Post on 18-Mar-2020
0001
AMO ENVIRONMENTAL DECISIONS
AUXIER & ASSOCIATES, INC.
West Lake Landfill Stormwater
ST AND ARD LEVEL IV REPORT OF ANALYSIS
WORK ORDER #18-03110-OR
May 11, 2018
EBERLINE ANALYTICAL/OAK RIDGE LABORATORY
OAK RIDGE, TN
0002
TABLE OF CONTENTS
SECTION DESCRIPTION PAGE
I Chain of Custody & pH Check 0004
II Sample Acknowledgement 0013
III Case Narrative 0016
IV Analytical Results Summary 0020
V Analytical Standards 0023
VI Quality Control Sample Results Summary 0059
VII Laboratory Technician's Notes 0072
VIII Analytical Data (Isotopic Uranium) 0102
IX Analytical Data (Total Uranium) 0141
X Analytical Data (Isotopic Thorium) 0192
XI Analytical Data (Radium-226) 0231
XII Analytical Data (Radium-228) 0265
XIII Barium-133 Analytical Tracer Data 0281
XIV Analytical Data (Gross Alpha/Beta) 0310
Last Page 0329
0003
STANDARD OPERATING PROCEDURE f~LINE
Sample Receiving
LABORATORY DATA SUPPORT CHECKLIST
MP-001-3
Eberline Services Work Order # ___ 1_8_-_0_3_1 _1 _Q ____ _
The checklist items listed below are to be initialed by appropriate staff upon completion/verification.
Date for Partial Initials Date Initials Checklist Items
Sample Log-In
Data Compilation
First Technical Data Review
MP-001, Rev. 19 Effective: 2111118
Page 14 of 15
Second Technical Data Review
Data Entry/Electronic Deliverable
Case Narrative
Electronic Deliverable Proof
Samples Analyzed within Holding Time es? No?
Technical/Clerical Corrections, Signatures Needed, Problems, Etc Date/Initials
Date package approved by:
Laboratory Manager Date
Copy No. ___ _ Radiochemistry Services
0004
SECTION I
CHAIN OF CUSTODY &pH CHECK
0005
Chain of ustody Record ~ ~ ,: No 001 ~~ EB ER.LINE
- --------- Oak Ridgll, TN 31830 s e: RV! c 11: s (865) 481-0083 Pt,o410 • (85.5) 483-4621 Fl!X
~
Project Name: West Lake Stormwater Project Number:
Send Report To: Paul Rosasco Sampler (i?rint Name):~ PageJ_ ot_L Address: EMSI Sampler (Print Name):~'kt @ .,.,,,,,.,,~,,._
Shipment Method: Fed Ex
Airbill Number: ~? Ol '1,f J M Phone: Laboratory Receiving:
Fax:
'j ,.. • , ~ ample I Sample ample Number ol l Lab ::;ample l r-,eld Sample iD I Date Time Matrix . Containers (to oo completed by lab)
ru - , ... 00! ~ 1eo2r ~id -2
l
by:
::::::::> L per; Received by: (Signature)
~d~ elinquished by: Received by: {Signature)
Dale: Time:
la 2, ,s i ":ko Date: Time:
Sample Custodian Remarks (Completed By Laboratory):
QA/QC Level I Turnaround I Sample Receip!
Total # Containers Received?
/2~-Relinquished by: (Signature) ~ec~~gnat~
s-,9.J-,r (ri3d Date: 1me:
Level n Routine )( COC Seals Present? ;_j
level ll 0 24 Hour 0 COC Seals Intact? Leve! m 0 1 Week 0 Received Containers intact? Other • Other ___
Temperature?
0006
EBERLINE ~3E.PVIC.:Et_,
Oak Ridge Laboratory
Internal Chain of Custody
Comments
Location (circle one)
Received by ~ Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep
Received by Sample Storage Rough Prep
Relinquished by Sample Storage Rough Prep Prep ~
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Work Order#
Lab Deadline
Analysis
Sample Matrix
Sample Fraction
04
Count Room
Count Room
Count Room
Count Room
Count Room
Count Room
Count Room
Count Room
Count Room
Count Room
Count Room
Count Room
18-03110 4/12/2018
UUISO - Level 4 Water
HP 210 / 270 Storage Detector Activity Location
38 DDl.4
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Ini ials Date
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Printed: 3/23/2018 4:37 PM
0007
EBERLINE
Oak Ridge Laboratory
Internal Chain of Custody
Comments
Location (circle one)
Received by ~ Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Work Order# 18-03110 Lab Deadline 4/12/2018
Analysis KPA_LIQ - Level 4
Sample Matrix Water
Sample I HP 210 / 270 Storage Fraction Detector Activity Location
04 38 DDl.4
:
i I
Initi.als Date
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Printed: 3/23/2018 4:37 PM
0008
EBERLINE r::;Er<VIC'.E._~J
Oak Ridge Laboratory
Internal Chain of Custody
Comments
Location (circle one)
Received by ~ Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep
Received by Sample Storage Rough Prep Prep
Relinquished by Sample Storage Rough Prep Prep ~ Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
/'
Received by Sa~l~l Rough Prep Prep Separations
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Relinquished by Sample Storage Rough Prep Prep Separations
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Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Work Order#
Lab Deadline
Analysis
Sample Matrix
Sample Fraction
04
Count Room
Count Room
Count Room
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i
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18-03110 4/12/2018
ThlSO - Level 4 Water
HP 210 / 270 Storage Detector Activity Location
38 DDl.4
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Printed: 3123/2018 4:37 PM
0009
EBERLINE ~3Er~VIC'.EG
Oak Ridge Laboratory
Internal Chain of Custody
Comments
Location (circle one)
Received by ~ Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Separations
Received by Sample Storage Rough Prep Prep S~ns
Relinquished by Sample Storage Rough Prep Prep ~~ Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
~------Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Work Order#
Lab Deadline
Analysis
Sample Matrix
Sample Fraction
04
Count Room ,-::;--
Count Room
Count Room
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Count Room
Count Room
Count Room
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Count Room
Count Room
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' /
18-03110 4/12/2018
Ra226 - Level 4 Water
HP 210 / 270 Storage
Detector Activity Location
38 DDl.4
'
.Initials Date
'{j) 4:/i,, irs ii p 4/3/!8 os-s--e
Printed 3/23/2018 4 37 PM
0010
EBERLINE
Oak Ridge Laboratory
Internal Chain of Custody
Comments
Location (circle one)
Received by ~ Rough Prep Prep Separations
Relinquished by Sample Storage Separations
Received by Sample Storage Stp~ns
Relinquished by Sample Storage s~~s
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep <ieP.<!@liQns
Relinquished by Sample Storage Rough Prep Prep Sefl(l@!lbns
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by s Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Work Order#
Lab Deadline
Analysis
Sample Matrix
Sample Fraction
04
Count Room
Count Room
Count Room
Count Room
cE9 ~ Count Room
Count Room
Count Room
Count Room
Count Room
Count Room
18-03110 4/12/2018
Ra228 - Level 4 Water
HP 210 / 270 Storage
Detector Activity : Location
38 DDl.4
;
Initials Date
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Printed; 312312018 4 37 PM
0011
, ~EBER~~,~:.~
- Oak Ridge Laboratory
Internal Chain of Custody
Comments
Location (circle one)
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by ~e
Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Work Order#
Lab Deadline
Analysis
Sample Matrix
Sample Fraction
04
Count Room;;a
Count Room
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18-03110 4/12/2018
GaGbT ThSr-Level4 Water
; HP 210 / 270 • Storage
Detector Activity Location
38 DDl.4
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Printed: 3/23/2018 4:37 PM
0012
Printed: 3/23/2018 11:40 AM
,: Sample Receiving Report EBER~~~c~ (Volumes, pH, & CPM)
FR ClientID # Btls Comments Matrix
01 LCS 0 WA
02 BLANK 0 WA
03 DUP 0 WA
04 OU-1-008 ; 2 WA V Container Number oHOria
1 <2 2 <2
Re~(#~ Date.$-;).3-fr
Page 1 of 1
Internal Work Order -"-~-··-·· -·~·•-~-.----·-··- -~-·--- ·-----.--·---
18-03110
Storage DDl.4
DDl.4
DDl.4
DDl.4 oH Final
<2 <2
Received By
]BAILEY
Rec Vol Ttl CPM Max
7.52 38 Volume Ill CPM
3.7600 38 3.7600 36
MP-001, Rev 5
Effective: 11/22/02
0013
SECTION II
SAMPLE ACKNOWLEDGEMENT
0014
Client Name
AMO Environmental Decisions
Project Name
WESTLAKE
Internal ID Client ID
01 LCS
02 BLANK
03 DUP
04 OU-1-008
~ EBERLINE SERVICES
Sample Log In Report
Contract/PO Project Type
WESTLAKE Environmental
Client WO Sample Disp
WESTLAKE STORMWATER w
Sample Date Matrix Storage
03/23/18 WA DDl.4
03/23/18 WA DDl.4
03/23/18 WA DDl.4
03/19/18 18:02 WA DDl.4
Totals Per Analysis (non QA samples)
Oak Ridge Laboratory 601 Scarboro Rd. Oak Ridge, TN 37830
Voice: (865) 481-0683 Fax: (865) 483-4621
Date Received
03/23/2018 Lab Deadline
04/12/2018 f- ::J <D co 0 ~I I .0 ' N N (f) ('.) < N N
"' CL "' "' -" ('.) CL 0:: 0:: f- :::J
X X X X X X I I
X X X X X XI I
X X X X X XI I
X X X X X XI I I I
1 1 1 1 1 1 0 0
Invoice J West Lake Landfill OU-1 Resp
AMO Environmental DecIsIons
PO Box 410
Danboro, PA 18916
Voice 215-230-8282
Fax 215-230-8283
Contact Marsha Joseph
Voice 865-675-3669
Fax 865-675-3677
Required Turnaround Days .. ~. - •fl:!'l!l"•l7if,C:
28 18-03110 Internal Deadline ,- ..
04/19/2018 04/20/2018
I I I I I I I I I I I I I I I I~
I I I I I I I I I I I I I I I I I 6
I I I I I I I I I I I I I I I I I 6
I I I I I I I I I I I I I I I I I 6
I I I I I I I I I I I I I I I I I ' I I I I I I I I I I I I I I I I I
0 -0 -0 -0 -0 -0 -0
0 -0 -0 -0 -0 -0 -0 -0 -0
0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
Report Data Paul Rosasco, P E
Eng Management Support, Inc
7220 W. Jefferson Ave, Suite 406
Lakewood, CO 80235
Voice 303-940-3426
Fax
Printed· 3/23/2018 4·37 PM
0015
EBERLIN STANDARD OPERATING PROCEDURE MP-001, Rev. 19
Effective: 2111/18 Page 13 of 15 Sample Receiving
SAMPLE RECEIPT CHECKLIST MP-001-2
WORKORDER#_....._1__..8.._-____;,,,Q-'-3_1_1_Q_
SAMPLE MATRIX/MATRICES:
WERE SAMPLES:
Received in good condition?
If aqueous, properly preserved
WERE CHAIN OF CUSTODY SEALS:
Present on outside of package?
Unbroken on outside of package?
Present on samples?
Unbroken on samples?
Was chain of custody present upon sample receipt?
(CIRCLE ONE OR BOTH)
C6UEO~ NON-AQUEOUS
(CIRCLE EITHER YES, NO, OR N/A)
N
N N/A
0 N
@ N
If) N
m N
(iJ N -IF THE RESPONSE TO ANY OF THE ABOVE IS NO, A DISCREPANT SAMPLE RECEIPT REPORT
(DSR) HAS BEEN ISSUED.
REMARKS: ____________________________ _
SI~ DATE: 3~:i.J-J ~
Copy No. ___ _ Radiochemistry Services
0016
SECTION III
CASE NARRATIVE
0017
• EBERLINE
"j EBS-OR-43704
May 11, 2018
Paul Rosasco
SERVICES
Engineering Management Support, Inc. 7220 W. Jefferson Ave., Suite 406 Lakewood, CO 80235
SAMPLE RECEIPT
CASE NARRATIVE Work Order# 18-03110-0R
EBERLINE ANALYTICAL CORf'ORATION
601 SCt\f~BOFW f~0/1D
OAK RIDGE. TEf\lNESSEf: 78;)()
PHONE (861>) L,81 0683 FAX (865) 483·-4621
This work order contains one water sample received 03/23/2018. Sample was analyzed for Isotopic Uranium, Total Uranium by KPA, Isotopic Thorium, Radium-226/228 and Gross Alpha/Beta.
CLIENT ID
OU-1-008
ANALYTICAL METHODS
LAB ID
18-03 110-04
Isotopic Uranium was analyzed using EPA Method 908.0 Modified. Total Uranium was analyzed using Method ASTM D5174 Modified. Isotopic Thorium was analyzed using EPA Method 907.0 Modified. Radium-226 was analyzed using EPA Method 903.0 Modified. Radium-228 was analyzed using EPA Method 904.0. Gross Alpha/Beta was performed using EPA Method 900.0 Modified.
ANALYTICAL RESULTS
Combined Standard Uncertainty is reported at 1-sigma value.
Minimum Detectable Activity (MDA) values for data represented in this report are sample-specific. MDA measurements are determined based on factors and conditions including instrument settings, aliquot size and matrix type.
ISOTOPIC URANIUM
Sample was prepared by removing a representative aliquot followed by mixed acid digestions as appropriate. Uranium was selectively extracted by ion exchange. Uranium was eluted, micro-precipitated and mounted on micro-porous filter media. Sample activities were then determined by alpha spectroscopy using energy specific regions of interest for Uranium-234, Uranium-235 and Uranium-238. Chemical recovery was determined by the use of a Uranium-232 tracer. Activity of the Uranium-232 tracer was determined by alpha spectroscopy using an energy specific region of interest.
Sample demonstrated acceptable results for all Uranium analyses. Chemical recovery was acceptable for all samples. The Uranium-234, Uranium-235 and Uranium-238 method blank demonstrated acceptable results. Results for the Uranium-234, Uranium-235 and Uranium-238 duplicate demonstrated an
Page I of 3
0018
ANALYTICAL RESULTS CONTINUED
ISOTOPIC URANIUM CONTINUED
acceptable relative percent difference and normalized difference. Results for the Uranium-234 and
Uranium-238 laboratory control sample demonstrated an acceptable percent recovery.
TOT AL URANIUM
A volumetric aliquot of the sample was removed and wet ashed until clear. Sample was muffled and
diluted to a known volume. An aliquot was removed from this dilution. This aliquot was oxidized,
complexed with Chem-Check, Ura-Plex and subsequently analyzed using a kinetic phosphorescent
analyzer.
Sample demonstrated acceptable results for all Total Uranium analyses. Chemical recovery was
acceptable for all samples. The Total Uranium method blank demonstrated an acceptable result. Results
for the Total Uranium duplicate demonstrated an acceptable relative percent difference and normalized
difference. Results for the Total Uranium low and high calibration range laboratory control sample
demonstrated an acceptable percent recovery.
ISOTOPIC THORIUM
Sample was prepared by removing a representative aliquot followed by mixed acid digestions as
appropriate. Thorium was selectively extracted by ion exchange. Thorium was eluted, micro-precipitated
and mounted on micro-porous filter media. Sample activities were then determined by alpha spectroscopy
using energy specific regions of interest for Thorium-228, Thorium-230 and Thorium-232. Chemical
recovery was determined by the use of a Thorium-229 tracer. Activity of the Thorium-229 tracer was
determined by alpha spectroscopy using an energy specific region of interest.
Sample demonstrated acceptable results for all Thorium analyses. Chemical recovery was acceptable for
all samples. The Thorium-228, Thorium-230 and Thorium-232 method blank demonstrated acceptable
results. Results for the Thorium-228, Thorium-230 and Thorium-232 duplicate demonstrated a high
relative percent difference; however, normalized difference is within acceptable limits for the analytical
technique. Results for the Thorium-228, Thorium-230 and Thorium-232 laboratory control sample
demonstrated an acceptable percent recovery.
RADIUM-226
Sample was prepared by removing a representative aliquot followed by mixed acid digestions as
appropriate. This was followed by precipitations of Radium/Barium Sulfate. Precipitates were dissolved
in alkaline EDT A. Radium was selectively precipitated and then mounted on micro-porous filter media.
Sample was counted by alpha spectroscopy using an energy specific region of interest for Radium-226.
Inherent self-absorption from elemental Barium was corrected for in the final result. Chemical recovery
was calculated by the use of a Barium-133 tracer, which was determined by HPGe gamma spectroscopy.
Sample demonstrated acceptable results for all Radium-226 analyses. Chemical recovery was acceptable
for all samples. The Radium-226 method blank demonstrated an acceptable result. Results for the
Radium-226 duplicate demonstrated an acceptable relative percent difference and normalized difference.
Results for the Radium-226 laboratory control sample demonstrated an acceptable percent recovery.
Page 2 of 3
0019
'
ANALYTICAL RESULTS CONTINUED
RADIUM-228
Following alpha spectroscopy analysis of Radium-226, Barium/Radium Sulfate precipitates were
redissolved and allowed for sufficient ingrowth of the Actinium-228 daughter. After ingrowth, Actinium-
228 was selectively precipitated. Precipitates were filtered and beta emissions for Actinium-228 were then
counted on a gas proportional counter. Chemical recovery was determined by the use of a Barium-133
tracer, the activity of which was determined by HPGe gamma spectroscopy and an elemental Yttrium
caITier by gravimetric measurements. The product of these two recoveries was used to calculate chemical
yield.
Sample demonstrated acceptable results for all Radium-228 analyses. Chemical recovery was acceptable
for all samples. The Radium-228 method blank demonstrated an acceptable result. Results for the
Radium-228 duplicate demonstrated a high relative percent difference; however, normalized difference is
within acceptable limits for the analytical technique. Results for the Radium-228 laboratory control
sample demonstrated an acceptable percent recovery.
GROSS ALPHA & BET A
Sample was prepared by evaporation of a representative volumetric aliquot acidified with HN03•
Reduced sample was then transfeITed to a steel planchet for final evaporation to dryness and flaming.
Sample was then counted on a gas proportional counter. Results were coITected as required for inherent
self-absorption based on residual mass present.
Sample demonstrated acceptable results for all Gross Alpha and Beta analyses. The Gross Alpha and Beta
method blank demonstrated acceptable results. Results for the Gross Alpha duplicate demonstrated a high
relative percent difference; however, normalized difference is within acceptable limits for the analytical
technique. Results for the Gross Beta duplicate demonstrated an acceptable relative percent difference and
normalized difference. Results for the Gross Alpha and Beta laboratory control sample demonstrated an
acceptable percent recovery.
CERTIFICATION OF ACCURACY
I certify that this data report is in compliance with the terms and conditions of the Purchase Order, both
technically and for completeness, for other than the conditions detailed above. Release of the data
contained in this hard copy data package has been authorized by the cognizant project manager or his/her
__ de§_jgnee to be accurate as verifi by the following signature.
M.R. McDougall ------------Laboratory Manager
Date: 5/11/2018
Eberline /\nalytical wants and encourages your feedback regarding our performance providing radioanalytical services. Please
visit http://eberlineanalytical.com/ to provide us with feedback on our services.
Page 3 of 3
0020
SECTION IV
ANALYTICAL RESULTS SUMMARY
0021
Printed: 5/11/2018 2:16 PM Page 1 of 2
Report To: Work Order Details:
Eberline Analytical Paul Rosasco, P.E. SDG:: 18-03110 ,•o•m•••••••••-••••-• --~-- •--•••• .. ' ·- -· ·- ~-,,, .... ,, .. ,
--~-----~l1JJ.:~am1_9_~ment Support1_Jnc. Project:: WEST LAKE Stormwater
Final Report of Analysis 7220 W. Jefferson Ave, Suite 40,~ Analysis Category: : ENVIRONMENTAL ·------------Lakewood, CO 80235 Sample Matrix:
1 WA Lab Sample Client Sample Receipt Analysis Batch
Analyte Method Result cu Report
ID Type : ID Date Date Date ID CSU MDA i CV
Units
18-03110-01 LCS KNOWN 03/23/18 00:00 3/23/2018 1 3/27/2018 1
18-0311 0 I Gross Alpha EPA 900.0 Modified 2.68E+02 I 1.15E+01 I I pCi/I
18-03110-01 LCS I SPIKE 03/23/18 00:00 3/23/2018 . 3/27/2018 i 18-03110 Gross Alpha EPA 900.0 Modified 3.10E+02 ! 3.98E+00 3.41E+01 2.54E-01 3.14E-01 pCin
18-03110-02 MBL I BLANK 03/23/18 00:00 3/23/2018 ; 3/27/2018 ; 18-03110 Gross Alpha EPA 900.0 Modified 3.97E-02 1.35E-01 1.35E-01 3.01E-01 3.65E-01 pCin
18-03110-03 DUP . OU-1-008 03/19/18 18:02 3/23/2018 3/27/2018 : 18-03110 Gross Alpha EPA 900.0 Modified 2.80E+00 , 1.94E+00 1.97E+00 3.35E+00 6.04E-01 pCin
I 3/23/2018 I 3/27/2018 : 18-03110
---18-03110-04 DO OU-1-008 03/19/18 18:02 Gross Alpha EPA 900.0 Modified 4.25E+00 1.96E+00 2.02E+00 2.55E+00 4.82E-01 pCi/I
:
18-03110-01 LCS KNOWN 03/23/18 00:00 3/23/2018 : 3/27/2018 i 18-03110 Gross Beta EPA 900.0 Modified 2.77E+02 8.30E+00 i pCin -----
18-03110-01 LCS : SPIKE 03/23/18 00:00 3/23/2018 3/27/2018 [ 18-03110 Gross Beta EPA 900.0 Modified 2.82E+02 ! 3.15E+00 3.91E+01 6.12E-01 1.95E+00 pCi/I
18-0311 0-02 MBL BLANK 03/23/18 00:00 3/23/2018 , 3/27/2018 i 18-03110 Gross Beta EPA 900.0 Modified -2.37E-01 2.57E-01 2.59E-01 5.78E-01 i 1.81E+00 1
pCin "---
18-03110-03 DUP OU-1-008 03/19/18 18:02 3/23/2018 ; 3/27/2018 I 18-03110 , Gross Beta EPA 900.0 Modified 1.95E+01 2.46E+00 3.64E+00 3.43E+00 7.70E+00 ; pCin
18-03110-04 DO OU-1-008 03/19/18 18:02 3/23/2018 i 3/27/2018 I 18-03110 i Gross Beta EPA 900.0 Modified 1.69E+01 2.31E+00 3.29E+00 3.30E+00 7.31E+00 pCin
I : . i : --
18-03110-01 LCS KNOWN 03/23/18 00:00 3/23/2018 4/2/2018 18-03110 Radium-226 EPA 903.0 Modified 1.00E+01 4.61E-01 pCi/I
18-03110-01 LCS . SPIKE 03/23/18 00:00 3/23/2018 i 4/2/2018 18-03110 1 Radium-226 EPA 903.0 Modified 9.91E+00 1.37E+00 2.50E+00 4.41E-01 5.56E-02 i pCin
18-03110-02 MBL : BLANK 03/23/18 00:00 3/23/2018 I 4/2/2018 ! 18-03110 Radium-226 EPA 903.0 Modified 2.23E-01 : 2.41E-01 2.45E-01 3.62E-01 I 3.68E-02 pCi/I ---
18-03110-03 DUP I OU-1-008 03/19/18 18:02 3/23/2018 4/2/2018 I 18-03110 Radium-226 EPA 903.0 Modified I I 1.19E-01 I 1.54E-01 1.56E-01 2.44E-01 2.36E-02 pCi/I
18-03110-04 DO OU-1-008 03/19/1818:02 3/23/2018 I 4/2/2018 ; 18-03110 Radium-226 EPA 903.0 Modified 1.47E-01 I 1.29E-01 1.33E-01 1.55E-01 1.54E-02 pCin
I I
18-03110-01 LCS KNOWN 03/23/18 00:00 3/23/2018 . 4/9/2018 i 18-03110 Radium-228 EPA 904.0 8.96E+00 ; 4.57E-01 I pCin
I
18-03110-01 LCS i SPIKE 03/23/18 00:00 3/23/2018 I 4/9/2018 ! 18-03110 Radium-228 EPA 904.0 8.43E+00 7.20E-01 2.04E+00 8.65E-01 1.06E-01 pCin
18-03110-02 MBL j BLANK 03/23/18 00:00 3/23/2018 i 4/9/2018 i 18-03110 Radium-228 EPA 904.0 2.64E-01 i 3.20E-01 3.25E-01 6.54E-01 1.07E-01 ! pCin
18-03110-03 DUP I OU-1-008 03/19/18 18:02 3/23/2018 : 4/9/2018 18-03110 Radium-228 EPA 904.0 9.25E-01 3.72E-01 4.27E-01 6.88E-01 1.06E-01 I pCi/1 I
18-03110-04 DO I OU-1-008 03/19/18 18:02 3/23/2018 ! 4/9/2018 ! 18-03110 Radium-228 EPA904.0 1.49E-01 3.36E-01 3.38E-01 7.03E-01 1.05E-01 I
pCin i I ; : i
18-03110-01 LCS : KNOWN 03/23/18 00:00 3/23/2018 ' 3/30/2018 : 18-03110 1
Thorium-228 EPA 907.0 Modified 4.80E+00 i 1.73E-01 •
pCin
18-03110-01 LCS I SPIKE 03/23/18 00:00 3/23/2018 1 3/30/2018 I 18-03110 Thorium-228 EPA 907.0 Modified 5.81E+00 , 1.09E+00 1.22E+00 1.20E-01 1.66E-02 pCi/I :
18-03110-02 MBL . BLANK 03/23/18 00:00 3/23/2018 3/30/2018 18-03110 Thorium-228 EPA 907.0 Modified 5.29E-03 3.43E-02 3.43E-02 9.33E-02 1.30E-02 : pCin
18-03110-03 DUP OU-1-008 03/19/1818:02 3/23/2018 3/30/2018 18-03110 Thorium-228 EPA 907.0 Modified -3.87E-02 7.02E-02 7.03E-02 1
2.14E-01 4.16E-02 pCin
18-03110-04 DO OU-1-008 03/19/18 18:02 3/23/2018 , 3/30/2018 18-03110 Thorium-228 EPA 907.0 Modified 3.44E-03 1.14E-01 1.14E-01 2.74E-01 9.26E-02 i pCin i
i :
18-03110-01 LCS I KNOWN 03/23/18 00:00 3/23/2018 i 3/30/2018 18-03110 Thorium-230 EPA 907.0 Modified 5.37E+00 1.45E-01 pCin
18-03110-01 LCS SPIKE 03/23/18 00:00 3/23/2018 I 3/30/2018 18-03110 Thorium-230 EPA 907.0 Modified 6.64E+00 1.22E+00 1.47E+00 1.34E-01 1.25E-01 i pCin
18-03110-02 MBL i BLANK 03/23/18 00:00 3/23/2018 ; 3/30/2018 18-0311 0 , Thorium-230 EPA 907.0 Modified 1.07E-01 i 9.52E-02 9.61E-02 1.18E-01 1.06E-01 pCin
18-03110-03 DUP OU-1-008 03/19/18 18102 3/23/2018 3/30/2018 18-03110 Thorium-230 EPA 907 .0 Modified 1.60E-01 1.59E-01 1.61E-01 2.03E-01 1.90E-01 pCin
18-03110-04 DO OU-1-008 03/19/18 18:02 3/23/2018 i 3/30/2018 18-03110 Thorium-230 EPA 907.0 Modified I 2.83E-01 ' 1.99E-01 2.02E-01 1.85E-01 1.77E-01 pCin i
CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample; MBL=Blank; DUP=Duplicate; TRG=Normal Sample; DO=Duplicate Original; CV=Critical Value
( . EBERLINE
~ ANALYT!CAL
EBERLINE CAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
0022
Printed: 5/11/2018 2:16 PM Page 2 of 2
Report To: Work Order Details:
Eberline Analytical .................... Paul Rosasco, P.E,:________ _ SDG:: 18-03110 ...... , .... ·•-·~ ·~~ ... ,,,_.,, •.. _~ •-'••·. --·-·-··-···-""- ·-··--·-
Eng. Management Support, Inc. _ -·· Project: j WEST LAKE Stormwater
Final Report of Analysis """"~•--·
7220 W. Jefferson Ave, Suite 406 . Analysis Category: ! ENVIRONMENTAL ------~-~-Lakewood, CO 80235 Sample Matrix: : WA
Lab Sample Client Sample Receipt Analysis Batch I Report I
Analyte Method ' Result cu CSU MDA CV ID Type ID Date Date : Date ID I Units
18-03110.01 LCS KNOWN 03/23/18 00:00 3/23/2018 • 3/30/2018 : 18-03110 Thorium-232 EPA 907.0 Modified ; 4.80E+00 1.73E-01 : pCi/1 ---18-03110-01 LCS SPIKE 03/23/18 00:00 3/23/2018 3/30/2018 • 18-03110 Thorium-232 EPA 907.0 Modified 5.80E+00 1.09E+00 1.21E+00 1.65E-01 4.54E-02 pCi/1
18-03110-02 MBL BLANK 03/23/18 00:00 3/23/2018 3/30/2018 ' 18-03110 Thorium-232 EPA 907.0 Modified -3.80E-03 6.11E-02 6.11E-02 1.50E-01 5.53E-02 pCi/I
18-0311 0-03 DUP OU-1-008 03/19/1818:02 3/23/2018 : 3/30/2018 : 18-03110 Thorium-232 EPA 907.0 Modified 1.58E-02 6.57E-02 6.57E-02 1.69E-01 1.97E-02 pCi/1
18-03110-04 DO OU-1-008 03/19/18 18:02 3/23/2018 : 3/30/2018 I 18-03110 Thorium-232 EPA 907.0 Modified -5.87E-03 6.64E-02 6.64E-02 2.04E-01 4.00E-02 pCi/1 -·-· - ---------
:
18-03110-01 LCS : KNOWN 03/23/18 00:00 3/23/2018 : 3/27/2018 : 18-03110 Total Uranium ASTM D5174 Modified 8.00E+00 1.60E-01 ug/I
18-03110-0H LCSH KNOWN-H 03/23/18 00:00 3/23/2018 I 3/27/2018 1 18-03110 Total Uranium ASTM D5174 Modified I 2.00E+02 4.00E+00 ug/I
18-03110.01 LCS SPIKE 03/23/18 00:00 3/23/2018 i 3/27/2018 , 18-03110 Total Uranium ASTM D5174 Modified 8.65E+00 1.88E-01 2.69E+00 1.01E+00 i 1.01E+00 ug/1 --
18-03110-0H LCSH SPIKE-H 03/23/18 00:00 3/23/2018 i 3/27/2018 1 18-03110 Total Uranium ASTM D5174 Modified 1.96E+02 3.99E+00 6.10E+01 1.01E+00 1.01E+00 ug/1
18-0311 0-02 MBL BLANK 03/23/18 00:00 3/23/2018 : 3/27/2018 i 18-03110 Total Uranium ASTM D5174 Modified 0.00E+00 1.01E+00 1.01E+00 1.01E+00 1.01E+00 ug/1 --
18-03110-03 DUP OU-1-008 03/19/18 18:02 3/23/2018 3/27/2018 : 18-03110 Total Uranium ASTM D5174 Modified j 4.12E+00 9.50E-02 1.28E+00 1.01E+00 1.01E+00 ug/1
18-03110-04 DO OU-1-008 03/19/18 18:02 3/23/2018 3/27/2018 • 18-03110 : Total Uranium ASTM D5174 Modified 4.23E+00 1 9.91E-02 1.32E+00 1.01E+00 1.01E+00 : ug/1
: 18-03110.01 LCS KNOWN 03/23/18 00:00 3/23/2018 i 3/30/2018 i 18-03110 Uranium-234 EPA 908.0 Modified 7.28E+00 l 2.62E-01 pCi/1
18-03110-01 LCS SPIKE 03/23/18 00:00 3/23/2018 ; 3/30/2018 1
18-03110 1 Uranium-234 EPA 908.0 Modified 6.06E+00 8.95E-01 9.95E-01 6.70E-02 7.31E-03 pCi/1
18-03110-02 MBL BLANK 03/23/18 00:00 3/23/2018 i 3/30/2018 : 18-03110 Uranium-234 EPA 908.0 Modified -9.93E-03 3.02E-02 3.03E-02 8.24E-02 1.26E-02 pCVI
18-03110-03 DUP OU-1-008 03/19/18 18:02 3/23/2018 · 3/30/2018 : 18-03110 Uranium-234 EPA 908.0 Modified i 1.17E+00 1 3.65E-01 3.74E-01 1.52E-01 2.62E-02 ' pCi/1
18-0311 Q.04 DO OU-1-008 03/19/18 18:02 3/23/2018 3/30/2018 ; 18-03110 Uranium-234 EPA 908.0 Modified 1.06E+00 3.62E-01 3.69E-01 1.48E-01 1.95E-02 pCi/1
; 18-03110-01 LCS i SPIKE 03/23/18 00:00 312312018 , 313012018 I 18-0311 o Uranium-235 EPA 908.0 Modified 4.67E-01 1.87E-01 1.90E-01 : 1.04E-01 1.55E-03 pCi/1
18-03110-02 MBL BLANK 03/23/18 00:00 3/23/2018 . 3/30/2018 I 18-03110 Uranium-235 EPA 908.0 Modified 5.76E-03 1 3.73E-02 3.73E-02 1.02E-01 1.15E-02 I pCi/1
18-03110-03 DUP I OU-1-008 03/19/1818:02 3/23/2018 3/30/2018 i 18-03110 Uranium-235 EPA 908.0 Modified 1.14E-01 I 1.24E-01 1.24E-01 1.50E-01 1.14E-02 pCi/I
18-03110-04 DO OU-1-008 03/19/1818:02 3/23/2018 : 3/30/2018 i 18-03110 Uranium-235 EPA 908.0 Modified 9.83E-02 i 1.19E-01 1.19E-01 I 1.45E-01 7.90E-03 pCi/1
I i : : :
18-0311().01 LCS . KNOWN 03/23/18 00:00 3/23/2018 i 3/30/2018 / 18-03110 Uranium-238 EPA 908.0 Modified 7.06E+00 2.54E-01 : pCi/1
18-03110-01 LCS : SPIKE 03/23/18 00:00 312312018 I 313012018 i 18-03110 Uranium-238 EPA 908.0 Modified 6.13E+00 9.03E-01 1.00E+00 6.67E-02 7.09E-03 pCi/1 ·-
18-03110-02 MBL : BLANK 03/23/18 00:00 3/23/2018 • 3/30/2018 , 18-03110 Uranium-238 EPA 908.0 Modified -2.91E-04 • 3.09E-02 3.09E-02 9.16E-02 1.73E-02 : pCi/1
18-03110-03 DUP I OU-1-008 03/19/1818:02 312312018 I 313012018 18-03110 Uranium-238 EPA 908.0 Modified 9.26E-01 3.18E-01 3.25E-01 1.21E-01 1.28E-02 pCi/1
18-03110-04 DO OU-1-008 03/19/18 18:02 3/23/2018 1 3/30/2018 i 18-03110 Uranium-238 EPA 908.0 Modified 1.04E+00 3.59E-01 3.67E-01 1.68E-01 4.68E-03 . pCi/1
CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample; MBL=Blank; DUP=Duplicate; TRG=Nonmal Sample; DO=Duplicate Original; CV=Critical Value
( . EBERLINE :@ ANALYTICAL
EBERLINE CAL CORPORATION
601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/ 483-4621
0023
SECTIONV
ANALYTICAL STANDARD
0024
. . ., ·,, ·.>;~
QA/QC REVIEWED CERTIFICATE OF CALIBRATION
Date t,q(lnitialsJ/£ ALPHA STANDARD SOLUTION
Radionuclide: U-238NAT
Half Life:
Customer:
P.O.No.:
TMA EBERLINE
OR2778
Catalog No.:
(4.468 ± 0.005) x lOA9 years
7338 Reference Date: January 1 1995 12:00 PST.
Source No.: 479-50 Contained Radioactivity: (Total U) 8.016 µ,Ci
Contained Radioactivity: (Total U) 297 kBq
Description of Solution a. Mass of solution:
b. Chemical form:
65.2896 gin a 50 ml flame sealed ampoule
Uranyl Nitrate in H2O
c. Carrier content: None
d. Density: Approximately 1.3202
Radioimpurities
Radioactive Daughters
Refer to attached technical data sheet
Refer to attached technical data sheet
Radionuclide Concentration
(Total U) 0.1228
Method of Calibration
Activity calculations are based upon known specific activity and mass.
Uncertainty of Measurement
a. Systematic uncertainty in instrument calibration:
b. Random uncertainty in assay:
c. Random uncertainty in weighing(s):
d. Total uncertainty at the 99 % confidence level:
NIST Traceability
±3,0%
±0,0%
±2,0%
±3,6%
•
g/ml @20°c.
µCi/g.
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Leak Test(s)
See reverse side for Leak Test(s) applied to this source.
Notes
1. Nuclear daw. were taken from "Table of Radioactive Isotopes•, edited by Virginia S. Shirley, 1986.
()..-8
2. IPL participates in an NIST measurement assurance program to e.tablish and maintain implicit traceability for a number of nuclides,
based on the blind assay (and later NIST certification) of Standard Reference Materials (As in NRC Regulatory Guidi: 4. I 5).
I .. · .... ~~.· .. · .. •.•t.·•··· ... ·.·/.·'·.··.• ... · .. \; .•....•...• ·•.·.··. '.l'J/. '·, ,_. ·. ··-.
. . .
ISOTOP.E
P R O [) ll C T .S
l,AB.ORATO!Ur:S
ISOTOPE PRODUCTS LABORATORIES
3017 N. SAN FERNANDO BLVD.
BURBANK, CALIFORNIA 91504
818 •843•7000 FAX 818 •843•6168
_,.._,,.
, ',,
lE(},lvAu...47 YCONfROL
~ t7et-fgv1~ 1931f-Date Signed
. ··, ',.•\''' ·,• .. '-'·.-·•" ! ,',' •,
0025
, ~--~-f;;;Rl,-1 N E I ~ ;,f:RVICf!S
QUALITY CONTROL PROGRAM MP-009
Rev.a; 11/01/03 Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY RADIOACTIVE REFERENCE SOLUTIONS PRIMARY DILUTION RECERTIFICATION
MP009
CURRENT DATE 7/12/2017 0:00
SOLUTION REFERENCE #r-lP_L_4 __ 7 __ 9-,,.5-o--.. -. ----- SOLUTION # ·. · . · ' u,;.a . · .
Half Life, Years Half Life, Days
I ., 4.46aE+oel I .1.e32E+12I
Radionuclide ...• • ... ~;~U
Certified Activity 8:016~+00 µCi Certified Concentration · · , . µCi per gram
Ampoule /Solution Gross Empty Ampoule
Solution Net Total Activity in Ampoule
Referen~e Date._l __ ·.-'· 1 .... 11 __ 11_9_9_5 __ 0:_oo_,!
· .. _. · .•97:6400 Weight, Grams
· .. 32;5020 Weight, Grams 65.1380 Weight, Grams
8.0160 µCl
Chemical Com osition of Standard Solution
Dilution Instructions: Dilution Solvent Used
Dilute to a volume ofj 1000;00. · !milliliters
Certified Total Activity ofl 8.0160jµCi Which EQuals . 1.780E+07jdpm at the date listed above
. . This activity concentration is based on the original
· And after dilution the activity of this solution isl _ 1. 77955E+04jdpm/m•eference date listed above, All activities are corrected to the date and time of analysis by the laboratory data
processing software.
Expiration Date:! June 28, 2018
Date: 7/12/2017 0:00 -------Date: __ 7_/_2';_$.,._/1 ___ 1_
0026
Rev.a; 11101103 Title: Radioactive Reference Standardi; Solutions & Records
EBERLINE SERVICES-OAK RIDGE LABORATORY RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION
MP-009 Date 7/12/2017 0:00
Solution Reference # IPL479~5o · Solution # U-Sa
Princi al Radionuclide Half Life, Years
~;2:1?,238l): !· . 4A6SE+oa! Half Life, Da):'.S I . 1.632E+12I
Radionuclide of Interest . 2.34: 2a,s.: ~~u; Reference Date!: ·'. ,1/1/19950:0o)
Parent Solution Cone. 17798E+04 · dpmlml
Chemical Com osition of Standard Solution
Uranly Nitrate.in 11V!'.J-JN03 : :
Dilution Instructions: Dilution Solvent Used !1MHNQ; · .. ••·
SECONDARY VOLUMETRIC DILUTION
Vol. Parent Solution: . . .·· > :ltOOOO ml
Total Activity: 7.1182E+04 dpm Final Volume: · ·. · 1000;00 ml
NOTES:
Final Activity Concentration:! 7.1182E+01 jdpmfml
This activity concentration is based on the original reference date listed above. All activities are corrected to the date and time of analysis by the laboratory data processing software.
1-------------------------, Isotopic Distribution as: U-238 Atom % = 48.239 U-235 Atom % = 2.25 U-234 Atom% .a 49.501 All values +/- 3.6%
U-238 = 71.162 dpm/rnl X 0.46249 "'34.345 dpmlml U-235 = 71.162 dpmlml X 0.0225 = 1.602 dpmlml U-236 = 71.162 dpmlml X 0.49501 .a 35.236 dpmlml
Isotopic ratios from manufacturer's d~ta sheet
Vertfied&Appr~
Expiration Date:i June 28, 2018
0027
RECORD co~·y Tracer Solution for Environmental Analysis & Disequilibrium Studies
Description
Product Description & Measurement Certificate
Principal radionuclide: Daughter Nuclide:
uranium 232 (U-232) Th-228
Product code: UDPl 0050 Batch Number: 92/232/67
Measurement Reference date: 01 March2000
Accuracy
Radionuclidic
Purity
Isotopic Purity
Chemical Composition
Physical Data
Remarks
Approved Signatory
Radioactive concentration U-232 which is equivalent to
Volume of solution Total activity ofU-232
which is equivalent to
6.739E+o3 becquerels per gram of solution
l.821E-0l microcuries per gram of solution
5.035 millilitres 3.61E+o4 becquerels 9.76E-0l microcuries
Method of measurement (see reverse of this certificate)
Random uncertainty is: ± 0. 7% Systematic uncertainty: ± 0.5%
Overall uncertainty in the radioactive concentration quoted above: ± 1.7%
Overall uncertainty is defined on the reverse of this certificate.
Any radioactive impurities measured are listed below, expressed as percentages
of the activity of the principle radionuclide at the reference date.
Th-228 and daughter activity removed 2 Feb 2000
U-232 daughters activity will increase with time. By alpha 88% U-232, 12% daughters on 1/3/00
,.,.ne isotopic composition, exprP.ssed as atom per cent at the reference date .
1'-l'ot measured
Calculated weight ofU-232, 4.42E-08 grams, as 2M HN03 solution in a flame sealed glass vial.
This Tracer solution has been produced 'carrier free'.
Recommended halflifo of uranium 232: 6.980E+0l years
Principle energies of alpha emissions {MeV): 5.26331 .7%, 5.320 68.0%
Branching ratio for alpha emission: 100%
Calculated specific activity of uranium 232: 8. 167E+o5 Bq per microgram U•232.
For safety information and notes to ensure correct usage by all persons handling this radior1ctive Tracer
solution please read the instructions accompanying the package.
AEA Technology operates a quality management system which has been independently audited and
approved to ISO 9001.
Project Ref. AE23 l 5
Roger Wiltshi.re
Prepared and characteri:;;ed in the UK, for world wide distribution by Isotrak, AEA Technology, QSA.
Trkcert.wps 10/03/00 AEA Technrilogy is the trading name of AEA Technology pie
0028
Rev.8; 11/01/03
QUALITY CONTROL PROGRAM MP-009
Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY
RADIOACTIVE REFERENCE SOLUTIONS
PRIMARY DILUTION RECERT/FICA T/ON
MP009
CURRENT DATE 10/7/2017 0:00
SOLUTION REFERENCE # ,...A_E_A/_A_m_e_rs_h_a_m_9_2/-2-32_/_67--, SOLUTION # 1--------,U...,._..,.1-=-o----1
Princi al Radionuclide 232u
Radionuclide 232U
Half Life, Years
I· 7.200E+01 I
Certified Activity 9. 760E-01 µCi
Certified Concentration µCi per gram .__ ___ _.
Half Life, Days
I 2.630E+04l
Reference Date 1~ ___ 3/_1/_2_0_00_0:_0~0 I
Ampoule /Solution Gross~Weight, Grams
Empty Ampoule Weight, Grams
Solution Net Weight, Grams
Total Activity in Ampoule 0.9760 µCi
Chemical Composition of Standard Solution
Dilution Instructions: Dilution Solvent Used
Dilute to a volume of I 1000. 00 I milliliters
Certified Total Activity of! 0.9760lµCi Which Eauals 2.167E+06ldpm at the date listed above
And after.dilution the activity of this· solution isl 2.167E+03jdp'm/ml This activity concentration is based on the original
reference date listed above. All activities are
corrected to the date and time of analysis by the
laboratory data processing software.
Expiration Date: I October 4, 2018
10/7/2017 0:00
Date:
0029
( EBERLINE ~ , ~,I !"1-✓ I• l '•
Rev.8; 1110110·3
QUALITY CONTROL PROGRAM , MP-009
Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY ·
RADIOACTIVE REFERENCE STANDARD SOLUTIONS SECONDARY DILUTION RECERTIFICATION
MP-009 Date 10/7/2017 0:00 1----------i
Solution Reference # AEA/Amersham 92/232/67 Solution # U-1 Oa
Principal Radionuclide 3 ,LJ
Half Life, Years Half Life, Days
I 7 .200E+01 I I 2.630E+04I
R_adionuclide of Interest' 232
U I Parent Solution Cone._ 2.167E+03 dpm/ml
Reference Date~l ___ 3_/1_/2_0_0_0_0_:o~ol
Chemical Composition of Standard Solution
Dilution Instructions: Dilution Solvent Used
SECONDARY VOLUMETRIC DILUTION
Vol. Parent Solution: Total Activity: Final Volume:
NOTES:
10.0000 ml 2.1670E+04 dpm
1000.00 ml
~--------------
Final Activity Concentration:! 2.1670E+01 I dpm/ml
This activity concentration is based on the original
reference date listed· above. All activities are ·
corrected to the date and time of analysis by the
laboratory data processing software. ·
Expiration Date:! October 4, 2018
Verified & Approved By_=~---"'.=rT"'"'ll='===--~--~>-s----~.,_ ____ _,,, ______ _
QC Approval _..,__....,..:.{,W,,µ..<-J---.i-..:;;.._-"'-..J,-,,t-.-..::.i.,="'---
0030
C!Irrtifi.catr of J\uaJ~ziz
Standard Reference Material® 3164
Uranium Standard Solution
Lot No. 080521
This Standard Reference Material (SRM) is intended for use as a primary calibration standard for the quantitative
determination of uranium. One unit of SRM 3 l 64 consists of five 10 mL sealed borosilicate glass ampoules of an
acidified aqueous solution. The solution contains nitric acid at a volume fraction of approximately 10 %.
Certified Value of Uranium: 9.994 mg/g ± 0.016 mg/g
The certified value is based on ( 1) gravimetric preparation using high-purity uranium oxide (U30 8) and
(2) inductively coupled plasma optical emissi011 spectrometry (TCP-OES) using four primary standards
independently prepared from high-purity uranium metal.
The uncertainty in the certified value is calculated as
U = kuc
where k = 2.14 is the coverage factor for a 95 % confidence interval. The quantity u, is the combined standard
uncertainty calculated according to the ISO Guide [ l]. The value of u0 is intended to represent, at the level of one
standard deviation, the combined effect of uncertainty components associated with the gravimetric preparation, the
lCP-OES determination, and method bias [2].
Expiration of Certification: The certification of SRM 3164 Lot No. 080521 is valid, within the measurement
uncertainty specified, until 20 July 2020, provided the SRM is handled in accordance with instructions given in this
certificate (see "Instructions for Use"). This certification is nullified if the SRM is damaged, contaminated, or
otherwise modified.
Maintenance of Certification: NIST will monitor this SRM over the period of its certification. If substantive
technical changes occur that affect the certification before the expiration of certification, NIST will notify the
purchaser. Registration (see attached sheet-) will facilitate notification.
Coordination of the technical measur~ leading to the certification of SRM 3164 was provided by
M.R. Winchester of the NIST Analytical Chemistry Division.
This SRM was prepared by T.A. Butler of the NIST Analytical Chemistry Division. The TCP-OES analysis was
performed by T.A. Butler and M.R. Winchester of the NIST Analytical Chemistry Division. Primary standards for
ICP-OES calibration were prepared by T.A. Butler of the NIST Analytical Chemistry Division. ;-
Statistical consultation was provided by S.D. Leigh of the NIST Statistical Engineering Divisidn.
Support aspects involved in the issuance of this SRM were coordinated through the NIST Measurement Services
Division.
Gaithersburg, MD 20899 Certificate Issue Date: 25 August 2009
SRM 3164
Stephen A. Wi~, Chiei
Analytical Chemistry Ii)ivision
Robert L. Watters, Jr., Chief
Measurement Services Division
Page I of3
0031
( E 8 ~ R ~l,~,~ : QUALITY ~~~o~~OL PROGRAM
Rev 8; 11/01/03 Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES -OAK RIDGE LABORATORY
RADIOACTIVE REFERENCE STANDARD SOLUTIONS INITIAL DILUTION
MP-009 Date 11/10/20170:00
Solution Reference # NlST3J64 Lot# 080521 Solution # •.... u~12
Princi al Radionuclide Natural U .
Half Life, Years 1 4.46as+o91
Half Life, Days I ·1.632E+12!
Radionuclide of Interest N~tllri'.iU.J, .. ·, Reference Date! '----"··..a.ff_/2_5'--/2~0_09-'-:-o_:O=Oj
Parent Solution Cone. .. 9 .. 99E+00· · ·· mglg
Chemical Com osition of Standard Solution
Dilution Instructions:
Vol. Parent Solution: Total Mass;
Final Volume:
NOTES:
Dilution Solvent Used
PRIMARY VOLUMETRIC DILUTION
·. 1:00QO g 9.9940E+00 mg
1000:0Q ml Final Mass Concentration:
Rounded Concentration: 9.9940E+03 nglg 1.0000E+04 nglg
This concentration is based on the original reference
date listed above.
Expiration Date:I November 9, 2018
Date: November 11, 2017
Date: i1 lei7 I I
0032
QUALITY CONTROL PROGRAM MP-009
Rev.8; 11 /01 /03 Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY
RADIOACTIVE REFERENCE STANDARD SOLUTIONS SECONDARY DILUTION (Recertification)
MP-009
Princi al Radionuclide NaturalU
Half Life, Years I · AA68E;+09.l
Half Life, Days I 1.632E+12I
Radionuclide of Interest N;).fura(JJ .. Reference Date! · 8/25/20090:00!
Parent Solution Cone. 1'.008+02 ng/ml
U-15-5
Chemical Com osition of Standard Solution
Dilution Instructions: Dilution Solvent Used l10%HNO~ ·.···
SECONDARY VOLUMETRIC DILUTION
Vol. Parent Solution: · .1Q'.0000 ml
Total Mass: 1.0000E+03 ng
Final Volume: , J000,0.0 ml
NOTES:
/
Final Activity Concentration:! 1.0000E+OO!ng/ml
This concentration is based on the original reference
date listed above.
Expiration Date:f November 9, 2018!
Date: 11/11/2017 0:00
~--·~-·--~ -··~
QC Approval ......a....,,.,..-c-'d-'..,.___._,,,,,...~-~~r+-- Date: lj/, :3[17 r,
0033
l;;:.~.E;; .. ~k.lN_S;:;: ; !:-iERVICE!'..S .
Rev.8; 11 /01 /03
QUALITY CONTROL PROGRAM MP-009
Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES- OAK RIDGE LABORATORY
RADIOACTIVE REFERENCE STANDARD SOLUTIONS SECONDARY DILUTION Initial Dilution
MP-009
Princi al Radionuclide NaturallJ ,
Half Life, Years .I' , Ai468E;+09!
Half Life, Days ! 1.6~2E+12I
Radionuclide of Interest Natu.raJ\tJ . Reference Date!<· 812$i2Q09 b:ooj
Parent Solution Cone. 1.:'00~+02 ng/ml
U-12-5
Chemical Com osition of Standard Solution
Dilution Instructions: Dilution Solvent Used
SECONDARY VOLUMETRIC DILUTION
Vol. Parent Solution: . 50.0000 ml
Total Mass: 5.0000E+03 ng
Final Volume: ... 1,0QQ,00 ml
NOTES:
Fina.I Activity Concentration: I 5.0000E+OO!ng/ml
This concentration is based on the original reference
date listed above.
Expiration Date:jNovember 9, 20181
Date: 11/11/20170:00
Date: I i/L:.,? ft 7 I f
0034
~BERL,!NJ;;:: QUALITY CONTROL PROGRAM
' SP.:AVICl:.S MP-009
Rev.8; 11/01103 Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY
RADIOACTIVE REFERENCE STANDARD SOLUTIONS SECONDARY DILUTION Initial Dilution
MP-009 Date 11/11/2017 0:00
Solution Reference·# J:iJl:ST3164'Lot# 0805Zt Solution# ':.Q.~}·2::~·";
Princi al Radionuclide
Natural u
Radionuclide of Interest · Natur!;ill lJ
Half Life, Years I · .· 4.468~+o9l
Parent Solution Cone. 1.Q0E+03 : ng/ml
U-12-6
Half Life, Days ! 1.632E+12!
Reference Date! · 8/25/20090:00!
Chemical Com osition of Standard Solution
Dilution Instructions: Dilution Solvent Used
SECONDARY VOLUMETRIC DILUTION
Vol. Parent Solution: '10,P:QOO ml
Total Mass: 1.0000E+04 ng
Final Volume: JOOQ;QQ ml
NOTES:
Final Activity Concentration:! 1.0000E+01 Ing/ml
This concentration is based on the original reference
date listed above.
Expiration Date:I November 9, 201 Bl
Date: 11/11/2017 0:00
Date: 1d1~/17 r 7
.· .. 1
0035
Rev.8; 11/01/03 Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY
RADIOACTIVE REFERENCE STANDARD SOLUTIONS SECONDARY DILUTION Initial Dilution
MP-009 Date. 11/11/20170:00
Solution Reference# NIS'T3'1,$4,Lot#080:52.1 Solution # l;;!d2~4;
Princi al Radionuclide Na.turaltJ
· Half Life, Years I 4A68E+09I
Half Life, Days I 1.632E+12l
Radionuclide of Interest Parent Solution Coric. i,,--,-,,.,....,,,,,....,_,......-1ng/ml
Reference Date I .. • · • . &/~5/~Q.09 Ci:QO'I
U-12
Chemical Com osition of Standard Solution
Dilution Instructions: Dilution Solvent Used l1Ci%HNQ3 '
SECONDARY VOLUMETRIC DILUTION
Vol. Parent Solution:' ·, .. · ,5>0000 ml
Total Mass: 5.0000E+04 ng
Final Volume: ··.• ./1'QQO,OQ ml
NOTES:
Final Activity Concentration: l 5.0000E+01 Ing/ml
This concentration is based on the original reference
date listed above.
Expiration Date:! November 9, 2018 I
0036
Rev.8; 11/01/03
QUALITY CONTROL PROGRAM MP-009
Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY
RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION (Recertification)
MP-009. Date 11/11/2017 0:00
Solution Reference# :Nl$T31J54:Lot#0805:~:r Solution # · lP1V5.< -
Princi al Radionuclide
Natural U
-Half Life, Years r 4.4aag+os.j
Half Life, Days I 1.632E+12)
Radionuclide of Interest N~tura_l W __ ---_: Reference Date I · 8125[2009 0:00,I
Parent Solution Cone. i:Ot:1E;t04' '; ng/ml
U-12
Chemical Com osition of Standard Solution
Dilution Instructions: Dilution Solvent Used
SECONDARY VOLUMETRIC DILUTION
Vol. Parent Solution:•·----• --- ?tQ:OOOQ ml
Total Mass: 1.0000E+05 ng
Final Volume: 1 '-•• ;t000,00, ml
NOTES:
Final Activity Concentration: I 1.0000E+02jng/ml
This concentration is based on the original reference
date listed above.
Expiration Date:! November 9, 2018 !
Date: November 11, 2017
Date: 1,jrit '?
0037
Rev.8; 11/01/03
QUALITY CONTROL PROGRAM MP-009
Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES~ OAK RIDGE LABORATORY
RADIOACTIVE REFERENCE STANDARD SOLUTIONS SECONDARY DILUTION (Recertification)
MP-009 Date 11/11/20170:00
Solution Reference# Nl$::t'$1E?4 t::.9f#Ql3Q52l ' Solution#; , :1P::\f~/p[ '
Princi al Radionuclide
Natural U,,
Radionuclide of Interest . Natural U ,
Half Life, Years I. . 4A68E+09'!
Parent Solution Cone. 1:d0Sf04' • ng/ml
U-12
Half Life, Days
I 1.634E+12I
Reference Date!, 8725/2009 0:001
Chemical Com osition of Standard Solution
Dilution Instructions: Dilution Solvent Used ltQ%HN93
SECONDARY VOLUMETRIC DILUTION
Vol. Parent Solution: 10d;b,OOO ml
Total Mass: 1-.0000E+06 ng
Final Volume: , 1'000;00 ml
NOTES:
(------
\ ·,-.. .... -....
Final Activity Concentration: I 1.0000E+03!ng/ml
This concentration is based on the original reference
date listed above.
Expiration Date:!November 9, 2018!
Date: 11/11/2017 0:00
Date: 1' /13U.,..,.) _....,,~....._,., ___ .,._, -
0038
CERTIFICATE OF CALIBRATION ALPHA STANDARD SOLUTION
Radionuclide: Th-232
Half Life: . (1.405 ± 0.006) x 10~ 10 years
Customer:
P.O.No.:
TMA EBERLINE
VH1632
1h-8
Catalog No.: 7232
435-104-2
Reference Date: November 1 1993 12:00 PST.
Source No.: Contained Radioactivity: (fh-232) 0.0933 µCi.
Contained Radioactivity: (Th-232) 3.45 kBq.
Description of Solution a. Mass of solution:
b. Chemical form:
c. Carrier content:
11.9712 g (in a 10 ml flame sealed ampoule)
Th(NO3)4 in water
None added
d. Density: Approx. 1.21 g/ml@20°C.
Radioimpurities None detected (other than daughters).
Radioactive Daughters Ra-228, Ac-228, Th-228, Ra-224, Rn-220, Po-216, Pb-212, Bi-212, Po-212, Tl-208
Radionuclide Concentration (Th-232) 0.00779
Method of Calibration
Activity calculations are based upon known specific activity and mass.
Uncertainty of Measurement
a. Systematic uncertainty in instrument calibration:
b. Random uncertainty in assay:
c. Random uncertainty in weighing(s):
d. Total uncertainty at the 99% confidence level:
NIST Traceability
±3.0%
±0.0%
±2.0%
±3.6%
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Leak Test(s)
See reverse side for Leak Test(s) applied to this source.
Notes
1. Nuclear data were taken from "'(able of Radioactive Isotopes", edited by Virginia S. Shirley, ·i986.
µCi/g,
2. IPL participates in an NIST measurement assurance program to establish and maintain implicit traceability for a number of nuclid~s,
based on the blind assay (and later NIST certification) of Standard Reference Materials (As in NRC Regulatory Guide 4.15).
ISOTOPE PRODUCTS LABORATORIES
1800 North Keystone Street
Burbank, California 91504
818 843 ~ 7000
QUALITY CONTROL
Date Signed
0039
;: EJ>E R \--,~!;;'c~ I QUALITY CONTROL PROGRAM
MP-009
Rev.8; 1110/03 Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY RADIOACTIVE REFERENCE SOLUTIONS PRIMARY DILUTION RECERTIFICATION
MP009
CURRENT DATE 8/16/2017 0:00 ,,.........,--..,.....--------..... t--------SOLUTION REFERENCE # IPL435"-104;,2 · ' . SOLUTION # Th~ .
Radionuctide · · 232 & .. h ·
Half Life, Years
I · · ·.1AOSE+10I
Certified Activity . · <9.330E;cfJ2 µCi
Certified Concentration.___ ___ _.µCi per gram
Half Life, Days
j 5.132E+12j
Reference DateJ._.-. _ _;.1.1_/1_1_19..,..9_3_0_:o ..... ol
Ampoule /Solution Gross 18:8415 Weight, Grams
Empty Ampoule .. :.:.6.9296 Weight, Grams
Solution Net 11.9119 Weight, Grams
Total Activity in Ampoule 0.0933 µCi
Chemical Composition of Standard Solution
l"fh(N03)4 in H2O,
DIiution Instructions: Dilution Solvent Used . j1% NitricAcid
Dilute to a volume of! -1000.00 . !milliliters
Certified Total Activity of! 0.0933!µCi Which Eauals 2.071 E+05jdpm at the date listed above
And after dilution the activity of this solution isl 2.071E+02!dprn/ml This activity concentration is based on the original reference date listed above. All activities are corrected to the date and time of analysis by the laboratory data processing software.
Expiration Date:! August 11, 2018
VArifiArl P. AnnrnvArl Rv " ✓ ---,,,-;:--------+----
Rt1R1?n11 n·nn
Date:
0040
~ ~J::RLIN,_t;; I QUALITY COMPN-OTO~OL PROGRAM ~ Si:tRv1ce.:s
Rev.8; 1/10/03 Title: Radioactive Reference Standards· Solutions & Records
EBERLINE SERVICES~ OAK RIDGE LABORATORY RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION
MP-009 Solution Reference# IPL435"104'--2
Prine! al Radionuclide ·· Z!ij&232Th
Radionuclide of Interest • ·. 228 &
232Th ·
Half Life, Years
I . t405E+10!
Parent Solution Cone. 2.07E+02 ·· dpm/ml
Chemical Com osition of Standard Solution
Date 8/16/2017 0:00 Solution # > · · Th~Bb
Half Life, Dar I 5.132E+12I
Reference Date .... I __ 1..a1 .... 11 __ 11 ..... 9_93_·• '""o:_oo ..... l
Dilution Instructions: Dilution Solvent Used l 1 % Nitric Acid
SECONDARY VOLUMETRIC DILUTION
Vol. Parent Solution: · · · · · soo:0000 ml
Total Activity: 1.0355E+05 dpm
Final Volume: 1000,00 ml
NOTES:
Final Activity Concentration: I 1. 0355E+02! dpmlml
This activity concentration is based on the original reference date listed above. All activities are corrected to the date and time of analysis by the laboratory data processing software.
Expiration Date:I August 11, 2018
Date: 8/16/2017 0:00 ----,----Date: ____ e;+-'-'b (?"'+/ ...... 17_
I
0041
RTIFICATE OF ALIBRATI~et q\
LPHA ST AND ARD SOLUTION" \)\J' \ ~:~\\t\i
Radionuclide
Half Life:
Th-230 Customer:
P.O.No.:
~f&l\\l t~ ~v(); TMA EBERLM~ I\\\'' TI4944 \\I~
Catalog No.:
(7 .54 ± 0.03) x 10"4 years
7230 Reference Date: November 1 1991 12;00 PST.
Source No.: Contained Radioactivity: 1.036 µCi.
Description of Solution a. Mass of solution:
b. Chemical form:
c. Carrier content:
d. Density:
Radioimpurities
Radioactive Daughters
Radionuclide Concentration
Method of Calibration
5.0042 Th(NO3)4 in 0.lN HNO3
None added
1.0016
See attached technical data sheet
See attached technical data sheet
0.207
Weighed aliquots of the solution were assayed using a liquid scintillation counter.
Uncertainty of Measurement a. Systematic uncertainty in instrument calibration:
b. Random uncertainty in assay:
c. Random uncertainty in weighing(s):
d. Total uncertainty at the 99% confidence level:
NIST Traceability
±2.0% ±0,5%
±0,2%
±2.7%
grams.
gram/ml @ 20°C.
µCi/gram.
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Notes 1. Nuclear data were taken from "Table of Isotopes\ Seventh Edition, edited by Virginia S. Shirley.
2. IPL participates in an NIST measurement assurance program to establish and maintain implicit
traceability for a number of nuclides, based on the blind assay(and later NIST certification) of
Standard Reference Materials. (As in NRC Regulatory Guide 4.15)
ISOTOPE PRODUCTS LABORATORIES 1800 No. Keystone Street.,
Burbank, California 91S04 818 843 - 7000
0042
'.~® ....... , """.··:.E1S·e:RLINE , ._.·. ~· . ~·-,, 1-:v••:f· ,;
QUALITY CONTROL PROGRAM MP-009
Rev.14; 10/10/2012
Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES -OAK RIDGE LABORATORY
RADIOACTIVE REFERENCE SOLUTIONS
PRIMARY DILUTION RECERTIFICA TfON
MP009
CURRENT DATE 2/10/2018 0:00
SOLUTION REFERENCE #,...IP_L_3_8_8_-1_1_6 ____ ...., SOLUTION #i-------,,T,,...h-..,.1-----t
Princi al Radionuclide 230Th
Half Life, Years
I 7.540E+04I
Radionuclide 230Thorium
Certified Activity 1.036E+00 µCi
Certified Concentration,__ ___ _.µCi per gram
Ampoule /Solution Gross Empty Ampoule
Solution Net
Total Activity in Ampoule
Chemical Com osition of Standard Solution
Half Life, Days
I 2.754E+07I
Reference Date!~ __ 1_1/_1_/1_9_9_1 _0:_o_.ol
9.2660 Weight, Grams
4.6218 Weight, Grams
4.6442 Weight, Grams
1.0360 µCi
Dilution Instructions: Dilution Solvent Used !0.1N HN03
Dilute to a volume of! 1000. 00 I milliliters
Certified Total Activity of! 1.0360lµCi Which Eauals 2.300E+06jdpm at the date listed above
This activity concentration is based on the original
And after dilution the activity of this solution isl 2.300E+03ldprruml-ence date listed above. All activities .ire
corrected to the date and time of analysis by tl1e
laboratory data processing software.
Expiration Date:! January 10, 2019
Date: 2/10/2018 0:00
Date: '3 cg;· __ .......__ ...... ____ _
0043
Rev.14; 10/10/2012
QUALITY CONTROL PROGRAM MP-009
Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES-OAK RIDGE LABORATORY
RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION
MP-009 Date 2/10/2018 0:00
Solution Reference# IPL 388-116 Solution #,,_ __ T_h--1-b __ _.
Half Life, Years
I 7.540E+04I
Half Life, Days
I 2.754E+07I
Radionuclide of Interest 0Thorium Reference Date! .... __ 1_1_/1_/1_9_9_1 _0_:0__.0 I Parent Solution Cone. 2.30E+03 dpm/ml
Chemical Com osition of Standard Solution
Dilution Instructions:
Vol. Parent Solution:
Total Activity:
Final Volume:
NOTES:
Dilution Solvent Used jo.1N HNO3
SECONDARY VOLUMETRIC DILUTION
10.0000 ml
2.2999E+04 dpm 1000.00 ml
Final Activity Concentration: I 2.2999E+01 jdpm/ml
This activity concentration is based on the original
reference date listed above. All activities are
corrected to the date and time of analysis by the
laboratory data processing software.
Expiration Date:I January 10, 2019
Date: 2/10/20180:00
Date: --'~I---+----
0044
-~ Isotope Products . Laboratories
An Eckert & Ziegler Company
24937 Avenue Tibbitts Valencia, California 91355
Tel 661•309·1010 Fax 661•257•8303
CERTIFICATE OF CALIBRATION ALPHA STANDARD SOLUTION
Radionuclide: Half-life: Catalog No.:
Th-229 7340 ± 160 years 7229
Customer: P.O.No.: Reference Date:
EBERLINE SERVICES 00009633 15-Jan-02 12:00 PST
Source No.: 867-54 Contained Radioactivity:
(Th-229 only) 1.013 µCi 37.48
Physical Description: A. Mass of solution:
B. Chemical form:
5.0147 gin 5 ml flame-sealed ampoule
Th(NO3)4 in 0.1M HN03
C. Carr[er content: 10µg Th/ml
D. Density: 1.0016 g/ml @ 20°C.
Radioimpurities:
None detected (daughters in equilibrium)
Radionuclide Concentration: 0.2020 µCi/g, 7.474 kBq/g
Method of Calibration:
This source was prepared from a weighed aliquot of solution whose activity in µCi/g was determined
using gamma ray spectrometry.
Peak energy used for integration: 193.5 keV
Branching ratio used: 0.0441 gammas per decay
Uncertainty of Measurement: A. Type A (random) uncertainty:
B. Type B (systematic) uncertainty:
C. Uncertainty in aliquot weighing:
D. Total uncertainty at the 99% confidence level:
Notes: - See reverse side for leak test(s) performed on this source.
± 0.7 % ± 3.0 % ± 0.0 % ± 3.1 %
7li-!8
kBq
- IPL participates in a NIST measurement assurance program to establish and maintain implicit traceability
for a number of nuclides, based on the blind assay (and later NIST certification) of Standard Reference
Materials (As in NRC Regulatory Guide 4.15).
- Nuclear data was taken from IAEA Technical Report Series No. 261.
- This solution has a working life of 5 years.
1-Tt½i-o2... Quality'control Date Signed IPL Ref. No.: 867-54
------------------ISO 9001 CERTIFIED ------------------
Medical Imaging Laboratory Industrial Gauging Laboratory
24937 Avenue Tibbitts Valencia, California 91355 1800 North Keystone Street Burbank, California 91504
0045
;: E;e E"" b~!:'o!'i I QUALITY CONTROL PROGRAM
MP-009
Rev.a; 1110/03 Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY RADIOACTIVE REFERENCE SOLUTIONS PRIMARY D/LUnON RECERTIFICATION
MP 009
CURRENT DATE 8/16/2017 0:00
SOLUTION REFERENCE #,...IP_L_8_67--5-4...,_·::--_.·:--.. -.. -.,...----, SOLUTION #1-'°---.-.• T"""h-.,.1,_,8,-·. ---i
Half Life, Years 1 · . 7~340E+031
Half Life, Days
I 2.s81 E+oel
Radionuclide 1 • :~h Reference Date! · . 1/15/2002 o:ooj Certified Activity ·· t013E+00 µCi
Certified Concentration.__ ___ __.µCi per gram
Ampoule /Solution Gross Empty Ampoule .
Solution Net Total Activity in Ampoule
·· 8.7752 Weight, Grams
. 3.75~1 Weight, Grams 5.0161 Weight, Grams 1.0130 µCi
Chemical Com osition_of Standard Solution
·h(N03)4 in0:1M·HNOi .• . .
Dilution Instructions: Dilution Solvent Used
Dilute to a volume of! • 1000~00. !milliliters
Certified Total Activity ofl 1.0130lµCi Which Equals 2.249E+06jdpm at the date listed above
I
This activity concentration is based on the original
And after dilution the activity of this solution is I 2.249E+03j dpm/ml reference date listed above. All activities are corrected to the date and time of analysis by the laboratory dat.a processing software,
Expiration Date: I August 11, 2018
n~tA· R/1Rt?n11 n·nn
0046
Rev.7; 9129/99 Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES-OAK RIDGE LABORATORY RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTJFICA TION
MP-009 Solution Reference # IPL 867c-54
Princi al Radionuclide · · 229rh ·
Radionuclide of Interest · 229Th .·
Half Life, Years
l i.340E+os!
Parent Solution Cone. ·· 2.25E+03 • dpm/ml
Chemical Com osition of Standard Solution
TH(NO3)4 in 0.1 M H NQ3 · ..
Date 8/16/2017 0:00 Solution# Th-18a ...
Half Life, Days
I 2.aa1 E+osj
Reference Date! 1/15/2002 o:oo!
Dilution Instructions: Dilution Solvent Used I0~1M HNO~
Vol. Parent Solution: Total Activity: Final Volume:
NOTES:
SECONDARY VOLUMETRIC DILUTION
10'.0000 ml 2:2490E+04 dpm
1000;00 ml Final Activity Concentration: I 2.2490E+01 ldpm/ml
This activity concentration is based on the original reference date listed above. All activities are corrected to the date and time of analysis by the laboratory data processing software.
Expiration Date: I August 11, 2018
0047
J}ational Jf nstftutt of $tanbatb!i & m;ecbnologp
<t'erttf tcate,· Standard Reference Material 425 lC Barium-133 Radioactivity _Standard
This Standard Reference Material (SRM) consists of radioactive barium-133. c~loride,. non-radioactive barium
chloride, and hydrochloric acid dissolved in 5 rnL of distilled water. The solution is contained in a flame
sealed NIST borosilicate-glass ampoule. The SRM is intended for the calibration of ionization chambers and
solid-state gamma-ray_spectrometry systems.
Radiological Hazard
The SRM ampoule contains barium-133 with a total activity of approximately 2.5 MBq. Barium-133 decays
by electron capture and during tlle decay process X-rays and gamma:rays with energies from 4 to 400 ke V are
emitted. Most of these photons escape from the SRM ampoule and can represent a radiation hazard.
Approximate unshielded dose rates at several distances (as of the reference time) are given in note [a]*.
Appropriate shielding and/or distance should be used to minimize personnel exposure. ,The SRM should be
used only by persons qualified to· han?le radioactive material. , ·
Chemical Hazard
The SRM ampoule contains .hydrochloric acid (HCl) with a concentration of 1 mole per liter .of water. The
solution is corrosive and represents a health hazard if it comes in contact with eyes or skin:, If the ampoule
is to be opened to transfer the solution, the recommended procedure is given on page 2. The ampoule should
be opened only by person,s qualified to h.andle both radioactive material and strong acid solution.
Storage and Handling
The SRM should be stored and used at a temperature between 5 and 65 °C. The solution in an unopened
ampoule should remain stable and homogeneous until at least June 2004.
The ampoule (or any subsequent container) should always be clearly marked as containing radioactive
material. If the ampoule is transported it should be packed, marked, labeled, and shipped in accordance with
the applicable national, international, and carrier regulations. The solution in the ampoule is a dangerous
good (hazardous material) both because of the radioactivity and because of the strong acid.
Preparation
This Standard Reference Material was prepared in the Physics Laboratory, Ionizing Radiation Division,
Radioactivity Group, J.M.R. Hutchinson, Group Leader. The overall technical direction and physical
measurements leading to certification were provided by L.L. Lucas of the Radioactivity Group and D.B. Golas,
Nuclear Energy Institute Research Associate.
The support aspects involved in the preparation, certification, and issuance of this SRM were coordinated
through the Standar~ Reference Materials Program by N.M. Trahey.
Gaithersburg, Maryland 20899
October 1994
SRM 4251C, p~ge 1 of 6
Thomas E. Gills, Chief
Standard Reference Materials Program
*Notes and references are on pages 5 and 6.
0048
~EB_ERLI_N_E I ~ SERVICES
QUALITY CONTROL PROGRAM QCP-009
Rev.8; 11/10/03 Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY
RADIOACTIVE REFERENCE SOLUTIONS
PRIMARY DILUTION RE CERT/FICA TION
QCP 009-1
CURRENT DATEI 4/29/2017 0:00
SOLUTION REFERENCE #..,.N.,.,.IS"""T""'s.,,..,R""'M,..,.4_2,...5,--1 C-,----...., SOLUTION #l.,_ _ __,,,.B_a_..,,.6---il
Principal Radionuclide 1~Barium I
Radionuclide 133Barium
Half Life, Years
I 1.048E+o1 I
Certified Actlvlty.,.._,...,,.....,...._,,...,-1µCi
Certified Concentration 1.318E+01 µCi per gram
Half Life, Days
I 3.828E+03!
Reference Date .... l ___ 9/_1_/1_9_9_3_0_:o ...... oj
Ampoule /Solution Gross
Empty Ampoule Solution Net
Total Activity in Ampoule
9.3081 Weight, Grams
.. 4.2582 Weight, Grams
5.0499 Weight, Grams
66.5577 µCl
Chemical Composition of Standard Solution
I '""BaCl2 in 1 M HCI
Dilution Instructions: Dilution Solvent Used 11M HCI
Dilute to a volume of! 1000.00 jmillillters
Certified Total Activity of! 66.5577jµCi Which Eauals I 1.478E+08ldpm at the date listed above
And after dilution the activity of this solution is! 1.478E+OS)dpm/ml This activity concentration is based on the original
reference date listed above. All activities are corrected
to the date and time of analysis by the laboratory data
processing software.
Expiration Date:! April 27, 2018 I
" ----------- I Verified & Approved By I"--- -- ~~
-----d""~ n--.....--::---=7~---1~\---ac Approval, :,.,~j ~ -~ "i, \.
\. l
Date: 4/29/17 -------Date: s/;i./n ---1,""'--+,------
0049
Rev.B; 11/10/03
QUALITY CONTROL PROGRAM QCP-009
Title: Radioactive Reference Standards Solutlcms & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY
RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION
QCP-009-1-A
Solution Reference # NIST SRM4251 C · Date 4/29/17
Solution # ... _.----s-a_..S_a_·_· __
Prinoi al Radionuclide 133sa
Half Life, Years
I · 1.048E+01 ! Half Life, Days
j 3.828E+03j
Reference Datel ... ___ 9_/1_/1_9_93_0:_oo ..... l
Chemical Composition of Standard Solution
Dilution Instructions: Dilution Solvent Used l1MHCI ·
SECONDARY VOLUMETRIC DILUTION
Vol. Parent Solution: .• .>,,25i0000 ml
Total Activity: 3.6950E+06 dpm
Final Volume: . 1000.00 ml
NOTES:
Final Activity Concentration: I 3. 6950E+03l dpm/ml
This activity concentration is based on the original
reference date listed above. All activities are
corrected to the date and time of analysis by the
laboratory data processing software.
e, Gr '"' 1(\-Expiration Date: .. I _A_p_r.,.il 2-7-,-2-01"'"2,_'. _I
;
Date: 4/29/17
Date: #0/1') I
0050
CERTIFICATE OF CALIBRATI lijA/OC REVIEWED ALPHA STANDARD SOLUTIO om d" g
t.=-=t.=t=.:t..::~::::::.J
Radionuclide:
Half Life:
Customer:
P'.O.No.:
TMA EBERLINE
VH1888
Catalog No.:
Ra-226
1600 ± 7 years
7226
453-26
Reference Date: February 1 1994 12:00 PST.
Source No.: Contained Radioactivity: (Ra-226) 1.001 µ.Ci.
Contained Radioactivity: (Ra-226) 37.0 kBq.
Description of Solution a. Mass of solution:
b. Chemical form:
c. Carrier content:
5.1864 g (in a 5 ml Flame Sealed Ampoule)
Ra(NO3)2 in 1 N HNO3
None added
d. Density: 1..0318 g/ml @20°C.
Radioimpurities None detected(other than daughters)·
Radioactive Daughters Rn-222, Po-218, At-218, Pb-214, Bi-214, Po-214, Tl-210, Pb-210, Bi-210, Po-210 and Tl-206.
Radionuclide Concentration (Ra-226) 0.1929
Method of Calibration
Weighed aliquots of the solution were assayed using gamma spectrometry:
Energy peak(s) integrated under: 186 keV.
Branching ratio(s) used: 0.0351 gamma rays per decay.
Uncertainty of Measurement
a. Systematic uncertainty in instrument calibration:
b. Random uncertainty in assay:
c. Random uncertainty in weigbing(s):
d. Total uncertainty at the 99 % confidence level:
NIST Traceability
±3.4%
±3.1%
±0.2%
±4,6%
µ.Ci/g.
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Leak Test(s)
See reverse side for Leak Test(s) applied to this source,
Notes
1. Nuclear data were taken from "Table of Radioactive Isotopes", edited by Virginia S. Shirley, 1986.
2. IPL participates in an NIST measurement assurance program to establish and maintain implicit traceability for a number of nuclides,
b&sed on the blfo.d assay (arid later NIST certification) ofStimdiird Reference Miiterfals(As iii NRC Reguliitory Guide 4.15).
ISOTOPE PRODUCTS LABORATORIES
1800 North Keystone Street
Burbank, California 91504
818 843 -7000
QUALITY CONTROL
0,. 3, l99't Date Signed
0051
~ E a ER !a; ~!::lo!';; I
'
QUALITY CONTROL PROGRAM MP009
Rev.8; 11/01/03 Title: Radioactive Reference Standards Solutlons & Records
EBERLINE SERVICES• OAK RIDGE LABORATORY
RADIOACTIVE REFERENCE SOLUTIONS
PRIMARY DILUTION RECERTIFICATION MP009
CURRENT DATE! 9/20/2017 0:001
SOLUTION REFERENCE# IPL453c.26 I SOLUTION #I . : Ra;.s.· · I
Principal Radionuclide Half Life, Years Half Life, Da~s
226Radiuiri I I· .. 1.600E+03! I s.844E+osl
Radionuclide ~Radium· Reference Date! • 21111994 o:ool Certified Activity 1:001E+oo µCi
Certified Concentration , , µCi per gram
Ampoule /Solution Gross~Welgh~ Grams Empty Ampoule ·. . · · ·. Weight, Grams
Solution Net Weight, Grams
Total Activity in Ampoule 1.0010 µCi
Chemical Composition of Standard Solution
l.<.«>Rfl(NO~hi.n 1MHNQ3·•. ·,'' . . I . ,,.
Dilution Instructions: Dilution Solvent Used ,~M HN03. · I Dilute to a volume ofl · 1000;00 · I milliliters
Certified Total Activity of! : 1.0010lµCi Which Ecauals I 2.222E+06!dpm at the date listed above
This activity concentration is based on the original
And after dilution the activity of this solution isl 2.222E+03ldpm/ml reference date listed above. All activities are corrected
to the date and time of analysis by the laboratory data
processing software.
Expiration Date: I Seetember 20, 2018 I
~~ \
Verified & Approved By Date: 9/20/2017
~q\~ _? I \ \_
QC Approval \. ~~ ~ Date: 9/20/2017
- ~ J --
0052
Rev.a; 11/01103 Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY
RADIOACTIVE REFERENCE STANDARD SOLUTIONS SECONDARY DILUTION RECERTIFICA TJON
MP009
Solution Reference # IPL-453,.26
Princi al Radionuclide
··· 226.Radium
Radionuclide of Interest ·. . ~ 6Radium .
Half Life, Years
I · 1;600E+03!
Parent Solution Cone. 2.22E+03 · dpmlml
Chemical Com osition of Standard Solution
.. Ra(N9s)2 in 1M HNOs ....
Date 9/20/2017 0:00
Solution # . Ra-5b .
Half Life, Daxs I s.844E+os!
Reference Date ... ! __ 21_1_11_9_94_. ·:·_o:_oo_,!
Dilution Instructions: Dilution Solvent Used j1MHNQj
Vol. Parent Solution: Total Activity: Final Volume:
NOTES:
SECONDARY VOLUMETRIC DILUTION
20;0000 ml 4.4440E+04 dpm
1000.00 ml Final Activity Concentration: I 4.4440E+01 jdpmlml
This activity concentration is based on the original
reference date listed above. All activities are
corrected to the date and time of analysis by the
laboratory data processing software.
Expiration Date:._l __ 2_0_-s_e_p-_1_a _ _.
Date:
Date:
9/20/2017 0:00
9/20/2017 0:00
0053
ANALYTICS
CERTIFICATE OF CALIBRATION Standard Radionuclide Source
62680-416
Ra-228 5 mL Liquid in Flame Sealed Vial
1380 Seaboard Industrial Blvd. Atlanta, Georgia 30318 · U.S.A.
Phone (404) 352-8677 Fax (404) 352-2837
This standard radionuclide source was prepared
gravimetrically from a calibrated master solution. The
master solution was calibrated using a germanium gamma
spectrometer system.
Radionuclide purity and calibration were checked using a
germanium gamma spectrometer system. The nuclear decay rate
and assay date for this source are given below.
ANALYTICS maintains traceability to the National Institute
of Standards and Technology through Measurements Assurance
Programs as described in USNRC Reg. Guide 4.15, Revision 1.
ISOTOPE:
ACTIVITY (dps):
HALF-LIFE:
CALIBRATION DATE:
TOTAL UNCERTAINTY*:
SYSTEMATIC:
RANDOM:
*99% Confidence Level
Ra-228
2.585 E3
5.75 years
November 7, 2001 12:00 EST
4.0%
3.0%
1.0%
Impurities: y-impurities (other than decay products) <0.1%
5.07198 grams 0.lM HCl solution with 50 µg/g Ba carrier.
PO NUMBER 9508, Item 1 (Part #4339A)
SOURCE PREPARED BY, M~~4i~ QA APPROVED:
0054
E BERLIN_J;: SE:~VICE$
Rev.a; 1/10/03
I QUALITY CONTROL PROGRAM MP--009
Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY RADIOACTIVE REFERENCE SOLUTIONS
RECERTIFICATION MP009
CURRENT DATE 2/28/2017 0:00
SOLUTION REFERENCE # ... A-ri-a!--·. -ics-, ,-6-268...,,-0-.:4--1-6..,..'",---. SOLUTION #.,.._.._....,R __ a ___ ;.;1-,1-· ---1
Princi al Radionuclide . 226Ra •
Half Life, Years
I s.1soE+ciol Half Life, Days
I 2.1 OOE+03!
Radionuclide . · _ 228Ra _ · Certified Activity 6. 986E-02 µCi
Reference Date._j __ 1_1/7_· _I2_0 ___ 0_1 _0_:0__,0j
Certified Concentration..__ ___ _,µCi per gram
Ampoule /Solution Gross Empty Ampoule
Solution Net Total Activity in Ampoule
: 9A9.82 Weight, Grams 4:4895 Weight, Grams 5.-0087 Weight, Grams 0.0699 µCi
Chemical Com osition of Standard Solution
Dilution Instructions: Dilution Solvent Used
Dilute to a volume ofl · - 1000;00 !milliliters
I0.5MHCI'
Certified Total Activity ofl 0.0699lµCi Which Equals 1.551 E+05jdpm at the date listed above
I
And after dilution the activity of this solution is! 1.551 E+02!dpm/ml This activity concentration Is based on the original reference date listed above. All activities are corrected
to the date and time of analysis by the laboratory data
processing software.
Expiration Date:( February 20, 2018
Date: 2/28/17
0055
QA/QC REVIEWED ANALYTICS
Date Initials w(
CERTIFICATE OF CALIBRATION Standard Radionuclide Source
52094-416
Am-241 10 mL Liquid in Flame Sealed Vial
1380 Seaboard Industrial Blvd. Atlanta, Georgia 30318 · U.S.A.
Phone (404) 352-8677 Fax (404) 352-2837
This standard radionuclide source was prepared gravimetrically
from a calibrated master liquid radionuclide solution source.
The master source was calibrated by liquid scintillation
counting.
ANALYTICS maintains traceability to the National Institute of
Standards and Technology through Measurements Assurance Programs
as described in USNRC Reg. Guide 4.15, Revision 1.
ISOTOPE:
ACTIVITY (dps):
HALF-LIFE:
CALIBRATION DATE:
TOTAL ERROR:
Am-241
1.975 E+05
432.2 years
March 19, 1996 12:00 EST
3.0%
SYSTEMATIC ERROR: 2.37%
RANDOM ERROR: 0.63%
10.01177 grams of solution lM HCl.
PO NUMBER OR3830, Item 1
SOURCE PREPARED BY: Beverly,
QA APPROVED: M-~
0056
, e:;a ~J~J . .,.JN g I QUALITY c~~1~0L PROGRAM ~ SE.RV1ce.s
Rev.8; 1/10/03 Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES-OAK RIDGE LABORATORY
RADIOACTIVE REFERENCE STANDARD SOLUTIONS SECONDARY DILUTION (RE-CERT/FICA TION)
Date 7/29/2017 0:00
Solution Reference # Anal cs 52094-416 Solution # A/B-7 al ha
Radionuclide of Interest 241Am
Half Life, Years
I 4.322E+02!
Parent Solution Cone. 1.19E+04 dpm/ml
Chemical Composition of Standard Solution
j241AmCl3 in 1 M HCL
Half Life, Days l 1.579E+05 [
Reference Date .... I __ 3_/_19_/_19_9_6_0_:oo_.l
Dilution Instructions: Dilution Solvent Used
Vol. Parent Solution: Total Activity: Final Volume:
NOTES:
SECONDARY VOLUMETRIC DILUTION
60.0000 ml 7.1100E+05 dpm
1000.00 ml Final Activity Concentration: I . 7.1100E+02jdpmlml
This activity concentration is based on the original
reference date listed above. All activities are
corrected to the date and time of analysis by the
laboratory data processing software.
Expiration Date:I July 29, 2018
0057
Jlattonal 1htstttute of ~tanbarb~ & m;ccbnologp
ctertif tcate Standard Reference Material 4234A
Strontium-90 Radioactivity Standard
1bis Standard Reference Material (SRM) consists of radioactive strontium-90 chloride, non-radioactive
strontium chloride, non-radioactive yttrium chloride, and hydrochloric acid dissolved in 5 mL of distilled water.
The solution is contained in a flame-sealed NIST borosilicate-glass ampoule. The SRM ·is intended for the
calibration of beta-particle counting instruments and for the monitoring of rll;diochemical procedures.
Radiological Hazard
The SRM ampoule contains strontium-90 with a total activity of approximately 13 MBq. Strontium-90 decays
by beta-particle emission to yttrium-90, which also decays by beta-particle emission. None of the beta particles
escape froni the SRM ampoule. The beta particles emitted from strontium-90 and yttrium-90 produce
bremsstrahlung photons with energies up to 2 MeV. Most of these photons escape from the SRM ampoule
and can represent a radiation hazard. Approximate unshielded dose rates at several distances (as of the
reference time) are given in note [ a J*. Appropriate shielding and/or distance should be used to minimize
personnel exposure. The SRM should be used only by persons qualified to handle radioactive material.
Chemical Hazard
The SRM ampoule contains hydrochloric acid (HCl) with a concentration of 1 mole per liter of water. The
solution is corrosive and represents a health hazard if it comes in contact with eyes or skin. If the ampoule
is to be opened to transfer the solution, the recommended procedure is given on page 2. The ampoule should
be opened only by persons qualified to handle both radioactive material and strong acid solution.
Storage and Handling
The SRM should be stored and used at a temperature between 5 and 65 °C. The solution in an unopened
ampoule should remain stable and homogeneous until at least March 2005.
The ampoule (or any subsequent container) should always be clearly marked as containing radioactive
material. If the ampoule is transported it should be packed, marked, labeled, and shipped in accordance with
the applicable national, international, and carrier regulations. The solution in the ampoule is a dangerous
good (hazardous material) both because of the radioactivity and because of the strong acid.
Preparation
This Standard Reference Material was prepared in the Physics Laboratory, Ionizing Radiation Division,
Radioactivity Group, J.M.R. Hutchinson, Group Leader. The overall technical direction and physical
measurements leading to certification were provided by L.L. Lucas of the Radioactivity Group and D.B. Golas,
Nuclear Energy Institute Research Associate.
The support aspects involved in the preparation, certification, and issuance of this SRM were coordinated
through the Standard Reference Materials Program by N.M. Trahey.
Gaithersburg, Maryland 20899
May 1995 (Text only revised November 1997)
SRM 4234A, page 1 of 6
Thomas E. Gills, Chief
Standard Reference Materials Program
*Notes and references are on pages 5 and 6.
0058
Rev.7; 9/29199 Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES • OAK RIDGE LABORATORY
RADIOACTIVE REFERENCE STANDARD SOLUTIONS SECONDARY DJLUTION (RE•CERTIFICA TION)
QCP-009-1-A Date 7/29/2017 0:00
Solution Reference # NIST 4234A Solution # • A/B--7 beta
Princi al Radionuclide 00strontium
Half Life, Years
I : 2:878E+01 ! Half Life, Days
I 1.051E+04)
Radionuclide of Interest' . . .90Sr ' I Parent Solution Cone .. · f;52E+06 : dpmlml
Reference Date!: •· · '3h3h995·o:ool
The beta activity of solution reflects the original 90Strontium concentration and an equal concentration of OOVttrium.
Chemical Composition of Standard Solution
l~sre~ .inJ ·M HCI ' . < I
Dilution Instructions: Dilution Solvent Used ltM HN03.
SECONDARY VOLUMETRIC DILUTJON
Vol. Parent Solution: 0'.5000 ml Total Activity: 7.5764E+05 dpm Final Volume: . . .. . · 1000.00 ml
NOTES:
Final Activity Concentration: I 7.5764E+02jdpm/ml
This activity concentration is based on the original reference date listed above. All activities are corrected to the date and time of analysis by the laboratory data processing software.
Expiration Date:I July 29, 2018
Date: ___ 0_7 __ /2_9_/1_7 __
Date: __ ,;-_f 1_(!_] __
0059
SECTION VI
QUALITY CONTROL SAMPLE RESULTS SUMMARY
0060
Eberline Analytical
Analysis Control Chart
w ... 18-03110
Analyte
U-234
U-238
Analyte
Analyte
U-234
U-238
U-235
Version
Nonnalized Difference
Analysis
UUISO
LCS Measured
83.21%
86.91%
MS Actual %Rec
I CSU
Measured
16.41%
16.37%
Expected MS Result
Duplicate Results
Nonnalized RPD Original
Difference Result
0.43 10.27 1.06E+00
0.45 11.42 1.04E+00
0.18 15.18 9.83E-02
Run Activity Units Aliquot Units
1 pCi
Laboratory Control Sample
LCS Expected
100.00%
100.00%
Expected MS Uncert
Original CSU
3.69E-01
3.67E-01
1.19E-01
Uncert. Known Expected
3.60% 7.28E+00
3.60% 7.06E+00
Matrix Spike
Actual MS Result
Duplicate Result
1.17E+00
9.26E-01
1.14E-01
Actual MS CSU
Duplicate CSU
3.74E-01
3.25E-01
1.24E-01
I
Known Error
2.62E-01
2.54E-01
Sample Result
LCS Relative Bias
0.83
0.87
Result
6.06E+00
6.13E+00
Sample CSU
LCS%R I
OK
OK
OK
Printed: 4/2/2018 8:22 AM
Page 1 of 2
Client Name
AMO Environmental Decisions
CSU
9.95E-01
1.00E+00
Sample Aliquot
Standard
ID
U-8a
U-8a
Standard ID
Standard
ACT(dpm)
3.20E+01
3.10E+01
Standard ACT{dpm)
QC Summary
I MS%R I MSND I
Standard
Error
3.60E+00
3.60E+00
Standard Error%
RepRPD
OK
OK
NA
I
Standard
Added (Q)
5.0SE-01
5.0SE-01
Standard Added(g)
Rep ND
OK
OK
OK
0061
Eberline Analytical Analysis Control Chart
WO • 18-03110
130.00
120.00
110.00
100.00
90.00
BO.OD
Analysis
UUISO
LCS % Recovery
I _________ I
Run Activity Units Aliguot Units
1 pCi
40.00
35.00
30.00
25.00
20.00
15.00
10.00 I
Printed: 4/2/2018 8:22 AM Page 2 of 2
Client Name
AMO Environmental Decisions
Replicate Sample RPO
! 70.00 +---------~-----------------~--------~
l U-234 U-238 5.00
- Lower Error ~~ ~%
- Upper Error 103.22 106.88 0.00 +-------------~--------------,-------
I U-235 U-234 U-238
• %R 83.21 86.91 - LowerError 11.98 13.43 I 23.87
- -LCL 75 75 - Upper Error 8.55 9.41 I 6.49
--Mean 100 100 • RPO 10.27 11.42 I 15.18
- -UCL 125 I 125 --CL 35 35 i 35
Normalized Difference
3.50
No Matrix Spike
3.00
2.50
2.00
1.50
1.00
0.50
0.00 LCS ND REP ND MSND
-U-234 0.00 0.43 0.00
=u-238 0.00 0.45 0.00
~UCL I 0.00
3
0.00
3
0.00
3
Version
0062
Eberline Services Analysis Control Chart
WO
18-03110
Analyte
TOTALU
TOTAL U (LCS-H)
Analyte
Analysis
KPA_LIQ
Nonnatized Difference
LCS Measured
108.14%
98.04%
MS Actual %Rec
I CSU
Measured
31.13%
31.12%
Expected MS Result
I I
Run Activity_ Units Aliguot Units
1 ug
Laboratory Control Sample !
LCS
I Expected
100.00% I
100.00% I
Expected MS Uncert
Uncert. Known
Expected
2.00% 8.00E+00
2.00% 2.00E+02
Matrix Spike
Actual MS Result
Actual MS CSU
Known j Result Error
i
1.60E-01 I 8.65E+00 f
! 4.00E+00 \ 1.96E+02
Sample Result
Sample CSU
-···-·-i--------
Replicate Sample
Analyte Normalized I RPO
Original I Original Replicate Replicate LCS Relative I LCS%R
Difference Result I CSU Result CSU Bias ,
I
TOTAL U 0.11 I 2.47 I 4.23E+00 1.32E+00 ! 4.12E+00 I 1.28E+00 I 1.08 OK
Version
I
Printed: 4/12/2018 1:12 PM Page 1 of 2
Client Name
AMO Environmental Decisions
CSU
2.69E+00
6.10E+01
Sample Aliquot
Standard ID
LCS-L
LSC-H
Standard ID
Standard ACT(dpm)
8.00E+00
2.00E+02
Standard Cone
QC Summary
MS%R MSND
Standard Error
1.60E-01
4.00E+00
Standard Error%
Rep RPO
NA
Standard Added (g)
1.00E+00
1.00E+00
Standard Added (g)
Rep ND
OK
0063
Eberline Services Analysis Control Chart
WO
18-03110
130.00
120,00
110.00
100.00
90.00
80.00
Analysis Run Activity Units
KPA_LIQ 1 ug
LCS % Recovery
70.00 +-------------------~---------+--------~ TOTAL U TOTAL U (LCS-H)
- Lower Error 75.01 64.92
- Upper Error 141.28 131.16
• o/oR 108.14 98.04 -- -LCL 75 75
---Mean 100 100 • - -UCL 125 125
Normalized Difference
3.50
3.00 ----2.50
2.00
1.50
1.00
0.50
0.00 LCS ND REP ND MSND
0.00 0.11 0.00
0.00 0.00 0.00
•UCL 3 3 3
Version
Aliguot Units
40.00
35.00
30.00
25.00
2000
15.00
10.00
5.00
0 00
Lower Error
u er Error
RPD
CL
Printed: 4/12/20181:12 PM Page 2 of 2
Client Name
AMO Environmental Decisions
Replicate Sample RPD
• TOTAL U
2.85
2.08
2.47
35
No Matrix Spike
0064
Eberline Analytical Analysis Control Chart
• 0
18-03110
Analyte
TH-228
TH-230
TH-232
Analyte
Analyte
TH-228
TH-230
TH-232
Version
Analysis
ThlSO
LCS CSU Measured Measured
121.11% 21.04%
123.56% 22.13%
120.87% 20.80%
Normalized MS Actual Expected Difference %Rec MS Result
Duplicate Results
Normalized RPD
Original
Difference Result
0.61 239.02 3.44E-03
0.93 55.41 2.83E-01
0.45 437.75 -5.87E-03
Run Activity Units Aliquot Units
1 pCi I
Laboratory Control Sample
LCS Uncert. Known
Known Result
Expected Expected Error
100.00% 3.60% 4.S0E+00 1.73E-01 5.81E+00
100.00% 2.70% 5.37E+00 1.45E-01 6.64E+00
100.00% 3.60% 4.S0E+00 1.73E-01 5.S0E+00
Matrix Spike
Expected Actual Actual Sample Sample
MSUncert MS Result MS CSU Result CSU
I Original Duplicate Duplicate LCS Relative I
LCS%R CSU Result CSU Bias
1.14E-01 -3.87E-02 7.03E-02 1.21 OK
2.02E-01 1.S0E-01 1.61E-01 1.24 OK
6.64E-02 1.58E-02 6.57E-02 1.21 OK
Printed: 3/30/2018 11:55 AM Page 1 of 2
Client Name
AMO Environmental Decisions
CSU Standard Standard
I Standard Standard
ID ACT(dpm) Error Added (g)
1.22E+00 Th-Sb 1.04E+02 3.60E+00 1.03E-01
1.47E+00 Th-1b 2.35E+01 2.70E+00 5.07E-01
1.21E+00 Th-Sb 1.04E+02 3.60E+00 1.03E-01
Sample
I Standard Standard
I Standard Standard
Aliquot ID ACT(dpm) Error% Added(g)
QC Summary
I I MS¾R I MSND I RepRPD I Rep ND
NA OK
NA OK
NA OK
0065
Eberline Analytical Analysis Control Chart
• 18-03110
130.00
120.00
110.00
100.00
90.00
80.00
Analysis Run
ThlSO 1
LCS % Recovery
~------] UCL
l
1000 ------------ - LCL
TH-230 TH-232 TH-228
- Lower Error 96.47 98.73 96.47
- Upper Error, 145.76 148.39 145.28
• %R 121.11 123.56 120.87
--LCL 75 75 75
--Mean 100 100 100
- -UCL 125 I 125 125
Normalized Difference
3.50
3.00
2.50
2.00
1.50
1.00
0.50
0.00 I LCSND
-TH-228. 0.00 0.61
MSND
0.00
=TH-2301 0.00 0.93 0.00
- UCL I 3 3 3
Version
Activity Units
pCi
40.00
35.00
30.00
25.00
20.00
15.00
10.00
5.00
Ali_guot Units
Printed: 3/30/2018 11 :55 AM Page 2 of 2
Client Name
AMO Environmental Decisions
Replicate Sample RPO
------1-------
0.00 +------~-------------------------------~ TH-228 TH-230 TH-232
- LowerError -387.38 78.07 3366.24
- UpperError 865.42 32.75 -2490.73
• RPO 239.02 55.41 437.75
- -CL 35 35 i 35
No Matrix Spike
0066
Eberline Analytical
Analysis Control Chart
18-03110
Analyte
RA-226
Analyte
Analyte
RA-226
Version
Normalized Difference
Analysis
Ra226
LCS Measured
98.94%
MS Actual ¾Rec
CSU Measured
25.25%
Expected MS Result
Duplicate Results
Normalized Difference
0.27
RPD
21.16
Original Result
1.47E-01
Printed: 4/3/2018 7:07 AM
Page 1 of2
Run Activity Units Ali_g_uot Units Client Name
1 pCi
Laboratory Control Sample
LCS Expected
100.00%
Expected MS Unce,t
Original CSU
1.33E-01
Uncert. Expected
4.60%
Known
1.00E+01
Known Error
4.61E-01
Matrix Spike
Actual MS Result
Duplicate Result
1.19E-01
Actual MS CSU
Sample Result
Duplicate I LCS Relative
CSU Bias
1.56E-01 0.99
AMO Environmental Decisions
Result CSU
9.91E+00 I 2.50E+00
Sample CSU
Sample Aliquot
Standard ID
Ra-5b
Standard ID
Standard I Standard
ACT (dpm) Error
4.40E+01 I 4.60E+00
Standard ACT(dpm)
Standard Error%
QC Summary
LCS¾R MS¾R MSND RepRPD
OK NA
Standard Added (g)
5.06E-01
Standard Added(g)
Rep ND
OK
0067
Eberline Analytical Analysis Control Chart
WO
18-03110
130.00
120.00
110.00
100.00
90.00
80.00
Analysis
Ra226
LCS % Recovery
70.00 RA-226
- Lower Error 69.09
- Upper Error 128.80
• %R 98.94
- -LCL 75
--Mean 100
--UCL 125
Normalized Difference
Run
1
3.50 --------------------------------
3.00 +------------~-------------------
2.50 +--------------------------------
2.00 +--------------------------------
1.50 +--------------------------------
1.00 +--------------------------------
0.50 +--------------------------------
O.OO I LCS ND REP ND MS ND
-RA-226I 0.00 0.27 0.00
- UCL 3 3 3
Version
Activity Units
pCi
40.00
35.00
30.00
25.00
20.00
15.00
10.00
5.00
Ali_g_uot Units
Printed: 4/3/2018 7:07 AM Page 2 of 2
Client Name
AMO Environmental Decisions
Replicate Sample RPO
o.oo RA-226
- LowerError 32.66
- UpperError 9.67
• RPD 21.16
- -CL 35
No Matrix Spike
0068
Eberline Analytical
Analysis Control Chart
WO • 18-03110
Analyte
RA-228
Analyte
Analyte
RA-228
Version
Normalized Difference
Analysis
Ra228
LCS Measured
94.01%
MS Actual %Rec
CSU Measured
24.20%
Expected MS Result
Duplicate Results
Normalized Difference
2.80
RPD
144.60
Original Result
1.49E-01
Printed: 4/9/2018 1 :57 PM Page 1 of 2
Run Activity_ Units Ali_guot Units Client Name
1 pCi
Laboratory Control Sample
LCS Expected
100.00%
Expected MS Uncert
Original CSU
3.38E-01
Uncert. Expected
5.10%
Known
8.96E+00
Known Error
4.57E-01
Matrix Spike
Actual MS Result
Duplicate Result
9.25E-01
Actual MS CSU
Sample Result
Duplicate I L CS Relative
CSU Bias
4.27E-01 0.94
AMO Environmental Decisions
Result CSU
8.43E+00 I 2.04E+00
Sample CSU
Sample Aliquot
Standard ID
Ra-12
Standard ID
Standard I Standard
ACT (dpm) Error
5.62E+01 I 5.10E+00
Srandard ACT(dpm)
Srandard Error%
QC Summary
LCS%R MS%R MSND RepRPD
OK NA
Standard Added (g)
3.54E-01
Srandard Added(g)
Rep ND
OK
0069
Eberline Analytical Analysis Control Chart
WO •
18-03110
130.00
- Lower Error
- Upper Error
• %R
- -LCL
--Mean
- -UCL
3.50
3.00
2.50
2.00
1.50
1.00
0.50
0.00 LCS ND
-RA-228 0.00
- UCL 3
Version
Analysis
Ra228
LCS % Recovery
.
RA-228
64.71
123.31
94.01
75
100
125
Normalized Difference
REP ND
2.80
3
Run Activity Units
1 pCi
"IU.UU
35.00
30.00
25.00
20.00
15.00
10.00
5.00
0.00
- Lower Error
i - Upper Error
• RPD
--CL
MSND
0.00
3
Aliguot Units
Printed: 4/9/20181:57 PM Page 2 of 2
Client Name
AMO Environmental Decisions
Replicate Sample RPO
RA-228
196.08
93.13
144.60
35
No Matrix Spike
0070
Eberline Analytical Analysis Control Chart
WO • 18-03110
Analyte
GROSS ALPHA_ TH
GROSS BETA_SR
Analyte
Analyte
GROSS ALPHA_TH
GROSS BETA_SR
Version
I
Analysis
GaGbT_ThSr
Normalized Difference
LCS I Measured
115.57%
101.91%
MS Actual %Rec
CSU Measured
11.00%
13.86%
Expected MS Result
Duplicate Results
Normalized RPD
Original
Dffference Result
1.01 41.05 4.25E+00
Run Activity Units Ali_g_uot Units
1 pCi
Laboratory Control Sample
LCS Expected
100.00%
100.00%
Expected MS Uncert
Original CSU
2.02E+00
Uncert. Known Expected
4.30% 2.68E+02
3.00% 2.77E+02
Matrix Spike
Actual MS Result
Duplicate Result
2.S0E+00
Actual MS CSU
Duplicate CSU
1.97E+00
I
Known Error
1.15E+01
8.30E+00
Sample Result
LCS Relative I Bias
1.16 I
Result
3.10E+02
2.82E+02
Sample CSU
LCS¾R
OK
1.00 13.79 I 1.69E+01 I 3.29E+00 I 1.95E+01 3.64E+00 I 1.02 I OK
I
I
I
Printed: 3/27/2018 9:24 AM Page 1 of 2
Client Name
AMO Environmental Decisions
CSU
3.41E+01
3.91E+01
Sample Aliquot
Standard ID
A/B-07
A/B-07
Standard ID
Standard ACT(dpm)
5.94E+02
6.12E+02
Standard ACT(dpm)
QC Summary
I MS¾R I MSND
I I
I I
I
I
Standard Error
4.30E+00
3.00E+00
Standard Error¾
RepRPD
NA
OK
I
I
I
Standard Added(g)
1.00E+00
1.00E+00
Standard Addecl(g)
Rep ND
OK
OK
0071
Eberline Analytical Analysis Control Chart
• 0
18-03110
130.00
120.00
110.00
100.00
90.00
80.00
70.00 I - Lower Error
- Upper Error
• o/oR
- -LCL
--Mean
--UCL
3.50
3.00
2.50
2.00
1.50
1.00
0.50
000
- GROSS ALPHA TH = GROSS BETA SR
= - UCL
Version
Analysis Run
GaGbT ThSr 1
LCS % Recovery
1--------- I [ __ 1
GROSS ALPHA TH GROSS BETA_SR
100.28 85.05
130.87 118.77
115.57 101.91
~ ~
100 100
125 125
Normalized Difference
LCSND MSND
0.00 1.01 0.00
0.00 1.00 0.00
0.00 0.00 0.00
3 3 3
Activity Units Aliquot Units
pCi
40.00
35.00
30.00
25.00
20.00
15.00
10.00
5.00
Printed: 3/27/2018 9:24 AM Page 2 of 2
Client Name
AMO Environmental Decisions
Replicate Sample RPO
}------------
i
o.oo +1-----G-R_O_S_S_A_L_P_H_A_-T_H ___________ G_R_O_S_S_B_E_TA ___ S_R-----~
- LowerError 52.64 15.11
- UpperError 29.45 12.48
• RPO 41.05 13.79
--CL ~ ~
No Matrix Spike
0072
SECTION VII
LABO RA TORY TECHNICIAN'S NOTES & RUN LOGS
0073
ISOUNOTES
0074
Printed: 3/28/2018 9:19 AM
a,~EBERLINE ~ SERVICES
Work Order Analysis Notes
# Date Dept User
1 03/28/18 09: 19 PREP JHARVEY
Oak Ridge Laboratory
601 Scarboro Rd. Oak Ridqe, TN 37830 Voice: 865,481.0683 www.eberlineservices.com
Page 1 of 1
Notes
AUQUOTED AND ADDED $PIKES AND TRACERS- DRll:D SAMPLES DOWN AND SUBMITTED
SAMPLES TO SEPARATIONS
0075
Printed: 3/29/2018 3:17 PM Page 1 of 1
( Oak Ridge Laboratory Internal Work Order 18-03110 601 Scarboro Rd. --.. ---·•-Oo~,. _______ .,,
EBER~~~!=; Oak Ridge, TN 37830 Analysis Code UUISO Voice: 865.481.0683
Work Order Analysis Notes .. ••-'-'••·•-., ... www.eberlineservices.com Run Number 1
# I Date Dept I User Notes '
1 03/28/18 09: 19 PREP JHARVEY ALIQUOTED AND ADDED SPIKES AND TRACERS- DRIED SAMPLES DOWN AND SUBMITTED
SAMPLES TO SEPARATIONS ,·-···-- ···-----··----
2 03/29/18 15: 17 CHEM JDEMELAS Added concentrated HCI to sample beakers and heated to dryness; Added 20 ml 8N HCL to samples and
transferred to new, labeled C-Tubes, rinsing with 8N HCI to bring volume to ~35 ml; Preconditioned resin
columns with 35 ml 8N HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 ml 8N
HCI, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml 8N HCI - 0.1 N NH41, 35 ml
of 6.5N HCI- 0.04N HF, and 10 ml of 6.5N HCI; Eluted Uranium with 50 ml of 0.5N HCI into clean, labeled 100
ml beakers; Dried-down samples on hotplate; Dissolved samples in ~10 ml of concentrated HCI; Transferred to
new, labeled C-Tubes with DI H2O. Set samples aside for later precipitation and filtering.
0076
Printed: 3/30/2018 4:51 AM
(EBER~~~~ Work Order Analysis Notes
# Date Dept User
1 03/28/18 09: 19 PREP JHARVEY
2 03/29/18 15: 17 CHEM JDEMEL.AS
3 03/30/18 04:51 CHEM TSMITH
Oak Ridge Laboratory
601 Scarboro Rd. Oak Ridge, TN 37830 Voice: 865.481,0683 www.eberlineservices.com
Internal Work Order
Analysis Code
Run Number
Notes
Page 1 of 1
18-03110
UUISO 1
ALIQUOTED AND ADDED SPIKES AND TRACERS- DRIED SAMPLES DOWN AND SUBMITTED
SAMPLES TO SEPARATIONS
Added concentrated HCI to sample beakers and heated to dryness; Added 20 ml 8N HCL to samples and
transferred to new, labeled C-Tubes, rinsing with 8N HCI to bring volume to ~35 ml; Preconditioned resin
columns with 35 ml 8N HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 ml 8N
HCI, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml 8N HCI - 0.1 N NH4I, 35 ml
of 6.5N HCI - 0.04N HF, and 10 ml of 6.5N HCI; Eluted Uranium with 50 ml of 0.5N HCI into clean, labeled 100
ml beakers; Dried-down samples on hotplate; Dissolved samples in ~1 O ml of concentrated HCI; Transferred tc
new, labeled C-Tubes with DI H2O. Set samples aside for later precipitation and filtering.
Followed steps 12.1.7 to 12.4.5 in AP-005. ( Precipitated and filtered samples for Uranium}
0077
Eberline Analytical
Oak Ridge Laboratory
Q EBERLINE .® ·············································-·················siRv1-c·is
Reagents Used in an Analysis
Reagent Reagent
ID Name
017230P Anion Exchange Resin -·~•~·--·- -·-·····-·--··---·····--~-
019826S HCI - HF -- . --·--·····-· ----·~·-
019775D02 Hydrochloric Acid
019827S Hydrochloric Acid -~-...... __.., •><••--·-····
019842S Hydrochloric Acid
Reagent
Printed: 3/30/2018 4:58 AM Page 1 of 1
Internal Work Order
18-03110 Analysis Code Run
UUISO 1
Analyst Date
Concentration ID Recorded
Reagent Grade JDEMELAS 3/29/2018
6.5N - 0.04N JDEMELAS 3/29/2018
0.5N JDEMELAS 3/29/2018
6.5N JDEMELAS 3/29/2018 ·=···----·-·-·--
SN JDEMELAS 3/29/2018 ···-·-••,.-····--·~·-·~· ···-•-•>•--·
019861S HCI - NH41 SN - 0.1M JDEMELAS 3/29/2018 -·--···--·-··-·-----.,~··· . ----·--------·~···· ··-·--·-~
019831P Hydrochloric Acid Reagent Grade JDEMELAS 3/29/2018 ~•w•-~•--••'"--•-
-••m•-•----
019803S Carbon substrate Solution TSMITH 3/30/2018
019525P Hydrofluoric Acid Reagent Grade TSMITH 3/30/2018
···-·- ·-·--· _______ ,. __ ~·····-• --•--•••••••••--••••-•~•••••M•-•••-~•••-' •
019640S Neodymium Carrier 1 mg/ml TSMITH 3/30/2018
··-··. ---·--·~•>••·-------
019599P Reagent Alcohol Reagent Grade TSMITH 3/30/2018 __ " ___ .,, _____________
019433P Titanous Chloride Reagent Grade TSMITH 3/30/2018
0078
;
A-\ehc"- ·-. _S
- . --- 67 -·----...__ 001:\-e,... $c~111-t-:>le.,, tr l'Ji'e'.i'lt lor1)._ fi,Me,. Co1J;1fJ;\i,1t~ Arw,1~ ·"f:Lc~
, -1,)h; 1 t1o·~, ei \ \'\ l t--t) u (_f::,:{I._ ' l l'-'S-<"' ~o-, ~v,:v-r~ \Ll2 --~------ C
~Gtc\£i -I L~~~~1~UM,A ~'i\ 'i.-\:L\J ;lf'\v!S)..:__ ~ .
',,, ·,,
UG""I'- /JO - . -Ii-- -- \,,~, +_[;j-(3/t; 101--lci\ l\29 J,-\\.,-0\)....,;; I
~ti) -.. ·. •.
-------------. <;:;,_l,26 ·~ UI.J::::, {l ,~~])'\) ------- t J 6d1(ci A __ {JI 4) Yuzi.i·z_ - ••• >
---------- 2/JQfJ_f/;_ UtrJP- 1-SZlf (.,.,h -SV/0(6'1 KP' -7/'3o[l8 lBP3ll& /+( \-4) U(D\K, t')Zi' uu V,P ·-
·,·,
--- 7.J,1 S-6 fill I fl -")/30/lB / 80lli O A LL1i2 rsi& 'lht;61v1( ~'l !lU xP
. ·-
/V\O ·.,,
·-
3 l:3dlf'l ___ l~ C?:, l l_u_11__C::) -~ y ) tA.>Y'f\;0 l'3tS'1- (.J-1~1)·-_;. \(1-;, ·- ·._, ...
l 1 ~J
" --~
--., l,
~--.
_,, ..
·-
l ·-
----·
--_,,,.
------
--. '
·-
I I I
,. ',.
--· "• \;,
' '
--
,\,
' " ' , __
i .
t
--~·--··-·-
0079
TOTUNOTES
0080
#
1
Printed: 4/12/2018 1 :09 PM
~ E E:I E:: R L.,,J ....._. E:: ~ SERVICES
Work Order Analysis Notes
Date Dept User
04/12/18 13:09 PREP JPACHELLA
Oak Ridge Laboratory
601 Scarboro Rd. Oak Ridge, TN 37830 Voice: 865.481.0683 www.eberlineservices.com
Internal Work Order
, ............................. ,. ............................... + Analysis Code
Run Number
Notes
Page 1 of 1
18-03110
Samples were aliquoted and wet ashed until clear. Samples were diluted. Dilution was aliquoted and mixed
with Uraplex. Samples were analyzed by KPA. Samples demonstrated intensities within the calibration range.
q f/ r;.~/r _,. .. / ye:cA-L-L(_,('_,
0081
Eberline Analytical Oak Ridge Laboratory
EBERLINE sic::RvtcEs
Reagents Used in an Analysis
Reagent ID
Reagent Name
018695P Hydrogen Peroxide ,,,,,,,,-,,,,,,,,,,,, ____ ,,,,,, ,_,,,
019318D01 Nitric Acid ,,,,,,,,,,,,,,,,,,,
019436P Nitric Acid
019079P Uraplex
Printed: 4/12/2018 1:10 PM Page 1 of 1
Internal Work Order
18-03110 Analysis Code
KPA_LIQ
0.3
0.8N
Reagent Concentration
Reagent Grade
Reagent Grade
Analyst ID
JPACHELLA
,,,,,,,,,,,,,,,,,_, __ ,,,_,_,,,_,,,,,,/,,,,,,,,,,,,,,,,,,,,,,,
0082
ISO TH NOTES
0083
Printed: 3/28/2018 9:19 AM Page 1 of 1
-~ . . Oak Ridge Laboratory Internal Work Order 18-03110 ~EBERLINE 601 Scarboro Rd. V-N--•--,-~~•·----- --•--••-•-•••-•••M•-•-•-•-- ss~-
.. SEHYICES Oak Ridae, TN 37830 Analysis Code ThlSO Voice: 865.481.0683
Work Order Analysis Notes ... --··- . ···-· ··-----·-··--···-··-·· ---·--·-,-~
www.eberlineservices.com Run Number 1
# Date Dept User Notes
1 03/28/18 09: 19 PREP JHARVEY ALIQUOTED AND ADDED SPIKES AND TRACERS- DRIED SAMPLES DOWN AND SUBMITTED
SAMPLES TO SEPARATIONS
0084
Printed: 3/29/2018 3:18 PM
(l:'.BERh~~c~ Work Order Analysis Notes
II Date Dept User
1 03/28/18 09: 19 PREP JHARVEY
2 03/29/18 15:18 CHEM JDEMELAS
Oak Ridge Laboratory
601 Scarboro Rd. Oak Ridge, TN 37830 Voice: 865.481.0683 www.eberlineservices.com
Internal Work Order
Analysis Code
Run Number
Notes
Page 1 of 1
18-03110
ThlSO 1
ALIQUOTED AND ADDED SPIKES AND TRACERS- DRIED SAMPLES DOWN AND SUBMITTED
SAMPLES TO SEPARATIONS
Added concentrated HNO3 to sample beakers and heated to dryness; Added 20 ml 8N HNO3 to samples and
transferred to new, labeled C-Tubes, adding 8N HNO3 to bring volume to ~35 ml; Preconditioned resin
columns with 50 ml 8N HNO3; Centrifuged samples as needed, and passed through columns; Rinsed C-Tubes
with 20 ml 8N HNO3; Centrifuged rinsates and loaded onto columns; Rinsed columns with 40 ml 8N HNO3;
Eluted Thorium with 50 ml of 8N HCI into clean, labeled 100-ml beakers; Dried-down samples on hotplate;
Dissolved samples in ~10 ml of concentrated HCI; Transferred to new, labeled C-Tubes with deiononized
water, bringing volume to ~15ml. Set sam12les aside for later 12reci12itation and filterina.
0085
Printed: 3/30/2018 4:53 AM
,: E B E R ~ ~!;':10
!;';; Work Order Analysis Notes
# Date Dept User
1 03/28/18 09: 19 PREP JHARVEY
2 03/29/18 15:18 CHEM JDEMEl..AS
3 03/30/18 04:53 CHEM TSMITH
Oak Ridge Laboratory
601 Scarboro Rd. Oak Ridge, TN 37830 Voice: 865,481.0683 www.eberlineservices.com
Page 1 of 1
Internal Work Order 18-03110 t--••-----~--------------•-~"•w-
Analysis Code Th I SO Run Number 1
Notes
ALIQUOTED AND ADDED SPiKES AND TRACERS- DRIED SAMPLES DOWN AND SUBMITTED
SAMPLES TO SEPARATIONS
Added concentrated HNO3 to sample beakers and heated to dryness; Added 20 ml 8N HNO3 to samples and
transferred to new, labeled C-Tubes, adding 8N HNO3 to bring volume to ~35 ml; Preconditioned resin
columns with 50 ml 8N HNO3; Centrifuged samples as needed, and passed through columns; Rinsed C-Tubes
with 20 ml 8N HNO3; Centrifuged rinsates and loaded onto columns; Rinsed columns with 40 ml 8N HNO3;
Eluted Thorium with 50 ml of 8N HCI into clean, labeled 100-ml beakers; Dried-down samples on hotplate;
Dissolved samples in ~10 ml of concentrated HCI; Transferred to new, labeled C-Tubes with deiononized
water, bringi!!_g volume to ~15ml. Set samples aside for later precipitation and filtering.
Followed steps 12.2.5 to 12.4.5 in AP-005. ( Precipitated and filtered samples for Thorium)
0086
Eberline Analytical Oak Ridge Laboratory
Reagents Used in an Analysis
Reagent Reagent
ID Name
017230P Anion Exchange Resin
Printed: 3/30/2018 4:59 AM Page 1 of 1
Internal Work Order
18-03110 Analysis Code
ThISO
Reagent Concentration
Reagent Grade
Analyst ID
JDEMELAS
Run
1 Date
Recorded
3/29/2018 -···-···············-----····· --~·-·"'--·--·---·····--·~-.. ~~---- ·---·"
019842S Hydrochloric Acid SN JDEMELAS 3/29/2018
019831P Hydrochloric Acid Reagent Grade JDEMELAS 3/29/2018 -<--<-~••--"'-=M= ···················-···-···-
019859S Hydrochloric Acid 8N JDEMELAS 3/29/2018 -..... •·-----,--~---.. ---·~·-·-·
019673P Nitric Acid Reagent Grade JDEMELAS 3/29/2018
019860S Nitric Acid SN JDEMELAS 3/29/2018
019803S Carbon substrate Solution TSMITH 3/30/2018
019578S Cerrium Carrier 0.lmg/ml TSMITH 3/30/2018 -~~---·-----.-·-·~·~
019525P Hydrofluoric Acid Reagent Grade TSMITH 3/30/2018
019599P Reagent Alcohol Reagent Grade TSMITH 3/30/2018 •- ~ --•••-•u-.-w --•--H•ll--••-
0087
0088
RA-226 NOTES
0089
Printed: 3/28/2018 9:27 AM
~ E;:BERh~!;:Jc~ · Work Order Analysis Notes
# Date Dept User
1 03/28/18 09:27 PREP JHARVEY .
Oak Ridge Laboratory
601 Scarboro Rd. Oal< Ridae, TN 37830 Voice: 865.481.0683 www.eberlineservices.com
Page 1 of 1
Internal Work Order 18-03110 Analysis Code Ra226
---·-------------------·----Run Number 1
Notes
ALIOUOTED AND ADDED SPIKES AND TRACERS- PH'D SAMPLES- PRECIPITATED WITH BA AND PB
CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND CENTRIFUGED- SUBMITTED
RADIUM PRECIP TO SEPARATIONS
0090
Printed: 4/2/2018 3:07 PM Page 1 of 1
,: Oalc Ridge Laboratory Internal Work Order 18-03110 601 Scarboro Rd. ,. ____ ,. __
~• -----• •-w~--•--H• •••- ••-----•- ---EBER~~~c~ Oak Ridge, TN 37830 Analysis Code Ra226
Work Order Analysis Notes Voice: 865.481.0683 ·-.
www.eberlineservices.com Run Number 1
# Date Dept User Notes
1 03/28/18 09:27 PREP JHARVEY ALIQUOTED AND ADDED SPIKES AND TRACERS- PH'D SAMPLES- PRECIPITATED WITH BA AND PB
CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND CENTRIFUGED- SUBMITTED
RADIUM PRECIP TO SEPARATIONS
2 04/02/18 15:07 CHEM EBAILEY ADDED EDTA TO SAMPLES AND LET SIT. ADDED AMMONIUM SULFATE AND ACETIC ACID TO
SAMPLES. FILTERED ONTO TARED FILTER PAPERS, LET DRY UNDER HEAT LAMP, REWEIGHED,
ANn "'' 11:a.,TT<=l"I Tn r-rn 1NT.
0091
Eberline Analytical Oak Ridge Laboratory
. . -~ $'"¼ - I:;: ae:: .. R .. k-J .....,. e:: ~
SERVICES
Reagents Used in an Analysis -~~-~,,~-
Reagent Reagent ID Name
019782P Ammonium Hydroxide
019713D03 Ammonium Sulfate
019792D01 Barium Carrier -
019464D01 Lead Carrier
019673P Nitric Acid
019210P Acetic Acid -·
019065D02 Ammonium Sulfate
019226S EDTA
Reagent
Printed: 4/2/2018 3: 54 PM Page 1 of 1
Internal Work Order
18-03110 Analysis Code Run
Ra226 1 Analyst Date
Concentration ID Recorded
Reagent Grade JHARVEY 3/28/2018
200 mg/ml JHARVEY 3/28/2018
1 mg/ml JHARVEY 3/28/2018
166 mg/ml JHARVEY 3/28/2018
Reagent Grade JHARVEY 3/28/2018
Reagent Grade EBAILEY 4/2/2018
200 mg/ml EBAILEY 4/2/2018
0.25M EBAILEY 4/2/2018
0092
s .. · •Cb·i.•·•·(';c > ...•.. ; \ ..
A--\~h°' 3 . ...:::, 67 ----
Dc,:\-e, ~':i(hl__'lj~-:>le.. ·j+ ----~CL~1t loo.A''?iMe C OVltl"li\vt,(~ ArV,\\Y5, \ i-lciri ~~1·~hA iJ_'jti!l\c\\Z\l t--t)
-
ll w'I"- ll\5-.~--- cll/4o, ~v~?.J-r'J \LI)
~ ' )t\v~.!.,. \lf) -
_ID~ V~u- ~ 1\ \j,G-.,.\L \\,rt,~ AJo f / (J~ - ~~ULL · . -:_--_:t
~
·O V __
;z.\:}'.~~--_lIB_tC3 l ~ i 14-' Y:j \ l\2~ ,A.w,_ I I ~lb
-.
\. l SJ,::, .. l\._,,,, __ ~ ~--- 7)--\ # ----- _]}30/25_ U3ciitci J+ (31f:i'> UfQR.. a ;zl( 0 h ~-cfll!( 6'1
·l'""', lt[l. KP --
---Pu··
1fsoho UCD\R l>Z~ 1,);1 S--0 !1111 ~1 _lLU V,P -
---JEi\:)31 I & A-( \-L{
:;/30/t8 l863J19A 61 i2 AMo t)Zl .. , 'l f1 ~M [ ~1 uu XP --
e~tl_ li,~_2Lln.il.~)--"-t ) ,w_y_'{\J:J l>G'1- ~t'6:D~ lCP -
l LL,{
~,.\ ?)-ki,~C1kcA-II . I lc/3 -
§1_\L~ l-0...Jv:.,1 lli.50_ l!;,,'i\J hr." d-
Y/L/18 ·rx; \ i ¥ RJ l i;1// 1 _c1.:b os-1° I C1tvu>1 f\lr.:,._ Y\P -
!Jiwa_ Jt6o3/z&A-( 1-'-i) U(D/( ci'll..-:f- -fJl 13"0""1, '.1 tP -. uu
11 I ·z_ A 8 t fb··3rzli A-(1 -L\J ~ll~ ,~1\i 11. ef+Zo -;-, XP --
zh s1',,,,1, ·11 1-11
-'1L?J18. \66-SI zq A-(!;J) \ 0 '),.? 17v --
- 5~y /VJi-fll . 2J,, ~-0111.;~,J KP"
jji/J 8 I '3o ~ lsz A (1 -'-0 (<c,,,.__ ,.
- us io3& i --Z-h S"'t?t-n /,1 t:,,P
l//t,.,/( 6 lt'X'fSl~A u 1 'D tifof:.. \D)~~ 'Z✓h St:'1ii11~11 JGP --
uu lf /;Zll6 1f2Q~~&AL1 -rs) 5015 f\h,r+h t zs--1 t(cr.._ KP
.,,
7, lr1 7'°'0V\t\;~
~l~ill- Q,,_ \J -
- _l~ c :> \ \.':l \ Ji::Lj~)__ u~ <L LS~:3:: -Ll--tm ~ _w __
~{L fb?__ b.l-~3-~~!t>-~\.-~
-, ·-. ~r,_\f ll__-_·
5'.;,SJ~ .. 1-\-~~ _\uc+ ;2,\,.~t) -J.
~l1,, n \1>tJ'3 \ \0~L,-1':) fJ.ryv\,\) ~h,,;:so ....I- 2t»"¼ .• \l!J ---
- l on9
-~lb L_Y_ i{ ~3 ti 91-A- l.\ ~ l!.)) 6('..~ tJ,Avv...eo_LQ,,. ;;h;0J -i w -.
'\,~1.,,'t) ~lv-~
✓
--
-- ,_____ ___ --·~- --·-·-·
-- - -
-- '----
-- ---~-- I -·-· I ;
,,/ '
- ----- ---
- ,.____ --~-~--
-, "
_,,. ----
~,-.. ·--- - ~-~---------·
~,, __ ...., e ~--
I I ..
--·,
- ,,
0093
RA-228 NOTES
0094
Printed: 3/28/2018 9:28 AM
,: E BER!;;:,ls~c~
Worlc Order Analysis Notes
# Date Dept User
1 03/28/18 09:28 PREP JHARVEY
Oak Ridge Laboratory
601 Scarboro Rd. Oak Ridqe, TN 37830 Voice: 865,481.0683 www.eberlineservices.com
Internal Work Order
Analysis Code
Run Number
Notes
Page 1 of 1
18-03110 Ra228
1
ALIQUOTED AND ADDED SPIKES AND TRACERS- PH'D SAMPLES- PRECIPITATED WITH BA AND PB
CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND CENTRIFUGED- SUBMITTED
RADIUM PRECIP TO SEPARATIONS
0095
Printed: 4/9/2018 11 :27 AM
(EBER~~~c!=,; Work Order Analysis Notes
# Date Dept User
1 03/28/18 09:28 PREP JHARVEY
1,.,.--~---· --2 04/09/18 11 :27 CHEM EBAILEY
Oalc Ridge Laboratory
601 Scarboro Rd. Cale Ridge, TN 37830 Voice: 865.481.0683 www.eberlineservices.com
Internal Work Order
Analysis Code
Run Number
Notes
Page 1 of 1
18-03110
Ra228 1
ALIQUOTED AND ADDED SPIKES AND TRACERS- PH'D SAMPLES- PRECIPITATED WITH BA AND PB
CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND CENTRIFUGED- SUBMITTED
RADIUM PRECIP TO SEPARATIONS
ADDED FILTER PAPERS FROM COUNT ROOM TO LABELED C-TUBES, FILLED WITH EDTA SOLUTI-OtT
AND LET SIT OVERNIGHT. REMOVED FILTER FROM EDT A-ADDED 2MLS YTTRIUM 9MG/ML CARRIER
ADDED 18N NAOH TO SAMPLES AND RECORDED T1. HOT BATHED FOR 15 MIN, CENTRIFUGED AND
DISCARDED SUPERNANT. ADDED 6N HNO3, DI WATER, AND 10N NAOH. HOT BATHED FOR 15 MIN,
CENTRIFUGED AND DISCARDED SUPERNANT. ADDED 1 N HNO3, DI WATER, AND AMMONIUM
OXALATE. FILTERED ONTO TARED FILTER PAPERS. LET DRY UNDER HEAT LAMP, REWEIGHED AND
SUBMITTED TO COUNT.
0096
Eberline Analytical Oak Ridge Laboratory
Q EBERLINE _@ ....... ············· ........ SERv1cEs
Reagents Used in an Analysis
Reagent ID
................................................ , .......... - ........ , ... _. __ _ Reagent
Name
Printed: 4/9/2018 11:27 AM Page 1 of 1
18-03110 Analysis Code
Ra228
Reagent Concentration
Analyst ID
Run
1 Date
Recorded
019782P Ammonium Hydroxide Reagent Grade JHARVEY 3/28/2018 · ............ ..................... ......................... ---1 .......................... - ....... _____ 1------............................ f
019713D03 Ammonium Sulfate 200 mg/ml JHARVEY 3/28/2018 .......................... _, ......... - ............. -+--~-----·-···~-------~----·----------·-----~--.... -, ................................................. ..
019792D01 Barium Carrier 1 mg/ml JHARVEY 3/28/2018
019464D01 Lead Carrier 166 mg/ml JHARVEY 3/28/2018 ................ + .......................................... _________________________ .... _+-_
019673P Nitric Acid Reagent Grade JHARVEY 3/28/2018 _____ ____, ....
018122D04 Ammonium Oxalate 5% EBAILEY 4/9/2018 ---
019226S EDTA 0.25M EBAILEY 4/9/2018 -- -·- ·------·•-"-" _____ _,
018971D06 Nitric Acid lN EBAILEY 4/9/2018 .........................
019673D02 Nitric Acid 6N EBAILEY 4/9/2018 .... ,.,_ ........................................ .
018699D10 Sodium Hydroxide lOM EBAILEY 4/9/2018 .... , ........................... , ..
018699D07 Sodium Hydroxide 18M EBAILEY 4/9/2018
0097
--·-···-- ·----- -----·--l-·----------1-------~- ____ ____,_ __ ... ··,.
····-··--·-·-·-,----------'f-------~-------j-------t-----------f---------+-----c,,i.: .. ;
-·------------1--------+----------I---------·-----··---·----· -----1--·-----.. •:,
··,,··•,
. ·-·-·--··•--t-------t-----------l------ ___ ___,__ ___ ·--·-···· --~····--·--··-------1··-··-------,,, ...... ,,
·- -··---·-···-·--·· ----1-----------1-----------1-------·--···--------~--I----•-
.,
'
-- . ... . -- . . ·----- . . --- ·\ ·'1
·-···-- ----·-·---------,\---·-------·-·------•---~--------I
····---·--1-----·------+--------·-·--··--·---···------·····-··-··-•-----i-----------1- ....... --·- . - --·· ·,,.
-----··--- -·-•--I----------~--------·-·------------------------~----•--------- -··-------.s••-·--------··-· ·•·--··-·-·----·-·-···,.,, ...
"--·····---·---··-··-·--1---·---------·--------·--- ·--·----··-----·------------·------·----- -·-- --------·--------- ------ --- --------·--- - ·--------···---- 1--··---- -- -- - -···· -·-·- 1-----·
·----··--·- ·-· _.,-•-·--····-··--···•)~---._ .. ___ -----+------ .---·-· -··---·---·····---····--····-··---··•---··-··-·· ---·---·- ·-·· ----··-----· ··-· ·--···-. --
. -•·-----·---------Ji---------
..... --·---·--------+---- -····-·--·--···----·---·· -- ·-···- -··-- ·····-·-·------·----~----i-----.-----·----·-----·- ·--·-·-- -··-·----·-·-··---···.«'·'
-- ----·····--····---.,,r-----_ ___ --------1-____ ________, ____ __.__ __ ----I---____ ....... -- ----·-··-·-,.-·-···-----·-·· --
--·----1---------+----·--··-·--·--·---------t-• -·- .. --···-·····-····--·-·-··- -- -·-······-----·--- , .. --
0098
ALPHA/BET A NOTES
0099
Printed: 3/27/2018 3:00 AM
~Ea E Rh~r:I!;;; Work Order Analysis Notes
# Date Dept User
1 03/27/18 03:00 PREP MHIGHTOWER
Oak Ridge Laboratory
601 Scarboro Rd. Internal Work Order
Analysis Code
Page 1 of 1
18-03110
GaGbT ThSr Oak Ridge, TN 37830 Voice: 865.481.0683 www.eberlineservices.com
······-------+--------=------11 Run Nurnber 1
Notes
Ran TDS/TSS to determine aliquot. Aliquoted samples, dried, nitrated, transferred to tared planchets, dried,
flamed, re-weighed, and submitted to count room
0100
Eberline Analytical Oak Ridge Laboratory
. . -~ Q EBERLINE _"'@ ......................... ···························· ......... SERvicEs
Reagents Used in an Analysis
Reagent Reagent
ID Name ----~----·==-•--"=·--~
019074D01 Nitric Acid , .........
3N
Printed: 3/27/2018 4:09 AM Page 1 of 1
Internal Work Order
18-03110 --·~·-
Analysis Code Run ·------
GaGbT _ThSr 1 ~~-·
Reagent Analyst Date
Concentration ID Recorded
MHIGHTOWER 3/27/2018
0101
~G>8 P -=-----1--_c=.__--+-~~---i~"-l---------J--/-
c -:r, z y /( <
I---os V\,
~~-~~-~~6q~---+---'-~~~~-~~p__
,"---+~~-1-K p 'Cb
~~--=-4 ~~~~----1:~--l--~n&_------i-~~_J_t':r;g
, \lb
____ __c;c'-~--r---------',-----!-----+-------------!i:---------4------
0102
SECTION VIII
ANALYTICAL DAT A (ISOTOPIC URANIUM)
0103
Eberline Analytical
Oak Ridge Laboratory
Analysis Sheet
Work Order
Analysis Code ~ UUISO 1
Date Received 3/23/2018
Lab Deadline 4/12/2018
Client I AMO Environmental Decisions
Project WESTLAKE
Report Level 4
Activity Units pCi
Aliquot Units
Matrix WA
Method EPA 908.0 Modified
Instrument Type Alpha Spectroscopy
Radiometric Tracer U-232
Radiometric Sol# U-10a
Tracer Act (dpm/g) 18.21
Carrier
Carrier Cone (mg/ml)
18-03110 UUISO Run 1
Printed: 313012018 4:58 AM
Page 1 of 3
I i i
Internal Sample [ Client Login i Sample Sample
Fraction Desc I ID CPM / Date Aliquot
~. 01 Les ~cs I 03123I1s 00:00 ~1.ooooE+oo
02 MBL BLANK · 03/23/18 00:00 1 1.0000E+00 I
I i
I
03 I DUP OU-1-008 38 I 03/19/18 18:02 : 5.0000E-01
- ! I
04 I DO OU-1-008 38 I 03/19/18 18:02 5.0000E-01 .
1
I 1
I I l~--------~
I i !
i I
I
1
!
I I
J--------"----f-------······ ... . +- I ' ··_ ·--__ _____,
* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. A Indicates estimated SAF value.
** Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
0104
Eberline Analytical
Oak Ridge Laboratory
Analysis Sheet
Internal Sample I Tracer
Fraction Desc I
Aliquot (g)
01 LCS 0.6058
02 MBL 0.6057
03 DUP 0.5941
04 DO 0.6001
I I
I
I I
I I
I Tracer Total I
Radiometric
ACT(dpm) Tracer (pCi) I
11.0 ~-·---
11.0 --~--
10.8
10.9
18-03110 UUISO Run 1
I R d. tr· : G C . ; a ,ome 1c rav arr,er
I % Rec i Added (ml) Grav Filter
Tare (g)
I 0.00 1
i !
I 0.00/ I
o.ooi I !
0.001 !
i !
! I I !
i i
I I I I
i I
I I
I
! Grav Filter Final (g)
I
• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. ~ Indicates estimated SAF value.
•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
I Grav Filter Grav I Net (g) %Rec i
I I
I !
i i I I I i
!
I i
I
I I
I
j
I
I !
I I
Printed: 313012018 4:58 AM Page 2 of 3
Mean I SAF I SAF
I ! %Rec 1* 2· i
I ~ ..
-·-··-~
I
0105
Eberline Analytical Oak Ridge Laboratory
Analysis Sheet
Internal [ Sample
Fraction I Desc
01 LCS
02 MBL
03 DUP
04 DO
Rough Prep Rough Prep
Date By
-
-
:
i
I
i I I
l
Prep I Date !
03/28/18 08:39
03/28/18 08:39
03/28/18 08:39
03/28/18 08:39
'
I
18-03110 UUISO Run 1
Prep By
JHARVEY
JHARVEY
JHARVEY
JHARVEY
I Sep to
I Date/Time
• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. " Indicates estimated SAF value.
•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Sep tO I I
By I I
I
I
\
i
I
! -
;
Printed: 3/3012018 4:58 AM Page 3 of 3
Sep t1 Sep t1
Date/Time By
i
I I
0106
Eberline Analytical Oak Ridge Laboratory
~ Lab Nuclide
Fraction
01 U-234
C: :::s ct:
.g 0 0 .!!!
i C: "'(
C: -!!! u
""'"
0 u, -::> ::>
1/) C: 0 "in ·c:; Q)
C cu -C: Q)
E C: 0 I,..
·s; C: w 0 :!:: ~
02 U-234
03 U-234
04 U-234
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-0311 0-UUISO-1
Client Activity Results Error Estimate MDA
Identification Units
LCS pCi/1 6.06E+00 8.95E-01 6.70E-02
BLANK pCi/1 -9.93E-03 3.02E-02 8.24E-02
OU-1-008 pCi/1 1.17E+00 3.65E-01 1.52E-01
OU-1-008 pCi/1 1.06E+00 3.62E-01 1.48E-01
LCS I LCS
Known I ¾R
7.28E+00 83.21
Printed: 4/2/2018 8:22 AM Page 1 of 3
LCS RPD MDA Blank
Flag Flag Flag Flag
OK OK
OK OK
OK OK
OK
0107
Eberline Analytical
Oak Ridge Laboratory
( Lab Nuclide Fraction
01 U-234
§ a::
{: 8 .!!? ~
1a C: c:(
jl 0
~
0 u, -::, ::,
1/) C: 0 iii u (I)
C
Jg C: (I)
E C: 0 I..
·s;: C: w 0 ~ <
02 U-234
03 U-234
04 U-234
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03110-UUISO-1
Sample I Sample Radiometric Grav Mean
Date I Aliquot %Rec %Rec %Rec
03/23/18 00:00 1.00E+00 114.68 0.00 0.00
03/23/18 00:00 1.00E+00 106.37 0.00 0.00
03/19/18 18:02 5.00E-01 110.03 0.00 0.00
03/19/18 18:02 5.00E-01 102.43 0.00 0.00
SAF SeptO
Date/Time
Printed: 4/2/2018 8:22 AM Page 2 of 3
I Sept1
I Date/Time
0108
Eberline Analytical
Oak Ridge Laboratory
( Lab Nuclide
Fraction
01 U-234
i:: ::, Q:
Cl)
"0 0 0 .!/? ~ cij i::
c:i:
II
~
0 en -::, ::,
II) C: 0
.!!? u Q)
C
.s C: Q)
E C: 0 ... ·s; C: w 0 :E <(
02 U-234
03 U-234
04 U-234
I Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-0311 0-UUISO-1
Counting Halflife Detect Carrier Count
Counts
DatefTime (days) Time
03/30/18 13:25 A_Spec Alpha_057 170 4.33 E+02
03/30/18 13:25 A_Spec Alpha_058 170 -6.80 E-01
03/30/18 13:56 A_Spec Alpha_043 170 4.62 E+01
03/30/18 13:56 A_Spec Alpha_044 170 3.75 E+01
I Bkg CPM
2.00 E-03
4.00 E-03
5.00 E-03
3.00 E-03
Printed: 4/2/2018 8:22 AM Page 3 of 3
Eff
16.5
17.1
19
18.4
0109
Eberline Analytical
Oak Ridge Laboratory
<( Lab Nuclide Fraction
01 U-238
§ 0::
{: 0 0 .!/.! ~ iii c:: "(
~I
T""
0 u, -:::, :::,
1/) s::: .2 .!!! CJ Q)
C
Jg s::: Q)
E s::: 0 ... ·s;
s::: w 0 ::l!: <(
02 U-238
03 U-238
04 U-238
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-0311 0-UUISO-1
Client Activity Results Error Estimate MDA Identification Units
LCS pCi/I 6.13E+00 9.03E-01 6.67E-02
BLANK pCi/I -2.91E-04 3.09E-02 9.16E-02
OU-1-008 pCi/I 9.26E-01 3.18E-01 1.21E-01
OU-1-008 pCi/I 1.04E+00 3.59E-01 1.68E-01
LCS LCS
I Known %R
7.06E+00 86.91
Printed: 4/2/2018 8:22 AM Page 1 of 3
LCS RPO MDA Blank
Flag Flag Flag Flag
OK OK
OK OK
OK OK
OK
0110
Eberline Analytical Oak Ridge Laboratory
~ Lab I Nuclide
Fraction
01 U-238
s:::: ::, a:::
(I)
~ 0 u .!!! ~ "iii s:::: <t
11 u
~
0 u, -:::, :::,
U) C: 0
:!!? 0 Cl)
C
s C: Cl)
E C: 0 ... ·s: C: w 0 :E <(
02 U-238
03 U-238
04 U-238
Sample Oesc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03110-UUISO-1
Sample Sample Radiometric
I Grav Mean
Date Aliquot %Rec %Rec %Rec
03/23/18 00:00 1.00E+00 114.68 0.00 0.00
03/23/18 00:00 1.00E+00 106.37 0.00 0.00
03/19/18 18:02 5.00E-01 110.03 0.00 0.00
03/19/18 18:02 5.00E-01 102.43 0.00 0.00
SAF I
SeptO OatefTime
Printed: 4/2/2018 8:22 AM Page 2 of 3
I Sept1
OatefTime
0111
Eberline Analytical Oak Ridge Laboratory
~ Lab Nuclide
Fraction
01 U-238
C: :, ll:
.g 0 (.)
.!!! ~ 'iij C: ,q;
~
~
T-
0 UJ -::, ::,
u, C 0
.!!? c., Q)
C
~ C Q)
E C 0 ... > C w 0 :!: <(
02 U-238
03 U-238
04 U-238
I I Sample
Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03110-UUISO-1
Counting Halflife Detect Carrier Count
Counts
Date/Time (days) Time
03/30/18 13:25 A_Spec Alpha_057 170 4.40 E+02
03/30/18 13:25 A_Spec Alpha_058 170 -2.00 E-02
03/30/18 13:56 A_Spec Alpha_043 170 3.67 E+01
03/30/18 13:56 A_Spec Alpha_044 170 3.70 E+01
I Bkg CPM
2.00 E-03
6.00 E-03
2.00 E-03
0.00 E+00
Printed: 4/2/2018 8:22 AM Page 3 of 3
Eff
16.5
17.1
19
18.4
0112
Eberline Analytical Oak Ridge Laboratory
~ Lab Nuclide
Fraction
01 U-235
§ a:
.g 8 ,!!! II)
~ a, C: "(
--~ 0
~
0 en -::::, ::::,
U) s:: 0
.!!? c., Q)
C
.B s:: Q)
E s:: 0 11-·s: s:: w 0 :ii! <(
02 U-235
03 U-235
04 U-235
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-0311 0-UUISO-1
Client I Activity Results Error Estimate MDA
Identification I Units
LCS pCi/1 4.67E-01 1.87E-01 1.04E-01
BLANK pCi/1 5.76E-03 3.73E-02 1.02E-01
OU-1-008 pCi/1 1.14E-01 1.24E-01 1.S0E-01
OU-1-008 pCi/1 9.83E-02 1.19E-01 1.45E-01
LCS LCS
I Known ¾R
Printed: 4/2/2018 8:22 AM Page 1 of 3
LCS RPD MDA Blank
Flag Flag Flag Flag
OK
OK OK
NA OK
OK
0113
Eberline Analytical
Oak Ridge Laboratory
( Lab Nuclide
Fraction
01 U-235
§ a::
.g 0 u .!!,!
~ '"iii C: ct
~I
~
0
"' -::::, ::::,
ti) C: 0 ti)
·c:; Q)
0 iii -C: Q)
E C: 0 ... ·s; C: w 0 == <(
02 U-235
03 U-235
04 U-235
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03110-UUISO-1
Sample Sample Radiometric Grav Mean
I Date Aliquot %Rec % Rec % Rec
03/23/18 00:00 1.00E+00 114.68 0.00 0.00
03/23/18 00:00 1.00E+00 106.37 0.00 0.00
03/19/18 18:02 5.00E-01 110.03 0.00 0.00
03/19/18 18:02 5.00E-01 102.43 0.00 0.00
I SeptO
SAF DatefTime
Printed: 4/2/2018 8:22 AM Page 2 of 3
Sept1 DatefTime
0114
Eberline Analytical Oak Ridge Laboratory
( Lab Nuclide Fraction
01 I U-235
C: :, a:
.g 8 .!!,!
~ ca C: q;
1: -!!! 0
T-
0 en -:::> :::>
1/) C: 0 ·;; ·c:; Cl)
C cu -C: Cl)
E C: 0 I-
> C: w 0 ::!!: <(
02 U-235
03 U-235
04 U-235
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03110-UUISO-1
Counting Halflife Detect Carrier I
Count Counts
Date/Time (days) Time
03/30/18 13:25 A_Spec Alpha_057 170 2.70 E+01
03/30/18 13:25 A_Spec Alpha_058 170 3.20 E-01
03/30/18 13:56 A_Spec Alpha_043 170 3.66 E+00
03/30/18 13:56 A_Spec Alpha_044 170 2.83 E+00
1 Bkg
I CPM
0.00 E+00
4.00 E-03
2.00 E-03
1.00 E-03
Printed: 4/2/2018 8:22 AM Page 3 of 3
Eff
16.5
17.1
19
18.4
0115
Count Room Report Client: AMO Environmental Decisio
~E f' 11ntema~ \-sa~ple-\ Client
Fraction Desc I ID
01 LCS LCS
02 MBL BLANK
I 03 DUP OU-1-008
04 DO OU-1-008
18-03110-UUISO-1 (pCi/1) in WA
Tracer ID: U-1 0a
Sample
I Sample I Tracer
I Date Aliquot I
A/iquot(g)
03123118 00:00 I 1.0000 i 0.6058
03/23/18 00:00 I 1.0000 I 0.6057
03/19/18 18:02 I 0.5000 I 0.5941
03/19/18 18:02 0.5000 0.6001
: :
Tracer
I Radiometric
ACT(dpm) Tracer (pCi)
i 11.0316 I I
11.0298 I
10.8186
10.9278
:
Printed: 313012018 4:58 AM Page 1 of 1
I Radiometric-I SAF SAF
I %Rec I 1* 2*
I
0.00 . ' I i I I
0.00 !
0.00 r-----
0.00 -1 ----
I i i
l
•
I i i
I I
I I
t I _J___--i
-~---· -- ~- - -· 1-· - -- --- ~------·-----i·· -
!
:
I I )
I
:
I
1 I I
- I +-~-, ---,------1 !
r---L----~----------t-------i------
i i ,--7---i
. I
I
·----1= I i i I
I t----I !
I
I I ---
i r-·------------:
I I
----
l I ! !
0116
Eberline Analytical
Oak Ridge Laboratory
Isotope I
So/# Activity
I dpmlg
U-234 I U-8a 32.000/
U-238 I U-8a 31.oool
fraction I
Isotope I So/# I 01 U-232 U-10a
02 U-232 U-10a
03 U-232 U-10a
04 U-232 U-10a
Version 2.0 08/99
Solution Approx Date Addition
3/28/2018 0.550
3/28/2018 0.550
Tracers Activity Solution
dpmlg Date
18.210 3/28/2018
18.210 3/28/2018
18.210 3/28/2018
18.210 3/28/2018
Spike and Tracer Worksheet
Analysis Code Date Technician
UUISO 3/28/2018 8:36 JHARVEY
LCS MS LCSD MSD LCS MS
Volume Volume Volume Volume
Used (g) Used(g) Used(g) Used (g) Known I Error Added I Error
I
pCi I Estimate pCi ! Estimate I
0.5053 I
oool 7.28/ 0.262 0.000 i
0.5053 7.061 0.254 oool 0.000
Balance Printer Tapes
Volume Approx Tracer Used (g) Addition
0.6058 0.6600
0.6057 0.6600
0.5941 0.6600
0.6001 0.6600
Page 1 of 1 Printed: 3/28/2018 8:39 AM
Witness Initials
LCSD -
MSD Known
I Error Added Error
pCi Estimate pCi Estimate
o.ooi 0.000 0.00 0.000
o.ooi 0.000 0.00 0.000
f I
LCS
Matrix Spike
0117
Eberline Analytical Oak Ridge Laboratory
Lab I AMO Environmental Decisions
Fraction Client ID
01 LCS 02 BLANK 03 OU-1-008
04 OU-1-008
Comments
Analysis Code
UUISO
Sample Muffle Data Ratio
Type Post/Pre
LCS MBL DUP DO
Aliquot Worksheet
Rpt Units Lab Deadline
liters 4/12/2018
Dilution Data Aliquot Data
I No of Dils Oil Factor I Ratio Aliquot Net Equiv
1.0000E+OO 1.0000E+OO
1.0000E+OO 1.0000E+OO
5.0000E-01 5.0000E-01
5.0000E-01 5.0000E-01
Technician: ~~.3(&£(
Tech11ician
JHARVEY
MS Aliquot Data
Printed: 3/28/2018 9:23 AM Page 1 of 1
H-3 Solids Only waterAaaea H30~
Aliquot Net Equiv (ml) Aliq
I
I
0118
~-~tlt'Apex-AI p ha™ Sample Description: Spectrum File: Batch Identification:
SPIKE \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002099
1803110A-UU
Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Tracer Certificate: Tracer Quantity: Effective Efficiency:
01 Shelf 2 U iso
Alpha_057 01017326A 57 System Bkgd 211478
<not performed>
l.000E+000 3/30/2018 3/30/2018
170.0
+/- 0.000E+000 liter 6:46:41 AM 1:25:57 PM
minutes 170.0 minutes
0.0110
Counting Efficiency:
U232 UU-l0A 0.606 mL 0.1895 +/-0.1653 +/-1.1468 +/-
0.0029 on 2/16/2018 0.0696
12:37:04 PM
Chem. Recovery Factor:
Control Certificate Name: NatU U-8A
Chem. Recov. of Control: U-238 0.764606 +/- 0.061860
Peak Match Tolerance: 0.150 MeV
Nuclide
U-232 T U-234 U-235 U-238
T =
Energy (MeV)
5.265 4.724 4.387 4.143
Tracer
PEAK AREA REPORT
Net Pk Area
352.66 432.66
27.00 439.66
Pk Area Error%
10.44 9.43
38.41 9.35
Ambient Backgnd
0.34 0.34 0.00 0.34
Reagent Backgnd
0.00E+000 0.00E+000 0.00E+000 0.00E+000
Peak used for Effective Efficiency
NUCLIDE ANALYSIS RESULTS
FWHM (keV)
29.2 28.3 4.5
46.5
Nuclide Id
Conf. Energy (keV)
Activity (pCi/liter )
MDA (pCi/liter
U-232 U-234 U-235 U-238
0.990 0.990 1.000 0.988
5302.50* 4761.50* 4385.50* 4184.40*
4.94E+000 6.06E+000 4.67E-001 6.13E+000
+/- 5.62E-001 +/- 8.95E-001 +/- 1. 87E- 001 +/- 9.03E-001
~ ef1Wrs
6.70E-002 +/- 7.62E-003 6.70E-002 +/- 7.62E-003 1. 04E-001 +/- l.18E-002 6.67E-002 +!- 7.59E-003
0119
60
55
50
45
40
35 V'l -I-' C :::,
8 30
25
20
15
10
5
0 I
3500 4000 4500
ROI Type: 1
0000209988.CNF
i /!
~ I
5000 Energy(kev)
5500
Live Time :10200.000 sec Real Time :10200.000 sec Start: 1:3442.S(keV) Stop : 1024:6481.S(keV) Acq. Start :Fri Mar 30 13:25:57 2018
6000
ROI Type: 3
0120
Channel Data Report 3/30/2018 4:51:44 PM Page 1
******************************************************* ***** s p E C T R A L DAT A R E P O R T ***** *******************************************************
Sample Title: 01
Elapsed Live time: 10200 Elapsed Real Time: 10200
Channell------l-------l-------l-------1-------1-------1-------I-------I 1: 0 0 0 0 0 0 0 0
9 : 0 0 0 0 0 0 0 0
17: 0 0 0 0 0 0 0 0
25: 0 0 0 0 0 0 0 0
33: 0 0 0 0 0 0 0 0
41: 0 0 0 0 0 0 0 0
49: 0 0 0 0 0 0 0 0
57: 0 1 0 0 0 0 0 0
65: 0 0 0 0 0 0 1 0
73: 0 0 0 0 0 0 0 0
81: 0 0 0 0 0 0 0 0
89: 0 0 0 0 0 0 0 0
97: 0 0 0 0 0 0 0 0
105: 0 1 0 0 0 1 0 1
113: 0 0 0 0 0 0 0 0
121: 0 0 0 0 0 1 0 1
129: 0 0 0 1 1 1 0 0
137: 0 0 0 0 1 0 0 0
145: 1 0 0 0 0 0 0 0
153: 0 0 0 0 0 1 0 0
161: 0 0 0 0 0 0 0 1
169: 1 2 0 0 0 0 1 0
177: 0 0 0 0 1 1 0 0
185: 1 1 2 1 2 2 0 1
193: 0 0 1 0 1 1 2 0
201: 0 0 2 2 1 0 3 0
209: 1 1 0 4 4 6 3 5
217: 0 5 6 6 1 4 4 4
225: 3 14 8 9 14 6 8 5
233: 6 16 16 10 9 13 13 10
241: 13 17 10 13 12 14 16 15
249: 13 18 10 11 8 9 10 7
257: 7 2 0 0 0 0 0 0
265: 0 1 0 0 0 0 0 0
273: 0 0 0 0 0 0 1 0
281: 0 0 0 0 0 0 0 0
289: 0 0 1 1 0 1 1 0
297: 0 0 0 0 0 1 0 0
305: 1 1 0 0 0 0 1 0
313: 0 1 1 0 2 1 1 3
321: 1 0 1 0 0 0 1 0
329: 0 0 0 1 1 1 0 0
337: 0 0 0 1 0 1 0 0
345: 0 1 0 0 0 0 0 0
353: 0 0 0 1 2 1 0 0
361: 1 0 0 1 0 0 0 1
0121
Channel Data Report
369: 1 0 0
Sample Title: 01
3/30/2018
0
4:51:44 PM
3 1 1
Page 2
0
Channell------l-------l-------l-------l-------l-------1-------1-------1
377: 0 0 0 0 0 0 3 0
385: 0 1 2 1 2 1 1 1
393: 0 2 1 1 2 1 0 1
401: 3 1 1 2 1 2 2 2
409: 4 4 2 3 1 6 1 3
417: 5 7 7 8 7 9 8 7
425: 8 17 3 12 15 12 12 9
433: 10 13 8 10 12 11 9 21
441: 12 16 20 14 14 12 16 15
44 9: 8 4 8 2 3 0 0 0
457: 0 0 0 0 0 0 0 0
465: 0 0 0 0 0 0 0 0
473: 0 0 1 0 0 0 0 0
481: 0 0 0 0 0 0 0 0
489: 0 0 0 0 0 0 0 0
497: 0 0 0 0 0 0 0 0
505: 0 0 0 0 0 0 0 0
513: 0 0 0 0 0 0 0 0
521: 1 0 0 0 0 0 0 1
52 9: 1 1 0 0 1 0 0 0
537: 1 0 1 1 0 0 0 0
54 5: 0 0 0 0 0 0 0 0
553: 0 1 1 0 0 0 2 0
561: 0 0 1 1 0 1 1 0
56 9: 1 0 0 0 0 1 1 0
577: 1 0 1 2 4 1 0 1
585: 2 0 2 3 2 2 1 2
593: 3 3 7 3 3 3 4 6
601: 7 10 10 6 3 4 5 4
609: 5 8 11 9 5 9 7 12
617: 12 12 8 13 8 14 12 12
625: 6 12 7 8 13 12 7 7
633: 3 4 4 2 2 1 2 0
641: 0 0 0 0 0 0 0 0
64 9: 0 0 0 0 0 0 0 0
657: 0 0 0 0 0 0 0 0
665: 0 0 0 0 0 0 0 0
673: 0 0 0 0 0 0 0 0
681: 0 0 0 0 0 0 0 0
689: 0 0 0 0 0 0 0 0
6 97: 0 0 0 0 0 0 0 0
705: 0 0 0 0 0 0 0 0
713: 0 0 0 0 0 0 0 0
721: 0 0 0 0 0 0 0 0
729: 0 0 0 0 0 0 0 1
737: 0 0 0 0 0 0 0 0
745: 0 0 0 0 0 0 0 0
753: 0 0 0 0 0 0 0 0
761: 0 0 0 0 0 0 0 0
769: 0 0 0 0 0 0 0 0
777: 0 0 0 0 0 0 0 0
785: 0 0 0 0 0 0 0 0
793: 0 1 0 0 0 0 0 0
0122
Channel Data Report 3/30/2018 4:51:44 PM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 01
Channell------l-------l-------l-------l-------1-------1-------1-------I 809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 0 0 0 0 0 0
833: 0 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 0 0
865: 0 0 0 0 0 0 0 0
873: 0 0 0 0 0 0 0 0
881: 0 0 0 0 0 0 0 0
889: 0 0 0 0 0 0 0 0
897: 0 0 0 0 0 0 0 0
905: 0 0 0 0 0 0 0 0
913: 0 0 0 0 0 0 0 0
921: 0 0 0 0 0 0 0 0
929: 0 0 0 0 0 0 0 0
937: 0 0 0 0 0 0 0 0
945: 0 0 0 0 0 0 0 0
953: 0 0 0 0 0 0 0 0
961: 0 0 0 0 0 0 0 0
969: 0 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 0 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0123
_,A Al h TM ~-~~l""\pex- p a Sample Description: Spectrum File: Batch Identification:
BLANK \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002099
1803110A-UU
Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Tracer Certificate: Tracer Quantity: Effective Efficiency:
02 Shelf 2 U iso
Alpha_058 01017326B 58 System Bkgd 211479
<not performed>
l.000E+000 3/30/2018 3/30/2018
+/- 0.000E+000 liter 6:46:41 AM 1:25:58 PM
170.0 minutes 170.0 minutes
U232 UU-l0A 0.606 mL 0.1819 +/- 0.0107
Counting Efficiency: Chem. Recovery Factor:
0.1710 +/- 0.0030 on 2/16/2018 12:37:03 PM
1.0637 +/- 0.0656
Peak Match Tolerance:
Nuclide
U-232 T U-234 U-235 U-238
Energy (MeV)
5.275 4.716 4.431 4 .196
0.150 MeV
PEAK AREA REPORT
Net Pk Area
338.32 -0.68 0.32
-0.02
Pk Area Error%
10.67 304.44 646.93 10615.
Ambient Backgnd
0.68 0.68 0.68 1. 02
Reagent Backgnd
0.00E+000 0.00E+000 0.00E+000 0.00E+000
FWHM (keV)
9.8 0.0 3.0 3.0
T Tracer Peak used for Effective Efficiency
Nuclide
U-232 U-234 U-235 U-238
Id Conf.
0.995 0.986 0.985 0.999
NUCLIDE ANALYSIS RESULTS
Energy (keV)
5302.50* 4761.50* 4385.50* 4184.40*
Activity (pCi/liter )
4.94E+000 +/- 5.72E-001 -9.93E-003 +/- 3.02E-002
5.76E-003 +/- 3.73E-002 -2.91E-004 +/- 3.09E-002
fG 1!o1/~
MDA (pCi/liter
8.24E-002 +/- 9.54E-003 8.24E-002 +/- 9.54E-003 l.02E-001 +/- l.18E-002 9.16E-002 +/- l.06E-002
0124
60
55
50
45
40
35 VI .f.-1 C: :::s 8 30
25
20
15
10
5
0 I
3500 4000
= = ~ ' :::,
ROI Type: 1
4500
0000209989.CNF
5000 Energy ( kev)
5500
Live Time 10200.000 sec Real Time 10200.000 sec Start: 1 3453.S(keV) stop : 1024 6492. 7(kev) Acq. Start Fri Mar 30 13:25:58 2018
6000
ROI Type: 3
0125
Channel Data Report 3/30/2018 4:51:52 PM Page 1
******************************************************* ***** s P E C T R A L DAT A R E P O R T ***** *******************************************************
Sample Title: 02
Elapsed Live time: 10200 Elapsed Real Time: 10200
Channell------l-------l-------l-------l-------1-------1-------1-------I 1: 0 0 0 0 0 0 0 0
9 : 0 0 0 0 0 0 0 0
17: 0 0 0 0 0 0 0 0
25: 0 0 0 0 0 0 0 0
33: 0 0 0 0 0 0 0 0
41: 0 0 0 0 0 0 0 0
49: 0 0 0 0 0 0 0 0
57: 0 0 0 0 0 0 0 1
65: 0 0 0 0 0 0 0 0
73: 0 0 0 0 0 0 0 0
81: 0 0 1 0 0 0 0 0
89: 0 0 0 0 0 0 0 0
97: 0 0 0 0 0 0 0 0
105: 0 0 0 0 0 0 0 0
113: 0 0 0 0 0 0 0 0
121: 0 0 0 0 0 0 0 0
129: 0 0 0 0 0 0 0 0
137: 0 0 0 0 0 0 0 0
145: 0 0 0 0 0 0 1 0
153: 0 0 0 0 0 0 0 0
161: 0 0 0 0 0 0 0 0
169: 0 0 0 0 0 0 0 0
177: 0 0 0 0 0 0 0 0
185: 0 0 0 0 0 0 0 0
193: 0 0 0 0 0 0 0 0
201: 0 0 0 0 0 0 0 0
209: 0 0 0 0 0 0 0 0
217: 0 0 0 0 0 0 0 0
225: 0 0 0 0 0 0 0 0
233: 0 0 0 0 0 0 0 0
241: 0 0 0 0 0 0 0 0
249: 0 0 1 0 0 0 0 0
257: 0 0 0 0 0 0 0 0
265: 0 0 0 0 0 0 0 0
273: 0 0 0 0 0 0 0 0
281: 0 0 0 0 0 0 0 0
289: 0 0 0 0 0 0 0 0
297: 0 0 0 0 0 0 0 0 305: 0 0 0 0 0 0 0 0
313: 0 0 0 0 0 0 0 0 321: 0 0 0 0 0 0 0 0 329: 0 1 0 0 0 0 0 0 337: 0 0 0 0 0 0 0 0 345: 0 0 0 0 0 0 0 0 353: 0 0 0 0 0 0 0 0 361: 0 0 0 0 0 0 0 0
0126
Channel Data Report 3/30/2018 4:51:52 PM Page 2
369: 0 0 0 0 0 0 0 0
Sample Title: 02
Channell------l-------l-------l-------l-------1-------1-------1-------I 377: 0 0 0 0 0 0 0 0
385: 0 0 0 0 0 0 0 0
393: 0 0 0 0 0 0 0 0
401: 0 0 0 0 0 0 0 0
409: 0 0 0 0 0 0 0 0
417: 0 0 0 0 0 0 0 0
425: 0 0 0 0 0 0 0 0
433: 0 0 0 0 0 0 0 0
441: 0 0 0 0 0 0 0 0
449: 0 0 0 0 0 0 0 0
457: 0 0 0 0 0 0 0 0
465: 0 0 0 1 0 0 0 0
473: 0 0 0 0 0 0 0 0
481: 0 0 0 0 0 0 0 0
489: 0 0 0 0 0 0 0 0
497: 0 0 0 0 0 0 0 0
505: 0 0 0 1 0 0 0 0
513: 0 0 0 0 1 0 0 0
521: 0 0 0 0 0 0 0 0
529: 0 0 0 0 0 0 0 0
537: 0 0 0 0 0 1 0 0
545: 0 0 0 0 0 0 0 0
553: 1 0 0 0 0 0 0 0
561: 0 0 0 0 1 0 1 0
569: 0 0 1 1 1 1 0 2
577: 2 0 1 2 2 1 0 0
585: 1 2 2 0 2 2 2 2
593: 4 0 4 5 3 3 4 5
601: 5 7 5 4 5 10 5 10
609: 4 10 8 14 7 6 8 6
617: 10 9 8 7 14 11 9 11
625: 12 7 4 15 13 16 4 8
633: 5 4 3 1 0 0 0 0
641: 0 0 0 0 0 0 0 0
649: 0 0 0 0 0 0 0 0
657: 0 0 1 0 0 0 0 0
665: 0 0 0 0 0 0 0 0
673: 0 0 0 0 0 0 0 0
681: 0 0 0 0 0 0 0 0
689: 0 0 0 0 0 0 0 0
697: 0 0 0 0 0 0 0 0
705: 0 0 0 0 0 0 0 0
713: 0 0 0 1 0 0 0 0
721: 0 0 0 0 0 0 0 0
729: 0 0 0 0 0 0 0 0
737: 0 0 0 0 0 0 0 0
745: 0 0 0 0 0 0 0 0
753: 0 0 0 0 0 0 0 0
761: 0 0 0 0 0 0 0 0
769: 0 0 0 0 0 0 0 0
777: 0 0 0 0 0 0 0 0
785: 0 0 0 0 0 0 0 0
793: 0 0 0 0 0 0 0 0
0127
Channel Data Report 3/30/2018 4:51:52 PM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 02
Channell------l-------1-------1-------1-------I-------I-------I-------I 809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 0 0 0 0 0 0
833: 0 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 0 0
865: 0 0 0 0 0 0 0 0
873: 0 0 0 0 0 0 0 0
881: 0 0 0 0 0 0 0 0
889: 0 0 0 0 0 0 0 0
897: 0 0 0 0 0 0 0 0
905: 0 0 0 0 0 0 0 0
913: 0 0 0 0 0 0 0 0
921: 0 0 0 0 0 0 0 0
929: 0 0 0 0 0 0 0 0
937: 0 0 0 0 0 0 0 0
945: 0 0 0 0 0 0 0 0
953: 0 0 0 1 0 0 0 0
961: 0 0 0 0 0 0 0 0
969: 0 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 0 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0128
cittA Al h TM ~J-\pex- p a Sample Description: Spectrum File: Batch Identification:
OU-1-008 DUP \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002099
1803110A-UU Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Tracer Certificate: Tracer Quantity: Effective Efficiency:
03 Shelf 2 U iso
Alpha_043 04026481A 91088 System Bkgd 211466
<not performed>
5.000E-001 3/19/2018 3/30/2018
+/- 0:000E+000 liter 6:46:41 AM 1:56:21 PM
170.0 minutes 170.0 minutes
U232 UU-l0A 0.594 mL 0.2094 +/- 0.0118
Counting Efficiency: 0.1903 +/- 0.0033 on 2/16/2018 1.1003 +/- 0.0648
9:34:21 AM
Chem. Recovery Factor:
Peak Match Tolerance:
Nuclide
U-232 U-234 U-235 U-238
T
Energy (MeV)
5.252 4. 716 4.372 4 .137
0.150 MeV
PEAK AREA REPORT
Net Pk Area
382.13 46.15
3.66 36.66
Pk Area Error%-
10.06 29.16
107.87 32.55
Ambient Backgnd
1. 87 0.85 0.34 0.34
Reagent Backgnd
0.00E+000 0.00E+000 0.00E+000 0.00E+000
FWHM (keV)
11.5 3.0 3.0 6.0
T = Tracer Peak used for Effective Efficiency
Nuclide
U-232 U-234 U-235 U-238
Id Conf.
0.982 0.985 0.999 0.984
NUCLIDE ANALYSIS RESULTS
Energy (keV)
5302.50* 4761.50* 4385.50* 4184.40*
Activity (pCi/liter )
9.69E+000 +/- l.07E+000 l.17E+000 +/- 3.65E-001 1.14E-001 +/- l.24E-001 9.26E-001 +/- 3.18E-001
4,/('t
MDA (pCi/liter
l.92E-001 +/- 2.12E-002 1. 52E-001 +!- l.67E-002 l.50E-001 +!- l.65E-002 l.21E-001 +!- l.33E-002
0129
0000209990.CNF
Live Time :10200.000 sec
60+ Real Time :10200.000 sec start: 1: 3497 .0(kev) Stop : 1024:6579.9(keV) Acq. Start :Fri Mar 30 13:56:21 2018
L 55
50
45
40
35 VI -I-' C:
8 30
25
20
15
10
5
0 I I I I I I I
3500 4000 4500 5000 5500 6000 6500 Energy(kev)
ROI Type: 1 ROI Type: 3
0130
Channel Data Report 3/30/2018 4:51:59 PM Page 1
******************************************************* ***** s p E C T R A L DAT A R E P O R T ***** *******************************************************
Sample Title: 03
Elapsed Live time: 10200 Elapsed Real Time: 10200
Channell------l-------1-------1-------1-------I-------I-------I-------I 1: 0 0 0 0 0 0 0 0
9 : 0 0 0 0 0 0 1 0
17: 0 0 0 0 0 0 0 0
25: 0 0 0 0 0 0 0 0
33: 0 0 0 0 1 0 0 0
41: 0 0 0 0 0 0 0 0
49: 0 0 0 0 0 0 0 0
57: 0 1 0 0 0 0 0 0
65: 0 0 0 0 0 0 0 0
73: 0 0 0 0 0 0 0 1
81: 0 0 0 0 0 0 0 0
89: 0 0 0 0 0 0 0 0
97: 0 0 0 0 0 0 0 0
105: 0 0 0 0 0 0 0 0
113: 0 0 0 0 0 0 0 0
121: 0 0 0 0 0 0 0 0
129: 0 0 0 0 0 0 0 0
137: 0 0 0 0 0 0 0 0
145: 0 0 0 0 2 0 0 0
153: 0 1 0 0 0 0 0 0
161: 0 0 0 0 0 0 0 0
169: 0 0 0 0 0 0 0 0
177: 0 1 0 1 0 0 0 1
185: 0 1 0 0 1 0 0 0
193: 0 0 0 0 0 0 0 0
201: 0 0 2 3 1 1 2 2
209: 1 0 0 0 0 1 0 0
217: 1 1 2 2 3 1 1 0
225: 0 0 1 0 1 1 0 0
233: 1 0 0 2 0 0 0 0
241: 1 0 1 0 0 0 0 0
249: 0 0 0 0 0 0 0 0
257: 0 0 0 0 1 0 0 0
265: 0 0 0 0 0 0 0 0
273: 0 0 0 0 0 0 1 0
281: 0 0 0 0 0 0 1 0
289: 0 0 0 0 0 0 0 1
297: 0 0 0 0 0 0 1 0
305: 0 0 0 0 0 0 0 0
313: 0 0 0 0 0 0 0 0
321: 0 0 0 0 0 0 0 0
329: 0 0 0 0 0 0 0 0
337: 1 1 0 0 0 0 0 0
345: 0 0 0 1 0 0 0 0
353: 0 0 0 0 0 0 0 0
361: 0 0 0 0 0 0 0 0
0131
Channel Data Report 3/30/2018 4:51:59 PM Page 2
369: 0 0 0 0 0 2 0 0
Sample Title: 03
Channell------l-------l-------l-------l-------1-------1-------1-------I 377: 0 0 0 1 0 0 1 0
385: 0 0 2 0 1 0 0 0
393: 1 1 1 0 1 1 1 0
401: 0 4 0 1 2 3 0 3
409: 1 1 2 0 2 3 1 1
417: 2 2 2 1 0 0 0 1
425: 0 1 0 1 0 0 0 0
433: 0 0 0 0 0 0 0 0
441: 0 0 0 0 0 0 0 0
449: 0 1 0 0 0 0 0 0
457: 0 0 0 0 0 0 0 0
465: 0 0 0 0 1 0 0 0
473: 0 0 0 0 0 0 0 0
481: 0 0 0 0 0 0 0 0
489: 1 0 0 0 0 0 0 0
497: 0 0 0 1 0 0 0 0
505: 1 0 0 0 0 0 0 0
513: 0 0 0 0 0 1 0 1
521: 0 0 0 0 0 0 0 0
529: 0 0 0 0 0 1 1 1
537: 0 0 1 1 1 0 0 0
545: 1 1 1 0 0 3 0 2
553: 3 3 0 0 0 1 2 2
561: 4 3 7 9 4 4 6 4
569: 2 9 8 8 7 2 12 9
577: 6 11 6 15 12 13 5 10
585: 10 11 5 10 12 9 18 13
593: 18 7 11 8 10 5 12 10
601: 8 3 3 5 0 1 1 1
609: 0 0 0 0 0 1 0 0
617: 0 0 0 0 0 0 0 0
625: 0 0 0 0 0 0 0 0
633: 1 0 0 0 0 0 0 0
641: 0 0 0 0 0 0 0 0
649: 0 0 0 0 0 0 0 0
657: 0 0 0 0 0 0 0 0
665: 0 0 0 0 0 0 0 0
673: 0 0 0 0 0 0 0 0
681: 0 0 0 0 0 0 0 0
689: 0 0 0 0 0 0 0 0
697: 0 0 0 0 0 0 0 0
705: 0 0 0 0 0 0 0 0
713: 1 0 0 0 0 0 0 0
721: 0 0 0 0 0 0 1 0
729: 0 0 0 0 0 0 0 0
737: 0 0 0 0 0 0 0 0
745: 0 0 0 0 0 0 0 0
753: 0 0 0 0 0 0 0 0
761: 0 0 0 0 0 0 0 0
769: 0 0 0 0 0 0 0 0
777: 0 0 0 0 0 0 0 0
785: 0 0 0 0 0 0 0 0
793: 0 0 0 0 0 0 0 0
0132
Channel Data Report 3/30/2018 4:51:59 PM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 03
Channell------l-------l-------1-------1-------1-------I-------I-------I 809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 1 0 0 0 0 0
833: 0 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 0 0
865: 0 0 0 0 0 0 0 0
873: 0 0 0 0 0 0 0 0
881: 0 0 0 0 0 0 0 0
889: 0 0 0 0 0 0 0 0
897: 0 0 0 0 0 0 0 0
905: 0 0 0 0 0 0 0 0
913: 0 0 0 0 0 0 0 0
921: 0 0 0 0 0 0 0 0
929: 0 0 0 0 0 0 0 0
937: 0 0 0 0 0 0 0 0
945: 0 0 0 0 0 0 0 0
953: 0 0 0 0 0 0 0 0
961: 0 0 0 0 0 0 0 0
969: 0 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 0 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0133
~Apex-Alpha™ Sample Description: Spectrum File: Batch Identification:
OU-1-008 \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002099 1803110A-UU
Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Tracer Certificate: Tracer Quantity: Effective Efficiency:
04 Shelf 2 u iso
Alpha_044 04026481B 84168 System Bkgd 211467
<not performed>
5.000E-001 3/19/2018 3/30/2018
+/- 0.000E+000 liter 6:46:41 AM 1:56:22 PM
170.0 minutes 170.0 minutes
U232 UU-l0A 0.600 mL 0.1885 +/- 0.0110
Counting Efficiency: 0.1840 +/- 0.0032 on 2/16/2018 1.0243 +/- 0.0625
9:34:19 AM
Chem. Recovery Factor:
Peak Match Tolerance:
Nuclide
U-232 T U-234 U-235 U-238
Energy (MeV)
5.261 4.705 4.435 4 .142
0.150 MeV
PEAK AREA REPORT
Net Pk Area
347.49 37.49
2.83 37.00
Pk Area Error%
10.52 32.26
120.53 32.65
Ambient Backgnd
0.51 0.51 0.17 0.00
Reagent Backgnd
0.00E+000 0.00E+000 0.00E+000 0.00E+000
FWHM (keV)
39.3 4.4 3.0 4.5
T = Tracer Peak used for Effective Efficiency
Nuclide
U-232 U-234 U-235 U-238
Id Conf.
0.988 0.978 0.983 0.987
NUCLIDE ANALYSIS RESULTS
Energy (keV)
5302.50* 4761.50* 4385.50* 4184.40*
Activity (pCi/liter )
9.79E+000 +!- l.12E+000 l.06E+000 +!- 3.62E-001 9.83E-002 +!- l.19E-001 l.04E+000 +!- 3.59E-001
ftj 1-(~rt
MDA (pCi/liter
l.48E-001 +!- l.69E-002 1. 48E-001 +!- 1. 69E-002 1. 45E-001 +!- l.66E-002 l.68E-001 +/- l.93E-002
0134
60
55
50
45
40
35 V> ,j-1 C: :::3
8 30
25
20
15
10
5 00
0 [I 1 ~! I I! I I I jd!' I'' 3 500 -~1Jc1 I :,\\f ::J.:i'Yulrh]j]ll[
1
(!( _..1,__J'Li....1-W..J.JJ1 I\ I ,1 ' . ' ,, I, I ! 111,
4000 4500
ROI Type: 1
0000209991.CNF
- ....,;,.,..:''_;LI Li _tLI!' IL ~11ullln___1 \ lo! Mlj!IU (m/V,111 I 1• 1
5000 Energy(kev)
Live Time :10200.000 sec Real Time :10200.000 sec Start: 1:3463.G(keV) Stop : 1024:6522.9(kev) Acq. Start :Fri Mar 30 13:56:22 2018
I n i i I I n I j 1 I I I I I
5500 6000 6500
ROI Type: 3
0135
Channel Data Report 3/30/2018 4:52:06 PM Page 1
******************************************************* ***** s p E C T R A L DAT A R E P O R T ***** *******************************************************
Sample Title: 04
Elapsed Live time: 10200 Elapsed Real Time: 10200
Channell------l-------l-------l-------l-------1-------1-------1-------I 1: 0 0 0 0 0 0 0 0
9 : 0 0 0 0 0 0 0 0
17: 0 0 0 0 0 0 0 0
25: 0 0 0 0 0 0 0 0
33: 0 0 0 0 0 0 0 0
41: 0 0 0 0 0 0 0 0
49: 0 0 0 0 0 0 0 0
57: 0 0 0 0 0 0 0 0
65: 0 0 0 0 0 0 0 0
73: 0 0 0 0 0 0 0 0
81: 0 0 0 0 0 0 0 0
89: 0 0 0 0 0 0 0 0
97: 0 0 0 0 0 0 0 0
105: 0 0 0 0 0 0 0 0
113: 0 0 0 0 0 0 1 0
121: 0 0 0 0 0 0 0 0
129: 0 0 0 0 0 0 0 0
137: 0 0 0 0 0 0 0 0
145: 0 0 0 0 0 0 0 0
153: 0 0 0 0 0 0 0 0
161: 0 0 0 0 0 0 0 0
169: 0 0 1 0 0 1 0 0
177: 0 0 0 0 0 0 0 0
185: 0 0 0 0 0 0 0 0
193: 0 0 0 1 0 0 0 0
201: 0 0 0 0 0 0 1 0
209: 0 2 0 0 0 0 2 1
217: 1 1 0 0 1 1 1 3
225: 1 1 0 2 1 1 0 2
233: 3 0 0 0 1 0 2 0
241: 2 2 0 1 2 0 0 1
249: 0 0 0 0 0 0 0 0
257: 0 0 0 0 0 0 0 0
265: 0 0 0 0 0 0 0 0
273: 0 0 0 0 0 0 0 0
281: 0 0 0 0 0 0 0 0
289: 0 0 0 0 0 0 0 0
297: 0 0 0 0 0 0 0 0
305: 0 0 0 0 1 0 0 0
313: 0 0 0 0 0 0 0 0
321: 0 0 0 0 0 0 0 0
329: 1 0 0 0 0 0 0 0
337: 0 0 1 0 0 0 0 0
345: 0 0 0 0 0 0 0 0
353: 0 0 0 0 0 0 0 0
361: 0 1 0 0 0 0 0 0
0136
Channel Data Report 3/30/2018 4:52:06 PM Page 2
369: 0 0 0 1 0 0 0 1
Sample Title: 04
Channell------l-------l-------1-------1-------1-------I-------I-------I 377: 0 0 0 0 0 0 0 0
385: 1 0 0 0 0 0 0 1
393: 1 1 1 0 0 0 0 1
401: 0 1 0 1 0 0 2 1
409: 0 1 0 0 1 2 2 5
417: 1 0 0 1 0 0 0 0
425: 0 1 1 2 2 1 2 0
433: 1 2 2 0 0 0 0 0
441: 0 0 0 0 0 0 0 0
449: 0 0 0 0 0 0 0 0
457: 0 0 0 0 0 1 0 0
465: 0 0 0 0 0 0 0 0
473: 0 0 0 0 0 0 0 0
481: 0 0 0 0 1 0 0 0
489: 0 0 0 0 1 0 0 1
497: 0 0 0 0 0 0 0 0
505: 0 1 0 0 2 1 0 0
513: 0 0 0 0 0 1 0 0
521: 0 0 0 0 0 1 1 1
529: 1 0 1 0 0 0 0 0
537: 2 0 1 0 0 0 0 0
545: 0 0 0 1 1 1 3 0
553: 2 0 1 0 0 0 0 2
561: 1 1 0 1 0 2 0 2
569: 2 1 6 3 2 0 1 2
577: 1 2 3 1 5 2 2 2
585: 4 5 3 3 5 6 9 8
593: 4 10 11 11 7 5 12 6
601: 8 4 8 6 7 11 10 11
609: 8 8 15 8 13 14 13 11
617: 8 8 6 8 3 5 2 2
625: 1 0 1 0 0 0 0 0
633: 0 0 0 0 0 0 0 0
641: 0 0 0 0 0 0 0 0
649: 0 0 0 0 0 0 0 0
657: 0 0 0 0 0 0 0 0
665: 0 0 0 0 0 0 0 0
673: 0 0 0 0 0 0 0 0
681: 0 0 0 0 0 0 0 0
689: 0 0 0 0 0 0 0 0
697: 0 0 0 0 0 0 0 0
705: 0 0 0 1 1 0 0 0
713: 0 0 0 0 0 0 0 0
721: 0 0 0 0 0 0 0 0
729: 0 0 0 0 0 0 0 0
737: 0 0 0 0 0 0 0 0
745: 0 0 0 0 0 0 0 0
753: 0 0 0 0 0 0 0 0
761: 0 0 0 0 0 0 0 0
769: 0 0 0 0 0 0 0 0
777: 0 0 0 0 0 0 0 0
785: 0 0 0 0 0 0 0 0
793: 0 0 0 0 0 0 0 0
0137
Channel Data Report 3/30/2018 4:52:06 PM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 04
Channell------l-------l-------l-------l-------1-------1-------1-------I 809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 0 0 0 0 0 0
833: 0 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 0 0
865: 0 0 0 0 0 0 0 0
873: 0 0 0 0 0 0 0 0
881: 0 0 0 0 0 0 0 0
889: 0 0 0 0 0 0 0 0
897: 0 0 0 0 0 0 0 0
905: 0 0 0 0 0 0 0 0
913: 0 0 0 0 0 0 0 0
921: 0 0 0 0 0 0 0 0
929: 0 0 0 0 0 0 0 0
937: 0 0 0 0 0 0 0 0
945: 0 0 0 0 0 0 0 0
953: 0 0 0 0 0 0 0 0
961: 0 0 0 0 0 0 0 0
969: 0 0 0 1 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 0 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0138
!"'age I m L. 3/30/2018 5:55:22 AM
ex-Al OA .c::;111\AMARY REPORT
... ~ u • ~ ,, .... ,, "-. ~ - - •• -- -- - -
Review Of QA Results - Pulser Check
Date : 3/30/2018 Time : 5:55:22 AM
CHAMBER DEVICE PARAMETER FLAG DATE
Alpha 001 21f ALL Not Done
Alpha 002 21f ALL Not Done
Alpha 003 21f ALL Passed 3/30/2018 5:03:13 AM
Alpha 004 21f ALL Passed 3/30/2018 5:03:14 AM
Alpha 005 21f ALL Not Done
Alpha 006 21f ALL Not Done
Alpha 007 21f ALL Not Done
Alpha 008 21f ALL Not Done
Alpha 009 2lf ALL Not Done
Alpha 010 21f ALL Passed 3/30/2018 5:03:15 AM
Alpha 011 21f ALL Passed 3/30/2018 5:03:16 AM
Alpha 012 21f ALL Passed 3/30/2018 5:03:17 AM
Alpha 013 21f ALL Not Done
Alpha 014 21f ALL Passed 3/30/2018 5:03:18 AM
Alpha 015 2lf ALL Not Done
Alpha 016 21f ALL Not Done
Alpha 033 Alpha Analystl 00DC ALL Passed 3/30/2018 5:03:19 AM
Alpha 034 Alpha Analystl 00DC ALL Passed 3/30/2018 5:03:21 AM
Alpha 035 Alpha Analystl00DC ALL Passed 3/30/2018 5:03:22 AM
Alpha 036 Alpha Analystl00DC ALL Passed 3/30/2018 5:03:24 AM
Alpha 037 Alpha Analystl 00DC ALL Not Done
Alpha 038 Alpha Analystl00DC ALL Passed 3/30/2018 5:03:26 AM
Alpha 039 Alpha Analystl00DC ALL Not Done
Alpha 040 Alpha Analyst! 00DC ALL Passed 3/30/2018 5:03:28 AM
Alpha 041 Alpha Analyst! 00DC ALL Passed 3/30/2018 5:03:30 AM
Alpha 042 Alpha Analyst 1 00DC ALL Passed 3/30/2018 5:03:32 AM
Alpha 043 Alpha Analystl00DC ALL Passed 3/30/2018 5:03:34 AM
Alpha 044 Alpha Analystl00DC ALL Passed 3/30/2018 5:03:37 AM
Alpha 045 Alpha Analystl00DC ALL Passed 3/30/2018 5:03:39 AM
Alpha 046 Alpha Analystl00DC ALL Passed 3/30/2018 5:03:42 AM
Alpha 047 Alpha Analystl00DC ALL Not Done
Alpha 048 Alpha Analyst 1 00DC ALL Not Done
Alpha 049 Alpha Analyst! 00DC ALL Passed 3/30/2018 5:03:44 AM
Alpha 050 Alpha Analystl00DC ALL Passed 3/30/2018 5:03:47 AM
Alpha 051 Alpha Analystl00DC ALL Passed 3/30/2018 5:03:49 AM
Alpha 052 Alpha Analystl00DC ALL Passed 3/30/2018 5:03:52 AM
Alpha 053 Alpha Analyst 1 00DC ALL Passed 3/30/2018 5:03:54 AM
Alpha 054 Alpha Analyst 1 00DC ALL Passed 3/30/2018 5:03:57 AM
Alpha 055 Alpha Analystl00DC ALL Passed 3/30/2018 5:03:59 AM
Alpha 056 Alpha Analystl00DC ALL Passed 3/30/2018 5:04:02 AM
Alpha 057 Alpha Analystl00DC ALL Passed 3/30/2018 5:04:05 AM
Alpha 058 Alpha Analyst 1 00DC ALL Passed 3/30/2018 5:04:08 AM
0139
Page 2 of 2 Kev1ew ot UA Kesu1ts - t-'Ulser L;necK 3/30/2018 5:55:22 AM
CHAMBER DEVICE PARAMETER FLAG DATE
Alpha 059 Alpha Analystl00DC ALL Not Done
Alpha 060 Alpha Analystl00DC ALL Not Done
APPROVED BY:
APPROVAL DATE: <-S /3()/[ 8
0140
Library Listing Report 6/12/12 12:17:04 PM Page 1
*************************************************************************
***** L I B R A R Y L I S T I N G R E P O R T *****
*************************************************************************
Nuclide Library Title: Uranium
Nuclide Library Description: U-232,-234,-235,-238
Nuclide Half-Life Energy Energy Yield Yield
Name (Seconds) (keV ) Uncert. (keV ( % ) Uncert. (Abs.+-)
U-232 2.174E+009 5302.500* 0.000 99.8000 0.0000
U-234 7.731E+Ol2 4761.500* 0.000 99.8000 0.0000
U-235 2.221E+Ol6 4385,500* 0.000 80.9000 0.0000
U-238 1. 410E+Ol 7 4184.400* 0.000 100.2300 0.0000
* == key line
TOTALS: 4 Nuclides 4 Energy Lines
0141
SECTION IX
ANALYTICAL DATA (TOTAL URANIUM)
0142
Eberline Services Oak Ridge Laboratory Analysis Sheet
Work Order
Analysis Code
Run
Date Received
Lab Deadline
18-03110
KPA_LIQ I
1 3/23/2018
4/12/2018
Client I AMO Environmental Decisions
Project WESTLAKE
Report Level 4
Activity Units ug
Aliquot Units
Matrix WA
Method ASTM D5174 Modified
Instrument Type KPA
Radiometric Tracer
Radiometric Sol#
Tracer Act (dprn/g)
Carrier
Carrier Cone (mg/ml)
Internal Sample I Fraction Desc I
01 LCS
02 MBL
03 DUP
04 DO
I
j
18-03110 KPA_LIQ
Run 1
Client ID
LCS
BLANK
OU-1-008
OU-1-008
--·~---. ..
* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. A Indicates estimated SAF value.
** Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
I
Login CPM
I
I '
I 38 i !
38
I
:
I I I
I
I I i I
I
I
i I I
I
I I
I
I I
Printed: 4/12/2018 1 :10 PM Page 1 of 3
Sample I Sample
Date I
Aliquot
03/23/18 00:00 1.0000E+00
03/23/18 00:00 1.0000E+00
03/19/18 18:02 1.0000E+00
03/19/18 18:02 I 1.0000E+00
I
'
I
I
I
I
i
! !
i
!
i
0143
Eberline Services
Oak Ridge Laboratory
Analysis Sheet
Internal Sample Tracer
Fraction Desc Aliquot(g)
01 LCS
02 MBL
03 DUP
04 DO
i
Tracer Total ACT(dpm)
I
I
I
Radiometric Radiometric
Tracer (pCi) %Rec
0.00
0.00
0.00
0.00
I I I i !
I
i I i I
I
18-03110 KPA_LIQ
Run 1
Grav Carrier Grav Filter
Added(ml) Tare (g)
I I
I
I I
Grav Filter Final (g)
I
• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. A Indicates estimated SAF value.
•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Grav Filter Grav Net(g) %Rec
I
I I I I I I
Printed: 4112120181:10 PM Page 2 of 3
Mean SAF SAF %Rec 1* 2*
0144
Eberline Services Oak Ridge Laboratory Analysis Sheet
Internal Sample Fraction Desc
01 LCS
02 MBL
03 DUP
04 DO
Rough Prep Date
Rough Prep Prep
By Date
i
' I I I
i
I I
l
I
I
I i
I
18-03110 KPA_LIQ
Run 1
Prep By
I
Sep to Date/Time
-~·
* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. h Indicates estimated SAF value.
** Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Sep to By
I i
I I
'
\
Printed: 4/12/20181:10 PM Page 3 of 3
Sep t1 Sep t1
Date/Time By
'
I
0145
Eberline Services Oak Ridge Laboratory
~ Lab
Nuclide Fraction
01 TOTAL U
i:: :::i ct:
.g 0
(.)
,!!: ~
<U i:: <t
it (.)
""""'
a -..J I
<C Q. ~
ti)
·u <1' 0 co -C: <1' E C: 0 ... ·s; C: w 0 :i!: <
OH TOTAL U
02 TOTAL U
03 TOTAL U
04 TOTAL U
I
Sample Oesc
LCS
LCSH
MBL
DUP
DO
'1
i I
···---
Preliminary Data Report & Analytical Calculations
Work Order: 18-03110-KPA_LIQ-1
Client
I Activity
Results I Error Estimate[ MDA I LCS
I Identification Units Known
I 8.00E+ool LCS ug/1 8.65E+00 1.88E-01 1.01E+00
LCS-H ug/1 1.96E+02 3.99E+00 1.01E+00 2.00E+02
BLANK ug/1 0.00E+00 0.00E+00 1.01E+00 I !
OU-1-008 ug/1 4.12E+00 9.50E-02 1.01E+00 I OU-1-008 ug/1 4.23E+00 9.91E-02 1.01E+00
I I
I I
I I
I I i l
I I I
i I
I i I I
I I
I I
! I
-----
I I I
I I I I
LCS
I %R
108.14
98.04
I
I
I
i I
I I i
I
I I
Printed: 4/12/20181:12 PM Page 1 of 3
LCS RPO
I MDA I Blank
Flag Flag Flag I Flag
OK I OK i
OK OK
OK OK
NA OK
OK
i i I
I
I I
I
I I
0146
Eberline Services Oak Ridge Laboratory
( Lab I Nuclide Fraction
01 TOTAL U
i:: ::i ll:
G> ,:, 0
(.J
-~ ~ iu i:: q:
11 u
"""'"
0 -.J <Cl a. ~
en C: 0 en
·c:3 Cl)
C
B C: Cl)
E C: 0 I-
> C: w 0 ~ <
OH TOTAL U
02 TOTAL U
03 TOTAL U
04 TOTAL U
I I
Sample Desc
LCS
LCSH
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03110-KPA_LIQ-1
Sample Sample Radiometric Grav Mean
I SAF Date Aliquot %Rec %Rec %Rec
I
03/23/18 00:00 1.00E+00 0.00 0.00 98.691
03/23/18 00:00 1.00E+00 0.00 0.00 98.691 I
03/23/18 00:00 1.00E+00 0.00 0.00 98.69
I
03/19/18 18:02 1.00E+00 0.00 0.00 98.69
03/19/18 18:02 1.00E+00 0.00 0.00 98.69
I I I
I
I I
I !
I I I I I
I I I
I I I I !
i i
I I
I I
I I ·-~----I
i I
I I
I
SeptO
Printed: 4/12/2018 1:12 PM Page 2 of 3
Sept1
Date/Time Date/Time
I
I
I
I i
I I
I
I
I
I
I
I
0147
.!!1 ~ Ill C: ct
II
Eberline Services Oak Ridge Laboratory
Lab I Fraction
Nuclide
01 TOTAL U
OH TOTAL U
"""" 02 TOTAL U
a 03 TOTAL U
-..J <Cl
04 TOTAL U
a. ~
1/) s:: 0
-~ (.) Cl)
0
.!9 s:: Cl)
E s:: 0 ... > s:: w 0 ::l!:: <(
Sample Desc
LCS
LCSH
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03110-KPA_LIQ-1
Counting Halflife
I Detect Carrier
Count Counts
Date/Time {days) Time
03/27/18 09:51
03/27/18 09:53
03/27/18 09:55 I
03/27/18 10:01
03/27/18 09:57
I
I
I I
I I I
I Bkg CPM
I
I
I
I
I I
I
!
i
I I
Printed: 4/12/20181:12 PM Page 3 of 3
Eff
0148
Count Room Report
Client: AMO Environmental Decisio
Internal Sample Client
Fraction Desc ID
01 LCS LCS
02 MBL BLANK
03 DUP OU-1-008
04 DO OU-1-008
i
!
I
-- -
I
···-
I !
i I
18-03110-KPA_LIQ-1 (ug/1) in WA
Tracer ID:
I I
Sample Sample Tracer
Date I Aliquot Aliquot (g)
03/23/18 00:00 1.0000
I
I 03123118 00:00 I 1.0000 I
03/19/18 18:02 \ 1.0000
03/19/18 18:02 t 1.0000
I I
I
I I
I
I I
I i
I I
I
i I
I I
I I I
I I
I !
I ! I
Tracer ACT(dpm)
I Radiometric Tracer (pC1)
I I
I
I !
Printed: 4/12/2018 1:10 PM Page 1 of 1
I Radiometric SAF SAF
%Rec 1* 2*
0.00
0.00 1
o.oo I
0.00
I
I I
I I
I
I I
I --I I !
I
0149
Eberline Services Oak Ridge Laboratory
Recovery Spike Cone. '
Isotope I Sol# I '
nglml
TOTAL U U-9-3 I 10
'
LCS Low Range
Isotope !
Sol# Cone.
I I nglml
TOTAL U LCS-L i sl
Solution Date
1/7/2004
Solution Date
1/7/2004
LCS High Range
I I Cone. I Solution
Isotope Sol# I
I ng/ml i Date
TOTAL U LSC-H I 2001 1/7/2004
Matrix Spikes
Sol# Cone. Solution
Isotope ng/ml Date
TOTAL U U-9-5 • 100 1 1/7/2004
Version 2.5 01/05
Dilution factor
1.000
I Dilution
' factor
1.000 '
1 Dilution factor
1.000
Dilution factor
0.500
KPA Spike Worksheet Page 1 of 1
Printed: 4/12/2018 1:09 PM
Analysis Code Date Technician
KPA_LIQ 4/12/2018 13:09 JPACHELLA
Current Sample Type Evaluation 1~hnicia9_:jnitials
Volume Theoretical LIQUID ~j/' Used (g) Yield ,,
1.0000 10.0000 Witness Initials
LCS LCSD LCS LCSD
Volume Volume Known I Error Known Error
Used(g) Used(g) ng Estimate ng I Estimate
' I 1.0000 8.0000 0.1600 i
LCSH LCSDH LCSH LCSDH
Volume Volume Known Error Known I Error
Used (g) Used (g) ng Estimate ng i Estimate I
I 1.0000 200.0000· 4.0000 I
MSD MS MSD
Volume Volume Added I
Error Added I Error
Used (g) Used (g) ng I Estimate ng Estimate
I
0150
Lab
Eberline Analytical Oak Ridge Laboratory
AMO Environmental Decisions
Analysis Code
KPA_LIQ
Sample Muffle Data
Fraction Ratio
Client ID Type Post/Pre
01 LCS LCS
02 BLANK MBL
03 OU-1-008 DUP
04 OU-1-008 DO
Comments
0 )../~ ;J lilt
Technician: . t,1-t:(~L y
Aliquot Worksheet
Rpt \Jolts lab Dead!lne
liters 4/12/2018
Dilution Data Aliquot Data
Noof Dils Dil Factor Ratio Aliquot Net Equiv
1.0000E+00 1.0000E+00
i 1.0000E+00 1.0000E+00
! 1.0000E+00 1.0000E+00
: 1.0000E+00 1.0000E+00 '"·--··
/
'
: -·
~~·-
---·----·------
-
Date: ±_, ~ ; J 7f
Technician
JPACHELLA
MS Aliquot Data
Printed: 4/12/2018 1 :08 PM Page 1 of 1
H-3 Solids Only Water Added H3 Dist
Aliquot Net Equiv (ml) Aliq
---
I
---·· ·-·
0151
KPAWin© Single Sample Report - Sample
Customer ID: Sample ID: Description: Batch ID:
Configuration
Sample Unit: Performance: QC Limits:
None 1803110-00
RECOVERY SPIKE 5826
µg/1 1003 Config
1000 Release
Sample Preparation & Analysis
Procedure ID: Range: Calibration ID: Equation: Specific Gravity:
None Low
Default Y= +249.459X +68.687
1
Range Sample Results
Reference Lifetime: LSR Time Gates: Sample Lifetime (µsec): Sample R 2 Intensity: Reference Ratio: Sample Intercept: Analytical Result: Dilution Factor: Aliquot Factor: Final Result: Uncertainty:
Interpreted Results
Detection Limit(IDL): Detection Limit(MDL):
(Low)
1803110-00
5 211
- 49 375
.998 1.031
2531 9.869 1.00 1.00
9.869 .208
N/A N/A
Min Significant Sample Limit: 3.00E-01
Date Analyzed: Analyte: Analyst: Date Printed:
KPA Unit Calibration: Alarms:
03/27/2018 09:49 AM Uranium
JPachella 03/27/2018 09:51 AM
1001 Config 1000 Release
1003 Config
Specific Activity (Bq/g): 25000
Flags
IDL Flags: MDL Flags: Calibration: Sample:
0152
I n t e n s i t y
Net Intensities
Low: 1803110-00 3/27/2018 9:49:42 AM
10000
1000
' "-, '
100
10
1 --l----------+--------+---------1---------+--------1-------------a----'-
0 20 40 60 80 100 120
Time Gate
o Sample 0 Ref
0153
Lab: No Lab Date: 3/27/2018 9:49:42 AM
Net Intensities
Low: 1803110-00 Sample Intensities 0 1 2 3 4 5 6 7 8 9
0 2496 2314 2432 2217 2158 2087 2016 1949 1876
10 1840 1769 1706 1625 1580 1500 1430 1373 1344 1273
20 1233 1222 1170 1133 1101 1051 996 978 938 915
30 891 863 824 791 761 736 716 696 682 658
40 636 601 586 563 554 542 536 514 492 471
50 454 437 416 400 376 359 348 340 336 332
60 325 308 304 281 274 265 270 254 254 242
70 236 221 212 207 203 198 188 180 168 163
80 154 154 155 155 150 145 133 130 120 113
90 110 108 104 106 104 100 98 95 89 84
100 83 78 75 78 75 72 70 69 65 62
110 64 69 66 65 64 60 58 60 57 53
120 51 47 40 42 42 39 36 24
Low: 1803110-00 Reference Intensities 0 1 2 3 4 5 6 7 8 9
0 4095 1300 1056 1043 939 864 799 742 681
10 631 589 538 501 464 434 402 377 345 322
20 300 279 256 235 223 206 194 185 174 170
30 161 151 143 133 116 113 112 107 103 100
40 94 87 83 80 81 74 71 70 67 62
50 63 61 53 51 48 44 40 42 41 38
60 37 35 35 33 32 34 34 33 31 31
70 31 29 26 25 25 22 24 24 22 20
80 20 17 18 17 16 16 14 13 15 14
90 13 14 13 11 10 11 9 8 9 9
100 8 8 8 7 8 8 7 7 7 5
110 4 4 3 2 2 2 2 3 3 3
120 3 3 4 4 3 2 1 3
0154
KPAWin© Single Sample Report - Sample
Customer ID: Sample ID: Description: Batch ID:
Configuration
Sample Unit: Performance: QC Limits:
None 1803110-01
LCS LOW 5826
µg/1 1003 Config
1000 Release
Sample Preparation & Analysis
Procedure ID: Range: Calibration ID: Equation: Specific Gravity:
None Low
Default Y= +249.459X +68.687
1
Range Sample Results
Reference Lifetime: LSR Time Gates: Sample Lifetime (µsec): Sample R 2 Intensity: Reference Ratio: Sample Intercept: Analytical Result: Dilution Factor: Aliquot Factor: Final Result: Uncertainty:
Interpreted Results
Detection Limit(IDL): Detection Limit(MDL):
(Low)
1803110-01
5 213
- 49 335
.998 1.009
2199 8.538 1.00 1. 00
8.538 .186
N/A N/A
Min Significant Sample Limit: 3.00E-01
Date Analyzed: Analyte: Analyst: Date Printed:
KPA Unit Calibration: Alarms:
03/27/2018 09:51 AM Uranium
JPachella 03/27/2018 09:52 AM
1001 Config 1000 Release
1003 Config
Specific Activity (Bq/g): 25000
Flags
IDL Flags: MDL Flags: Calibration: Sample:
0155
I n t e n s i t y
Net Intensities
Low: 1803110-01 3/27/2018 9:51:33 AM
100000
10000
1000
100
10
1 +-------i------/--------+----------------1------/------+---.J
0 20 40 60 80 100 120
Time Gate
o Sample 0 Ref
0156
Lab: No Lab Date: 3/27/2018 9:51:33 AM
Net Intensities
Low: 1803110-01 Sample Intensities 0 1 2 3 4 5 6 7 8 9
0 4047 2129 2016 1913 1957 1676 1699 1612 1568
10 1516 1442 1392 1325 1274 1225 1189 1144 1102 1047
20 1007 969 923 899 868 829 786 762 725 701
30 678 662 626 600 583 566 543 524 501 477
40 451 429 417 410 398 391 382 374 361 342
50 325 312 297 279 265 252 240 230 225 226
60 219 215 203 192 184 173 164 161 154 152
70 148 142 139 140 129 128 121 118 114 111
80 108 105 96 93 90 84 79 84 75 73
90 71 70 66 67 64 62 61 58 54 52
100 52 49 50 50 48 47 44 41 39 39
110 38 39 36 36 33 31 28 28 25 25
120 25 26 23 25 23 22 17 16
Low: 1803110-01 Reference Intensities 0 1 2 3 4 5 6 7 8 9
0 4044 1300 1146 999 871 841 768 715 667
10 613 578 538 501 457 426 391 362 337 312
20 293 269 246 231 220 207 203 197 189 179
30 168 154 145 135 130 121 113 108 105 97
40 96 91 86 78 74 69 68 66 65 62
50 60 59 55 54 50 46 42 43 40 41
60 41 40 39 34 34 33 33 32 31 28
70 27 26 24 26 26 25 24 20 16 15
80 15 13 13 15 16 15 15 15 14 13
90 13 12 13 11 9 9 10 8 7 7
100 6 6 6 7 7 7 7 6 6 6
110 6 6 6 5 4 4 4 3 3 3
120 3 3 3 3 3 3 3 1
0157
KPAWin© Single Sample Report - Sample
Customer ID: Sample ID: Description: Batch ID:
Configuration
Sample Unit: Performance: QC Limits:
None 1803110-0H
LCS HIGH 5826
µg/1 1003 Config
1000 Release
Sample Preparation & Analysis
Procedure ID: Range: Calibration ID: Equation: Specific Gravity:
None Low
Default Y= +249.459X +68.687
1
Range Sample Results
Reference Lifetime: LSR Time Gates: Sample Lifetime (µsec): Sample R 2 Intensity: Reference Ratio: Sample Intercept: Analytical Result: Dilution Factor: Aliquot Factor: Final Result: Uncertainty:
Interpreted Results
Detection Limit(IDL): Detection Limit(MDL):
(Low) 1803110-0H
211 5 - 49
291 1.000 1.015 48340
193.506 1.00 1.00
193.506 3.936
N/A N/A
Min Significant Sample Limit: 3.00E-01
Date Analyzed: Analyte: Analyst: Date Printed:
KPA Unit Calibration: Alarms:
03/27/2018 09:53 AM Uranium
JPachella 03/27/2018 09:54 AM
1001 Config 1000 Release
1003 Config
Specific Activity (Bq/g): 25000
Flags
IDL Flags: MDL Flags: Calibration: Sample:
0158
I n t e n s i t y
Net Intensities
Low: 1803110-0H 3/27/2018 9:53:23 AM
100000
10000
1000
100
10
1 +--------+-------"!------+---------t-------1--------+-~
0 20 40 60 80 100 120
Time Gate
o Sample 0 Ref
0159
Lab: No Lab Date: 3/27/2018 9:53:23 AM
Net Intensities
Low: 1803110-0H Sample Intensities 0 1 2 3 4 5 6 7 8 9
0 33599 44066 42813 40781 38992 37643 35764 34084 32453
10 30934 29599 28241 27101 25877 24764 23547 22503 21460 20521
20 19640 18829 18014 17278 16569 15807 15157 14514 13866 13231
30 12648 12052 11517 10955 10516 10046 9611 9180 8813 8360
40 8041 7726 7406 7064 6813 6522 6251 6008 5772 5516
50 5272 5027 4794 4562 4387 4192 4030 3873 3716 3548
60 3414 3239 3089 2978 2832 2694 2600 2495 2381 2301
70 2203 2087 1987 1901 1803 1727 1664 1589 1525 1482
80 1424 1376 1331 1271 1210 1151 1087 1035 996 948
90 904 869 828 792 757 728 700 672 658 633
100 608 580 556 520 497 487 467 453 433 421
110 394 377 355 334 310 301 294 287 287 275
120 267 250 237 219 208 200 182 207
Low: 1803110-0H Reference Intensities 0 1 2 3 4 5 6 7 8 9
0 4150 1236 1124 1055 977 906 813 734 659
10 608 562 520 489 461 417 384 362 331 313
20 298 278 257 245 223 208 190 179 164 154
30 148 146 138 131 127 120 112 107 107 101
40 92 89 86 80 75 77 72 68 61 61
50 57 54 50 51 49 41 38 39 36 32
60 34 34 33 32 31 28 28 26 26 24
70 25 24 25 23 23 24 23 22 22 22
80 19 17 15 16 15 15 15 16 14 13
90 13 11 10 9 7 7 7 8 8 8
100 9 9 6 7 7 6 5 6 6 6
110 5 6 5 5 5 5 3 3 4 3
120 4 5 4 4 3 2 3 1
0160
KPAWin© Single Sample Report - Sample
Customer ID: Sample ID: Description: Batch ID:
Configuration
Sample Unit: Performance: QC Limits:
None 1803110-02
BLANK 5826
µg/1 1003 Config
1000 Release
Sample Preparation & Analysis
Procedure ID: Range: Calibration ID: Equation: Specific Gravity:
None Low
Default Y= +249.459X +68.687
1
Range Sample Results
Reference Lifetime: LSR Time Gates: Sample Lifetime (µsec): Sample R 2 Intensity: Reference Ratio: Sample Intercept: Analytical Result: Dilution Factor: Aliquot Factor: Final Result: Uncertainty:
Interpreted Results
Detection Limit(IDL): Detection Limit(MDL):
(Low)
1803110-02
214 5 - 5
0 .000 .997
.000 .00 .00
.000
.000
N/A N/A
Min Significant Sample Limit: 3.00E-01
Date Analyzed: Analyte: Analyst: Date Printed:
KPA Unit Calibration: Alarms:
03/27/2018 09:55 AM Uranium
JPachella 03/27/2018 09:56 AM
1001 Config 1000 Release
1003 Config
Specific Activity (Bq/g): 25000
Flags
IDL Flags: MDL Flags: Calibration: Sample: E202, A72
0161
I n t e n s i t y
10000
1000
100
10
1
\
0 20
Net Intensities
Low: 1803110-02 3/27/2018 9:55:09 AM
,\ r-
II 40 60 80 100
Time Gate
i\ \! I
120
o Sample 0 Ref
0162
Lab: No Lab Date: 3/27/2018 9:55:09 AM
Net Intensities
Low: 1803110-02 Sample Intensities 0 1 2 3 4 5 6 7 8 9
0 606 -144 26 17 0 10 7 8 8
10 7 8 6 4 4 2 0 3 4 3
20 3 5 4 4 2 1 0 0 0 1
30 0 1 2 1 1 3 3 3 4 4
40 2 3 3 3 3 3 3 2 1 2
50 2 1 1 1 1 0 0 0 0 -1
60 0 0 0 0 1 0 1 1 1 0
70 0 0 0 -1 -1 0 -2 -1 -2 -1
80 0 1 1 1 1 -1 -1 -1 -2 0
90 1 1 0 1 0 0 0 0 0 0
100 0 0 1 0 0 -1 -1 -1 -1 -1
110 0 1 2 2 1 2 0 0 0 0
120 0 0 1 1 0 0 1 -2
Low: 1803110-02 Reference Intensities 0 1 2 3 4 5 6 7 8 9
0 4416 1315 1117 1017 944 868 785 712 651
10 604 557 512 478 439 405 380 354 326 305
20 281 267 259 245 229 218 204 186 177 172
30 162 152 142 133 125 122 115 111 107 102
40 95 90 86 83 77 73 71 66 59 58
50 58 57 54 55 53 49 45 44 42 38
60 41 38 36 32 31 27 25 24 22 22
70 20 19 21 22 20 21 21 19 18 17
80 17 15 13 14 13 12 12 14 13 12
90 11 12 11 9 10 10 8 8 8 8
100 7 7 7 7 7 6 5 5 5 5
110 6 6 5 5 5 6 6 6 6 4
120 4 4 3 2 2 3 1 5
0163
KPAWin© Single Sample Report - Sample
Customer ID: Sample ID: Description: Batch ID:
Configuration
Sample Unit: Performance: QC Limits:
None 1803110-03
OU-1-008 5826
µg/1 1003 Config
1000 Release
Sample Preparation & Analysis
Procedure ID: Range: Calibration ID: Equation: Specific Gravity:
None Low
Default Y= +249.459X +68.687
1
Range Sample Results
Reference Lifetime: LSR Time Gates: Sample Lifetime (µsec): Sample R 2 Intensity: Reference Ratio: Sample Intercept: Analytical Result: Dilution Factor: Aliquot Factor: Final Result: Uncertainty:
Interpreted Results
Detection Limit(IDL): Detection Limit(MDL):
(Low)
1803110-03
5 209
- 49 278
.997 1.029
1084 4.069
1.00 1.00
4.069 .094
N/A N/A
Min Significant Sample Limit: 3.00E-01
Date Analyzed: Analyte: Analyst: Date Printed:
KPA Unit Calibration: Alarms:
03/27/2018 10:01 AM Uranium
JPachella 03/27/2018 10:34 AM
1001 Config 1000 Release
1003 Config
Specific Activity (Bq/g): 25000
Flags
IDL Flags: MDL Flags: Calibration: Sample:
0164
I n t e n s i t y
Net Intensities
Low: 1803110-03 3/27/2018 10:01:11 AM
100000
10000
1000
100
10
l"-l-------1-------+------+---------1-------t-------i--
0 20 40 60 80 100 120
Time Gate
o Sample 0 Ref
0165
Lab: No Lab Date: 3/27/2018 10:01:11 AM
Net Intensities
Low: 1803110-03 Sample Intensities 0 1 2 3 4 5 6 7 8 9
0 18877 1626 1092 986 942 892 813 751 701
10 669 636 599 583 554 530 499 480 454 432
20 407 395 385 372 356 345 328 307 288 271
30 256 247 232 226 221 211 199 198 187 179
40 175 170 158 145 141 130 128 120 114 106
50 106 97 97 97 96 91 88 83 76 73
60 69 63 59 58 57 57 59 60 62 59
70 55 53 53 46 42 39 37 34 33 35
80 33 29 27 28 25 25 30 31 28 29
90 28 23 20 22 19 19 17 18 16 16
100 16 16 15 14 14 13 13 13 13 13
110 13 14 14 13 11 12 10 8 9 9
120 7 8 8 7 8 10 16 10
Low: 1803110-03 Reference Intensities 0 1 2 3 4 5 6 7 8 9
0 4350 1278 1113 1032 945 869 812 746 684
10 635 585 529 483 450 409 369 346 324 300
20 283 270 252 242 226 209 196 184 172 168
30 162 155 147 139 127 122 118 110 105 101
40 94 83 82 76 70 68 66 65 62 59
50 53 50 46 43 43 43 44 41 39 36
60 35 34 34 34 35 34 33 32 30 27
70 26 25 26 24 26 24 21 19 20 16
80 17 16 15 14 13 11 11 11 11 11
90 11 12 10 11 12 12 10 10 9 6
100 6 7 8 7 8 8 7 7 7 6
110 6 6 5 4 4 3 3 4 4 5
120 5 4 4 4 4 3 3 0
0166
KPAWin© Single Sample Report - Sample
Customer ID: Sample ID: Description: Batch ID:
Configuration
Sample Unit: Performance: QC Limits:
None 1803110-04
OU-1-008 5826
µg/1 1003 Config
1000 Release
Sample Preparation & Analysis
Procedure ID: Range: Calibration ID: Equation: Specific Gravity:
None Low
Default Y= +249.459X +68.687
1
Range Sample Results
Reference Lifetime: LSR Time Gates: Sample Lifetime (µsec) Sample R 2 Intensity: Reference Ratio: Sample Intercept: Analytical Result: Dilution Factor: Aliquot Factor: Final Result: Uncertainty:
Interpreted Results
Detection Limit(IDL): Detection Limit(MDL):
(Low)
1803110-04
5 215
- 49 285
.997 1.004
1109 4.171
1. 00 1. 00
4.171 .098
N/A N/A
Min Significant Sample Limit: 3.00E-01
Date Analyzed: Analyte: Analyst: Date Printed:
KPA Unit Calibration: Alarms:
03/27/2018 09:57 AM Uranium
JPachella 03/27/2018 10:45 AM
1001 Config 1000 Release
1003 Config
Specific Activity (Bq/g) 25000
Flags
IDL Flags: MDL Flags: Calibration: Sample:
0167
I n t e n s l
t y
100000
10000
1000
100
10
\
'
Net Intensities
Low: 1803110-04 3/27/2018 9:57:17 AM
1 +----------1------+-------+-------------t------+------+-LJ-
0 20 40 60 80 100 120
Time Gate
o Sample 0 Ref
0168
Lab: No Lab Date: 3/27/2018 9:57:17 AM
Net Intensities
Low: 1803110-04 Sample Intensities 0 1 2 3 4 5 6 7 8 9
0 20302 1701 1115 1025 929 875 824 792 749
10 720 687 649 602 581 560 535 518 505 470
20 436 420 390 364 350 344 324 316 304 296
30 274 266 254 248 235 228 210 197 183 177
40 172 175 171 164 156 150 144 137 127 118
50 112 102 98 99 101 97 96 91 83 75
60 74 72 68 65 66 64 60 54 56 56
70 50 50 51 44 41 42 38 39 42 40
80 39 39 35 33 33 30 30 31 30 29
90 27 25 24 23 23 23 22 20 20 18
100 18 19 21 20 20 19 15 15 15 14
110 15 16 15 15 14 15 14 14 13 12
120 11 10 9 9 9 9 9 7
Low: 1803110-04 Reference Intensities 0 1 2 3 4 5 6 7 8 9
0 4270 1302 1160 992 967 859 804 739 684
10 63 9 594 534 488 445 406 379 359 330 309
20 286 261 243 229 224 219 207 193 182 164
30 151 148 143 138 132 125 117 108 102 98
40 93 89 88 86 83 80 75 69 65 58
50 53 53 52 48 46 46 42 40 40 41
60 41 41 38 36 34 29 28 27 26 24
70 23 22 22 20 18 18 17 16 16 19
80 19 18 18 18 14 15 15 14 12 13
90 12 13 12 13 12 11 10 10 9 7
100 5 5 4 5 7 8 8 7 7 5
110 4 4 4 3 4 4 3 3 3 3
120 3 2 2 1 1 1 3 2
0169
KPAWin© (Version 1.2.9) Multiple Sample Report
Laboratory: ANALYTE: Uranium ANALYST: JPachella
Calibration Report Results
Low Calibration ID - Default High Calibration ID - None Date - 3/27/2018 9:32:50 AM
Calibration Report Results
Std Std Percent Time Reference
Range!Used!Sample IDI Cone I ID I Intercept I Uncert IDiscrepjGatesl Ratio jLifetimej R 2 L liW F_l..ags
Low + BCKGRND 0.000 24 5 .000 5-49 1.0000 248 .9240
Low + CAL STD 1 1. 000 U-12-1 381 20 25.076 5-49 1.0275 355 .9926
Low + CAL STD 2 5.000 U-12-2 1271 36 -3.625 5-49 1.0060 362 .9983
Low + CAL STD 3 10.000 U-12-3 2544 50 -.774 5-49 1.0182 375 .9987
Low + CAL STD 4 50.000 U-12-4 12572 112 .242 5-49 .9986 352 .9997
Low + CAL STD 5 100.000 U-12-5 24970 158 -.180 5-49 1.0177 368 .9998
Low + CAL STD 6 200.000 U-12-6 49977 224 .033 5-49 1.0341 293 .9999
Page 1 Date Printed - 3/27/2018 9:31:58 AM
0170
Low Range Calibration Curve
50000T
40000
. 30000 Intensity Intercept
20000
10000 __ ,/)±f
Qi illq:(,,, :
0 50
__ ,,,,,,//
,,,,,,-',,,,,,
,,,----m,,, ,,,," ,'
I I I
I I I
100 150 200
Concentration
0171
KPAWin© Single Sample Report - BckGnd
Customer ID: Sample ID: Description: Batch ID:
Configuration
Sample Unit: Performance: QC Limits:
None BCKGRND
BACKGROUND 5826
µg/1 1003 Config
1000 Release
Sample Preparation & Analysis
Procedure ID: None Low
Default 1
Range: Calibration ID: Specific Gravity:
Range Sample Results
Reference Lifetime: LSR Time Gates: Sample Lifetime (µsec): Sample R 2 Intensity: Reference Ratio: Sample Intercept:
Interpreted Results
(Low)
BCKGRND
221 5 - 49
248 .924
1.000 24
Date Analyzed: Analyte: Analyst: Date Printed:
KPA Unit Calibration: Alarms:
03/27/2018 09:10 AM Uranium
JPachella 03/27/2018 09:12 AM
1001 Config 1000 Release
1003 Config
Specific Activity (Bq/g): 25000
Flags
Sample:
0172
I n t e n s i t y
10000
1000
100
10
1 0 20
Net Intensities
Low: BCKGRND 3/27/2018 9:10:55 AM
"\
J\JlA ·11 ' \ \
;/ ·~ I~
\i
40 60 80
Time Gate
I I 100 120
I
o Sample 0 Ref
0173
Lab: No Lab Date: 3/27/2018 9:10:55 AM
Net Intensities
Low: BCKGRND Sample Intensities 0 1 2 3 4 5 6 7 8 9
0 7269 478 37 31 32 18 19 15 13
10 12 11 10 11 11 11 11 9 8 9
20 8 6 7 7 7 8 8 7 6 5
30 5 5 5 5 5 4 4 3 3 3
40 3 2 3 3 3 3 2 1 2 2
50 2 3 3 3 2 2 2 2 2 3
60 3 3 3 3 2 3 2 2 2 2
70 2 2 1 2 2 1 2 2 2 2
80 2 2 2 1 1 2 2 1 2 1
90 0 0 1 0 1 1 1 1 1 1
100 1 1 0 1 1 1 1 1 1 1
110 1 0 0 0 1 0 1 1 1 1
120 1 1 1 1 1 1 1 2
Low: BCKGRND Reference Intensities 0 1 2 3 4 5 6 7 8 9
0 4117 1168 1116 1009 941 832 796 738 681
10 627 581 542 503 467 432 410 374 345 327
20 313 286 268 251 234 221 208 203 193 189
30 173 162 150 140 128 123 117 113 106 103
40 96 90 87 87 80 82 85 83 77 75
50 69 60 56 54 54 53 52 51 51 47
60 43 44 43 39 37 39 36 36 36 36
70 34 33 31 30 29 28 27 25 22 24
80 21 20 20 23 21 23 24 23 22 21
90 19 18 19 18 18 17 18 15 14 14
100 13 12 12 13 13 13 14 13 13 14
110 14 13 14 13 11 11 10 10 11 13
120 11 11 10 9 9 9 14 8
0174
KPAWin© Single Sample Report - CalStd
Customer ID: Sample ID: Description: Batch ID:
Configuration
Sample Unit: Performance: QC Limits:
None CAL STD 1 CAL STD 1
5826
µg/1 1003 Config
1000 Release
Sample Preparation & Analysis
Procedure ID: Range: Calibration ID: Specific Gravity:
Range Sample Results
Reference Lifetime: LSR Time Gates: Sample Lifetime (µsec): Sample R 2 Intensity: Reference Ratio: Sample Intercept:
Interpreted Results
Detection Limit(IDL): Detection Limit(MDL):
None Low
Default 1
(Low) CAL STD 1
5 222
- 49 355
.993 1. 028
381
N/A N/A
Date Analyzed: Analyte: Analyst: Date Printed:
KPA Unit Calibration: Alarms:
03/27/2018 09:16 AM Uranium
JPachella 03/27/2018 09:17 AM
1001 Config 1000 Release
1003 Config
Standard ID: U-12-1 Standard Cone (µg/1): 1.000E+00
Specific Activity (Bq/g): 25000
Flags
IDL Flags: MDL Flags: Sample:
0175
10000
I 1000 I ' ' n ' ' ' ' t ' ' e ' \
n \ s ' l i '·· , ... ,
t ~ y "
100
10
1 0
' ' " ' ' •,
', ' ' '
20
Net Intensities
Low: CAL STD 1 3/27/2018 9:16:15 AM
' ' ' " '· '"\
40 60 80
Time Gate
100 120
o Sample 0 Ref
0176
Lab: No Lab Date: 3/27/2018 9:16:15 AM
Net Intensities
Low: CAL STD 1 Sample Intensities 0 1 2 3 4 5 6 7 8 9
0 1106 363 355 373 304 320 297 295 285
10 284 273 257 243 227 218 211 201 191 183
20 174 170 165 161 156 148 144 142 133 133
30 125 116 110 112 106 103 104 102 92 89
40 88 82 76 77 74 74 75 75 70 69
50 65 61 58 59 57 52 49 49 47 46
60 48 47 42 39 37 32 32 33 31 31
70 33 34 35 32 29 27 23 24 26 28
80 27 26 22 21 19 18 18 21 21 19
90 20 20 17 17 17 17 17 17 17 17
100 16 14 13 11 12 13 13 12 13 11
110 11 12 14 13 11 12 11 9 9 11
120 10 10 10 11 10 9 7 3
Low: CAL STD 1 Reference Intensities 0 1 2 3 4 5 6 7 8 9
0 3790 1343 1120 1058 962 886 820 753 698
10 640 598 556 512 468 441 404 371 353 337
20 313 291 273 256 234 218 212 205 197 190
30 182 171 165 155 144 138 135 124 115 114
40 108 101 96 93 90 85 77 73 70 67
50 66 66 70 68 66 64 63 57 52 51
60 49 46 45 44 40 38 36 33 34 34
70 32 33 32 30 28 29 28 29 29 29
80 26 27 26 25 25 26 23 24 24 22
90 21 19 18 19 18 18 18 16 17 17
100 16 16 16 13 12 12 10 12 12 11
110 12 13 12 14 13 14 12 12 10 11
120 9 10 10 9 9 10 9 15
0177
KPAWin© Single Sample Report - CalStd
Customer ID: Sample ID: Description: Batch ID:
Configuration
Sample Unit: Performance: QC Limits:
None CAL STD 2 CAL STD 2
5826
µg/1 1003 Config
1000 Release
Sample Preparation & Analysis
Procedure ID: None Low
Default 1
Range: Calibration ID: Specific Gravity:
Range Sample Results
Reference Lifetime: LSR Time Gates: Sample Lifetime (µsec): Sample R 2 Intensity: Reference Ratio: Sample Intercept:
Interpreted Results
Detection Limit(IDL): Detection Limit(MDL):
(Low) CAL STD 2
5 223
- 49 362
.998 1.006
1271
N/A N/A
Date Analyzed: Analyte: Analyst: Date Printed:
KPA Unit Calibration: Alarms:
03/27/2018 09:20 AM Uranium
JPachella 03/27/2018 09:24 AM
1001 Config 1000 Release
1003 Config
Standard ID: U-12-2 Standard Cone (µg/1): 5.000E+00
Specific Activity (Bq/g): 25000
Flags
IDL Flags: MDL Flags: Sample:
0178
10000
I 1000
n t e n s i t y
100
10
1 0
Net Intensities
Low: CAL STD 2 3/27/2018 9:20:17 AM
20 40 60 80
Time Gate
100 120
o Sample 0 Ref
0179
Lab: No Lab Date: 3/27/2018 9:20:17 AM
Net Intensities
Low: CAL STD 2 Sample Intensities 0 1 2 3 4 5 6 7 8 9
0 1455 1274 1203 1210 1086 1041 1001 959 912
10 877 854 825 793 772 752 717 687 670 651
20 617 603 585 560 538 517 501 481 468 446
30 424 402 386 373 368 358 351 335 323 306
40 298 293 282 266 259 252 242 244 241 230
50 217 204 198 188 181 178 173 160 152 147
60 138 134 133 128 126 124 121 116 118 112
70 106 99 94 83 83 82 78 78 80 72
80 71 71 67 66 66 62 57 58 53 52
90 51 51 47 45 43 45 43 42 44 40
100 37 35 30 28 30 28 28 30 28 26
110 28 27 25 24 23 22 20 21 20 20
120 20 20 19 19 17 14 17 6
Low: CAL STD 2 Reference Intensities 0 1 2 3 4 5 6 7 8 9
0 3897 1302 1151 1083 978 868 811 740 688
10 651 600 552 507 461 424 392 372 355 334
20 309 288 268 251 235 225 205 189 176 167
30 155 158 153 150 146 141 132 125 120 112
40 106 101 98 87 85 82 80 74 72 70
50 66 62 58 57 55 54 49 48 45 41
60 37 37 36 35 36 35 32 35 32 29
70 28 30 26 25 23 21 19 17 16 16
80 15 15 15 14 13 13 11 11 11 13
90 14 14 12 13 13 11 11 13 12 11
100 11 11 10 10 8 8 7 7 7 8
110 7 7 6 6 5 5 4 4 4 5
120 6 6 6 6 6 6 8 7
0180
KPAWin© Single Sample Report - CalStd
Customer ID: Sample ID: Description: Batch ID:
Configuration
Sample Unit: Performance: QC Limits:
None CAL STD 3 CAL STD 3
5826
µg/1 1003 Config
1000 Release
Sample Preparation & Analysis
Procedure ID: None Low
Default 1
Range: Calibration ID: Specific Gravity:
Range Sample Results
Reference Lifetime: LSR Time Gates: Sample Lifetime (µsec) Sample R 2 Intensity: Reference Ratio: Sample Intercept:
Interpreted Results
Detection Limit(IDL) Detection Limit(MDL)
(Low) CAL STD 3
5 220
- 49 375
.999 1.018
2544
N/A N/A
Date Analyzed: Analyte: Analyst: Date Printed:
KPA Unit Calibration: Alarms:
03/27/2018 09:24 AM Uranium
JPachella 03/27/2018 09:26 AM
1001 Config 1000 Release
1003 Config
Standard ID: U-12-3 Standard Cone (µg/1): 1.000E+0l
Specific Activity (Bq/g) 25000
Flags
IDL Flags: MDL Flags: Sample:
0181
I n t e n s i t y
10000
1000
100
10
1 0 20
Net Intensities
Low: CAL STD 3 3/27/2018 9:24:48 AM
40 60 80 100
Time Gate
120
o Sample 0 Ref
0182
Lab: No Lab Date: 3/27/2018 9:24:48 AM
Net Intensities
Low: CAL STD 3 Sample Intensities 0 1 2 3 4 5 6 7 8 9
0 2590 2403 2326 2263 2144 2139 1994 1928 1838 10 1788 1741 1687 1627 1584 1522 1465 1409 1361 1317 20 1278 1234 1184 1136 1089 1046 1006 977 955 929 30 899 874 848 816 785 770 738 717 689 653 40 621 597 573 551 547 536 527 511 494 480 50 467 447 428 421 408 387 368 359 347 334 60 327 314 298 294 284 272 274 264 248 237 70 224 217 215 206 201 196 188 181 174 168 80 164 160 156 152 151 152 147 141 137 131 90 121 116 116 114 109 104 105 99 94 90
100 89 81 81 79 81 80 77 76 74 74 110 69 71 67 63 56 55 50 48 46 44 120 48 48 46 44 42 37 39 28
Low: CAL STD 3 Reference Intensities 0 1 2 3 4 5 6 7 8 9
0 4026 1250 1123 1047 975 831 803 731 694 10 637 588 536 508 460 433 416 393 369 344 20 319 283 263 236 228 225 215 203 190 180 30 164 165 158 151 138 129 118 112 110 103 40 101 91 88 84 84 81 82 82 74 70 50 66 65 63 62 59 57 56 51 50 49 60 47 44 43 40 38 36 34 32 34 33 70 32 30 29 25 23 22 23 24 25 26 80 25 25 24 22 21 20 17 15 16 15 90 16 14 15 14 12 13 15 16 16 17
100 15 14 12 12 11 11 10 9 9 9 110 9 9 9 9 8 7 8 8 7 6 120 6 5 5 5 6 6 12 7
0183
KPAWin© Single Sample Report - CalStd
Customer ID: Sample ID: Description: Batch ID:
Configuration
Sample Unit: Performance: QC Limits:
None CAL STD 4 CAL STD 4
5826
µg/1 1003 Config
1000 Release
Sample Preparation & Analysis
Procedure ID: Range: Calibration ID: Specific Gravity:
Range Sample Results
Reference Lifetime: LSR Time Gates: Sample Lifetime (µsec): Sample R 2 Intensity: Reference Ratio: Sample Intercept:
Interpreted Results
Detection Limit(IDL): Detection Limit(MDL):
None Low
Default 1
(Low)
CAL STD 4
5 223
- 49 352
1.000 .999
12572
N/A N/A
Date Analyzed: Analyte: Analyst: Date Printed:
KPA Unit Calibration: Alarms:
03/27/2018 09:26 AM Uranium
JPachella 03/27/2018 09:29 AM
1001 Config 1000 Release
1003 Config
Standard ID: U-12-4 Standard Cone (µg/1): 5.000E+0l
Specific Activity (Bq/g): 25000
Flags
IDL Flags: MDL Flags: Sample:
0184
I n t e n s i t y
100000
1000
100
10
1 0 20
Net Intensities
Low: CAL STD 4 3/27/2018 9:26:59 AM
40 60 80 100
Time Gate
120
o Sample 0 Ref
0185
Lab: No Lab Date: 3/27/2018 9:26:59 AM
Net Intensities
Low: CAL STD 4 Sample Intensities 0 1 2 3 4 5 6 7 8 9
0 9735 11881 11456 10762 10422 10217 9817 9490 9118 10 8750 8396 8059 7732 7449 7186 6966 6720 6456 6231 20 5980 5737 5503 5351 5134 4962 4808 4654 4457 4329
30 4160 3981 3837 3686 3522 3390 3279 3166 3066 2961
40 2869 2768 2677 2570 2490 2387 2319 2237 2174 2079
50 2028 1945 1868 1794 1743 1657 1608 1554 1495 1443
60 1404 1350 1294 1246 1203 1167 1129 1091 1065 1028
70 979 93 9 927 890 854 828 794 748 724 708
80 689 659 644 624 591 563 559 534 519 503
90 492 462 452 433 429 411 400 385 377 353
100 342 331 315 298 285 276 267 260 257 249
110 234 230 227 216 216 213 202 188 179 170
120 165 160 159 157 153 150 144 145
Low: CAL STD 4 Reference Intensities 0 1 2 3 4 5 6 7 8 9
0 4017 1192 1106 1008 933 846 785 724 672
10 635 584 551 514 474 432 403 369 341 323
20 304 287 265 251 233 222 210 200 192 183
30 173 160 156 144 137 128 121 117 111 105
40 103 101 98 93 91 83 78 73 71 67
50 66 63 62 58 53 50 47 42 40 38
60 41 41 41 41 38 35 34 32 34 34
70 33 34 33 30 30 27 24 23 23 21
80 21 19 18 19 17 17 16 15 12 12
90 10 11 11 12 15 14 14 13 13 11
100 11 10 9 8 9 10 10 10 10 9
110 8 7 6 7 6 6 7 8 6 7
120 7 7 7 8 7 7 11 6
0186
KPAWin© Single Sample Report - CalStd
Customer ID: Sample ID: Description: Batch ID:
Configuration
Sample Unit: Performance: QC Limits:
None CAL STD 5 CAL STD 5
5826
µg/1 1003 Config
1000 Release
Sample Preparation & Analysis
Procedure ID: None Low
Default 1
Range: Calibration ID: Specific Gravity:
Range Sample Results
Reference Lifetime: LSR Time Gates: Sample Lifetime (µsec): Sample R 2 Intensity: Reference Ratio: Sample Intercept:
Interpreted Results
Detection Limit(IDL): Detection Limit(MDL):
(Low) CAL STD 5
220 5 - 49
368 1.000 1.018 24970
N/A N/A
Date Analyzed: Analyte: Analyst: Date Printed:
KPA Unit Calibration: Alarms:
03/27/2018 09:29 AM Uranium
JPachella 03/27/2018 09:31 AM
1001 Config 1000 Release
1003 Config
Standard ID: U-12-5 Standard Cone (µg/1): 1.000E+02
Specific Activity (Bq/g): 25000
Flags
IDL Flags: MDL Flags: Sample:
0187
I n t e n s i t y
Net Intensities
Low: CAL STD 5 3/27/2018 9:29:54 AM
100000
10000
1000
100
10
1 +---------1------1--------+--------l------+-----+--
0 20 40 60 80 100 120
Time Gate
o Sample 0 Ref
0188
Lab: No Lab Date: 3/27/2018 9:29:54 AM
1\T .-.. .._ ,.. _ _...,..._,......_..._.,: ..J-..: ,...._,.... .l'-.IC l- .L.L.LL,.C.::,.J..LCI .l. l-.l.~CI
Low: CAL STD 5 Sample Intensities 0 1 2 3 4 5 6 7 8 9
0 17901 23097 22756 21936 21114 20337 19603 18904 18231
10 17594 17005 16378 15770 15203 14621 14118 13591 13112 12652
20 12249 11824 11486 11119 10732 10392 10018 9648 9231 8920
30 8560 8229 7932 7720 7448 7199 6967 6757 6474 6252
40 6047 5860 5646 5542 5355 5144 4958 4779 4552 4408
50 4249 4094 3911 3795 3646 3579 3474 3369 3253 3146
60 3003 2890 2814 2729 2642 2564 2494 2415 2336 2242
70 2146 2082 2008 1945 1901 1873 1793 1724 1660 1595
80 1522 1471 1434 1382 1348 1317 1265 1200 1164 1107
90 1052 1044 1023 986 956 940 887 857 828 790
100 757 731 708 684 672 650 633 615 592 568
110 540 524 497 483 472 460 444 434 421 404
120 386 377 369 362 348 341 312 305
Low: CAL STD 5 Reference Intensities 0 1 2 3 4 5 6 7 8 9
0 3982 1350 1213 981 923 851 789 728 673
10 642 590 550 516 487 448 419 388 357 327
20 305 287 262 245 231 210 195 186 181 171
30 170 167 161 154 149 138 132 127 116 106
40 103 97 88 87 85 79 76 74 68 65
50 66 62 58 57 55 50 48 48 46 47
60 49 46 45 43 40 35 36 32 33 33
70 33 29 29 30 27 27 28 26 22 20
80 18 16 20 21 21 21 21 17 18 17
90 16 15 16 14 14 13 14 14 15 14
100 14 16 14 13 11 10 8 9 8 9
110 10 10 9 9 9 8 7 6 6 6
120 5 6 5 6 5 5 4 6
0189
KPAWin© Single Sample Report - CalStd
Customer ID: Sample ID: Description: Batch ID:
Configuration
Sample Unit: Performance: QC Limits:
None CAL STD 6 CAL STD 6
5826
µg/1 1003 Config
1000 Release
Sample Preparation & Analysis
Procedure ID: None Low
Default 1
Range: Calibration ID: Specific Gravity:
Range Sample Results
Reference Lifetime: LSR Time Gates: Sample Lifetime (µsec): Sample R 2 Intensity: Reference Ratio: Sample Intercept:
Interpreted Results
Detection Limit(IDL): Detection Limit(MDL):
(Low) CAL STD 6
5 217
- 49 293
1.000 1.034 49977
N/A N/A
Date Analyzed: Analyte: Analyst: Date Printed:
KPA Unit Calibration: Alarms:
03/27/2018 09:32 AM Uranium
JPachella 03/27/2018 09:34 AM
1001 Config 1000 Release
1003 Config
Standard ID: U-12-6 Standard Cone (µg/1): 2.000E+02
Specific Activity (Bq/g): 25000
Flags
IDL Flags: MDL Flags: Sample:
0190
I n t e n s i t y
Net Intensities
Low: CAL STD 6 3/27/2018 9:32:50 AM
100000
10000
1000
100 '-, __
10
1+------+.--------+.--------1-------t-------+------f---
0 20 40 60 80 100 120
Time Gate
o Sample 0 Ref
0191
Lab: No Lab Date: 3/27/2018 9:32:50 AM
!:'!et T,-,t-0,-,c-1; t--: C('""t ..l- ........... - ...... 1---'...I.. '-"...I..._.'"-'
Low: CAL STD 6 Sample Intensities 0 1 2 3 4 5 6 7 8 9
0 34153 45378 44175 42508 40923 38444 36803 35085 33612 10 32200 30785 29547 28156 26849 25577 24479 23368 22354 21369 20 20482 19582 18731 17965 17160 16410 15676 15023 14333 13677 30 13091 12515 11943 11457 11012 10499 10103 9671 9235 8832 40 8508 8110 7738 7423 7136 6826 6523 6279 5980 5677 50 5418 5193 4998 4815 4647 4450 4272 4039 3852 3667 60 3509 3358 3227 3093 2959 2840 2713 2607 2499 2385 70 2285 2185 2091 1994 1910 1820 1733 1649 1582 1531 80 1476 1420 1367 1319 1253 1190 1151 1104 1061 1017 90 979 928 906 859 821 784 749 702 674 647
100 629 602 569 541 514 485 473 456 437 416 110 395 376 362 350 338 337 326 312 304 297 120 278 263 248 238 225 213 214 183
Low: CAL STD 6 Reference Intensities 0 1 2 3 4 5 6 7 8 9
0 3959 1335 1119 1028 944 975 827 769 691 10 636 585 551 508 474 437 405 372 346 318 20 303 288 274 257 237 219 203 190 177 172 30 160 156 144 138 133 127 120 117 113 110 40 107 102 99 92 84 82 77 72 67 62 50 56 52 51 54 53 51 53 53 47 47 60 47 43 38 37 34 33 31 30 30 32 70 27 27 26 25 25 26 23 21 19 17 80 15 15 16 17 16 17 18 18 17 18 90 17 15 14 13 14 13 13 13 13 10
100 11 11 12 11 12 11 10 9 10 9 110 9 11 9 9 9 11 10 8 7 6 120 4 4 5 5 5 6 7 5
0192
SECTIONX
ANALYTICAL DAT A (ISOTOPIC THORIUM)
0193
Eberline Analytical
Oak Ridge Laboratory
Analysis Sheet
Work Order
Analysis Code
Run
Internal Fraction
01
02
I
! Sample
Desc
LCS
18-03110 ThlSO Run 1
Client ID
LCS -
---------------t
MBL : BLANK i
Login CPM
Printed: 313012018 4:59 AM Page 1 of 3
Sample Date
03/23/18 00:00
03/23/18 00:00
Sample Aliquot
1.0000E+00
1.0000E+00
I I 3/23/2018 I 03 DUP I~- ___ ou_-_1-_00_8 ___ ---,----+-------+----------1
4/12/2018 04 DO I OU-1-008 I I---------------~
Date Received
Lab Deadline
38
38
03/19/18 18:02 5.0000E-01
03/19/18 18:02 5.0000E-01
Client I AMO Environmental Decisions
Project WESTLAKE
Report Level 4
Activity Units pCi
Aliquot Units
Matrix WA
Method EPA 907 .0 Modified
Instrument Type Alpha Spectroscopy
Radiometric Tracer Th-229
Radiometric Sol# Th-18a
Tracer Act (dpm/g) 22.46
Carrier
Carrier Cone (mg/ml)
I I I
!
I
--·-- I I I • ···
• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. h Indicates estimated SAF value.
•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
0194
Eberline Analytical
Oak Ridge Laboratory Analysis Sheet
Internal Sample J Tracer
Fraction Desc I Aliquot(g)
01 LCS 0.4666
02 MBL 0,2337
03 DUP 0,2314
04 DO 0,2306
I
Tracer Total ACT(dpm)
10,5
52
5,2
52
i !
i i
!
I
Radiometric Tracer (pCi)
18-03110 ThlSO Run 1
i Radiometric [ Grav Carrier I Grav Filter
%Rec Added(ml) [ Tare (g)
' I 0,00 I I I
0,00
' 0,00
0,00
I I
i
I
' '
I
Grav Filter Final (g)
I I
• SAF1 is used for-Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. A Indicates estimated SAF value,
** Actual mass exceeded the calibration curve range. Results should be qualified as appropriate,
i Grav Filter Grav
Net(g) %Rec
I i
I
Printed: 3/30/2018 4:59 AM Page 2 of 3
i i
Mean
I
SAF SAF %Rec 1* 2*
i I !
-
i --
!
I
I !
I '
I
!
I
0195
Eberline Analytical Oak Ridge Laboratory
Analysis Sheet
Internal Sample Fraction Desc
01 LCS
02 MBL
03 DUP
04 DO
1---
i I
~--
Rough Prep Date
I I i
Rough Prep I
Prep
I By I
Date
i
03/28/18 08:36 j
I 03/28/18 08:36 '
03/28/18 08:36
03/28/18 08:36
I
I
I I
18~03110 ThlSO Run 1
Prep By
JHARVEY
JHARVEY
JHARVEY
JHARVEY
Sep to Date/rime
* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. " Indicates estimated SAF value.
** Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
I Sep to
By
'
i I I
i
i
I
!
' !
'
Printed: 3/30/2018 4:59 AM Page 3 of 3
I Sep t1
I Sep t1
Date/rime By
--
0196
Eberline Analytical Oak Ridge Laboratory
<( Lab Fraction
Nuclide
01 TH-228
~
a, "0
8 -!!! ~ "iii C: q:
i1 0
T"'"
0 ti) -.c I-
1/) C .Q .!!? (.) Q)
C iii -C Q)
E C 0
·= > C w 0 ~ <(
02 TH-228
03 TH-228
04 TH-228
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03110-ThlSO-1
Client Activity Error Estimate MDA
Identification Units Results
LCS pCi/1 5.81E+00 1.09E+00 1.20E-01
BLANK pCi/1 5.29E-03 3.43E-02 9.33E-02
OU-1-008 pCi/I -3.87E-02 7.02E-02 2.14E-01
OU-1-008 pCi/I 3.44E-03 1.14E-01 2.74E-01
LCS LCS Known %R
4.80E+00 121.11
Printed: 3/30/2018 11 :54 AM Page 1 of 3
I LCS RPD MDA Blank Flag Flag Flag Flag
OK OK
OK OK
NA OK
OK
0197
Eberline Analytical Oak Ridge Laboratory
,: Lab Nuclide
Fraction
01 TH-228
;r-~ 0::
02 TH-228
03 TH-228
-04 TH-228
{: 0 0 0 u, .!!,!
~ -CII .c C: I-q;
1/) C: 0
-~ (.J Cl> C ns -11 C: Cl>
0 E C: 0 ... ·s;: C: w 0 :s <(
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03110-ThlSO-1
Sample Sample Radiometric Grav Mean
I Date Aliquot %Rec %Rec %Rec
03/23/18 00:00 1.00E+00 71.01 0.00 0.00
03/23/18 00:00 1.00E+00 85.02 0.00 0.00
03/19/18 18:02 5.00E-01 95.72 0.00 0.00
03/19/18 18:02 5.00E-01 90.10 0.00 0.00
SAF I
Printed: 3/30/2018 11 :54 AM Page 2 of 3
SeptO
I Sept1
DatefTime DatefTime
0198
Eberline Analytical Oak Ridge Laboratory
~ Lab
Nuclide Fraction
01 TH-228
~ I ~ 02 TH-228
03 TH-228
04 TH-228 .g 0 0 0 en ,!!! ~ -111 .c i::: I-'CC
u, C 0
.!!? (.) Q)
0 iu -~I C Q)
E C 0 ... '> C w 0 :ii: <(
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03110-ThlSO-1
Counting
I Halflife
Detect Carrier Count I Counts Date/Time (days) Time
1
03/30/18 08:10 A_Spec Alpha_040 170 2.73 E+02
03/30/18 08: 10 A_Spec Alpha_041 170 3.20 E-01
03/30/18 08:10 A_Spec Alpha_042 170 -1.19 E+00
03/30/18 08:10 A_Spec Alpha_043 170 1.10 E-01
I Bkg CPM
4.00 E-03
4.00 E-03
7.00 E-03
1.70 E-02
Printed: 3/30/2018 11 :54 AM Page 3 of 3
Eff
17.6
18.8
17.2
19
0199
Eberline Analytical Oak Ridge Laboratory
~ Lab I Nuclide
Fraction
01 TH-230
;r~ a:
02 TH-230
03 TH-230
04 TH-230
.g 0 0 0 UJ .!!!
i -Cll ..c: C: I-q:
fl) C: 2
.!:!? 0 Q)
C ni -~I C: Q)
E C: 0 ... "> C: w 0 ~ <(
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-0311 0-ThlSO-1
Client Activity Results Error Estimate I MDA
Identification Units I
LCS pCi/I 6.64E+00 1.22E+00 1.34E-01
BLANK pCi/I 1.07E-01 9.52E-02 1.18E-01
OU-1-008 pCi/I 1.S0E-01 1.59E-01 2.03E-01
OU-1-008 pCi/I 2.83E-01 1.99E-01 1.SSE-01
LCS LCS
Known %R
5.37E+00 123.56
Printed: 3/30/2018 11 :54 AM Page 1 of 3
LCS RPD MDA Blank
Flag Flag Flag Flag
OK OK
OK OK
NA OK
OK
..
0200
Eberline Analytical Oak Ridge Laboratory
( Lab Nuclide
Fraction
01 TH-230
§ a::
.g 0 0 -r!? ~ ai C: ct
II
"'"""
0 en -.c ~
1/) C: 0
:~ c., Cl)
C cu -C: Cl)
E C: 0 ... ·s: C: w 0 :i: <(
02 TH-230
03 TH-230
04 TH-230
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03110-ThlSO-1
Sample Sample Radiometric Grav Mean I
Date Aliquot %Rec %Rec %Rec I
03/23/18 00:00 1.00E+00 71.01 0.00 0.00
03/23/18 00:00 1.00E+00 85.02 0.00 0.00
03/19/18 18:02 5.00E-01 95.72 0.00 0.00
03/19/18 18:02 5.00E-01 90.10 0.00 0.00
SAF
Printed: 3/30/2018 11 :54 AM Page 2 of 3
SeptO
I Sept1
Date/Time Date/Time
0201
Eberline Analytical Oak Ridge Laboratory
~ ~
§ a:
-t 0 0 -!!! ~ iii i::: q:
1: -~ 0
~
0 U) -.c I-
rn C: 0
.!!? (.) Q)
C nJ -C: Q)
E C: 0 ... . > C: w 0 ~ <(
Lab Nuclide
Fraction
01 TH-230
02 TH-230
03 TH-230
04 TH-230
! Sample
Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-0311 0-ThlSO-1
Counting
I Halflife
Detect Carrier Count
Counts DatefTime (days) Time
03/30/18 08:10 A_Spec Alpha_040 170 3.12 E+02
03/30/18 08:10 A_Spec Alpha_041 170 6.47 E+00
03/30/18 08:10 A_Spec Alpha_042 170 4.98 E+00
03/30/18 08:10 A_Spec Alpha_043 170 9.15 E+00
8kg CPM
6.00 E-03
9.00 E-03
6.00 E-03
5.00 E-03
Printed: 3/30/2018 11 :54 AM Page 3 of 3
Eff
17.6
18.8
17.2
19
0202
Eberline Analytical Oak Ridge Laboratory
~ Lab
Nuclide Fraction
01 TH-232
;r~ 0::
02 TH-232
03 TH-232
04 TH-232 Cl) 0 "0 0 0 en -!!! ~ -QI .c c:: I-q;
1/) C: .2
.!!? (.) Q)
C
.fi
~I C: Q)
E C: 0 ... ·s: C: w 0 :E <i:
Sample Oesc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03110-ThlSO-1
Client Activity Results I Error Estimate
I Identification Units MDA
LCS pCi/I 5.S0E+00 1.09E+00 1.65E-01
BLANK pCi/I -3.S0E-03 6.11E-02 1.S0E-01
OU-1-008 pCi/I 1.58E-02 6.57E-02 1.69E-01
OU-1-008 pCi/I -5.87E-03 6.64E-02 2.04E-01
LCS LCS Known %R
4.80E+00 120.87
Printed: 3/30/2018 11 :55 AM Page 1 of 3
LCS RPO MDA Blank
Flag Flag Flag Flag
OK OK
OK OK
NA OK
OK
0203
Eberline Analytical Oak Ridge Laboratory
~ ~ I ~ -
Cl> 'ti 0
(.)
,!!! .; <II c::
C(
-~
0 en -.c I-
in C: .2 .!!! (.) Q)
C ns -C: Q)
E C: 2 ·s: C: w 0 :i: <(
Lab Nuclide
Fraction
01 TH-232
02 TH-232
03 TH-232
04 TH-232
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-0311 0-ThlSO-1
Sample Sample Radiometric Grav Mean
I Date Aliquot %Rec %Rec %Rec
03/23/18 00:00 1.00E+00 71.01 0.00 0.00
03/23/18 00:00 1.00E+00 85.02 0.00 0.00
03/19/18 18:02 5.00E-01 95.72 0.00 0.00
03/19/18 18:02 5.00E-01 90.10 0.00 0.00
SAF
Printed: 3/30/2018 11:55 AM Page 2 of 3
SeptO Sept1
DatefTime DatefTime
0204
Eberline Analytical Oak Ridge Laboratory
( Lab I
Fraction Nuclide
01 TH-232
;r~ a::
02 TH-232
03 TH-232
04 TH-232 CII 0 b 0 0 u, -!!! ~ -Ill .c t: ..... q:
II) C:
.2 -~ (.) Cl>
C ns -ll C: Cl> E C: 0 ... ·s; C: w 0 :!!: <
I Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03110-ThlSO-1
Counting Halflife i Count
DatefTime (days) Detect Carrier
Time Counts
03/30/18 08:10 A_Spec Alpha_040 170 2.73 E+02
03/30/18 08:10 A_Spec Alpha_041 170 -2.30 E-01
03/30/18 08:10 A_Spec Alpha_042 170 4.90 E-01
03/30/18 08:10 A_Spec Alpha_043 170 -1.90 E-01
Bkg I CPM '
1.20 E-02
1.90 E-02
3.00 E-03
7.00 E-03
Printed: 3/30/2018 11 :55 AM Page 3 of 3
Eff
17.6
18.8
17.2
19
0205
y /
0 ·S::
Count Room Report
Client: AMO Environmental Decisio
Internal Sample Client
Fraction Desc ID
01 LCS LCS
02 MBL BLANK
03 DUP OU-1-008
04 DO OU-1-008
...
I i I
I
18-0311 0-ThlSO-1 (pCi/I) in WA
Tracer ID: Th-18a
I
I I Sample I Sample Tracer I Date I
Aliquot Aliquot (g) i
03/23/18 00:00 1.0000 0.4666
03/23/18 00:00 1.0000 0.2337
03/19/18 18:02 0.5000 0.2314 I
03/19/18 18:02 0.5000 0.2306
I I I ;
I
I
I I I I
i I
!
i I
i I
Tracer Radiometric ACT(dpm) Tracer (pC1J
10.4798
5.2489
5.1972
5.1793
I
i
--·------- --
_, - --- ----- ..
-·---------
Printed: 3/30/2018 4:59 AM
Page 1 of 1
\ Radiometric I
SAF i SAF
I %Rec 1· I 2· I
0.00
0.00
0.00 I I
0.00
I
I I !
i I I I !
I
I
!
I
I
0206
Eberline Analytical Oak Ridge Laboratory
Activity Isotope
I Sol#
dpmlg
Th-228 i Th-Sb 103.560
Th-230 I Th-1b 23.520
Th-232 I Th-8b 103.560
fraction Isotope I
Sol#
01 Th-229 Th-18a
02 Th-229 Th-18a
03 Th-229 Th-18a
04 Th-229 Th-18a
I I
Version 2.0 08/99
Solution i Approx Date I Addition
3/28/20181 0.100
3/28/20181 0.500 !
3/28/2018! 0.100
Tracers Activity I Solution dpm/g Date
22.460 3/28/2018
22.460 3/28/2018
22.460 3/28/2018
22.460 3/28/2018
!
' ' i
Spike and Tracer Worksheet
Analysis Code Date Technician
ThlSO 3/28/2018 8:31 JHARVEY
LCS MS LCSD MSD LCS MS Volume Volume Volume Volume Known
1 Error Added i Error
Used{g) Used (g) Used{g) Used (g) pCi I Estimate pCi ! Estimate
0.1028 4.8of 0.173 0.00 0.000
0.5070 I
5 371 0.145 0.00 0.000
0.1028 4.801 0.173 0.00 0.000
Balance Printer Tapes Volume Approx Tracer Used(g) Addition
0.4666 0.2200
0.2337 0.2200
0.2314 0.2200
0.2306 0.2200
Page 1 of 1 Printed: 3/28/2018 8:36 AM
Technician Initials Witness Initials
LCSD MSD Known Error I Added Error
pCi Estimate pCi I Estimate
o.oo I 0.0001 o.oo, 0.000
o.oo I 0.0001 o.oo ! 0.000
0.00 I 0.0001 0.00 i 0.000
LCS
Matrix Spike
0207
Lab
Eberline Analytical Oak Ridge Laboratory
AMO Environmental Decisions
Fraction Client ID
01 LCS
02 BLANK
03 OU-1-008 04 OU-1-008
~-
Comments
Sample
Type
LCS MBL
DUP DO
Aliquot Worksheet
Analysis Code Rpt Units Lab Deadline
ThlSO liters 4/12/2018
Muffle Data Dilution Data Aliquot Data Ratio
Post/Pre No of Dils Oil Factor Ratio Aliquot Net Equiv
1.0000E+OO 1.0000E+OO
1.0000E+OO 1.0000E+OO
5.0000E-01 5.0000E-01·
5.0000E-01 5.0000E-01
Technician: ~Ll,N-(~~
Technician
JHARVEY
MS Aliquot Data
Printed: 3/28/2018 9:23 AM Page 1 of 1
H-3 Solids Only
Aliquot Net Equiv WaterAaaeai-A~
(ml) , Aliq
!
i
I
!
l
0208
Jt;Apex-Alpha,. Sample Description: Spectrum File: Batch Identification:
SPIKE \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002099
1803110A-TH Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Tracer Certificate: Tracer Quantity: Effective Efficiency:
01 Shelf 2 Th iso
Alpha_040 06027396B 91135 System Bkgd 211463
<not performed>
1. 000E+000 +!- 0.000E+000 3/30/2018 6:43:14 3/30/2018 8:10:31
170.0 minutes 170.0 minutes
Th229 S TH-18A 0.467 mL 0.1248 +/- 0.0093
AM AM
liter
Counting Efficiency: 0.1757 +/- 0.0031 on 2/16/2018 0.7101 +/- 0.0543
9:34:27 AM
Chem. Recovery Factor:
Control Certificate Name: NatTh Th-8 Chem. Recov. of Control: TH-232 1.208730 +/- 0.121742
Peak Match Tolerance: 0.175 MeV
Nuclide
TH-227 TH-228 TH-229 T TH-230 TH-232
Energy (MeV)
5.783 5.394 4.872 4.645 3.970
PEAK AREA REPORT
Net Pk Area
8.98 273.32 222.26 311. 98 272.96
Pk Area Error%
69.62 11. 87 13.28 11.12 11. 92
Ambient Backgnd
1. 02 0.68 3.74 1. 02 2.04
Reagent Backgnd
0.00E+000 0.00E+000 0.00E+000 0.00E+000 0.00E+000
FWHM (keV)
0.0 10.4 12.0
4.5 10.4
T Tracer Peak used for Effective Efficiency
Nuclide
TH-227 TH-228 TH-229 TH-230 TH-232
Id Conf.
0. 977 1.000 1.000 0. 996 0. 996
NUCLIDE ANALYSIS RESULTS
Energy (keV)
5850.00* 5400.00* 4872.00* 4672.00* 3997.00*
Activity (pCi/liter )
l.96E-001 +/- l.39E-001 5.81E+000 +/- l.09E+000 4.74E+000 +!- 6.92E-001 6.64E+000 +!- l.22E+000 5.80E+000 +/- l.09E+000
114 3/.Jrjri
MDA (pCi/liter
l.37E-001 +/- 2.00E-002 1. 20E-001 +!- 1. 75E-002 2.05E-001 +/- 2.99E-002 1. 34E-001 +/- l.96E-002 l.65E-001 +/- 2.41E-002
0209
60
55
50
45
40
35 V) .µ C: ::::s 8 30
25
20
15
10
5
0000209931.CNF
9 i=
O l,\~lft\llllMmw nil \NI wwum, 1 '" , r 1" ,I w Mlll\!111111!\mVII m1r I 'I . " ,, 3500 l/1. i Iii iliilmJ,r:', 111ill/111VIEll 11
4000
ROI Type: 1
4500 5000 Energy(kev)
Live Time :10200.000 sec Real Time :10200.300 sec start: 1:3473.6(kev) Stop : 1024:6542.9(keV) Acq. start :Fri Mar 30 08:10:31 2018
1 1 ~ I 111!1\IVIIIWll rn:;, ,'1 q ' ·1 II I ! ! 111,111111nm1 I 11 I
5500 6000 6500
ROI Type: 3
0210
Channel Data Report 3/30/2018 11:10:39 AM Page 1
******************************************************* ***** s p E C T R A L DAT A R E P O R T ***** *******************************************************
Sample Title: 01
Elapsed Live time: 10200 Elapsed Real Time: 10200
Channell------l-------1-------1-------1-------1------- 1-------1-------1 1: 1 1 0 1 0 0 1 0
9 : 1 0 1 0 1 1 1 0
17: 4 0 1 0 2 1 0 0
25: 1 1 0 0 0 1 1 0
33: 0 1 0 0 1 0 0 2
41: 0 1 2 1 2 0 1 0
49: 2 2 2 1 2 0 1 0
57: 0 0 3 3 0 2 2 1
65: 1 1 1 1 2 1 0 0
73: 1 0 1 1 1 1 3 3
81: 1 2 2 2 2 0 1 0
89: 1 1 0 1 0 3 2 2
97: 0 0 2 1 0 1 4 0
105: 3 2 0 2 5 0 4 3
113: 3 5 1 1 0 2 1 3
121: 1 3 2 2 3 2 6 3
129: 4 5 3 4 3 2 4 4
137: 6 6 6 3 6 8 8 4
145: 1 9 3 5 4 5 2 7
153: 12 5 9 2 5 7 5 11
161: 5 8 9 8 5 8 11 5
169: 5 6 7 6 6 7 7 5
177: 11 12 13 4 5 1 6 3
185: 5 4 1 1 1 0 2 0
193: 0 0 1 0 0 0 0 0
201: 0 0 0 1 0 0 0 0
209: 0 0 0 0 0 0 0 0
217: 0 0 0 0 1 0 0 0
225: 0 1 0 0 0 0 1 0
233: 0 0 0 0 0 0 0 0
241: 0 0 1 0 1 0 0 0
249: 0 3 1 0 0 0 0 0
257: 1 1 0 0 1 0 0 0
265: 0 0 1 1 1 2 1 1
273: 0 0 0 0 0 0 0 0
281: 0 0 2 1 2 0 0 2
289: 1 1 2 0 1 1 0 0
297: 0 0 0 1 0 1 1 0
305: 3 1 1 0 1 1 2 1
313: 1 0 1 1 2 2 3 2
321: 0 0 4 1 1 2 3 1
329: 1 2 0 1 0 1 3 4
337: 0 5 2 4 0 1 6 4
345: 4 2 0 1 2 1 2 6
353: 4 1 6 2 2 5 2 3
361: 3 6 3 5 1 1 3 3
0211
Channel Data Report 3/30/2018 11:10:39 AM Page 2
369: 6 9 8 2 3 3 5 7
Sample Title: 01
Channell------l-------1-------1-------1-------I-------I-------I-------I 377: 5 10 9 7 4 12 4 4
385: 6 9 7 4 5 4 12 10
393: 9 11 7 11 7 11 6 10
401: 6 7 9 8 4 8 8 5
409: 7 4 2 3 3 1 0 2
417: 4 2 1 3 0 0 2 5
425: 1 1 1 2 2 3 3 0
433: 1 4 3 1 1 2 1 1
441: 3 5 5 1 2 5 5 6
449: 4 1 1 0 3 5 4 4
457: 4 0 3 2 2 3 5 3
465: 2 5 6 3 3 3 1 4
473: 1 0 2 2 4 2 4 0
481: 1 3 1 4 1 4 1 0
489: 2 1 1 4 2 1 4 0
497: 2 0 1 0 2 0 1 3
505: 0 0 2 2 0 1 1 0
513: 0 0 1 1 0 1 1 2
521: 1 2 1 2 1 4 1 1
529: 0 1 1 0 0 0 0 0
537: 1 0 1 0 0 0 0 3
545: 1 1 3 0 0 0 1 1
553: 1 1 1 1 1 0 3 2
561: 1 1 3 3 1 0 0 1
569: 1 0 1 3 1 0 0 1
577: 0 2 0 4 2 4 2 2
585: 0 3 2 2 3 1 0 3
593: 2 1 2 2 3 3 5 6
601: 0 4 5 2 2 4 3 6
609: 5 6 4 6 3 6 6 8
617: 11 9 5 5 3 8 6 5
625: 8 5 7 7 7 10 9 5
633: 7 12 5 10 4 5 6 6
641: 8 12 7 4 11 10 6 14
649: 11 16 5 11 10 5 10 1
657: 3 3 3 2 1 0 0 0
665: 0 0 0 0 0 0 0 0
673: 0 0 1 0 0 0 0 0
681: 0 0 0 0 0 1 0 0
689: 0 0 0 0 1 1 1 0
697: 0 0 0 2 0 1 0 0
705: 1 1 0 0 0 1 1 0
713: 1 2 0 0 2 0 2 0
721: 1 0 1 1 1 0 2 3
729: 0 3 1 1 3 3 1 4
737: 3 1 0 1 1 2 1 1
745: 0 1 1 0 0 1 1 0
753: 0 0 0 0 0 0 0 0
761: 0 0 0 0 0 0 0 0
769: 0 0 0 0 0 1 0 0
777: 0 0 0 0 0 0 0 0
785: 0 0 0 0 0 0 0 0
793: 0 0 0 0 0 0 0 0
0212
Channel Data Report 3/30/2018 11:10:39 AM Page 3
801: 0 0 0 1 0 0 0 0
Sample Title: 01
Channell------l-------l-------l-------l-------l-------1-------1-------1 809: 1 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 0 0 0 0 0 0
833: 0 0 0 0 0 0 1 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 0 0
865: 1 1 0 0 0 0 0 0
873: 0 0 0 0 0 0 0 0
881: 0 0 0 0 0 0 0 0
889: 0 0 0 1 0 0 0 0
897: 0 0 0 0 1 0 0 0
905: 0 0 0 0 0 0 0 1
913: 0 1 0 1 0 0 0 0
921: 2 0 1 0 1 0 1 1
929: 1 1 1 1 0 0 0 0
937: 2 0 1 2 1 2 4 1
945: 0 0 1 0 0 1 1 0
953: 1 0 0 0 1 0 0 0
961: 0 0 0 0 0 0 0 0
969: 0 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 1 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0213
~!t'Apex-Alpha"' Sample Description: Spectrum File: Batch Identification:
BLANK \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002099
1803110A-TH Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Tracer Certificate: Tracer Quantity: Effective Efficiency:
02 Shelf 2 Th iso
Alpha_041 05026930A 91087 System Bkgd 211464
<not performed>
1. 000E+000 3/30/2018 3/30/2018
170.0
+/- 0.000E+000 liter 6:43:14 AM 8:10:27 AM
minutes 170.0 minutes
Th229 S TH-18A
0.0143
Counting Efficiency:
0.234 mL 0.1603 +/-0.1885 +/-0.8502 +/-
0.0033 on 2/16/2018 0.0775
9:34:24 AM
Chem. Recovery Factor:
Peak Match Tolerance:
Nuclide
TH-227 TH-228 TH-229 T TH-230 TH-232
Energy (MeV)
5.792 5.304 4.878 4.600 4.039
0.175 MeV
PEAK AREA REPORT
Net Pk Area
3.83 0.32
142.98 6.47
-0.23
Pk Area Error%
102.72 646.93
16.46 87.07
1605.4
Ambient Backgnd
0.17 0.68 1. 02 1. 53 3.23
Reagent Backgnd
0.00E+000 0.00E+000 0.00E+000 0.00E+000 0.00E+000
FWHM (keV)
3.0 3.0 5.9 3.0 3.0
T Tracer Peak used for Effective Efficiency
Nuclide
TH-227 TH-228 TH-229 TH-230 TH-232
Id Conf.
0. 983 0.953 1. 000 0.973 0. 991
NUCLIDE ANALYSIS RESULTS
Energy (keV)
5850.00* 5400.00* 4872.00* 4672.00* 3997.00*
Activity (pCi/liter )
6.49E-002 +!- 6.77E-002 5.29E-003 +!- 3.43E-002 2.38E+000 +/- 4.17E-001 l.07E-001 +!- 9.52E-002
-3.80E-003 +!- 6. llE-002
1t4S .3/3bf1
MDA (pCi/liter
7.08E-002 +/- l.24E-002 9.33E-002 +!- 1. 64E-002 l.05E-001 +/- l.84E-002 l.18E-001 +/- 2.07E-002 1. 50E-001 +!- 2.64E-002
0214
60
55
50
45
40
35 V> ...... s:::: :::I
8 30
25
20
15
10
5
0000209917.CNF
Live Time :10200.000 sec Real Time :10200.300 sec start: 1:3471.S(kev) stop : 1024:6544.G(kev) Acq. Start :Fri Mar 30 08:10:27 2018
0 [I I I I I j'" I ~ . ,, ., I I r ., .. :,·· .··· . ~
3500 I I ·- ,- ,, I I I l>A1 I \NI' !!\:\Ii!,, 1i,1J! ~ :::::. , . ,I ,,1 . II/iii il'i !r y ' I! ,_. ~ I',,,. I' "' I 1\ I i= I! I !I I, :q!, I
4000 4500 5000 Energy(kev)
5500 I I ! I I I I I
6000 6500
ROI Type: 1 ROI Type: 3
0215
Channel Data Report 3/30/2018 11:10:47 AM Page 1
******************************************************* ***** s p E C T R A L DAT A R E P O R T ***** *******************************************************
Sample Title: 02
Elapsed Live time: 10200 Elapsed Real Time: 10200
Channell------l-------l-------l-------l-------1-------1-------1-------I 1: 0 0 0 0 0 0 0 0
9: 0 0 0 0 0 0 0 0
17: 0 0 0 0 0 0 0 0
25: 0 0 0 0 0 0 0 0
33: 0 0 0 0 0 0 0 0
41: 0 0 0 0 0 0 0 0
49: 0 0 0 0 0 0 0 0
57: 0 0 0 0 0 0 0 0
65: 0 0 0 0 0 0 0 0
73: 0 0 0 0 0 0 0 0
81: 0 0 0 0 0 0 0 0
89: 0 0 0 0 0 0 0 0
97: 0 0 0 0 0 0 0 0
105: 0 0 0 0 0 0 0 0
113: 0 0 0 0 0 0 0 0
121: 0 0 0 0 0 0 0 0
129: 0 0 0 0 0 0 0 0
137: 0 0 0 0 0 0 0 0
145: 0 0 0 0 0 0 0 0
153: 0 0 0 0 0 0 0 0
161: 0 0 0 0 0 0 0 0
169: 0 0 0 0 0 0 0 0
177: 0 0 1 0 0 0 0 0
185: 0 0 0 0 0 1 0 0
193: 0 0 0 0 0 0 0 1
201: 0 0 0 0 0 0 0 0
209: 0 0 0 0 0 0 0 0
217: 0 0 0 0 0 0 0 0
225: 0 0 0 0 0 0 0 0
233: 0 0 0 0 0 0 0 0
241: 0 0 0 0 0 0 0 0
249: 0 0 0 0 0 0 0 0
257: 0 0 0 0 0 0 0 0
265: 0 0 0 0 0 0 0 0
273: 0 0 0 0 0 0 0 0
281: 0 0 0 0 0 0 0 0
289: 0 0 0 0 0 0 0 0
297: 0 0 0 0 0 0 0 0
305: 0 0 0 0 0 0 0 0
313: 0 0 0 0 0 0 0 0
321: 0 0 0 0 0 0 1 0
329: 0 0 0 0 0 0 0 0
337: 0 0 0 0 0 0 0 0
345: 0 0 0 0 0 0 0 0
353: 0 0 0 0 0 2 0 0
361: 0 1 0 0 0 0 0 0
0216
Channel Data Report 3/30/2018 11:10:47 AM Page 2
369: 0 0 0 0 0 0 0 0
Sample Title: 02
Channell------l-------1-------1-------1-------I-------I-------I-------I 377: 0 0 0 1 0 0 0 0
385: 0 0 0 0 0 0 0 0
393: 0 0 0 0 0 0 0 0
401: 1 0 0 0 0 0 0 0
409: 0 1 0 0 0 0 0 0
417: 1 0 0 0 0 0 0 0
425: 0 0 2 0 0 2 1 1
433: 2 1 1 0 0 1 0 1
441: 2 2 0 1 1 0 4 3
449: 5 4 1 2 2 6 3 3
457: 2 2 7 4 2 2 1 1
465: 2 1 2 3 0 4 3 4
473: 3 2 0 2 3 0 1 0
481: 1 3 3 0 1 2 1 1
489: 0 3 1 2 2 0 1 1
497: 0 2 0 0 1 0 0 0
505: 0 1 0 0 1 2 0 0
513: 1 1 2 0 0 0 0 3
521: 1 0 2 1 0 0 0 0
529: 0 0 1 1 0 0 0 0
537: 0 0 0 0 0 0 0 0
545: 0 0 1 0 0 0 0 0
553: 0 0 0 0 0 0 0 0
561: 0 0 0 0 0 0 0 0
569: 0 0 0 0 0 0 0 0
577: 0 0 0 0 0 0 0 0
585: 0 0 0 0 0 0 0 0
593: 0 0 0 0 0 0 0 0
601: 0 0 0 0 0 0 0 0
609: 0 0 1 0 0 0 0 0
617: 0 0 0 0 0 0 0 0
625: 0 0 0 0 0 0 0 0
633: 0 0 0 0 0 0 0 0
641: 0 0 0 0 0 0 0 0
649: 0 0 0 0 0 0 0 0
657: 0 0 0 0 0 0 0 0
665: 0 0 0 0 0 0 0 0
673: 0 0 0 0 0 0 0 0
681: 0 0 0 0 0 1 0 0
689: 0 0 0 0 0 0 0 0
697: 0 0 0 0 0 0 0 0
705: 0 0 0 0 0 0 0 0
713: 0 0 0 0 0 0 0 0
721: 0 0 0 0 0 0 0 0
729: 0 0 0 0 0 0 0 0
737: 1 0 0 0 0 0 0 0
745: 0 0 0 0 0 0 0 0
753: 0 0 0 0 0 0 0 0
761: 0 0 0 0 1 0 0 0
769: 0 0 0 0 1 1 0 0
777: 0 0 0 0 0 1 0 0
785: 0 0 0 0 0 0 0 0
793: 0 0 0 0 0 0 0 0
0217
Channel Data Report 3/30/2018 11:10:47 AM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 02
Channell------l-------l-------l-------l-------1-------1-------1-------I 809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 0 0 0 0 0 0
833: 0 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 0 0
865: 0 0 0 0 0 0 0 0
873: 0 0 0 0 0 0 0 0
881: 0 0 0 0 0 0 0 0
889: 0 0 0 0 0 0 0 0
897: 0 0 0 0 0 1 0 0
905: 0 0 0 0 0 0 0 0
913: 0 0 0 0 0 0 0 0
921: 0 0 0 0 0 0 0 0
929: 0 0 0 0 0 0 0 0
937: 0 0 0 0 0 0 1 0
945: 0 0 0 0 0 0 0 0
953: 0 0 0 0 0 0 0 0
961: 0 0 0 0 0 0 0 0
969: 0 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 0 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0218
¢t(A Al h TM ~~~~J-\pex- p a Sample Description: Spectrum File: Batch Identification:
OU-1-008 DUP \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002099
1803110A-TH
Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Tracer Certificate: Tracer Quantity: Effective Efficiency:
03 Shelf 2 Th iso
Alpha_042 05026930B 84185 System Bkgd 211465
<not performed>
5.000E-001 3/19/2018 3/30/2018
170.0
+/- 0.000E+000 liter 6:43:14 AM 8:10:29 AM
minutes 170.0 minutes
Th229 S TH-18A 0.231 mL 0.1649 +/- 0.0147
Counting Efficiency: 0.1722 +/- 0.0030 on 2/16/2018 0.9572 +/- 0.0867
9:34:23 AM
Chem. Recovery Factor:
Peak Match Tolerance:
Nuclide
TH-227 TH-228 TH-229 T TH-230 TH-232
Energy (MeV)
5.879 5.335 4.870 4.644 3.955
0.175 MeV
PEAK AREA REPORT
Net Pk Area
0.98 -1.19
145.64 4.98 0 .49
Pk Area Error%
294.85 180.60
16.33 97.79
416.98
Ambient Backgnd
1.02 1.19 1.36 1.02 0.51
Reagent Backgnd
0.00E+000 0.00E+000 0.00E+000 0.00E+000 0.00E+000
FWHM (keV)
3.0 0.0 3.4 3.0 3.0
T Tracer Peak used for Effective Efficiency
Nuclide
TH-227 TH-228 TH-229 TH-230 TH-232
Id Conf.
0.996 0.978 1.000 0. 996 0.991
NUCLIDE ANALYSIS RESULTS
Energy (keV)
5850.00* 5400.00* 4872.00* 4672.00* 3997.00*
Activity (pCi/liter )
3.23E-002 +/- 9.55E-002 -3.87E-002 +!- 7.02E-002
4.70E+000 +!- 8.20E-001 1.60E-001 +!- 1.59E-001 1.58E-002 +!- 6.57E-002
Af1 3/3o/(~
MDA (pCi/liter
2.08E-001 +/- 3.62E-002 2.14E-001 +!- 3.73E-002 2.21E-001 +!- 3.86E-002 2.03E-001 +!- 3.53E-002 1.69E-001 +!- 2.94E-002
0219
60
55
50
45
40
35 V)
-1-' s::: :::J
8 30
25
20
15
10
5 ~ = ~ ' cc l-
0000209932.CNF
Live Time :10200.000 sec Real Time :10200.300 sec Start: 1:3502. ?(kev) Stop : 1024:6565.S(kev) Acq. Start :Fri Mar 30 08:10:29 2018
' ,, I ' ' " I I ' ' 'l'I 'I" I~ ,I 11 I IA I I I A I I, I I I A I I I o I I I I ,I I I I <' Iii 11 1 I I
4000
ROI Type: 1
4500 5000 Energy(kev)
5500 6000 6500
ROI Type: 3
0220
Channel Data Report 3/30/2018 11:11:22 AM Page 1
******************************************************* ***** s P E C T R A L DAT A R E P O R T ***** *******************************************************
Sample Title: 03
Elapsed Live time: 10200 Elapsed Real Time: 10200
Channell------l-------1-------1-------1-------I-------I-------I-------I 1: 0 0 0 0 0 0 0 0
9 : 0 0 0 0 0 0 0 0
17: 0 0 0 0 0 0 0 0
25: 0 0 0 0 0 0 0 0
33: 0 0 0 0 0 0 0 0
41: 0 0 0 0 0 0 0 0
49: 0 0 0 0 0 0 0 0
57: 0 0 0 0 0 0 0 0
65: 0 0 0 0 0 0 0 0
73: 0 0 0 0 0 0 0 0
81: 0 0 0 0 0 0 0 0
89: 0 0 0 0 0 0 0 0
97: 0 0 0 0 0 0 0 0
105: 0 0 0 0 0 0 0 0
113: 0 0 0 0 0 0 0 0
121: 0 0 0 0 0 0 0 0
129: 0 0 0 0 0 0 0 0
137: 0 0 0 0 0 0 0 0
145: 0 0 0 0 0 0 0 1
153: 0 0 0 0 0 0 0 0
161: 0 0 0 0 0 0 0 0
169: 0 0 0 0 0 0 0 0
177: 0 0 0 0 0 0 0 0
185: 0 0 0 0 0 0 0 0
193: 0 0 0 0 0 0 0 0
201: 0 0 0 0 0 0 0 0
209: 0 0 0 0 0 0 0 0
217: 0 0 0 0 0 0 0 0
225: 0 0 0 0 0 0 0 0
233: 0 0 0 0 0 0 0 0
241: 0 0 0 0 0 0 0 0
249: 0 0 0 0 0 0 0 0
257: 0 0 0 0 0 0 0 0
265: 0 0 0 0 0 0 0 0
273: 0 0 0 0 0 0 0 0
281: 0 0 0 0 0 0 0 0
289: 0 0 0 0 0 0 0 0
297: 0 0 0 0 0 0 0 0
305: 0 0 0 0 0 0 0 0
313: 0 0 0 0 0 0 0 0
321: 0 0 0 0 0 0 0 0
329: 0 0 0 0 0 0 0 0
337: 0 0 0 0 0 0 0 0
345: 0 0 0 0 0 0 0 0
353: 0 0 0 0 0 0 0 1
361: 0 0 0 0 0 0 0 0
0221
Channel Data Report 3/30/2018 11:11:22 AM Page 2
369: 0 0 1 0 0 0 1 0
Sample Title: 03
Channell------l-------l-------l-------1-------1-------1-------I-------I 377: 0 0 0 0 0 0 0 0
385: 0 0 0 0 0 1 0 0
393: 0 0 0 1 0 0 0 0
401: 1 0 0 0 0 0 0 0
409: 0 0 0 0 0 2 0 1
417: 1 1 0 0 1 0 1 2
425: 1 0 2 1 3 2 0 2
433: 1 1 5 0 2 3 5 2
441: 5 5 3 1 3 4 3 2
449: 3 1 3 4 2 1 1 0
457: 3 2 3 3 5 2 1 1
465: 3 1 0 1 1 2 1 3
473: 1 1 0 1 0 1 0 0
481: 1 2 1 2 0 0 3 0
489: 2 0 2 1 1 1 1 1
497: 0 1 0 0 0 1 0 0
505: 0 0 1 0 1 1 1 1
513: 2 1 0 1 0 1 0 0
521: 0 0 0 0 1 0 0 0
529: 0 0 0 0 0 0 0 0
537: 0 0 0 0 0 0 0 0
545: 0 0 0 0 0 0 0 0
553: 0 0 0 0 0 0 0 0
561: 0 0 0 0 0 0 0 0
569: 0 0 1 0 0 0 0 0
577: 0 0 0 0 0 0 0 0
585: 0 0 0 0 0 0 0 0
593: 0 0 0 0 0 0 0 0
601: 0 0 0 0 0 0 0 0
609: 0 0 0 0 0 0 0 0
617: 0 0 0 0 0 0 0 0
625: 0 0 0 0 0 0 0 0
633: 0 0 0 0 0 0 0 0
641: 0 0 0 0 0 0 0 0
649: 0 0 0 0 0 0 0 0
657: 0 0 0 0 0 0 0 0
665: 0 0 0 0 0 0 0 0
673: 0 0 0 0 0 0 0 0
681: 0 0 0 0 0 0 0 0
689: 0 0 0 0 0 0 0 0
697: 0 0 0 0 0 0 0 0
705: 0 0 0 0 0 0 0 0
713: 0 0 1 0 0 0 0 0
721: 0 0 0 0 0 0 0 0
729: 0 0 0 0 0 0 0 0
737: 0 0 0 0 0 0 0 0
745: 0 0 0 0 0 0 0 0
753: 0 0 0 0 0 0 0 0
761: 0 0 0 0 0 0 0 0
769: 0 0 0 1 0 0 0 0
777: 0 0 0 0 0 0 0 0
785: 0 0 0 0 0 0 0 0
793: 0 0 0 0 0 0 0 0
0222
Channel Data Report 3/30/2018 11:11:22 AM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 03
Channell------l-------1-------1-------1-------I-------I-------I-------I 809: 0 0 0 0 0 0 0 0
817: 1 0 0 0 0 0 0 0
825: 0 0 0 0 0 0 0 0
833: 0 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 0 0
865: 0 0 0 0 0 0 0 0
873: 0 0 0 0 0 0 0 0
881: 0 0 0 0 0 0 0 0
889: 0 0 0 0 0 0 0 0
897: 0 0 0 0 0 0 0 0
905: 0 0 0 0 0 0 0 0
913: 0 0 0 0 0 0 0 0
921: 0 0 0 0 0 0 0 0
929: 0 0 0 0 0 0 0 0
937: 0 0 0 0 0 0 0 0
945: 0 0 0 0 0 0 0 1
953: 0 0 0 0 0 0 0 0
961: 0 0 0 0 0 0 0 0
969: 0 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 0 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0223
ct!,A Al h TM ~-~---1""\pex- p a Sample Description: Spectrum File: Batch Identification:
OU-1-008 \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002099
1803110A-TH Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Tracer Certificate: Tracer Quantity: Effective Efficiency:
04 Shelf 2 Th iso
Alpha_043 04026481A 91088 System Bkgd 211466
<not performed>
5.000E-001 3/19/2018 3/30/2018
170.0
+/- 0.000E+000 liter 6:43:14 AM 8:10:25 AM
minutes 170.0 minutes
Th229 S TH-18A 0.231 mL 0.1715 +/- 0.0150
Counting Efficiency: 0.1903 +/- 0.0033 on 2/16/2018 0.9010 +/- 0.0806
9:34:21 AM
Chem. Recovery Factor:
Peak Match Tolerance:
Nuclide
TH-227 TH-228 TH-229 T TH-230 TH-232
Energy (MeV)
5.840 5.325 4.860 4.662 3.955
0.175 MeV
PEAK AREA REPORT
Net Pk Area
3.30 0.11
150.96 9.15
-0.19
Pk Area Error%
136.59 3329.3 16.08 68.23
1131.1
Ambient Backgnd
1.70 2.89 2.04 0.85 1.19
Reagent Backgnd
0.00E+000 0.00E+000 0.00E+000 0.00E+000 0.00E+000
FWHM (keV)
6.0 3.0 9.2 3.0 3.0
T = Tracer Peak used for Effective Efficiency
Nuclide
TH-227 TH-228 TH-229 TH-230 TH-232
Id Conf.
0.999 0. 971 0.999 0.999 0.991
NUCLIDE ANALYSIS RESULTS
Energy (keV)
5850.00* 5400.00* 4872.00* 4672.00* 3997.00*
Activity (pCi/liter )
l.05E-001 +!- l.44E-001 3.44E-003 +/- l.14E-001 4.69E+000 +!- 8.06E-001 2.83E-001 +!- 1. 99E-001
-5.87E-003 +!- 6.64E-002
f4 3(so{r1
MDA (pCi/liter
2.33E-001 +/- 4.0lE-002 2.74E-001 +!- 4.70E-002 2.42E-001 +/- 4.16E-002 l.85E-001 +!- 3.19E-002 2.04E-001 +/- 3.50E-002
0224
60
55
50
45
40
35
0000209920.CNF
Live Time 10200.000 sec Real Ti me 10200. 300 sec start: 1 3497 .0(kev) stop : 1024 6579.9(kev) Acq. Start Fri Mar 30 08:10:25 2018
V) .µ C :::::s
8 30
25
20
15
10
5 = . "" f-
0 ' ~ ,, I ~
3500 ,u,,, ' , , ~ -~ /\ ,i, A
4000 4500
ROI Type: 1
5000 Energy(kev)
5500
ROI Type: 3
6000 6500
0225
Channel Data Report 3/30/2018 11:11:30 AM Page 1
******************************************************* ***** s p E C T R A L DAT A R E P O R T ***** *******************************************************
Sample Title: 04
Elapsed Live time: 10200 Elapsed Real Time: 10200
Channell------l-------l-------l-------l-------1-------1-------1-------I 1: 0 0 0 0 0 0 0 0
9 : 0 0 0 0 0 0 0 0
17: 0 0 0 0 0 0 0 0
25: 0 0 0 0 0 0 0 0
33: 0 0 0 0 0 0 0 0
41: 0 0 0 0 0 0 0 0
49: 0 0 0 0 0 0 0 0
57: 0 0 0 0 0 0 0 0
65: 0 0 0 0 0 0 0 0
73: 0 0 0 0 0 0 0 0
81: 0 0 0 0 0 0 0 0
89: 0 0 0 0 0 0 0 0
97: 0 0 0 0 0 0 0 0
105: 0 0 0 0 0 0 0 0
113: 0 0 0 0 0 0 0 0
121: 0 0 0 0 0 0 0 0
129: 0 0 0 0 0 0 0 0
137: 0 0 0 0 0 0 0 0
145: 0 0 0 0 0 0 0 0
153: 1 0 0 0 0 0 0 0
161: 0 0 0 0 0 0 0 0
169: 0 0 0 0 0 0 0 0
177: 0 0 0 0 0 0 0 0
185: 0 0 0 0 0 0 0 0
193: 0 0 0 0 0 0 0 0
201: 0 0 0 0 0 0 0 0
209: 0 0 0 0 0 0 0 0
217: 0 0 0 0 0 0 0 0
225: 0 0 0 0 0 0 0 0
233: 0 0 0 0 0 0 0 0
241: 0 0 0 0 0 0 0 0
249: 0 0 0 0 0 0 0 0
257: 0 0 0 0 0 0 0 0
265: 0 0 0 0 0 0 0 0
273: 0 0 0 0 0 0 0 0
281: 0 0 0 0 0 0 0 0
289: 0 0 0 0 0 0 0 0
297: 0 0 0 0 0 0 0 0
305: 0 0 0 0 0 0 0 0
313: 0 0 0 0 0 0 0 0
321: 0 0 0 0 0 0 0 0
329: 0 0 0 0 0 0 0 0
337: 0 0 0 0 0 0 0 0
345: 0 0 0 0 0 0 0 0
353: 0 0 0 0 0 0 0 0
361: 0 0 0 0 0 1 0 0
0226
Channel Data Report 3/30/2018 11:11:30 AM Page 2
369: 0 0 0 0 0 0 0 0
Sample Title: 04
Channell------l-------l-------l-------l-------1-------1-------1-------I 377: 1 0 0 1 0 0 0 1
385: 0 0 0 0 1 0 1 1
393: 0 0 2 0 0 0 0 0
401: 0 0 0 0 0 0 1 0
409: 1 0 0 0 0 2 1 0
417: 3 1 1 2 1 1 0 3
425: 3 1 2 4 0 2 1 2
433: 1 5 0 4 1 3 2 4
441: 3 7 5 4 1 3 6 3
449: 1 2 1 1 1 1 1 2
457: 4 0 3 4 1 2 3 2
465: 0 3 2 0 1 1 0 1
473: 1 0 0 1 2 1 1 2
481: 2 0 0 1 3 1 0 1
489: 1 0 0 0 0 0 1 1
497: 0 0 0 1 0 2 1 1
505: 2 1 0 0 2 1 0 1
513: 0 0 0 2 0 0 0 0
521: 0 0 0 0 0 0 0 0
529: 0 0 0 0 0 0 0 0
537: 0 0 0 0 0 0 0 0
545: 0 0 0 0 0 0 0 0
553: 0 0 0 0 0 0 0 0
561: 0 0 0 0 0 0 0 0
569: 0 0 0 0 0 0 0 0
577: 0 0 0 0 0 0 0 0
585: 0 0 0 1 0 0 0 0
593: 0 0 0 0 0 0 0 0
601: 0 0 0 0 0 0 0 0
609: 0 0 1 0 0 0 0 0
617: 0 0 0 0 0 0 0 1
625: 0 0 0 0 0 0 0 0
633: 0 0 0 0 0 0 0 0
641: 0 0 0 0 0 0 0 0
649: 0 0 0 0 0 0 0 0
657: 0 0 0 0 0 0 0 0
665: 0 0 0 0 0 0 0 0
673: 0 0 0 0 0 0 0 0
681: 0 0 0 0 0 0 0 0
689: 0 0 0 0 0 0 0 0
697: 0 0 0 0 0 0 0 0
705: 0 0 0 0 0 0 0 0
713: 0 0 0 0 0 0 0 0
721: 0 0 0 0 0 0 0 0
729: 0 0 0 0 0 0 0 0
737: 0 0 0 0 0 0 0 0
745: 0 0 0 0 0 0 0 0
753: 0 0 1 1 0 0 0 0
761: 0 0 0 0 0 0 1 0
769: 0 0 0 0 0 0 0 0
777: 0 1 0 0 0 0 0 0
785: 0 0 0 0 0 0 0 0
793: 0 0 0 0 0 0 0 0
0227
Channel Data Report 3/30/2018 11:11:30 AM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 04
Channell------l-------l-------l-------1-------1-------1-------I-------I 809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 0 0 0 0 0 0
833: 0 0 0 1 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 1 0
865: 0 0 0 0 0 0 0 0
873: 0 0 0 0 0 0 0 0
881: 0 0 0 0 0 1 0 0
889: 0 0 0 0 0 0 0 0
897: 0 0 0 0 0 0 0 0
905: 0 0 0 0 0 0 0 0
913: 0 0 0 0 0 0 0 0
921: 0 0 0 0 0 0 0 0
929: 0 0 0 0 0 0 0 0
937: 1 0 0 0 0 0 0 0
945: 0 0 0 0 0 0 0 0
953: 0 0 0 0 0 0 0 0
961: 0 0 0 0 0 0 0 0
969: 0 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 0 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0228
t-'age I OT ,:. 3/30/2018 5:55:22 AM
OA .<::;/ 11\A/\AARY REPORT .~., " . . -..- - ~ " ~ " .. "" . - ,. . - .. "". .
Review Of QA Results - Pulser Check
Date : 3/30/2018 Time : 5:55:22 AM
CHAMBER DEVICE PARAMETER FLAG DATE
Alpha 001 2lf ALL Not Done
Alpha 002 2lf ALL Not Done
Alpha 003 2lf ALL Passed 3/30/2018 5:03:13 AM
Alpha 004 2lf ALL Passed 3/30/2018 5:03:14 AM
Alpha 005 2lf ALL Not Done
Alpha 006 2lf ALL Not Done
Alpha 007 2lf ALL Not Done
Alpha 008 2lf ALL Not Done
Alpha 009 2lf ALL Not Done
Alpha 010 2lf ALL Passed 3/30/2018 5:03:15 AM
Alpha 011 2lf ALL Passed 3/30/2018 5:03:16 AM
Alpha 012 2lf ALL Passed 3/30/2018 5:03:17 AM
Alpha 013 2lf ALL Not Done
Alpha 014 2lf ALL Passed 3/30/2018 5:03:18 AM
Alpha 015 2lf ALL Not Done
Alpha 016 2lf ALL Not Done
Alpha 033 Alpha Analystl 00DC ALL Passed 3/30/2018 5:03:19 AM
Alpha 034 Alpha Analystl00DC ALL Passed 3/30/2018 5:03:21 AM
Alpha 035 Alpha Analystl 00DC ALL Passed 3/30/2018 5:03:22 AM
Alpha 036 Alpha Analystl 00DC ALL Passed 3/30/2018 5:03:24 AM
Alpha 037 Alpha AnalystlO0DC ALL Not Done
Alpha 038 Alpha Analystl00DC ALL Passed 3/30/2018 5:03:26 AM
Alpha 039 Alpha Analyst 1 00DC ALL Not Done
Alpha 040 Alpha Analvstl 00DC ALL Passed 3/30/2018 5:03:28 AM
Alpha 041 Alpha Analyst 1 00DC ALL Passed 3/30/2018 5:03:30 AM
Alpha 042 Alpha Analystl00DC ALL Passed 3/30/2018 5:03:32 AM
Alpha 043 Alpha Analystl00DC ALL Passed 3/30/2018 5:03:34 AM
Alpha 044 Alpha Analystl00DC ALL Passed 3/30/2018 5:03:37 AM
Alpha 045 Alpha Analystl00DC ALL Passed 3/30/2018 5:03:39 AM
Alpha 046 Alpha Analystl 00DC ALL Passed 3/30/2018 5:03:42 AM
Alpha 047 Alpha Analystl 00DC ALL Not Done
Alpha 048 Alpha Analyst 1 00DC ALL Not Done
Alpha 049 Alpha Analvstl 00DC ALL Passed 3/30/2018 5:03:44 AM
Alpha 050 Alpha Analystl00DC ALL Passed 3/30/2018 5:03:47 AM
Alpha 051 Alpha Analystl 00DC ALL Passed 3/30/2018 5:03:49 AM
Aloha 052 Alpha Analystl00DC ALL Passed 3/30/2018 5:03:52 AM
Alpha 053 Alpha Analystl 00DC ALL Passed 3/30/2018 5:03:54 AM
Alpha 054 Alpha Analystl 00DC ALL Passed 3/30/2018 5:03:57 AM
Alpha 055 Alpha Analystl00DC ALL Passed 3/30/2018 5:03:59 AM
Alpha 056 Alpha Analystl00DC ALL Passed 3/30/2018 5:04:02 AM
Alpha 057 Alpha Analystl00DC ALL Passed 3/30/2018 5:04:05 AM
Alpha 058 Alpha Analystl 00DC ALL Passed 3/30/2018 5:04:08 AM
0229
Page 2 of 2 Kev1ew ot UA Kesu1ts - 1-'Ulser 1_.;necK 3/30/2018 5:55:22 AM
CHAMBER DEVICE PARAMETER FLAG DATE
Aloha 059 Aloha AnalvstlO0DC ALL Not Done
Aloha 060 Aloha Analvstl 00DC ALL Not Done
APPROVED BY:
APPROVAL DATE:'<) /30/175
0230
Library Listing Report 6/12/12 12:16:29 PM Page 1
*************************************************************************
***** L I B R A R Y L I S T I N G R E P O R T *****
*************************************************************************
Nuclide Library Title: Thorium
Nuclide Library Description: Th-227,-228,-229,-230,-232
Nuclide Half-Life Energy Energy Yield Yield
Name (Seconds) (keV ) Uncert. (keV ( % ) Uncert. (Abs.+-)
TH-227 6.873E+008 5850.000* 0.000 97.5000 0.0000
TH-228 6.034E+007 5400.000* 0.000 99.9400 0.0000
TH-229 2.487E+Oll 4872.000* 0.000 99.5200 0,0000
TH-230 2.379E+012 4672.000* 0.000 99.8200 0.0000
TH-232 4.434E+017 3997.000* 0.000 100.0000 0.0000
* ::::: key line
TOTALS: 5 Nuclides 5 Energy Lines
0231
SECTION XI
ANALYTICAL DAT A (RADIUM-226)
0232
Eberline Services Oak Ridge Laboratory Analysis Sheet
Work Order 18-03110
Analysis Code ~_Ra226··~ J
Run 1 Date Received 3/23/2018
Lab Deadline 4/12/2018
Client I AMO Environmental Decisions
Project WESTLAKE
Report Level 4
Activity Units pCi
Aliquot Units
Matrix WA
Method EPA 903.0 Modified
Instrument Type Alpha Spectroscopy
Radiometric Tracer Ba-133
Radiometric Sol# Ba-Ga
Tracer Act (dpm/g) 489.45
Carrier
Carrier Cone (mg/ml)
I I
Internal i Sample Fraction Desc
01 LCS
02 MBL
03 DUP
04 DO
I
18-03110 Ra226 Run 1
Client ID
LCS
BLANK
OU-1-008
OU-1-008
• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. A Indicates estimated SAF value.
•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Login CPM
38
38
i
I
Printed: 4/2/2018 3:54 PM Page 1 of 3
Sample Sample Date Aliquot
03/23/18 00:00 1.0000E+00
03/23/18 00:00 1.0000E+00 i
03/19/18 18:02 1.0000E+00
03/19/18 18:02 1.0000E+00
:
i
0233
Eberline Services Oak Ridge Laboratory Analysis Sheet
Tracer Internal I Sample Fraction Desc Aliquot(g)
01 LCS 1.0027
02 MBL 1.0065
03 DUP 1.0011
04 DO 1.0043
Tracer Total ACT(dpm)
490.8
492.6
490.0
491.6
Radiometric Tracer (pC1)
297.0
339.0
352.0
277.0
18-03110 Ra226 Run 1
Radiometric I Grav Carrier I Grav Filter % Rec Added (ml) Tare (g)
134.35 0.0210
152.77 0.0210
159.48 0.0210
125.10 0.0215
I Grav Filter Final (g)
0.0311
0.0312
0.0272
0.0265
i
I
* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. "Indicates estimated SAF value.
- Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
i Grav Filter I Grav Net(g) %Rec
0.0101
0.0102
0.0062
0.0050
I
Printed: 41212018 3:54 PM Page 2 of 3
Mean SAF I
SAF %Rec 1* I 2*
I
110.00 3.oo" I 1.00
110.00 3.00" 1.00
110.00 2.23 1.00
110.00 1.71 1.00
0234
Eberline Services Oak Ridge Laboratory Analysis Sheet
Internal Sample Fraction Desc
01 LCS
02 MBL
03 DUP
04 DO
Rough Prep Rough Prep
Date By
i
I Prep I
I Date
I 03128118 08:31 I
03/28/18 08:31
03/28/18 08:31
03/28/18 08:31
18-03110 Ra226 Run 1
Prep By
JHARVEY
JHARVEY
JHARVEY
JHARVEY
I SeptO Date/Time
I
04/02/18 14:31
04/02/18 14:31
04/02/18 14:31
04/02/18 14:31
• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. "Indicates estimated SAF value.
** Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
I Sep to I By
I
EBAILEY
EBAILEY
EBAILEY
EBAILEY
I
Sep t1
Printed: 4/2/2018 3:54 PM Page 3 of 3
Sep t1 I Date/Time By I
0235
Eberline Analytical Oak Ridge Laboratory
~ Lab I Nuclide
Fraction
01 RA-226
i:: :, a::
.g 8 ,!!! ~ iii i:: <:(
~I
"""""
<D N N ns 0::
"' C 0
.!!? (.) Q)
C ni -C Q)
E C 0 ... > C w 0 :ii: <(
02 RA-226
03 RA-226
04 RA-226
[ Sample
1 Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-0311 0-Ra226-1
Client
I Activity
Results I Error Estimate MDA Identification Units
LCS pCi/1 9.91E+00 1.37E+00 4.41E-01
BLANK pCi/I 2.23E-01 2.41E-01 3.62E-01
OU-1-008 pCi/I 1.19E-01 1.54E-01 2.44E-01
OU-1-008 pCi/I 1.47E-01 1.29E-01 1.SSE-01
LCS LCS
Known ¾R
1.00E+01 98.94
Printed: 4/3/2018 7:07 AM Page 1 of 3
LCS
I RPO MDA Blank
Flag Flag Flag Flag
OK OK
OK OK
NA OK
OK
0236
Eberline Analytical Oak Ridge Laboratory
,: Lab Nuclide
Fraction
01 RA-226
C: ~ 0::
.g 8 .!(!
~ cii C: q;
~I
~
(0 N N CG ~
U) C:
.!2 U)
·o a, C ltl -C: a, E C:
_g > C: w 0 ~ <(
02 RA-226
03 RA-226
04 RA-226
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-0311 0-Ra226-1
Sample Sample Radiometric Grav Mean
Date Aliquot %Rec %Rec %Rec
03/23/18 00:00 1.00E+00 100.00 0.00 110.00
03/23/18 00:00 1.00E+00 100.00 0.00 110.00
03/19/18 18:02 1.00E+00 100.00 0.00 110.00
03/19/18 18:02 1.00E+00 100.00 0.00 110.00
SAF
Printed: 4/3/2018 7:07 AM Page 2 of 3
SeptO Sept1
DatefTime DatefTime
4/2/2018 14:31
4/2/2018 14:31
4/2/2018 14:31
4/2/2018 14:31
0237
Eberline Analytical Oak Ridge Laboratory
( Lab Nuclide Fraction
01 RA-226
~
.g 0 0 -!!! ~ c\i C: Cl:
~I
~
(0 N N ca ~
1/) C .2 1/)
·c:; Q)
C ns -C Q)
E C 0 ... ·:,; C w 0 :i1!E <(
02 RA-226
03 RA-226
04 RA-226
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-0311 0-Ra226-1
Counting I Halflife
I Count
1
Detect Carrier Counts DatefTime (days) Time
04/02/18 16:08 A_Spec Alpha_040 170 2.19 E+02
04/02/1816:08 A_Spec Alpha_041 170 5.28 E+00
04/02/18 16:08 A_Spec Alpha_042 170 3.47 E+00
04/02/18 16:08 A_Spec Alpha_044 170 5.98 E+00
Bkg CPM
2.30 E-02
1.60 E-02
9.00 E-03
6.00 E-03
Printed: 4/3/2018 7:07 AM Page 3 of 3
Eff
17.6
18.8
17.2
18.4
0238
Count Room Report
Client: AMO Environmental Decisio
.~
-~1 I
;fl Sample [ Internal Client
Fraction Desc ID
01 LCS LCS
02 MBL BLANK
03 DUP OU-1-008
04 DO ' OU-1-008
I
18-0311 0-Ra226-1 (pCi/1) in WA
Tracer ID: Ba-6a
I Sample Sample Tracer
Date Aliquot Aliquot(g)
03/23/18 00:00 1.0000 1.0027
03/23/18 00:00 1.0000 1.0065
03/19/18 18:02 1.0000 1.0011
03/19/18 18:02 1.0000 1.0043
Tracer Radiometric
ACT(dpm) Tracer (pCi)
490.7715 297.0000
492.6314 339.0000
489.9884 352.0000
491.5546 277.0000
Printed: 4/2/2018 3:54 PM Page 1 of 1
I I
I I Radiometric i SAF SAF
%Rec I 1* I 2*
I
134.35 3.00" 1.00
152.77 3.00" 1.00
159.48 2.23 1.00
125.10 1.71 1.00
i
I
0239
Eberline Analytical Oak Ridge Laboratory
Isotope So/# Activity dpmlg
Solution Date
Ra-226 Ra-Sb 43. 980 I 3/28/2018
Tracers i Activity
fraction Isotope So/# dpm/g
01 Ba-133 Ba-Ga 489.450
02 Ba-133 Ba-Ga 489.450
03 Ba-133 Ba-Ga i 489.450
04 Ba-133 Ba-Ga 489.450
I
Version 2.0 08/99
i !
Approx Addition
0.500
Solution Date
3/28/2018
3/28/2018
3/28/2018
3/28/2018
Spike and Tracer Worksheet
Analysis Code
Ra226 LCS
Volume Used{g)
0.5056
Volume Used(g)
1.0027
1.0065
1.0011
1.0043
I !
MS Volume Used (g)
Approx Addition
2.0700
2.0700
2.0700
2.0700
Date
3/28/2018 8:28
LCSD l MSD Volume l Volume Used{g) Used(g)
Technician
JHARVEY
T LCS --
MS
l Known Error Added Error pCi Estimate pCi Estimate
10.02 0.461 0.00 0.000
Balance Printer Tapes
Tracer
Page 1 of 1 Printed: 3/28/2018 8:31 AM
Technician Initials Witness Initials
-i:cso MSD Known
i Error Added Error
pCi Estimate pCi Estimate
o ool 0.000 0.00 0.000
LCS
Matrix Spike
0240
Lab
Eberline Analytical Oak Ridge Laboratory
AMO Environmental Decisions
Fraction Client ID
01 LCS
02 BLANK
03 OU-1-008
04 OU-1-008
Comments
Sample
Type
LCS
MBL
DUP
DO
Aliquot Worksheet
Analysis Code Rpt Units Lab Deadline
Ra226 liters 4/12/2018
Muffle Data Dilution Data Aliquot Data Ratio
Post/Pre No of Dils Oil Factor Ratio Aliquot Net Equiv
1.0000E+OO 1.0000E+OO
1.0000E+OO 1.0000E+OO
1.0000E+OO 1.0000E+OO
1.0000E+OO 1.0000E+OO
Technician: s::Jl \ a~'Wd •aIB ~
Technician
JHARVEY
MS Aliquot Data
Printed: 3/28/2018 9:26 AM Page 1 of 1
H-3 Solids Only
Aliquot Net Equiv water AaaejH3-D1st-
(ml) Aliq I
i
I
I
i
i
0241
Eberline Analytical - Oak Ridge Version 1.1 10/2015
Work Order
18-03110
TRetec AMO Environmental Decisions
Fraction Client ID
01 LCS
02 BLANK
03 DUP
04 OU-1-008
Technician: w&
Gravimetric Worksheet
-Sample
Type
LCS
MBL
DUP
DO
Analysis Code
Ra226
Carrier Data
Gravimetric Carrier
Filter Data
Carrier Added Filter Tare Filter Final
(ml) (g) (g)
0.0210 0.0311
0.0210 0.0312
0.0210 0.0272
0.0215 0.0265
Date: _:J_, 2_ / \8
I
Carrier Cone (mg/ml)
Filter Net (g)
0.0101
0.0102
0.0062
0.0050
Printed: 4/2/2018 3:05 PM Page 1 of 1
Technician
EBAILEY
Gravimetric %
Recovery
0242
~-~.,Apex-A Ip ha™ Sample Description: Spectrum File: Batch Identification:
SPIKE \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002100
1803110A-RA
Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Generic Mult. Factor: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Chem. Recovery Factor:
01 Shelf 2 Ra
Alpha_040 06027396B 91135 System Bkgd 211967
<not performed>
l.000E+000 +/- 0.000E+000 liter
3.000E+000 4/2/2018 4/2/2018
170.0
Generic Div. Factor: 3:20:11 PM 4:08:19 PM
minutes 170.0 minutes
1.0000 +/- 0.0000
l.000E+000
Counting Efficiency: 0.1757 +/- 0.0031 on 2/16/2018
0.1757 +/- 0.0031 9:34:27 AM
Effective Efficiency:
Control Certificate Name: Ra226 Ra-5b
Chem. Recov. of Control: RA-226 0.329818 +/- 0.025263
Peak Match Tolerance: 0.350 MeV
Nuclide
RA-224 RA-226
Nuclide
RA-224 RA-226
Energy (MeV)
Id Con£.
5.478 4.593
PEAK AREA REPORT
Net Pk Area
7.64 219.09
Pk Area Error%
77.95 13.38
Ambient Backgnd
1. 36 3.91
NUCLIDE ANALYSIS RESULTS
Energy (keV)
Activity (pCi/liter )
0.945 0.953
5685.50* 4785.00*
3.63E-001 +/- 2.84E-001 9.91E+000 +/- l.37E+000
Reagent Backgnd
0.00E+000 0.00E+000
FWHM (keV)
MDA
3.0 3.8
(pCi/liter
3.26E-001 +/- l.12E-002 4.41E-001 +/- l.51E-002
ft(P 4(3/18
0243
V) ...... C: ::::s
60
55
50
45
40
35
8 30
25
20
15
10
5
0 "'I'll 11111111111111111111
3500
ROI Type: 1
4000 4500
0000210090.CNF
5000 Energy(kev)
5500 :J
Live Time :10200.000 sec Real Time :10200.300 sec start: 1:3473.G(kev) stop : 1024:6542.9(kev) Acq. Start :Mon Apr 02 16:08:19 2018
6000 6500
0244
Channel Data Report 4/3/2018 5:49:39 AM Page 1
*******************************************************
***** s p E C T R A L DAT A R E P O R T *****
*******************************************************
Sample Title: 01
Elapsed Live time: 10200
Elapsed Real Time: 10200
Channell------l-------l-------l-------1-------1-------1-------I-------I
1: 1 1 2 0 3 1 1 0
9 : 1 4 0 1 3 1 1 1
17: 0 0 1 5 1 1 1 1
25: 0 0 1 0 0 1 1 1
33: 1 0 2 1 3 0 2 4
41: 0 0 1 1 2 1 0 1
49: 1 0 4 0 1 0 2 1
57: 1 1 2 0 1 2 0 1
65: 2 1 1 2 0 1 0 3
73: 2 1 1 0 2 1 2 2
81: 1 2 0 0 1 2 0 1
89: 1 2 2 1 4 1 1 3
97: 2 0 2 1 3 1 1 3
105: 1 1 2 0 3 1 4 1
113: 0 3 0 0 1 0 1 0
121: 0 2 0 1 1 2 0 1
129: 1 2 2 1 1 4 1 3
137: 0 0 0 0 0 0 1 1
145: 1 2 3 2 3 0 3 1
153: 3 1 1 1 1 3 2 3
161: 0 0 2 2 1 4 4 1
169: 0 0 1 2 0 1 0 2
177: 4 1 2 0 2 0 0 2
185: 2 1 1 3 5 2 2 1
193: 3 4 3 0 2 1 0 0
201: 0 4 0 1 0 2 0 6
209: 2 2 0 1 0 1 1 1
217: 4 2 1 3 3 1 2 4
225: 0 2 3 1 1 1 2 2
233: 0 4 0 3 1 0 2 2
241: 0 4 1 1 0 1 1 0
249: 1 3 1 3 0 3 0 0
257: 3 0 0 1 0 5 0 1
265: 2 0 0 0 4 3 1 0
273: 0 2 3 1 2 0 1 1
281: 2 5 1 1 2 1 2 1
289: 0 2 1 1 2 1 1 1
297: 2 2 2 0 1 3 1 1
305: 2 1 3 1 1 0 1 2
313: 1 1 2 2 2 0 1 3
321: 2 4 2 1 1 2 1 2
329: 1 0 2 3 1 2 0 2
337: 2 0 3 0 1 1 1 1
345: 2 0 3 2 2 0 0 3
353: 1 1 4 1 2 1 2 2
361: 1 1 3 3 3 2 1 0
0245
Channel Data Report 4/3/2018 5:49:39 AM Page 2
369: 0 1 0 3 3 0 0 3
Sample Title: 01
Channelj------l-------l-------l-------l-------1-------1-------1-------I
377: 1 4 1 3 2 2 3 0
385: 1 1 1 0 1 1 3 1
393: 2 1 1 2 0 2 0 1
401: 1 1 1 2 1 2 0 3
409: 1 1 1 1 4 1 3 1
417: 1 4 0 3 2 2 3 4
425: 1 1 1 3 4 1 5 1
433: 1 2 1 2 0 2 0 0
441: 1 3 0 2 1 0 0 0
449: 0 0 0 0 0 0 0 2
457: 1 0 0 0 0 0 0 0
465: 0 0 0 1 0 0 0 0
473: 0 0 0 1 0 0 0 0
481: 0 0 0 0 0 0 0 0
489: 0 0 0 0 0 0 0 1
497: 0 0 0 0 0 0 0 0
505: 0 0 0 0 0 0 0 0
513: 1 0 0 0 0 0 0 0
521: 0 1 0 0 0 0 0 0
529: 0 0 0 1 0 0 0 0
537: 0 0 2 0 0 0 0 0
545: 0 0 0 0 0 0 0 0
553: 0 0 0 0 0 0 0 0
561: 1 0 0 0 0 0 0 0
569: 0 0 0 0 0 0 0 0
577: 0 0 0 0 0 0 0 0
585: 0 0 1 0 0 0 0 1
593: 0 0 0 0 0 0 0 1
601: 0 0 0 0 0 0 0 0
609: 0 0 0 0 1 0 0 1
617: 0 0 0 0 1 0 0 0
625: 1 0 0 0 0 0 0 0
633: 0 1 0 0 0 0 0 0
641: 1 0 0 1 0 0 0 0
649: 0 0 0 0 0 0 0 1
657: 0 0 1 0 0 0 0 0
665: 0 1 0 0 0 0 0 0
673: 0 0 0 0 0 0 0 0
681: 0 0 0 0 0 1 0 0
689: 0 0 0 0 0 0 0 0
697: 0 0 0 0 0 0 0 0
705: 0 0 0 0 0 0 0 0
713: 0 0 0 1 0 0 0 1
721: 0 0 0 0 0 0 0 0
729: 0 0 0 0 0 0 0 0
737: 0 0 0 0 0 0 0 0
745: 0 0 0 0 0 0 0 0
753: 0 0 0 0 0 0 0 0
761: 0 0 0 0 0 0 0 1
769: 0 0 0 0 0 0 0 0
777: 0 0 0 0 0 0 0 0
785: 0 0 1 0 0 0 0 0
793: 0 0 0 0 0 1 0 0
0246
Channel Data Report 4/3/2018 5:49:39 AM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 01
Channell------l-------l-------l-------l-------1-------1-------1-------I 809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 0 0 0 0 0 0
833: 0 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 0 1
865: 0 0 0 0 0 0 0 1
873: 0 0 0 0 0 0 0 0
881: 0 0 0 0 0 0 0 0
889: 0 0 0 0 0 0 0 0
897: 0 0 0 0 0 0 0 0
905: 0 0 0 0 0 0 0 0
913: 0 0 0 0 0 0 0 0
921: 0 0 0 0 0 0 0 0
929: 0 0 0 0 0 0 0 0
937: 0 0 0 0 0 0 0 0
945: 1 0 0 0 0 0 0 0
953: 0 0 0 0 0 0 0 0
961: 0 0 0 0 0 0 0 0
969: 0 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 0 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0247
cfJ,A Al h TM ~~~---J-\pex- p a Sample Description: Spectrum File: Batch Identification: Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Generic Mult. Factor: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Chem. Recovery Factor: Counting Efficiency: Effective Efficiency:
Peak Match Tolerance:
Nuclide
RA-224 RA-226
Energy (MeV)
5.689 4.510
BLANK \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002100
1803110A-RA 02 Shelf 2 Ra
Alpha_041 05026930A 91087 System Bkgd 211968
<not performed>
1.000E+000 +/- 0.000E+000 liter
3.000E+000 4/2/2018 4/2/2018
170.0
Generic Div. Factor: 3:20:11 PM 4:08:15 PM
minutes 170.0 minutes
0.0000
1.000E+000
1. 0000 +/-0 .1885 +/-0.1885 +/-
0.0033 on 2/16/2018 0.0033
9:34:24 AM
0.350 MeV
PEAK AREA REPORT
Net Pk Area
0.15 5.28
Pk Area Error%
1397.8 107.99
Ambient Backgnd
0.85 2.72
NUCLIDE ANALYSIS RESULTS
Reagent Backgnd
0.00E+000 0.00E+000
FWHM (keV)
3.0 3.0
Nuclide Id
Conf. Energy (keV)
Activity (pCi/liter )
MDA (pci/liter
RA-224 RA-226
1.000 0.906
5685.50* 4785.00*
6.65E-003 +/- 9.30E-002 2.23E-001 +/- 2.41E-001
2.65E-001 +/- 9.04E-003 3.62E-001 +/- 1.23E-002
0248
60
55
50
45
40
35 V) ...., C :::s
8 30
25
20
15
10
5
0 I
3500
ROI Type: 1
1 Lill __ /'.
4000 4500
0000210088.CNF
5000 Energy(kev)
5500
Live Time :10200.000 sec Real Time :10200.200 sec Start: l:3471.8(keV) Stop : 1024:6544.G(kev) Acq. Start : Mon Apr 02 16: 08: 15 2018
.... ~ ~ ;;\;
6000 6500
0249
Channel Data Report 4/3/2018 5:49:46 AM Page 1
******************************************************* ***** s p E C T R A L DAT A R E P O R T ***** *******************************************************
Sample Title: 02
Elapsed Live time: 10200 Elapsed Real Time: 10200
Channell------l-------l-------1-------1-------1-------I-------I-------I
1: 0 0 0 0 0 0 0 0
9 : 0 0 0 0 0 0 0 0
17: 0 0 0 0 0 0 0 0
25: 0 0 0 0 0 0 0 0
33: 0 0 0 0 0 0 0 0
41: 0 0 0 0 0 0 0 2
49: 0 0 0 0 0 0 0 0
57: 1 0 0 0 0 0 0 0
65: 0 0 0 0 0 0 0 0
73: 0 0 0 0 0 0 0 0
81: 0 0 0 0 0 0 0 0
89: 0 0 0 0 0 0 0 0
97: 0 0 0 0 0 0 0 0
105: 0 0 0 0 0 0 0 0
113: 0 1 0 0 0 0 0 0
121: 0 0 0 0 0 0 0 0
129: 0 0 0 0 0 0 0 0
137: 0 0 0 0 0 0 0 0
145: 0 0 0 0 0 0 0 0
153: 0 0 0 0 0 0 0 0
161: 0 0 0 0 0 0 0 0
169: 0 0 0 0 0 0 0 0
177: 0 0 0 0 0 0 0 0
185: 0 0 0 0 0 0 1 0
193: 0 0 0 1 0 0 0 0
201: 0 0 0 0 0 0 1 1
209: 0 0 0 1 1 0 0 0
217: 1 0 0 0 0 0 0 0
225: 0 0 0 0 0 0 0 0
233: 0 0 0 0 0 0 0 0
241: 0 0 0 0 0 0 0 0
249: 1 0 0 0 0 0 0 0
257: 0 1 0 0 0 0 0 0
265: 0 0 0 0 0 0 0 0
273: 0 0 0 0 0 0 0 0
281: 0 0 0 0 0 0 0 0
289: 0 0 0 0 0 0 0 0
297: 0 0 0 0 0 0 0 0
305: 0 0 0 0 1 0 0 0
313: 0 0 1 0 0 0 0 0
321: 0 0 0 0 0 0 0 0
329: 0 0 0 0 0 0 1 0
337: 0 0 0 1 1 0 0 0
345: 0 0 0 0 0 0 0 0
353: 0 0 0 0 0 0 0 0
361: 0 0 0 1 0 0 0 0
0250
Channel Data Report 4/3/2018 5:49:46 AM Page 2
369: 0 0 0 0 0 0 0 1
Sample Title: 02
Channell------l-------l-------l-------1-------1-------1-------I-------I
377: 0 0 0 0 0 0 0 0
385: 0 0 0 0 0 0 0 1
393: 0 0 0 0 0 0 0 0
401: 0 0 0 0 0 0 0 0
409: 0 0 0 0 0 0 0 0
417: 0 0 0 0 0 0 0 0
425: 0 0 0 0 0 0 0 0
433: 0 0 0 0 0 0 0 0
441: 0 0 0 0 0 0 0 0
449: 0 0 0 0 0 0 2 0
457: 0 0 0 0 0 0 0 0
465: 0 0 0 0 0 0 0 0
473: 0 0 0 0 0 0 0 0
481: 0 0 0 0 0 0 0 0
489: 0 0 0 0 0 0 0 0
497: 0 0 0 0 1 0 0 0
505: 0 0 0 0 1 0 0 0
513: 0 1 0 0 1 0 0 0
521: 0 0 0 0 0 0 0 0
529: 0 0 0 0 0 0 0 0
537: 1 0 0 0 0 0 0 0
545: 1 0 0 0 0 1 0 0
553: 0 0 0 0 0 0 0 0
561: 0 0 0 1 0 0 0 0
569: 0 1 0 0 0 0 1 0
577: 1 0 0 0 0 0 0 0
585: 0 0 0 0 0 0 0 0
593: 1 0 0 0 0 0 0 0
601: 1 0 1 0 0 0 0 0
609: 0 0 0 0 0 0 0 0
617: 0 0 0 0 0 0 0 0
625: 0 0 0 0 0 0 0 0
633: 0 0 0 0 0 0 0 0
641: 0 0 0 0 0 0 0 0
649: 0 0 0 0 0 0 0 0
657: 0 0 0 0 0 0 0 0
665: 0 0 0 0 0 0 0 0
673: 0 0 0 0 0 0 0 0
681: 0 0 0 0 0 0 0 0
689: 0 0 0 0 0 0 0 0
697: 0 0 0 0 0 0 0 0
705: 0 0 0 0 0 0 0 0
713: 0 0 0 0 0 0 0 0
721: 0 0 0 0 0 0 0 0
729: 0 0 0 0 0 0 0 0
737: 0 0 1 0 0 0 0 0
745: 0 0 0 0 0 0 0 0
753: 0 0 0 0 0 0 0 0
761: 0 0 0 0 0 0 0 0
769: 0 0 0 0 0 0 0 0
777: 0 0 0 0 0 0 0 0
785: 0 0 0 0 0 0 0 0
793: 0 0 0 0 0 0 0 0
0251
Channel Data Report 4/3/2018 5:49:46 AM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 02
Channell------l-------l-------l-------l-------1-------1-------1-------I 0
809: 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 0 0 0 0 0 0
833: 0 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 0 0
865: 0 0 0 0 0 0 0 0
873: 0 0 0 0 0 0 0 0
881: 0 0 0 0 0 0 0 0
889: 0 0 0 0 0 0 0 0
897: 0 0 0 0 0 0 0 0
905: 0 0 0 0 0 0 0 0
913: 0 0 0 0 0 0 0 0
921: 0 0 0 0 0 0 0 0
929: 0 0 0 0 0 0 0 0
937: 0 0 0 0 0 0 0 0
945: 0 0 0 0 0 0 0 0
953: 0 0 0 0 0 0 0 0
961: 0 0 0 0 0 0 0 0
969: 0 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 0 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0252
c!!;'A Al h TM --=='J-\pex- p a Sample Description: Spectrum File: Batch Identification: Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Generic Mult. Factor: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Chem. Recovery Factor: Counting Efficiency: Effective Efficiency:
Peak Match Tolerance:
Nuclide
RA-224 RA-226
Energy (MeV)
5.493 4. 611
OU-1-008 DUP \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002100
1803110A-RA 03 Shelf 2 Ra
Alpha_042 05026930B 84185 System Bkgd 211969
<not performed>
l.000E+000 +/- 0.000E+000 liter
2.230E+000 4/19/2018 4/2/2018
170.0
Generic Div. Factor: 3:20:11 PM 4:08:17 PM
minutes 170.0 minutes
0.0000
l.000E+000
1. 0000 +/-0 .1722 +/-0.1722 +/-
0.0030 on 2/16/2018 0.0030
9:34:23 AM
0.350 MeV
PEAK AREA REPORT
Net Pk Area
2.15 3.47
Pk Area Error%
161.66 129.55
Ambient Backgnd
0.85 1. 53
NUCLIDE ANALYSIS RESULTS
Reagent Backgnd
0.00E+000 0.00E+000
FWHM (keV)
3.0 3.0
Nuclide Id
Conf. Energy (keV)
Activity (pCi/liter )
MDA (pCi/liter
RA-224 RA-226
0.953 0. 961
5685.50* 4785.00*
7.71E-002 +/- l.25E-001 l.19E-001 +/- l.54E-001
2.15E-001 +/- 7.40E-003 2.44E-001 +/- 8.39E-003
0253
60
55
50
45
40
35 V)
-1-' C: :::s
8 30
25
20
15
10
5
0 I
4000
ROI Type: 1
N,
4500
0000210089.CNF
,11 )
5000 Energy(kev)
5500
Live Time :10200.000 sec Real Time : 10200. 200 sec Start: 1:3502.?(kev) Stop : 1024:6565.S(keV) Acq. Start :Mon Apr 02 16:08:17 2018
6000 6500
0254
Channel Data Report 4/3/2018 5:49:53 AM Page 1
******************************************************* ***** s p E C T R A L DAT A R E P O R T ***** *******************************************************
Sample Title: 03
Elapsed Live time: 10200 Elapsed Real Time: 10200
Channell------l-------l-------l-------l-------1-------1-------1-------I 1: 0 0 0 0 0 0 0 0
9 : 0 0 0 0 0 0 0 0
17: 0 0 0 0 0 0 0 0
25: 0 0 0 0 0 0 0 0
33: 0 0 0 0 0 0 0 0
41: 0 0 0 0 0 0 0 0
49: 0 0 0 0 0 0 0 0
57: 0 0 0 0 0 0 0 0
65: 0 0 0 0 0 0 0 0
73: 0 0 0 0 0 0 0 0
81: 0 0 0 0 0 0 0 0
89: 0 0 0 0 0 0 0 0
97: 0 0 0 0 0 0 0 0
105: 0 0 0 0 0 0 0 0
113: 1 0 0 0 0 0 0 0
121: 0 0 0 0 0 0 0 0
129: 0 0 0 0 0 0 0 0
137: 0 0 0 0 0 0 0 0
145: 0 0 0 0 0 0 0 0
153: 0 0 0 0 0 0 0 0
161: 0 0 0 0 0 0 0 0
169: 0 0 0 0 0 0 0 0
177: 0 0 0 0 0 1 0 0
185: 0 0 0 0 0 0 0 0
193: 0 0 0 0 0 0 0 0
201: 0 0 0 0 1 0 0 0
209: 0 0 0 0 0 0 0 0
217: 1 0 0 0 0 0 0 0
225: 0 0 0 0 0 0 0 0
233: 0 0 0 0 0 0 0 0
241: 0 0 0 0 0 0 0 0
249: 0 0 0 0 0 0 0 0
257: 0 0 0 0 0 0 0 0
265: 0 0 0 0 0 0 0 0
273: 0 0 0 0 0 0 2 0
281: 0 0 0 0 0 0 0 0
289: 0 0 0 0 0 0 0 0
297: 0 0 0 0 0 0 0 0
305: 0 0 0 0 0 0 0 0
313: 0 0 0 0 0 0 0 0
321: 0 0 0 0 0 0 0 0
329: 0 0 0 0 0 0 0 1
337: 0 0 0 0 0 0 0 0
345: 0 0 0 0 1 0 1 0
353: 0 0 0 0 0 0 0 0
361: 0 0 0 0 0 0 0 0
0255
Channel Data Report 4/3/2018 5:49:53 AM Page 2
369: 0 0 0 0 0 0 0 0
Sample Title: 03
Channell------1-------1-------1-------I-------I-------I-------I-------I 377: 0 0 0 0 0 0 0 0
385: 0 0 0 0 0 0 0 0
393: 0 0 0 0 0 0 1 0
401: 0 0 0 0 0 0 0 0
409: 0 0 0 0 0 0 0 0
417: 0 0 0 0 1 0 0 0
425: 0 0 0 0 0 0 0 0
433: 0 0 0 0 0 0 0 0
441: 0 0 0 0 0 0 0 0
449: 0 0 0 0 0 0 0 0
457: 0 0 0 0 0 0 0 0
465: 0 0 0 0 0 0 0 0
473: 0 0 0 0 0 0 0 0
481: 0 0 0 0 0 0 0 0
489: 0 0 0 0 0 0 0 0
497: 0 0 0 0 0 0 0 0
505: 0 0 0 0 0 0 0 0
513: 0 0 0 0 0 0 0 0
521: 0 0 0 0 0 0 1 0
529: 0 0 0 0 0 0 0 0
537: 0 0 0 0 0 0 0 0
545: 0 0 0 1 0 0 0 0
553: 0 0 0 0 0 0 0 0
561: 0 0 0 0 0 0 0 0
569: 0 0 0 0 0 0 0 0
577: 0 0 0 0 0 0 0 1
585: 0 0 0 0 0 0 0 0
593: 0 0 0 0 0 0 0 0
601: 0 0 0 0 0 0 0 0
609: 0 0 0 0 0 0 0 0
617: 0 0 0 0 0 0 0 0
625: 0 0 0 0 0 0 0 0
633: 0 0 0 0 0 0 0 0
641: 0 0 0 0 0 0 0 0
649: 1 0 0 0 0 0 0 0
657: 0 0 0 0 0 0 0 0
665: 0 0 0 1 0 0 0 0
673: 0 0 0 0 0 0 0 1
681: 0 0 0 0 0 0 0 0
689: 0 0 0 0 0 0 0 0
697: 0 0 0 0 0 0 0 0
705: 0 0 0 0 0 0 0 0
713: 0 0 0 0 0 0 0 0
721: 0 0 0 0 0 0 0 0
729: 0 0 0 0 0 0 0 0
737: 0 0 0 0 0 0 0 0
745: 0 0 0 0 0 0 0 0
753: 0 0 0 0 0 0 0 0
761: 0 0 0 0 0 0 0 0
769: 0 0 0 0 0 0 0 0
777: 0 0 0 0 0 0 0 0
785: 0 1 0 0 0 0 0 0
793: 0 0 0 0 0 0 0 0
0256
Channel Data Report 4/3/2018 5:49:53 AM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 03
Channell------l-------l-------l-------1-------1-------1-------I-------I 809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 0 0 0 0 0 0
833: 0 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 0 0
865: 0 0 0 0 0 0 0 0
873: 0 0 0 0 0 0 0 0
881: 0 0 0 0 0 0 0 0
889: 0 0 0 0 0 0 0 0
897: 0 0 0 0 0 0 0 0
905: 0 0 0 0 0 0 0 0
913: 0 0 0 0 0 0 0 0
921: 0 0 0 0 0 0 0 1
929: 0 0 0 0 0 0 0 0
937: 0 0 0 0 0 0 0 0
945: 0 0 0 0 0 0 0 0
953: 0 0 0 0 0 0 0 0
961: 0 0 0 0 0 0 0 0
969: 0 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 1 0 0 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0257
c!t(A Al h TM ~J-\pex- p a Sample Description: Spectrum File: Batch Identification: Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Generic Mult. Factor: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Chem. Recovery Factor: Counting Efficiency: Effective Efficiency:
Peak Match Tolerance:
Nuclide
RA-224 RA-226
Energy (MeV)
5.572 4.584
OU-1-008 \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002100
1803110A-RA 04 Shelf 2 Ra
Alpha_044 04026481B 84168 System Bkgd 211971
<not performed>
l.000E+000 +/- 0.000E+000 liter
l.710E+000 4/19/2018 4/2/2018
170.0
Generic Div. Factor: 3:20:11 PM 4:08:13 PM
minutes 170.0 minutes
1.0000 +/- 0.0000
l.000E+000
0.1840 +/- 0.0032 on 2/16/2018
0.1840 +/- 0.0032 9:34:19 AM
0.350 MeV
PEAK AREA REPORT
Net Pk Area
-0.53 5.98
Pk Area Error%
415.13 87.78
Ambient Backgnd
1. 53 1. 02
NUCLIDE ANALYSIS RESULTS
Reagent Backgnd
0.00E+000 0.00E+000
FWHM (keV)
3.0 3.0
Nuclide Id
Con£. Energy (keV)
Activity (pCi/liter )
MDA (pCi/liter
RA-224 RA-226
0.983 0. 949
5685.50* -l.36E-002 +/- 5.66E-002
4785.00* l.47E-001 +/- l.29E-001 l.83E-001 +/- 6.29E-003 l.55E-001 +/- 5.32E-003
0258
60
55
50
45
40
35 U}
-1-' C:
8 30
25
20
15
10
5
0 I
3500 4000
ROI Type: 1
I/ .i.! ''il ~,,,
4500
0000210091.CNF
5000 Energy(kev)
5500
~
1
Live Time :10200.000 sec Real Time :10200.200 sec Start: l:3463.6(kev) Stop : 1024:6522.9(keV) Acq. Start :Mon Apr 02 16:08:13 2018
6000 6500
0259
Channel Data Report 4/3/2018 5:50:00 AM Page 1
******************************************************* ***** s p E C T R A L DAT A RE P O R T ***** *******************************************************
Sample Title: 04
Elapsed Live time: 10200 Elapsed Real Time: 10200
Channell------l-------l-------l-------1-------1-------1-------I-------I 1: 0 0 0 0 0 0 0 0
9: 0 0 0 0 0 0 0 0
17: 0 0 0 0 0 0 0 0
25: 0 0 0 0 0 0 0 0
33: 0 0 0 0 0 0 0 0
41: 0 0 0 0 0 0 0 0
49: 0 0 0 0 0 0 0 0
57: 0 0 0 0 0 0 0 0
65: 0 0 0 0 0 0 0 0
73: 0 0 0 0 0 0 0 0
81: 0 0 0 0 0 0 0 0
89: 0 0 0 0 0 0 0 0
97: 0 0 0 0 0 0 0 0
105: 0 0 0 0 0 0 0 0
113: 0 0 0 0 0 0 0 0
121: 0 0 0 0 0 0 0 0
129: 0 0 0 0 0 0 0 0
137: 0 0 0 0 0 0 0 0
145: 0 0 0 0 0 0 0 0
153: 0 0 1 0 0 0 0 0
161: 0 0 0 0 0 0 0 0
169: 0 0 0 0 0 0 0 0
177: 0 0 0 0 0 0 0 0
185: 0 0 0 0 0 0 0 0
193: 0 0 0 0 0 0 0 0
201: 0 0 0 0 0 0 0 0
209: 0 0 0 0 0 0 0 0
217: 0 0 0 0 0 0 0 0
225: 0 0 1 0 0 0 0 0
233: 0 0 0 0 0 0 0 0
241: 0 0 0 0 0 0 0 1
249: 0 0 0 0 0 0 0 0
257: 0 0 0 0 0 0 0 0
265: 0 0 0 0 0 0 0 0
273: 0 0 0 0 0 0 0 0
281: 0 0 0 0 0 0 0 0
289: 0 0 0 0 0 0 0 0
297: 0 0 1 1 0 0 0 0
305: 0 0 0 0 0 0 0 0
313: 0 0 0 0 1 0 0 0
321: 0 1 0 0 0 0 0 0
329: 0 0 0 0 0 0 0 0
337: 0 0 0 0 0 1 0 0
345: 0 1 0 0 0 0 0 0
353: 0 0 0 0 0 0 0 0
361: 0 0 0 0 0 0 0 0
0260
Channel Data Report 4/3/2018 5:50:00 AM Page 2
369: 0 0 0 0 0 0 0 0
Sample Title: 04
Channell------l-------1-------1-------1-------I-------I-------I-------I 377: 0 0 0 0 0 0 0 0
385: 0 0 0 0 0 0 0 0
393: 0 0 0 0 0 0 0 0
401: 0 0 0 0 0 0 0 1
409: 0 0 0 0 0 0 0 0
417: 0 0 0 0 0 0 0 0
425: 0 0 0 0 0 0 0 0
433: 0 0 0 0 0 0 0 1
441: 0 0 0 0 0 0 0 0
449: 0 0 0 0 0 0 1 0
457: 0 0 0 0 0 0 0 0
465: 0 0 0 0 0 0 0 0
473: 0 0 0 0 0 0 0 0
481: 0 0 0 0 0 0 0 0
489: 0 0 0 0 0 0 0 0
497: 0 0 1 0 0 1 0 0
505: 0 0 0 0 0 0 0 0
513: 0 0 0 0 0 0 0 0
521: 0 0 0 0 0 0 0 0
529: 0 0 0 0 0 0 0 0
537: 0 0 0 0 0 0 0 0
545: 0 0 0 0 0 0 0 0
553: 0 0 0 0 0 0 0 0
561: 0 0 0 0 1 0 0 0
569: 0 0 0 0 0 0 0 0
577: 0 0 0 0 0 0 0 0
585: 0 0 0 0 1 0 0 1
593: 0 0 0 0 0 0 0 0
601: 0 0 0 0 0 0 0 1
609: 0 0 0 2 0 0 0 0
617: 0 0 0 0 0 0 0 0
625: 0 0 0 0 0 0 0 0
633: 0 0 0 0 0 0 0 0
641: 0 0 0 0 0 0 0 0
649: 0 0 0 0 0 0 0 0
657: 0 0 0 0 0 0 0 0
665: 0 0 0 0 0 0 0 0
673: 0 0 0 0 0 0 0 0
681: 0 0 0 0 0 0 0 0
689: 0 0 0 0 0 0 0 0
697: 0 0 0 0 0 0 0 0
705: 0 1 0 0 0 0 0 0
713: 0 0 0 0 0 0 0 0
721: 0 0 0 0 0 0 0 0
729: 0 0 0 0 0 0 0 0
737: 0 0 0 0 0 0 0 0
745: 0 0 0 0 0 0 0 0
753: 0 0 0 0 0 0 0 0
761: 0 0 1 0 0 0 0 0
769: 0 0 0 0 0 0 0 0
777: 0 0 0 0 0 0 1 0
785: 0 0 0 0 0 0 0 0
793: 0 0 0 0 0 0 0 0
0261
Channel Data Report 4/3/2018 5:50:00 AM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 04
Channell------l-------l-------l-------1-------1-------1-------I-------I 809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 0 0 0 0 0 0
833: 0 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 1 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 0 0
865: 0 0 0 0 0 1 0 0
873: 0 0 0 0 0 0 0 0
881: 0 0 0 0 0 0 0 0
889: 0 0 0 0 0 0 0 0
897: 0 0 0 0 0 0 0 0
905: 0 0 0 0 0 0 0 0
913: 0 0 0 0 0 0 0 0
921: 0 0 0 0 0 0 0 0
929: 0 0 0 0 0 0 0 0
937: 0 0 0 0 0 0 1 0
945: 0 0 0 0 0 0 0 0
953: 0 0 0 0 0 0 0 0
961: 0 0 0 0 0 0 0 0
969: 0 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 1 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 0 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0262
Page 1 ot 2
Date : 4/2/2018
QA SU!Vlft.lA.RY REPORT Review Of QA Results - Pulser Check
Time : 5:27:26 AM
CHAMBER DEVICE PARAMETER FLAG
Alpha 001 21f ALL Not Done
Alpha 002 21f ALL Not Done
Alpha 003 21f ALL Passed
Alpha 004 21f ALL Passed
Alpha 005 2lf ALL Not Done
Alpha 006 21f ALL Not Done
Alpha 007 21f ALL Not Done
Alpha 008 2lf ALL Not Done
Alpha 009 2lf ALL Not Done
Alpha 010 21f ALL Passed
Alpha 011 21f ALL Passed
Alpha 012 21f ALL Passed
Alpha 013 21f ALL Not Done
Alpha 014 21f ALL Passed
Alpha 015 21f ALL Not Done
Alpha 016 21f ALL Not Done
Alpha 033 Alpha Analystl00DC Peak Energy Action
Alpha 034 Alpha Analystl00DC ALL Passed
Alpha 035 Alpha Analystl 00DC ALL Passed
Alpha 036 Alpha Analvstl00DC ALL Passed
Alpha 037 Alpha Analvstl00DC ALL Not Done
Alpha 038 Alpha Analystl00DC ALL Passed
Alpha 039 Alpha Analystl 00DC ALL Not Done
Alpha 040 Alpha Analvstl 00DC ALL Passed
Alpha 041 Alpha Analystl 00DC ALL Passed
Alpha 042 Alpha Analystl00DC ALL Passed
Alpha 043 Alpha Analvstl 00DC ALL Passed
Alpha 044 Alpha Analvstl00DC ALL Passed
Alpha 045 Alpha Analystl00DC ALL Passed
Alpha 046 Alpha Analystl00DC ALL Passed
Alpha 047 Alpha Analystl00DC ALL Not Done
Alpha 048 Alpha Analvstl 00DC ALL Not Done
Alpha 049 Alpha Analvstl 00DC ALL Passed
Alpha 050 Alpha Analystl 00DC ALL Passed
Alpha 051 Alpha Analyst 1 00DC ALL Passed
Alpha 052 Alpha Analystl 00DC ALL Passed
Alpha 053 Alpha Analvstl 00DC ALL Passed
Alpha 054 Alpha Analystl 00DC ALL Passed
Alpha 055 Alpha Analystl00DC ALL Passed
Alpha 056 Alpha Analystl00DC ALL Passed
Alpha 057 Alpha Analystl00DC ALL Passed
Alpha 058 Alpha Analystl00DC ALL Passed
4/2/2018 5:27:26 AM
DATE
4/2/2018 5:09:30 AM 4/2/2018 5:09:31 AM
4/2/2018 5:09:31 AM 4/2/2018 5:09:32 AM 4/2/2018 5:09:33 AM
4/2/2018 5:09:34 AM
4/2/2018 5:09:35 AM 4/2/2018 5:09:37 AM 4/2/2018 5:09:38 AM
4/2/2018 5:09:40 AM
4/2/2018 5:09:41 AM
4/2/2018 5:09:43 AM 4/2/2018 5:09:45 AM 4/2/2018 5:09:46 AM 4/2/2018 5:09:48 AM 4/2/2018 5:09:50 AM 4/2/2018 5:09:52 AM 4/2/2018 5:09:53 AM
4/2/2018 5:09:55 AM 4/2/2018 5:09:57 AM 4/2/2018 5:09:59 AM 4/2/2018 5:10:02 AM 4/2/2018 5:10:04 AM 4/2/2018 5:10:07 AM 4/2/2018 5:10:09 AM 4/2/2018 5:10:12 AM 4/2/2018 5:10:15 AM 4/2/2018 5:10:17 AM
0263
t-'age L OT L Kev1ew OT UA Kesuns - t-'u1ser 1.,necK 4/2/2018 5:27:26 AM
CHAMBER DEVICE PARAMETER FLAG DATE
Alpha 059 Alpha Analyst 1 00DC ALL Not Done
Alpha 060 Alpha Analyst! 00DC ALL Not Done
APPROVED BY:
APPROVAL DATE: _l---'/ l_·z,,,~/_18_· --
0264
Library Listing Report 6/12/12 12:16:17 PM Page l
*************************************************************************
***** L I B R A R Y L I S T I N G R E P O R T *****
*************************************************************************
Nuclide Library Title: Radium
Nuclide Library Description: Ra-226, Po-218, Rn-222
Nuclide Half-Life Energy Energy Yield Yield
Name (Seconds) (keV ) Uncert. (keV ( % ) Uncert. (Abs.+-)
PO-218 5.049E+0l0 6003.000* 0.000 99.9800 0.0000
RN-222 5.049E+010 5490.000* 0.000 99.9200 0.0000
RA-226 S.049E+0l0 4785.000* 0.000 100.0000 0.0000
* = key line
TOTALS: 3 Nuclides 3 Energy Lines
0265
SECTION XII
ANALYTICAL DATA (RADIUM-228)
0266
Eberline Analytical Oak Ridge Laboratory
Analysis Sheet
Work Order
·····-----
Date Recei~ed I_ 3/23/2018
Lab Deadline l 4/12/2018
Client I AMO Environmental Decisions
Project I WESTLAKE
Report Level / 4
Internal Sample Fraction Desc
01 LCS
02 MBL
03 i DUP
04 DO
18-03110 Ra228 Run 1
Client ID
LCS
BLANK
OU-1-008
i I
Printed: 4/9/201811:27 AM Page 1 of 3
Login Sample CPM Date
03/23/18 00:00
Sample Aliquot
1.0000E+00 -·--- ----·-···------ ----+----
03/23/18 00:00 1.0000E+00 ------~- --------- -- --
1.0000E+00 ·-' --··- --·· -----
i 38 i 03/19/18 18:02 ----------------- ' ·----~--·-·· I - -- - -- --- --+--------,
OU-1-008 i
. 38 . 03/19/18 18:02 1.0000E+00
----r-- _r-____ -_------------=- t =-- i ~ . -----"-I- . ----- --+--I ~
l----~--~--------+----------------1 ,_____ __ -+--------1------------ ---r------+---------·---~--. ----+--------'
Activity Units pCi
Aliquot Units
Matrix WA
Method EPA 904.0
Instrument Type Alpha/Beta GPC L~_:::-t. ____ !-------- =--1-= --=--L-------------+--------' Radiometric Tracer Ba-133 i
I
---- -+----------------+------!-----
Radiometric Sol# Ba-Ga -----
Tracer Act (dpm/g) 488.39 -----------+,- ----,-·----······ --··-
I Carrier Yttrium I ---··----,-- ···- --- ----·· ---·------i- '
Carrier Co~~~~~ml) I 30 11 l_ __ __ 1_____ ___________ +·-- _____ l __________________ ] _____ _ I I
I : i
··--- ----+--------------1 ,----~--------+ ----------------------;-- ------+-----· ··----·-·-·--+----------·-
I
-··· !-----····- :---··---·- ---, I I
i ' I
• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. ' Indicates estimated SAF value.
•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
0267
Eberline Analytical
Oak Ridge Laboratory
Analysis Sheet
18-03110 Ra228 Run 1
Printed: 4191201811:27 AM
Page 2 of 3
Internal Fraction
01
Sample Desc
LCS
Tracer Aliquot (g)
1.0027
I
I! Tracer Total
ACT(dpm)
489.7 ,
Radiometric Tracer (pCi)
297.0
Radiometric Ii Grav Carrier % Rec Added (ml)
134.64
Grav Filter Tare (g)
Grav Filter Final (g)
Grav Filter I Net (g) I
Grav %Rec
Mean %Rec
I
SAF I 1• I
SAF 2·
1.00 2.0501 0.0109! __ 0.1320: 0.06111 99.35! 109.28 1.00
2.150\ o.0116t--~.1;61. o.0645 100~-~o.~·~,-1.-oo-+-l-1-.0-0--11 I
1------r--~·+---------,~- ·----·------··--- - -- . ·-~----·- -+------.-i
491.6 i 02 MBL 1.0065 339.0 153.10 1 --- --
· ·~r I ·- i
488.9 352.0 159.83 2.300, 0.0708, 0.1397 0.0689 99.86, 109.84 1.00 I I 03 DUP 1.0011
04 DO 1.0043 490.5 l- -277.0 125.37 2.050 0.0714 0.1329 0.0615 100.00 110.00 1.00
!
L--t--+---+---1---+-----r-1--r----i I
I
7
7 I
i 7
I
i I
7
-----+-------+-------+--------+------
i
I I
·•
I ······-···-·
~~--t-----;-1~· ~ -----+-----+---~
* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. A Indicates estimated SAF value.
•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
1.00
1.00
0268
Eberline Analytical
Oak Ridge Laboratory
Analysis Sheet
18-03110 Ra228 Run 1
Printed: 4/9/2018 11 :27 AM Page 3 of3
Inter~ Sample I Rough Prep
Fraction I Desc Date
Rough Prep Prep
By Date Prep Sep to
By Date/Time Sep to
By Sep t1
Date/Time Sep t1
By
01 LCS
02 MBL
03 DUP
04/09/18 08:57 1 EBAILEY 04/02/1814:31 EBAILEY i 04/09/18 09:50 ·--'------+--- "-----~--!- .. --- ----·-- ---+--- -------+
i , I
04/09/18 08:57 I EBAILEY j 04/02/18 14:31 EBAILEY . 04/09/18 09:50 ----+------+--- ··· ----------~-~--------------·.....c_, __________ -- I --------·-1--·-
04/09/18 09:50
EBAILEY
EBAILEY
EBAILEY 04/09/18 08:57 I EBAILEY , 04/02/18 14:31 ' EBAILEY i -----<-------+-- I r---------- -----+---~-~· ------_.i...-------------·--
04 DO EBAILEY _j_ 04/02/18 14:31 EBAILEY ! 04/09/18 09:50 ---+-----
. I
04/09/18 08:57 EBAILEY
!
·-- ~----------+--------+-----------+--~ ·---··--~-
-1--------j-----1---~----------+----------+------------+-------~
1-------,-----1----~ -·-----~-----+--------+-----------+--------
l--------j-----1----· ··--···
---
--------+---------+------------+-----------+ ----------~---------+-----------+----------1
----i------+--------+-----· ··•··--···-
l--------j-----1-------
I I
f----
• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. A Indicates estimated SAF value.
•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
I
··--
0269
Eberline Analytical Oak Ridge Laboratory
~ Lab
Nuclide Fraction
01 RA-228
§ a:
~ 0 0 .!!! ~ iii s:::: q:
II
""""
co N N ns 0:::
1/) C: .2 .!? (.) Cl)
C ns -C: Cl)
E C: 0 II.. ·s;: C: w 0 ~ <
02 RA-228
03 RA-228
04 RA-228
I Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-0311 0-Ra228-1
Client I Activity
I Error Estimate I I Results MDA
Identification Units
LCS pCi/1 8.43E+00 7.20E-01 8.65E-01
BLANK pCi/1 2.64E-01 3.20E-01 6.54E-01
OU-1-008 pCi/1 9.25E-01 3.72E-01 6.SSE-01
OU-1-008 pCi/1 1.49E-01 3.36E-01 7.03E-01
LCS LCS Known %R
8.96E+00 94.01
Printed: 4/9/2018 1 :57 PM Page 1 of 3
LCS RPO
I MDA Blank
Flag Flag Flag Flag
OK OK
OK OK
NA OK
OK
0270
Eberline Analytical Oak Ridge Laboratory
~ ~
~
{: 8 .!!/ ~ cu t:: q;
11 0
~
00 N N cu ~
1/) C: 0 1/) ·c:; Q)
C cu -C: Q)
E C: 0 ... > C: w 0 :iE <(
Lab Fraction
Nuclide
01 RA-228
02 RA-228
03 RA-228
04 RA-228
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03110-Ra228-1
Sample
I Sample Radiometric Grav Mean
I Date Aliquot % Rec %Rec %Rec
03/23/18 00:00 1.00E+00 134.64 99.35 109.28
03/23/18 00:00 1.00E+00 153.10 100.00 110.00
03/19/18 18:02 1.00E+00 159.83 99.86 109.84
03/19/18 18:02 1.00E+00 125.37 100.00 110.00
I SAF
I
1.00
1.00
1.00
1.00
Printed: 4/9/2018 1 :57 PM Page 2 of 3
SeptO Sept1
Date/Time Date/Time
4/2/2018 14:31 4/9/2018 9:50
4/2/2018 14:31 4/9/2018 9:50
4/2/2018 14:31 4/9/2018 9:50
4/2/2018 14:31 4/9/2018 9:50
0271
Eberline Analytical Oak Ridge Laboratory
( Lab Nuclide Fraction
01 RA-228
§ a:
.g 8 -!!! ~ iii C:
<:(
~
~
""""'"
co N N ca 0::
1/) C: 0
-~ (.) Q)
C cu -C: Q)
E C: 0 ... "> C: w 0 :l:: <(
02 RA-228
03 RA-228
04 RA-228
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-0311 0-Ra228-1
Counting Halflife Detect Carrier I
Count Counts
Date/Time (days) Time
04/09/18 11 :42 LB4110A F1 I 120 948
04/09/18 11 :42 LB4110A F2 120 142
04/09/18 11 :42 LB4110A F3 120 224
04/09/18 11 :42 LB4110A F4 120 157
Bkg CPM
1.483333333
0.966666667
1.1
1.183333333
I
Printed: 4/9/2018 1 :57 PM Page 3 of 3
Eff
0.4754
0.4658
0.4713
0.4773
0272
Count Room Report Client: AMO Environmental Decisio
18-0311 0-Ra228-1 (pCi/1) in WA
Tracer ID: Ba-Ga
Printed: 4/9/2018 11:27 AM Page 1 of 1
Internal Sample I Client Sample Sample
1
, Tracer Tracer ---: Radiometric Radiometric
Fraction Desc i ID Date Aliquot Aliquot (g) ACT (dpm) j Tracer {pCi) % Rec SAF
1*
---- 02_j LCS i LCS I 03/23/18 00:00 1.00~~- I 1.0027 I 489.7087 297.0000 134.64 1.00
SAF 2*
1.00
-- : I I I
02 J MBL BLANK___ j 03/23/18 00:00 1.~000 I 1.0065 I 491.5645 339.000_~--~-1-53.10 1.00 1.00
03 DUP OU-1-008 03119/18 18:02 1.0000 I 1.0011 i 488.9272 352.0000 : 159.83 1.00 1.00
04 DO OU-1-008 I 03/19/18 18:02 1.0000 1.0043 I 490.4901 277.0000 i 125.37 1.00 1.00
1------I I -'---- --1-----------L..---'
j
,--·--·- I -// ______ _
I -~--·
I-~-- : l~==il--t--t--==t= I I ' I
--- I I ! I . - ' I i
T I ' ~J I - I -- ~ · 1
1
~+-___J
I --
1--·· --------+-- 1 ~ -,----+----+------1----~-- I I - - .. -- -i--- --------- -+-- ----- -----,----------,------l---------+----- ····--------···--+----+-----~
I
- - -- +-----------~-- ----- ____ ! - I -_ ~ ~-
0273
Eberline Analytical
Oak Ridge-Laboratory
LCS & Matrix Spikes
I Activity ! Solution
Isotope So/# : dpm/g i Date
Ra-228 Ra-12 I 56.230 4/9/2018
I :
i I
Tracers
I I I Activity
fraction Isotope !
So/# I
I dpm/g
01 Ba-133 Ba-6a 488.390
02 Ba-133 Ba-6a 488.390
03 Ba-133 Ba-6a 488.390
04 Ba-133 Ba-6a 488.390
I
i
Version 2.0 08/99
I Approx I Addition
0.360
\ Solution I I Date .
4/9/2018
4/9/2018
4/9/2018
4/9/2018
i I I !
I
I I
Spike and Tracer Worksheet
Analysis Code Date Technician
Ra228 4/9/2018 8:57 EBAILEY
LCS MS LCSD MSD LCS MS
Volume Volume Volume Volume Known I Error Added ! Error
Used(g) Used(g) Used(g) Used(g) pCi I Estimate pCi Estimate
0.3539 8.96[ 0.457 o.ooi 0.000
I I
i i .. ·- .....
I I I
Balance Printer Tapes
Volume Approx Tracer Used(g) Addition
1.0027 2.0700
1.0065 2.0700
1.0011 2.0700
1.0043 2.0700
--··--·--
Page 1 of 1 Printed: 4/9/2018 8:57 AM
Technician Initials Witness Initials
1(3
LCSD MSD
Known Error Added I Error pCi Estimate pCi , Estimate
0.00 0.000 o.oo( 0.000
i i
I
LCS
Matrix Spike
0274
Lab
Eberline Analytical Oak Ridge Laboratory
AMO Environmental Decisions
Fraction Client ID
01 LCS
02 BLANK
03 OU-1-008
04 OU-1-008
Comments
Analysis Code
Ra228
Sample Muffle Data Ratio
Type Post/Pre
LCS MBL
DUP DO
Techn;cian cc_ ~j.;: kwo,
Aliquot Worksheet
Rpt Units Lab Deadline
liters 4/12/2018
Dilution Data Aliquot Data
No of Dils Dil Factor Ratio Aliquot Net Equiv I 1.0000E+OO 1.0000E+OO
1.0000E+OO' 1.0000E+OO
1.0000E+OO 1.0000E+OO
1.0000E+OO 1.0000E+OO
I
Date:~
Technician
JHARVEY
MS Aliquot Data
Printed: 3/28/2018 9:26 AM Page 1 of 1
H-3 Solids Only vvater Aaaea A3u-.sr-
Aliquot Net Equiv (ml) I Aliq
!
i ! I :
!
0275
Eberline Analytical - Oak Ridge Version 1.1 10/2015
Work Order I
1s-03110 I TRetec AMO Environmental Decisions
Fraction Client ID
01 LCS
02 BLANK
03 DUP
04 OU-1-008
-
- --··-·---
~·-------·
--- ---
-- ... --····
/i ,,,-~, / 1_ //J ~✓
I ll/,, /. Technician: C:-:t / /(/ // l
Run
Sample
Type
LCS
MBL
DUP DO
Gravimetric Worksheet
I Analysis I Gravimetric
Code Carrier
Ra228 I Yttrium
Carrier Data Filter Data Carrier Added Filter Tare Filter Final
(ml) (g) (g)
2.0500 0.0109 I 0.1320
2.1500 0.0116 I 0.1361
2.3000 0.0708 0.1397
2.0500 0.0714 0.1329
f
I
I I i I
I
:
i
i
I ·---- ----··
-' I
Date: 11 I ti I /f./ V) ___ ,_.....,_._
Carrier Cone
(mg/ml)
30.0000
I Filter Net
(g)
0.0611
0.0645
0.0689 0.0615
I
I
Printed: 4/9/2018 11 :26 AM Page 1 of 1
Technician
EBAILEY
Gravimetric %
Recovery
99.35 100.00
99.86 100.00
0276
Detector ID Sample ID Alpha Beta Count Time Voltage TOD ·~
---t \-°" \vQ F1 1803110-01 33 948 120 1410 4/9/2018 11 :42:11 AM
F2 1803110-02 3 142 120 1410 4/9/2018 11 :42: 11 AM
F3 1803110-03 5 224 120 1410 4/9/2018 11 :42: 11 AM
F4 1803110-04 18 157 120 1410 4/9/2018 11 :42:11 AM
0277
Eberline Analytica Oak Ridge Labora·:ory
r J- Detector
LB4110A - Al
LB4110A - A2 -LB4110A - A3
LB4110A - A4
LB4110A - Bl
LB4110A - B2
LB4110A - B3 -l_B4110A - B4
LB4110A - Cl
LB4110A - C2 r-
LB4110A - C3
LB4110A - C4
LB4110A - D1
LB4110A - D2
LB4110A - D3
LB4110A - D4
LB4110A - El
l.B4110A - E2
l.B4110A - E3
LB4110A - E4
l.B4110A - Fl
LB4110A - F2
LB4110A - F3
LB4110A - F4
LB4110A - Gl
LB4110A - G2
LB4110A - G3 -LB4110A - G4 -
Alpha/Beta
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Calibration Date
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
GPC Detector Report (ALL Backgrounds)
Count Date Bkg CPM
4/9/2018 5.00E-02 j 4/9/2018 l.00E-01
4/9/2018 5.00E-02
4/9/2018 8.33E-02
4/9/2018 6.67E-02
4/9/2018 l.00E-01
4/9/2018 3.33E-02
4/9/2018 5.00E-02
4/9/2018 6.67E-02
4/9/2018 3.33E-02
4/9/2018 8.33E-02
4/9/2018 6.67E-02
4/9/2018 8.33E-02
4/9/2018 l.50E-01
4/9/2018 8.33E-02
4/9/2018 l.83E-01 I
3/23/2018 0.00E+00 i 3/23/2018 0.00E+00
3/23/2018 0.00E+00
3/23/2018 0.00E+00
4/9/2018 l.67E-02
4/9/2018 3.33E-02
4/9/2018 6.67E-02
4/9/2018 l.67E-02
4/9/2018 3.33E-02
4/9/2018 6.67E-02
4/9/2018 5.00E-02
4/9/2018 8.33E-02
PFW LCL Mean
p -5.83E-02 9.76E-02
p I -5.51E-02 8.94E-02
p -4.59E-02 l.05E-01
p -4.83E-02 9.12E-02
p -5.05E-02 l.06E-01
p j -3.02E-02 l.18E-01
p -6.47E-02 9.28E-02
p I -5.30E-02 8.43E-02
p -6.96E-02 9.57E-02
p -5.92E-02 7.03E-02
p -7.32E-02 9.30E-02
p -5.46E-02 8.29E-02
p -4.14E-02 l.54E-01
p -3.44E-02 l.39E-01
p -5.41E-02 l.14E-01
p -2.97E-02 l.43E-01
p ! -3.12E+0l 6.llE-01
p -3.93E-02 6.40E-02
p -6.26E-02 l.18E-01
p -3.22E+0l 5.72E-01
p -7.42E-02 9.58E-02
p -l.94E-01 7.50E-02
p -8.84E-02 l.25E-01
p I -5.45E-02 8.30E-02
p -5.85E-02 8.52E-02
p -5.46E-02 7.70E-02
p -5.29E-02 l.19E-01
p -3.18E-02 8.86E-02
i
I
µ_p Printed: 4/9/2018 6:44 AM L//Cf Ii §_i
Page 1 of 1
UCL
2.53E-01
2.34E-01
2.56E-01
2.31E-01
2.63E-01
2.65E-01
2.50E-01
2.22E-01
2.61E-01
2.00E-01
2.59E-01
2.20E-01
3.48E-01
3.12E-01 I 2.82E-01
3.15E-01 I 3.24E+0l
l.67E-01
2.99E-01 ,
3.34E+0l
2.66E-0·l
3.44E-01
3.38E-01
2.21E-01
2.29E-01
2.09E-01
2.90E-01
2.09E-01
0278
Eberline Analytical Oak Ridge Laboratory
,... Detector
LB4110A - Al
LB4110A - A2
LB4110A - A3
LB4110A - A4
. LB4110A - Bl
LB4110A - B2
LB4110A - B3
l_B4110A - B4
LB4110A - Cl
LB4110A - C2
LB4110A - C3
LB4110A - C4
LB4110A - D1
LB4110A - D2
LB4110A - D3
LB4110A - D4
LB4110A - El
LB4110A - E2
LB4110A - E3
I_B4110A - E4
LB4110A - Fl
LB4110A - F2
i_B4110A - F3
LB4110A - F4
LB4110A - Gl
LB4110A - G2
LB4110A - G3
LB4110A - G4
Alpha/Beta Calibration Date
Beta 10/20/2015
Beta 10/20/2015
Beta 10/20/2015
Beta 10/20/2015
Beta 10/20/2015
Beta 10/20/2015
Beta 10/20/2015
Beta 10/20/2015
Beta 10/20/2015
Beta 10/20/2015
Beta 10/20/2015
Beta 10/20/2015
Beta 10/20/2015
Beta 10/20/2015
Beta 10/20/2015
Beta 10/20/2015
Beta 10/20/2015
Beta 10/20/2015
Beta 10/20/2015
Beta 10/20/2015
Beta 10/20/2015
Beta 10/20/2015
Beta 10/20/2015
Beta 10/20/2015
Beta 10/20/2015
Beta 10/20/2015
Beta 10/20/2015
Beta 10/20/2015
GPC Detector Report (ALL Backgrounds)
Count Date Bkg CPM
4/9/2018 l.00E+00
4/9/2018 l.27E+00
4/9/2018 l.67E+00
4/9/2018 l.47E+00
4/9/2018 l.87E+00
4/9/2018 l.32E+00
4/9/2018 l.18E+00
4/9/2018 l.52E+00
4/9/2018 9.67E-01
4/9/2018 l.13E+00
4/9/2018 l.50E+00
4/9/2018 l.28E+00
4/9/2018 1.lOE+00
4/9/2018 1.48E+00 I
4/9/2018 l.07E+00
4/9/2018 l.80E+00
3/23/2018 3.33E-02
3/23/2018 l.67E-02
3/23/2018 6.67E-02
3/23/2018 0.00E+00
4/9/2018 1.48E+001
4/9/2018 9.67E-01
4/9/2018 l.lOE+00
4/9/2018 l.18E+0Q
4/9/2018 1.33E+00
4/9/2018 2.15E+00
4/9/2018 1.40E+00
4/9/2018 l.52E+00
PFW LCL
p 8.59E-01
p I 9.03E-01
p l.05E+00
p 3.07E-02
p l.05E+00
p 7.76E-01
p 9.46E-01
p 8.15E-01
p 8.67E-01
p 2.37E-01
p 9.16E-01
p 8.05E-01
p -2.14E+00
p -l.30E+00
p -9.79E-01
p -1.44E+00
p -4.88E+0l
p 5.69E-01
p 6.34E-01
p -5.22E+0l
p 6.42E-01
p -3.95E+02
p -4.86E+00
p -4.26E+00
p 8.27E-01
F 1.14E+00
p 8.63E-01
p 7.13E-01
Mean
l.44E+00
1.49E+00
l.58E+00
l.53E+00
l.61E+00
l.54E+00
l.45E+00
1.44E+00
l.34E+00
l.19E+00
l.75E+00
1.27E+00
2.03E+00
2.lOE+00
l.75E+00
2.16E+00
2.19E+00
9.46E-01
1.19E+00
l.87E+00
1.44E+00
2.03E+0l
2.09E+00
1.77E+00
1.29E+00
1.66E+00
1.42E+00
1.36E+00
KD Printed: 4/9/2018 6:44 AM L{ /Cf /J e£,
Page 1 of 1
UCL
2.03E+00
2.09E+00
2.12E+00
3.04E+00
2.17E+00
2.30E+00
l.96E+00
2.06E+00
l.81E+00
2.14E+00
2.59E+00
l.74E+00
6.19E+00
5.51E+00
4.48E+00
5.75E+00
5.32E+0l
l.32E+00
l.75E+00
5.59E+0l
2.24E+00
4.35E+02
9.05E+00
7.80E+00
1.75E+00
2.17E+00
l.98E+00
2.0lE+00
0279
Eberline Analytical Oak Ridge Laboi-atory
~:tor
i LB4110A - Al
LB4110A - A2
LB4110A - A3
LB4110A - A4
LB4110A - Bl
LB4110A - B2
LB4110A - B3
LB4110A - B4
LB4110A - Cl
LB4110A - C2
LB4110A - C3
LB4110A - C4
LB4110A - D1
LB4110A - D2
LB4110A - D3
LB4110A - D4
LB411CA - El
LB411CA - E2
LB411CA - E3
LB411CA - E4
LB411CA - Fl
LB411CA - F2
LB411CA - F3
LB411CA - F4
LB4110A - Gl
LB4110A - G2
LB4110A - G3
LB4110A - G4
Alpha/Beta
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Calibration Date
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
GPC Detector Report (ALL Efficiencies)
Count Date Eff
4/9/2018 0.2252
4/9/2018 0.2096
4/9/2018 0.2000
4/9/2018 0.2292
4/9/2018 0.2288
4/9/2018 0.2002
4/9/2018 0.2385
4/9/2018 0.2279
4/9/2018 0.2079
4/9/2018 0.2132
4/9/2018 0.2427
4/9/2018 0.2123
4/9/2018 0.2204
4/9/2018 0.2558
4/9/2018 0.2529
4/9/2018 0.1932
3/23/2018 0.0000
3/23/2018 0.0000
3/23/2018 0.0000
3/23/2018 0.0000
4/9/2018 0.2109
4/9/2018 0.1805
4/9/2018 0.2390
4/9/2018 0.2153
4/9/2018 0.2006
4/9/2018 0.2066
4/9/2018 0.2:;307
4/9/2018 0.2040
Printed: 4/9/2018 6:44 AM KP Page 1 of t;/Cf/i e>
PFW LCL Mean UCL
p 0.2190 0.2299 0.2409
p 0.2029 0.2118 0.2207
p 0.1909 0.2007 0.2106 I
p 0.2195 0.2295 0.2394
p 0.2013 0.2214 0.2416
p 0.1831 0.2042 0.2253
p 0.2217 0.2363 0.2508
p 0.2135 0.2249 0.2363
p 0.2009 0.2106 0.2203
p I 0.0288 0.2230 0.4172
p 0.2343 0.2458 0.2573
p 0.2067 0.2188 0.2309
p 0.2103 0.2232 0.2360
p 0.2356 0.2521 0.2685
p 0.2399 0.2522 0.2646
p 0.1848 0.1955 0.2062
F 0.1959 0.2303 0.2648
F 0.1833 0.2089 0.2345
F 0.1855 0.2092 0.2330
F 0.2024 0.2394 0.2765
p 0.0510 0.1838 0.3166
p 0.1005 0.1800 0.2594
p 0.1678 0.2334 0.2989
p 0.1471 0.2100 0.2729
p 0.1919 0.2032 0.2144
p 0.1942 0.2057 0.2172 '
p 0.2171 0.2275 0.2378
p 0.1918 0.2017 0.2115
0280
Eberline Analytical Oak Ridge Labo,·atory
Dete,:tor
LB4110A - Al
LB4110A - A2
LB4110A - A3
LB4110A - A4
LB4110A - Bl
LB4110A - B2
LB4110A - B3
LB4110A - B4
LB4110A - Cl
LB4110A - C2
LB4110A - C3
LB4110A - C4
LB4110A - D1
LB4110A - D2
LB4110A - D3
LB4110A - D4
LB4110A - El
LB4110A - E2
LB4110A - E3
LB4110A - E4
LB4110A - Fl
LB4110A - F2
LB4110A - F3
LB4110A - F4
LB4110A - Gl
LB4110,I\ - G2
LB4110A - G3
LB4110A - G4
Alpha/Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Calibration Date
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
GPC Detector Report (ALL Efficiencies)
Count Date Eff
4/9/2018 0.5328
4/9/2018 0.4651
4/9/2018 0.4793
4/9/2018 0.5356
4/9/2018 0.5397
4/9/2018 0.5071
4/9/2018 0.5872
4/9/2018 0.5506
4/9/2018 0.4813
4/9/2018 0.5255
4/9/2018 0.6052
4/9/2018 0.5300
4/9/2018 0.6321
4/9/2018 0.6437
4/9/2018 0.6456
4/9/2018 0.5040
3/23/2018 0.0436
3/23/2018 0.0428
3/23/2018 0.0551
3/23/2018 0.0569
4/9/2018 0.5242
4/9/2018 0.4434
4/9/2018 0.6177
4/9/2018 0.5364
4/9/2018 0.4642
4/9/2018 0.4834
4/9/2018 0.5380
4/9/2018 0.4830
Printed: 4/9/2018 6:44 AM
Page 1 of 1 J< p PFW I LCL Mean UCL 4/q)1 ~
p 0.5198 0.5427 0.5656
p 0.4457 0.4705 0.4952
p 0.4579 0.4783 0.4987
p 0.5294 0.5509 0.5724
p 0.5054 0.5379 0.5704
p 0.4714 0.5049 0.5385
p 0.5561 0.5849 0.6136
p 0.5274 0.5521 0.5767
p 0.4642 0.4906 0.5170
p 0.5045 0.5274 0.5503
p 0.5821 0.6110 0.6398
p 0.5064 0.5363 0.5661
w 0.6276 0.6526 0.6775
p 0.6171 0.6490 0.6809
p 0.6158 0.6409 0.6660
p 0.4643 0.5009 0.5374
F 0.4730 0.5519 0.6307
F 0.4450 0.5020 0.5591
F 0.4552 0.5070 0.5589
F 0.5130 0.5987 0.6844
p 0.2986 0.4669 0.6352
p 0.2966 0.4389 0.5812
p 0.4745 0.5896 0.7047
p 0.4114 0.5209 0.6305
p 0.4449 0.4650 0.4852
p 0.4729 0.4974 0.5219
p 0.5290 0.5538 0.5785
p 0.4706 0.4959 0.5213
0281
SECTION XIII
BARIUM-133 ANALYTICAL TRACER DATA
0282
4/2/2018 3:34:57PM Page I of6
pex-Gamma Analysis Report for 1803110-01
SPIKE
GAMMA SPECTRUM ANALYSIS
Sample Identification
Sample Description
Sample Type
Sample Size Facility
Sample Taken On
Acquisition Started
Procedure Operator Detector Name
Geometry Live Time Real Time
Dead Time
Peak Locate Threshold
Peak Locate Range (in channels)
Peak Area Range (in channels)
Identification Energy Tolerance
Energy Calibration Used Done On
Efficiency Calibration Used Done On
Efficiency Calibration Description
Sample Number
: 1803110-01
: SPIKE : RA RECOVERY
: 1.000E+00 units
: Countroom
: 4/2/2018 3: 18:22PM
: 4/2/2018 3:19:47PM
: BAFIL : Administrator
: GE1 : BAFIL : 900.0 seconds
: 900.2 seconds
: 0.02 %
: 2.50 : 1 - 4096 : 19 - 4096 : 1.000 keV
: 2/17/2018
: 2/17/2018
: 64152
PEAK ANALYSIS REPORT
Peak Analysis Performed on : 4/2/2018 3:34:50PM
Peak No.
Peak Analysis From Channel
Peak Analysis To Channel
Energy (keV)
ROI
start
ROI end
: 1 : 4096
Peak Centroid
Net Peak Area
Net Area Uncertainty
Continuum Counts
FWHM (keV)
0283
M m M m m M
M m
M m
m M m
M m
M m M m
4/2/2018 3:34:57PM Page 2 of6
Analysis Report for 1803110-01
SPIKE
Peak Energy ROI
No. (keV} start
1 30.68 27 -2 35.05 27 -3 53.08 50 -4 61.75 50 -5 65.84 50 -6 81.12 77 -7 93.08 91 -8 111.72 108 -9 115.73 108 -
10 160.44 158 -11 276.26 272 -12 303.05 299 -13 306.81 299 -14 334.45 330 -15 356.15 350 -16 384.81 382 -17 391.23 382 -18 414.54 411 -19 437.37 434 -20 456.70 455 -21 466.40 462 -22 606.28 605 -23 609.46 605 -24 1002.05 998 -25 1522.38 1518 -
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet Errors quoted at 2.000sigma
ROI Peak Net Peak Net Area Continuum
end Centroid Area Uncertainty Counts
40 31.18 l.17E+03 72. 52 1.32E+02
40 35.55 3.62E+02 59.52 1.22E+02
73 53.57 2.16E+0l 23.02 7.80E+0l
73 62.23 1.78E+02 34.15 7.80E+0l
73 66.31 5.96E+0l 32.35 9.l0E+0l
91 81.58 5.05E+02 51.40 1.35E+02
97 93.53 5.79E+0l 25.24 7.42E+0l
119 112.15 1.22E+02 29.08 7.85E+0l
119 116.15 2.0lE+0l 20.44 5.67E+0l
163 160.83 3.04E+0l 21. 21 6.52E+0l
282 276.54 5.51E+0l 25.86 5.78E+0l
318 303.31 7.14E+0l 20.90 2.98E+0l
318 307.07 1.80E+0l 17.46 2.26E+0l
340 334.69 7.07E+0l 29.39 7.85E+0l
367 356.36 3.52E+02 39.43 3.48E+0l
395 385.00 7.17E+0l 22.30 1.22E+0l
395 391.42 2.55E+0l 20.33 2.67E+0l
418 414.71 1.57E+0l 17.44 4.06E+0l
443 437.52 3.86E+0l 19.77 3.08E+0l
459 456.83 6.00E+00 4.90 0.00E+00
470 466.52 l.26E+0l 11. 69 1.28E+0l
611 606.29 5.06E+00 3.77 2.45E+00
611 609.47 8.90E+00 7.28 2.36E+00
1004 1001.78 9.00E+00 6.00 0.00E+00
1524 1521.80 5.00E+00 4.47 0.00E+00
BACKGROUND SUBTRACT REPORT
Peak Analysis Performed on
Env. Background File
Peak Energy
No. (keV)
1 30.68 2 35.05 3 53.08 4 61.75
: 4/2/2018 3:34:50PM
: \\OR-GAMMA 1 \ApexRoot\Countroom\Data\0000063824.CNF
Original Orig. Area Ambient Backgr. Subtracted
Area Uncertainty Background Uncert. Area
1.17E+03 72. 52 1.17E+03
3.62E+02 59.52 3.62E+02
2.16E+0l 23.02 2.16E+0l
l.78E+02 34.15 1.78E+02
FWHM (keV)
1. 74 2.08 2.15 2.13 2.18 2.01 1. 70 1. 70 1. 70 1. 60 2.02 2.05 2.06 1. 95 1. 94 1. 75 2.34 1. 34 1. 94 2.74 4.94 2.49 2.12 1. 77 2.75
Subtracted Uncert.
7.25E+0l 5.95E+0l 2.30E+0l 3.41E+0l
0284
4/2/2018 3:34:57PM Page 3 of6
Analysis Report for 1803110-01
SPIKE
Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted
No. {keV) Area Uncertainty Background Uncert. Area Uncert.
m 5 65.84 5.96E+0l 32.35 6.94E-0l 3.48E-01 5.89E+0l 3.24E+0l
M 6 81.12 5.05E+02 51.40 5.05E+02 5.14E+0l
7 93.08 5.79E+0l 25.24 3.26E+0l 2.92E+00 2.53E+0l 2.54E+0l
M 8 111.72 l.22E+02 29.08 l.22E+02 2.91E+0l
m 9 115.73 2.0lE+0l 20.44 2.0lE+0l 2.04E+0l
10 160.44 3.04E+0l 21. 21 3.04E+0l 2.12E+0l
11 276.26 5.51E+0l 25.86 5.51E+0l 2.59E+0l
M 12 303.05 7.14E+0l 20.90 7.14E+0l 2.09E+0l
m 13 306.81 l.80E+0l 17.46 l.80E+0l l.75E+0l
14 334.45 7.07E+0l 29.39 7.07E+0l 2.94E+0l
m 15 356.15 3.52E+02 39.43 3.52E+02 3.94E+0l
M 16 384.81 7.17E+0l 22.30 7.17E+0l 2.23E+0l
m 17 391.23 2.55E+0l 20.33 2.55E+0l 2.03E+0l
18 414.54 l.57E+0l 17.44 l.57E+0l l.74E+0l
19 437.37 3.86E+0l 19.77 3.86E+0l l.98E+0l
20 456.70 6.00E+00 4.90 6.00E+00 4.90E+00
21 466.40 l.26E+0l 11. 69 l.26E+0l l.17E+0l
M 22 606.28 5.06E+00 3.77 5.06E+00 3.77E+00
m 23 609.46 8.90E+00 7.28 2.56E+00 l.16E+00 6.33E+00 7.37E+00
24 1002.05 9.00E+00 6.00 9.51E-01 7.24E-01 8.05E+00 6.04E+00
25 1522.38 5.00E+00 4.47 5.00E+00 4.47E+00
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet Errors quoted at 2.000sigma
NUCLIDE IDENTIFICATION REPORT
Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\WSRC.NLB
IDENTIFIED NUCLIDES
Nuclide Id Energy Yield(%) Activity Activity
Name Confidence (keV) (pCilunits) Uncertainty
SN-113 0.94 255.12 1. 93 391.69 * 61.90 l.52E+0l l.21E+0l
I-125 0.97 35.49 * 6.49 3.37E+00 5.53E-01
BA-133 0.99 30.80 * 97.60 2.l0E-01 l.30E-02
302.84 * 17.80 3.16E+02 l.66E+02
356.01 * 60.00 2.97E+02 4.65E+0l
PA-231 0.99 9.28 42.00 10.11 20.20
0285
Analysis Report for 1803110-01
SPIKE
Nuclide Id Energy
Name Confidence (keV)
PA-231 0.99 283.67 302.67
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
*
@ = Energy line not used for Weighted Mean Activity
Energy Tolerance: 1.000 keV
Nuclide confidence index threshold = 0.30
Errors quoted at 2.000sigma
Yield(¾)
1. 60 2.30
4/2/2018 3:34:57PM Page 4 of 6
Activity
(pCilunits)
2.44E+03
Activity
Uncertainty
1.29E+03
INTERFERENCE CORRECTED REPORT
Nuclide Name
SN-113 I-125
Nuclide Id
Confidence
0.940 0.970
X I-129 0.681
? = X =
BA-133 PA-231
0.997 0.999
nuclide is part of an undetermined solution
nuclide rejected by the interference analysis
Wt mean Activity
(pCilunits)
1.52E+0l 3.37E+00
2.l0E-01 2.44E+03
@ = nuclide contains energy lines not used in Weighted Mean Activity
Errors quoted at 2.000sigma
Wt mean Comments Activity
Uncertainty
1.21E+0l 5.53E-01
1.30E-02 1.29E+03
0286
Analysis Report for 1803110-01
M
m m M
M
m
m
M
M
m
SPIKE
Peak Locate Performed on
Peak Locate From Channel
Peak Locate To Channel
Peak No. Energy (keV)
3 53.08
4 61.75
5 65.84
6 81.12
7 93.08
8 111.72
9 115. 73
10 160.44
11 276.26
13 306.81
14 334.45
16 384.81
18 414.54
19 437.37
20 456.70
21 466.40
22 606.28
23 609.46
24 1002.05
25 1522.38
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
4/2/2018 3:34:57PM
UNIDENTIFIED PEAKS
: 4/2/2018 3:34:50PM
: 1 : 4096
Peak Size (CPS)
2.40359E-02
1.97417E-01
6.54781E-02
5.60890E-01
2.80855E-02
1.35124E-01
2.23089E-02
3.37566E-02
6.12103E-02
2.00002E-02
7. 85960E-02
7. 96880E-02
1. 74691E-02
4.28704E-02
6.66667E-03
1.40058E-02
5.61935E-03
7.03687E-03
8.94381E-03
5.55556E-03
Peak CPS(%)
Uncertainty
53. 21 9.61
27.45
5.09
50. 27
11. 96 50.90 34.91 23.47
48.51 20.77
15.55 55.45
25.62
40.82 46.39
37.32 58.20 37.54
44. 72
NUCLIDE MDA REPORT
Peak Type
Sum Sum
Sum
Sum
Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\WSRC.NLB
Page 5 of6
Tolerance Nuclide
0287
4/2/2018 3:34:57PM Page 6 of6
Analysis Report for 1803110-01
SPIKE
Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCi/units) (pCilunits) (pCi/units) (pCi/units)
FE-55 5.89 24.50 l.90E-13 1.90E-13 0.00E+00 0.00E+00
CO-57 122.06 85.51 2.68E+0l 2.68E+0l -2.16E+00 1.22E+0l
136.48 10.60 2.82E+02 -3.88E+0l 1.29E+02
NI-59 6.92 29.80 2.77E-12 2.77E-12 0.00E+00 0.00E+00
MO-93 16.59 52.90 7.83E-06 7.83E-06 0.00E+00 3.47E-06
18.60 10.00 3.54E-04 -4.81E-04 l.67E-04
NB-93M 16.57 9.43 4.32E-05 4.32E-05 0.00E+00 l.92E-05
CD-109 88.03 3. 72 2. 78E+02 2. 78E+02 4.73E+0l 1.30E+02
+ SN-113 255.12 1. 93 1.40E+03 1.98E+0l 1.26E+02 6.26E+02
391.69 * 61.90 1.98E+0l 1.52E+0l 9.llE+00
SN-119M 23.87 16.10 6.46E-03 4.62E-03 1.23E-02 3.12E-03
25.10 22.70 4.62E-03 -1.04E-02 2.18E-03
+ I-125 35.49 * 6.49 8.26E-01 8.26E-01 3.37E+00 4.00E-01
I-129 29. 78 * 57.00 2.73E-02 2.73E-02 3.59E-0l 1.32E-02
33.60 13. 20 3.98E-01 -1.73E+00 1.95E-01
39.58 7.52 8.46E-01 9.55E-02 3.92E-01
+ BA-133 30.80 * 97.60 1.59E-02 1.59E-02 2.l0E-01 7.73E-03
302.84 * 17.80 2.37E+02 3.16E+02 1. 13E+02
356.01 * 60.00 4.53E+0l 2.97E+02 2.15E+0l
CE-139 165.85 80.35 4.36E+0l 4.36E+0l -3.19E+00 1.97E+0l
CE-144 133. 54 10.80 2.68E+02 2.68E+02 8.35E-01 1.23E+02
HG-203 279.19 77.30 4.89E+0l 4.89E+0l 5.36E+0l 2.28E+0l
PB-210 46.50 4.25 5.0lE+00 5.0lE+00 1.79E+00 2.31E+00
+ PA-231 9.28 42.00 2.61E-10 2.61E-10 0.00E+00 0.00E+00
10 .11 20.20 2.08E-09 0.00E+00 0.00E+00
283.67 1. 60 l.17E+03 -3.28E+02 5.10E+02
302.67 * 2.30 1.83E+03 2.44E+03 8.71E+02
TH-231 25.64 14.70 8. 96E-03 8.96E-03 -2.0lE-02 4.22E-03
84.21 6.40 1.66E+02 -9.94E+02 7.84E+0l
PA-234M 9.89 89.00 3.36E-10 3.36E-10 0.00E+00 0.00E+00
21. 72 64.90 5.99E-04 l.59E-03 2.90E-04
37.93 23.75 3.75E-01 5.19E-01 1.81E-01
131.42 20.40 l.34E+02 -4.17E+00 6.14E+0l
TH-234 63.29 3.80 9.02E+0l 9.02E+0l 5.84E+0l 4.34E+0l
NP-237 2 9. 37 14.00 1.34E-01 1.34E-01 8.67E-01 6.59E-02
86.50 12.60 8.23E+0l 1.88E+0l 3.86E+0l
U-237 97.08 16.30 7.35E+0l 5.97E+0l -7.24E+00 3.37E+0l
101.07 26.30 5.97E+0l 1.84E+0l 2.76E+0l
114.00 12.30 3.03E+02 4.64E+02 1.45E+02
208.01 22.00 1.68E+02 -7. 21E+0 1 7.62E+0l
AM-241 59.54 35.90 5.89E+00 5.89E+00 4.22E+00 2.82E+00
AM-243 74.67 66.00 6.79E+00 6.79E+00 5.13E-02 3.15E+00
+ = Nuclide identified during the nuclide identification
• = Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
0288
105
104
~ lQ3t.~ ro <(
u !;:: Vl
en 0 ..-
1 Vl .µ C: ::;j
0 u 102
101
= = '";' ~
= = ...... ' ~
~ JI ;t
100 !fti $'~/~ fl ff I
500 1000
1111 ROI Type: 1
1500
0000064152.CNF
2000 channel
2500
Live Time :900.000 sec Real Time :900.210 sec start: 1: 0. S(kev) Stop : 4096: 4096. 9 (kev) Acq. start :Mon Apr 02 15:19:47 2018
3000
11111 ROI Type: 2
3500 4000
0289
4/2/2018 3:35:09PM Pagel of6 \~ \v\l 4Lv
f\pex-Gamma Analysis Report for 1803110-02
BLANK
GAMMA SPECTRUM ANAL YS/S
Sample Identification
Sample Description
Sample Type
Sample Size
Facility
Sample Taken On
Acquisition Started
Procedure Operator
Detector Name
Geometry
Live Time
Real Time
Dead Time
Peak Locate Threshold
Peak Locate Range (in channels)
Peak Area Range (in channels)
Identification Energy Tolerance
Energy Calibration Used Done On
Efficiency Calibration Used Done On
Efficiency Calibration Description
Sample Number
: 1803110-02
: BLANK
: RA RECOVERY
: 1.000E+00 units
: Countroom
: 4/2/2018 3:18:32PM
: 4/2/2018 3:19:56PM
: BAFIL : Administrator
: GE3 : BAFIL : 900.0 seconds
: 901.8 seconds
: 0.20 %
: 2.50
: 1 - 4096
: 9 - 4096 : 1.000 keV
: 2/17/2018
: 11/9/2014
: 64153
PEAK ANALYSIS REPORT
Peak Analysis Performed on : 4/2/2018 3:35:05PM
Peak No.
Peak Analysis From Channel
Peak Analysis To Channel
Energy (keV)
ROI start
ROI end
: 4096
Peak Centroid
Net Peak Area
Net Area Uncertainty
Continuum Counts
FWHM (keV)
0290
4/2/2018 3:35:09PM Page 2 of6
Analysis Report for 1803110-02
M m M M m m
M m M m
M m M M m m
M m
BLANK
Peak Energy ROI
No. (keV) start
1 31.31 14 -2 61.98 54 -3 66.59 54 -4 80. 96 7 4 -5 105.41 104 -6 111.68 104 -7 116. 62 104 -8 183.40 1 74 -9 276.37 2 68 -
10 302.74 296 -11 308.30 296 -12 334.54 329 -13 355.78 329 -14 386.39 379 -15 416.56 410 -16 436.20 428 -17 468.32 4 63 -18 609.29 604 -
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet Errors quoted at 2.000sigma
ROI end
41 72 72 99
119 119 119 191 286 326 326 367 367 400 424 442 475 614
Peak Net Peak Net Area Continuum
Centroid Area Uncertainty Counts
31.75 1. 51E+03 139.36 1.25E+03
62.39 2.20E+02 52.35 3.16E+02
67.00 6.99E+0l 48.59 2.43E+02
81.36 6.14E+02 52.91 1.48E+02
105.79 1.68E+0l 14.64 5.00E+0l
112.06 2.01E+02 40.60 1.40E+02
117. 00 5.45E+0l 22.00 6.53E+0l
183.74 3.28E+0l 41. 38 1. 96E+02
27 6. 64 4.88E+0l 35.92 9.65E+0l
303.00 2.37E+02 33.56 9.14E+0l
308.56 2.85E+0l 37.60 8.llE+0l
334.77 9.71E+0l 24.55 6.43E+0l
356.00 3.47E+02 39.33 4.27E+0l
386.60 2.20E+02 41.69 6.60E+0l
416.75 5.71E+0l 20.99 2.18E+0l
436.37 7.00E+0l 16.73 0.00E+00
468.47 3.13E+0l 13. 50 7.31E+00
609.36 1.22E+0l 11. 34 9.53E+00
BACKGROUND SUBTRACT REPORT
Peak Analysis Performed on
Env. Background File
Peak Energy
No. (keV)
1 31.31 2 61.98 3 66.59 4 80. 96 5 105.41 6 111.68 7 116. 62 8 183.40 9 276.37
10 302.74 11 308.30
: 4/2/2018 3:35:05PM
: \\OR-GAMMA 1 \ApexRoot\Countroom\Data\0000063826.CNF
Original Orig. Area Ambient Backgr. Subtracted
Area Uncertainty Background Uncert. Area
1.51E+03 139.36 1.51E+03
2.20E+02 52.35 7.99E+0l 1.37E+00 1.40E+02
6.99E+0l 48.59 6.99E+0l
6.14E+02 52.91 6.14E+02
1.68E+0l 14.64 1.68E+0l
2.01E+02 40.60 2.01E+02
5.45E+0l 22.00 5.45E+0l
3.28E+0l 41.38 3.28E+0l
4.88E+0l 35.92 4.88E+0l
2.37E+02 33.56 2.37E+02
2.85E+0l 37.60 2.85E+0l
FWHM (keV)
2.08 3.84 6.93 2.63 3.99 4.04 6.55 7.49 2.26 5.61 6.15
11.77 2.89 2.59 3.51 1. 62 2.25 3.82
Subtracted Uncert.
1.39E+02 5.24E+0l 4.86E+0l 5.29E+0l 1.46E+0l 4.06E+0l 2.20E+0l 4.14E+0l 3.59E+0l 3.36E+0l 3.76E+0l
0291
4/2/2018 3:35:09PM Page 3 of6
Analysis Report for 1803110-02
M m
BLANK
Peak Energy Original
No. (keV) Area
12 334.54 9.71E+0l 13 355.78 3.47E+02 14 386.39 2.20E+02 15 416.56 5.71E+0l 16 436.20 7.00E+0l 17 468.32 3.13E+0l 18 609.29 1.22E+0l
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
Orig. Area Ambient Backgr. Subtracted
Uncertainty Background Uncert. Area
24.55 9.71E+0l
39.33 3.47E+02
41.69 2.20E+02
20.99 5.71E+0l
16.73 7.00E+0l
13. 50 3.13E+0l
11. 34 1.89E+00 1.35E+00 1.03E+0l
NUCLIDE IDENTIFICATION REPORT
Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\WSRC.NLB
IDENTIFIED NUCLIDES
Nuclide Id Energy
Name Confidence (keV)
BA-133 0.97 30.80 302.84 356.01
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
* * *
@ = Energy line not used for Weighted Mean Activity
Energy Tolerance : 1.000 keV
Nuclide confidence index threshold = 0.30
Errors quoted at 2.000sigma
Yield(%)
97.60 17.80 60.00
Activity
(pCi/units)
1.31E+00 1.03E+03 3.39E+02
Activity
Uncertainty
1.21E-01 3.99E+02 5.19E+0l
INTERFERENCE CORRECTED REPORT
Subtracted Uncert.
2.45E+0l 3.93E+0l 4.17E+0l 2.l0E+0l 1.67E+0l 1.35E+0l 1.14E+0l
0292
Analysis Report for 1803110-02
? =
X =
BLANK
Nuclide Name
BA-133
Nuclide Id
Confidence
0.974
nuclide is part of an undetermined solution
nuclide rejected by the interference analysis
4/2/2018 3:35:09PM
Wt mean Wt mean
Activity Activity
(pCi/units) Uncertainty
1.31E+00 1.21E-01
@ = nuclide contains energy lines not used in Weighted Mean Activity
Errors quoted at 2.000sigma
Page 4 of 6
Comments
0293
Analysis Report for 1803110-02
M
m M
M
m m
m M
BLANK
Peak Locate Performed on
Peak Locate From Channel
Peak Locate To Channel
Peak No. Energy {ke V)
2 61.98
3 66.59
4 80. 96
5 105.41
6 111.68
7 116. 62
8 183.40
9 276.37
11 308.30
12 334.54
14 386.39
15 416.56
16 436.20
17 468.32
18 609.29
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
4/2/2018 3:35:09PM
UNIDENTIFIED PEAKS
: 4/2/2018 3:35:05PM
: 1 : 4096
Peak Size (CPS)
1.55904E-01
7.76879E-02
6.81897E-0l
1.86972E-02
2.23059E-01
6.05725E-02
3.64179E-02
5.41924E-02
3.16614E-02
1.07891E-01
2.44444E-01
6.34559E-02
7.77778E-02
3.48254E-02
1.14920E-02
Peak CPS(%)
Uncertainty
18.66
34.74
4.31
43.49
10 .11
20.18
63.12
36.83
65.98
12.64 9.47
18.38
11. 95 21.54
55.19
NUCLIDE MDA REPORT
Peak Type
Sum
Sum
Sum
Page 5 of6
Tolerance
Nuclide
Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\WSRC.NLB
Nuclide Name
Energy
(keV)
Yield(%) Line MDA
(pCi/units)
Nuclide MDA
(pCilunits)
Activity
(pCi/units)
Dec. Level
(pCi/units)
0294
4/2/2018 3:35:09PM Page 6 of 6
Analysis Report for 1803110-02
BLANK
Nuclide Energy Yield(¾) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCilunits) (pCi/units) (pCilunits) (pCi/units)
FE-55 5.89 24.50 4.27E-09 4.27E-09 5.68E-09 2.06E-09
CO-57 122.06 85.51 5.61E+0l 5.61E+0l -5.77E+0l 2.72E+0l
136.48 10.60 4.43E+02 3.03E+02 2.12E+02
NI-59 6.92 29.80 3.32E-08 3.32E-08 4.24E-08 l.60E-08
MO-93 16.59 52.90 6.83E-04 6.83E-04 6.38E-04 3.33E-04
18.60 10.00 l.39E-02 l.08E-02 6.79E-03
NB-93M 16.57 9.43 3.79E-03 3.79E-03 3.54E-03 l.85E-03
CD-109 88.03 3.72 7.97E+02 7.97E+02 3.29E+03 3.90E+02
SN-113 255.12 1. 93 2.13E+03 5.46E+0l -2.28E+02 l.00E+03
391.69 61.90 5.46E+0l l.32E+02 2.62E+0l
SN-119M 23.87 16.10 l.26E-01 l.26E-01 8.98E-01 6.22E-02
25.10 22.70 l.40E-01 l.04E+00 6.89E-02
I-125 35.49 6. 4 9 6.65E+00 6.65E+00 -3.29E+00 3.28E+00
I-129 29.78 57.00 2.17E-01 2.17E-01 l.70E+00 l.07E-01
33.60 13.20 2.23E+00 -5.81E-01 l.l0E+00
39.58 7.52 l.19E+0l -l.03E+0l 5.86E+00
+ BA-133 30.80 * 97.60 l.67E-01 l.67E-01 l.31E+00 8.25E-02
302.84 * 17.80 3.78E+02 l.03E+03 l.83E+02
356.01 * 60.00 l.03E+02 3.39E+02 5.0lE+0l
CE-139 165.85 80.35 6.82E+0l 6.82E+0l 4.14E+0l 3.26E+0l
CE-144 133.54 10.80 4.19E+02 4.19E+02 2.58E+02 2.01E+02
HG-203 279.19 77.30 5.58E+0l 5.58E+0l l.30E+00 2.64E+0l
PB-210 46.50 4.25 2.63E+0l 2.63E+0l -5.95E+0l l.28E+0l
PA-231 9.28 42.00 l.13E-06 l .13E-06 l.29E-06 5.49E-07
10.11 20.20 7.00E-06 7.51E-06 3.40E-06
283.67 1. 60 2.65E+03 l.89E+02 l.25E+03
302. 67 2.30 2.01E+03 2.85E+03 9.58E+02
TH-231 25.64 14.70 2.57E-01 2.57E-01 l.92E+00 l.27E-01
84.21 6.40 3.99E+02 l.64E+03 l.95E+02
PA-234M 9.89 89.00 l.15E-06 l.15E-06 l.31E-06 5.59E-07
21. 72 64. 90 l.33E-02 4.43E-03 6.58E-03
37.93 23.75 2.85E+00 -l.95E+00 l.41E+00
131.42 20.40 2.12E+02 -l.05E+02 l.02E+02
TH-234 63.29 3.80 l.66E+02 l.66E+02 -4.14E+02 8.l0E+0l
NP-237 29.37 14.00 7.93E-01 7.93E-01 6.22E+00 3.92E-01
86.50 12.60 2.22E+02 9.44E+02 l.09E+02
U-237 97.08 16.30 l.34E+02 l.01E+02 -l.51E+0l 6.42E+0l
101.07 26.30 l.01E+02 -l.05E+0l 4.88E+0l
114.00 12.30 3.53E+02 -l.42E+02 l.71E+02
208.01 22.00 2.47E+02 -7.29E+0l l.17E+02
AM-241 59.54 35.90 l.33E+0l l.33E+0l 9.72E-01 6.46E+00
AM-243 74.67 66.00 2.59E+0l 2.59E+0l 6.18E+0l l.27E+0l
+ = Nuclide identified during the nuclide identification
* = Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
0295
105
104
~ 103 ro u V)
O'I 0 r-
1 V)
-1-' C: :::s 0 u
102
101
100
¥ -ls
...... ' ;;!;
I
500 I
1000
-ROI Type: 1
0000064153.CNF
I ' ' 1500 2000 2500
channel
Live Time :900.000 sec Rea 1 Ti me : 901. 800 sec Start: 1: 0.S(kev) Stop : 4096:4097 .3(kev) Acq. Start :Man Apr 02 15:19:56 2018
' 3000 3500
tlllI . ROI Type: 2
4000
0296
4/2/2018 3:35:21PM Page 1 of6
~pex-Gamma Analysis Report for 1803110-03
OU-1-008
GAMMA SPECTRUM ANAL YS/S
Sample Identification
Sample Description
Sample Type
Sample Size
Facility
Sample Taken On
Acquisition Started
Procedure
Operator
Detector Name
Geometry
Live Time
Real Time
Dead Time
Peak Locate Threshold
Peak Locate Range (in channels)
Peak Area Range (in channels)
Identification Energy Tolerance
Energy Calibration Used Done On
Efficiency Calibration Used Done On
Efficiency Calibration Description
Sample Number
: 1803110-03
: OU-1-008 : RA RECOVERY
: 1.000E+00 units
: Countroom
: 4/2/2018 3:18:44PM
: 4/2/2018 3:20:03PM
: BAFIL : Administrator
: GE4 : BAFIL : 900.0 seconds
: 900.3 seconds
: 0.04 %
: 2.50 : 1 - 4096 : 15 - 4096
: 1.000 keV
: 2/24/2018
: 11/9/2014
: 64154
PEAK ANALYSIS REPORT
Peak Analysis Performed on : 4/2/2018 3:35:17PM
Peak No.
Peak Analysis From Channel
Peak Analysis To Channel
Energy (keV)
ROI
start ROI end
: 1 : 4096
Peak Centroid
Net Peak Area
Net Area Uncertainty
Continuum Counts
FWHM (keV)
0297
4/2/2018 3:35:21PM Page 2 of6
Analysis Report for 1803110-03
M m m M m m
M m m m M m
M m m M m
OU-1-008
Peak Energy ROI
No. (keV) start
1 27.62 24 -2 31.10 24 -3 35.37 24 -4 53.61 4 7 -5 62.18 4 7 -6 66.73 4 7 -7 81. 20 75 -8 113.31 108 -9 180.44 177 -
10 304.30 2 99 -11 334.59 330 -12 356.57 350 -13 365.14 362 -14 374.66 371-15 384.58 371 -16 388.16 371 -17 392.15 371 -18 410.57 408 -19 414.66 408 -20 438.04 431 -21 459.59 455 -22 469.50 465 -23 511. 92 505 -24 588.31 584 -
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet Errors quoted at 2.000sigma
ROI end
41 41 41 72 72 72 86
118 183 309 336 361 367 395 395 395 395 417 417 442 462 472 516 590
Peak Net Peak Net Area Continuum
Centroid Area Uncertainty Counts
26.68 2.62E+0l 38.16 1.27E+02
30.16 9.38E+02 67. 71 1.16E+02
34.43 2.41E+02 53.55 8.15E+0l
52.68 2. llE+0l 30.00 1.47E+02
61. 26 1.08E+02 36.00 1.36E+02
65.81 3.94E+0l 34.76 1.27E+02
80.30 4.37E+02 56.43 1. 7 9E+02
112.43 1.14E+02 39.12 1.44E+02
179.61 2.04E+0l 19.80 5.72E+0l
303.58 7.24E+0l 23.10 3.12E+0l
333.89 2.06E+0l 16.57 3.47E+0l
355.89 2.24E+02 35.10 4.13E+0l
364.47 9.79E+00 9.11 8.43E+00
374.00 1.00E+0l 7.40 9.86E+00
383.92 6.86E+0l 23.68 1.41E+0l
387.51 5.82E+0l 24.08 1.08E+0l
391.51 1.82E+0l 18.57 9.74E+00
409.93 8.67E+00 8.00 1.20E+0l
414.03 1.61E+0l 13.56 2.40E+0l
437.43 2.90E+0l 14.56 1.20E+0l
459.00 1.00E+0l 6.32 0.00E+00
468.92 1.20E+0l 6.93 0.00E+00
511.38 3.20E+0l 11. 31 0.00E+00
587.83 6.00E+00 4.90 0.00E+00
BACKGROUND SUBTRACT REPORT
Peak Analysis Performed on : 4/2/2018 3:35: 17PM
Env. Background File : \\OR-GAMMA 1 \ApexRoot\Countroom\Data\0000063827. CNF
Peak Energy Original Orig. Area Ambient Backgr. Subtracted
No. (keV) Area Uncertainty Background Uncert. Area
1 27.62 2.62E+0l 38.16 2.62E+0l
2 31.10 9.38E+02 67.71 9.38E+02
3 35.37 2.41E+02 53.55 2.41E+02
4 53.61 2.llE+0l 30.00 2.llE+0l
5 62.18 1.08E+02 36.00 1.08E+02
FWHM (keV)
2. 72 2.17 2.49 2.78 2.80 2.81 2.25 2.04 2.65 2.69 2.24 2.02 2.79 2.34 2.84 2.80 2.85 2.60 2.60 1. 87 3.00 4.00 3.27 1. 98
Subtracted Uncert.
3.82E+0l 6.77E+0l 5.36E+0l 3.00E+0l 3.60E+0l
0298
4/2/2018 3:35:21PM Page 3 of6
Analysis Report for 1803110-03
OU-1-008
Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted
No. (keV) Area Uncertainty Background Uncert. Area Uncert.
m 6 66.73 3.94E+0l 34.76 3.94E+0l 3.48E+0l
7 81. 20 4.37E+02 56.43 4.37E+02 5.64E+0l
8 113. 31 1.14E+02 39.12 1.14E+02 3.91E+0l
9 180.44 2.04E+0l 19.80 2.04E+0l 1.98E+0l
10 304.30 7.24E+0l 23.10 7.24E+0l 2.31E+0l
11 334.59 2.06E+0l 16.57 2.06E+0l 1.66E+0l
12 356.57 2.24E+02 35.10 2.24E+02 3.51E+0l
13 365.14 9.79E+00 9 .11 9.79E+00 9.llE+00
M 14 374.66 1.00E+0l 7.40 1.00E+0l 7.40E+00
m 15 384.58 6.86E+0l 23.68 6.86E+0l 2.37E+0l
m 16 388.16 5.82E+0l 24.08 5.82E+0l 2.41E+0l
m 17 392.15 1.82E+0l 18.57 1.82E+0l 1.86E+0l
M 18 410.57 8.67E+00 8.00 8.67E+00 8.00E+00
m 19 414.66 1.61E+0l 13.56 1. 61E+0l 1.36E+0l
20 438.04 2.90E+0l 14.56 2.90E+0l 1.46E+0l
21 459.59 1.00E+0l 6.32 1.00E+0l 6.32E+00
22 469.50 1.20E+0l 6.93 1.20E+0l 6.93E+00
23 511. 92 3.20E+0l 11.31 1.30E+0l 9.71E-01 1.90E+0l 1.14E+0l
24 588.31 6.00E+00 4.90 6.00E+00 4.90E+00
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet Errors quoted at 2.000sigma
NUCLIDE IDENTIFICATION REPORT
Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\WSRC.NLB
IDENTIFIED NUCLIDES
Nuclide Id Energy Yield(%) Activity Activity
Name Confidence (keV) (pCi/units) Uncertainty
SN-113 0.91 255.12 1. 93 391.69 * 61,90 2.86E+0l 2.95E+0l
1-125 0.99 35.49 * 6.49 2.16E+02 4.84E+0l
BA-133 0.92 30.80 * 97.60 4.29E+0l 3.20E+00
302.84 17.80 356.01 * 60.00 3.52E+02 7.18E+0l
0299
Analysis Report for 1803110-03
OU-1-008
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity
Energy Tolerance : 1.000 keV
Nuclide confidence index threshold = 0.30
Errors quoted at 2.000sigma
4/2/2018 3:35:21 PM
INTERFERENCE CORRECTED REPORT
? = X = @ =
Nuclide Name
SN-113 I-125 BA-133
Nuclide Id
Confidence
0.914 0.998 0.920
nuclide is part of an undetermined solution
nuclide rejected by the interference analysis
Wt mean Activity
(pCi/units)
2.86E+0l 2.16E+02 4.35E+0l
nuclide contains energy lines not used in Weighted Mean Activity
Errors quoted at 2.000sigma
Wt mean Activity
Uncertainty
2.95E+0l 4.84E+0l 3.20E+00
Page 4 of 6
Comments
0300
Analysis Report for 1803110-03
M
M
m m
M
m m M
m
OU-1-008
Peak Locate Performed on
Peak Locate From Channel
Peak Locate To Channel
Peak No. Energy (keV)
1 27. 62
4 53.61
5 62.18
6 66.73
7 81. 20
8 113.31
9 180.44
10 304.30
11 334.59
13 365.14
14 374.66
15 384.58
16 388.16
18 410.57
19 414.66
20 438.04
21 459.59
22 469.50
23 511.92
24 588.31
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
4/2/2018 3:35:21PM
UNIDENTIFIED PEAKS
: 4/2/2018 3:35:17PM
: 1 : 4096
Peak Size (CPS)
2.90804E-02
2.34171E-02
1.19923E-01
4.37535E-02
4.85230E-01
1.26392E-01
2.26644E-02
8.04419E-02
2.29240E-02
1.08730E-02
l. llll 7E-02
7.62156E-02
6.46793E-02
9.63757E-03
1.79225E-02
3.22222E-02
1. lllllE-02
1.33333E-02
2. 11004E-02
6.66667E-03
Peak CPS(%) Uncertainty
72. 90
71.17 16.68 44.13
6.46
17.20
48.53 15.95
40.15
46.55
36.99 17.26
20.69 46.12
42.05 25.10 31.62
28.87 29.90
40.82
NUCLIDE MDA REPORT
Peak Type
Sum Sum
Tol.
Sum
Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\WSRC.NLB
Page 5 of6
Tolerance Nuclide
U-237
0301
4/2/2018 3:35:21PM Page 6 of6
Analysis Report for 1803110-03
OU-1-008
Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCi/units) (pCilunits) (pCilunits) (pCi/units)
FE-55 5.89 24.50 5.43E-03 5.43E-03 0.00E+00 0.00E+00
CO-57 122.06 85.51 1.70E+0l 1.70E+0l 7.40E-01 7.83E+00
136.48 10.60 1.49E+02 5.13E+0l 6.84E+0l
NI-59 6.92 29.80 7.53E-03 7.53E-03 0.00E+00 0.00E+00
MO-93 16.59 52.90 8.43E-01 8.43E-0l l.03E-02 3.95E-01
18.60 10.00 7.92E+00 l.46E+0l 3.78E+00
NB-93M 16.57 9.43 4. 72E+00 4. 72E+00 5.77E-02 2.21E+00
CD-109 88.03 3. 72 2.80E+02 2.80E+02 -5.68E+0l 1.30E+02
+ SN-113 255.12 1. 93 1.09E+03 6.14E+0l 4.30E+02 4.89E+02
391.69 * 61.90 6.14E+0l 2.86E+0l 2.86E+0l
SN-119M 23.87 16.10 8.51E+00 6.30E+00 5.43E+00 4.05E+00
25.10 22.70 6.30E+00 5.69E-01 2.98E+00
+ I-125 35.49 * 6.49 7.99E+0l 7.99E+0l 2.16E+02 3.87E+0l
I-129 29.78 57.00 1.08E+0l 1.08E+0l 5.61E+0l 5.32E+00
33.60 13. 20 6.0lE+0l 3.11E+02 2.95E+0l
39.58 7.52 4.56E+0l -1.21E+02 2.15E+0l
+ BA-133 30.80 * 97.60 4.12E+00 4.12E+00 4.29E+0l 2.00E+00
302.84 17.80 2.05E+02 2.10E+02 9.58E+0l
356.01 * 60.00 5.15E+0l 3.52E+02 2.36E+0l
CE-139 165.85 80.35 2.41E+0l 2.41E+0l -7.81E+00 1.llE+0l
CE-144 133. 54 10.80 1.40E+02 1.40E+02 4.02E+0l 6.41E+0l
HG-203 279.19 77.30 3.49E+0l 3.49E+0l 1.88E+0l 1.60E+0l
PB-210 46.50 4.25 9.14E+01 9.14E+0l 1.19E+0l 4.25E+0l
PA-231 9.28 42.00 1.32E-02 1.32E-02 0.00E+00 0.00E+00
10 .11 20.20 3.53E-02 0.00E+00 0.00E+00
283.67 1. 60 1.30E+03 -1.32E+02 5.78E+02
302.67 2.30 1.59E+03 1.62E+03 7.42E+02
TH-231 25.64 14.70 1.06E+0l 1.06E+0l -1.59E+00 5.03E+00
84.21 6.40 3.93E+02 l.23E+03 1.91E+02
PA-234M 9.89 89.00 7.52E-03 7.52E-03 0.00E+00 0.00E+00
21. 72 64.90 1.78E+00 1.79E+00 8.48E-01
37.93 23.75 2.22E+0l 4.52E+0l 1.07E+0l
131.42 20.40 7.34E+0l 9.95E+00 3.37E+0l
TH-234 63.29 3.80 2. 91E+02 2.91E+02 3.24E+02 1.39E+02
NP-237 29.37 14.00 4.14E+0l 4.14E+0l 2. 21E+02 2.03E+0l
86.50 12.60 8.12E+0l 1.42E-01 3.77E+0l
U-237 97.08 16.30 6.53E+0l 4.47E+0l -5.13E+0l 3.00E+0l
101.07 26.30 4.47E+0l -1.96E+00 2.07E+0l
114.00 12.30 1.90E+02 3.06E+02 9.06E+0l
208.01 22.00 1.07E+02 2.29E+0l 4.91E+0l
AM-241 59.54 35.90 2.61E+0l 2.61E+0l 2.54E+0l 1.25E+0l
AM-243 74.67 66.00 1.33E+0l 1.33E+0l 7.40E-01 6.21E+00
+ = Nuclide identified during the nuclide identification
* = Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
0302
105
104
~ 103 ro u V)
en 0
..-I
V)
+-' s::: ::::s 0 u
102
500 1000
-ROI Type: 1
1500
0000064154.CNF
2000 channel
2500
Live Time :900.000 sec Real Time :900.320 sec Start: 1: 2.0(kev) stop : 4096:4091.G(kev) Acq. start :Mon Apr 02 15:20:03 2018
3000 3500
ROI Type: 2
4000
0303
4/2/2018 3:51 :24PM Page I of6
pex-Gamma Analysis Report for 1803110-04
OU-1-008
GAMMA SPECTRUM ANALYSIS
Sample Identification
Sample Description
Sample Type
Sample Size
Facility
Sample Taken On
Acquisition Started
Procedure
Operator Detector Name
Geometry
Live Time
Real Time
Dead Time
Peak Locate Threshold
Peak Locate Range (in channels)
Peak Area Range (in channels)
Identification Energy Tolerance
Energy Calibration Used Done On
Efficiency Calibration Used Done On
Efficiency Calibration Description
Sample Number
: 1803110-04
: OU-1-008
: RA RECOVERY
: 1.000E+00 units
: Countroom
: 4/2/2018 3:18:55PM
: 4/2/2018 3:36: 14PM
: BAFIL
: Administrator
: GE4 : BAFIL
: 900.0 seconds
: 900.3 seconds
: 0.03 %
: 2.50
: 1 - 4096
: 15 - 4096
: 1.000 keV
: 2/24/2018
: 11/9/2014
: 64156
PEAK ANALYSIS REPORT
Peak Analysis Performed on : 4/2/2018 3:51:17PM
Peak No.
Peak Analysis From Channel
Peak Analysis To Channel
Energy (keV)
ROI
start
ROI end
: 1 : 4096
Peak Centroid
Net Peak Area
Net Area Uncertainty
Continuum Counts
FWHM (keV)
0304
4/2/2018 3:51:24PM Page 2 of6
Analysis Report for 1803110-04
M m M m
m M m M m
M m
M m M m
OU-1-008
Peak Energy ROI
No. (keV) start
1 31.06 24 -2 35.34 24 -3 62.60 56 -4 66.61 56 -5 81.33 75 -6 113.10 107 -7 276.02 270 -8 286.93 282 -9 295.01 2 91 -
10 303.38 299 -11 333.28 328 -12 356. 72 350 -13 385.74 378 -14 391.89 378 -15 415.39 411 -16 418.95 411 -17 437.86 433 -18 510.34 507 -19 513.30 507 -20 521. 37 51 7 -21 610.36 605 -22 1069.42 1066 -23 1319.10 1316 -
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet Errors quoted at 2.000sigma
ROI Peak Net Peak Net Area Continuum
end Centroid Area Uncertainty Counts
39 30.12 8.53E+02 65.37 1.33E+02
39 34.40 2.15E+02 51.55 9.44E+0l
68 61.69 8.39E+0l 37.26 1.49E+02
68 65.70 1.87E+0l 30.00 1.13E+02
85 80.43 2.91E+02 49.37 1.68E+02
118 112. 22 8.40E+0l 36.00 1.20E+02
281 275.28 3.86E+0l 19.90 3.08E+0l
289 286.19 1.llE+0l 13.71 2.38E+0l
298 294.28 l.80E+0l 12. 96 1.60E+0l
308 302.66 4.23E+0l 21.35 4.35E+0l
338 332.59 1.71E+0l 21.97 5.58E+0l
362 356.04 1.76E+02 27.78 1.20E+0l
396 385.09 7.92E+0l 22.93 7.89E+00
396 391.24 1.73E+0l 16.75 1.62E+0l
420 414.76 1.34E+0l 9.62 7.00E+00
420 418.33 7.69E+00 7.52 5.00E+00
441 437.25 2.65E+0l 14.87 1.70E+0l
516 509.80 1.70E+0l 9.43 2.00E+00
516 512.76 1.15E+0l 11.14 5.89E+00
524 520.83 6.25E+00 6.93 3.50E+00
615 609.90 1.35E+0l 11. 51 9.00E+00
1071 1069.42 3.30E+00 5.39 3.40E+00
1322 1319.36 5.36E+00 6.34 3.29E+00
BACKGROUND SUBTRACT REPORT
Peak Analysis Performed on : 4/2/2018 3:51: 17PM
Env. Background File : \\OR-GAMMA 1 \ApexRoot\Countroom\Data\0000063827 .CNF
Peak Energy Original Orig. Area Ambient Backgr. Subtracted
No. (keV) Area Uncertainty Background Uncert. Area
1 31.06 8.53E+02 65.37 8.53E+02
2 35.34 2.15E+02 51.55 2.15E+02
3 62.60 8.39E+0l 37.26 8.39E+0l
4 66.61 1.87E+0l 30.00 1.87E+0l
5 81.33 2.91E+02 49.37 2. 91E+02
6 113.10 8.40E+0l 36.00 8.40E+0l
FWHM (keV)
2.20 2.32 3.06 2.22 2.17 2.29 2.56 2.70 2.22 1. 81 1. 86 2.04 3.44 2.85 2.86 2.26 1. 50 3.21 2.65 1.11 2.14 1. 65 3.30
Subtracted Uncert.
6.54E+0l 5.15E+0l 3.73E+0l 3.00E+0l 4.94E+0l 3.60E+0l
0305
4/2/2018 3:51:24PM Page 3 of6
Analysis Report for 1803110-04
OU-1-008
Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted
No. (keV) Area Uncertainty Background Uncert. Area Uncert.
7 276.02 3.86E+0l 19.90 3.86E+0l 1.99E+0l
8 286.93 1.llE+0l 13.71 1.llE+0l 1.37E+0l
9 295.01 1.80E+0l 12. 96 1.80E+0l 1.30E+0l
10 303.38 4.23E+0l 21.35 4.23E+0l 2.14E+0l
11 333.28 1.71E+0l 21.97 1.71E+0l 2.20E+0l
m 12 356.72 1.76E+02 27. 78 1.76E+02 2.78E+0l
M 13 385.74 7.92E+0l 22.93 7.92E+0l 2.29E+0l
m 14 391.89 1.73E+0l 16.75 1.73E+0l 1.67E+0l
M 15 415.39 1.34E+0l 9.62 1.34E+0l 9.62E+00
m 16 418.95 7.69E+00 7.52 7.69E+00 7.52E+00
17 437.86 2.65E+0l 14.87 2.65E+0l 1.49E+0l
M 18 510.34 1.70E+0l 9.43 1.70E+0l 9.43E+00
m 19 513.30 1.15E+0l 11.14 1.15E+0l 1. llE+0l
20 521.37 6.25E+00 6.93 6.25E+00 6.93E+00
21 610.36 1.35E+0l 11. 51 1.29E+00 1.12E+00 1.22E+0l 1.16E+0l
22 1069.42 3.30E+00 5.39 3.30E+00 5.39E+00
23 1319.10 5.36E+00 6.34 5.36E+00 6.34E+00
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
NUCLIDE IDENTIFICATION REPORT
Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\WSRC.NLB
IDENTIFIED NUCLIDES
Nuclide Id Energy Yield(%) Activity Activity
Name Confidence (keV) (pCilunits) Uncertainty
SN-113 0.94 255.12 1.93 391.69 * 61.90 2. 72E+0l 2.66E+01
I-125 0.99 35.49 * 6.49 1.92E+02 4.64E+0l
BA-133 0. 96 30.80 * 97.60 3.89E+0l 3.07E+00
302.84 * 17.80 2.08E+02 1.23E+02
356.01 * 60.00 2.77E+02 5.66E+01
PA-231 0.99 9.28 42.00 10 .11 20.20
283.67 1. 60 302.67 * 2.30 1.61E+03 9.53E+02
TH-234 0.92 63.29 * 3.80 3.64E+02 1.64E+02
0306
Analysis Report for 1803110-04
OU-1-008
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity
Energy Tolerance: 1.000 keV
Nuclide confidence index threshold = 0.30
Errors quoted at 2.000sigma
4/2/2018 3:51 :24PM
INTERFERENCE CORRECTED REPORT
? = X =
Nuclide Name
SN-113 I-125 BA-133 PA-231 TH-234
Nuclide Id
Confidence
0.941 0. 996 0. 962 0.995 0.927
nuclide is part of an undetermined solution
nuclide rejected by the interference analysis
Wt mean Activity
(pCi/units)
2.72E+0l 1.92E+02 3.96E+0l 1.31E+03 3.64E+02
@ = nuclide contains energy lines not used in Weighted Mean Activity
Errors quoted at 2.000sigma
Wt mean Activity
Uncertainty
2.66E+0l 4.64E+0l 3.07E+00 9.53E+02 1.64E+02
Page 4 of6
Comments
0307
Analysis Report for 1803110-04
m
M
M
m
M
m
OU-1-008
Peak Locate Performed on
Peak Locate From Channel
Peak Locate To Channel
Peak No. Energy (keV)
4 66.61
5 81.33
6 113.10
7 276.02
8 286.93
9 295.01
11 333.28
13 385.74
15 415.39
16 418.95
17 437.86
18 510.34
19 513.30
20 521.37
21 610.36
22 1069.42
23 1319.10
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
4/2/2018 3:51:24PM
UNIDENTIFIED PEAKS
: 4/2/2018 3:51:17PM
: 1 : 4096
Peak Size (CPS)
2.07732E-02
3.23101E-01
9.33333E-02
4.29012E-02
1.23188E-02
2.00000E-02
1.90247E-02
8. 7 9683E-02
1.48468E-02
8.54903E-03
2.94444E-02
1.89280E-02
1.27578E-02
6.94444E-03
1.35676E-02
3.66667E-03
5.95238E-03
Peak CPS(%) Uncertainty
80.24 8.49
21.43
25.77
61.84
36.00 64.14 14.48
35.99 48.85
28.05 27.69
48.49
55.43 47.36
81.59 59.21
NUCLIDE MDA REPORT
Peak Type
Sum
Tol.
Sum
Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\WSRC.NLB
Page 5 of6
Tolerance Nuclide
U-237
0308
4/2/2018 3:51:24PM Page 6 of6
Analysis Report for 1803110-04
OU-1-008
Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCilunits) (pCi/unlts) (pCilunits) (pCl/units)
FE-55 5.89 24.50 5.43E-03 5.43E-03 0.00E+00 0.00E+00
CO-57 122.06 85.51 1.61E+0l 1.61E+0l -3.70E-01 7.41E+00
136.48 10.60 1.53E+02 -l.30E+0l 7.07E+0l
NI-59 6.92 29.80 7.53E-03 7.53E-03 0.00E+00 0.00E+00
MO-93 16.59 52.90 8.43E-01 8,43E-01 3.65E-01 3.95E-01
18.60 10.00 7.40E+00 1.05E+0l 3.51E+00
NB-93M 16.57 9.43 4. 72E+00 4. 72E+00 2.04E+00 2.21E+00
CD-109 88.03 3. 72 2.40E+02 2.40E+02 -9.13E+0l 1.10E+02
+ SN-113 255.12 1. 93 9.91E+02 4.20E+0l -4. 13E+02 4.40E+02
391.69 * 61.90 4.20E+0l 2.72E+0l 1.89E+0l
SN-119M 23.87 16.10 7.95E+00 6.05E+00 1.03E+00 3.77E+00
25.10 22.70 6.05E+00 -1.23E+00 2.86E+00
+ I-125 35.49 * 6.49 7.69E+0l 7.69E+0l 1.92E+02 3.73E+0l
I-129 29.78 57.00 1.03E+0l 1.03E+0l 4.79E+0l 5.05E+00
33.60 13. 20 5.69E+0l 2.82E+02 2.79E+0l
39.58 7.52 3.89E+0l -1.51E+00 1.82E+0l
+ BA-133 30.80 * 97.60 3.97E+00 3.97E+00 3.89E+0l 1.92E+00
302.84 * 17.80 1.51E+02 2.08E+02 6.87E+0l
356.01 * 60.00 4.0lE+0l 2.77E+02 1.79E+0l
CE-139 165.85 80.35 2.12E+0l 2.12E+0l -1.14E+0l 9.63E+00
CE-144 133. 54 10.80 1.47E+02 1.47E+02 4.19E+0l 6.78E+0l
HG-203 279.19 77.30 3.45E+0l 3.45E+0l 2.49E+0l 1.58E+0l
PB-210 46.50 4.25 9.14E+0l 9.14E+0l 9.89E+00 4.25E+0l
+ PA-231 9.28 42.00 1.32E-02 1.32E-02 0.00E+00 0.00E+00
10.11 20.20 3.53E-02 0.00E+00 0.00E+00
283.67 1. 60 l.30E+03 2.43E+02 5.78E+02
302.67 * 2.30 l.17E+03 1.61E+03 5.31E+02
TH-231 25.64 14.70 1.09E+0l 1.09E+0l -1.39E+00 5.18E+00
84.21 6.40 3.37E+02 9.23E+02 1.63E+02
PA-234M 9.89 89.00 7.52E-03 7.52E-03 0.00E+00 0.00E+00
21. 72 64.90 1.67E+00 5.67E-01 7.92E-01
37.93 23.75 2.02E+0l 3.81E+0l 9.71E+00
131.42 20.40 7.l0E+0l -1.20E+0l 3.25E+0l
+ TH-234 63.29 * 3.80 3.05E+02 3.05E+02 3.64E+02 1.47E+02
NP-237 29.37 14.00 4.00E+0l 4.00E+0l 2.07E+02 1.96E+0l
86.50 12.60 7.30E+0l 1.34E+0l 3.36E+0l
U-237 97.08 16.30 6.67E+0l 4.56E+0l -4.43E+0l 3.07E+0l
101.07 26.30 4.56E+0l 1.06E+0l 2.llE+0l
114.00 12.30 1.66E+02 2.57E+02 7.89E+0l
208.01 22.00 9.26E+0l 1.29E+00 4.21E+0l
AM-241 59.54 35.90 2.35E+0l 2.35E+0l 2.46E+0l 1.12E+0l
AM-243 74.67 66.00 1.30E+0l 1.30E+0l -1.77E+00 6.07E+00
+ = Nuclide identified during the nuclide identification . = Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
0309
105
104
~ 103 rd u V)
O'l 0 r-
1 V)
+-' C :::I 0 u
102
101
~
~ ~ :r-
'7 ;;'i -~
-i
~·1 ~
100 WI "1'12 • , r,
500 1000
1111 ROI Type: 1
1500
0000064156.CNF
2000 channel
2500
Live Time :900.000 sec Real Ti me : 900. 290 sec Start: 1: 2. 0(kev) Stop : 4096: 4091. 6(kev) Acq. Start :Mon Apr 02 15:36:14 2018
3000 3500
ROI Type: 2
4000
0310
SECTION XIV
ANALYTICAL DATA (GROSS ALPHA/BETA)
0311
Eberline Services Oak Ridge Laboratory
Analysis Sheet
Work Order 18-031.10 Analysis Code I GaGbT _ThSr J
Run 1 Date Received 3/23/2018
Lab Deadline 4/12/2018
Client I AMO Environmental Decisions
Project WESTLAKE
Report Level 4
Activity Units pCi
Aliquot Units
Matrix WA
Method EPA 900.0 Modified
Instrument Type Alpha/Beta GPC
Radiometric Tracer
Radiometric Sol#
Tracer Act (dpm/g)
Carrier
Carrier Cone (mg/ml)
Internal Fraction
01 --
02
03
04
I.
....,__ ____ ,.......
I ,__ !
I I ! l ·, I
i L i I I -
i ' i
I
Sample / Desc I
I
LCS I
MBL
DUP
DO
18-03110 GaGbT_ThSr
Run 1
Client ID
I
I ! Login CPM
LCS i -~+- . -- _____ !
BLANK j
OU-1-008 i 38 7
I i
OU-1-008 i
38
I
' l
-- .
I
• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. A Indicates estimated SAF value.
•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Printed: 312712018 4:09 AM Page 1 of 3
Sample Sample Date Aliquot
03/23/18 00:00 1.0000E+00 ·-··-·~-
03/23/18 00:00 1.0000E+00
03/19/18 18:02 2.0000E-01
03/19/18 18:02 2.0000E-01 --
--
·-
I
0312
Eberline Services Oak Ridge Laboratory
Analysis Sheet
I Internal Sample l Tracer
Fraction Desc [ Aliquot(g)
01 LCS
02 MBL
03 DUP
04 DO
Tracer Total ACT(dpm)
i I
Radiometric Tracer (pCi)
I
18-03110 GaGbT_ThSr
Run 1
Radiometric I Grav Carrier I Grav Filter
% Rec Added (ml) [ Tare (g)
0.00 7.7518
0.00 7.7368
' 0.00 7.7136
0.00 7.7781
Grav Filter Final (g)
7.7519
7.7369
7.7914
7.8585
* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. "Indicates estimated SAF value.
** Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
I I I Grav Filter Grav
Net(g) %Rec
0.0001
0.0001
0.0778
0.0804
Printed: 312712018 4:09 AM Page 2 of 3
I
I Mean
I
SAF SAF %Rec 1* 2*
1.00 1.00
1.00 1.00
1.00 1.00
1.00 1.00
0313
Eberline Services
Oak Ridge Laboratory
Analysis Sheet
Internal [ Sample Fraction Desc
01 LCS
02 MBL
03 DUP
04 DO
I Rough Prep
I Rough Prep
Date By I Prep
I Date
03/27/18 03:01
03/27/18 03:01
03/27/18 03:01
03/27/18 03:01
I I
18-03110 GaGbT_ThSr
Run 1
I I
Prep
l By i
MHIGHTOWER
MHIGHTOWER
MHIGHTOWER
MHIGHTOWER
-·
l
I Sep to
I Date/Time
I
I I
i I
i I
I
• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. A Indicates estimated SAF value.
** Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
I Sep to
I By I
Printed: 3/2712018 4:09 AM Page 3 of 3
Sep t1 Sep t1 Date/Time By
I
I
0314
Eberline Analytical Oak Ridge Laboratory
~ Lab Nuclide
Fraction
01 GROSS ALPHA
i::: 02 GROSS ALPHA
::: ""'" a:: 03 GROSS ALPHA
1--04 GROSS ALPHA
.c ~ C) ~ Ill ca i::: q; C)
II) s::: 0 II)
·c:; a, C ca -ii s::: a, E s::: 0 ... ·s: s::: w 0 :E <(
I Sample Oesc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03110-GaGbT-1
Client Activity Results Error Estimate I MOA
Identification Units
LCS pCi/1 3.10E+02 3.98E+00 2.54E-01
BLANK pCi/1 3.97E-02 1.35E-01 3.01E-01
OU-1-008 pCi/1 2.S0E+00 1.94E+00 3.35E+00
OU-1-008 pCi/1 4.25E+00 1.96E+00 2.55E+00
LCS
I LCS
Known %R
2.68E+02 115.57
Printed: 3/27/2018 9:24 AM Page 1 of 3
LCS
I RPO MOA Blank
Flag Flag Flag Flag
OK OK
OK OK
NA OK
OK
0315
Eberline Analytical Oak Ridge Laboratory
~ Lab
Nuclide Fraction
01 GROSS ALPHA
§ a::
~ 8 ,!!? ~ cii C: <:t
~I
~
1-.c C) ca
C)
(/) C
.2
.!!? (.J Cl)
C ca -C Q)
E C 0 a..
"> C w 0 :!: <(
02 GROSS ALPHA
03 GROSS ALPHA
04 GROSS ALPHA
I Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-0311 0-GaGbT-1
Sample Sample I Radiometric
I Grav Mean
Date Aliquot %Rec %Rec %Rec
03/23/18 00:00 1.00E+00 0.00 0.00 0.00
03/23/18 00:00 1.00E+00 0.00 0.00 0.00
03/19/18 18:02 2.00E-01 0.00 0.00 0.00
03/19/18 18:02 2.00E-01 0.00 0.00 0.00
SAF
1.00
1.00
2.62
2.68
SeptO
Printed: 3/27/2018 9:24 AM Page 2 of 3
Sept1
DatefTime DatefTime
0316
Eberline Analytical Oak Ridge Laboratory
( Lab Nuclide
Fraction
01 GROSS ALPHA
c:: ::,
0::
.g 0 0 -!!! ~ Ill c::
Cl;
j 0
~
I-..a (!) ns
(!)
1/j C: 0
.!!? CJ Q)
C
s C: Q)
E C: 0 ... ·s: C: w 0 :ii: <(
02 GROSS ALPHA
03 GROSS ALPHA
04 GROSS ALPHA
I Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-0311 0-GaGbT-1
Halflife
I I Bkg
Counting Detect CalTier Count
Counts DatefTime (days) Time CPM
03/27/18 07:02 LB4110A B1 120 2330510.066666667
03/27/18 07:02 LB4110A B2 120 15 0.1
03/27/18 07:02 LB4110A B3 120 24 0.066666667
03/27/18 07:02 LB4110A B4 120 28 0.033333333
I
I
Printed: 3/27/2018 9:24 AM Page 3 of 3
Eff
0.2821
0.2835
0.2804
0.2843
0317
Eberline Analytical Oak Ridge Laboratory
( Lab Nuclide Fraction
01 GROSS BETA
§ II::
.g 8 -~ ~ qj c:: "(
--~ 0
~
1-.c (!) «s
(!)
(/) C .2 .!!? (.) Q)
C
s C Q)
E C e
·s;: C w 0 :iii: <(
02 GROSS BETA
03 GROSS BETA
04 GROSS BETA
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-0311 0-GaGbT-1
I
Client Activity Results Error Estimate I MDA
Identification Units
LCS pCi/1 2.82E+02 3.15E+00 6.12E-01
BLANK pCi/I -2.37E-01 2.57E-01 5.78E-01
OU-1-008 pCi/I 1.95E+01 2.46E+00 3.43E+00
OU-1-008 pCi/I 1.69E+01 2.31E+00 3.30E+00
I LCS LCS Known %R i
2.77E+02 101.91
Printed: 3/27/2018 9:24 AM Page 1 of 3
I I LCS RPD MDA Blank
Flag Flag Flag Flag
OK OK
OK OK
OK OK
OK
0318
Eberline Analytical Oak Ridge Laboratory
( Lab Nuclide
Fraction
01 GROSS BETA
i::: 02 GROSS BETA
::s T"'" 0:: 03 GROSS BETA
Cl> I-"0
8 .c 04 GROSS BETA
,!2 C) ~ 111 ca i::: C) "'(
II) C .2 .!!! 0 Cl)
C
.l!! jl C Cl)
0 E C 0 ... "> C w 0 :!?: <(
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03110-GaGbT-1
Sample Sample Radiometric Grav
I Mean
Date Aliquot %Rec %Rec %Rec
03/23/18 00:00 1.00E+00 0.00 0.00 0.00
03/23/18 00:00 1.00E+00 0.00 0.00 0.00
03/19/18 18:02 2.00E-01 0.00 0.00 0.00
03/19/18 18:02 2.00E-01 0.00 0.00 0.00
SAF
1.00
1.00
1.17
1.18
SeptO
Printed: 3/27/2018 9:24 AM Page 2 of 3
Sept1 I Date/Time I
Date/Time
0319
Eberline Analytical Oak Ridge Laboratory
~ Lab I Nuclide
Fraction
01 GROSS BETA
C: ::s a:
.g 8 ,!!? ~ ai C: ct
~I
""""'
1-.c (!)
CG (!)
,,, C: 0
-~ c., Q)
C ni -C: Q)
E C: 0 ... ·s; C: w 0 :iii: <(
02 GROSS BETA
03 GROSS BETA
04 GROSS BETA
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-0311 0-GaGbT-1
Counting Halflife Detect Carrier
I Count
Counts DatefTime (days) Time
03/27/18 07:02 LB4110A B1 120 42352
03/27/18 07:02 LB4110A B2 120 131
03/27/18 07:02 LB4110A B3 120 568
03/27/18 07:02 LB4110A B4 120 519
Bkg CPM
1.466666667
1.35
1.266666667
1.233333333
Printed: 3/27/2018 9:24 AM Page 3 of 3
Eff Ato B, Cor
0.4817 302.8858458
0.4903 1.091666667
0.4703 4. 733333333
0.484 4.325
0320
Count Room Report Client: AMO Environmental Decisio
18-03110-GaGbT_ThSr-1 (pCi/1) in WA Tracer ID:
Printed: 312712018 4:09 AM Page 1 of 1
Internal Sample Client Sample i Sample Tracer Tracer I
Radiometric I Radiometric
11 SAF
11 SAF
Fraction Desc ID Date Aliquot Aliquot {g) ACT (dpm) Tracer (pCi) % Rec 1* 2• I I
01 LCS LCS 03/23/18 00:00 1.0000 l 0.00 1.00 1.00
02 MBL BLANK 03/23/18 00:00 1.0000 0.00 1.00 1.00
03 DUP OU-1-008 03/19/1818:02 0.2000 0.00 1.00 1.00 I
04 DO OU-1-008 03/19/18 18:02 0.2000 I 0.00 1.00 1.00
I I
! !
--- i i
0321
Eberline Services Oak Ridge Laboratory
LCS & Matrix Spikes
I Sol# Actwity I Solution
Isotope dpmlg ! Date
Am-241 NB-07 I
593.680! 3/27/2018
SrY-90 NB-07 612.180 3/27/2018 -
I IC-::J::J 1v1v IC-La .:.,u.,_,.4'! _,, //LU I I
Tracers
fraction Isotope I Sol# I Activity dpmlg
i i I
I i I I I
I
Version 2.0 08/99
\ Approx 1 Addff.ion
0.800
0.900
U. I
Solution Date
Spike and Tracer Worksheet
Analysis Code Date Technician
GaGbT ThSr 3/27/2018 3:00 MHIGHTOWER
LCS MS LCSD MSD LCS MS
Volume Volume Volume Volume Known I Error Added i Error
Used (g) Used (g) Used(g) Used(g) pCi [ Estimate pCi I Estimate
1.0030 268.231 11.534 O.OOi 0.000
1.0030 276.58! 8.298 0.00 0.000
I i
Balance Printer Tapes
Volume Approx Tracer Used (g) Addition
Page 1 of 1 Printed: 3/27/2018 3:01 AM
Technician Initials Witness Initials
Jltlf, LCSD MSD
Known Error Added i Error
pCi Estimate pCi I Estimate
0 00 0.000 I 0.00! 0.000
0.00 0.000 o.ooi 0.000 I
i I
LCS
Matrix Spike
0322
Lab
Eberline Analytical Oak Ridge Laboratory
AMO Environmental Decisions
GaGbT_ThSr
Sample Muffle Data
Fraction Ratio
Client ID Type Post/Pre
01 LCS LCS 02 BLANK MBL 03 OU-1-008 DUP
04 OU-1-008 DO
--·---
-------
--------------
··-··----··
------------~--- ---
-----
Comments
/-----i ;/ ,., !'\'</ j// - ;J -- ~.
Technician: ~ {,,U.-,/'vl!l--,,0,
J
Aliquot Worksheet
liters 4/12/2018
Dilution Data Aliquot Data
No of Dils I Dil Factor ! Ratio Aliquot Net Equiv
! 1.0000E+00 1.0000E+00 . ---··----··---··-·--·--
1----·-----------· I 1.0000E+00 1.0000E+00
2.0000E-01 2.0000E-01
2.0000E-01 2.0000E-01
--- --- -- --------
---···-------
i
i -----·-------
---+. --r -·-·· -1- ···-··· -- - ---·-- --
-------
----·--------
__ ,, _______ ----------
Date: '2:) / ~ / ~
Printed: 3/26/201811:47 AM Page 1 of 1
JPACHELLA
MS Aliquot Data H-3 Solids Only Water Added H3 Dist
Aliquot Net Equiv (ml) Aliq
·-------·-·--··-----
------·-··--·-~-
-.--~----
-- . -·--------·--··-·-· -
---~--l
0323
Eberline Services - Oak Ridge Version 1.09/1999 Gravimetric Worksheet
Work Order
18-03110 ~ Analysis
Code
GaGbT_ThSr
Gravimetric
Carrier
TRetec AMO Environmental Decisions Sample Carrier Data Filter Data
Carrier Added Filter Tare Filter Final
Fraction Client ID Type (ml) (g) (g)
01 LCS LCS 7.7518 7.7519
02 BLANK MBL 7.7368 7.7369
03 DUP DUP 7.7136 7.7914
04 OU-1-008 DO 7.7781 7.8585
Technician: h:n Date: J_;l 1 1_!1
Carrier Cone {mg/m!)
Filter Net (g)
0.0001 0.0001 0.0778 0.0804
Printed: 3/27/2018 4:09 AM Page 1 of 1
Technician
MHIGHTOWER
Gravimetric %
Recovery
0324
Eberline Analytical - Oak Ridge Version 1.1 10/2015
TRetec AMO Environmental Decisions
Fraction Client ID
04 OU-1-008
-----
' .. -'1 ,, f-L..J-o l /l ;J
Technician: ~ t).J-fve,/(_J__L,e____ I
I >" V
TDS / TSS Worksheet
Cede
GaGbT ThSr
Filter Data Aliquot Filter Tare Filter Final
I Filter Net
ml (g) (g) (g)
Printed: 3/26/2018 11 :47 AM Page 1 of 1
JPACHELLA
TDS/TSS Maximum Aliq
(mg/L) (ml)
100.0000 7.7727 7.7728 +--- -__ 0.0001_
1.0000 100000.00 ---- ---- - - ···- - --···-·-- ------ -···--- - -------. -
- -··- _______ ,, _________________
-------· -------------- ---·---- ---·--·---------------·- ______ ,. ______ . __ --- . --"··· - - --·--·--
·-·--------·--·- --- ---- ----------·-
-·---- ---- -- - -------------··- ----------------- -------·----------
----· ------- ----
---- - --------- ----- . .. ·--- "--- -·- -------- ----
------- ----·-- --------
_I ______ ·---~------ --- -----------
------------- ------------·-------·--- ------~-----------·-·--
-··-··-· - --- ------ ---------·-··--·- ---- --~~ --··-- - -~
--··~-·· ---·-·------- .~
i ---~-·----
Date: 0 I ~l_jj_
0325
Detector ID Sample ID Alpha Beta Count Time Voltage TOD K? B1 1803110-01 23305 42352 120 1410 3/27/2018 7:02:03 AM
B2 1803110-02 15 131 120 1410 3/27/2018 7:02:03 AM ·5 ;-zt-/! t:) B3 1803110-03 24 568 120 1410 3/27/2018 7:02:04 AM
B4 1803110-04 28 519 120 1410 3/27/2018 7:02:04 AM
0326
Eberline Analytica Oak Ridge Laboracory
[ Detector
LB4110A - Al
LB4110A - A2
LB4110A - A3
LB4110A - A4
LB4110A - Bl
LB4110A - B2
LB4110A - B3
LB4110A - B4
LB4110A - Cl
LB4110A - C2
LB4110A - C3
LB4110A - C4
LB4110A - D1
LB4110A - D2
LB4110A - D3
LB4110A - D4
LB4110A - El
LB4110A - E2
LB4110A - E3
LB4110A - E4
I_B4110A - Fl
LB4110A - F2
LB4110A - F3
LB4110A - F4
LB4110A - Gl
LB4110A - G2
LB4110A - G3
L.B4110A - G4
Alpha/Beta Calibration Date
Alpha 10/20/2015
Alpha 10/20/2015
Alpha 10/20/2015
Alpha 10/20/2015
Alpha 10/20/2015
Alpha 10/20/2015
Alpha 10/20/2015
Alpha 10/20/2015
Alpha 10/20/2015
Alpha 10/20/2015
Alpha 10/20/2015
Alpha 10/20/2015
Alpha 10/20/2015
Alpha 10/20/2015
Alpha 10/20/2015
Alpha 10/20/2015
Alpha 10/20/2015
Alpha 10/20/2015
Alpha 10/20/2015
Alpha 10/20/2015
Alpha 10/20/2015
Alpha 10/20/2015
Alpha 10/20/2015
Alpha 10/20/2015
Alpha 10/20/2015
Alpha 10/20/2015
Alpha 10/20/2015
Alpha 10/20/2015
GPC Detector Report (ALL Backgrounds)
Count Date Bkg CPM
3/27/2018 1.00E-01
3/27/2018 5.00E-02
3/27/2018 6.67E-02
3/27/2018 1.33E-01
3/27/2018 6.67E-02,
3/27/2018 1.00E-01
3/27/2018 6.67E-02'
3/27/2018 3.33E-02,
3/27/2018 1.17E-01
3/27/2018 5.00E-02
3/27/2018 5.00E-02
3/27/2018 1.17E-01
3/27/2018 1.00E-01
3/27/2018 1.67E-01
3/27/2018 1.17E-01
3/27/2018 1.33E-01
3/23/2018 0.00E+00
3/23/2018 0.00E+00
3/23/2018 0.00E+00
3/23/2018 0.00E+00
1/13/2017 1.67E-02
1/13/2017 3.33E-02
1/13/2017 3.33E-02
1/13/2017 6.67E-02
3/27/2018 1.67E-02
3/27/2018 1.00E-01
I
3/27/2018 1.00E-01 j 3/27/2018 1.67E-02
PFW LCL
p -5.87E-02
p -5.59E-02
p -4.69E-02
p -4.78E-02
p , -5.02E-02
p -3.05E-02
p -6.53E-02
p -5.37E-02
p -7.06E-02
p -6.00E-02
p -7.35E-02
p -5.51E-02
p -4.22E-02
p -3.58E-02
p -5.50E-02
p -2.92E-02
p -3.12E+0l
p -3.93E-02
p -6.26E-02
p -3.22E+0l
p -7.24E-02
p -1.97E-01
p -8.54E-02
p -5.55E-02
p -5.76E-02
p -5.47E-02
p -5.33E-02
p -3.00E-02
Mean
9.77E-02
8.94E-02
1.05E-01
9.16E-02
1.06E-01
1.18E-01
9.26E-02
8.44E-02
9.56E-02
7.03E-02
9.34E-02
8.30E-02
1.54E-01
1.38E-01
1.14E-01
1.43E-01
6.llE-01
6.40E-02
1.18E-01
5.72E-01
9.77E-02
7.60E-02
1.27E-01
8.28E-02
8.59E-02
7.74E-02
1.19E-01
8.94E-02
Printed:
KP 3/27/2018 6:54 AM)!Zt-/18
Page 1 of 1
UCL
2.54E-01
2.35E-01
2.57E-01 I 2.31E-01 I 2.63E-01
2.67E-01
2.50E-01
2.23E-01
2.62E-01
2.0lE-01 I 2.60E-01
2.21E-01
3.50E-01
3.13E-01
2.84E-01
3.16E-01
3.24E+0l
1.67E-01
2.99E-01
3.34E+0l
2.68E-01
3.49E-01
3.40E-01
2.21E-01
2.29E-01
2.l0E-01
2.91E-01
2.09E-01
0327
Eberline Analytical Oak Ridge Laboratory
lF h Detector
LB4110A - Al
LB4110A - A2
LB4110A - A3
LB4110A - A4
LB4110A - Bl
LB4110A - B2
LB4110A - B3
LB4110A - B4
LB4110A - Cl
LB4110A - C2
LB4110A - C3
LB4110A - C4
LB4110A - D1
LB4110A - D2
LB4110A - D3
LB4110A - D4
_B4110A - El
i_B4110A - E2
_B4110A - E3
_B4110A - E4
_B4110A - Fl
_B4110A - F2
_B4110A - F3
_B4110A - F4
LB4110A - Gl
LB4110A - G2
LB4110A - G3
I_B4110A - G4 -
Alpha/Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Calibration Date
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
GPC Detector Report (ALL Backgrounds)
Count Date Bkg CPM
3/27/2018 1.48E+OO
3/27/2018 1.42E+OO
3/27/2018 1.28E+OO
3/27/2018 1.55E+OO
3/27/2018 1.47E+OO•
3/27/2018 1.35E+OO'
3/27/2018 1.27E+OO
3/27/2018 1.23E+OO ·
3/27/2018 1.18E+OO
3/27/2018 1.20E+OO
3/27/2018 2.12E+OO
3/27/2018 1.lOE+OO
3/27/2018 l.33E+OO
3/27/2018 1.47E+OO
3/27/2018 l.07E+OO
3/27/2018 1.45E+OO
3/23/2018 3.33E-02
3/23/2018 1.67E-02
3/23/2018 6.67E-02
3/23/2018 O.OOE+OO
1/13/2017 5.50E-01
1/13/2017 3.42E+OO
1/13/2017 8.52E+OO
1/13/2017 6.57E+OO
3/27/2018 1.35E+OO
3/27/2018 1.75E+OO
3/27/2018 1.43E+OO
3/27/2018 1.25E+OO
I PFW I LCL
p 8.58E-01
p I 9.14E-01
p I 1.04E+OO
p 2.37E-02
p 1.05E+OO
p 7.79E-01
p 9.46E-01
p 8.18E-01
p 8.76E-01
p 2.32E-01
F 9.13E-01
p 8.02E-01
p -2.15E+OO
p -l.31E+OO
p -9.89E-01
p -1.44E+OO
p -4.88E+Ol
p 5.69E-01
p 6.34E-01
p -5.22E+Ol
p 6.30E-01
F -4.00E+02
F -4.94E+OO
f -4.32E+OO
p 8.24E-01
p 1.14E+00
p 8.60E-01
p 7.12E-01
Mean
1.44E+OO
1.50E+OO
1.58E+OO
1.54E+OO
1.61E+OO
1.54E+OO
1.45E+OO
1.44E+OO
1.34E+OO
1.19E+OO
1.75E+OO
l.27E+OO
2.04E+OO
2.12E+OO
1.76E+OO
2.17E+OO
2.19E+OO
9.46E-01
1.19E+OO
1.87E+OO
1.44E+OO
2.09E+Ol
2.12E+OO
l.79E+OO
l.29E+OO
1.65E+OO
1.42E+OO
1.36E+OO
{\y Printed: 3/27/2018 6:54 AM '5/ZM8
Page 1 of 1
UCL
2.03E+OO
2.08E+OO
2.12E+OO
3.05E+OO
2.17E+OO
2.30E+OO
1.96E+OO
2.07E+00
1.81E+OO
2.15E+OO
2.59E+OO
1.74E+OO
6.23E+OO
5.54E+OO
4.51E+OO
5.78E+OO
5.32E+Ol
l.32E+OO
1.75E+OO
5.59E+Ol
2.25E+OO
4.42E+02
9.17E+OO
7.90E+OO
1.75E+OO
2.17E+OO
1.98E+OO
2.02E+OO
0328
Eberline Analytical Oak Ridge Labo-atory
I Dete:tor
LB4110A - Al
LB4110A - A2
LB4110A - A3
LB4110A - A4
LB4110A - Bl
LB4110A - B2
LB4110A - B3
LB4110A - B4
LB4110A - Cl
LB4110A - C2
LB4110A - C3
LB4110A - C4
LB4110A - D1
LB4110.A - D2
LB4110.A - D3
LB4110A - D4
LB4110A - El
LB4110A - E2
LB4110A - E3
LB4110.A - E4
LB4110A - Fl
LB4110A - F2
LB4110A - F3
LB4110A - F4
LB4110A - Gl
LB4110/\ - G2
LB4110J\ - G3
LB4110A - G4
Alpha/Beta
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Calibration Date I 10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
GPC Detector Report (ALL Efficiencies)
Count Date Eff
3/27/2018 0.2265
3/27/2018 0.2101
3/27/2018 0.1984
3/27/2018 0.2248
3/27/2018 0.2260
3/27/2018 0.2019
3/27/2018 0.2361
3/27/2018 0.2204
3/27/2018 0.2067
3/27/2018 0.2201
3/27/2018 0.2398
3/27/2018 0.2126
3/27/2018 0.2200
3/27/2018 0.2534
3/27/2018 0.2549
3/27/2018 0.1958
3/23/2018 0.0000
3/23/2018 0.0000
3/23/2018 0.0000
3/23/2018 0.0000
1/13/2017 0.0095
1/13/2017 0.0912
1/13/2017 0.1614
1/13/2017 0.1342
3/27/2018 0.1984
3/27/2018 0.1992
3/27/2018 0.2227
3/27/2018 0.1953
Printed: 3/27/2018 6:55 AM f'(_ p Page 1 of ½ {-z,':f-/(8
I PFW LCL Mean UCL I I
p I 0.2190 0.2300 0.2410 I , i p I 0.2030 0.2119 0.2207 I I p I 0.1909 0.2008 0.2106 i
I I p I 0.2194 0.2295 0.2395
p 0.2011 0.2213 0.2415
p 0.1830 0.2043 0.2255
p 0.2216 0.2363 0.2509
p 0.2134 0.2249 0.2363
p 0.2009 0.2106 0.2204
p 0.0275 0.2231 0.4187
p 0.2342 0.2458 0.2573
p 0.2068 0.2189 0.2310
p 0.2102 0.2232 0.2361
p 0.2355 0.2520 0.2686
p 0.2398 0.2522 0.2646
p 0.1848 0.1955 0.2063
F 0.1959 0.2303 0.2648
F 0.1833 0.2089 0.2345
F 0.1855 0.2092 0.2330
F 0.2024 0.2394 0.2765
F 0.0488 0.1829 0.3169
F 0.0992 0.1799 0.2605
F 0.1667 0.2332 0.2997
f 0.1462 0.2100 0.2738
p 0.1919 0.2032 0.2145
p 0.1943 0.2057 0.2171
p 0.2171 0.2275 0.2379
p 0.1918 0.2017 0.2116
0329
Eberline Analytical Oak Ridge Laboratory
Detector
LB411CA - Al
LB411CA - A2
LB411CA - A3
LB411CA - A4
LB411CA - Bl
LB411CA - B2
LB411CA - B3
LB411CA - B4
LB4110A - Cl
LB4110A - C2
LB4110A - C3
LB4110A - C4
LB4110A - D1
LB4110A - D2
LB4110A - D3
LB4110A - D4
LB4110A - El
LB4110A - E2
LB4110A - E3
• LB4110A - E4
LB4110A - Fl
LB4110A - F2
LB4110A - F3
LB4110A - F4
LB4110A - Gl
LB4110!.\ - G2
LB411OA - G3
LB4110A - G4
Alpha/Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Calibration Date
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
10/20/2015
GPC Detector Report (ALL Efficiencies)
Count Date Eff
3/27/2018 0.5375
3/27/2018 0.4598
3/27/2018 0.4786
3/27/2018 0.5399
3/27/2018 0.5565
3/27/2018 0.5041
3/27/2018 0.5869
3/27/2018 0.5628
3/27/2018 0.4773
3/27/2018 0.5129
3/27/2018 0.6067
3/27/2018 0.5266
3/27/2018 0.6394
3/27/2018 0.6510
3/27/2018 0.6411
3/27/2018 0.5035
3/23/2018 0.0436
3/23/2018 0.0428
3/23/2018 0.0551
3/23/2018 0.0569
1/13/2017 0.2843
1/13/2017 0.2896
1/13/2017 0.5003
1/13/2017 0.4054
3/27/2018 0.4575
3/27/2018 0.4874
3/27/2018 0.5436
3/27/2018 0.4954
Printed: 3/27/2018 6:55 AM t(p Page 1 of1/2,t-/f@
PFW LCL Mean UCL
p i 0.5198 0.5428 0.5658
p 0.4456 0.4705 0.4955
p 0.4581 0.4782 0.4983
p 0.5311 0.5511 0.5712
p i 0.5052 0.5379 0.5705
p 0.4712 0.5049 0.5386
p 0.5560 0.5848 0.6136
p 0.5274 0.5520 0.5767
p 0.4647 0.4906 0.5166
p 0.5045 0.5275 0.5504
p 0.5821 0.6111 0.6400
p I 0.5063 0.5364 0.5664
p 0.6277 0.6527 0.6776
p 0.6169 0.6491 0.6812
p 0.6157 0.6407 0.6658
p 0.4640 0.5008 0.5377
F 0.4730 0.5519 0.6307
F 0.4450 0.5020 0.5591
F 0.4552 0.5070 0.5589
F 0.5130 0.5987 0.6844
F 0.2965 0.4651 0.6337
F 0.2942 0.4385 0.5828
w 0.4726 0.5889 0.7052
F 0.4095 0.5204 0.6312
p 0.4455 0.4650 0.4846
p 0.4732 0.4976 0.5219
p 0.5292 0.5539 0.5786
p 0.4706 0.4960 0.5214