENE 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL)ETHER 4-METHYLPHENOL N-NITROSO-DI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BENZOIC ACID BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOP ENTADIENE 2,4,5-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYLPHTHALATE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE 2, 6-DINITROTOLUENE DIETHYLPHTHALATE 4-CHLOROPHENYL-PHENYLETHER
< 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 8 5 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 8 5 < 0 . 1 7 < 0 . 8 S < 0 . 1 7 < 0 . 1 7 < 0 . 8 S < 0 . 1 7 < 0 . 8 5 < 0 . 8 5 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7 < 0 . 1 7
(CONTINUED NEXT PAGE) A-89
A j S AnalyticalTechnologies,I
GCMS - RESULTS
REAGENT BLANK ATI I.D. 105574
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
COMPOUNDS RESULTS
FLUORENE 4-NITROANILINE 4,6-DINITRO-2-METHYLPHENOL N-NITROSODIPHENYLAMINE 4-BROMOPHENYL-PHENYLETHER HEXACHLOROBENZENE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE DI-N-BUTYLPHTHALATE FLUORANTHENE BENZIDINE PYRENE BUTYLBENZYLPHTHALATE 3,3-DICHLOROBENZIDINE BENZO(a)ANTHRACENE BIS ( 2-ETHYLHEXYL ) PHTflALATE CHRYSENE DI-N-OCTYLPHTHALATE BENZO(b)FLUORANTHENE BENZO(k)FLUORANTHENE BENZO(a)PYRENE INDENO(1,2,3-cd)PYRENE DIBENZO(a,h)ANTHRACENE BENZO(g,h,i)PERYLENE
<0, <0, <0, <0. <o. <0. <0, <0 <0 <0. <0. < 1 <0. <0. <0. <0 <0. <o. <0 <0 <0 <0 <0 <0 <0
17 85 85 17 17 17 85 17 17 17 17 7 17 17 34 17 17 17 17 17 17 17 17 17 17
SURROGATE PERCENT RECOVERIES
NITROBENZENE-DS (%) 2-FLUOROBIPHENYL (%) TERPHENYL (%) PHEN0L-D6 (%) 2-FLUOROPHENOL (%) 2,4,6-TRIBROMOPHENOL (%)
49 68 80 35 34 34
A-90
^ j ^ AnalyticalTechnologies,Inc.
TEST
QUALITY CONTROL DATA
SEMI-VOLATILE ORGANICS (EPA 8270)
CLIENT PROJECT # PROJECT NAME REF I.D.
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA 10599922
S73-r;
ATI I.D,
DATE ANALYZED SAMPLE MATRIX UNITS
105574
05/17/91
MG/KG
COMPOUNDS
DUP. DUP, SAMPLE CONC. SPIKED % SPIKED % RESULT SPIKED SAMPLE REC.SAMPLE REC, RPD
1, 2,4-TRICHLOROBENZENE ACENAPHTHENE 2,4-DINITROTOLUENE PYRENE N-NITROSO-DI-N-PROPYLAMINE 1,4-DICHLOROBENZENE PENTACHLOROPHENOL PHENOL 2-CHLOROPHENOL 4-CHLORO-3-METHYLPHENOL 4-NITROPHENOL
<0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.8S <0.17 <0.17 <0.17 <0.85
1.7 1.7 1.7 1.7 1.7 1.7 3.3 3.3 3.3 3.3 3.3
0.8 0.8 0.8 1.0 1.0 1.1 1.8 2.2 2.2 1.9 1.2
47 47 47 59 59 65 55 67 67 58 36
0.8 0.9 0.8 1.0 0.9 1.1 2.0 2.1 2.4 1.8 1.1
47 53 47 59 53 65 61 64 73 55 33
0 12 0 0 11 0 11 5 9 5 9
% Recovery = (Spike Sample Result - Sample Result)
Spike Concentration X 100
RPD (Relative % Difference) = (Spiked Sample - Duplicate Spike) Result Sample Result
Average of Spiked Sample X 100
A-91
AjS AnalyticalTechnologies, Inc.
QUALITY CONTROL DATA
TEST : SEMI-VOLATILE ORGANICS (EPA 8270)
CLIENT PROJECT # PROJECT NAME REF I.D.
MONTGOMERY 652-A HASSAYAMPA 10557409
& ASSOCIATES
ATI I.D,
DATE ANALYZED SAMPLE MATRIX UNITS
105574
06/21/91 NON-AQUEOUS MG/KG
COMPOUNDS
DUP. DUP SAMPLE CONC. SPIKED % SPIKED % RESULT SPIKED SAMPLE REC.SAMPLE REC
% Recovery = (Spike Sample Result - Sample Result)
Spike Concentration X 100
RPD (Relative % Difference) = (Spiked Sample - Duplicate Spike) Result Sample Result
Average of Spiked Sample 100
RPD
1, 2 , 4-TRICHLOROBENZENE ACENAPHTHENE 2,4-DINITROTOLUENE PYRENE N-NITROSO-DI-N-PROPYLAMINE 1,4-DICHLOROBENZENE P ENTACHLOROPHENOL PHENOL 2-CHLOROPHENOL 4-CHLORO-3-METHYLPHENOL 4-NITROPHENOL
<0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.85 <0.17 <0.17 <0.17 <0.85
1.7 1.7 1.7 1.7 1.7 1.7 3.3 3.3 3.3 3.3 3.3
1.0 1.1 1.4 1.6 1.1 1.0 3.7 2.7 2.9 2.7 1.4
59 55 82 94 65 59 112 82 88 82 42
1.2 1.2 1.4 1.7 1.3 1.2 3,7 2.6 2.8 3.0 1.2
71 71 82 100 76 71 112 79 85 91 36
18 9 0 6 17 18 0 4 4 11 15
A-92
A j S AnalyticalTechnologies,!
GCMS - RESULTS
6'^-)-7 S^-9'
ATI I.D. : 10557401
TEST : METHOD 8 27 0 (TCLP EXTRACT)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX : NON-AQUEOUS
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA 03-004442
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
04/30/91 05/02/91 05/21/91 05/30/91 UG/L
1
COMPOUNDS RESULTS
N-NITROSODIMETHYLAMINE PHENOL ANILINE BIS(2-CHLOROETHYL)ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE BENZYL ALCOHOL 1, 2-DICHLOROBENZENE 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL)ETHER 4-METHYLPHENOL N-NITROSO-DI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2, 4-DIMETHYLPHENOL BENZOIC ACID BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE 2,4,6-TRICHLOROPHENOL 2 , 4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYLPHTHALATE ACENAPHTHYLENE 3-NITROANINLINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2, 4-DINITROTOLUENE 2,6-DINITROTOLUENE
<10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <50 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <50 <10 <50 <10 <10 <50 <10 <50 <50 <10 <10 <10
(CONTINUED NEXT PAGE) A-93
A j S AnalyticalTechnologies,Inc.
GCMS - RESULTS
TEST : METHOD 8270 (TCLP EXTRACT)
5-B-17 S-^
ATI I.D. : 10557401
COMPOUNDS RESULTS
DIETHYLPHTHALATE 4-CHLOROPHENYL-PHENYLETHER FLUORENE 4-NITROANILINE 4 , 5-DINITRO-2-METHYLPHENOL N-NITROSODIPHENYLAMINE 4-BROMOPHENYL-PHENYLETHER HEXACHLOROBENZENE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE DI-N-BUTYLPHTHALATE FLUORANTHENE BENZIDINE PYRENE BUTYLBENZYLPHTHALATE •3 , 3-DlCHLOROBENZIDINE BENZO(a)ANTHRACENE BIS(2-ETHYLHEXYL)PHTHALATE CHRYSENE DI-N-OCTYLPHTHALATE BENZO(b)FLUORANTHENE BENZO(k)FLUORANTHENE BENZO(a)PYRENE INDENO(1,2,3-cd)PYRENE DIBENZO(a,h)ANTHRACENE BENZO(g,h,i)PERYLENE
<10 <10 <10 <50 <50 <10 <10 <10 <50 <10 <10 <10 <10 <100 <10 <10 <20 <10 86 <10 <10 <10 <10 <10 <10 <10 <10
SURROGATE PERCENT RECOVERIES
NITROBENZENE-DS (%) 2-FLUOROBIPHENYL (%) TERPHENYL (%) PHEN0L-D6 (%) 2-FLUOROPHENOL (%) 2,4,6-TRIBROMOPHENOL (%)
57 55 65 32 32 31
A-94
513-n S ' l
AJS^ AnalyticalTechnologies, Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED)
A J S Analytic
TEST : METHOD 827 0 (TCLP EXTRACT)
ATI I.D. : 10557401
COMPOUNDS RESULTS
300
50
TOTAL ORGANIC ACIDS TOTAL EXTRACTABLE HYDROCARBONS C8-C20
A-95
AiS AnalyticalTechnologies,Inc.
SB-n S ' L '
GCMS - RESULTS
ATI I.D. 10557402
TEST : METHOD 8 27 0 (TCLP EXTRACT)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX : NON-AQUEOUS
MONTGOMERY 652-A HASSAYAMPA 03-004447
& ASSOCIATES DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/01/91 05/02/91 05/06/91 05/17/91 UG/L
1
COMPOUNDS RESULTS
N-NITROSODIMETHYLAMINE PHENOL ANILINE BIS(2-CHLOROETHYL)ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE BENZYL ALCOHOL 1,2-DICHLOROBENZENE 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL)ETHER 4-METHYLPHENOL N-NITROSO-DI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BENZOIC ACID BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYLPHTHALATE ACENAPHTHYLENE 3-NITROANINLINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE 2,6-DINITROTOLUENE
<10 <10 <10 <10 <10 <10 <10 <10
TR <10 <10 <10 <10 <10 <10 <10 <10 <10 <50 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <50 <10 <50 <10 <10 <50 <10 <50 <50 <10 <10 <10
TR - Compound detected at an unquantifiable trace level ^ pnwT'TMTTTrn MrvT •ot.n.-v\
A-96
/ \ AnalyticalTechnologies,Inc.
GCMS - RESULTS ATI I.D.
515~IS S - L '
10557402
TEST : METHOD 827 0 (TCLP EXTRACT)
COMPOUNDS RESULTS
DIETHYLPHTHALATE 4-CHLOROPHENYL-PHENYLETHER FLUORENE 4-NITROANILINE 4,6-DINITRO-2-METHYLPHENOL N-NITROSODIPHENYLAMINE 4-BROMOPHENYL-PHENYLETHER HEXACHLOROBENZENE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE DI-N-BUTYLPHTHALATE FLUORANTHENE BENZIDINE PYRENE BUTYLBENZYLPHTHALATE 3,3-DICHLOROBENZIDINE BENZO(a)ANTHRACENE BIS(2-ETHYLHEXYL)PHTHALATE CHRYSENE DI-N-OCTYLPHTHALATE BENZO(b)FLUORANTHENE BENZO(k)FLUORANTHENE BENZO(a)PYRENE INDENO(1,2,3-cd)PYRENE DIBENZO(a,h) ANTHRACENE BENZO(g,h,i)PERYLENE
SURROGATE PERCENT RECOVERIES
NITROBENZENE-DS (%) 2-FLUOROBIPHENYL (%) TERPHENYL (%) PHEN0L-D6 (%) 2-FLUOROPHENOL (%) 2,4,6-TRIBROMOPHENOL (%)
<10 <10 <10 <50 <50 <10 <10 <10 <50 <10 <10 <10 <10 <100 <10 <10 <20 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10
55 58 95 37 63 39
A-97
A J S Analytii
sib-i"^: ^ ' O '
^JS^ AnalyticalTechnologies, Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED)
TEST : METHOD 827 0 (TCLP EXTRACT)
ATI I.D. : 10557402
COMPOUNDS
BENZOPHENONE
RESULTS
200
A-98
AjS AnalyticalTechnologies, Inc.
GCMS - RESULTS
6l5-»5 T-(. ' SPi-ir
ATI I.D. 10557403
TEST : METHOD 8 27 0 (TCLP EXTRACT)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX : NON-AQUEOUS
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA 03-004447 DUPLICATE
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/01/91 05/02/91 05/06/91 05/17/91 UG/L
1
COMPOUNDS RESULTS
N-NITROSODIMETHYLAMINE PHENOL ANILINE BIS(2-CHLOROETHYL)ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE BENZYL ALCOHOL 1,2-DICHLOROBENZENE • 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL)ETHER 4-METHYLPHENOL N-NITROSO-DI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BENZOIC ACID BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL 1, 2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE 2,4,6-TRICHLOROPHENOL 2, 4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYLPHTHALATE ACENAPHTHYLENE 3-NITROANINLINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE 2,6-DINITROTOLUENE
<10 <10 <10 <10 <10 <10 <10 <10
TR <10 <10 <10 <10 <10 <10 <10 <10 <10 <50 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <50 <10 <50 <10 <10 <50 <10 <50 <50 <10 <10 <10
TR - Compound detected at an unquantifiable trace level (CONTINUED NEXT PAGE^
A-99
/ \ AnalyticalTechnologies,Inc.
GCMS - RESULTS ATI I.D,
60-/S' S-L'
10557403
sPLC
TEST : METHOD 827 0 (TCLP EXTRACT)
COMPOUNDS RESULTS
DIETHYLPHTHALATE 4-CHLOROPHENYL-PHENYLETHER FLUORENE 4-NITROANILINE 4,6-DINITRO-2-METHYLPHENOL N-NITROSODIPHENYLAMINE 4-BROMOPHENYL-PHENYLETHER HEXACHLOROBENZENE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE DI-N-BUTYLPHTHALATE FLUORANTHENE BENZIDINE PYRENE BUTYLBENZYLPHTHALATE 3,3-DICHLOROBENZIDINE BENZO(a)ANTHRACENE BIS(2-ETHYLHEXYL)PHTHALATE CHRYSENE DI-N-OCTYLPHTHALATE BENZO(b)FLUORANTHENE BENZO(k)FLUORANTHENE BENZO(a)PYRENE INDENO(1,2,3-cd)PYRENE DIBENZO(a,h)ANTHRACENE BENZO(g,h,i)PERYLENE
<10 <10 <10 <50 <50 <10 <10 <10 <50 <10 <10 <10 <10 <100 <10 <10 <20 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10
SURROGATE PERCENT RECOVERIES
NITROBENZENE-DS (%) 2-FLUOROBIPHENYL (%) TERPHENYL (%) PHEN0L-D5 (%) 2-FLUOROPHENOL (%) 2,4,6-TRIBROMOPHENOL (%)
59 63 109 38 66 48
A-lOO
y ^ AnalyticalTechnologies, Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED)
"B-i'i" 5~ 'b ' t>?i-zr
TEST : METHOD 827 0 (TCLP EXTRACT)
ATI I.D. : 10557403
COMPOUNDS
BENZOPHENONE
RESULTS
200
A-101
A i S AnalyticalTechnologies,Inc. ^ V i ^ s--^'
GCMS - RESULTS
ATI I.D, 10557406
TEST : METHOD 827 0 (TCLP EXTRACT)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX
MONTGOMERY & 562-A HASSAYAMPA 03-004449 NON-AQUEOUS
ASSOCIATES DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/02/91 05/02/91 05/06/91 05/17/91 UG/L
20
COMPOUNDS RESULTS
N-NITROSODIMETHYLAMINE PHENOL ANILINE BIS(2-CHLOROETHYL)ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1, 4-DICHLOROBENZENE BENZYL ALCOHOL 1, 2-DICHLOROBENZENE 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL)ETHER 4-METHYLPHENOL N-NITROSO-DI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BENZOIC ACID BIS(2-CHLOROETHOXY)METHANE 2, 4-DICHLOROPHENOL 1 , 2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYLPHTHALATE ACENAPHTHYLENE 3-NITROANINLINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE 2,6-DINITROTOLUENE
<200 9400 <200 <200 <200 <200 <200 <200 <200 <200 <200 2800 <200 <200 <200 <200 <200 <200 1200 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 <1000 <200 <1000 <200 <200 <1000 <200 <1000 <1000 <200 <200 <200
(CONTINUED NEXT PAGE) A-102
A j S AnalyticalTechnologies,I
GCMS - RESULTS ATI I.D,
5^-1^ S-I
10557406
TEST : METHOD 8 27 0 (TCLP EXTRACT)
COMPOUNDS RESULTS
DIETHYLPHTHALATE 4-CHLOROPHENYL-PHENYLETHER FLUORENE 4-NITROANILINE 4,6-DINITRO-2-METHYLPHENOL N-NITROSODIPHENYLAMINE 4-BROMOPHENYL-PHENYLETHER HEXACHLOROBENZENE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE DI-N-BUTYLPHTHALATE FLUORANTHENE BENZIDINE PYRENE BUTYLBENZYLPHTHALATE 3,3-DICHLOROBENZIDINE BENZO(a)ANTHRACENE BI S(2-ETHYLHEXYL)PHTHALATE CHRYSENE DI-N-OCTYLPHTHALATE BENZO(b)FLUORANTHENE BENZO(k)FLUORANTHENE BENZO(a)PYRENE INDENO(1,2,3-cd)PYRENE DIBENZO(a,h) ANTHRACENE BENZO(g,h,i)PERYLENE
<200 <200 <200 <1000 <1000 <200 <200 <200 <1000 <200 <200 <200 <200 <2000 <200 <200 <400 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200
SURROGATE PERCENT RECOVERIES
NITROBENZENE-DS (%) 2-FLUOROBIPHENYL (%) TERPHENYL (%) PHEN0L-D5 (%) 2-FLUOROPHENOL (%) 2,4,5-TRIBROMOPHENOL (%)
112 77 94 68 75 29
A-103
A 61h~>^ Z-
AJS AnalyticalTechnologies,Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED)
TEST : METHOD 827 0 (TCLP EXTRACT)
ATI I.D. : 10557406
COMPOUNDS
OXYGENATED HYDROCARBON C7
RESULTS
70000
A-104
^ j ^ AnalyticalTechnologies
Sih- \o-i5"
GCMS - RESULTS
ATI I.D. : 10557407
TEST : METHOD 8 270 (TCLP EXTRACT)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE M-ATRIX : NON-AQUEOUS
MONTGOMERY 662-A HASSAYAMPA 03-004450
& ASSOCIATES DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/02/91 05/02/91 05/06/91 05/17/91 UG/L
20
COMPOUNDS RESULTS
N-NITROSODIMETHYLAMINE PHENOL ANILINE BIS(2-CHLOROETHYL)ETHER 2-CHLOROPHENOL 1, 3-DICHLOROBENZENE 1, 4-DICHLOROBENZENE BENZYL ALCOHOL 1, 2-DICHLOROBENZENE 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL)ETHER 4-METHYLPHENOL N-NITROSO-DI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BENZOIC ACID BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAP HTHALENE HEXACHLOROCYCLOPENTADIENE 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYLPHTHALATE ACENAPHTHYLENE 3-NITROANINLINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE 2,6-DINITROTOLUENE
<200 1400 <200 <200 <200 <200 <200 <200 <200 <200 <200 970 <200 <200 <200 <200 <200 <200 <1000 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 <1000 <200 <1000 <200 <200 <1000 <200 <1000 <1000 <200 <200 <200
(CONTINUED NEXT PAGE) A-105
AiS AnalyticalTechnologies,Inc.
GCMS - RESULTS ATI I.D,
5^-1 7 10-15"
10557407
TEST : METHOD 8 270 (TCLP EXTRACT)
COMPOUNDS RESULTS
DIETHYLPHTHALATE 4-CHLOROPHENYL-PHENYLETHER FLUORENE 4-NITROANILINE 4 , 6-DINITRO-2-METHYLPHENOL N-NITROSODIPHENYLAMINE 4-BROMOPHENYL-PHENYLETHER HEXACHLOROBENZENE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE DI-N-BUTYLPHTHALATE FLUORANTHENE BENZIDINE PYRENE BUTYLBENZYLPHTHALATE 3,3-DICHLOROBENZIDINE BENZO(a)ANTHRACENE BIS(2-ETHYLHEXYL)PHTHALATE CHRYSENE DI-N-OCTYLPHTHALATE BENZO(b)FLUORANTHENE BENZO(k)FLUORANTHENE BENZO(a)PYRENE INDENO(1,2,3-cd)PYRENE DIBENZO(a,h)ANTHRACENE BENZO(g,h,i)PERYLENE
<200 <200 <200 <1000 <1000 <200 <200 <200 <1000 <200 <200 <200 <200 <2000 <200 <200 <400 <200 <200 <200 <200 <200 <200 <200 <200 <200 <200
SURROGATE PERCENT RECOVERIES
NITROBENZENE-DS (%) 2-FLUOROBIPHENYL (%) TERPHENYL (%) PHEN0L-D6 (%) 2-FLUOROPHENOL (%) 2,4,5-TRIBROMOPHENOL (%)
33 45 54 54 51 36
A-106
A AJS AnalyticalTechnologies,Inc.
ADDITIONAL COMPOUNDS (SEMI-QUANTITATED)
TEST : METHOD 827 0 (TCLP EXTRACT)
ATI I.D. : 10557407
COMPOUNDS
OXYGENATED HYDROCARBON C7
RESULTS
20000
A-107
A j S AnalyticalTechnologies,!
GCMS - RESULTS
K.B •?<"-; 515-'9 S-L '^
REAGENT BLANK
TEST : METHOD 8 27 0 (TCLP EXTRACT)
CLIENT PROJECT # PROJECT NAME CLIENT I . D .
MONTGOMERY & ASSOCIATES 562-A HASSAYAMPA REAGENT BLANK
ATI I.D. DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
105574 05/06/91 05/17/91 UG/L N/A
COMPOUNDS RESULTS
N-NITROSODIMETHYLAMINE PHENOL ANILINE BIS(2-CHLOROETHYL)ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE BENZYL ALCOHOL 1,2-DICHLOROBENZENE 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL)ETHER 4-METHYLPHENOL N-NITROSO-DI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BENZOIC ACID BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOP ENTADIENE 2 , 4,5-TRICHLOROPHENOL 2 , 4., 5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYLPHTHALATE ACENAPHTHYLENE 3-NITROANINLINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE 2, 6-DINITROTOLUENE DIETHYLPHTHALATE 4-CHLOROPHENYL-PHENYLETHER
<10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <50 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <50 <10 <50 <10 <10 <S0 <10 <50 <50 <10 <10 <10 <10 <10
(CONTINUED NEXT PAGE) A-108
AjS AnalyticalTechnologies,I
GCMS - RESULTS
REAGENT BLANK
TEST : METHOD 827 0 (TCLP EXTRACT)
ATI I.D. : 105574
COMPOUNDS RESULTS
FLUORENE 4-NITROANILINE 4,6-DINITRO-2-METHYLPHENOL N-NITROSODIPHENYLAMINE 4-BROMOPHENYL-PHENYLETHER HEXACHLOROBENZ ENE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE DI-N-BUTYLPHTHALATE FLUORANTHENE BENZIDINE PYRENE BUTYLBENZYLPHTHALATE 3,3-DICHLOROBENZIDINE BENZO(a j ANTHRACENE BIS(2-ETHYLHEXYL)PHTHALATE CHRYSENE DI-N-OCTYLPHTHALATE BENZO(b)FLUORANTHENE BENZO(k)FLUORANTHENE BENZO(a)PYRENE INDENO(1,2,3-cd)PYRENE DIBENZO(a,h)ANTHRACENE BENZO(g,h,i)PERYLENE
SURROGATE PERCENT RECOVERIES
NITROBENZENE-DS (%) 2-FLUOROBIPHENYL (%) TERPHENYL (%) PHEN0L-D6 (%) 2-FLUOROPHENOL (%) 2,4,5-TRIBROMOPHENOL (%)
<10 <50 <50 <10 <10 <10 <50 <10 <10 <10 <10 <100 <10 <10 <20 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10
42 47 65 35 64 31
A-109
A j S AnalyticalTechnologies,Inc.
12 •B. f o r :
S-B-/7 S ' - ^ '
GCMS - RESULTS
REAGENT BLANK
TEST : METHOD 82 7 0 (TCLP EXTRACT)
CLIENT PROJECT # PROJECT NAME CLIENT I.D.
MONTGOMERY & ASSOCIATES 652-A HASSAYAMPA REAGENT BLANK
ATI I.D. DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
105574 05/20/91 05/29/91 UG/L N/A
COMPOUNDS RESULTS
N-NITROSODIMETHYLAMINE PHENOL . ANILINE BIS(2-CHLOROETHYL)ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE BENZYL ALCOHOL 1,2-DICHLOROBENZENE 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL)ETHER 4-METHYLPHENOL N-NITROSO-DI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BENZOIC ACID BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYLPHTHALATE ACENAPHTHYLENE 3-NITROANINLINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE 2,6-DINITROTOLUENE DIETHYLPHTHALATE 4-CHLOROPHENYL-PHENYLETHER
<10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <S0 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <50 <10 <50 <10 <10 <50 <10 <50 <50 <10 <10 <10 <10 <10
;CONTINUED NEXT PAGE) A-110
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GCMS - RESULTS
REAGENT BLANK
TEST : METHOD 8 27 0 (TCLP EXTRACT)
'?i:h-9or:
t? ib-n s - 7 '
ATI I . D . : 105574
COMPOUNDS RESULTS
FLUORENE 4-NITROANILINE 4 , 6-DINITRO-2-METHYLPHENOL N-NITROSODIPHENYLAMINE 4-BROMOPHENYL-PHENYLETHER HEXACHLOROBENZENE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE DI-N-BUTYLPHTHALATE FLUORANTHENE BENZIDINE PYRENE BUTYLBENZYLPHTHALATE 3, 3-DICHLOROBENZIDINE BENZO(a)ANTHRACENE BIS(2-ETHYLHEXYL)PHTHALATE CHRYSENE DI-N-OCTYLPHTHALATE BENZO(b)FLUORANTHENE BENZO(k)FLUORANTHENE BENZO(a)PYRENE INDENO(1,2 ,3-cd)PYRENE DIBENZO(a,h)ANTHRACENE BENZO(g,h, i)PERYLENE
SURROGATE PERCENT RECOVERIES
NITROBENZENE-DS (%) 2-FLUOROBIPHENYL (%) TERPHENYL (%) PHEN0L-D6 (%) 2-FLUOROPHENOL (%) 2,4,6-TRIBROMOPHENOL (%)
<10 <50 <50 <10 <10 <10 <50 <10 <10 <10 <10 <100 <10 <10 <20 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10
44 37 65 35 40 37
A-111
AjS AnalyticalTechnologies,Inc.
QUALITY CONTROL DATA
TEST : METHOD 827 0 (TCLP EXTRACT)
SB-\S
CLIENT PROJECT # PROJECT NAME REP I.D.
MONTGOMERY & ASSOCIATES 552-A HASSAYAMPA 10599919
ATI I.D.
DATE ANALYZED SAMPLE MATRIX UNITS
: 105574
05/15/91
UG/L
COMPOUNDS
DUP. DUP SAMPLE CONC. SPIKED % SPIKED % RESULT SPIKED SAMPLE REC.SAMPLE REC RPD
1,2,4-TRICHLOROBENZENE ACENAPHTHENE 2,4-DINITROTOLUENE PYRENE NITROSO-DI-PROPYLAMINE 1,4-DICHLOROBENZENE PENTACHLOROPHENOL PHENOL 2-CHLOROPHENOL 4-CHLORO-3-METHYLPHENOL 4-NITROPHENOL
<10 <10 <10 <10 <10 <10 <50 <10 <10 <10 <50
50 50 50 50 50 50 100 100 100 100 100
31 32 26 52 26 37 61 50 52 47 40
62 64 52 104 52 74 61 50 52 47 40
33 37 31 55 29 38 65 52 58 47 41
66 74 62 110 58 76 65 52 58 47 41
6 14 18 6 11 3 6 4 11 0 2
% Recovery = (Spike Sample Result - Saraple Result)
Spike Concentration X 100
RPD (Relative % Difference) = (Spiked Sample - Duplicate Spike) Result Scimple Result
Average of Spiked Sample X 100
A-112
^T3-n
A A j S AnalyticalTechnologies,Inc.
QUALITY CONTROL DATA
TEST : METHOD 827 0 (TCLP EXTRACT)
CLIENT PROJECT # PROJECT NAME REF I.D.
MONTGOMERY & ASSOCIATES 652-A HASSAYAMPA 10599922
ATI I.D.
DATE ANALYZED SAMPLE MATRIX UNITS
105574
05/29/91 NON-AQUEOUS UG/L
COMPOUNDS
DUP. DUP. SAMPLE CONC. SPIKED % SPIKED % RESULT SPIKED SAMPLE REC.SAMPLE REC RPD
1,2,4-TRICHLOROBENZENE ACENAPHTHENE 2,4-DINITROTOLUENE PYRENE NITROSO-DI-PROPYLAMINE 1,4-DICHLOROBENZENE PENTACHLOROPHENOL PHENOL 2-CHLOROPHENOL 4-CHLORO-3-METHYLPHENOL 4-NITROPHENOL
<10 <10 <10 <10 <10 <10 <50 <10 <10 <10 <50
50 50 SO 50 50 50 100 100 100 100 100
20 23 23 36 23 20 90 55 59 51 52
40 46 45 72 46 40 90 56 59 61 62
21 23 26 44 23 20 98 63 69 59 70
42 45 52 88 45 40 98 63 69 69 70
5 0 12 20 0 0 9 12 16 12 12
% Recovery = (Spike Sample Result - Sample Result)
Spike Concentration 100
RPD (Relative % Difference) = (Spiked Sample - Duplicate Spike) Result Sample Result
Average of Spiked Sample 100
A-113
A J S AnalyticalTechnologies,Inc.
^B-/? ^B-/?
^ ACCESSION: 105574
LABORATORY CONTROL STANDARD 889 BN/A METHOD 8270
CLIENT: MONTGOMERY AND ASSOCIATES UNITS: UG/L ANALYSIS DATE: 05/15/91
PHENOL 1,2-DICHLOROBENZENE HEXACHLOROETHANE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL HEXACHLOROBUTADIENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE ACENAPHTHYLENE 4-NITROPHENOL 2,6-DINITROTOLUENE 4-CHLOROPHENYL PHENYLETHER N-NITROSODI-N-PHENYLAMINE PENTACHLOROPHENOL DI-N-BUTYLPHTHALATE PYRENE BIS(2-ETHYLHEXYL)PHTHALATE
TRUE VALUE
100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100
OBSERVED VALUE
60 73 94 84 85 69 98 76 77 66 51 89 82 64 54 92 116 155
% R
60 73 94 84 85 69 98 76 77 66 51 89 82 64 54 92 116 155
A-114
/ \ AnalyticalTechnologies,Inc. ACCESSION: 105574
LABORATORY CONTROL STANDARD 889 BN/A METHOD 827 0
CLIENT: MONTGOMERY AND ASSOCIATES UNITS: UG/L ANALYSIS DATE: 05/20/91
PHENOL 1,2-DICHLOROBENZENE HEXACHLOROETHANE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL HEXACHLOROBUTADIENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE ACENAPHTHYLENE 4-NITROPHENOL 2,6-DINITROTOLUENE 4-CHLOROPHENYL PHENYLETHER N-NITROSODI-N-PHENYLAMINE PENTACHLOROPHENOL DI-N-BUTYLPHTHALATE PYRENE BIS(2-ETHYLHEXYL)PHTHALATE
TRUE VALUE
100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100
OBSERVED VALUE
89 78 94 99 83 72 100 88 62 73 90 87 100 92 66 108 94 122
% R
89 78 94 99 83 72 100 88 62 73 90 87 100 92 66 108 94 122
A-115
^ % ' ^
A j S AnalyticalTechnologies,Inc.
Sh~n
ACCESSION: 105574
LABORATORY CONTROL STANDARD 889 BN/A METHOD 8270
CLIENT: MONTGOMERY AND ASSOCIATES UNITS: UG/L ANALYSIS DATE: 05/30/91
PHENOL 1,2-DICHLOROBENZENE HEXACHLOROETHANE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL HEXACHLOROBUTADIENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE ACENAPHTHYLENE 4-NITROPHENOL 2,6-DINITROTOLUENE 4-CHLOROPHENYL PHENYLETHER N-NITROSODI-N-PHENYLAMINE PENTACHLOROPHENOL DI-N-BUTYLPHTHALATE PYRENE BIS(2-ETHYLHEXYL)PHTHALATE
TRUE VALUE
100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100
OBSERVED VALUE
44 86 97 92 96 76 109 80 73 83 29 84 76 103 55 98 113 141
% R
44 86 97 92 96 76 109 80 73 83 29 84 76 103 55 98 113 141
A-116
/f .xV
AjS AnalyticalTechnologies,Inc.
6 B - n • -i^.s-'Zo'
GAS CHROMATOGRAPHY - RESULTS
ATI I.D, 10557408
TEST : ORGANOCHLORINE PESTICIDES/PCB'S (EPA 8080
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX
MONTGOMERY & ASSOCIATES 562-A HASSAYAMPA 03-004444 NON-AQUEOUS
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
04/30/91 05/02/91 05/07/91 05/18/91 MG/KG
1
COMPOUNDS RESULTS
ALDRIN ALPHA - BHC BETA - BHC GAMMA - BHC DELTA - BHC ALPHA-CHLORDANE GAMMA-CHLORDANE 4,4'-DDD 4,4'-DDE 4,4'-DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN KETONE HEPTACHLOR HEPTACHLOR EPOXIDE METHOXYCHLOR TOXAPHENE AROCLOR 1016 AROCLOR 1221 AROCLOR 123 2 AROCLOR 124 2 AROCLOR 124 8 AROCLOR 1254 AROCLOR 12 6 0
<0. <0. <0. <0. <0. <0. <0. <0. <0. <0, <0, <0, <0, <0, <0, <0, <0, <0. <0, <0, <0, <0. <0. <0 <o. <0 <0
005 005 005 005 005 05 05 01 01 01 01 01 01 01 01 01 005 005 05 1 05 05 05 05 OS 05 OS
SURROGATE PERCENT RECOVERIES
DBC (%) 76
A-117
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AJS AnalyticalTechnologies,Inc.
GAS CHROMATOGRAPHY - RESULTS
TEST : ORGANOCHLORINE PESTICIDES/PCB'S (EPA 8080)
ATI I.D. 10557409
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA 0 3 - 0 0 4 4 4 3 NON-AQUEOUS
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
0 4 / 3 0 / 9 1 0 5 / 0 2 / 9 1 0 5 / 0 7 / 9 1 0 5 / 1 7 / 9 1 MG/KG
1
COMPOUNDS RESULTS
ALDRIN ALPHA - BHC BETA - BHC GAMMA - BHC DELTA - BHC ALPHA-CHLORDANE GAMMA-CHLORDANE 4 , 4'-DDD 4 , 4 ' - D D E 4 , 4 ' -DDT DIELDRIN ENDOSULFAN I ENDOSULFAN I I ENDOSULFAN SULFATE ENDRIN ENDRIN KETONE HEPTACHLOR HEPTACHLOR EPOXIDE METHOXYCHLOR TOXAPHENE AROCLOR 1016 AROCLOR 1221 AROCLOR 123 2 AROCLOR 124 2 AROCLOR 124 8 AROCLOR 1254 AROCLOR 1260
SURROGATE PERCENT RECOVERIES
< 0 . < 0 . < 0 . < 0 . < 0 . < 0 . < 0 . < 0 . < 0 . < 0 . < 0 . < 0 . < 0 . < 0 . < 0 , <0 , <0 , <0 , <0 , <0 ,
<o. <0 <0 <0. <0 <0 <0
005 005 005 005 005 OS 05 01 01 01 01 01 01 01 01 01 005 005 05 1 05 05 05 05 05 OS 05
DBC (%) 108
A-118
A ^B-'7 3^^- ' ^o '
Inc. AJS AnalyticalTechnologies,lr
GAS CHROMATOGRAPHY - RESULTS
TEST : ORGANOCHLORINE PESTICIDES/PCB'S (EPA 8080)
ATI I.D. : 10557410
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX
MONTGOMERY E. ASSOCIATES 662-A HASSAYAMPA 03-004445 NON-AQUEOUS
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
04/30/91 05/02/91 05/07/91 05/18/91 MG/KG
1
COMPOUNDS RESULTS
ALDRIN ALPHA - BHC BETA - BHC GAMMA - BHC DELTA - BHC ALPHA-CHLORDANE GAMMA-CHLORDANE 4, 4'-DDD 4, 4'-DDE 4,4'-DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN KETONE HEPTACHLOR HEPTACHLOR EPOXIDE METHOXYCHLOR TOXAPHENE AROCLOR 1016 AROCLOR 1221 AROCLOR 1232 AROCLOR 124 2 AROCLOR 124 8 AROCLOR 1254 AROCLOR 1260
SURROGATE PERCENT RECOVERIES
<0. <0. <0. <0. <0. <0. <0. <0. <0. <0. <0. <0. <0. <0. <0, <0, <0, <0, <0. <0, <0, <0 <0, <0, <0, <0. <0
005 005 005 005 005 05 OS 01 01 01 01 01 01 01 01 01 005 005 OS 1 OS 05 05 05 05 05 OS
DBC (%) 100
A-119
^ j ^ AnalyticalTechnologies, Inc. •D~b-n H^. i r -STJ'
GAS CHROMATOGRAPHY - RESULTS
ATI I.D. 10557411
TEST : ORGANOCHLORINE PESTICIDES/PCB'S (EPA 8080)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA 03-004446 NON-AQUEOUS
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/01/91 05/02/91 05/07/91 05/18/91 MG/KG
1
COMPOUNDS RESULTS
ALDRIN ALPHA - BHC BETA - BHC GAMMA - BHC DELTA - BHC ALPHA-CHLORDANE GAMMA-CHLORDANE 4,4'-DDD 4, 4'-DDE 4,4'-DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN KETONE HEPTACHLOR HEPTACHLOR EPOXIDE METHOXYCHLOR TOXAPHENE AROCLOR 1016 AROCLOR 1221 AROCLOR 1232 AROCLOR 124 2 AROCLOR 124 8 AROCLOR 1254 AROCLOR 1260
<0. <0. <0. <0. <0. <0. <0. <0. <0. <0. <0. <0, <0. <0, <0, <0, <o, <0, <0, <0, <0. <0. <o. <0 <0 <0 <0
005 005 005 005 005 05 OS 01 01 01 01 01 01 01 01 01 005 005 05 1 05 05 OS 05 OS 05 05
SURROGATE PERCENT RECOVERIES
DBC (%) 98
A-120
ZlS Anc e ' ^ - i ^ 2H.15--2S'
AJS AnalyticalTechnologies, Inc.
GAS CHROMATOGRAPHY - RESULTS
TEST : ORGANOCHLORINE PESTICIDES/PCB'S (EPA 8080)
ATI I.D. : 10557412
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX
MONTGOMERY & ASSOCIATES 652-A HASSAYAMPA 03-004451 NON-AQUEOUS
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/02/91 05/02/91 05/07/91 05/19/91 MG/KG
10
COMPOUNDS RESULTS
ALDRIN ALPHA - BHC BETA - -BHC GAMMA - BHC DELTA - BHC ALPHA-CHLORDANE GAMMA-CHLORDANE 4,4'-DDD 4,4'-DDE 4,4'-DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN KETONE HEPTACHLOR HEPTACHLOR EPOXIDE METHOXYCHLOR TOXAPHENE AROCLOR 1015 AROCLOR 1221 AROCLOR 1232 AROCLOR 124 2 AROCLOR 124 8 AROCLOR 125 4 AROCLOR 125 0
SURROGATE PERCENT RECOVERIES
< 0 . 0 5 0 < 0 . 0 5 0 < 0 . 0 5 0 < 0 . 0 5 0 < 0 . 0 5 0 < 0 . 5 < 0 . 5 < 0 . 1 < 0 . 1 <0 <0
<0 <0 <0 <0
< 0 . 1
DBC (%)
< 0 . 0 5 0 < 0 . 0 S 0 < 0 . 5 < 1 . 0 < 0 . 5 < 0 . 5 < 0 . 5 < 0 . 5 < 0 . 5 < 0 . 5 < 0 . 5
90
A-121
AiS AnalyticalTechnologies,lr
615-1^ 3 : r ' 3 s . S '
GAS CHROMATOGRAPHY - RESULTS
ATI I.D, 10557413
TEST : ORGANOCHLORINE PESTICIDES/PCB'S (EPA 8080)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE >LATRIX
MONTGOMERY & ASSOCIATES 652-A HASSAYAMPA 03-004452 NON-AQUEOUS
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/02/91 05/02/91 05/07/91 05/19/91 MG/KG
50
COMPOUNDS RESULTS
ALDRIN ALPHA - BHC BETA - BHC GAMMA - BHC DELTA - BHC ALPHA-CHLORDANE GAMMA-CHLORDANE 4,4'-DDD 4,4'-DDE 4, 4'-DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN KETONE HEPTACHLOR HEPTACHLOR EPOXIDE METHOXYCHLOR TOXAPHENE AROCLOR 1016 AROCLOR 1221 AROCLOR 1232 AROCLOR 124 2 AROCLOR 124 8 AROCLOR 1254 AROCLOR 12 50
<0.250 <0.250 <0.250 <0.2S0 <0.250 <2.5 <2.S <0.5 <0.S <0.S <0.5 <0.S <0.5 <0.5 <0.5 <0.5 <0.250 <0.2S0 <2.5 <5.0 <2.5 <2.5 <2.S <2.S <2.5 <2.5 <2.5
SURROGATE PERCENT RECOVERIES
DBC (%) ** ** Due to the necessary dilution of the sample, result was not attainable
A-122
AjS AnalyticolTechnologies,Inc.
GAS CHROMATOGRAPHY - RESULTS
TEST : ORGANOCHLORINE PESTICIDES/PCB'S (EPA 8080)
5"B-I ^ 6 - - ^ ^ , '
ATI I.D. : 10557414
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX
MONTGOMERY & ASSOCIATES 652-A HASSAYAMPA 03-004453 NON-AQUEOUS
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/02/91 05/02/91 05/07/91 05/19/91 MG/KG
10
COMPOUNDS RESULTS
ALDRIN ALPHA - BHC BETA - BHC GAMMA - BHC DELTA - BHC ALPHA-CHLORDANE GAMMA-CHLORDANE 4,4'-DDD 4,4'-DDE 4,4'-DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN KETONE HEPTACHLOR HEPTACHLOR EPOXIDE METHOXYCHLOR TOXAPHENE AROCLOR 1016 AROCLOR 1221 AROCLOR 123 2 AROCLOR 124 2 AROCLOR 124 8 AROCLOR 1254 AROCLOR 126 0
SURROGATE PERCENT RECOVERIES
<0.050 <0.050 <0.050 <0.050 <0.050 <0.5 <0.5 <0 <o. <0 <0 <0 <0 <0 <0 <0
DBC (%)
< 0 . 0 5 0 < 0 . 0 5 0 < 0 . 5 < 1 . 0 < 0 . 5 < 0 . 5 < 0 . 5 < 0 . 5 <0.S <0.5 <0.5
85
A-123
A SB-i'i iT-^it,' SP. i . l T
AJS AnalyticalTechnologies,Inc.
GAS CHROMATOGRAPHY - RESULTS
TEST : ORGANOCHLORINE PESTICIDES/PCB'S (EPA 8080)
ATI I.D, 10557415
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX
MONTGOMERY & ASSOCIATES 552-A HASSAYAMPA 03-004453 DUPLICATE NON-AQUEOUS
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/02/91 05/02/91 05/07/91 05/19/91 MG/KG
20
COMPOUNDS RESULTS
ALPHA - BHC BETA - BHC GAMMA - BHC DELTA - BHC ALPHA-CHLORDANE GAMMA-CHLORDANE 4,4'-DDD 4,4'-DDE 4,4'-DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN KETONE HEPTACHLOR HEPTACHLOR EPOXIDE METHOXYCHLOR TOXAPHENE AROCLOR 1015 AROCLOR 1221 AROCLOR 1232 AROCLOR 124 2 AROCLOR 124 8 AROCLOR 1254 AROCLOR 126 0
SURROGATE PERCENT RECOVERIES
<0.100 <0.100 <0.100 <0.100 <0.100 <1 <1 <0 <0 <0 <0 <0 <0 <0 <0 <0
0 0 2 2 2 2 2 2 2 2 2
DBC (%)
< 0 . 1 0 0 < 0 . 1 0 0 < 1 . 0 < 2 . 0 < 1 . 0 < 1 . 0 < 1 . 0 < 1 . 0 < 1 . 0 < 1 . 0 < 1 . 0
102
A-124
A j S AnalyticalTechnologies,
6i3-i' S t r . ^ ' S Z , '
inc.
GAS CHROMATOGRAPHY - RESULTS
ATI I.D. : 10557418
TEST : ORGANOCHLORINE PESTICIDES/PCB'S (EPA 8080)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE M-ATRIX
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA 03-004455 NON-AQUEOUS
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/02/91 05/02/91 05/07/91 05/19/91 MG/KG
50
COMPOUNDS RESULTS
ALDRIN ALPHA - BHC BETA - BHC GAMMA - BHC DELTA - BHC ALPHA-CHLORDANE GAMMA-CHLORDANE 4, 4'-DDD 4,4'-DDE 4,4'-DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN KETONE HEPTACHLOR HEPTACHLOR EPOXIDE METHOXYCHLOR TOXAPHENE AROCLOR 1016 AROCLOR 1221 AROCLOR 1232 AROCLOR 124 2 AROCLOR 124 8 AROCLOR 1254 AROCLOR 1260
<0.250 <0.250 <0.250 <0.250 <0.250 <2.5 <2 <0 <0 <0 <0
<0 <0 <0
<5 <2 <2
<2 <2 <2
<0.5 <0.5
<0.250 <0.250 <2.5
<2.5 <2.5
SURROGATE PERCENT RECOVERIES
DBC (%) ** ** Due to the necessary dilution of the sample, result was not attainable
A-125
A j S AnalyticalTechnologies, ;nc.
GAS CHROMATOGRAPHY - RESULTS
6B-/9 S6.rr-^7'
ATI I.D, 10557419
TEST : ORGANOCHLORINE PESTICIDES/PCB'S (EPA 8080)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX
MONTGOMERY & ASSOCIATES 552-A HASSAYAMPA 03-004456 NON-AQUEOUS
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/02/91 05/02/91 05/07/91 05/19/91 MG/KG
50
COMPOUNDS RESULTS
ALDRIN ALPHA - BHC BETA - BHC GAMMA - BHC DELTA - BHC ALPHA-CHLORDANE GAMMA-CHLORDANE 4,4'-DDD 4,4'-DDE 4,4'-DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN KETONE HEPTACHLOR HEPTACHLOR EPOXIDE METHOXYCHLOR TOXAPHENE AROCLOR 1015 AROCLOR 1221 AROCLOR 1232 AROCLOR 124 2 AROCLOR 124 8 AROCLOR 1254 AROCLOR 126 0
<0.250 <0.250 <0.250 <0.250 <0.250 <2.S <2 <0
<5 <2
<0.5 <0.S <0.5 <0.5 <0.S <0.5 <0.5 <0.5 <0.250 <0.250 <2.5
<2.5 <2.5 <2.S <2.5 <2.5 <2.5
SURROGATE PERCENT RECOVERIES
DBC (%) ** ** Due to the necessary dilution of the sample, result was not attainable
A-125
A j S AnalyticolTechnologies, Inc.
• 1 ^ . g ^ r :
GAS CHROMATOGRAPHY - RESULTS
REAGENT BLANK
TEST : ORGANOCHLORINE PESTICIDES/PCB'S (EPA 8080)
CLIENT PROJECT # PROJECT NAME CLIENT I . D .
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA REAGENT BLANK
ATI I.D. DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
105574 05/07/91 05/17/91 MG/KG N/A
COMPOUNDS RESULTS
ALDRIN ALPHA - BHC BETA - BHC GAMMA - BHC DELTA - BHC ALPHA-CHLORDANE GAMMA-CHLORDANE 4, 4'-DDD 4,4'-DDE 4, 4'-DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN KETONE HEPTACHLOR HEPTACHLOR EPOXIDE METHOXYCHLOR TOXAPHENE AROCLOR 1016 AROCLOR 1221 AROCLOR 123 2 AROCLOR 124 2 AROCLOR 124 8 AROCLOR 125 4 AROCLOR 126 0
SURROGATE PERCENT RECOVERIES
DBC (%)
<0.005 <0.005 <0,00S <0.005 <0.005 <0.0S <0.0S <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.005 <0.005 <0.05 <0.1 <0.05 <0.05 <0.05 <0.05 <0.05 <0.0S <0.05
107
A-127
J j ] ^ AnalyticalTechnologies, Inc.
SB-ll
QUALITY CONTROL DATA
TEST : ORGANOCHLORINE PESTICIDES/PCB'S (EPA 8080) ATI I.D, 105574
CLIENT PROJECT # PROJECT NAME REF I.D.
MONTGOMERY 652-A HASSAYAMPA 10557409
& ASSOCIATES DATE ANALYZED SAMPLE MATRIX UNITS
05/17/91 NON-AQUEOUS MG/KG
COMPOUNDS
DUP. DUP SAMPLE CONC. SPIKED % SPIKED % RESULT SPIKED SAMPLE REC.SAMPLE REC. RPD
GAMMA BHC HEPTACHLOR ALDRIN DIELDRIN ENDRIN DDT
<0.005 <0.005 <0.005 <0.01 <0.01 <0.01
0.07 0.07 0.07 0.07 0.07 0.07
0.07 0.07 0.06 0.07 0.07 0.07
100 100 85 100 100 100
0.06 0.06 0.06 0.07 0.07 0.07
86 86 86 100. 100 100
15 15 0 0 0 0
% Recovery = (Spike Sample Result - Sample Result)
Spike Concentration 100
RPD (Relative % Difference) = (Spiked Sample - Duplicate Spike) Result Sample Result
Average of Spiked Sample X 100
A-128
^JS^ AnolyticolTechnologies,
4,15-/7
ACCESSION: 105574
LABORATORY CONTROL SAMPLE METHOD 8080
CLIENT: MONTGOMERY AND ASSOCIATES UNITS: MG/KG ANALYSIS DATE: 05/17/91
LINDANE HEPTACHLOR ALDRIN DIELDRIN ENDRIN DDT
TRUE VALUE
2.0 2.0 2.0 2.0 2.0 2.0
FOUND
2.0 2.0 2.0 1.9 1.9 1.9
% R
100 100 100 95 95 95
A-129 \
f ^ '
AjS AnolyticolTechnologies,Inc.
6B-)7 §--7'
GAS CHROMATOGRAPHY - RESULTS
ATI I.D. : 10557401
TEST : TCLP ORGANOCHLORINE PESTICIDES (EPA 1311)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA 03-004442 NON-AQUEOUS
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
04/30/91 05/02/91 05/06/91 05/15/91 UG/L
5
COMPOUNDS RESULTS
ALDRIN ALPHA BHC BETA BHC GAMMA BKC (LINDANE) DELTA BHC CHLORDANE 4,4'-DDD 4,4'-DDE 4,4'-DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHYDE ENDRIN KETONE HEPTACHLOR HEPTACHLOR EPOXIDE METHOXYCHLOR TOXAPHENE AROCLOR 1016 AROCLOR 12 21 AROCLOR 123 2 AROCLOR 124 2 AROCLOR 124 8 AROCLOR 1254 AROCLOR 12 50
<0. <0. <0. <0. <0. <2. <0. <0. <0. <0, <0. <0, <0. <0, <0, <0, <0, <0, <2, <5. <2 <2 <2 <2 <2 <2 <2
25 25 25 25 25 5 5 5 5 5 25 5 5 5 5 5 25 25 5 0 5 5 5 5 5 5 5
SURROGATE PERCENT RECOVERIES
DBC (%) 75
A-130
AjS AnolyticolTechnologies,Inc.
6-p.-)? ^ - W
GAS CHROMATOGRAPHY - RESULTS
ATI I.D. 10557402
TEST : TCLP ORGANOCHLORINE PESTICIDES (EPA 1311)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX : NON-AQUEOUS
MONTGOMERY St ASSOCIATES 662-A HASSAYAMPA 03-004447
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/01/91 05/02/91 05/05/91 05/16/91 UG/L
5
COMPOUNDS RESULTS
(LINDANE)
ALDRIN ALPHA BHC BETA BKC GAMMA BHC DELTA BHC CHLORDANE 4, 4'-DDD 4, 4'-DDE 4,4'-DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN -ALDEHYDE ENDRIN KETONE HEPTACHLOR HEPTACHLOR EPOXIDE METHOXYCHLOR TOXAPHENE AROCLOR 1016 AROCLOR 12 21 AROCLOR 12 3 2 AROCLOR 124 2 AROCLOR 1248 AROCLOR 1254 AROCLOR 1260
SURROGATE PERCENT RECOVERIES
<0 <0 <0 <0 <0 <2 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <0 <2 <5 <2 <2 <2 <2 <2 <2 <2
25 25 25 25 25 5 5 5 5 5 25 5 5 5 5 5 25 25 5 0 5 5 5 5 5 5 5
DBC (%) 68
A-131
AjS AnolyticolTechnologies,Inc.
5B-/? ^-^' 5PL>-r
GAS CHROMATOGRAPHY - RESULTS
ATI I.D. : 10557403
TEST : TCLP ORGANOCHLORINE PESTICIDES (EPA 1311)
CLIENT . PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX : NON-AQUEOUS
MONTGOMERY & ASSOCIATES 652-A HASSAYAMPA 03-004447 DUPLICATE
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/01/91 05/02/91 05/06/91 05/15/91 UG/L
5
COMPOUNDS RESULTS
(LINDANE)
ALDRIN ALPHA BHC BETA BHC GAMMA BHC DELTA BHC CHLORDANE 4,4'-DDD 4,4'-DDE 4,4'-DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHYDE ENDRIN KETONE HEPTACHLOR HEPTACHLOR EPOXIDE METHOXYCHLOR TOXAPHENE AROCLOR 1016 AROCLOR 1221 AROCLOR 123 2 AROCLOR 124 2 AROCLOR 124 8 AROCLOR 1254 AROCLOR 126 0
<0.25 <0.25 <0.25 <0.25 <0.25 <2.5 <0 <0 <0 <0
<0 <0 <0 <0
<0.25 <0.5
<0.25 <0.25 <2.S <5 <2 <2.5 <2.5 <2 <2 <2 <2
0 5
SURROGATE PERCENT RECOVERIES
DBC (% 83
A-132
A \ AnolyticolTechnologies,!
• 5 - ^ - ] ^ S"-^'
GAS CHROMATOGRAPHY - RESULTS
ATI I.D. 10557405
TEST : TCLP ORGANOCHLORINE PESTICIDES (EPA 1311)
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE -MATRIX
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA 03-004449 NON-AQUEOUS
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/02/91 05/02/91 05/06/91 05/16/91 UG/L
50
COMPOUNDS RESULTS
ALDRIN ALPHA BHC BETA BHC GAMMA BHC (LINDANE) DELTA BHC CHLORD-ANE 4,4'-DDD 4, 4'-DDE 4,4'-DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHYDE ENDRIN KETONE HEPTACHLOR HEPTACHLOR EPOXIDE METHOXYCHLOR TOXAPHENE AROCLOR 1015 AROCLOR 12 21 AROCLOR 1232 AROCLOR 124 2 AROCLOR 124 8 AROCLOR 1254 AROCLOR 126 0
<2, <2. <2 <2 <2 <25.0 <S.O <S.O <5.0 <5.0 <2.5 <5.0 <5 <5 <5 <S <2 <2
0 0 0 0 5 5
<25.0 <50.0 <25.0 <25.0 <25.0 <25.0 <2S.O <25.0 <25.0
SURROGATE PERCENT RECOVERIES
DBC (%) ** ** Due to the necessary dilution of the sample, result was not attainable
A-133
A j S AnalyticalTechnologies,Inc.
5 -l<=! )o - 1 5
GAS CHROMATOGRAPHY - RESULTS
TEST : TCLP ORGANOCHLORINE PESTICIDES (EPA 1311)
ATI I.D. : 10557407
CLIENT PROJECT # PROJECT NAME CLIENT I.D. SAMPLE MATRIX : NON-AQUEOUS
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA 03-004450
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
05/02/91 05/02/91 05/05/91 05/16/91 UG/L
10
COMPOUNDS RESULTS
(LINDANE)
ALDRIN ALPHA BHC BETA BHC GAMMA BKC DELTA BHC CHLORDANE 4, 4'-DDD 4,4'-DDE 4,4'-DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHYDE ENDRIN KETONE HEPTACHLOR HEPTACHLOR EPOXIDE METHOXYCHLOR TOXAPHENE AROCLOR 1016 AROCLOR 1221 AROCLOR 1232 AROCLOR 124 2 AROCLOR 124 8 AROCLOR 1254 AROCLOR 126 0
<0 <0 <0 <0 <0 <5 <1 <1 <1
<1 <1 <0 <0 <5
<1.0 <0.5 <1.0 <1.0 <1.0
0
<10.0 <5 <5
0 0
<5.0 <S.O <5.0 <5.0 <S.O
SURROGATE PERCENT RECOVERIES
DBC ( 69
A-134
-i:^.9or:
^JSj AnolyticolTechnologies, Inc.
5J2^I7, 51^-1^, 55-1^
GAS CHROMATOGRAPHY - RESULTS
REAGENT BLANK
TEST : TCLP ORGANOCHLORINE PESTICIDES (EPA 1311)
CLIENT PROJECT # PROJECT NAME CLIENT I.D.
MONTGOMERY & ASSOCIATES 662-A HASSAYAMPA REAGENT BLANK
ATI I.D. DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
105574 05/06/91 05/16/91 UG/L N/A
COMPOUNDS RESULTS
ALDRIN ALPHA BHC BETA BHC GAMMA BHC (LINDANE) DELTA BHC ALPHA-CHLORDANE 4, 4'-DDD 4,4'-DDE 4,4'-DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHYDE ENDRIN KETONE HEPTACHLOR HEPTACHLOR EPOXIDE METHOXYCHLOR TOXAPHENE AROCLOR 1016 AROCLOR 12 21 AROCLOR 123 2 AROCLOR 124 2 AROCLOR 124 8 AROCLOR 1254 AROCLOR 126 0 GAMMA-CHLORDANE
SURROGATE PERCENT RECOVERIES
<0.05 <0.0S <0.05 <0.05 <0.05 <0.S <0.1 <0.1 <0.1 <0.1 <0.05 <0 <0 <0 <0 <0
<0 <1 <0 <0 <0
<0 <0 <0. <0
<0.05 <0.05
<0.S
DBC (%) 85
A-135
A
TEST
AJS AnalyticolTechnologies,Inc.
QUALITY CONTROL DATA
TCLP ORGANOCHLORINE PESTICIDES (EPA 1311)
CLIENT PROJECT # PROJECT NAME REF I.D.
MONTGOMERY & ASSOCIATES 652-A HASSAYAMPA 10599919
^B77 5B-I.?-
ATI I.D,
DATE ANALYZED SAMPLE MATRIX UNITS
105574
05/16/91
UG/L
COMPOUNDS
DUP. DUP SAMPLE CONC. SPIKED % SPIKED % RESULT SPIKED SAMPLE REC.SAMPLE REC RPD
LINDANE ENDRIN
0.05 0.1
2.0 2.0
2.0 2.1
100 1.9 105 1.9
95 95
5 10
% Recovery = (Spike Sample Result - Sample Result)
Spike Concentration 100
RPD (Relative % Difference) = (Spiked Sample - Duplicate Spike) Result Sample Result
Average of Spiked Sample 100
A-136
Jl ^^-n / j j ^ AnalyticolTechnologies, Inc.
ACCESSION: 105574
LABORATORY CONTROL SAMPLE METHOD 8080 (TCLP)
B
68 CLIENT: MONTGOMERY AND ASSOCIATES UNITS: ug/L ANALYSIS DATE: 05/16/91
I I
LINDANE HEPTACHLOR ALDRIN DIELDRIN ENDRIN DDT
TRUE VALUE
2.0 2.0 2.0 2.0 2.0 2.0
FOUND
2.1 2.1 2.1 2.1 2.2 2.0
% R
105 105 105 105 110 100
I I I I I I I B
A-137
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